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    GFREE RESEARCH PROJECT

    Everything you always wanted to know aboutPickett Plots*

    * BUT WERE AFRAID TO ASK

    Roberto Aguilera

    Schulich School of Engineering

    University of Calgary

    April 24, 2011

    Roberto Aguilera (2012)

    GFREE

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    OUTLINE

    GFREE RESEARCH PROJECT

    Pickett plots, basic equations

    Clean formations, shaly formations

    m, n and Sw

    k, rp35, Pc, h

    In the case of shale formations:

    Sw, TOC, LOM, viscous vs. diffusion-like flow Conclusions

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    BASIC EQUATIONS (1942)

    GFREE RESEARCH PROJECT

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    PICKETT PLOT (CLEAN FORMATIONS)

    GFREE RESEARCH PROJECT

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    PICKETT PLOT (CLEAN FORMATIONS)

    GFREE RESEARCH PROJECT

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    PICKETT PLOT (CLEAN FORMATIONS)

    GFREE RESEARCH PROJECT

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    CARBONATE EXAMPLE

    Integrate in a Pickett Plot:

    GFREE RESEARCH PROJECT

    Porosity and water saturationPermeability and process speed

    Capillary pressureHeight above free water tablePore throat aperture and particle size

    KozenisconstantRock fabric number (grainstones, packstones, wackstones)

    Range of initial flow rates

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    PROCESS or DELIVERY) SPEED

    GFREE RESEARCH PROJECT

    IS THE RATIO OF PERMEABILITY AND

    POROSITY (k / )AND IS RELATED

    DIRECTLY TO PORE THROATAPERTURE. IT PROVIDES A RELATIVE

    INDICATION OF HOW QUICKLY FLUIDS

    CAN MOVE THROUGH POROUS MEDIA(Chopra et al., 1987; Gunter et al., 1997)

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    PERMEABILITY

    GFREE RESEARCH PROJECT

    K1/2= 250 3/ Swi1AT IRREDUCIBLE

    CONDITIONS (MEDIUM

    GRAVITY OIL)(Source: Morris and Biggs)

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    PORE THROAT RADIUS (m)

    GFREE RESEARCH PROJECT

    r = 108.1 / PcHg-Air

    ASSUMING:

    INTERFACIAL TENSION:Hg-Air= 480 Dyne/cm

    AIR/MERCURY CONTACT ANGLE:

    Hg-Air= 140 Degrees

    (Aguilera, AAPG, 2004)

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    HEIGHT ABOVE

    FREE WATER TABLE h)

    GFREE RESEARCH PROJECT

    h (ft) 0.705 PcHg-Air

    ASSUMING A MEDIUM

    GRAVITY OIL RESERVOIR(Aguilera, AAPG, 2004)

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    HEIGHT ABOVE

    FREE WATER TABLE h)

    GFREE RESEARCH PROJECT

    h (ft) 0.405 PcHg-Air

    ASSUMING A DRY GAS OIL

    RESERVOIR(Aguilera, AAPG, 2004)

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    HEIGHT ABOVE

    FREE WATER TABLE h)

    GFREE RESEARCH PROJECT

    h (ft) 0.205 PcHg-Air

    ASSUMING A GEOTHERMAL

    RESERVOIR(Aguilera, AAPG, 2004)

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    CARMAN-KOZENY EQUATION

    GFREE RESEARCH PROJECT

    (k/) = 1014 [2

    /(1-)2

    ].[1/(Fst

    2

    Sgv2

    )]rmh= / [Sgv(1-)]

    (k/) = 1014 rmh2/ Fst

    2

    rmh rp35

    rp35= 2.665 (0.01k/)0.45Fst

    2= 114.14 (k/)-0.1

    Fst2= 89.543 rp35

    -0.2222

    Fs

    t2= Kozenysconstant

    Sgv2 = surface area per unit grain volume, microns

    rmh= mean hydraulic radius, microns

    rp35=pore throat aperture at 35% cumulative pore volume

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    ROCK FABRIC ()

    GFREE RESEARCH PROJECT

    (Aguilera, AAPG, 2004)

    Rock fabric () refers to the geologic

    description of particle size (dpin

    microns) and sorting (Lucia, 1983,1995). Pore size distribution is

    related to rock fabric and controls

    permeability and saturation.

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    Porosity and permeability relationship for

    various particle size groups in uniform

    cemented non-vuggy rocks (After Lucia, 1983)

    GFREE RESEARCH PROJECT

    (Aguilera, AAPG, 2004)

    Grainstone

    Packstone

    Wackstone

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    Lucias straight lines (1983) intersect at porosity of

    3.5% and permeability of 0.0015 md.

    GFREE RESEARCH PROJECT

    (Aguilera, AAPG, 2004)

    0.001

    0.01

    0.1

    1

    10

    100

    1000

    10000

    0.01 0.1 1

    INTERPARTICLE POROSITY (fraction)

    PERMEABIL

    ITY(md)

    =0.5 1.0 1.5 2.0 2.5 3.0

    4.0

    dp=500 m

    100 m 20 m

    1.8

    mGrainstone

    Packstone

    Wackstone

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    ROCK FABRIC ()

    GFREE RESEARCH PROJECT

    (Jennings and Lucia, 2002)

    = - 0.6213 ln (dp) + 4.3614

    k = e a( ) b( )

    a() = 22.5612.08 ln ()

    b() = 8.671 3.603 ln ()

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    PICKETT PLOT (MISSION CANYON CARBONATES)Little Knife field, North Dakota. Flow units after Martin et al. (1997)

    GFREE RESEARCH PROJECT

    (Aguilera, AAPG, 2004)

    0.01

    0.1

    1

    0.01 0.1 1 10 100

    RESISTIVITY, Ohm-m

    POROSI

    TY

    Sw=

    100% 90% 50% 30%

    10md

    1 md

    100 md

    1000 md

    k/

    =10000 md

    15%

    Pc=10 psi

    rp=10.8 m Pc=25 psi

    rp=4.32 m

    Pc=50 psi

    rp=2.16 m

    Pc=100 psi

    rp=1.08 m

    Pc=200 psi

    rp=0.54 m

    Pc=400 psi

    rp=0.27 m

    Pc=800 psi

    rp=0.14 m

    Pc=1600 psi

    rp=0.07 m

    46

    3

    2

    9

    107

    85

    1311

    15

    1412

    65%

    m=2.0

    n=2.0

    Pcand rpare valid between

    Sw=30% and 90%

    =0.5

    1.5=2.0

    =2.5

    =4.0

    =

    h=18'

    h=35'

    h=71'

    h=141'

    h=282'

    h=7'

    45.4

    57.2

    72.0

    91.5

    117.2

    Fst2

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    SHALY FORMATIONS

    GFREE RESEARCH PROJECT

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    PICKETT PLOT (SHALY FORMATIONS)

    GFREE RESEARCH PROJECT

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    SHALE GAS: log R Technique

    GFREE RESEARCH PROJECT

    Fine-grained, non-source rock

    Clast with a

    mean grain size

    of less than

    0.0625 mm

    includingsiltstone,

    mudstone,

    claystone and

    carbonates

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    PASSEY ET AL CURVES FOR Sw =100%

    from log R Technique

    GFREE RESEARCH PROJECT

    -1

    0

    1

    2

    3

    50 60 70 80 90 100 110 120 130 140 150

    L

    R

    m

    )

    t s/ft)

    Log R

    t

    ) vs t

    Shale

    Sandstone

    Limestone

    Dolomite

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    PICKETT PLOT USING PASSEY ET AL

    DATA FOR Sw =100%

    GFREE RESEARCH PROJECT

    1

    10

    100

    0.1 1 10 100

    m

    f

    R

    t

    m)

    t-tm

    ) vs R

    t

    Dolomite

    Shale

    Sandstone

    Limestone

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    PICKETT PLOT (HAYNESVILLE SHALE)

    Sw data from Ramirez et al. (2011)

    GFREE RESEARCH PROJECT

    0.01

    0.1

    1

    0.01 0.1 1 10 100

    R

    t

    m)

    vs R

    t

    25%

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    TOC on Pickett Plot

    TOC=total organic carbon

    LOM=level or organic metamorphism(Yu and Aguilera, 2011)

    GFREE RESEARCH PROJECT

    log= 0.02 0.02+ 0.02 + log, + 100.16882.297

    Bc= correction between density porosity and core crushed sample

    Rov= vitrinite reflectance, m= porosity exponent

    Baseline: The transit time and resistivity logs are scaled in such a way thattheir relative scaling is -50s/ft per logarithmic resistivity cycle.

    These two logs need to be overlain and baselined in a

    fine-grained, non-source rock.

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    Prediction of TOC and LOM

    with the Use of Pickett Plot

    (TOC and LOM Data from Passey et al., 1990)

    GFREE RESEARCH PROJECT

    0.01

    0.1

    1

    0.01 0.1 1 10 100

    Rt(m)

    vs Rt

    0%

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    GFREE RESEARCH PROJECT

    0.01

    0.1

    1

    0.01 0.1 1 10 100

    R

    t

    m)

    vs R

    t

    Kn = 0.01

    Kn = 0.1

    Kn = 0.001

    5%

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    Integrated Pickett Plot

    (TOC Data from Passey et al., 1990)

    GFREE RESEARCH PROJECT

    0.01

    0.1

    1

    0.01 0.1 1 10 100

    R

    t

    m)

    vs R

    t

    Log Data

    Log. (TOC=0%)

    Log. (TOC=5%)

    Log. (TOC=10%)

    Log. (TOC=15%)Power (Sw=100%)

    Power (Sw=50%)

    Power (Sw=25%)

    Power (Kn=0.1)

    Power (Kn=0.01)

    Power (Kn=0.001)

    5%

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    Conclusion (1)

    GFREE RESEARCH PROJECT

    Pickett plots are not a panacea but are useful

    for estimating:

    Porosity and water saturation

    Permeability and process speed

    Capillary pressure

    Height above free water table

    Pore throat aperture and particle size

    Kozenisconstant

    Rock fabric number (grainstones, packstones,wackstones)

    Range of initial flow rates

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    Conclusion (2)

    GFREE RESEARCH PROJECT

    Pickett plots are not a panacea but are useful

    for estimating:

    Porosity and water saturation

    Permeability and process speed

    Capillary pressure

    Height above free water table

    Pore throat aperture and particle size

    Kozenisconstant

    In carbonates: Rock fabric number (grainstones,packstones, wackstones)

    In shales: TOC, LOM, viscous vs. diffusion-like flow

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    Acknowledgement

    GFREE RESEARCH PROJECT

    Parts of this work were funded by

    ConocoPhillips, the Natural Sciences and

    Engineering Research Council of Canada(NSERC), and the Alberta Innovates

    Energy and Environmental Solutions

    (formerly AERI). Their contributions aregratefully acknowledged.

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    GFREE RESEARCH PROJECT

    Thank you