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Overview of Nanofabrication Techniques
Experimental Methods ClubMonday, July 7, 2014
Evan Miyazono
Outline
• Addition (deposition)• Subtraction (etching, milling)• Patterning
Deposition• figures of merit– uniform– conformal/edge coverage– deposition temperature– deposition material– lattice mismatch & / built in strain
Deposition
• Thermal evaporation• e-beam evaporation• Sputtering
Other deposition
• chemical vapor deposition (CVD)
• vapor liquid solid (VLS) method of nanowire growth
Deposition tricks
Etching
• figures of merit– isotropy/anisotropy– selectivity– redeposition?• check volatility/solubility of products
Dry Etching• reactive ion etching (RIE)• inductively coupled plasma (ICP)• sputtering– includes FIB Ga+ milling
• chemical assisted ion beam etching
ICP RIERIE FIB
CAIBE
Exotic Dry Etches
Burek et al., Nano. Lett. 2012, 12, 6084-6089
Angled ICP
Wet Etching
• often more selective & isotropic– some etch along crystal planes
• ion beam enhanced etching
KOH etching of silicon
He+
LiNbO/YSO
Patterning
• e-beam lithography• photolithography
• patterning a uniform layer– polymer used as etch mask
• patterning something hard to etch?– deposit on polymer and lift-off unwanted material
Beating patterning limitations
• cheating positive feature limits with sacrificial masks & conformal deposition
• cheating negative feature limits with built in stress and
Case Study: SOI
Silicon on insulator
Wafer bonding: plasma clean + heat + pressure
Dry etchDevelop resist
Strip resist
Spin coat photoresistHF undercut
Transfer to REI host
photoresist
My GaAs/YSO device Fabrication
AlGaAs
GaAs
GaAs
Strip photoresistapply e-beam resistDirect write
e-