Black Pot Beach Park Coastal Assessment

Black Pot Beach Park Coastal Assessment Hanalei, Kauai, Hawaii October 2016

Prepared for: Helber Hastert & Fee, Planners, Inc. 733 Bishop Street, Suite 2590 Pacific Guardian Center, Makai Tower Honolulu, Hawaii 96813 Prepared by: Sea Engineering, Inc. Makai Research Pier Waimanalo, HI 96795 Job No. 25525

Black Pot Beach Park Coastal Assessment Helber Hastert & Fee, Planners, Inc.

Sea Engineering, Inc. i

TABLE OF CONTENTS 1. INTRODUCTION ................................................................................................................. 3

1.1 PROJECT SITE LOCATION ................................................................................................... 3 1.2 BEACH PARK USE CHARACTERISTICS ............................................................................... 5

2. PROJECT SITE DESCRIPTION ........................................................................................ 6

2.1 SITE CHARACTERIZATION ................................................................................................. 6 2.2 NEARSHORE ENVIRONMENT .............................................................................................. 8 2.3 VEHICLE USE ASSESSMENT ............................................................................................. 10

3. COASTAL SETTING ......................................................................................................... 13

3.1 GENERAL DESCRIPTION .................................................................................................. 13 3.2 OCEANOGRAPHIC CONDITIONS ....................................................................................... 13

3.2.1 Wind ........................................................................................................................ 13 3.2.2 Waves ...................................................................................................................... 13 3.2.3 Still Water Levels and Nearshore Wave Heights .................................................... 15

3.3 SHORELINE PROCESSES ................................................................................................... 15

4. BEACH DYNAMICS .......................................................................................................... 16

4.1 HISTORICAL SHORELINE CHANGE ANALYSIS .................................................................. 19 4.2 FIELD INVESTIGATIONS ................................................................................................... 23

4.2.1 Site Visit 1 ............................................................................................................... 25 4.2.2 Site Visit 2 ............................................................................................................... 27 4.2.3 Site Visit 3 ............................................................................................................... 27

4.3 CHEMICAL ANALYSIS OF SAND AND WATER SAMPLES ................................................... 29 4.3.1 Impacts from Vehicles ............................................................................................. 31

4.4 GRAIN SIZE ANALYSIS OF SAND SAMPLES ...................................................................... 31 4.4.1 Impacts from Vehicles ............................................................................................. 32

5. CONCLUSION .................................................................................................................... 36

6. REFERENCES .................................................................................................................... 37

APPENDIX A: BLACK POT BEACH SOIL AND WATER SAMPLING REPORT ......... A

APPENDIX B: BLACK POT BEACH GRAIN SIZE ANALYSIS DATA SHEET ............... B


Sea Engineering, Inc. ii

LIST OF FIGURES

FIGURE 1-1 PROJECT SITE LOCATION ON THE ISLAND OF KAUAI (DIGITALGLOBE)........................................................ 3 FIGURE 1-2 PROJECT SITE WITHIN HANALEI BAY (DIGITALGLOBE) .............................................................................. 4 FIGURE 1-3 BLACK POT BEACH AND HANALEI PIER ..................................................................................................... 4 FIGURE 1-4 AMENITIES AND ACTIVITIES AT BLACK POT BEACH PARK .......................................................................... 5 FIGURE 2-1 FRINGING REEF EXTENDING 1,500 FEET OFFSHORE (UH COASTAL GEOLOGY GROUP) ............................... 7 FIGURE 2-2 NAUTICAL CHART 19385 – DEPTH IN FATHOMS (NOAA)............................................................................ 7 FIGURE 2-3 NOAA NEARSHORE GEOGRAPHY (PACIOOS) ............................................................................................ 9 FIGURE 2-4 NOAA NEARSHORE GEOMORPHOLOGY (PACIOOS) ................................................................................... 9 FIGURE 2-5 VEHICLE USE ON THE BEACH AT BLACK POT BEACH PARK ....................................................................... 10 FIGURE 2-6 VEHICLE USE PATTERNS AT BLACK POT BEACH PARK (GOOGLE EARTH) ................................................. 11 FIGURE 2-7 AERIAL PHOTOGRAPHS SHOWING VEHICLE PARKING AT BLACK POT BEACH PARK ................................... 12 FIGURE 3-1 HAWAII DOMINANT SWELL REGIMES (VITOUSEK AND FLETCHER, 2008) ................................................... 14 FIGURE 4-1 SHORELINE REACHES AND CORRESPONDING TRANSECTS ........................................................................... 17 FIGURE 4-2 REACH 1 (TRANSECT 229-233) EXTENDING 300 FEET SOUTH OF HANALEI PIER ........................................ 17 FIGURE 4-3 REACH 2 (TRANSECTS 234-238) EXTENDING 300 FEET NORTH OF HANALEI PIER...................................... 18 FIGURE 4-4 REACH 3 (TRANSECTS 239-243) EXTENDING 300 FEET TO THE HANALEI RIVER MOUTH ........................... 18 FIGURE 4-5 CGG HISTORICAL SHORELINE CHANGE RATES FOR BLACK POT BEACH PARK (1930-2008) ...................... 19 FIGURE 4-6 MAXIMUM EROSION (1962) AND ACCRETION (1975) AT BLACK POT BEACH PARK ................................... 20 FIGURE 4-7 SEI HISTORICAL SHORELINE CHANGE RATES FOR BLACK POT BEACH PARK (1968-2016)......................... 21 FIGURE 4-8 AERIAL PHOTOGRAPHS SHOWING MIGRATION OF THE SAND SPIT (1987-2013) .......................................... 22 FIGURE 4-9 VARIABILITY OF THE SAND SPIT AT THE HANALEI RIVER MOUTH (MAY TO JULY 2016) ............................ 23 FIGURE 4-10 VARIABILITY OF THE SAND SPIT AT THE HANALEI RIVER MOUTH (JULY TO AUGUST 2016) .................... 23 FIGURE 4-11 STREAM GAGE HEIGHTS FOR THE HANALEI RIVER (MAY TO AUGUST 2016) ........................................... 24 FIGURE 4-12 STREAM DISCHARGE FOR THE HANALEI RIVER (MAY TO AUGUST 2016) ................................................ 24 FIGURE 4-13 LOCATION OF DECISION UNITS (DU) FOR SAND AND RIVER WATER SAMPLE COLLECTION ...................... 26 FIGURE 4-14 SURFACE RUNOFF ENTERING THE OCEAN ADJACENT TO HANALEI PIER (MAY 24, 2016) ......................... 26 FIGURE 4-15 VARIABILITY OF THE BEACH TOE FROM MAY TO AUGUST, 2016 ............................................................. 28 FIGURE 4-16 GRAIN SIZE ANALYSIS FOR EACH DECISION UNIT (LOG SCALE BASE 10 FOR X-AXIS) ................................ 33 FIGURE 4-17 GRAIN SIZE ANALYSIS FOCUSED ON THE SILT SIZED FRACTIONS .............................................................. 34 FIGURE 4-18 COMPACTED BERM ALONG THE EDGE OF THE ESTABLISHED VEHICLE ACCESS ROUTE .............................. 35


Sea Engineering, Inc. 3

1. INTRODUCTION Sea Engineering, Inc. (SEI) prepared this coastal assessment for Black Pot Beach Park to assess coastal dynamics along the shoreline and identify potential impacts resulting from the use of automotive vehicles on the beach. The project site is located at the northeast end of Weke Road in Hanalei, Kauai, Hawaii; Tax Map Key (4) 5-5-001:004 & 011. The study area includes the beach seaward of parcels (4) 5-5-001:008, 012, 013, and 014. The project site consists of Black Pot Beach Park and the beach extending from the Hanalei River mouth to a point approximately 300 feet south of the Hanalei Pier. SEI was contracted to assess coastal processes and sediment characteristics in the project area. Grain size and chemical analyses were conducted in order to assess sand characteristics and identify potential contaminants. This assessment provides a discussion of the coastal setting, shoreline processes, historical shoreline change, beach sand characteristics, and potential impacts resulting from the use of vehicles on the beach.

1.1 Project Site Location The project site is located on the north shore of the island of Kauai (Figure 1-1), within Hanalei bay, at the northeast end of Hanalei Beach (Figure 1-2). The project site includes the southern bank of the Hanalei River at the river mouth, and the sandy beach extending south from the Hanalei River to Hanalei Pier.

Figure 1-1 Project site location on the Island of Kauai (DigitalGlobe)

Kauai

PROJECT SITE



Figure 1-2 Project site within Hanalei Bay (DigitalGlobe)

Figure 1-3 Black Pot Beach and Hanalei Pier

Hanalei Bay

Hanalei

PROJECT SITE

Black Pot Beach Park

Hanalei Pier

Hanalei River Mouth Hanalei Bay



1.2 Beach Park Use Characteristics Hanalei Bay and surrounding areas are subject to extensive coastal use. Black Pot Beach Park is a convenient and well used launching point for coastal, marine, and river activities. Coastal uses include, but are not limited to, the following: surfing, swimming, fishing, spear fishing, walking, sunbathing, kayaking and canoeing, stand up paddling, parking, and sightseeing. River uses include paddling, boating, and sightseeing. Black Pot Beach Park is owned and managed by the County of Kauai Department of Parks and Recreation. The park is approximately 5.5 acres and consists of a grassy inshore area with approximately 500 feet of sandy beach along the shoreline (Figure 1-3). Park amenities include picnic tables, a comfort station, and an outdoor shower. The park is used as a water entry point for paddlers, surfers, swimmers, and boaters. Typical park uses include picnicking, sunbathing, beach access, pier access, and ocean access (Figure 1-4). The park is also a destination for visiting tourists due to the excellent views of Hanalei Bay and convenient access to Hanalei Pier. A small parking lot with an estimated capacity of 30 vehicles is located on the landward side of the lawn. Additional parking is available along the south side of the comfort station, which can accommodate an additional 20 vehicles. Overflow parking on the sandy beach seaward of the park has been a common practice for the past several decades. During high use periods, it is common for up to several hundred vehicles to occupy the parking lot areas and the beach.

Figure 1-4 Amenities and activities at Black Pot Beach Park

1. Canoe and kayak launch 2. Boat launch 3. Ocean access 4. Beach parking 5. Shore fishing 6. Hanalei Pier 7. Canoe access 8. Picnic and camping area 9. Bathroom and shower 10. Parking lot

Black Pot Beach Park

Hanalei Bay

Hanalei River



2. PROJECT SITE DESCRIPTION 2.1 Site Characterization The project site is located on the north end of the sandy coastal plain inshore of Hanalei Bay, south of the Hanalei River, on the north coast of Kauai. The embayed shoreline is along the low-lying beach, with broad shallow fringing reefs extending offshore along the northeast and southwest sides of the bay. This region is moderately developed along the coastline with residential development on the coastal plain. The neighboring property to the north, across the Hanalei River, is an elevated basalt ridge line. The southern neighbors are residential lots, some of which are undeveloped, and to mauka are open lots with mixed uses. This west-facing shoreline is near the southern edge of the shallow fringing reef on the northeast side of the bay. The reef is approximately 1,500 feet wide, makai of the mouth of the Hanalei River; however, the reef ends just north of the Hanalei Pier (Figure 2-1). The center of the bay’s seafloor is dominantly sandy substrate that gradually slopes to deeper depths from the beach to the mouth of the bay. LiDAR data and nautical charts (Figure 2-2) show that depths measured over the reef are typically less than 1 fathom (6 feet), and generally range from 2 to 4 feet below water, and depths in the sandy middle of the bay increase from 6 feet just off the shoreline to approximately 40 feet in depth by the center of the bay. The dominant wave regimes are the northeast tradewinds in the summer and north swell in the winter. The shallow reef dissipates a high percentage of the offshore wave energy through broken waves, while the sandy seafloor allows larger waves to reach the middle of the bay, where they break on nearshore sandbars. The waves over both the reef and sandbars are depth limited, meaning that the maximum wave height is a function of water depth. More wave energy can impact the shoreline where water levels are deeper near shore. The beach park is located on a sandy coastal plain, with low elevations, minimal dune development, and dynamic, sandy margins on the seaward and riverside edges. The sandy coastal plain is also part of the Hanalei River flood plain and is a mixture of both fluvial and marine sediment. The beach is predominantly carbonate sand of marine origin, deposited and transported through marine and coastal processes. The river bank is composed of sandy fluvial deposits mixed with marine sediment, abutting the coastal plain. There is a dynamic, ephemeral sand spit that exists at the north end of the beach, extending into the river mouth. The spit is composed primarily of marine carbonate sand. Spit volume and shape are affected by marine waves, littoral currents, and fluvial flow, resulting in changes that are both more frequent and higher magnitude than nearby shorelines.



Figure 2-1 Fringing reef extending 1,500 feet offshore (UH Coastal Geology Group)

Figure 2-2 Nautical chart 19385 – depth in fathoms (NOAA)



2.2 Nearshore Environment The wide fringing reef extends approximately 1,500 feet from the shoreline to the shallow reef crest as shown in Figure 2-1. The reef structure is incised by several small channels that are filled with sand and rubble. This carbonate structure’s southern edge is offshore of the southern side of Black Pot Beach park. The sandy seafloor in the middle of Hanalei Bay is a gentle slope of unconsolidated marine sediment extending from the beach toe to the well outside the mouth of the bay. The Pacific Island Ocean Observing System’s (PacIOOS) Voyager web-based mapping program displays the National Oceanographic and Atmospheric Administration’s (NOAA) benthic habitat maps. These maps show the geomorphology and geography of benthic habitat for the project area. The offshore area of the project site (shown in red) is characterized by expansive reef structure incised by narrow channels on the north side and a sandy bank in the middle of the bay. Figure 2-3 shows the area covered by river bed on the north side, reef with a large channel directly offshore of the project site, and a sand bank offshore and south of the project site. Figure 2-4 identifies the type of material in the river bed, the reef on the north side of the bay, and the sand bank in the center of the bay. The river bed is identified as mud substrate. The majority of the carbonate reef structure is pavement, with portions identified as aggregate reef, and the small channel on the south edge called out as a reef rubble filled depression. South of the reef’s edge is the bank, comprised almost entirely of marine sediment.



Figure 2-3 NOAA nearshore geography (PacIOOS)

Figure 2-4 NOAA nearshore geomorphology (PacIOOS)



2.3 Vehicle Use Assessment Vehicular use on the beach at Black Pot Beach Park has been ongoing for nearly half a century. The property was privately owned from 1967 to 1973, during which time it was closed to the public. The property was purchased by the County of Kauai and reopened to the public in July 1973 (Clark 1990). Based on a review of historical aerial photographs, it appears that vehicles began accessing the beach in the early 1970’s, which correlates with the establishment of Black Pot Beach Park. Vehicle access and parking are primarily limited to the area north of Hanalei Pier (Figure 2-5). Vehicle traffic does occur, but is less frequent, on the sand spit at the Hanalei river mouth, presumably due to the unconsolidated nature of the sand in this area. However, this area is used daily for boat launching purposes. Parking occurs in two rows (one on the upper beach, one on the lower beach) separated by an established vehicle access route. Vehicular use on the beach occurs daily but is likely greatest on weekends and holidays.

Figure 2-5 Vehicle use on the beach at Black Pot Beach Park

Vehicle estimates were calculated based on a review of 22 historical aerial photos ranging from 1950-2014, and field observations on three separate dates in May, July, and August 2016. Estimates were rounded up by 10% to account for tree cover that obscures the presence of vehicles along the upper beach, which is typically occupied by parked vehicles. The estimated number of vehicles identified in the historical aerial photographs is shown in Table 2-1.



Average Vehicles

Average Area Occupied

Maximum Vehicles

Maximum Area Occupied

Percent Increase

1950-1968 0 0 0 0 N/A

1975-1997 30 6,000 square feet (12% of available area) 48 9,600 square feet

(19% of available area) N/A


(33% of available area) 83%


(51% of available area) 36%

Table 2-1 Summary of vehicle use estimates for Black Pot Beach Park

The number of vehicles present on the beach reduces the amount of beach area available for public access and recreational uses, which has the potential to impact the accessibility and usability of the beach. The area north of Hanalei Pier, which experiences the greatest volume of vehicular traffic and parking, is approximately 500 feet long x 100 feet wide (50,000 square feet) (Figure 2-6). The established vehicular access route located between the two parking rows is approximately 10,000 square feet, which represents 20% of the available beach area. The average space occupied by a single vehicle is 200 square feet (FWHA). Based on these dimensions, it is estimated that the area north of Hanalei Pier can accommodate a maximum of 100 vehicles at any given time.

Figure 2-6 Vehicle use patterns at Black Pot Beach Park (Google Earth)

Beach parking – seaward row (20,000 sq.ft.) Established vehicle access route (10,000 sq.ft.) Beach parking – landward row (20,000 sq.ft.)



A review of historical aerial photographs indicates that vehicle use has continued to increase over time and that vehicle parking occupies a significant portion of the available beach space north of Hanalei Pier. The number of vehicles that access or park on the beach varies on a daily basis. A review of recent aerial photographs from 2012 to 2016, found that the average number of vehicles present on the beach was 75, which occupies approximately 15,000 square feet (26%) of the available beach area (Figure 2-7). The maximum number of vehicles present on the beach was 125, which occupies approximately 25,000 square feet (50%) of the available beach area. Based on these estimates, approximately 70% of the available beach area can be occupied by vehicles (50%) and the established access route (20%) during periods of heavy use.

Figure 2-7 Aerial photographs showing vehicle parking at Black Pot Beach Park



3. COASTAL SETTING 3.1 General Description The project site is located on a low-lying coastal plain, adjacent to the Hanalei River, at the north end of beach within Hanalei Bay. This area is exposed to large winter surf, refracted tradewind wind waves, coastal storms, tsunamis, and river flooding.

3.2 Oceanographic Conditions 3.2.1 Wind The prevailing winds from the northeast, tradewinds, blow along the coastline of the project area. The tradewinds are typically present 80 percent of the time during the summer season from April to November, with wind speeds of 10 to 20 mph. During the winter months there is a general weakening of the tradewind system and the occurrence of southerly and westerly winds (Kona winds) due to both frontal systems passing through the islands and local low-pressure systems. 3.2.2 Waves The wave climate in Hawaii is typically characterized by four general wave types. These include northeast tradewind waves, southern swell, North Pacific swell, and Kona wind waves. Tropical storms and hurricanes also generate waves that can approach the islands from virtually any direction. Unlike winds, any and all of these wave conditions may occur at the same time. The dominant swell regimes for Hawaii are shown in Figure 3-1. Tradewind waves occur throughout the year and are the most persistent April through September when they usually dominate the local wave climate. They result from the strong and steady tradewinds blowing from the northeast quadrant over long fetches of open ocean. Tradewind deepwater waves are typically between 3 to 8 feet high with periods of 5 to 10 seconds, depending upon the strength of the tradewinds and how far the fetch extends east of the Hawaiian Islands. The direction of approach, like the tradewinds themselves, varies between north-northeast and east-southeast and is centered on the east-northeast direction. The reef offshore of the project site is directly exposed to both tradewind waves and North Pacific swell. Southern swell is generated by storms in the southern hemisphere and is most prevalent during the summer months of April through September. Traveling distances of up to 5,000 miles, these waves arrive with relatively low deepwater wave heights of 1 to 4 feet and periods of 14 to 20 seconds. Depending on the positions and tracks of the southern hemisphere storms, southern swells approach between the southeasterly and southwesterly directions. The project site is sheltered from southern swell.



Figure 3-1 Hawaii dominant swell regimes (Vitousek and Fletcher, 2008)

During the winter months in the northern hemisphere, strong storms are frequent in the North Pacific in the mid latitudes and near the Aleutian Islands. These storms generate large North Pacific swells that range in direction from west-northwest to northeast and arrive at the northern Hawaiian shores with little attenuation of wave energy. These are the waves that have made surfing beaches on the north shores of the Hawaiian Islands famous. Deepwater wave heights often reach 15 feet and in extreme cases can reach 30 feet. Periods vary between 12 and 20 seconds, depending on the location and track of the storm. The reef offshore of the project site is exposed to swell approach from the west-northwest through the north. Kona storm waves do not directly approach the project site; however, these waves are fairly infrequent, occurring only about 10 percent of the time during a typical year. Kona waves typically range in period from 6 to 10 seconds with heights of 5 to 10 feet, and approach from the southwest. Deepwater wave heights during the severe Kona storm of January 1980 were about 17 feet. These waves had a significant impact on the south and west shores of the islands. Severe tropical storms and hurricanes obviously have the potential to generate extremely large waves, which in turn could potentially result in large waves at the project site. Recent hurricanes impacting the Hawaiian Islands include Hurricane Iwa in 1982, Hurricane Iniki in 1992, Hurricane Iselle in 2014, and Hurricane Darby in 2016. Iwa passed on the west side of Kauai, inflicting severe property damage to the island. Iniki directly hit the island of Kauai and resulted in large waves along the southern shores of all the Hawaiian Islands. Damage on Kauai from these two hurricanes was extensive.



3.2.3 Still Water Levels and Nearshore Wave Heights During high wave conditions, the nearshore water level may be elevated above the tide level by the action of breaking waves. This water level rise, termed wave setup, could be as much as 1 to 2 feet during severe storm wave conditions. During hurricane conditions, an additional water level rise due to wind stress and reduced atmospheric pressure can occur. Collectively termed “storm surge,” this can potentially add another 1 to 2 feet to the stillwater level. For example, during the 1992 passage of Hurricane Iniki over Port Allen Harbor on the island of Kauai, a National Weather Service tide gauge recorded a water level rise of 4.4 feet above the predicted tide elevation. During storm or large wave conditions, there may be multiple zones of wave breaking. Wave heights are said to be depth-limited because once the water depth becomes shallow enough the wave breaks, losing size and energy. The wave, however, may reform before it reaches the shoreline and break again when the depth-limited ratio is again attained. The still water level rise during storm events is an important consideration because it allows larger wave heights to reach the shoreline than during lower water levels. Still water level rise at the shoreline is a combination of astronomical tide, storm surge, and wave setup. Wave setup is a function of the breaking wave height, period, and bottom topography. The mass transport of water due to breaking waves produces wave setup—the increase in water depth shoreward of the breaker zone.

3.3 Shoreline Processes Shoreline processes at the project site are a result of combined marine and fluvial influences. The beach face at the north end, connected to the sandy spit on the southern side of the Hanalei River mouth, is affected by both seasonal variations in the wave environment and flow characteristics of the Hanalei River. The spit migrates on a physical scale that is considerably larger than the adjacent beach face dynamics. The beach face between the south side of the spit and the north side of the pier is also affected by the large changes on the spit. Moving south along the coastline, the beach face south of the pier responds as part of the larger beach system extending along the inner shoreline of Hanalei Bay. Nearshore and coastal sand are moved along the larger beach’s shoreline by the attenuated wave energy and nearshore currents. Beach face morphology is related to inclement wave energy, creating pronounced sand bars during high wave events and recovering in quieter and calmer conditions. During recent history, the broader embayment’s shoreline has suffered from mild chronic erosion. The mobile sand bank of the Hanalei River contains a high fraction of marine sands and is occasionally washed by waves coming past the river mouth; however, the dominant control on the sand bank is the river system. Bank dynamics along the park are typically less dynamic than the beach face morphology changes. The bank is partially stabilized by vegetation, with root structure providing some consolidation to the upper stream bank.



4. BEACH DYNAMICS Black Pot Beach Park is located at the northeastern end of Hanalei Bay where the beach terminates at the Hanalei River mouth. The property is bordered by residential properties to the south, Weke Road to the east, Hanalei River to the north, and Hanalei Bay and the Pacific Ocean to the west. Hanalei Bay is a horseshoe-shaped embayment with a crescent-shaped beach along the shoreline that is approximately 3 km long. The nearshore geology is characterized by a wide fringing limestone reef that extends over 1,500 feet offshore. The fringing reef is incised with channels or depressions at numerous locations. Black Pot Beach Park consists of approximately 5.5 acres with a total shoreline frontage of approximately 500 feet. The surficial geology is classified as quaternary beach deposits, and the local soils consist primarily of beach sand and Mokuleia fine sandy loam. Shoreline processes at the project site are driven by a combination of marine and fluvial processes. The beach is composed of carbonate sand mixed with terrigenous sediments discharged from the Hanalei River. The beach sand is very fine-to-fine with grain sizes ranging from 0.075 mm to 0.250 mm. For the purposes of this study, the shoreline was divided into three (3) reaches (Figure 4-1). Reach 1 (Transects 229-233) is located along the southern portion of the shoreline and extends 300 feet south of Hanalei Pier. The backshore consists of a stable upper berm with well-established vegetation (Naupaka). The foreshore is gently-sloping with a transient lower berm, a moderately-steep lower beach face, and an abrupt, well-defined beach toe. A ground photo showing the location of Reach 1 is shown in Figure 4-2. Reach 2 (Transects 234-238) is located along the central portion of the shoreline and extends 300 north. The backshore consists of a stable upper berm with well-established vegetation (Seashore Paspalum). The foreshore is gently-sloping with a compacted lower berm along the edge of the established vehicle access route, a moderately-steep lower beach face, and a well-defined beach toe. The beach toe becomes progressively less well-defined along the northern end of Reach 2 (Transects 238-239). A ground photo showing the location of Reach 2 is shown in Figure 4-3. Reach 3 (Transects 239-243) is located along the northern portion of the shoreline and includes the ephemeral sand spit located at the Hanalei River mouth. The backshore consists of a stable upper berm with well-established vegetation (Seashore Paspalum). The foreshore consists of an ephemeral sand spit with a mounded shape. The transient lower berm is slightly elevated and arcs landward toward the river mouth. The slope of the lower beach face becomes progressively lower toward the river mouth as the sand spit progrades onto the reef flat. The beach toe is poorly-defined along the seaward side of the sand spit, but well-defined along the landward side. A ground photo showing the location of Reach 3 is shown in Figure 4-4.



Figure 4-1 Shoreline reaches and corresponding transects

Figure 4-2 Reach 1 (Transect 229-233) extending 300 feet south of Hanalei Pier

Reach 1



Figure 4-3 Reach 2 (Transects 234-238) extending 300 feet north of Hanalei Pier

Figure 4-4 Reach 3 (Transects 239-243) extending 300 feet to the Hanalei River mouth

Reach 2

Reach 3



4.1 Historical Shoreline Change Analysis A series of historical aerial photographs can be used to determine long-term shoreline trends. The University of Hawaii Coastal Geology Group (CGG) has undertaken historical analysis of Kauai’s shoreline and has produced a shoreline change map for the Hanalei region based on survey data and aerial imagery from 1930 to 2008. Their analyses use the beach toe as the reference feature for measuring shoreline change. The analyses for the project site shoreline are presented as Transects 229 through 241 (Figure 4-5). The CGG study indicates that there is an average, smoothed, long-term trend of erosion (-0.4 feet/year) for the entire project site (Transects 229-241). The CGG study indicates a long-term trend of accretion (+0.25 feet/year) along the southern portion of the shoreline (Reach 1, Transects 229-233), a long-term trend of erosion (-0.64 feet/year) along the central portion of the shoreline (Reach 2, Transects 234-238), and a long-term trend of erosion (-1.10 feet/year) along the northern portion of the shoreline (Reach 3, Transects 239-241). CGG reports average annual accretion rates as high as +0.4 feet/year at Transect 229 along the southern portion of the shoreline, transitioning from long-term accretion to long-term erosion between Transects 232 and 233. Average annual long-term erosion rates increase to -1.3 feet/year at Transect 239 along the northern portion of the shoreline, where fluvial processes become more dominant. Though these rates are representative of the average, smoothed, long-term trends for the project site from 1930 to 2008, they are not indicative of the conditions that have been persistent in the region for the previous three decades.

Figure 4-5 CGG historical shoreline change rates for Black Pot Beach Park (1930-2008)



Sandy shorelines in general are very dynamic and are subject to rapid change in response to incident wave conditions, such as high surf, which can quickly alter the beach width. The shoreline at Black Pot Beach Park is subject to dramatic short-term fluctuations in beach width caused by flooding of the Hanalei River. The CGG analysis was updated for this study by surveying the 2016 shoreline position. To be consistent with the CGG shorelines, the 2016 shoreline was determined by surveying the location of the beach toe, which was located using a Trimble Geo7X handheld system that utilizes global positioning satellites (GPS) with a positional accuracy of approximately 0.5 meter. The project site corresponds to Transects 229 through 241 from the CGG study, whose locations are replicated in the SEI study. To show specific shoreline trends within the long-term record, SEI performed shoreline change analyses using the shoreline positions from 1988 to 2016. There were extreme erosion and accretion events, in 1962 and 1975, respectively, that are not representative of the trend that has been consistent since the 1988 shoreline (Figure 4-6). The SEI study did not include the two events, as they confound the erosion study events and are not indicative of the current state of the beach.

Figure 4-6 Maximum erosion (1962) and accretion (1975) at Black Pot Beach Park



As opposed to the CGG analyses, which employed smoothing techniques and provides a best fit for a long-term trend, the SEI analyses are considered “endpoint” analyses, in which only the change between the first and last shorelines in the analysis period is considered. This is useful in showing sub-trends within the entire data series. The sub-trends in this case are for the time period showing the most recent long-term trend (1988-2016). Note that the CGG analysis does not include Transects 242 and 243. These transects were added in order to analyze the dynamics of the ephemeral sand spit at the Hanalei River mouth but were not included in the endpoint rate calculations. The results of the SEI endpoint analysis are shown in Figure 4-7, which shows the average rate of shoreline change from 1988 to 2016. The study indicates that, from 1988 to 2016, the project site shoreline eroded at an average rate of approximately -1.34 feet/year. The southern portion of the shoreline (Transects 229-233) eroded at an average rate of approximately -1.77 feet/year, the central portion of the shoreline (Transects 234-238) eroded at an average rate of approximately -2.15 feet/year, and the northern portion of the shoreline (Transects 239-241) accreted at an average rate of approximately +2.39 feet/year.

Figure 4-7 SEI historical shoreline change rates for Black Pot Beach Park (1968-2016)

SEI found average erosion rates as high as -3.01 feet/year along the southern portion of the shoreline (Transect 235), transitioning from long-term erosion to long-term accretion between Transects 239 and 241, with a maximum long-term accretion rate of +1.59 feet/year at Transect 241 along the northern portion of the shoreline where fluvial processes become more dominant. The ephemeral sand spit located at the Hanalei River mouth is a complex morphologic feature that is highly dynamic and mobile. The morphology of the sand spit is influenced by a combination of wind, wave transformation, tidal variation, longshore currents, availability of sediment, and river discharge. The sand spit was present in approximately 75% of the aerial photographs from 1950 to 2016. This portion of the shoreline experiences extreme fluctuations in sediment volume and exhibits dramatic seasonal and intraseasonal variability. The variability of the sand spit is evident in the aerial photographs shown in Figure 4-8.



Figure 4-8 Aerial photographs showing migration of the sand spit (1987-2013)

The shape and volume of the sand spit can change rapidly and is likely influenced by fluvial discharge from the Hanalei River. The sand spit corresponds with Transects 239-243, which are located in Reach 3 along the northern portion of the project site shoreline. SEI conducted an endpoint analysis for Reach 3 for the period of May through August 2016 in order to analyze the intraseasonal dynamics of the sand spit. The results of the endpoint analysis are shown in Figure 4-9 and Figure 4-10. the 41-day period from May 24 to July 5, the sand spit eroded an average of -101.4 feet with maximum erosion of -138.9 feet at Transect 243 (Figure 4-9). For the 26-day period from July 5 through August 1, the sand spit accreted an average of +145.9 with maximum accretion of +202.5 feet at Transect 242 (Figure 4-10). These results clearly demonstrate the extreme variability of the sand spit and the dramatic changes that can occur within very short time periods. These results also indicate that beach stability decreases significantly north of Transect 239 within the vicinity of the Hanalei River mouth.



Figure 4-9 Variability of the sand spit at the Hanalei River mouth (May to July 2016)

Figure 4-10 Variability of the sand spit at the Hanalei River mouth (July to August 2016)

4.2 Field Investigations SEI and Elemental Environmental (E2) conducted a series of three site visits in order to assess the condition of the shoreline, survey the location of physical features, observe short-term fluctuations in beach width, and collect sand and river water samples. Composite sand samples consisted of 30 aliquots grab samples collected from 4 to 6 inches below the surface. Water samples were collected from the center of the Hanalei River. These samples were collected in order to conduct chemical and grain size analyses to identify potential impacts of vehicular use on the beach. The site visits were conducted on May 24, July 5, and August 1, 2016. These dates were selected in order to observe the shoreline following periods of high-use. Hanalei has had an average rainfall of 77.8 inches over the last 30 years, which is 15.03 inches more than the average in Hawaii. The region frequently experiences flash flooding that often generates flooding in the coastal zone. Three decades of stream gauge data show that the Hanalei River overflowed its banks at the Hanalei Bridge 29 out of 32 years (Fletcher et. al. 2008). All of the site visits were conducted during periods of heavy rainfall that resulted in surface runoff and elevated water levels in the Hanalei River. Stream gage heights and discharge volumes for the Hanalei River from May to August 2016 are shown Figure 4-11 and Figure 4-12.



Figure 4-11 Stream gage heights for the Hanalei River (May to August 2016)

Figure 4-12 Stream discharge for the Hanalei River (May to August 2016)



4.2.1 Site Visit 1 The first site visit was conducted on May 24, 2016, following the Memorial Day holiday weekend. Weather was mostly cloudy with variable winds and intermittent showers. Very heavy showers were sustained from 1:00pm to 3:30pm. Daily precipitation was 0.34 inches, and the maximum stream gage height for the Hanalei River was 4.74 feet. Low tide was +0.17 feet at 10:12am, and high tide was +2.29 feet at 6:06pm. Wave energy was very low with wave heights of 0-1 feet offshore, and 0-1 feet at the waterline. This was the first of three sampling events and provided the baseline event for future data comparison. Six Decision Units (DU) were established. DU-1 was a control site located along the shoreline north of the Hanalei River mouth. DU-2A and DU-2B were located in Reach 1, south of Hanalei Pier where there is no vehicular use. DU-3 and DU-4 were located in Reach 2, north of Hanalei Pier where vehicular use is the highest. DU-5 was the water sample site located in the center of the Hanalei River. DU-6 was located in Reach 3 and included the ephemeral sand spit at the Hanalei River mouth where vehicular use is moderate. The locations of the DU’s are shown in Figure 4-13. A composite sand sample consisting of 30 aliquot grab samples was collected for each DU. The composite sample for DU-3, where vehicular use is the highest, was a triplicate sample consisting of 90 aliquot grab samples. Sustained heavy rainfall resulted in run-off from the parking lot area entering the ocean adjacent to Hanalei Pier (Figure 4-14). A sample of the runoff water was collected and tested for contaminants. A Trimble Geo7X handheld GPS unit was used to collect location data for physical features including the top bank, edge of vegetation, and beach toe. Reach 1 exhibited a typical profile with a stable upper berm, transient lower berm, and a well-defined beach toe. Reach 2 consisted of a stable upper berm, a compacted lower berm along the seaward edge of the established vehicle access route, and a well-defined beach toe. Reach 3 was substantially prograded with the ephemeral sand spit extending approximately 350 feet seaward of the vegetation line. Approximately 20 vehicles were observed in Reach 2 and Reach 3.



Figure 4-13 Location of Decision Units (DU) for sand and river water sample collection

Figure 4-14 Surface runoff entering the ocean adjacent to Hanalei Pier (May 24, 2016)

Surface Runoff Surface Runoff



4.2.2 Site Visit 2 The second site visit was conducted on July 5, 2016, following the Independence Day holiday weekend. Weather was partly cloudy with moderate tradewinds and intermittent heavy showers. Daily precipitation was 3.21 inches, and the maximum stream gage height for the Hanalei River was 5.25 feet. Low tide was +0.17 feet at 10:00am, and high tide was +2.71 feet at 4:42pm. Wave energy was very low with wave heights of 0-1 feet offshore, and 0-1 feet at the waterline. This was the second of three sampling events. A composite sand sample consisting of 30 aliquot grab samples was collected for each DU. The composite sample for DU-3, where vehicular use is the highest, was a triplicate sample consisting of 90 aliquot grab samples. Sustained heavy rainfall resulted in run-off from the parking lot area entering the ocean adjacent to Hanalei Pier. Samples of the runoff water were not collected. Reach 1 remained stable with some minor erosion observed along Transects 230-231. Reach 2 remained stable across Transects 234-237 and transitioned to erosion at Transect 238. The erosion continued through Transects 239-243 as the entire length of Reach 3 was erosive. The sand spit was present but less prograded onto the reef flat. Approximately 20 vehicles were observed in Reach 2 and Reach 3. 4.2.3 Site Visit 3 The third site visit was conducted on August 1, 2016, following the last weekend of Summer Break for the Hawaii State Department of Education school system. Weather was partly cloudy with light tradewinds and intermittent heavy showers. Daily precipitation was 0.83 inches, and the maximum stream gage height for the Hanalei River was 5.33 feet. Low tide was +0.10 feet at 8:06am, and high tide was +2.76 feet at 3:18pm. Wave energy was very low with wave heights of 0-1 feet offshore, and 0-1 feet at the waterline. This was the last of three sampling events. A composite sand sample consisting of 30 aliquot grab samples was collected for each DU. The composite sample for DU-3, where vehicular use is the highest, was a triplicate sample consisting of 90 aliquot grab samples. Sustained heavy rainfall again caused run-off from the parking lot area to enter the ocean adjacent to Hanalei Pier. Reach 1 remained stable with some minor erosion observed along Transects 230-231. The southern portion of Reach 2 (Transects 234-235) was relatively stable but transitioned to erosion along the northern portion (Transects 236-238). The erosion continued through Transects 239-243 as the entire length of Reach 3 was erosive. The sand spit was present and a prograded shoal extended onto the reef flat. Approximately 60 vehicles were observed in Reach 2 and Reach 3. Field observations from May to August 2016 confirmed that beach width along the project site shoreline is intraseasonally variable. During the 41-day period from May 24 to July 5, Reach 1 (Transects 229-233) eroded -4.79 feet, Reach 2 (Transects 234-238) accreted +0.29 feet, and Reach 3 (Transects 239-243) eroded -76.4 feet. During the 26-day period from July 5 to August 1, Reach 1 (Transects 229-233) eroded -2.11 feet, Reach 2 (Transects 234-238) eroded -11.9 feet, and Reach 3 (Transects 239-243) accreted +80.8 feet. In general, based on these observations, Reach 1 is considered moderately stable, Reach 2 is considered moderately unstable, and Reach 3 is considered extremely unstable. The variability of the location of the beach toe from May to August 2016 is shown in Figure 4-15.



Figure 4-15 Variability of the beach toe from May to August, 2016



4.3 Chemical Analysis of Sand and Water Samples Chemical analysis was conducted for composite sand samples collected within each DU and water samples collected from the middle of the Hanalei River. The samples were analyzed to identify the following contaminants:

• Total petroleum hydrocarbons (TPH) as diesel; • TPH as oil; • TPH as gasoline; • Polynuclear aromatic hydrocarbons (PAHs); and • RCRA Metals (arsenic, barium, cadmium, chromium, lead, mercury, selenium, silver).

All soil samples from each of the three sampling events only contained trace or non-detectable concentrations of petroleum related contaminants, and significant beach contamination was not observed. The highest detected concentration of diesel from any event was detected in DU-3 during the May 2016 sampling event at a concentration of 25 mg/kg. This is significantly below the respective environmental action level (EAL) for residential properties of 500 mg/kg. The highest detected concentration of oil was also detected in DU-3 during the May 2016 event at a concentration of 47 mg/kg; which is also significantly below the EAL of 500 mg/kg. The highest detected concentration of gasoline was detected in DU-3 during the July 2016 event at a concentration of 1.9 mg/kg, which is significantly below the EAL of 100 mg/kg. No PAHs were detected in any of the soil samples during any of the events at concentrations worth noting. Metals were detected the most in soil out of any contaminant, which is to be expected due to its background nature occurring in most soils. The highest detected concentration of arsenic from any event was detected in DU-2A during the August 2016 sampling event at a concentration of 27 mg/kg. This slightly exceeds the EAL of 24 mg/kg. Arsenic exceeded its EAL one other time throughout the project in the sample from DU-2B from the same event at a concentration of 26 mg/kg. Both of these exceedances are consistent in value with concentrations observed in other DUs and during other sampling events. The slight exceedances over the EAL can be attributed to laboratory instrument interference and variability of its outputted results, and are of no concern to the project. Detections of barium, cadmium, chromium, lead, selenium, silver and mercury from all sampling events were at concentrations not worth noting. The highest gasoline concentration detected in any of the water samples collected from DU-5 was 22 μg/L in the sample from July 2016. This is significantly below the EAL of 500 μg/L. No other contaminants were detected in water samples from any of the events at concentrations worth noting. The soil and water sample analytical results from each of the three sampling events are summarized in Table 4-1. The full results of the chemical analyses are included in Appendix A.



Table 4-1 Analytical data summary table for all sampling events (Element Environmental LLC)



4.3.1 Impacts from Vehicles When looking at the sample data, we do see a higher occurrence of diesel and oil detections in the samples from DU-3, which contains the heaviest vehicle traffic/parking out of any of the DUs. Therefore, we can draw the conclusion that there is a direct correlation between vehicle traffic and the presence of diesel and oil on the beach. However, when looking at the detected concentrations, we see the concentrations are very low (at least one order of magnitude lower than the respective EAL). Therefore, we can determine that although there is some impact related to vehicles on the beach, the impact is not significant. Additionally, when comparing the diesel and oil data from DU-3 between sampling events, the detected concentrations are consistent in value, and no increasing or decreasing trend is observed as the summer progressed. Rather, the diesel and oil results fluctuate randomly, and their general values remain similar. If vehicles were having a significant impact, one would expect to see higher concentrations later in the summer months (increasing trend) following consistent beach usage and/or holidays when vehicle traffic is heaviest. However, the data does not show this. There appears to be no accumulative nature to the diesel and oil detected on the beach throughout the summer; therefore, vehicle impact can be considered minimal. The detected metals concentrations are fairly consistent between the DUs south of the pier and the DUs in the parking lot area; as well as between individual sampling events. Therefore, it is safe to conclude that these detections are not related to impact by traffic on the beach, but rather are a product of naturally occurring background concentrations inland. The only comparison that would be worth noting is between the control DU-1 and the rest of the DUs. The control contained detections of the same metals, just at lower levels. This is most likely related to outfall from the Hanalei River depositing background concentrations more heavily on parts of the beach in its immediate vicinity.

4.4 Grain Size Analysis of Sand Samples Grain size analysis was conducted for composite samples collected within each DU during the first site visit on May 24, 2016. Each composite sample comprised 30 individual samples collected at even spacing across the length of the DU. A wet sieve analysis was conducted for smaller size fractions, and a dry sieve analysis was conducted for coarser size fractions. A summary of the results of the grain size analyses are shown in Figure 4-16. The full results of the grain size analyses are included in Appendix B. In general, the composite samples from each DU have similar grain size distribution. Between 75% - 80% of the sample weights were within the fine sand fraction (0.25 mm – 0.125 mm). Between 84% - 94% of the composite samples were within the fine and very fine sand fractions (0.25 mm - 0.075 mm). The samples are all similar in their general distribution of grain sizes, except for the fractions ranging from very fine sand (0.075 mm) to fine silt (0.0078 mm).



4.4.1 Impacts from Vehicles The subrange of the size fractions ranging from very fine sand (0.075 mm) to fine silt (0.0078 mm) identify a departure within DU-3 from the rest of the samples (Figure 4-17). Table 4-2 presents this subset of the grain analysis data, which focuses on the size fractions between medium sand (0.25 mm) and fine silt (0.0078 mm). The shaded grey columns indicate where most of the sample volume was present in each of the samples, and the red section of DU-3 indicates where the sample values depart from the other decision units. DU-3 shows an increase in fine sediment, relative to adjacent sample sites. This increase in fines is likely the result of continued vehicle traffic on the sand berm, causing mechanical abrasion of the grains. The beach area within the established vehicle access route is very compacted in comparison to the surrounding areas. The sand berm along the seaward edge of the established vehicle access route is much harder and more pronounced than the transient berms present along the adjacent portions of the shoreline (Figure 4-18). These data suggest that vehicle use on the beach is resulting in compaction and hardening of the berm.



Figure 4-16 Grain size analysis for each decision unit (log scale base 10 for x-axis)

-10

0

10

20

30

40

50

60

70

80

90

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0.000100.001000.010000.100001.0000010.00000

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ive

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enta

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DU 2B

DU 3

DU 4

DU 5



Figure 4-17 Grain size analysis focused on the silt sized fractions

-5

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0.001000.010000.10000

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DU 4

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Size

(mm) 0.25000 0.12500 0.07500 0.06300

0.04400 0.03100 0.02200 0.01600 0.00780

DU-3 94.200 19.200 3.000 2.430 2.160 2.080 1.810 1.810 0.990

DU-4 92.190 16.000 1.250 1.010 0.950 0.850 0.790 0.720 0.650

DU-6 90.770 10.880 0.740 0.610 0.560 0.510 0.410 0.410 0.410

DU-2A 95.130 16.960 0.790 0.600 0.480 0.480 0.370 0.370 0.210

DU-2B 85.410 12.240 1.680 1.310 1.210 0.980 0.760 0.700 0.600

Table 4-2 Subset of cumulative size fraction data for composite samples focused on the range between medium sand and fine silt.

Figure 4-18 Compacted berm along the edge of the established vehicle access route



5. CONCLUSION Shoreline processes at the project site are a result of combined marine and fluvial influences. The project site shoreline exhibits a historical trend of erosion ranging from -0.4 feet/year (1930-2008) to -1.34 feet/year (1988 to 2016). The shoreline is relatively stable along the southern portion of the project site and becomes progressively more dynamic and unstable along the northern portion of the shoreline. The ephemeral sand spit located at the Hanalei River mouth is a complex morphologic feature that is highly dynamic and mobile. This portion of the shoreline experiences extreme fluctuations in sediment volume and exhibits dramatic seasonal and intraseasonal variability. Vehicular use on the beach at Black Pot Beach Park has been ongoing for nearly half a century. Vehicle access and parking are primarily limited to the area north of Hanalei Pier. Vehicular use on the beach occurs daily but is likely greatest on weekends and holidays. During periods of heavy use, parked vehicles and the established access route occupy approximately 70% of the available beach area. Chemical analyses of sand samples detected a higher occurrence of diesel and oil detections in the area that experiences the highest amount of vehicle traffic, indicating that there is a direct correlation between vehicle traffic and the presence of diesel and oil on the beach. However, these concentrations are very low, thus vehicle impact can be considered minimal. Given the high amount of annual rainfall in the Hanalei region, it is possible that contaminants are being released through chemical erosion and weathering. Grain size fraction analyses of sand samples detected an increase in fine sediment in DU-3, relative to adjacent sample sites. This increase in fines is likely the result of continued vehicle traffic on the sand berm, causing mechanical abrasion of the grains. These observations suggest that vehicle use on the beach is resulting in compaction and hardening of the berm. Additional observations indicate that the area routinely used by vehicles is significantly more compacted than adjacent areas. Compaction in DU-3 is noticeably greater than compaction in DU-4 and DU-2B, seaward and south of DU-3, respectively.



6. REFERENCES Clark, John R. K. Beaches of Kaua‘i and Ni‘ihau. University of Hawai‘i Press. Honolulu, 1990. Fletcher, C., Grossman, E., Richmond, B., and Gibbs, A. (2002) Atlas of Natural Hazards in the Hawaiian Coastal Zone. U.S. Geological Survey. Geologic Investigations Series I-2761. United States Government Printing Office. Loomis, H. (1976) Tsunami Wave Runup Heights in Hawaii. Hawaii Institute of Geology and Geophysics and NOAA Joint Tsunami Research Effort, Pacific Marine Environmental Laboratory. NOAA-JTRE-161. HIG-76-5. Honolulu, Hawaii. University of Hawaii Coastal Geology Group, 2010, Hawaii Coastal Erosion Website - Kauai. http://www.soest.hawaii.edu/coasts/erosion/

http://www.soest.hawaii.edu/coasts/erosion/


Sea Engineering, Inc. a

APPENDIX A: BLACK POT BEACH SOIL AND WATER SAMPLING REPORT

98-030 Hekaha Street, Unit 9, Aiea, Hawaii 96701 tel: (808) 488-1200 fax: (808) 488-1300

September 15, 2016 Mr. Chris Conger Costal Scientist/Project Manager Sea Engineering, Inc. 41-305 Kalanianaole Hwy. Makai Research Pier Waimanalo, Hawaii 96795 Subject: Environmental Soil and Water Sampling Services Black Pot Beach Strand Sampling Hanalei, Kauai, Hawaii Dear Mr. Conger: Element Environmental LLC (E2) has prepared this letter report to describe the activities, observations, and findings resulting from environmental soil and water sampling performed at Black Pot Beach in Hanalei, Kauai, Hawaii. Sampling was performed on three separate occasions (24 May, 5 July, and 1 August 2016) in order to detect any contamination present at Black Pot Beach as well as to capture any variability or trends in detected contaminant concentrations between each sampling event.

Soil and Water Sampling Activities

E2 collected MULTI INCREMENT®1 (MI) soil samples from 3 to 6 inches below ground surface (bgs) from six predetermined beach parcels (decision units [DUs]) located in the vicinity of Black Pot Beach during each sampling event. DU-1 is located in “clean” sand north of the Hanalei River mouth and provided the location for a background/control sample; DU-3 is located north of the Hanalei Pier adjacent to the park where vehicle traffic is heaviest; DU-4 is also located north of the Hanalei Pier, makai of DU-3, where vehicle traffic is still heavy; DU-6 is located north of DUs 3 and 4, adjacent to the Hanalei River mouth; and DUs 2A and 2B are located south of the Hanalei Pier where beach conditions are similar to DUs 3 and 4, but access by vehicles does not occur (Figure 1). E2 also collected a single water sample from the mouth of the Hanalei River (DU-5) during each sampling event in order to screen for contaminants related to those potentially detected on the beach. The river sample was collected from approximately 150 feet off the south shore of the river, near the middle, where the ocean meets fresh water flowing from the mountains.

Soil and water samples were submitted to an analytical laboratory for analysis of the following contaminants:

1 MULTI INCREMENT® is a registered trademark of EnviroStat, Inc.

September 15, 2016 Page 2


Total petroleum hydrocarbons (TPH) as diesel;

TPH as oil;

TPH as gasoline;

Polynuclear aromatic hydrocarbons (PAHs); and

8 RCRA Metals (arsenic, barium, cadmium, chromium, lead, mercury, selenium and silver).

Sample Results

All soil samples from each of the three sampling events only contained trace or non-detectable concentrations of petroleum related contaminants, and significant beach contamination was not observed. The highest detected concentration of diesel from any event was detected in DU-3 during the May 2016 sampling event at a concentration of 25 mg/kg. This is significantly below the respective environmental action level (EAL) for residential properties of 500 mg/kg. The highest detected concentration of oil was also detected in DU-3 during the May 2016 event at a concentration of 47 mg/kg; which is also significantly below the EAL of 500 mg/kg. The highest detected concentration of gasoline was detected in DU-3 during the July 2016 event at a concentration of 1.9 mg/kg, which is significantly below the EAL of 100 mg/kg.

No PAHs were detected in any of the soil samples during any of the events at concentrations worth noting.

Metals were detected the most in soil out of any contaminant, which is to be expected due to its background nature ocurring in most soils. The highest detected concentration of arsenic from any event was detected in DU-2A during the August 2016 sampling event at a concentration of 27 mg/kg. This slightly exceeds the EAL of 24 mg/kg. Arsenic exceeded its EAL one other time throughout the project in the sample from DU-2B from the same event at a concentration of 26 mg/kg. Both of these exceedances are consistent in value with concentrations observed in other DUs and during other sampling events. The slight exceedances over the EAL can be attributed to laboratory instrument interference and variability of its outputted results, and are of no concern to the project. Detections of barium, cadmium, chromium, lead, selenium, silver and mercury from all sampling events were at concentrations not worth noting.

The highest gasoline concentration detected in any of the water samples collected from DU-5 was 22 µg/L in the sample from July 2016. This is significantly below the EAL of 500 µg/L. No other contaminants were detected in water samples from any of the events at concentrations worth noting.

All soil and water sample analytical retults from each of the three sampling events are summarized in Table 1.

Conclusions

When looking at the sample data, we do see a higher occurrence of diesel and oil detections in the samples from DU-3, which contains the heaviest vehicle traffic/parking out of any of the DUs. Therefore we can draw the conclusion that there is a direct correlation between vehicle traffic and the presence of diesel and oil on the beach. However when looking at the detected concentrations, we see the concentrations are very low (at least one order of magnitude lower than the respective EAL). Therefore we can determine that although there is some impact related to vehicles on the beach, the impact is not signigicant.



Additionally, when comparing the diesel and oil data from DU-3 between sampling events, the detected concentrations are consistent in value, and no increasing or decreasing trend is observed as the summer progressed. Rather, the diesel and oil results fluctuate randomly, and their general values remain similar.

If vehicles were having a significant impact, one would expect to see higher concentrations later in the summer months (increasing trend) following consistent beach usage and/or holidays when vehicle traffic is heaviest. However the data does not show this. There appears to be no accumulative nature to the diesel and oil detected on the beach throughout the summer; therefore vehicle impact can be considered minimal.

The detected metals concentrations are fairly consistent between the DUs south of the pier and the DUs in the parking lot area; as well as between individual sampling events. Therefore it is safe to conclude that these detections are not related to impact by traffic on the beach, but rather are a product of naturally occurring background concentrations inland. The only comparison that would be worth noting is between the control DU and the rest of the DUs. The control contained detections of the same metals, just at lower levels. This is most likely related to outfall from the Hanalei River depositing background concentrations more heavily on parts of the beach in its immediate vicinity.

Please feel free to contact me at (808) 294-4660 if you have any questions regarding the information presented in this letter report.

Sincerely,

Austin Lutey Environmental Engineer Element Environmental, LLC



Attachments

Table 1: Data Summary Table Figure 1: Black Pot Beach Decision Units Complete Laboratory Analytical Reports

Black Pot Beach Sand Analysis ProjectTable 1: Analytical Data Summary Table for All Sampling Events

Soil Water Soila Waterb

Gasoline Range Organics (GRO) mg/kg ug/L 100 500 ND 1.4 ND ND 1.5 ND ND 1.3 ND ND 1.9 ND ND 1.6 ND ND 1.5 ND ND 1.5 ND ND 1.4 ND ND 22 ND

Diesel Range Organics (DRO) mg/kg ug/L 500 640 ND 0.63 ND ND 0.87 ND ND 0.65 ND 25 1.4 ND 3.3 1.8 ND 1.1 6.6 ND ND 1.1 ND ND 0.63 ND ND ND ND

Residual Range Organics (RRO) mg/kg ug/L 500 640 ND ND ND ND ND ND ND ND ND 47 15 20 22 23 21 18 20 27 ND 3.9 ND ND ND 4.6 ND ND ND

1-Methylnaphthalene ug/kg ug/L 790 2.1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

2-Methylnaphthalene ug/kg ug/L 870 2.1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Acenaphthene ug/kg ug/L 120000 20 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Acenaphthylene ug/kg ug/L 13000 30 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Anthracene ug/kg ug/L 4300 0.73 ND ND ND ND ND 2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Benzo[a]anthracene ug/kg ug/L 1500 0.018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Benzo[a]pyrene ug/kg ug/L 150 0.014 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Benzo[b]fluoranthene ug/kg ug/L 1500 0.018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Benzo[g,h,i]perylene ug/kg ug/L 27000 0.1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Benzo[k]fluoranthene ug/kg ug/L 15000 0.018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Chrysene ug/kg ug/L 11000 0.018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Dibenzo(a,h)anthracene ug/kg ug/L 150 0.018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Fluoranthene ug/kg ug/L 87000 8 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Fluorene ug/kg ug/L 100000 3.9 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Indeno[1,2,3-cd]pyrene ug/kg ug/L 1500 0.018 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Naphthalene ug/kg ug/L 4500 21 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1.1 ND ND ND ND ND ND ND

Phenanthrene ug/kg ug/L 69000 4.6 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Pyrene ug/kg ug/L 44000 2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND

Arsenic mg/kg mg/L 24 0.00014 5.7 4.6 8.6 23 17 27 22 17 26 21 19 23 21 20 23 21 12 23 21 19 23 19 15 22 0.0091 ND ND

Barium mg/kg mg/L 1000 0.2 4.6 3.1 5.8 4.3 3.3 4.9 4.0 3 4.6 4.4 5.1 4.8 5.2 4.2 5.1 6.7 2.9 5.6 4.7 4.6 5.1 4.5 3.9 5.1 ND 0.0029 0.0079

Cadmium mg/kg mg/L 14 0.003 ND ND 0.16 0.11 0.033 0.6 0.15 0.049 0.6 0.15 0.048 0.52 0.13 0.11 0.77 0.14 0.043 0.76 0.12 0.1 0.74 0.095 0.055 0.73 ND ND ND

Chromium mg/kg mg/L 1100 0.074 23 21 28 55 36 66 71 49 75 75 70 85 71 66 89 78 49 94 72 73 84 69 56 88 ND 0.0038 0.031

Lead mg/kg mg/L 200 0.0056 1.2 ND ND 2.0 0.39 0.79 1.9 0.45 0.4 2.4 0.92 0.79 2.5 0.62 0.64 1.9 ND 0.4 1.6 0.57 0.55 1.8 0.55 0.4 ND ND ND

Selenium mg/kg mg/L 78 0.005 ND ND ND ND ND ND ND ND 0.68 ND ND 1.2 ND ND 1.2 ND ND ND ND ND 1.2 ND ND 0.97 ND ND ND

Silver mg/kg mg/L 78 0.001 ND ND ND ND ND ND ND ND ND 0.091 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.0009 ND

Mercury mg/kg mg/L 4.7 0.000025 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.008 ND ND 0.0062 ND ND ND ND ND ND NDaHDOH Tier 1 Unrestricted (Residential) land use Environmental Action Levels (EALs) for sites where groundwater is not a current or potential source of drinking water and the site is less than 150 meters to a surface water body (HDOH Fall 2011 revised January 2012).bHDOH Environmental Action Levels (EALs) for estuarine surface water bodies (HDOH Fall 2011 revised January 2012).

Bold, italicized and red font indicates the respective HDOH EAL was exceeded.

mg/kg = milligrams per kilogram

ug/kg = micrograms per kilogram

mg/L = milligrams per liter

ug/L = micrograms per liter

ND = not detected at or above the laboratory reporting limit

Analyte

HDOH Environmental Action Level

May 2016

Result

July 2016

Result

May 2016

Result

Sampling Location

Units

Matrix

July 2016

Result

May 2016

Result

July 2016

Result

May 2016

Result

August 2016

Result

DU-3

Sand

May 2016

Result

July 2016

Result

May 2016

Result

July 2016

Result

July 2016

Result

May 2016

Result

July 2016

Result

May 2016

Result

July 2016

Result

May 2016

Result

July 2016

Result

DU-3 (1st replicate)

Sand

August 2016

Result

DU-3 (2nd replicate)

Sand

August 2016

Result

Sand

August 2016

Result

DU-6

Sand

August 2016

Result

Total Metals (SW-846 6010B/7471A)

DU-1

Sand

August 2016

Result

DU-5

Water

August 2016

Result

Total Petroleum Hydrocarbons (TPH) (SW-846 8260/8015B)

Polynuclear Aromatic Hydrocarbons (PAHs) (SW-846 8270CSIM)

DU-2A

Sand

August 2016

Result

DU-2B

Sand

August 2016

Result

DU-4

ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Honolulu4429 Malaai St. #104Honolulu, HI 96818Tel: (808)486-5227

TestAmerica Job ID: 370-603-1Client Project/Site: Black Pot Beach Sand Analysis

For:Element Environmental, LLC98-030 Hekaha Street, Unit 9Aiea, Hawaii 96701

Attn: Matt Neal

Authorized for release by:6/15/2016 10:49:07 PM

Craig Pilialoha, Project Manager I(808)[email protected]

This report has been electronically signed and authorized by the signatory. Electronic signature isintended to be the legally binding equivalent of a traditionally handwritten signature.

Results relate only to the items tested and the sample(s) as received by the laboratory.

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https://secure.testamericainc.com/TotalAccess/login.aspx

http://www.testamericainc.com/AskTheExpert/Expert_index.htm

http://www.testamericainc.com

mailto:[email protected]

Table of Contents

Client: Element Environmental, LLCProject/Site: Black Pot Beach Sand Analysis

TestAmerica Job ID: 370-603-1

Page 2 of 55TestAmerica Honolulu

6/15/2016

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1

Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6

Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 19

Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 20

QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 26

QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46

Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 47

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 49

Receipt Checklists . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53

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Sample SummaryTestAmerica Job ID: 370-603-1Client: Element Environmental, LLC

Project/Site: Black Pot Beach Sand Analysis

Lab Sample ID Client Sample ID ReceivedCollectedMatrix

370-603-1 BPB-DU-2A Solid 05/24/16 09:40 05/25/16 13:20

370-603-2 BPB-DU-2B Solid 05/24/16 12:00 05/25/16 13:20

370-603-3 BPB-DU-5 Water 05/24/16 11:00 05/25/16 13:20

370-603-4 BPB-DU-3-1 Solid 05/24/16 13:45 05/25/16 13:20

370-603-5 BPB-DU-3-2 Solid 05/24/16 14:30 05/25/16 13:20

370-603-6 BPB-DU-3-3 Solid 05/24/16 14:45 05/25/16 13:20

370-603-7 BPB-DU-4 Solid 05/24/16 15:20 05/25/16 13:20

370-603-8 BPB-DU-6 Solid 05/24/16 15:40 05/25/16 13:20

370-603-9 BPB-DU-1 Solid 05/24/16 17:00 05/25/16 13:20

370-603-10 BPB-SW-2016524 Water 05/24/16 10:30 05/25/16 13:20

TestAmerica Honolulu

Page 3 of 55 6/15/2016

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Case NarrativeClient: Element Environmental, LLC TestAmerica Job ID: 370-603-1Project/Site: Black Pot Beach Sand Analysis

Job ID: 370-603-1

Laboratory: TestAmerica Honolulu

Narrative

Job Narrative370-603-1

Comments

No additional comments.

Receipt

The samples were received on 5/25/2016 1:20 PM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperatures of the 3 coolers at receipt time were 5.2º C, 5.8º C and 6.0º C.

GC/MS VOA Method(s) 8260/CALUFT DOD: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD)

associated with analytical batch 112518.

Method(s) 8260/CALUFT DOD, 8260B/CA_LUFTMS: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with analytical batch 112651.

Method(s) 8260/CALUFT DOD, 8260B/CA_LUFTMS: The method blank for preparation batch 111964 and analytical batch 113153

contained C4-C12 above the method detection limit. This target analyte concentration was less than the reporting limit (RL); therefore, re-extraction and/or re-analysis of samples was not performed.

No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.

GC/MS Semi VOA Method(s) 8270C SIM: The d5-Nitrobenzene surrogate recovery in the Laboratory Control Sample associated with prep batch 320-112764 is greater than the historical limit. Re-analysis confirms the high surrogate recovery. The data has been evaluated and as the LCS is in control for all target analytes, and the method blank and field samples are in control for all surrogates, narration is the corrective action.

BPB-DU-2A (370-603-1), BPB-DU-2B (370-603-2), BPB-DU-3-1 (370-603-4), BPB-DU-3-2 (370-603-5), BPB-DU-3-3 (370-603-6), BPB-DU-4 (370-603-7), BPB-DU-6 (370-603-8), BPB-DU-1 (370-603-9), (LCS 320-112764/2-A), (370-603-B-8-L MS) and (370-603-B-8-M MSD)

Method(s) 8270C SIM: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch 440-332987 and analytical batch 440-333626. The laboratory control sample (LCS) was performed in duplicate to

provide precision data for this batch.

Method(s) 8270C SIM: Surrogate recovery for the following sample was outside control limits: BPB-SW-2016524 (370-603-10). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed.


GC VOA Method(s) 8015B: The laboratory control sample (LCS) for 334438 recovered outside control limits for the following analytes: C4-C12.

These analytes were biased high in the LCS and were not detected in the associated samples; therefore, the data have been reported.


GC Semi VOA

Method(s) 8015B: The C24-C40 range extracted for sample 370-603-B-8-N was extracted outside of hold time because sample did not dry

in time. As a result, the C24-C40 range is being reported from the wet aliquot within hold. It is also being reported out of hold from the aliquot that was dried and sieved per the ISM process: BPB-DU-6 (370-603-8).

Method(s) 8015B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with

preparation batch 320-112589, 320-112766 and 320-112766 and analytical batch 320-113177. An MS/MSD was extracted with the job but

not reported with these samples due to differing limit groups.

TestAmerica HonoluluPage 4 of 55 6/15/2016

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Job ID: 370-603-1 (Continued)

Laboratory: TestAmerica Honolulu (Continued)

Method(s) 8015B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with batch preparation batch 440-333500 and analytical batch 440-333532. The laboratory control sample

(LCS) was performed in duplicate to provide precision data for this batch.(LCS 440-333500/2-A)

Method(s) 8015B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate

(MS/MSD/DUP) associated with batch preparation batch 440-333613 and analytical batch 440-333534. The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch.(LCS 440-333613/2-A)


Metals Method(s) 6010B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 320-112758 and 320-113070 and

analytical batch 320-113260 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the

associated laboratory control sample (LCS) recovery was within acceptance limits.

Method(s) 7471A: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 320-111799 and 320-113315 and

analytical batch 320-113617 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits.

Method(s) 6010B: The continuing calibration blank (CCB) for analytical batch 440-335425 contained Lead above the reporting limit (RL). All reported samples associated with this CCB were either ND for this analyte or contained this analyte at a concentration greater than 10X

the value found in the CCB; therefore, re-analysis of samples was not performed.


General Chemistry

Method(s) Moisture: There is no regulatory holding time for percent moisture analysis. The H flag for the following samples: BPB-DU-2A (370-603-1), BPB-DU-2B (370-603-2), BPB-DU-3-1 (370-603-4), BPB-DU-3-2 (370-603-5), BPB-DU-3-3 (370-603-6) and BPB-DU-4 (370-603-7) have been removed. This non-conformance indicates that the samples were analyzed out of 14 days of collection.

Method(s) Moisture: There is no regulatory holding time for percent moisture analysis. The H flag for the following samples: BPB-DU-6

(370-603-8) and BPB-DU-1 (370-603-9) have been removed. This non-conformance indicates that the samples were analyzed out of 14 days of collection.


Organic Prep

Method(s) 3550B: A deviation from the Standard Operating Procedure (SOP) occurred. Details are as follows: the following samples and

associated Method Blank (MB) and Laboratory Control Sample (LCS) were concentrated between 70-75 Celsius instead of the method specific 80-85 Celsius. Since this is a lower temperature, this should not affect analyte recoveries. This is applicable to preparation batch

320-112758 for method 8015-solid.

Method(s) 3550B: Sample BPB-DU-6 (370-603-8) for method 8015 was prepared outside of preparation holding time due to incomplete

drying on the final day of the holding time. The sample requested the Incremental Subsampling Procedure (ISM) and this method specifies complete drying prior to processing.

Method(s) 3520C: Elevated reporting limits are provided for the following sample due to insufficient sample provided for 3520/8270

Sample volume 500mL Amber preparation/analysis: BPB-SW-2016524 (370-603-10).

Method(s) 3510C: Elevated reporting limits are provided for the following sample(s) due to insufficient sample provided for 3510C/8015B

preparation/analysis:


VOA Prep

No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.


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Client Sample ResultsTestAmerica Job ID: 370-603-1Client: Element Environmental, LLC


Lab Sample ID: 370-603-1Client Sample ID: BPB-DU-2AMatrix: SolidDate Collected: 05/24/16 09:40

Percent Solids: 92.3Date Received: 05/25/16 13:20

Method: 8260/CALUFT DOD - Volatile Organic Compounds by GC/MSRL MDL

Gasoline Range Organics (GRO)

-C4-C12

ND 5.4 1.1 mg/Kg 05/31/16 12:27 06/04/16 20:32 1

Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier

4-Bromofluorobenzene (Surr) 96 59 - 120 05/31/16 12:27 06/04/16 20:32 1

Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery

Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)RL MDL

1-Methylnaphthalene ND 5.9 0.53 ug/Kg ☼ 06/07/16 08:27 06/08/16 14:22 1


5.9 0.51 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼2-Methylnaphthalene ND

5.9 0.55 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Acenaphthene ND

5.9 0.39 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Acenaphthylene ND

5.9 0.46 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Anthracene ND

5.9 0.36 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Benzo[a]anthracene ND

5.9 0.47 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Benzo[a]pyrene ND

5.9 0.59 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Benzo[b]fluoranthene ND

5.9 1.2 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Benzo[g,h,i]perylene ND

5.9 0.89 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Benzo[k]fluoranthene ND

5.9 0.41 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Chrysene ND

5.9 1.4 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Dibenz(a,h)anthracene ND

5.9 0.34 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Fluoranthene ND

5.9 0.58 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Fluorene ND

5.9 0.56 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Indeno[1,2,3-cd]pyrene ND

5.9 0.36 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Naphthalene ND

5.9 0.41 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Phenanthrene ND

5.9 0.41 ug/Kg 06/07/16 08:27 06/08/16 14:22 1☼Pyrene ND

2-Fluorobiphenyl (Surr) 75 53 - 113 06/07/16 08:27 06/08/16 14:22 1


Nitrobenzene-d5 105 06/07/16 08:27 06/08/16 14:22 153 - 113

Terphenyl-d14 94 06/07/16 08:27 06/08/16 14:22 170 - 144

Method: 8015B - Diesel Range Organics (DRO) (GC)RL MDL

DRO (C10-C25) ND 1.1 0.55 mg/Kg ☼ 06/07/16 08:34 06/09/16 22:19 1


5.0 3.7 mg/Kg 06/07/16 18:12 06/09/16 04:20 1RRO (C24-C40) ND

o-Terphenyl (Surr) 96 63 - 141 06/07/16 18:12 06/09/16 04:20 1


o-Terphenyl (Surr) 95 06/07/16 08:34 06/09/16 22:19 163 - 141

Method: 6010B - Metals (ICP)RL MDL

Arsenic 23 2.0 1.3 mg/Kg 06/09/16 06:45 06/09/16 19:06 2


1.0 0.12 mg/Kg 06/09/16 06:45 06/09/16 19:06 2Barium 4.3

0.20 0.030 mg/Kg 06/09/16 06:45 06/09/16 19:06 2Cadmium 0.11 J

0.50 0.14 mg/Kg 06/09/16 06:45 06/09/16 19:06 2Chromium 55

1.0 0.26 mg/Kg 06/09/16 06:45 06/09/16 19:06 2Lead 2.0 F1 B

2.0 1.4 mg/Kg 06/09/16 06:45 06/09/16 19:06 2Selenium ND

0.50 0.090 mg/Kg 06/09/16 06:45 06/09/16 19:06 2Silver ND


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Lab Sample ID: 370-603-1Client Sample ID: BPB-DU-2AMatrix: SolidDate Collected: 05/24/16 09:40


Method: 7471A - Mercury (CVAA)RL MDL

Mercury ND 0.026 0.0056 mg/Kg ☼ 06/10/16 10:05 06/10/16 16:41 1


General ChemistryRL MDL

Percent Moisture 7.7 0.1 0.1 % 06/08/16 20:00 1


0.1 0.1 % 06/08/16 20:00 1Percent Solids 92.3

Lab Sample ID: 370-603-2Client Sample ID: BPB-DU-2BMatrix: SolidDate Collected: 05/24/16 12:00




-C4-C12

ND 5.1 1.0 mg/Kg 05/31/16 12:27 06/06/16 19:02 1
















5.1 0.36 ug/Kg 06/07/16 08:27 06/08/16 14:51 1☼Chrysene ND



5.1 0.50 ug/Kg 06/07/16 08:27 06/08/16 14:51 1☼Fluorene ND




5.1 0.36 ug/Kg 06/07/16 08:27 06/08/16 14:51 1☼Pyrene ND



Nitrobenzene-d5 104 06/07/16 08:27 06/08/16 14:51 153 - 113

Terphenyl-d14 93 06/07/16 08:27 06/08/16 14:51 170 - 144


DRO (C10-C25) ND 1.1 0.57 mg/Kg ☼ 06/07/16 08:34 06/09/16 22:48 1


5.0 3.8 mg/Kg 06/07/16 18:12 06/09/16 05:47 1RRO (C24-C40) ND


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Lab Sample ID: 370-603-2Client Sample ID: BPB-DU-2BMatrix: SolidDate Collected: 05/24/16 12:00


o-Terphenyl (Surr) 98 63 - 141 06/07/16 18:12 06/09/16 05:47 1


o-Terphenyl (Surr) 93 06/07/16 08:34 06/09/16 22:48 163 - 141


Arsenic 22 2.0 1.3 mg/Kg 06/09/16 06:45 06/09/16 19:22 2


0.99 0.12 mg/Kg 06/09/16 06:45 06/09/16 19:22 2Barium 4.0

0.20 0.030 mg/Kg 06/09/16 06:45 06/09/16 19:22 2Cadmium 0.15 J

0.50 0.14 mg/Kg 06/09/16 06:45 06/09/16 19:22 2Chromium 71

0.99 0.26 mg/Kg 06/09/16 06:45 06/09/16 19:22 2Lead 1.9 B

2.0 1.4 mg/Kg 06/09/16 06:45 06/09/16 19:22 2Selenium ND

0.50 0.089 mg/Kg 06/09/16 06:45 06/09/16 19:22 2Silver ND


Mercury ND 0.027 0.0058 mg/Kg ☼ 06/10/16 10:05 06/10/16 16:43 1





0.1 0.1 % 06/08/16 20:00 1Percent Solids 88.7

Lab Sample ID: 370-603-3Client Sample ID: BPB-DU-5Matrix: WaterDate Collected: 05/24/16 11:00

Date Received: 05/25/16 13:20


1-Methylnaphthalene ND 0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1


0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 12-Methylnaphthalene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Acenaphthene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Acenaphthylene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Anthracene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Benzo[a]anthracene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Benzo[a]pyrene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Benzo[b]fluoranthene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Benzo[g,h,i]perylene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Benzo[k]fluoranthene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Chrysene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Dibenz(a,h)anthracene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Fluoranthene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Fluorene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Indeno[1,2,3-cd]pyrene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Naphthalene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Phenanthrene ND

0.21 0.11 ug/L 05/27/16 10:51 06/01/16 16:43 1Pyrene ND



Nitrobenzene-d5 69 05/27/16 10:51 06/01/16 16:43 146 - 109

Terphenyl-d14 101 05/27/16 10:51 06/01/16 16:43 128 - 124


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Lab Sample ID: 370-603-3Client Sample ID: BPB-DU-5Matrix: WaterDate Collected: 05/24/16 11:00


Method: 8015B - Gasoline Range Organics - (GC)RL MDL

GRO (C6-C12) ND 50 25 ug/L 06/04/16 08:03 1


4-Bromofluorobenzene (Surr) 104 65 - 140 06/04/16 08:03 1



DRO (C9-C25) ND 0.52 0.10 mg/L 05/31/16 07:52 05/31/16 19:04 1


0.52 0.10 mg/L 05/31/16 07:52 05/31/16 19:04 1RRO (C24-C40) ND

n-Octacosane 83 45 - 120 05/31/16 07:52 05/31/16 19:04 1


Method: 6010B - Metals (ICP) - Total RecoverableRL MDL

Arsenic 0.0091 J 0.010 0.0050 mg/L 06/03/16 12:27 06/08/16 15:22 1


0.010 0.0050 mg/L 06/03/16 12:27 06/08/16 15:22 1Barium ND

0.0050 0.0020 mg/L 06/03/16 12:27 06/08/16 15:22 1Cadmium ND

0.0050 0.0025 mg/L 06/03/16 12:27 06/08/16 15:22 1Chromium ND

0.0050 0.0025 mg/L 06/03/16 12:27 06/08/16 15:22 1Lead ND

0.010 0.0061 mg/L 06/03/16 12:27 06/08/16 15:22 1Selenium ND

0.010 0.0050 mg/L 06/03/16 12:27 06/08/16 15:22 1Silver ND


Mercury ND 0.00020 0.00010 mg/L 05/27/16 18:29 05/31/16 20:34 1


Lab Sample ID: 370-603-4Client Sample ID: BPB-DU-3-1Matrix: SolidDate Collected: 05/24/16 13:45




-C4-C12

ND 4.4 0.88 mg/Kg 05/31/16 12:27 06/06/16 19:24 1
















5.6 0.39 ug/Kg 06/07/16 08:27 06/08/16 15:20 1☼Chrysene ND


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Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)RL MDL

Dibenz(a,h)anthracene ND 5.6 1.3 ug/Kg ☼ 06/07/16 08:27 06/08/16 15:20 1



5.6 0.55 ug/Kg 06/07/16 08:27 06/08/16 15:20 1☼Fluorene ND




5.6 0.39 ug/Kg 06/07/16 08:27 06/08/16 15:20 1☼Pyrene ND



Nitrobenzene-d5 94 06/07/16 08:27 06/08/16 15:20 153 - 113

Terphenyl-d14 93 06/07/16 08:27 06/08/16 15:20 170 - 144


DRO (C10-C25) 25 1.2 0.62 mg/Kg ☼ 06/07/16 08:34 06/09/16 23:17 1


4.9 3.7 mg/Kg 06/07/16 18:12 06/09/16 06:16 1RRO (C24-C40) 47

o-Terphenyl (Surr) 97 63 - 141 06/07/16 18:12 06/09/16 06:16 1


o-Terphenyl (Surr) 96 06/07/16 08:34 06/09/16 23:17 163 - 141


Arsenic 21 2.0 1.3 mg/Kg 06/09/16 06:45 06/09/16 19:25 2


0.99 0.12 mg/Kg 06/09/16 06:45 06/09/16 19:25 2Barium 4.4

0.20 0.030 mg/Kg 06/09/16 06:45 06/09/16 19:25 2Cadmium 0.15 J

0.50 0.14 mg/Kg 06/09/16 06:45 06/09/16 19:25 2Chromium 75

0.99 0.26 mg/Kg 06/09/16 06:45 06/09/16 19:25 2Lead 2.4 B

2.0 1.4 mg/Kg 06/09/16 06:45 06/09/16 19:25 2Selenium ND

0.50 0.089 mg/Kg 06/09/16 06:45 06/09/16 19:25 2Silver 0.091 J


Mercury ND 0.029 0.0063 mg/Kg ☼ 06/10/16 10:05 06/10/16 16:50 1





0.1 0.1 % 06/08/16 20:00 1Percent Solids 83.1





-C4-C12

ND 6.0 1.2 mg/Kg 05/31/16 12:27 06/06/16 19:47 1





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5.9 0.41 ug/Kg 06/07/16 08:27 06/08/16 15:49 1☼Chrysene ND



5.9 0.58 ug/Kg 06/07/16 08:27 06/08/16 15:49 1☼Fluorene ND




5.9 0.41 ug/Kg 06/07/16 08:27 06/08/16 15:49 1☼Pyrene ND



Nitrobenzene-d5 85 06/07/16 08:27 06/08/16 15:49 153 - 113

Terphenyl-d14 95 06/07/16 08:27 06/08/16 15:49 170 - 144


DRO (C10-C25) 3.3 1.2 0.59 mg/Kg ☼ 06/07/16 08:34 06/09/16 23:46 1


5.0 3.8 mg/Kg 06/07/16 18:12 06/09/16 06:45 1RRO (C24-C40) 22

o-Terphenyl (Surr) 101 63 - 141 06/07/16 18:12 06/09/16 06:45 1


o-Terphenyl (Surr) 98 06/07/16 08:34 06/09/16 23:46 163 - 141


Arsenic 21 2.0 1.3 mg/Kg 06/09/16 06:45 06/09/16 19:28 2


1.0 0.12 mg/Kg 06/09/16 06:45 06/09/16 19:28 2Barium 5.2

0.20 0.031 mg/Kg 06/09/16 06:45 06/09/16 19:28 2Cadmium 0.13 J

0.51 0.14 mg/Kg 06/09/16 06:45 06/09/16 19:28 2Chromium 71

1.0 0.27 mg/Kg 06/09/16 06:45 06/09/16 19:28 2Lead 2.5 B

2.0 1.4 mg/Kg 06/09/16 06:45 06/09/16 19:28 2Selenium ND

0.51 0.092 mg/Kg 06/09/16 06:45 06/09/16 19:28 2Silver ND


Mercury ND 0.028 0.0060 mg/Kg ☼ 06/10/16 10:05 06/10/16 16:52 1





0.1 0.1 % 06/08/16 20:00 1Percent Solids 86.1


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-C4-C12

ND 4.7 0.94 mg/Kg 05/31/16 12:27 06/06/16 20:09 1
















5.5 0.38 ug/Kg 06/07/16 08:27 06/08/16 16:19 1☼Chrysene ND



5.5 0.54 ug/Kg 06/07/16 08:27 06/08/16 16:19 1☼Fluorene ND




5.5 0.39 ug/Kg 06/07/16 08:27 06/08/16 16:19 1☼Pyrene ND



Nitrobenzene-d5 88 06/07/16 08:27 06/08/16 16:19 153 - 113

Terphenyl-d14 91 06/07/16 08:27 06/08/16 16:19 170 - 144


DRO (C10-C25) 1.1 J 1.2 0.58 mg/Kg ☼ 06/07/16 08:34 06/10/16 00:15 1


5.1 3.8 mg/Kg 06/07/16 18:12 06/09/16 07:14 1RRO (C24-C40) 18

o-Terphenyl (Surr) 98 63 - 141 06/07/16 18:12 06/09/16 07:14 1


o-Terphenyl (Surr) 88 06/07/16 08:34 06/10/16 00:15 163 - 141


Arsenic 21 2.0 1.3 mg/Kg 06/09/16 06:45 06/09/16 19:31 2


1.0 0.12 mg/Kg 06/09/16 06:45 06/09/16 19:31 2Barium 6.7

0.20 0.030 mg/Kg 06/09/16 06:45 06/09/16 19:31 2Cadmium 0.14 J

0.51 0.14 mg/Kg 06/09/16 06:45 06/09/16 19:31 2Chromium 78

1.0 0.26 mg/Kg 06/09/16 06:45 06/09/16 19:31 2Lead 1.9 B

2.0 1.4 mg/Kg 06/09/16 06:45 06/09/16 19:31 2Selenium ND

0.51 0.091 mg/Kg 06/09/16 06:45 06/09/16 19:31 2Silver ND


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Mercury ND 0.028 0.0061 mg/Kg ☼ 06/10/16 10:05 06/10/16 16:54 1





0.1 0.1 % 06/08/16 20:00 1Percent Solids 86.4

Lab Sample ID: 370-603-7Client Sample ID: BPB-DU-4Matrix: SolidDate Collected: 05/24/16 15:20




-C4-C12

ND 5.0 1.0 mg/Kg 05/31/16 12:27 06/06/16 20:31 1
















6.3 0.44 ug/Kg 06/07/16 08:27 06/08/16 16:48 1☼Chrysene ND



6.3 0.61 ug/Kg 06/07/16 08:27 06/08/16 16:48 1☼Fluorene ND




6.3 0.44 ug/Kg 06/07/16 08:27 06/08/16 16:48 1☼Pyrene ND



Nitrobenzene-d5 108 06/07/16 08:27 06/08/16 16:48 153 - 113

Terphenyl-d14 94 06/07/16 08:27 06/08/16 16:48 170 - 144


DRO (C10-C25) ND 1.2 0.59 mg/Kg ☼ 06/07/16 08:34 06/10/16 00:44 1


5.1 3.9 mg/Kg 06/07/16 18:12 06/09/16 07:43 1RRO (C24-C40) ND


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o-Terphenyl (Surr) 96 63 - 141 06/07/16 18:12 06/09/16 07:43 1


o-Terphenyl (Surr) 91 06/07/16 08:34 06/10/16 00:44 163 - 141


Arsenic 21 2.0 1.3 mg/Kg 06/09/16 06:45 06/11/16 08:41 2


0.98 0.12 mg/Kg 06/09/16 06:45 06/11/16 08:41 2Barium 4.7

0.20 0.029 mg/Kg 06/09/16 06:45 06/11/16 08:41 2Cadmium 0.12 J

0.49 0.14 mg/Kg 06/09/16 06:45 06/11/16 08:41 2Chromium 72

0.98 0.26 mg/Kg 06/09/16 06:45 06/11/16 08:41 2Lead 1.6 B

2.0 1.4 mg/Kg 06/09/16 06:45 06/11/16 08:41 2Selenium ND

0.49 0.088 mg/Kg 06/09/16 06:45 06/11/16 08:41 2Silver ND


Mercury ND 0.027 0.0058 mg/Kg ☼ 06/10/16 10:05 06/10/16 16:57 1





0.1 0.1 % 06/08/16 20:00 1Percent Solids 86.9





-C4-C12

ND 4.4 0.88 mg/Kg 05/31/16 12:27 06/06/16 20:54 1
















6.2 0.43 ug/Kg 06/07/16 08:27 06/08/16 17:17 1☼Chrysene ND



6.2 0.61 ug/Kg 06/07/16 08:27 06/08/16 17:17 1☼Fluorene ND




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Phenanthrene ND 6.2 0.43 ug/Kg ☼ 06/07/16 08:27 06/08/16 17:17 1


6.2 0.43 ug/Kg 06/07/16 08:27 06/08/16 17:17 1☼Pyrene ND



Nitrobenzene-d5 108 06/07/16 08:27 06/08/16 17:17 153 - 113

Terphenyl-d14 93 06/07/16 08:27 06/08/16 17:17 170 - 144


DRO (C10-C25) ND 1.2 0.60 mg/Kg ☼ 06/07/16 08:34 06/10/16 01:13 1


6.0 4.5 mg/Kg 06/07/16 08:34 06/13/16 21:19 1☼RRO (C24-C40) ND

o-Terphenyl (Surr) 94 63 - 141 06/07/16 08:34 06/10/16 01:13 1


o-Terphenyl (Surr) 92 06/07/16 08:34 06/13/16 21:19 163 - 141

Method: 8015B - Diesel Range Organics (DRO) (GC) - RERL MDL

RRO (C24-C40) ND H 5.2 3.9 mg/Kg 06/08/16 14:41 06/10/16 19:36 1


o-Terphenyl (Surr) 108 63 - 141 06/08/16 14:41 06/10/16 19:36 1



Arsenic 19 2.0 1.3 mg/Kg 06/09/16 06:45 06/11/16 08:44 2


1.0 0.12 mg/Kg 06/09/16 06:45 06/11/16 08:44 2Barium 4.5

0.20 0.030 mg/Kg 06/09/16 06:45 06/11/16 08:44 2Cadmium 0.095 J

0.51 0.14 mg/Kg 06/09/16 06:45 06/11/16 08:44 2Chromium 69

1.0 0.26 mg/Kg 06/09/16 06:45 06/11/16 08:44 2Lead 1.8 B

2.0 1.4 mg/Kg 06/09/16 06:45 06/11/16 08:44 2Selenium ND

0.51 0.091 mg/Kg 06/09/16 06:45 06/11/16 08:44 2Silver ND


Mercury ND 0.029 0.0063 mg/Kg ☼ 06/10/16 10:05 06/10/16 16:59 1





0.1 0.1 % 06/09/16 18:48 1Percent Solids 81.7





-C4-C12

ND 5.7 1.1 mg/Kg 05/31/16 12:27 06/06/16 21:16 1



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5.7 0.39 ug/Kg 06/07/16 08:27 06/08/16 18:44 1☼Chrysene ND



5.7 0.56 ug/Kg 06/07/16 08:27 06/08/16 18:44 1☼Fluorene ND




5.7 0.40 ug/Kg 06/07/16 08:27 06/08/16 18:44 1☼Pyrene ND



Nitrobenzene-d5 111 06/07/16 08:27 06/08/16 18:44 153 - 113

Terphenyl-d14 92 06/07/16 08:27 06/08/16 18:44 170 - 144


DRO (C10-C25) ND 1.1 0.54 mg/Kg ☼ 06/07/16 08:34 06/10/16 01:42 1


5.1 3.8 mg/Kg 06/07/16 18:12 06/09/16 08:12 1RRO (C24-C40) ND

o-Terphenyl (Surr) 96 63 - 141 06/07/16 18:12 06/09/16 08:12 1


o-Terphenyl (Surr) 95 06/07/16 08:34 06/10/16 01:42 163 - 141


Arsenic 5.7 2.0 1.3 mg/Kg 06/09/16 06:45 06/11/16 08:47 2


1.0 0.12 mg/Kg 06/09/16 06:45 06/11/16 08:47 2Barium 4.6

0.20 0.030 mg/Kg 06/09/16 06:45 06/11/16 08:47 2Cadmium ND

0.50 0.14 mg/Kg 06/09/16 06:45 06/11/16 08:47 2Chromium 23

1.0 0.26 mg/Kg 06/09/16 06:45 06/11/16 08:47 2Lead 1.2 B

2.0 1.4 mg/Kg 06/09/16 06:45 06/11/16 08:47 2Selenium ND

0.50 0.090 mg/Kg 06/09/16 06:45 06/11/16 08:47 2Silver ND


Mercury ND 0.026 0.0056 mg/Kg ☼ 06/10/16 10:05 06/10/16 17:01 1



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0.1 0.1 % 06/09/16 18:48 1Percent Solids 92.8

Lab Sample ID: 370-603-10Client Sample ID: BPB-SW-2016524Matrix: WaterDate Collected: 05/24/16 10:30














0.47 0.24 ug/L 05/27/16 10:51 06/01/16 17:04 1Chrysene ND



0.47 0.24 ug/L 05/27/16 10:51 06/01/16 17:04 1Fluorene ND




0.47 0.24 ug/L 05/27/16 10:51 06/01/16 17:04 1Pyrene ND

2-Fluorobiphenyl (Surr) 45 X 50 - 104 05/27/16 10:51 06/01/16 17:04 1


Nitrobenzene-d5 58 05/27/16 10:51 06/01/16 17:04 146 - 109

Terphenyl-d14 12 X 05/27/16 10:51 06/01/16 17:04 128 - 124


DRO (C9-C25) ND 1.3 0.26 mg/L 05/31/16 14:28 06/01/16 01:43 1


1.3 0.26 mg/L 05/31/16 14:28 06/01/16 01:43 1RRO (C24-C40) ND

n-Octacosane 75 45 - 120 05/31/16 14:28 06/01/16 01:43 1



Arsenic 0.17 0.010 0.0050 mg/L 06/03/16 12:27 06/08/16 15:46 1


0.010 0.0050 mg/L 06/03/16 12:27 06/08/16 15:46 1Barium 0.24

0.0050 0.0020 mg/L 06/03/16 12:27 06/08/16 15:46 1Cadmium ND

0.0050 0.0025 mg/L 06/03/16 12:27 06/08/16 15:46 1Chromium 0.52

0.0050 0.0025 mg/L 06/03/16 12:27 06/08/16 15:46 1Lead 0.041

0.010 0.0061 mg/L 06/03/16 12:27 06/08/16 15:46 1Selenium ND

0.010 0.0050 mg/L 06/03/16 12:27 06/08/16 15:46 1Silver ND


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Lab Sample ID: 370-603-10Client Sample ID: BPB-SW-2016524Matrix: WaterDate Collected: 05/24/16 10:30



Mercury 0.00033 0.00020 0.00010 mg/L 05/27/16 18:29 05/31/16 20:37 1



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Method SummaryTestAmerica Job ID: 370-603-1Client: Element Environmental, LLC


Method Method Description LaboratoryProtocol

SW8468260/CALUFT

DOD

Volatile Organic Compounds by GC/MS TAL SAC

SW8468270C SIM Semivolatile Organic Compounds (GC/MS SIM) TAL SAC

SW8468270C SIM Semivolatile Organic Compounds (GC/MS SIM) TAL IRV

SW8468015B Gasoline Range Organics - (GC) TAL IRV

SW8468015B Diesel Range Organics (DRO) (GC) TAL SAC

SW8468015B Diesel Range Organics (DRO) (GC) TAL IRV

SW8466010B Metals (ICP) TAL SAC

SW8466010B Metals (ICP) TAL IRV

SW8467470A Mercury (CVAA) TAL IRV

SW8467471A Mercury (CVAA) TAL SAC

ASTMD 2216 Percent Moisture TAL SAC

Protocol References:

ASTM = ASTM International

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.

Laboratory References:

TAL IRV = TestAmerica Irvine, 17461 Derian Ave, Suite 100, Irvine, CA 92614-5817, TEL (949)261-1022

TAL SAC = TestAmerica Sacramento, 880 Riverside Parkway, West Sacramento, CA 95605, TEL (916)373-5600


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Lab ChronicleClient: Element Environmental, LLC TestAmerica Job ID: 370-603-1Project/Site: Black Pot Beach Sand Analysis

Client Sample ID: BPB-DU-2A Lab Sample ID: 370-603-1Matrix: SolidDate Collected: 05/24/16 09:40


Prep 5035 05/31/16 12:27 KAG111964 TAL SAC

Type

Batch Batch

MethodPrep Type LabAnalystRun

Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8260/CALUFT DOD 1 112518 06/04/16 20:32 SS TAL SACTotal/NA

ISM Prep Increment, prep 112758 06/07/16 07:57 M1A TAL SACTotal/NA

Prep 3550B 112901 06/07/16 18:12 R1D TAL SACTotal/NA

Analysis 8015B 1 112981 06/09/16 04:20 UFB TAL SACTotal/NA


Prep 3050B 113070 06/09/16 06:45 NIM TAL SACTotal/NA

Analysis 6010B 2 113260 06/09/16 19:06 CV1 TAL SACTotal/NA

ISM Prep Increment, Prep 112589 06/06/16 10:05 M1A TAL SACTotal/NA

Analysis D 2216 1 113066 06/08/16 20:00 JMD TAL SACTotal/NA

Client Sample ID: BPB-DU-2A Lab Sample ID: 370-603-1Matrix: SolidDate Collected: 05/24/16 09:40


ISM Prep Increment, Prep 06/06/16 10:05 M1A112589 TAL SAC

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Prep 3550B 112764 06/07/16 08:27 NGK TAL SACTotal/NA

Analysis 8270C SIM 1 112998 06/08/16 14:22 AP1 TAL SACTotal/NA



Analysis 8015B 1 113177 06/09/16 22:19 RS1 TAL SACTotal/NA


Prep 7471A 113315 06/10/16 10:05 CV1 TAL SACTotal/NA

Analysis 7471A 1 113617 06/10/16 16:41 CV1 TAL SACTotal/NA

Client Sample ID: BPB-DU-2B Lab Sample ID: 370-603-2Matrix: SolidDate Collected: 05/24/16 12:00


Prep 5035 05/31/16 12:27 KAG111964 TAL SAC

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











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Client Sample ID: BPB-DU-2B Lab Sample ID: 370-603-2Matrix: SolidDate Collected: 05/24/16 12:00



Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA









Client Sample ID: BPB-DU-5 Lab Sample ID: 370-603-3Matrix: WaterDate Collected: 05/24/16 11:00


Prep 3520C 05/27/16 10:51 FTD332987 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8270C SIM 1 333742 06/01/16 16:43 AI TAL IRVTotal/NA

Analysis 8015B 1 334438 06/04/16 08:03 JB TAL IRVTotal/NA

Prep 3510C 333500 05/31/16 07:52 L1A TAL IRVTotal/NA

Analysis 8015B 1 333532 05/31/16 19:04 CN TAL IRVTotal/NA

Prep 3005A 334362 06/03/16 12:27 Q1N TAL IRVTotal Recoverable

Analysis 6010B 1 335425 06/08/16 15:22 VS TAL IRVTotal Recoverable

Prep 7470A 333309 05/27/16 18:29 DB TAL IRVTotal/NA

Analysis 7470A 1 333867 05/31/16 20:34 DB TAL IRVTotal/NA

Client Sample ID: BPB-DU-3-1 Lab Sample ID: 370-603-4Matrix: SolidDate Collected: 05/24/16 13:45


Prep 5035 05/31/16 12:27 KAG111964 TAL SAC

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











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Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











Prep 5035 05/31/16 12:27 KAG111964 TAL SAC

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA










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Prep 5035 05/31/16 12:27 KAG111964 TAL SAC

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA









Client Sample ID: BPB-DU-4 Lab Sample ID: 370-603-7Matrix: SolidDate Collected: 05/24/16 15:20


Prep 5035 05/31/16 12:27 KAG111964 TAL SAC

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











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Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











Prep 5035 05/31/16 12:27 KAG111964 TAL SAC

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA


ISM Prep Increment, prep RE 112758 06/07/16 07:57 M1A TAL SACTotal/NA

Prep 3550B RE 113025 06/08/16 14:41 NGK TAL SACTotal/NA

Analysis 8015B RE 1 113302 06/10/16 19:36 UFB TAL SACTotal/NA









Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













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Prep 5035 05/31/16 12:27 KAG111964 TAL SAC

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA









Client Sample ID: BPB-SW-2016524 Lab Sample ID: 370-603-10Matrix: WaterDate Collected: 05/24/16 10:30


Prep 3520C 05/27/16 10:51 FTD332987 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA


Prep 3510C 333613 05/31/16 14:28 L2A TAL IRVTotal/NA





Analysis 7470A 1 333867 05/31/16 20:37 DB TAL IRVTotal/NA





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QC Sample ResultsTestAmerica Job ID: 370-603-1Client: Element Environmental, LLC


Method: 8260/CALUFT DOD - Volatile Organic Compounds by GC/MS

Client Sample ID: Method BlankLab Sample ID: MB 320-111964/3-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 113153 Prep Batch: 111964

RL MDL


-C4-C12

1.14 J 5.0 1.0 mg/Kg 05/31/16 12:27 06/09/16 18:25 1

MB MB

Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier


MB MB

Surrogate

05/31/16 12:27

Dil FacPrepared AnalyzedQualifier Limits%Recovery

Client Sample ID: Lab Control SampleLab Sample ID: LCS 320-111964/1-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 113153 Prep Batch: 111964


-C4-C12

50.0 41.7 mg/Kg 83 70 - 130

Analyte

LCS LCS

DUnitResult Qualifier %Rec

Spike

Added

%Rec.

Limits

4-Bromofluorobenzene (Surr) 59 - 120

Surrogate

97

LCS LCS

Qualifier Limits%Recovery

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 320-111964/2-AMatrix: Solid Prep Type: Total/NAAnalysis Batch: 113153 Prep Batch: 111964


-C4-C12

50.0 43.2 mg/Kg 86 70 - 130 4 30

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Surrogate

99

LCSD LCSD


Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)


RL MDL

1-Methylnaphthalene ND 5.0 0.45 ug/Kg 06/07/16 08:27 06/08/16 13:24 1

MB MB


ND 0.435.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 12-Methylnaphthalene

ND 0.475.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Acenaphthene

ND 0.335.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Acenaphthylene

ND 0.405.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Anthracene

ND 0.305.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Benzo[a]anthracene

ND 0.405.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Benzo[a]pyrene

ND 0.515.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Benzo[b]fluoranthene

ND 1.05.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Benzo[g,h,i]perylene

ND 0.765.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Benzo[k]fluoranthene

ND 0.355.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Chrysene

ND 1.25.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Dibenz(a,h)anthracene

ND 0.295.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Fluoranthene


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Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM) (Continued)


RL MDL

Fluorene ND 5.0 0.49 ug/Kg 06/07/16 08:27 06/08/16 13:24 1

MB MB


ND 0.485.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Indeno[1,2,3-cd]pyrene

ND 0.315.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Naphthalene

ND 0.355.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Phenanthrene

ND 0.355.0 ug/Kg 06/07/16 08:27 06/08/16 13:24 1Pyrene

2-Fluorobiphenyl (Surr) 78 53 - 113 06/08/16 13:24 1

MB MB

Surrogate

06/07/16 08:27


105 06/07/16 08:27 06/08/16 13:24 1Nitrobenzene-d5 53 - 113

91 06/07/16 08:27 06/08/16 13:24 1Terphenyl-d14 70 - 144


2-Methylnaphthalene 25.0 19.3 ug/Kg 77 54 - 114

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Acenaphthene 25.0 19.1 ug/Kg 76 51 - 111

Acenaphthylene 25.0 19.4 ug/Kg 78 51 - 111

Anthracene 25.0 19.7 ug/Kg 79 54 - 114

Benzo[a]anthracene 25.0 20.7 ug/Kg 83 66 - 126

Benzo[a]pyrene 25.0 19.2 ug/Kg 77 64 - 124

Benzo[b]fluoranthene 25.0 20.9 ug/Kg 84 65 - 125

Benzo[g,h,i]perylene 25.0 20.1 ug/Kg 81 54 - 134

Benzo[k]fluoranthene 25.0 20.4 ug/Kg 82 69 - 129

Chrysene 25.0 20.4 ug/Kg 81 67 - 127

Dibenz(a,h)anthracene 25.0 21.8 ug/Kg 87 58 - 128

Fluoranthene 25.0 20.6 ug/Kg 82 67 - 127

Fluorene 25.0 19.6 ug/Kg 78 54 - 114

Indeno[1,2,3-cd]pyrene 25.0 20.7 ug/Kg 83 59 - 133

Naphthalene 25.0 19.2 ug/Kg 77 52 - 112

Phenanthrene 25.0 18.8 ug/Kg 75 59 - 119

Pyrene 25.0 20.2 ug/Kg 81 71 - 131

2-Fluorobiphenyl (Surr) 53 - 113

Surrogate

81

LCS LCS


114 XNitrobenzene-d5 53 - 113

94Terphenyl-d14 70 - 144

Client Sample ID: BPB-DU-6Lab Sample ID: 370-603-8 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 112998 Prep Batch: 112764

2-Methylnaphthalene ND 30.4 22.7 ug/Kg 75 54 - 114☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Acenaphthene ND 30.4 22.4 ug/Kg 74 51 - 111☼

Acenaphthylene ND 30.4 23.0 ug/Kg 76 51 - 111☼

Anthracene ND 30.4 23.8 ug/Kg 78 54 - 114☼


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Client Sample ID: BPB-DU-6Lab Sample ID: 370-603-8 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 112998 Prep Batch: 112764

Benzo[a]anthracene ND 30.4 24.4 ug/Kg 80 66 - 126☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Benzo[a]pyrene ND 30.4 23.1 ug/Kg 76 64 - 124☼

Benzo[b]fluoranthene ND 30.4 24.1 ug/Kg 79 65 - 125☼

Benzo[g,h,i]perylene ND 30.4 24.0 ug/Kg 79 54 - 134☼

Benzo[k]fluoranthene ND 30.4 23.2 ug/Kg 77 69 - 129☼

Chrysene ND 30.4 23.9 ug/Kg 79 67 - 127☼

Dibenz(a,h)anthracene ND 30.4 25.9 ug/Kg 85 58 - 128☼

Fluoranthene ND 30.4 24.4 ug/Kg 80 67 - 127☼

Fluorene ND 30.4 23.0 ug/Kg 76 54 - 114☼

Indeno[1,2,3-cd]pyrene ND 30.4 24.6 ug/Kg 81 59 - 133☼

Naphthalene ND 30.4 22.7 ug/Kg 75 52 - 112☼

Phenanthrene ND 30.4 22.2 ug/Kg 73 59 - 119☼

Pyrene ND 30.4 23.8 ug/Kg 79 71 - 131☼


Surrogate

77

MS MS


109Nitrobenzene-d5 53 - 113


Client Sample ID: BPB-DU-6Lab Sample ID: 370-603-8 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 112998 Prep Batch: 112764

2-Methylnaphthalene ND 31.9 23.2 ug/Kg 73 54 - 114 2 30☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Acenaphthene ND 31.9 23.3 ug/Kg 73 51 - 111 4 30☼

Acenaphthylene ND 31.9 24.1 ug/Kg 76 51 - 111 5 30☼

Anthracene ND 31.9 24.9 ug/Kg 78 54 - 114 5 30☼

Benzo[a]anthracene ND 31.9 28.5 ug/Kg 89 66 - 126 16 30☼

Benzo[a]pyrene ND 31.9 27.2 ug/Kg 85 64 - 124 16 30☼

Benzo[b]fluoranthene ND 31.9 28.3 ug/Kg 89 65 - 125 16 30☼

Benzo[g,h,i]perylene ND 31.9 26.8 ug/Kg 84 54 - 134 11 30☼

Benzo[k]fluoranthene ND 31.9 26.8 ug/Kg 84 69 - 129 14 30☼

Chrysene ND 31.9 27.8 ug/Kg 87 67 - 127 15 30☼

Dibenz(a,h)anthracene ND 31.9 28.3 ug/Kg 89 58 - 128 9 30☼

Fluoranthene ND 31.9 27.8 ug/Kg 87 67 - 127 13 30☼

Fluorene ND 31.9 23.9 ug/Kg 75 54 - 114 4 30☼

Indeno[1,2,3-cd]pyrene ND 31.9 27.8 ug/Kg 87 59 - 133 12 30☼

Naphthalene ND 31.9 23.5 ug/Kg 74 52 - 112 3 30☼

Phenanthrene ND 31.9 23.3 ug/Kg 73 59 - 119 5 30☼

Pyrene ND 31.9 27.5 ug/Kg 86 71 - 131 14 30☼


Surrogate

76

MSD MSD





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Client Sample ID: Method BlankLab Sample ID: MB 440-332987/1-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 333626 Prep Batch: 332987

RL MDL


MB MB


ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 12-Methylnaphthalene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Acenaphthene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Acenaphthylene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Anthracene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Benzo[a]anthracene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Benzo[a]pyrene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Benzo[b]fluoranthene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Benzo[g,h,i]perylene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Benzo[k]fluoranthene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Chrysene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Dibenz(a,h)anthracene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Fluoranthene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Fluorene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Indeno[1,2,3-cd]pyrene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Naphthalene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Phenanthrene

ND 0.100.20 ug/L 05/26/16 14:21 05/31/16 16:56 1Pyrene


MB MB

Surrogate

05/26/16 14:21


70 05/26/16 14:21 05/31/16 16:56 1Nitrobenzene-d5 46 - 109

86 05/26/16 14:21 05/31/16 16:56 1Terphenyl-d14 28 - 124

Client Sample ID: Lab Control SampleLab Sample ID: LCS 440-332987/2-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 333626 Prep Batch: 332987

2-Methylnaphthalene 1.00 0.660 ug/L 66 48 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Acenaphthene 1.00 0.758 ug/L 76 54 - 120

Acenaphthylene 1.00 0.751 ug/L 75 55 - 120

Anthracene 1.00 0.740 ug/L 74 56 - 120

Benzo[a]anthracene 1.00 0.836 ug/L 84 63 - 120

Benzo[a]pyrene 1.00 0.796 ug/L 80 54 - 120

Benzo[b]fluoranthene 1.00 0.889 ug/L 89 60 - 120

Benzo[g,h,i]perylene 1.00 1.24 ug/L 124 61 - 139

Benzo[k]fluoranthene 1.00 0.901 ug/L 90 62 - 120

Chrysene 1.00 0.871 ug/L 87 65 - 120

Dibenz(a,h)anthracene 1.00 0.894 ug/L 89 61 - 120

Fluoranthene 1.00 0.840 ug/L 84 61 - 120

Fluorene 1.00 0.842 ug/L 84 53 - 120

Indeno[1,2,3-cd]pyrene 1.00 0.912 ug/L 91 61 - 122

Naphthalene 1.00 0.675 ug/L 67 46 - 120

Phenanthrene 1.00 0.825 ug/L 82 60 - 120

Pyrene 1.00 0.836 ug/L 84 63 - 120


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Surrogate

70

LCS LCS




Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 440-332987/3-AMatrix: Water Prep Type: Total/NAAnalysis Batch: 333626 Prep Batch: 332987

2-Methylnaphthalene 1.00 0.717 ug/L 72 48 - 120 8 35

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Acenaphthene 1.00 0.804 ug/L 80 54 - 120 6 35

Acenaphthylene 1.00 0.792 ug/L 79 55 - 120 5 35

Anthracene 1.00 0.766 ug/L 77 56 - 120 3 35

Benzo[a]anthracene 1.00 0.857 ug/L 86 63 - 120 2 35

Benzo[a]pyrene 1.00 0.799 ug/L 80 54 - 120 0 35

Benzo[b]fluoranthene 1.00 0.924 ug/L 92 60 - 120 4 35

Benzo[g,h,i]perylene 1.00 1.24 ug/L 124 61 - 139 0 35

Benzo[k]fluoranthene 1.00 0.922 ug/L 92 62 - 120 2 35

Chrysene 1.00 0.892 ug/L 89 65 - 120 2 35

Dibenz(a,h)anthracene 1.00 0.899 ug/L 90 61 - 120 1 35

Fluoranthene 1.00 0.876 ug/L 88 61 - 120 4 35

Fluorene 1.00 0.881 ug/L 88 53 - 120 5 35

Indeno[1,2,3-cd]pyrene 1.00 0.926 ug/L 93 61 - 122 2 35

Naphthalene 1.00 0.749 ug/L 75 46 - 120 10 35

Phenanthrene 1.00 0.862 ug/L 86 60 - 120 4 35

Pyrene 1.00 0.874 ug/L 87 63 - 120 4 35


Surrogate

77

LCSD LCSD




Method: 8015B - Gasoline Range Organics - (GC)

Client Sample ID: Method BlankLab Sample ID: MB 440-334438/31Matrix: Water Prep Type: Total/NAAnalysis Batch: 334438

RL MDL

GRO (C6-C12) ND 50 25 ug/L 06/03/16 23:40 1

MB MB



MB MB

Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery


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Method: 8015B - Gasoline Range Organics - (GC) (Continued)

Client Sample ID: Lab Control SampleLab Sample ID: LCS 440-334438/30Matrix: Water Prep Type: Total/NAAnalysis Batch: 334438

GRO (C4-C12) 800 987 * ug/L 123 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

115

LCS LCS


Client Sample ID: Matrix SpikeLab Sample ID: 440-148235-A-2 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 334438

GRO (C4-C12) ND * 800 964 ug/L 121 65 - 140

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Surrogate

108

MS MS


Client Sample ID: Matrix Spike DuplicateLab Sample ID: 440-148235-A-2 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 334438

GRO (C4-C12) ND * 800 949 ug/L 119 65 - 140 2 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Surrogate

107

MSD MSD


Method: 8015B - Diesel Range Organics (DRO) (GC)


RL MDL

DRO (C10-C25) ND 1.0 0.50 mg/Kg 06/07/16 08:34 06/09/16 19:54 1

MB MB


o-Terphenyl (Surr) 93 63 - 141 06/09/16 19:54 1

MB MB

Surrogate

06/07/16 08:34



RL MDL

RRO (C24-C40) ND 5.0 3.8 mg/Kg 06/07/16 08:34 06/13/16 20:50 1

MB MB


o-Terphenyl (Surr) 101 63 - 141 06/13/16 20:50 1

MB MB

Surrogate

06/07/16 08:34



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Method: 8015B - Diesel Range Organics (DRO) (GC) (Continued)


DRO (C10-C25) 10.0 8.98 mg/Kg 90 67 - 113

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

o-Terphenyl (Surr) 63 - 141

Surrogate

105

LCS LCS



RL MDL

RRO (C24-C40) ND 5.0 3.8 mg/Kg 06/07/16 18:12 06/09/16 03:23 1

MB MB


o-Terphenyl (Surr) 94 63 - 141 06/09/16 03:23 1

MB MB

Surrogate

06/07/16 18:12



RRO (C24-C40) 30.0 22.2 mg/Kg 74 50 - 150

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

95

LCS LCS


Client Sample ID: BPB-DU-2ALab Sample ID: 370-603-1 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 112981 Prep Batch: 112901

RRO (C24-C40) ND 30.3 24.3 mg/Kg 80 50 - 150

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Surrogate

97

MS MS


Client Sample ID: BPB-DU-2ALab Sample ID: 370-603-1 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 112981 Prep Batch: 112901

RRO (C24-C40) ND 30.1 25.9 mg/Kg 86 50 - 150 6 30

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Surrogate

102

MSD MSD



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RL MDL

RRO (C24-C40) ND 5.0 3.8 mg/Kg 06/08/16 14:41 06/10/16 20:05 1

MB MB


o-Terphenyl (Surr) 104 63 - 141 06/10/16 20:05 1

MB MB

Surrogate

06/08/16 14:41



RRO (C24-C40) 30.0 29.0 mg/Kg 97 50 - 150

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

112

LCS LCS



RL MDL

DRO (C9-C25) ND 0.50 0.10 mg/L 05/31/16 07:52 05/31/16 14:04 1

MB MB


ND 0.100.50 mg/L 05/31/16 07:52 05/31/16 14:04 1RRO (C24-C40)

n-Octacosane 75 45 - 120 05/31/16 14:04 1

MB MB

Surrogate

05/31/16 07:52



C10-C28 1.00 0.632 mg/L 63 40 - 115

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

n-Octacosane 45 - 120

Surrogate

84

LCS LCS



C10-C28 1.00 0.649 mg/L 65 40 - 115 3 25

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Surrogate

84

LCSD LCSD



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RL MDL

DRO (C9-C25) ND 0.50 0.10 mg/L 05/31/16 14:28 06/01/16 01:11 1

MB MB


ND 0.100.50 mg/L 05/31/16 14:28 06/01/16 01:11 1RRO (C24-C40)

n-Octacosane 87 45 - 120 06/01/16 01:11 1

MB MB

Surrogate

05/31/16 14:28



C10-C28 1.00 0.656 mg/L 66 40 - 115

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

81

LCS LCS



C10-C28 1.00 0.662 mg/L 66 40 - 115 1 25

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Surrogate

84

LCSD LCSD


Method: 6010B - Metals (ICP)


RL MDL

Arsenic ND 2.0 1.3 mg/Kg 06/09/16 06:45 06/09/16 17:02 1

MB MB


ND 0.121.0 mg/Kg 06/09/16 06:45 06/09/16 17:02 1Barium

ND 0.0300.20 mg/Kg 06/09/16 06:45 06/09/16 17:02 1Cadmium

ND 0.140.50 mg/Kg 06/09/16 06:45 06/09/16 17:02 1Chromium

0.648 J 0.261.0 mg/Kg 06/09/16 06:45 06/09/16 17:02 1Lead

ND 1.42.0 mg/Kg 06/09/16 06:45 06/09/16 17:02 1Selenium

ND 0.0900.50 mg/Kg 06/09/16 06:45 06/09/16 17:02 1Silver


Arsenic 200 194 mg/Kg 97 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


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Method: 6010B - Metals (ICP) (Continued)


Barium 200 198 mg/Kg 99 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Cadmium 5.00 5.00 mg/Kg 100 80 - 120

Chromium 20.0 19.7 mg/Kg 98 80 - 120

Lead 50.0 49.4 mg/Kg 99 80 - 120

Selenium 200 200 mg/Kg 100 80 - 120

Silver 5.00 4.91 mg/Kg 98 80 - 120

Client Sample ID: BPB-DU-2ALab Sample ID: 370-603-1 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 113260 Prep Batch: 113070

Arsenic 23 102 117 mg/Kg 92 80 - 120

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 4.3 102 93.2 mg/Kg 87 80 - 120

Cadmium 0.11 J 2.54 2.14 mg/Kg 80 80 - 120

Chromium 55 10.2 64.2 4 mg/Kg 86 80 - 120

Lead 2.0 F1 B 25.4 21.9 F1 mg/Kg 78 80 - 120

Selenium ND 102 90.9 mg/Kg 89 80 - 120

Silver ND 2.54 2.30 mg/Kg 90 80 - 120

Client Sample ID: BPB-DU-2ALab Sample ID: 370-603-1 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 113260 Prep Batch: 113070

Arsenic 23 100 114 mg/Kg 91 80 - 120 3 35

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium 4.3 100 91.0 mg/Kg 86 80 - 120 2 35

Cadmium 0.11 J 2.51 2.13 mg/Kg 81 80 - 120 0 35

Chromium 55 10.0 63.5 4 mg/Kg 79 80 - 120 1 35

Lead 2.0 F1 B 25.1 21.7 F1 mg/Kg 78 80 - 120 1 35

Selenium ND 100 89.7 mg/Kg 89 80 - 120 1 35

Silver ND 2.51 2.24 mg/Kg 89 80 - 120 3 35

Client Sample ID: Method BlankLab Sample ID: MB 440-334362/1-AMatrix: Water Prep Type: Total RecoverableAnalysis Batch: 335425 Prep Batch: 334362

RL MDL

Arsenic ND 0.010 0.0050 mg/L 06/03/16 12:27 06/08/16 15:16 1

MB MB


ND 0.00500.010 mg/L 06/03/16 12:27 06/08/16 15:16 1Barium

ND 0.00200.0050 mg/L 06/03/16 12:27 06/08/16 15:16 1Cadmium

ND 0.00250.0050 mg/L 06/03/16 12:27 06/08/16 15:16 1Chromium

ND 0.00250.0050 mg/L 06/03/16 12:27 06/08/16 15:16 1Lead

ND 0.00610.010 mg/L 06/03/16 12:27 06/08/16 15:16 1Selenium

ND 0.00500.010 mg/L 06/03/16 12:27 06/08/16 15:16 1Silver


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Client Sample ID: Lab Control SampleLab Sample ID: LCS 440-334362/2-AMatrix: Water Prep Type: Total RecoverableAnalysis Batch: 335425 Prep Batch: 334362

Arsenic 1.00 0.957 mg/L 96 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 1.00 0.998 mg/L 100 80 - 120

Cadmium 1.00 0.980 mg/L 98 80 - 120

Chromium 1.00 0.977 mg/L 98 80 - 120

Lead 1.00 0.984 mg/L 98 80 - 120

Selenium 1.00 0.934 mg/L 93 80 - 120

Silver 0.500 0.484 mg/L 97 80 - 120

Client Sample ID: BPB-DU-5Lab Sample ID: 370-603-3 MSMatrix: Water Prep Type: Total RecoverableAnalysis Batch: 335425 Prep Batch: 334362

Arsenic 0.0091 J 1.00 0.996 mg/L 99 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium ND 1.00 0.961 mg/L 96 75 - 125

Cadmium ND 1.00 0.936 mg/L 94 75 - 125

Chromium ND 1.00 0.987 mg/L 99 75 - 125

Lead ND 1.00 0.915 mg/L 91 75 - 125

Selenium ND 1.00 0.918 mg/L 92 75 - 125

Silver ND 0.500 0.486 mg/L 97 75 - 125

Client Sample ID: BPB-DU-5Lab Sample ID: 370-603-3 MSDMatrix: Water Prep Type: Total RecoverableAnalysis Batch: 335425 Prep Batch: 334362

Arsenic 0.0091 J 1.00 0.972 mg/L 96 75 - 125 2 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium ND 1.00 0.943 mg/L 94 75 - 125 2 20

Cadmium ND 1.00 0.925 mg/L 93 75 - 125 1 20

Chromium ND 1.00 0.972 mg/L 97 75 - 125 1 20

Lead ND 1.00 0.900 mg/L 90 75 - 125 2 20

Selenium ND 1.00 0.907 mg/L 91 75 - 125 1 20

Silver ND 0.500 0.476 mg/L 95 75 - 125 2 20

Method: 7470A - Mercury (CVAA)


RL MDL

Mercury ND 0.00020 0.00010 mg/L 05/27/16 18:29 05/31/16 20:20 1

MB MB



Mercury 0.00800 0.00817 mg/L 102 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


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Client Sample ID: Matrix SpikeLab Sample ID: 440-148327-A-3-C MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 333867 Prep Batch: 333309

Mercury ND 0.00800 0.00777 mg/L 97 70 - 130

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 440-148327-A-3-D MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 333867 Prep Batch: 333309

Mercury ND 0.00800 0.00771 mg/L 96 70 - 130 1 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD



RL MDL

Mercury ND 0.040 0.0086 mg/Kg 06/10/16 10:05 06/10/16 15:14 1

MB MB



Mercury 0.0833 0.0780 mg/Kg 94 86 - 114

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Matrix SpikeLab Sample ID: 320-19027-A-2-Q MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 113617 Prep Batch: 113315

Mercury 0.18 F1 0.151 0.307 F1 mg/Kg 84 86 - 114

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-19027-A-2-R MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 113617 Prep Batch: 113315

Mercury 0.18 F1 0.148 0.301 F1 mg/Kg 82 86 - 114 2 17

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


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QC Association SummaryTestAmerica Job ID: 370-603-1Client: Element Environmental, LLC


GC/MS VOA

Prep Batch: 111964

Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch

Solid 5035370-603-1 BPB-DU-2A Total/NA

Solid 5035370-603-2 BPB-DU-2B Total/NA

Solid 5035370-603-4 BPB-DU-3-1 Total/NA



Solid 5035370-603-7 BPB-DU-4 Total/NA



Solid 5035LCS 320-111964/1-A Lab Control Sample Total/NA

Solid 5035LCSD 320-111964/2-A Lab Control Sample Dup Total/NA

Solid 5035MB 320-111964/3-A Method Blank Total/NA

Analysis Batch: 112518


Solid 8260/CALUFT

DOD

111964370-603-1 BPB-DU-2A Total/NA



Solid 8260/CALUFT

DOD

111964370-603-2 BPB-DU-2B Total/NA

Solid 8260/CALUFT

DOD

111964370-603-4 BPB-DU-3-1 Total/NA

Solid 8260/CALUFT

DOD

111964370-603-5 BPB-DU-3-2 Total/NA

Solid 8260/CALUFT

DOD

111964370-603-6 BPB-DU-3-3 Total/NA

Solid 8260/CALUFT

DOD

111964370-603-7 BPB-DU-4 Total/NA

Solid 8260/CALUFT

DOD

111964370-603-8 BPB-DU-6 Total/NA

Solid 8260/CALUFT

DOD

111964370-603-9 BPB-DU-1 Total/NA



Solid 8260/CALUFT

DOD

111964LCS 320-111964/1-A Lab Control Sample Total/NA

Solid 8260/CALUFT

DOD

111964LCSD 320-111964/2-A Lab Control Sample Dup Total/NA

Solid 8260/CALUFT

DOD

111964MB 320-111964/3-A Method Blank Total/NA

GC/MS Semi VOA

ISM Prep Batch: 112589


Solid Increment, Prep370-603-1 BPB-DU-2A Total/NA

Solid Increment, Prep370-603-2 BPB-DU-2B Total/NA

Solid Increment, Prep370-603-4 BPB-DU-3-1 Total/NA



Solid Increment, Prep370-603-7 BPB-DU-4 Total/NA


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GC/MS Semi VOA (Continued)

ISM Prep Batch: 112589 (Continued)



Solid Increment, Prep370-603-8 MS BPB-DU-6 Total/NA

Solid Increment, Prep370-603-8 MSD BPB-DU-6 Total/NA


Prep Batch: 112764


Solid 3550B 112589370-603-1 BPB-DU-2A Total/NA

Solid 3550B 112589370-603-2 BPB-DU-2B Total/NA

Solid 3550B 112589370-603-4 BPB-DU-3-1 Total/NA



Solid 3550B 112589370-603-7 BPB-DU-4 Total/NA


Solid 3550B 112589370-603-8 MS BPB-DU-6 Total/NA

Solid 3550B 112589370-603-8 MSD BPB-DU-6 Total/NA


Solid 3550BLCS 320-112764/2-A Lab Control Sample Total/NA

Solid 3550BMB 320-112764/1-A Method Blank Total/NA



Solid 8270C SIM 112764370-603-1 BPB-DU-2A Total/NA

Solid 8270C SIM 112764370-603-2 BPB-DU-2B Total/NA

Solid 8270C SIM 112764370-603-4 BPB-DU-3-1 Total/NA



Solid 8270C SIM 112764370-603-7 BPB-DU-4 Total/NA


Solid 8270C SIM 112764370-603-8 MS BPB-DU-6 Total/NA

Solid 8270C SIM 112764370-603-8 MSD BPB-DU-6 Total/NA


Solid 8270C SIM 112764LCS 320-112764/2-A Lab Control Sample Total/NA

Solid 8270C SIM 112764MB 320-112764/1-A Method Blank Total/NA

Prep Batch: 332987


Water 3520C370-603-3 BPB-DU-5 Total/NA

Water 3520C370-603-10 BPB-SW-2016524 Total/NA

Water 3520CLCS 440-332987/2-A Lab Control Sample Total/NA

Water 3520CLCSD 440-332987/3-A Lab Control Sample Dup Total/NA

Water 3520CMB 440-332987/1-A Method Blank Total/NA



Water 8270C SIM 332987LCS 440-332987/2-A Lab Control Sample Total/NA

Water 8270C SIM 332987LCSD 440-332987/3-A Lab Control Sample Dup Total/NA

Water 8270C SIM 332987MB 440-332987/1-A Method Blank Total/NA


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Water 8270C SIM 332987370-603-3 BPB-DU-5 Total/NA

Water 8270C SIM 332987370-603-10 BPB-SW-2016524 Total/NA

GC VOA



Water 8015B370-603-3 BPB-DU-5 Total/NA

Water 8015B440-148235-A-2 MS Matrix Spike Total/NA

Water 8015B440-148235-A-2 MSD Matrix Spike Duplicate Total/NA

Water 8015BLCS 440-334438/30 Lab Control Sample Total/NA

Water 8015BMB 440-334438/31 Method Blank Total/NA

GC Semi VOA













Solid Increment, prep370-603-1 BPB-DU-2A Total/NA

Solid Increment, prep370-603-1 MS BPB-DU-2A Total/NA

Solid Increment, prep370-603-1 MSD BPB-DU-2A Total/NA

Solid Increment, prep370-603-2 BPB-DU-2B Total/NA

Solid Increment, prep370-603-4 BPB-DU-3-1 Total/NA



Solid Increment, prep370-603-7 BPB-DU-4 Total/NA

Solid Increment, prep370-603-8 - RE BPB-DU-6 Total/NA


Prep Batch: 112766












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GC Semi VOA (Continued)

Prep Batch: 112766 (Continued)



Prep Batch: 112901



Solid 3550B 112758370-603-1 MS BPB-DU-2A Total/NA

Solid 3550B 112758370-603-1 MSD BPB-DU-2A Total/NA




















Solid 8015B 112901LCS 320-112901/2-A Lab Control Sample Total/NA

Solid 8015B 112901MB 320-112901/1-A Method Blank Total/NA

Prep Batch: 113025


Solid 3550B 112758370-603-8 - RE BPB-DU-6 Total/NA
















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Solid 8015B 113025370-603-8 - RE BPB-DU-6 Total/NA







Prep Batch: 333500


Water 3510C370-603-3 BPB-DU-5 Total/NA






Water 8015B 333500370-603-3 BPB-DU-5 Total/NA

Water 8015B 333500LCS 440-333500/2-A Lab Control Sample Total/NA

Water 8015B 333500LCSD 440-333500/3-A Lab Control Sample Dup Total/NA

Water 8015B 333500MB 440-333500/1-A Method Blank Total/NA



Water 8015B 333613370-603-10 BPB-SW-2016524 Total/NA






Prep Batch: 333613


Water 3510C370-603-10 BPB-SW-2016524 Total/NA




Metals



Solid Increment, prep320-19027-A-2-Q MS Matrix Spike Total/NA

Solid Increment, prep320-19027-A-2-R MSD Matrix Spike Duplicate Total/NA





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Metals (Continued)












Solid Increment, prep370-603-1 BPB-DU-2A Total/NA

Solid Increment, prep370-603-1 MS BPB-DU-2A Total/NA

Solid Increment, prep370-603-1 MSD BPB-DU-2A Total/NA

Solid Increment, prep370-603-2 BPB-DU-2B Total/NA







Prep Batch: 113070

























Prep Batch: 113315


Solid 7471A 111799320-19027-A-2-Q MS Matrix Spike Total/NA


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Metals (Continued)



Solid 7471A 111799320-19027-A-2-R MSD Matrix Spike Duplicate Total/NA

Solid 7471A 112589370-603-1 BPB-DU-2A Total/NA

Solid 7471A 112589370-603-2 BPB-DU-2B Total/NA

Solid 7471A 112589370-603-4 BPB-DU-3-1 Total/NA



Solid 7471A 112589370-603-7 BPB-DU-4 Total/NA



Solid 7471ALCS 320-113315/12-A Lab Control Sample Total/NA

Solid 7471AMB 320-113315/11-A Method Blank Total/NA








Solid 7471A 113315320-19027-A-2-Q MS Matrix Spike Total/NA

Solid 7471A 113315320-19027-A-2-R MSD Matrix Spike Duplicate Total/NA

Solid 7471A 113315370-603-1 BPB-DU-2A Total/NA

Solid 7471A 113315370-603-2 BPB-DU-2B Total/NA







Solid 7471A 113315LCS 320-113315/12-A Lab Control Sample Total/NA

Solid 7471A 113315MB 320-113315/11-A Method Blank Total/NA

Prep Batch: 333309


Water 7470A370-603-3 BPB-DU-5 Total/NA

Water 7470A370-603-10 BPB-SW-2016524 Total/NA

Water 7470A440-148327-A-3-C MS Matrix Spike Total/NA

Water 7470A440-148327-A-3-D MSD Matrix Spike Duplicate Total/NA

Water 7470ALCS 440-333309/2-A Lab Control Sample Total/NA

Water 7470AMB 440-333309/1-A Method Blank Total/NA



Water 7470A 333309370-603-3 BPB-DU-5 Total/NA

Water 7470A 333309370-603-10 BPB-SW-2016524 Total/NA

Water 7470A 333309440-148327-A-3-C MS Matrix Spike Total/NA

Water 7470A 333309440-148327-A-3-D MSD Matrix Spike Duplicate Total/NA

Water 7470A 333309LCS 440-333309/2-A Lab Control Sample Total/NA

Water 7470A 333309MB 440-333309/1-A Method Blank Total/NA


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Metals (Continued)

Prep Batch: 334362


Water 3005A370-603-3 BPB-DU-5 Total Recoverable

Water 3005A370-603-3 MS BPB-DU-5 Total Recoverable

Water 3005A370-603-3 MSD BPB-DU-5 Total Recoverable

Water 3005A370-603-10 BPB-SW-2016524 Total Recoverable

Water 3005ALCS 440-334362/2-A Lab Control Sample Total Recoverable

Water 3005AMB 440-334362/1-A Method Blank Total Recoverable



Water 6010B 334362370-603-3 BPB-DU-5 Total Recoverable

Water 6010B 334362370-603-3 MS BPB-DU-5 Total Recoverable

Water 6010B 334362370-603-3 MSD BPB-DU-5 Total Recoverable

Water 6010B 334362370-603-10 BPB-SW-2016524 Total Recoverable

Water 6010B 334362LCS 440-334362/2-A Lab Control Sample Total Recoverable

Water 6010B 334362MB 440-334362/1-A Method Blank Total Recoverable

General Chemistry













Solid D 2216 112589370-603-1 BPB-DU-2A Total/NA

Solid D 2216 112589370-603-2 BPB-DU-2B Total/NA

Solid D 2216 112589370-603-4 BPB-DU-3-1 Total/NA



Solid D 2216 112589370-603-7 BPB-DU-4 Total/NA






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Definitions/GlossaryTestAmerica Job ID: 370-603-1Client: Element Environmental, LLC


Qualifiers

GC/MS VOA

Qualifier Description

J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.

Qualifier

GC/MS Semi VOA


X Surrogate is outside control limits

Qualifier

GC VOA


* LCS or LCSD is outside acceptance limits.

Qualifier

GC Semi VOA



Qualifier

H Sample was prepped or analyzed beyond the specified holding time

Metals


F1 MS and/or MSD Recovery is outside acceptance limits.

Qualifier


B Compound was found in the blank and sample.

4 MS, MSD: The analyte present in the original sample is greater than 4 times the matrix spike concentration; therefore, control limits are not

applicable.

Glossary

These commonly used abbreviations may or may not be present in this report.

¤ Listed under the "D" column to designate that the result is reported on a dry weight basis

Abbreviation

%R Percent Recovery

CFL Contains Free Liquid

CNF Contains no Free Liquid

DER Duplicate error ratio (normalized absolute difference)

Dil Fac Dilution Factor

DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample

DLC Decision level concentration

MDA Minimum detectable activity

EDL Estimated Detection Limit

MDC Minimum detectable concentration

MDL Method Detection Limit

ML Minimum Level (Dioxin)

NC Not Calculated

ND Not detected at the reporting limit (or MDL or EDL if shown)

PQL Practical Quantitation Limit

QC Quality Control

RER Relative error ratio

RL Reporting Limit or Requested Limit (Radiochemistry)

RPD Relative Percent Difference, a measure of the relative difference between two points

TEF Toxicity Equivalent Factor (Dioxin)

TEQ Toxicity Equivalent Quotient (Dioxin)


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Certification SummaryClient: Element Environmental, LLC TestAmerica Job ID: 370-603-1Project/Site: Black Pot Beach Sand Analysis

Laboratory: TestAmerica HonoluluAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.

Authority Program EPA Region Certification ID Expiration Date

Hawaii N/A9State Program 06-28-10 *

USDA Federal HON-S-206 11-04-16

Laboratory: TestAmerica IrvineAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.


Alaska CA0153110State Program 06-30-16 *

Arizona State Program 9 AZ0671 10-13-16

California LA Cty Sanitation Districts 9 10256 01-31-17 *

California State Program 9 CA ELAP 2706 06-30-16 *

Guam State Program 9 Cert. No. 12.002r 01-23-17

Hawaii State Program 9 N/A 01-29-17

Kansas NELAP Secondary AB 7 E-10420 07-31-16

Nevada State Program 9 CA015312016-2 07-31-16

New Mexico State Program 6 N/A 01-29-17

Northern Mariana Islands State Program 9 MP0002 01-29-17

Oregon NELAP 10 4028 01-29-17

USDA Federal P330-09-00080 07-08-18

Washington State Program 10 C900 09-03-16

Laboratory: TestAmerica SacramentoAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.


A2LA 2928-01DoD ELAP 01-31-17

Alaska (UST) State Program 10 UST-055 12-18-16


Arkansas DEQ State Program 6 88-0691 06-17-17

California State Program 9 2897 01-31-17

Colorado State Program 8 CA00044 08-31-16

Connecticut State Program 1 PH-0691 06-30-17

Florida NELAP 4 E87570 06-30-16


Illinois NELAP 5 200060 03-17-17

Kansas NELAP 7 E-10375 07-31-16

Louisiana NELAP 6 30612 06-30-16

Maine State Program 1 CA0004 04-18-18

Michigan State Program 5 9947 01-31-18

Nevada State Program 9 CA00044 07-31-16

New Jersey NELAP 2 CA005 06-30-16

New York NELAP 2 11666 04-01-17

Oregon NELAP 10 4040 01-29-17

Pennsylvania NELAP 3 68-01272 03-31-17

Texas NELAP 6 T104704399 07-31-17

US Fish & Wildlife Federal LE148388-0 10-31-16

USDA Federal P330-11-00436 12-30-17

USEPA UCMR Federal 1 CA00044 11-06-16

Utah NELAP 8 CA00044 02-28-17

Virginia NELAP 3 460278 03-14-17



* Certification renewal pending - certification considered valid.

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Laboratory: TestAmerica Sacramento (Continued)All certifications held by this laboratory are listed. Not all certifications are applicable to this report.


West Virginia (DW) 9930C3State Program 12-31-16

Wyoming State Program 8 8TMS-L 01-29-17


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Login Sample Receipt Checklist

Client: Element Environmental, LLC Job Number: 370-603-1

Login Number: 603

Question Answer Comment

Creator: Baldomero, Reed K

List Source: TestAmerica Honolulu

List Number: 1

TrueRadioactivity wasn't checked or is </= background as measured by a survey meter.

TrueThe cooler's custody seal, if present, is intact.

TrueSample custody seals, if present, are intact.

TrueThe cooler or samples do not appear to have been compromised or tampered with.

TrueSamples were received on ice.

TrueCooler Temperature is acceptable.

TrueCooler Temperature is recorded.

TrueCOC is present.

TrueCOC is filled out in ink and legible.

TrueCOC is filled out with all pertinent information.

TrueIs the Field Sampler's name present on COC?

TrueThere are no discrepancies between the containers received and the COC.

TrueSamples are received within Holding Time (excluding tests with immediate HTs)

TrueSample containers have legible labels.

TrueContainers are not broken or leaking.

TrueSample collection date/times are provided.

TrueAppropriate sample containers are used.

TrueSample bottles are completely filled.

N/ASample Preservation Verified.

TrueThere is sufficient vol. for all requested analyses, incl. any requested MS/MSDs

TrueContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").

TrueMultiphasic samples are not present.

TrueSamples do not require splitting or compositing.

N/AResidual Chlorine Checked.


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Login Number: 603


Creator: Perez, Angel

List Source: TestAmerica Irvine

List Creation: 05/27/16 12:04 PMList Number: 2

N/ARadioactivity wasn't checked or is </= background as measured by a survey meter.







TrueCOC is present.



N/AIs the Field Sampler's name present on COC?










N/AContainers requiring zero headspace have no headspace or bubble is <6mm (1/4").





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Login Number: 603


Creator: Hytrek, Cheryl

List Source: TestAmerica Sacramento




N/ASample custody seals, if present, are intact.





TrueCOC is present.



N/AIs the Field Sampler's name present on COC?















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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Sacramento880 Riverside ParkwayWest Sacramento, CA 95605Tel: (916)373-5600



Attn: Matt Neal



The test results in this report meet all 2003 NELAC and 2009 TNI requirements for accreditedparameters, exceptions are noted in this report. This report may not be reproduced except in full,and with written approval from the laboratory. For questions please contact the Project Managerat the e-mail address or telephone number listed on this page.



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Table of Contents



Page 2 of 55TestAmerica Sacramento

8/22/2016

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1


Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4

Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6


Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21


QC Association Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 37

Lab Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45


Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 52

Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 53

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 54


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Qualifiers

GC/MS VOA



Qualifier


GC/MS Semi VOA



Qualifier

GC Semi VOA



Qualifier


X Surrogate is outside control limits


Metals



Qualifier



applicable.

Glossary



Abbreviation

%R Percent Recovery












NC Not Calculated



QC Quality Control






TestAmerica Sacramento

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Job ID: 320-20109-1

Laboratory: TestAmerica Sacramento

Narrative


Comments

Final Report: A partial final report was last generated on 08/11/16 to include all data except for 8015B DRO (C10-C25) for sample DU-3-2-20160705 (320-20109-2) which required re-extraction out of hold due to low failing surrogate for the initial extraction which was done within hold. Both sets of data are being report. All other data already reported remain unchanged. COP 08/22/16

Receipt

The samples were received on 7/8/2016 9:20 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperatures of the 2 coolers at receipt time were 2.7º C and 3.2º C.

GC/MS VOA

Method(s) 8260B/CA_LUFTMS: The method blank for analytical batch 320-117842 contained gasoline ranges above the method detection limit. This target analyte concentration was less than half the reporting limit (1/2RL); therefore, re-extraction and re-analysis of samples was not performed.

Method(s) 8260B/CA_LUFTMS: The following samples were diluted to bring the concentration of target analytes within the calibration

range: (320-20046-C-2), (320-20046-C-2 MS) and (320-20046-C-2 MSD). Elevated reporting limits (RLs) are provided.

Method(s) 8260B/CA_LUFTMS: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch 117535 and analytical batch 117842.

Method(s) 8260B/CA_LUFTMS: The closing continuing calibration verification (CCV) associated with analytical batch 117842 was analyzed approximately 6 hours past the analysis of the samples.

(CCV 320-117842/59)


GC/MS Semi VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

GC Semi VOA

Method(s) 8015B: Surrogate recovery for the following samples was outside control limits: DU-2B-20160705 (320-20109-7). Evidence of matrix interference is present; therefore, re-extraction and/or re-analysis was not performed. Since this was present in both the DRO

sample and the RRO sample (which had two different extractions), matrix can be confirmed as the potential interference.

Method(s) 8015B: Surrogate recovery for the following sample for DRO (C10-C25) analysis was outside control limits: DU-3-2-20160705 (320-20109-2). Re-extraction and/or re-analysis was performed outside of holding time with acceptable results.

Method(s) 8015B: A matrix spike/matrix spike duplicate/sample duplicate (MS/MSD/DUP) associated with preparation batch 320-121672 was extracted and analyzed, however due to differing limit groups the MS/MSD is not associated with sample DU-3-2-20160705

(320-20109-2) for method 8015-solid.


Metals

Method(s) 6010B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries for preparation batch 320-117636 and 320-119391 and

analytical batch 320-119908 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample (LCS) recovery was within acceptance limits.

Method(s) 6010B: The matrix spike duplicate (MSD) recovery for preparation batch 320-119581 and analytical batch 320-119908 were

outside control limits for titanium. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory

control sample (LCS) recovery was within acceptance limits.

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Laboratory: TestAmerica Sacramento (Continued)

Method(s) 6010B: The serial dilution performed for the following samples associated with batch 320-119908 was outside control limits. Matrix interference is suspected. : (320-20109-A-1-J SD ^)


General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

Organic Prep Method(s) 3510C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with

analytical batch 320-117570 for 8270 SIM aqueous extraction.

Method(s) 3510C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with

analytical batch 320-117567 for 8015B_DRO aqueous extraction.

Method(s) 3550B: The following sample was re-prepared outside of preparation holding time due to sample DU-3-2-20160705

(320-20109-2) having low surrogate for diesel portion for 320-117428 for 8015-solid.



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Detection SummaryTestAmerica Job ID: 320-20109-1Client: Element Environmental, LLC


Client Sample ID: DU-3-1-20160705 Lab Sample ID: 320-20109-1


-C4-C12

RL

5.7 mg/Kg

MDL

1.1

Analyte Result Qualifier Unit Dil Fac D Method Prep Type

Total/NA1J B1.9 8260B/CA_LUFT

MS☼DRO (C10-C25) 1.1 mg/Kg0.54 Total/NA11.4 B 8015B

RRO (C24-C40) 5.0 mg/Kg3.7 Total/NA115 8015B

Arsenic 2.0 mg/Kg1.3 Total/NA219 6010B

Barium 1.0 mg/Kg0.12 Total/NA25.1 F1 6010B

Cadmium 0.20 mg/Kg0.030 Total/NA20.048 J F1 6010B

Chromium 0.50 mg/Kg0.14 Total/NA270 6010B

Copper 1.5 mg/Kg0.22 Total/NA211 6010B

Lead 1.0 mg/Kg0.26 Total/NA20.92 J F1 6010B

Strontium 5.0 mg/Kg1.0 Total/NA21900 6010B

Titanium 1.5 mg/Kg0.22 Total/NA2600 6010B

Zinc 2.0 mg/Kg0.19 Total/NA231 F1 6010B



-C4-C12

RL

5.2 mg/Kg

MDL

1.0



MS☼DRO (C10-C25) 1.1 mg/Kg0.55 Total/NA10.73 J B 8015B


☼DRO (C10-C25) - RE 1.1 mg/Kg0.53 Total/NA11.8 H 8015B


Barium 0.99 mg/Kg0.12 Total/NA24.2 6010B

Cadmium 0.20 mg/Kg0.030 Total/NA20.11 J 6010B



Lead 0.99 mg/Kg0.26 Total/NA20.62 J 6010B



Zinc 2.0 mg/Kg0.19 Total/NA228 6010B



-C4-C12

RL

5.0 mg/Kg

MDL

1.0



MS☼DRO (C10-C25) 1.1 mg/Kg0.54 Total/NA16.6 B 8015B






Copper 1.5 mg/Kg0.22 Total/NA27.2 6010B




☼Mercury 0.026 mg/Kg0.0056 Total/NA10.0080 J 7471A

Client Sample ID: DU-4-20160705 Lab Sample ID: 320-20109-4


This Detection Summary does not include radiochemical test results.

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Client Sample ID: DU-4-20160705 (Continued) Lab Sample ID: 320-20109-4


-C4-C12

RL

5.0 mg/Kg

MDL

1.0



MS☼Naphthalene 5.6 ug/Kg0.34 Total/NA11.1 J 8270C SIM

☼DRO (C10-C25) 1.1 mg/Kg0.55 Total/NA11.1 B 8015B

RRO (C24-C40) 5.0 mg/Kg3.8 Total/NA13.9 J 8015B










☼Mercury 0.027 mg/Kg0.0058 Total/NA10.0062 J 7471A



-C4-C12

RL

5.1 mg/Kg

MDL

1.0













Client Sample ID: DU-2A-20160705 Lab Sample ID: 320-20109-6


-C4-C12

RL

5.1 mg/Kg

MDL

1.0













Client Sample ID: DU-2B-20160705 Lab Sample ID: 320-20109-7



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Client Sample ID: DU-2B-20160705 (Continued) Lab Sample ID: 320-20109-7


-C4-C12

RL

4.7 mg/Kg

MDL

0.94















-C4-C12

RL

50 ug/L

MDL

15


Total/NA1J B22 8260B/CA_LUFT

MSBarium 0.0050 mg/L0.0025 Total/NA10.0029 J 6010B

Chromium 0.0080 mg/L0.0012 Total/NA10.0038 J 6010B

Silver 0.0050 mg/L0.00084 Total/NA10.00090 J 6010B

Strontium 0.050 mg/L0.0050 Total/NA10.14 6010B

Titanium 0.010 mg/L0.0021 Total/NA10.068 F1 6010B



-C4-C12

RL

5.0 mg/Kg

MDL

0.99




Arsenic 2.0 mg/Kg1.3 Total/NA24.6 6010B






Zinc 2.0 mg/Kg0.19 Total/NA26.9 6010B



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Lab Sample ID: 320-20109-1Client Sample ID: DU-3-1-20160705Matrix: SolidDate Collected: 07/05/16 09:30


Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSRL MDL

Gasoline Range Organics (GRO)-C4-C12

1.9 J B 5.7 1.1 mg/Kg 07/12/16 13:24 07/14/16 18:26 1
















5.4 0.38 ug/Kg 07/19/16 11:49 07/26/16 00:50 1☼Chrysene ND



5.4 0.53 ug/Kg 07/19/16 11:49 07/26/16 00:50 1☼Fluorene ND




5.4 0.38 ug/Kg 07/19/16 11:49 07/26/16 00:50 1☼Pyrene ND



Nitrobenzene-d5 74 07/19/16 11:49 07/26/16 00:50 153 - 113

Terphenyl-d14 79 07/19/16 11:49 07/26/16 00:50 170 - 144


DRO (C10-C25) 1.4 B 1.1 0.54 mg/Kg ☼ 07/18/16 11:09 07/30/16 12:35 1


5.0 3.7 mg/Kg 07/18/16 11:09 08/01/16 14:32 1RRO (C24-C40) 15

o-Terphenyl (Surr) 91 63 - 141 07/18/16 11:09 07/30/16 12:35 1


o-Terphenyl (Surr) 92 07/18/16 11:09 08/01/16 14:32 163 - 141


Arsenic 19 2.0 1.3 mg/Kg 07/26/16 07:00 07/28/16 12:12 2


1.0 0.12 mg/Kg 07/26/16 07:00 07/28/16 12:12 2Barium 5.1 F1

0.20 0.030 mg/Kg 07/26/16 07:00 07/28/16 12:12 2Cadmium 0.048 J F1

0.50 0.14 mg/Kg 07/26/16 07:00 07/28/16 12:12 2Chromium 70

1.5 0.22 mg/Kg 07/26/16 07:00 07/28/16 12:12 2Copper 11

1.0 0.26 mg/Kg 07/26/16 07:00 07/28/16 12:12 2Lead 0.92 J F1

2.0 1.4 mg/Kg 07/26/16 07:00 07/28/16 12:12 2Selenium ND

0.50 0.090 mg/Kg 07/26/16 07:00 07/28/16 12:12 2Silver ND F1


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Method: 6010B - Metals (ICP) (Continued)RL MDL

Strontium 1900 5.0 1.0 mg/Kg 07/26/16 07:00 07/28/16 12:12 2


10 3.0 mg/Kg 07/26/16 07:00 07/28/16 12:12 2Tin ND F1

1.5 0.22 mg/Kg 07/26/16 07:00 07/28/16 12:12 2Titanium 600

2.0 0.19 mg/Kg 07/26/16 07:00 07/28/16 12:12 2Zinc 31 F1


Mercury ND 0.026 0.0056 mg/Kg ☼ 07/26/16 18:20 07/27/16 14:09 1









1.6 J B 5.2 1.0 mg/Kg 07/12/16 13:24 07/14/16 18:49 1
















5.5 0.38 ug/Kg 07/19/16 11:49 07/26/16 01:20 1☼Chrysene ND



5.5 0.54 ug/Kg 07/19/16 11:49 07/26/16 01:20 1☼Fluorene ND




5.5 0.38 ug/Kg 07/19/16 11:49 07/26/16 01:20 1☼Pyrene ND



Nitrobenzene-d5 69 07/19/16 11:49 07/26/16 01:20 153 - 113

Terphenyl-d14 88 07/19/16 11:49 07/26/16 01:20 170 - 144


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DRO (C10-C25) 0.73 J B 1.1 0.55 mg/Kg ☼ 07/18/16 11:09 07/30/16 13:04 1


5.0 3.8 mg/Kg 07/18/16 11:09 08/01/16 15:59 1RRO (C24-C40) 23

o-Terphenyl (Surr) 28 X 63 - 141 07/18/16 11:09 07/30/16 13:04 1


o-Terphenyl (Surr) 90 07/18/16 11:09 08/01/16 15:59 163 - 141

Method: 8015B - Diesel Range Organics (DRO) (GC) - RERL MDL

DRO (C10-C25) 1.8 H 1.1 0.53 mg/Kg ☼ 08/11/16 10:11 08/18/16 16:23 1


o-Terphenyl (Surr) 94 63 - 141 08/11/16 10:11 08/18/16 16:23 1



Arsenic 20 2.0 1.3 mg/Kg 07/26/16 07:00 07/27/16 17:14 2


0.99 0.12 mg/Kg 07/26/16 07:00 07/27/16 17:14 2Barium 4.2

0.20 0.030 mg/Kg 07/26/16 07:00 07/27/16 17:14 2Cadmium 0.11 J

0.50 0.14 mg/Kg 07/26/16 07:00 07/27/16 17:14 2Chromium 66

1.5 0.22 mg/Kg 07/26/16 07:00 07/27/16 17:14 2Copper 11

0.99 0.26 mg/Kg 07/26/16 07:00 07/27/16 17:14 2Lead 0.62 J

2.0 1.4 mg/Kg 07/26/16 07:00 07/27/16 17:14 2Selenium ND

0.50 0.089 mg/Kg 07/26/16 07:00 07/27/16 17:14 2Silver ND

5.0 0.99 mg/Kg 07/26/16 07:00 07/27/16 17:14 2Strontium 1900

9.9 3.0 mg/Kg 07/26/16 07:00 07/27/16 17:14 2Tin ND

1.5 0.22 mg/Kg 07/26/16 07:00 07/27/16 17:14 2Titanium 430

2.0 0.19 mg/Kg 07/26/16 07:00 07/27/16 17:14 2Zinc 28


Mercury ND 0.026 0.0057 mg/Kg ☼ 07/26/16 18:20 07/27/16 14:11 1









1.5 J B 5.0 1.0 mg/Kg 07/12/16 13:24 07/14/16 19:12 1








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5.5 0.38 ug/Kg 07/19/16 11:49 07/26/16 01:49 1☼Chrysene ND



5.5 0.53 ug/Kg 07/19/16 11:49 07/26/16 01:49 1☼Fluorene ND




5.5 0.38 ug/Kg 07/19/16 11:49 07/26/16 01:49 1☼Pyrene ND



Nitrobenzene-d5 72 07/19/16 11:49 07/26/16 01:49 153 - 113

Terphenyl-d14 83 07/19/16 11:49 07/26/16 01:49 170 - 144


DRO (C10-C25) 6.6 B 1.1 0.54 mg/Kg ☼ 07/18/16 11:09 07/30/16 13:33 1


5.0 3.8 mg/Kg 07/18/16 11:09 08/01/16 16:28 1RRO (C24-C40) 20

o-Terphenyl (Surr) 97 63 - 141 07/18/16 11:09 07/30/16 13:33 1


o-Terphenyl (Surr) 84 07/18/16 11:09 08/01/16 16:28 163 - 141


Arsenic 12 2.0 1.3 mg/Kg 07/26/16 07:00 07/27/16 17:17 2


0.98 0.12 mg/Kg 07/26/16 07:00 07/27/16 17:17 2Barium 2.9

0.20 0.029 mg/Kg 07/26/16 07:00 07/27/16 17:17 2Cadmium 0.043 J

0.49 0.14 mg/Kg 07/26/16 07:00 07/27/16 17:17 2Chromium 49

1.5 0.22 mg/Kg 07/26/16 07:00 07/27/16 17:17 2Copper 7.2

0.98 0.26 mg/Kg 07/26/16 07:00 07/27/16 17:17 2Lead ND

2.0 1.4 mg/Kg 07/26/16 07:00 07/27/16 17:17 2Selenium ND

0.49 0.088 mg/Kg 07/26/16 07:00 07/27/16 17:17 2Silver ND

4.9 0.98 mg/Kg 07/26/16 07:00 07/27/16 17:17 2Strontium 1100

9.8 2.9 mg/Kg 07/26/16 07:00 07/27/16 17:17 2Tin ND

1.5 0.22 mg/Kg 07/26/16 07:00 07/27/16 17:17 2Titanium 330

2.0 0.19 mg/Kg 07/26/16 07:00 07/27/16 17:17 2Zinc 20


Mercury 0.0080 J 0.026 0.0056 mg/Kg ☼ 07/26/16 18:20 07/27/16 14:13 1



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Lab Sample ID: 320-20109-4Client Sample ID: DU-4-20160705Matrix: SolidDate Collected: 07/05/16 10:40




1.5 J B 5.0 1.0 mg/Kg 07/12/16 13:24 07/14/16 19:34 1
















5.6 0.39 ug/Kg 07/19/16 11:49 07/26/16 02:18 1☼Chrysene ND



5.6 0.54 ug/Kg 07/19/16 11:49 07/26/16 02:18 1☼Fluorene ND


5.6 0.34 ug/Kg 07/19/16 11:49 07/26/16 02:18 1☼Naphthalene 1.1 J


5.6 0.39 ug/Kg 07/19/16 11:49 07/26/16 02:18 1☼Pyrene ND



Nitrobenzene-d5 68 07/19/16 11:49 07/26/16 02:18 153 - 113

Terphenyl-d14 70 07/19/16 11:49 07/26/16 02:18 170 - 144


DRO (C10-C25) 1.1 B 1.1 0.55 mg/Kg ☼ 07/18/16 11:09 07/30/16 14:02 1


5.0 3.8 mg/Kg 07/18/16 11:09 08/01/16 16:57 1RRO (C24-C40) 3.9 J

o-Terphenyl (Surr) 86 63 - 141 07/18/16 11:09 07/30/16 14:02 1


o-Terphenyl (Surr) 91 07/18/16 11:09 08/01/16 16:57 163 - 141


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Arsenic 19 2.0 1.3 mg/Kg 07/26/16 07:00 07/27/16 17:20 2


0.99 0.12 mg/Kg 07/26/16 07:00 07/27/16 17:20 2Barium 4.6

0.20 0.030 mg/Kg 07/26/16 07:00 07/27/16 17:20 2Cadmium 0.10 J

0.50 0.14 mg/Kg 07/26/16 07:00 07/27/16 17:20 2Chromium 73

1.5 0.22 mg/Kg 07/26/16 07:00 07/27/16 17:20 2Copper 17

0.99 0.26 mg/Kg 07/26/16 07:00 07/27/16 17:20 2Lead 0.57 J

2.0 1.4 mg/Kg 07/26/16 07:00 07/27/16 17:20 2Selenium ND

0.50 0.089 mg/Kg 07/26/16 07:00 07/27/16 17:20 2Silver ND

5.0 0.99 mg/Kg 07/26/16 07:00 07/27/16 17:20 2Strontium 1900

9.9 3.0 mg/Kg 07/26/16 07:00 07/27/16 17:20 2Tin ND

1.5 0.22 mg/Kg 07/26/16 07:00 07/27/16 17:20 2Titanium 460

2.0 0.19 mg/Kg 07/26/16 07:00 07/27/16 17:20 2Zinc 30


Mercury 0.0062 J 0.027 0.0058 mg/Kg ☼ 07/26/16 18:20 07/27/16 14:15 1









1.4 J B 5.1 1.0 mg/Kg 07/12/16 13:24 07/14/16 19:57 1
















5.8 0.40 ug/Kg 07/19/16 11:49 07/26/16 02:47 1☼Chrysene ND



5.8 0.57 ug/Kg 07/19/16 11:49 07/26/16 02:47 1☼Fluorene ND




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Phenanthrene ND 5.8 0.41 ug/Kg ☼ 07/19/16 11:49 07/26/16 02:47 1


5.8 0.41 ug/Kg 07/19/16 11:49 07/26/16 02:47 1☼Pyrene ND



Nitrobenzene-d5 70 07/19/16 11:49 07/26/16 02:47 153 - 113

Terphenyl-d14 82 07/19/16 11:49 07/26/16 02:47 170 - 144


DRO (C10-C25) 0.63 J B 1.2 0.58 mg/Kg ☼ 07/18/16 11:09 07/30/16 14:31 1


4.9 3.7 mg/Kg 07/18/16 11:09 08/01/16 17:26 1RRO (C24-C40) ND

o-Terphenyl (Surr) 90 63 - 141 07/18/16 11:09 07/30/16 14:31 1


o-Terphenyl (Surr) 92 07/18/16 11:09 08/01/16 17:26 163 - 141


Arsenic 15 2.0 1.3 mg/Kg 07/26/16 07:00 07/27/16 17:23 2


1.0 0.12 mg/Kg 07/26/16 07:00 07/27/16 17:23 2Barium 3.9

0.20 0.030 mg/Kg 07/26/16 07:00 07/27/16 17:23 2Cadmium 0.055 J

0.50 0.14 mg/Kg 07/26/16 07:00 07/27/16 17:23 2Chromium 56

1.5 0.22 mg/Kg 07/26/16 07:00 07/27/16 17:23 2Copper 9.5

1.0 0.26 mg/Kg 07/26/16 07:00 07/27/16 17:23 2Lead 0.55 J

2.0 1.4 mg/Kg 07/26/16 07:00 07/27/16 17:23 2Selenium ND

0.50 0.090 mg/Kg 07/26/16 07:00 07/27/16 17:23 2Silver ND

5.0 1.0 mg/Kg 07/26/16 07:00 07/27/16 17:23 2Strontium 1500

10 3.0 mg/Kg 07/26/16 07:00 07/27/16 17:23 2Tin ND

1.5 0.22 mg/Kg 07/26/16 07:00 07/27/16 17:23 2Titanium 360

2.0 0.19 mg/Kg 07/26/16 07:00 07/27/16 17:23 2Zinc 23


Mercury ND 0.028 0.0060 mg/Kg ☼ 07/26/16 18:20 07/27/16 14:17 1





Lab Sample ID: 320-20109-6Client Sample ID: DU-2A-20160705Matrix: SolidDate Collected: 07/05/16 11:30




1.5 J B 5.1 1.0 mg/Kg 07/12/16 13:24 07/14/16 20:19 1





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5.7 0.40 ug/Kg 07/19/16 11:49 07/26/16 03:16 1☼Chrysene ND



5.7 0.56 ug/Kg 07/19/16 11:49 07/26/16 03:16 1☼Fluorene ND




5.7 0.40 ug/Kg 07/19/16 11:49 07/26/16 03:16 1☼Pyrene ND



Nitrobenzene-d5 67 07/19/16 11:49 07/26/16 03:16 153 - 113

Terphenyl-d14 85 07/19/16 11:49 07/26/16 03:16 170 - 144


DRO (C10-C25) 0.87 J B 1.1 0.57 mg/Kg ☼ 07/18/16 11:09 08/09/16 14:00 1


5.0 3.8 mg/Kg 07/18/16 11:09 08/01/16 17:55 1RRO (C24-C40) ND

o-Terphenyl (Surr) 78 63 - 141 07/18/16 11:09 08/01/16 17:55 1


o-Terphenyl (Surr) 82 07/18/16 11:09 08/09/16 14:00 163 - 141


Arsenic 17 2.0 1.3 mg/Kg 07/26/16 07:00 07/27/16 17:27 2


1.0 0.12 mg/Kg 07/26/16 07:00 07/27/16 17:27 2Barium 3.3

0.20 0.030 mg/Kg 07/26/16 07:00 07/27/16 17:27 2Cadmium 0.033 J

0.50 0.14 mg/Kg 07/26/16 07:00 07/27/16 17:27 2Chromium 36

1.5 0.22 mg/Kg 07/26/16 07:00 07/27/16 17:27 2Copper 7.5

1.0 0.26 mg/Kg 07/26/16 07:00 07/27/16 17:27 2Lead 0.39 J

2.0 1.4 mg/Kg 07/26/16 07:00 07/27/16 17:27 2Selenium ND

0.50 0.091 mg/Kg 07/26/16 07:00 07/27/16 17:27 2Silver ND

5.0 1.0 mg/Kg 07/26/16 07:00 07/27/16 17:27 2Strontium 1800

10 3.0 mg/Kg 07/26/16 07:00 07/27/16 17:27 2Tin ND

1.5 0.22 mg/Kg 07/26/16 07:00 07/27/16 17:27 2Titanium 320

2.0 0.19 mg/Kg 07/26/16 07:00 07/27/16 17:27 2Zinc 16


Mercury ND 0.027 0.0059 mg/Kg ☼ 07/26/16 18:20 07/27/16 14:22 1



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Lab Sample ID: 320-20109-7Client Sample ID: DU-2B-20160705Matrix: SolidDate Collected: 07/05/16 11:45




1.3 J B 4.7 0.94 mg/Kg 07/12/16 13:24 07/14/16 20:41 1
















5.7 0.40 ug/Kg 07/19/16 11:49 07/26/16 03:45 1☼Chrysene ND



5.7 0.56 ug/Kg 07/19/16 11:49 07/26/16 03:45 1☼Fluorene ND




5.7 0.40 ug/Kg 07/19/16 11:49 07/26/16 03:45 1☼Pyrene ND



Nitrobenzene-d5 73 07/19/16 11:49 07/26/16 03:45 153 - 113

Terphenyl-d14 85 07/19/16 11:49 07/26/16 03:45 170 - 144


DRO (C10-C25) 0.65 J B 1.1 0.55 mg/Kg ☼ 07/18/16 11:09 07/30/16 15:29 1


5.0 3.8 mg/Kg 07/18/16 11:09 08/08/16 18:34 1RRO (C24-C40) ND

o-Terphenyl (Surr) 55 X 63 - 141 07/18/16 11:09 07/30/16 15:29 1


o-Terphenyl (Surr) 16 X 07/18/16 11:09 08/08/16 18:34 163 - 141


Arsenic 17 2.0 1.3 mg/Kg 07/26/16 07:00 07/27/16 17:30 2


1.0 0.12 mg/Kg 07/26/16 07:00 07/27/16 17:30 2Barium 3.0

0.20 0.030 mg/Kg 07/26/16 07:00 07/27/16 17:30 2Cadmium 0.049 J

0.50 0.14 mg/Kg 07/26/16 07:00 07/27/16 17:30 2Chromium 49


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Copper 8.3 1.5 0.22 mg/Kg 07/26/16 07:00 07/27/16 17:30 2


1.0 0.26 mg/Kg 07/26/16 07:00 07/27/16 17:30 2Lead 0.45 J

2.0 1.4 mg/Kg 07/26/16 07:00 07/27/16 17:30 2Selenium ND

0.50 0.091 mg/Kg 07/26/16 07:00 07/27/16 17:30 2Silver ND

5.0 1.0 mg/Kg 07/26/16 07:00 07/27/16 17:30 2Strontium 1500

10 3.0 mg/Kg 07/26/16 07:00 07/27/16 17:30 2Tin ND

1.5 0.22 mg/Kg 07/26/16 07:00 07/27/16 17:30 2Titanium 350

2.0 0.19 mg/Kg 07/26/16 07:00 07/27/16 17:30 2Zinc 20


Mercury ND 0.026 0.0057 mg/Kg ☼ 07/26/16 18:20 07/27/16 14:24 1





Lab Sample ID: 320-20109-8Client Sample ID: DU-5-20160705Matrix: WaterDate Collected: 07/05/16 12:30




22 J B 50 15 ug/L 07/14/16 21:26 1
















0.057 0.0046 ug/L 07/12/16 16:02 07/21/16 23:01 1Chrysene ND



0.057 0.0046 ug/L 07/12/16 16:02 07/21/16 23:01 1Fluorene ND




0.057 0.0048 ug/L 07/12/16 16:02 07/21/16 23:01 1Pyrene ND


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Nitrobenzene-d5 86 07/12/16 16:02 07/21/16 23:01 120 - 123

Terphenyl-d14 100 07/12/16 16:02 07/21/16 23:01 146 - 137


DRO (C10-C25) ND 56 18 ug/L 07/12/16 15:58 08/07/16 20:07 1


560 180 ug/L 07/12/16 15:58 08/07/16 20:07 1RRO (C24-C40) ND

o-Terphenyl (Surr) 77 56 - 145 07/12/16 15:58 08/07/16 20:07 1



Arsenic ND 0.020 0.012 mg/L 07/27/16 07:00 07/28/16 12:59 1


0.0050 0.0025 mg/L 07/27/16 07:00 07/28/16 12:59 1Barium 0.0029 J

0.0020 0.00050 mg/L 07/27/16 07:00 07/28/16 12:59 1Cadmium ND

0.0080 0.0012 mg/L 07/27/16 07:00 07/28/16 12:59 1Chromium 0.0038 J

0.010 0.0021 mg/L 07/27/16 07:00 07/28/16 12:59 1Copper ND

0.0050 0.0025 mg/L 07/27/16 07:00 07/28/16 12:59 1Lead ND

0.020 0.013 mg/L 07/27/16 07:00 07/28/16 12:59 1Selenium ND

0.0050 0.00084 mg/L 07/27/16 07:00 07/28/16 12:59 1Silver 0.00090 J

0.050 0.0050 mg/L 07/27/16 07:00 07/28/16 12:59 1Strontium 0.14

0.020 0.0050 mg/L 07/27/16 07:00 07/28/16 12:59 1Tin ND

0.010 0.0021 mg/L 07/27/16 07:00 07/28/16 12:59 1Titanium 0.068 F1

0.010 0.0030 mg/L 07/27/16 07:00 07/28/16 12:59 1Zinc ND


Mercury ND 0.00020 0.00010 mg/L 07/20/16 08:34 07/20/16 12:31 1






1.4 J B 5.0 0.99 mg/Kg 07/12/16 13:24 07/14/16 21:04 1














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Benzo[b]fluoranthene ND 5.3 0.53 ug/Kg ☼ 07/19/16 11:49 07/26/16 04:14 1




5.3 0.37 ug/Kg 07/19/16 11:49 07/26/16 04:14 1☼Chrysene ND



5.3 0.52 ug/Kg 07/19/16 11:49 07/26/16 04:14 1☼Fluorene ND




5.3 0.37 ug/Kg 07/19/16 11:49 07/26/16 04:14 1☼Pyrene ND



Nitrobenzene-d5 84 07/19/16 11:49 07/26/16 04:14 153 - 113

Terphenyl-d14 86 07/19/16 11:49 07/26/16 04:14 170 - 144


DRO (C10-C25) 0.63 J B 1.0 0.52 mg/Kg ☼ 07/18/16 11:09 07/30/16 15:58 1


5.0 3.8 mg/Kg 07/18/16 11:09 08/01/16 18:53 1RRO (C24-C40) ND

o-Terphenyl (Surr) 90 63 - 141 07/18/16 11:09 07/30/16 15:58 1


o-Terphenyl (Surr) 69 07/18/16 11:09 08/01/16 18:53 163 - 141


Arsenic 4.6 2.0 1.3 mg/Kg 07/26/16 07:00 07/27/16 17:33 2


1.0 0.12 mg/Kg 07/26/16 07:00 07/27/16 17:33 2Barium 3.1

0.20 0.030 mg/Kg 07/26/16 07:00 07/27/16 17:33 2Cadmium ND

0.50 0.14 mg/Kg 07/26/16 07:00 07/27/16 17:33 2Chromium 21

1.5 0.22 mg/Kg 07/26/16 07:00 07/27/16 17:33 2Copper 3.0

1.0 0.26 mg/Kg 07/26/16 07:00 07/27/16 17:33 2Lead ND

2.0 1.4 mg/Kg 07/26/16 07:00 07/27/16 17:33 2Selenium ND

0.50 0.090 mg/Kg 07/26/16 07:00 07/27/16 17:33 2Silver ND

5.0 1.0 mg/Kg 07/26/16 07:00 07/27/16 17:33 2Strontium 1500

10 3.0 mg/Kg 07/26/16 07:00 07/27/16 17:33 2Tin ND

1.5 0.22 mg/Kg 07/26/16 07:00 07/27/16 17:33 2Titanium 150

2.0 0.19 mg/Kg 07/26/16 07:00 07/27/16 17:33 2Zinc 6.9


Mercury ND 0.026 0.0056 mg/Kg ☼ 07/26/16 18:20 07/27/16 14:26 1






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Surrogate SummaryTestAmerica Job ID: 320-20109-1Client: Element Environmental, LLC


Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSPrep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (59-120)

BFB

95320-20109-1

Percent Surrogate Recovery (Acceptance Limits)

DU-3-1-20160705

91320-20109-2 DU-3-2-20160705

94320-20109-3 DU-3-3-20160705

92320-20109-4 DU-4-20160705

91320-20109-5 DU-6-20160705

92320-20109-6 DU-2A-20160705

93320-20109-7 DU-2B-20160705

95320-20109-9 DU-1-20160705

91LCS 320-117535/1-A Lab Control Sample

95LCSD 320-117535/2-A Lab Control Sample Dup

90MB 320-117535/3-A Method Blank

Surrogate Legend

BFB = 4-Bromofluorobenzene (Surr)

Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MSPrep Type: Total/NAMatrix: Water


BFB

97320-20046-C-2 MS


Matrix Spike

97320-20046-C-2 MSD Matrix Spike Duplicate

92320-20109-8 DU-5-20160705

99LCS 320-117842/7 Lab Control Sample

96LCSD 320-117842/8 Lab Control Sample Dup

93MB 320-117842/10 Method Blank

Surrogate Legend

BFB = 4-Bromofluorobenzene (Surr)

Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)Prep Type: Total/NAMatrix: Solid

Lab Sample ID Client Sample ID (53-113) (53-113) (70-144)

FBP NBZ TPH

71 74 79320-20109-1


DU-3-1-20160705

64 69 88320-20109-2 DU-3-2-20160705

63 72 83320-20109-3 DU-3-3-20160705

67 68 70320-20109-4 DU-4-20160705

71 70 82320-20109-5 DU-6-20160705

72 67 85320-20109-6 DU-2A-20160705

72 73 85320-20109-7 DU-2B-20160705

84 84 86320-20109-9 DU-1-20160705

71 70 85320-20109-9 MS DU-1-20160705

75 72 84320-20109-9 MSD DU-1-20160705

75 70 82LCS 320-118487/2-A Lab Control Sample

77 77 85MB 320-118487/1-A Method Blank


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Surrogate Legend

FBP = 2-Fluorobiphenyl (Surr)

NBZ = Nitrobenzene-d5

TPH = Terphenyl-d14

Method: 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM)Prep Type: Total/NAMatrix: Water

Lab Sample ID Client Sample ID (31-107) (20-123) (46-137)

FBP NBZ TPH

90 86 100320-20109-8


DU-5-20160705

100 95 107LCS 320-117570/2-A Lab Control Sample

99 92 98LCSD 320-117570/3-A Lab Control Sample Dup

101 99 111MB 320-117570/1-A Method Blank

Surrogate Legend

FBP = 2-Fluorobiphenyl (Surr)

NBZ = Nitrobenzene-d5

TPH = Terphenyl-d14

Method: 8015B - Diesel Range Organics (DRO) (GC)Prep Type: Total/NAMatrix: Solid


OTPH1

91320-20109-1


DU-3-1-20160705

92320-20109-1 DU-3-1-20160705

89320-20109-1 MS DU-3-1-20160705

97320-20109-1 MSD DU-3-1-20160705

28 X320-20109-2 DU-3-2-20160705

90320-20109-2 DU-3-2-20160705

94320-20109-2 - RE DU-3-2-20160705

97320-20109-3 DU-3-3-20160705

84320-20109-3 DU-3-3-20160705

86320-20109-4 DU-4-20160705

91320-20109-4 DU-4-20160705

90320-20109-5 DU-6-20160705

92320-20109-5 DU-6-20160705

78320-20109-6 DU-2A-20160705

82320-20109-6 DU-2A-20160705

55 X320-20109-7 DU-2B-20160705

16 X320-20109-7 DU-2B-20160705

90320-20109-9 DU-1-20160705

69320-20109-9 DU-1-20160705

117320-20109-9 MS DU-1-20160705

111320-20109-9 MSD DU-1-20160705






Surrogate Legend


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OTPH = o-Terphenyl (Surr)

Method: 8015B - Diesel Range Organics (DRO) (GC)Prep Type: Total/NAMatrix: Water


OTPH1

77320-20109-8


DU-5-20160705


80LCSD 320-117567/3-A Lab Control Sample Dup


Surrogate Legend

OTPH = o-Terphenyl (Surr)


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Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS


RL MDL


-C4-C12

1.12 J 5.0 1.0 mg/Kg 07/12/16 13:24 08/01/16 15:01 1

MB MB



MB MB

Surrogate

07/12/16 13:24




-C4-C12

50.0 47.8 B mg/Kg 96 70 - 130

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

91

LCS LCS




-C4-C12

50.0 48.2 B mg/Kg 96 70 - 130 1 30

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Surrogate

95

LCSD LCSD



RL MDL


-C4-C12

17.7 J 50 15 ug/L 07/14/16 15:18 1

MB MB



MB MB




-C4-C12

1000 918 ug/L 92 78 - 118

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


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Method: 8260B/CA_LUFTMS - Volatile Organic Compounds by GC/MS (Continued)



Surrogate

99

LCS LCS


Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 320-117842/8Matrix: Water Prep Type: Total/NAAnalysis Batch: 117842


-C4-C12

1000 923 ug/L 92 78 - 118 1 23

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Surrogate

96

LCSD LCSD


Client Sample ID: Matrix SpikeLab Sample ID: 320-20046-C-2 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 117842


-C4-C12

1600 B 20000 19500 ug/L 89 78 - 118

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Surrogate

97

MS MS


Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-20046-C-2 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 117842


-C4-C12

1600 B 20000 19700 ug/L 91 78 - 118 1 23

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Surrogate

97

MSD MSD




RL MDL


MB MB








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RL MDL

Benzo[a]pyrene ND 0.050 0.0044 ug/L 07/12/16 16:02 07/21/16 21:33 1

MB MB



ND 0.00550.050 ug/L 07/12/16 16:02 07/21/16 21:33 1Benzo[g,h,i]perylene


ND 0.00400.050 ug/L 07/12/16 16:02 07/21/16 21:33 1Chrysene



ND 0.00400.050 ug/L 07/12/16 16:02 07/21/16 21:33 1Fluorene




ND 0.00420.050 ug/L 07/12/16 16:02 07/21/16 21:33 1Pyrene


MB MB

Surrogate

07/12/16 16:02


99 07/12/16 16:02 07/21/16 21:33 1Nitrobenzene-d5 20 - 123

111 07/12/16 16:02 07/21/16 21:33 1Terphenyl-d14 46 - 137



Analyte

LCS LCS


Spike

Added

%Rec.

Limits



Anthracene 0.250 0.226 ug/L 90 40 - 100






Chrysene 0.250 0.248 ug/L 99 57 - 117



Fluorene 0.250 0.216 ug/L 86 44 - 106


Naphthalene 0.250 0.207 ug/L 83 42 - 105


Pyrene 0.250 0.237 ug/L 95 54 - 114


Surrogate

100

LCS LCS





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Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD



Anthracene 0.250 0.219 ug/L 87 40 - 100 3 30






Chrysene 0.250 0.240 ug/L 96 57 - 117 3 30



Fluorene 0.250 0.214 ug/L 86 44 - 106 1 30


Naphthalene 0.250 0.202 ug/L 81 42 - 105 3 30


Pyrene 0.250 0.231 ug/L 92 54 - 114 2 30


Surrogate

99

LCSD LCSD





RL MDL


MB MB











ND 0.355.0 ug/Kg 07/19/16 11:49 07/25/16 23:52 1Chrysene



ND 0.495.0 ug/Kg 07/19/16 11:49 07/25/16 23:52 1Fluorene




ND 0.355.0 ug/Kg 07/19/16 11:49 07/25/16 23:52 1Pyrene


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MB MB

Surrogate

07/19/16 11:49


77 07/19/16 11:49 07/25/16 23:52 1Nitrobenzene-d5 53 - 113

85 07/19/16 11:49 07/25/16 23:52 1Terphenyl-d14 70 - 144


2-Methylnaphthalene 25.0 16.6 ug/Kg 66 54 - 114

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Acenaphthene 25.0 16.8 ug/Kg 67 51 - 111

Acenaphthylene 25.0 16.0 ug/Kg 64 51 - 111

Anthracene 25.0 16.9 ug/Kg 68 54 - 114

Benzo[a]anthracene 25.0 18.0 ug/Kg 72 66 - 126

Benzo[a]pyrene 25.0 17.3 ug/Kg 69 64 - 124

Benzo[b]fluoranthene 25.0 18.9 ug/Kg 75 65 - 125

Benzo[g,h,i]perylene 25.0 19.4 ug/Kg 78 54 - 134

Benzo[k]fluoranthene 25.0 18.3 ug/Kg 73 69 - 129

Chrysene 25.0 18.6 ug/Kg 75 67 - 127

Dibenz(a,h)anthracene 25.0 19.9 ug/Kg 80 58 - 128

Fluoranthene 25.0 19.4 ug/Kg 77 67 - 127

Fluorene 25.0 16.3 ug/Kg 65 54 - 114

Indeno[1,2,3-cd]pyrene 25.0 19.1 ug/Kg 76 59 - 133

Naphthalene 25.0 16.6 ug/Kg 66 52 - 112

Phenanthrene 25.0 16.6 ug/Kg 66 59 - 119

Pyrene 25.0 19.3 ug/Kg 77 71 - 131


Surrogate

75

LCS LCS




Client Sample ID: DU-1-20160705Lab Sample ID: 320-20109-9 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 119388 Prep Batch: 118487

2-Methylnaphthalene ND 27.6 17.6 ug/Kg 64 54 - 114☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Acenaphthene ND 27.6 17.6 ug/Kg 64 51 - 111☼

Acenaphthylene ND 27.6 16.9 ug/Kg 61 51 - 111☼

Anthracene ND 27.6 19.3 ug/Kg 70 54 - 114☼

Benzo[a]anthracene ND 27.6 18.9 ug/Kg 68 66 - 126☼

Benzo[a]pyrene ND 27.6 18.3 ug/Kg 66 64 - 124☼

Benzo[b]fluoranthene ND 27.6 21.8 ug/Kg 79 65 - 125☼

Benzo[g,h,i]perylene ND 27.6 23.0 ug/Kg 83 54 - 134☼

Benzo[k]fluoranthene ND 27.6 21.2 ug/Kg 77 69 - 129☼

Chrysene ND 27.6 21.0 ug/Kg 76 67 - 127☼

Dibenz(a,h)anthracene ND 27.6 24.2 ug/Kg 88 58 - 128☼


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Fluoranthene ND 27.6 20.5 ug/Kg 74 67 - 127☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Fluorene ND 27.6 18.2 ug/Kg 66 54 - 114☼

Indeno[1,2,3-cd]pyrene ND 27.6 22.9 ug/Kg 83 59 - 133☼

Naphthalene ND 27.6 17.2 ug/Kg 62 52 - 112☼

Phenanthrene ND 27.6 18.3 ug/Kg 66 59 - 119☼

Pyrene ND 27.6 19.9 ug/Kg 72 71 - 131☼


Surrogate

71

MS MS




Client Sample ID: DU-1-20160705Lab Sample ID: 320-20109-9 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 119388 Prep Batch: 118487

2-Methylnaphthalene ND 25.8 17.9 ug/Kg 69 54 - 114 1 30☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Acenaphthene ND 25.8 16.7 ug/Kg 65 51 - 111 5 30☼

Acenaphthylene ND 25.8 17.0 ug/Kg 66 51 - 111 1 30☼

Anthracene ND 25.8 18.0 ug/Kg 70 54 - 114 7 30☼

Benzo[a]anthracene ND 25.8 19.3 ug/Kg 75 66 - 126 2 30☼

Benzo[a]pyrene ND 25.8 18.4 ug/Kg 71 64 - 124 1 30☼

Benzo[b]fluoranthene ND 25.8 19.2 ug/Kg 75 65 - 125 13 30☼

Benzo[g,h,i]perylene ND 25.8 21.8 ug/Kg 84 54 - 134 5 30☼

Benzo[k]fluoranthene ND 25.8 18.2 ug/Kg 71 69 - 129 15 30☼

Chrysene ND 25.8 20.0 ug/Kg 78 67 - 127 5 30☼

Dibenz(a,h)anthracene ND 25.8 22.0 ug/Kg 85 58 - 128 10 30☼

Fluoranthene ND 25.8 20.1 ug/Kg 78 67 - 127 2 30☼

Fluorene ND 25.8 17.7 ug/Kg 69 54 - 114 3 30☼

Indeno[1,2,3-cd]pyrene ND 25.8 21.2 ug/Kg 82 59 - 133 8 30☼

Naphthalene ND 25.8 17.2 ug/Kg 67 52 - 112 0 30☼

Phenanthrene ND 25.8 17.5 ug/Kg 68 59 - 119 4 30☼

Pyrene ND 25.8 19.4 ug/Kg 75 71 - 131 2 30☼


Surrogate

75

MSD MSD





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RL MDL

DRO (C10-C25) ND 50 16 ug/L 07/12/16 15:58 08/07/16 18:40 1

MB MB


ND 170500 ug/L 07/12/16 15:58 08/07/16 18:40 1RRO (C24-C40)

o-Terphenyl (Surr) 85 56 - 145 08/07/16 18:40 1

MB MB

Surrogate

07/12/16 15:58



DRO (C10-C25) 300 198 ug/L 66 53 - 123

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

71

LCS LCS



DRO (C10-C25) 300 224 ug/L 75 53 - 123 12 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Surrogate

80

LCSD LCSD



RL MDL

DRO (C10-C25) 0.516 J 1.0 0.50 mg/Kg 07/18/16 11:09 07/30/16 11:08 1

MB MB


ND 3.85.0 mg/Kg 07/18/16 11:09 07/30/16 11:08 1RRO (C24-C40)

o-Terphenyl (Surr) 73 63 - 141 07/30/16 11:08 1

MB MB

Surrogate

07/18/16 11:09



DRO (C10-C25) 10.0 8.83 mg/Kg 88 67 - 113

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

104

LCS LCS



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RRO (C24-C40) 30.0 21.8 mg/Kg 73 50 - 150

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

68

LCS LCS


Client Sample ID: DU-3-1-20160705Lab Sample ID: 320-20109-1 MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 120305 Prep Batch: 118337

RRO (C24-C40) 15 30.2 41.8 mg/Kg 88 50 - 150

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Surrogate

89

MS MS


Client Sample ID: DU-3-1-20160705Lab Sample ID: 320-20109-1 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 120305 Prep Batch: 118337

RRO (C24-C40) 15 29.8 42.6 mg/Kg 91 50 - 150 2 30

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Surrogate

97

MSD MSD



DRO (C10-C25) 0.63 J B 11.0 11.1 mg/Kg 95 67 - 113☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Surrogate

117

MS MS


Client Sample ID: DU-1-20160705Lab Sample ID: 320-20109-9 MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 121159 Prep Batch: 118337

DRO (C10-C25) 0.63 J B 10.8 10.8 mg/Kg 95 67 - 113 2 30☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Surrogate

111

MSD MSD



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RL MDL

DRO (C10-C25) ND 1.0 0.50 mg/Kg 08/11/16 10:11 08/18/16 15:44 1

MB MB


o-Terphenyl (Surr) 93 63 - 141 08/18/16 15:44 1

MB MB

Surrogate

08/11/16 10:11



DRO (C10-C25) 10.0 8.76 mg/Kg 88 67 - 113

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

98

LCS LCS




RL MDL

Arsenic ND 2.0 1.3 mg/Kg 07/26/16 07:00 07/28/16 12:06 1

MB MB


ND 0.121.0 mg/Kg 07/26/16 07:00 07/28/16 12:06 1Barium

ND 0.0300.20 mg/Kg 07/26/16 07:00 07/28/16 12:06 1Cadmium

ND 0.140.50 mg/Kg 07/26/16 07:00 07/28/16 12:06 1Chromium

ND 0.221.5 mg/Kg 07/26/16 07:00 07/28/16 12:06 1Copper

ND 0.261.0 mg/Kg 07/26/16 07:00 07/28/16 12:06 1Lead

ND 1.42.0 mg/Kg 07/26/16 07:00 07/28/16 12:06 1Selenium

ND 0.0900.50 mg/Kg 07/26/16 07:00 07/28/16 12:06 1Silver

ND 1.05.0 mg/Kg 07/26/16 07:00 07/28/16 12:06 1Strontium

ND 3.010 mg/Kg 07/26/16 07:00 07/28/16 12:06 1Tin

ND 0.221.5 mg/Kg 07/26/16 07:00 07/28/16 12:06 1Titanium

ND 0.192.0 mg/Kg 07/26/16 07:00 07/28/16 12:06 1Zinc


Arsenic 10.0 9.92 mg/Kg 99 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 50.0 49.2 mg/Kg 98 80 - 120

Cadmium 10.0 10.1 mg/Kg 101 80 - 120

Chromium 50.0 50.2 mg/Kg 100 80 - 120

Copper 50.0 49.5 mg/Kg 99 80 - 120

Lead 10.0 10.3 mg/Kg 103 80 - 120

Selenium 10.0 10.6 mg/Kg 106 80 - 120


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Silver 10.0 9.86 mg/Kg 99 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Strontium 50.0 49.4 mg/Kg 99 80 - 120

Tin 50.0 49.8 mg/Kg 100 80 - 120

Titanium 20.0 19.5 mg/Kg 97 80 - 120

Zinc 50.0 50.5 mg/Kg 101 80 - 120


Arsenic 19 5.01 23.5 mg/Kg 85 80 - 120

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 5.1 F1 25.0 24.4 F1 mg/Kg 77 80 - 120

Cadmium 0.048 J F1 5.01 3.79 F1 mg/Kg 75 80 - 120

Chromium 70 25.0 92.1 mg/Kg 87 80 - 120

Copper 11 25.0 32.6 mg/Kg 85 80 - 120

Lead 0.92 J F1 5.01 4.56 F1 mg/Kg 73 80 - 120

Selenium ND 5.01 4.04 mg/Kg 81 80 - 120

Silver ND F1 5.01 3.95 F1 mg/Kg 79 80 - 120

Strontium 1900 25.0 1970 4 mg/Kg 143 80 - 120

Tin ND F1 25.0 17.4 F1 mg/Kg 70 80 - 120

Titanium 600 10.0 617 4 mg/Kg 120 80 - 120

Zinc 31 F1 25.0 49.9 F1 mg/Kg 76 80 - 120


Arsenic 19 5.02 23.8 mg/Kg 89 80 - 120 1 35

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium 5.1 F1 25.1 24.9 F1 mg/Kg 79 80 - 120 2 35

Cadmium 0.048 J F1 5.02 3.83 F1 mg/Kg 75 80 - 120 1 35

Chromium 70 25.1 91.6 mg/Kg 85 80 - 120 1 35

Copper 11 25.1 32.5 mg/Kg 84 80 - 120 0 35

Lead 0.92 J F1 5.02 4.99 mg/Kg 81 80 - 120 9 35

Selenium ND 5.02 4.03 mg/Kg 80 80 - 120 0 35

Silver ND F1 5.02 4.12 mg/Kg 82 80 - 120 4 35

Strontium 1900 25.1 1940 4 mg/Kg 14 80 - 120 2 35

Tin ND F1 25.1 17.8 F1 mg/Kg 71 80 - 120 2 35

Titanium 600 10.0 598 4 mg/Kg -68 80 - 120 3 35

Zinc 31 F1 25.1 49.8 F1 mg/Kg 76 80 - 120 0 35


RL MDL

Arsenic ND 0.020 0.012 mg/L 07/27/16 07:00 07/28/16 17:06 1

MB MB


ND 0.00250.0050 mg/L 07/27/16 07:00 07/28/16 17:06 1Barium


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RL MDL

Cadmium ND 0.0020 0.00050 mg/L 07/27/16 07:00 07/28/16 17:06 1

MB MB


ND 0.00120.0080 mg/L 07/27/16 07:00 07/28/16 17:06 1Chromium

ND 0.00210.010 mg/L 07/27/16 07:00 07/28/16 17:06 1Copper

ND 0.00250.0050 mg/L 07/27/16 07:00 07/28/16 17:06 1Lead

ND 0.0130.020 mg/L 07/27/16 07:00 07/28/16 17:06 1Selenium

ND 0.000840.0050 mg/L 07/27/16 07:00 07/28/16 17:06 1Silver

ND 0.00500.050 mg/L 07/27/16 07:00 07/28/16 17:06 1Strontium

ND 0.00500.020 mg/L 07/27/16 07:00 07/28/16 17:06 1Tin

ND 0.00210.010 mg/L 07/27/16 07:00 07/28/16 17:06 1Titanium

ND 0.00300.010 mg/L 07/27/16 07:00 07/28/16 17:06 1Zinc


Arsenic 0.100 0.0970 mg/L 97 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 0.500 0.495 mg/L 99 80 - 120

Cadmium 0.100 0.100 mg/L 100 80 - 120

Chromium 0.500 0.507 mg/L 101 80 - 120

Copper 0.500 0.496 mg/L 99 80 - 120

Lead 0.100 0.101 mg/L 101 80 - 120

Selenium 0.100 0.102 mg/L 102 80 - 120

Silver 0.100 0.0971 mg/L 97 80 - 120

Strontium 0.500 0.495 mg/L 99 80 - 120

Tin 0.500 0.500 mg/L 100 80 - 120

Titanium 0.200 0.201 mg/L 100 80 - 120

Zinc 0.500 0.502 mg/L 100 80 - 120

Client Sample ID: DU-5-20160705Lab Sample ID: 320-20109-8 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 119908 Prep Batch: 119581

Arsenic ND 0.100 0.101 mg/L 101 80 - 120

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 0.0029 J 0.500 0.498 mg/L 99 80 - 120

Cadmium ND 0.100 0.0985 mg/L 99 80 - 120

Chromium 0.0038 J 0.500 0.495 mg/L 98 80 - 120

Copper ND 0.500 0.502 mg/L 100 80 - 120

Lead ND 0.100 0.100 mg/L 100 80 - 120

Selenium ND 0.100 0.104 mg/L 104 80 - 120

Silver 0.00090 J 0.100 0.0998 mg/L 99 80 - 120

Strontium 0.14 0.500 0.633 mg/L 99 80 - 120

Tin ND 0.500 0.498 mg/L 100 80 - 120

Titanium 0.068 F1 0.200 0.241 mg/L 86 80 - 120

Zinc ND 0.500 0.490 mg/L 98 80 - 120


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Client Sample ID: DU-5-20160705Lab Sample ID: 320-20109-8 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 119908 Prep Batch: 119581

Arsenic ND 0.100 0.0919 mg/L 92 80 - 120 9 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium 0.0029 J 0.500 0.450 mg/L 89 80 - 120 10 20

Cadmium ND 0.100 0.0896 mg/L 90 80 - 120 10 20

Chromium 0.0038 J 0.500 0.451 mg/L 89 80 - 120 9 20

Copper ND 0.500 0.454 mg/L 91 80 - 120 10 20

Lead ND 0.100 0.0927 mg/L 93 80 - 120 8 20

Selenium ND 0.100 0.0947 mg/L 95 80 - 120 9 20

Silver 0.00090 J 0.100 0.0922 mg/L 91 80 - 120 8 20

Strontium 0.14 0.500 0.568 mg/L 87 80 - 120 11 20

Tin ND 0.500 0.449 mg/L 90 80 - 120 10 20

Titanium 0.068 F1 0.200 0.221 F1 mg/L 77 80 - 120 8 20

Zinc ND 0.500 0.446 mg/L 89 80 - 120 9 20



RL MDL

Mercury ND 0.00020 0.00010 mg/L 07/20/16 08:34 07/20/16 12:17 1

MB MB



Mercury 0.00100 0.00103 mg/L 103 82 - 113

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Matrix SpikeLab Sample ID: 320-20190-A-1-B MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 118718 Prep Batch: 117503

Mercury ND 0.00100 0.00102 mg/L 102 82 - 113

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-20190-A-1-C MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 118718 Prep Batch: 117503

Mercury ND 0.00100 0.00104 mg/L 104 82 - 113 2 17

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


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RL MDL

Mercury ND 0.040 0.0086 mg/Kg 07/26/16 18:20 07/27/16 13:42 1

MB MB



Mercury 0.0833 0.0850 mg/Kg 102 86 - 114

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Matrix SpikeLab Sample ID: 320-20107-A-6-L MSMatrix: Solid Prep Type: Total/NAAnalysis Batch: 119738 Prep Batch: 119509

Mercury 0.013 J 0.167 0.169 mg/Kg 93 86 - 114☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 320-20107-A-6-M MSDMatrix: Solid Prep Type: Total/NAAnalysis Batch: 119738 Prep Batch: 119509

Mercury 0.013 J 0.169 0.171 mg/Kg 93 86 - 114 1 17☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Method: D 2216 - Percent Moisture

Client Sample ID: DuplicateLab Sample ID: 660-74532-A-6 DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 118572

Percent Moisture 14.9 14.6 % 2 20

Analyte

DU DU

DUnitResult Qualifier

Sample

Result

Sample

Qualifier LimitRPD

RPD


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GC/MS VOA

Prep Batch: 117535


Solid 5035320-20109-1 DU-3-1-20160705 Total/NA

Solid 5035320-20109-2 DU-3-2-20160705 Total/NA

Solid 5035320-20109-3 DU-3-3-20160705 Total/NA

Solid 5035320-20109-4 DU-4-20160705 Total/NA

Solid 5035320-20109-5 DU-6-20160705 Total/NA

Solid 5035320-20109-6 DU-2A-20160705 Total/NA

Solid 5035320-20109-7 DU-2B-20160705 Total/NA

Solid 5035320-20109-9 DU-1-20160705 Total/NA

Solid 5035MB 320-117535/3-A Method Blank Total/NA

Solid 5035LCS 320-117535/1-A Lab Control Sample Total/NA

Solid 5035LCSD 320-117535/2-A Lab Control Sample Dup Total/NA



Solid 8260B/CA_LUFT

MS

117535320-20109-1 DU-3-1-20160705 Total/NA

Solid 8260B/CA_LUFT

MS

117535320-20109-2 DU-3-2-20160705 Total/NA

Solid 8260B/CA_LUFT

MS

117535320-20109-3 DU-3-3-20160705 Total/NA

Solid 8260B/CA_LUFT

MS

117535320-20109-4 DU-4-20160705 Total/NA

Solid 8260B/CA_LUFT

MS

117535320-20109-5 DU-6-20160705 Total/NA

Solid 8260B/CA_LUFT

MS

117535320-20109-6 DU-2A-20160705 Total/NA

Solid 8260B/CA_LUFT

MS

117535320-20109-7 DU-2B-20160705 Total/NA

Water 8260B/CA_LUFT

MS

320-20109-8 DU-5-20160705 Total/NA

Solid 8260B/CA_LUFT

MS

117535320-20109-9 DU-1-20160705 Total/NA

Water 8260B/CA_LUFT

MS

MB 320-117842/10 Method Blank Total/NA

Water 8260B/CA_LUFT

MS

LCS 320-117842/7 Lab Control Sample Total/NA

Water 8260B/CA_LUFT

MS

LCSD 320-117842/8 Lab Control Sample Dup Total/NA

Water 8260B/CA_LUFT

MS

320-20046-C-2 MS Matrix Spike Total/NA

Water 8260B/CA_LUFT

MS

320-20046-C-2 MSD Matrix Spike Duplicate Total/NA



Solid 8260B/CA_LUFT

MS

117535MB 320-117535/3-A Method Blank Total/NA

Solid 8260B/CA_LUFT

MS

117535LCS 320-117535/1-A Lab Control Sample Total/NA

Solid 8260B/CA_LUFT

MS

117535LCSD 320-117535/2-A Lab Control Sample Dup Total/NA


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GC/MS Semi VOA



Solid Increment, Prep320-20109-1 DU-3-1-20160705 Total/NA



Solid Increment, Prep320-20109-4 DU-4-20160705 Total/NA


Solid Increment, Prep320-20109-6 DU-2A-20160705 Total/NA

Solid Increment, Prep320-20109-7 DU-2B-20160705 Total/NA


Solid Increment, Prep320-20109-9 MS DU-1-20160705 Total/NA

Solid Increment, Prep320-20109-9 MSD DU-1-20160705 Total/NA

Prep Batch: 117570


Water 3510C320-20109-8 DU-5-20160705 Total/NA




Prep Batch: 118487


Solid 3550B 117428320-20109-1 DU-3-1-20160705 Total/NA



Solid 3550B 117428320-20109-4 DU-4-20160705 Total/NA


Solid 3550B 117428320-20109-6 DU-2A-20160705 Total/NA

Solid 3550B 117428320-20109-7 DU-2B-20160705 Total/NA




Solid 3550B 117428320-20109-9 MS DU-1-20160705 Total/NA

Solid 3550B 117428320-20109-9 MSD DU-1-20160705 Total/NA



Water 8270C SIM 117570320-20109-8 DU-5-20160705 Total/NA

Water 8270C SIM 117570MB 320-117570/1-A Method Blank Total/NA

Water 8270C SIM 117570LCS 320-117570/2-A Lab Control Sample Total/NA

Water 8270C SIM 117570LCSD 320-117570/3-A Lab Control Sample Dup Total/NA



Solid 8270C SIM 118487320-20109-1 DU-3-1-20160705 Total/NA



Solid 8270C SIM 118487320-20109-4 DU-4-20160705 Total/NA


Solid 8270C SIM 118487320-20109-6 DU-2A-20160705 Total/NA

Solid 8270C SIM 118487320-20109-7 DU-2B-20160705 Total/NA


Solid 8270C SIM 118487MB 320-118487/1-A Method Blank Total/NA


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Analysis Batch: 119388 (Continued)


Solid 8270C SIM 118487320-20109-9 MS DU-1-20160705 Total/NA

Solid 8270C SIM 118487320-20109-9 MSD DU-1-20160705 Total/NA



Solid 8270C SIM 118487LCS 320-118487/2-A Lab Control Sample Total/NA

GC Semi VOA





Solid Increment, Prep320-20109-2 - RE DU-3-2-20160705 Total/NA







Solid Increment, Prep320-20109-9 MS DU-1-20160705 Total/NA

Solid Increment, Prep320-20109-9 MSD DU-1-20160705 Total/NA

Prep Batch: 117567


Water 3510C320-20109-8 DU-5-20160705 Total/NA






Solid Increment, prep320-20109-1 DU-3-1-20160705 Total/NA



Solid Increment, prep320-20109-4 DU-4-20160705 Total/NA


Solid Increment, prep320-20109-6 DU-2A-20160705 Total/NA

Solid Increment, prep320-20109-7 DU-2B-20160705 Total/NA


Solid Increment, prep320-20109-1 MS DU-3-1-20160705 Total/NA

Solid Increment, prep320-20109-1 MSD DU-3-1-20160705 Total/NA

Prep Batch: 118337








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Solid 3550B 117636320-20109-1 MS DU-3-1-20160705 Total/NA

Solid 3550B 117636320-20109-1 MSD DU-3-1-20160705 Total/NA




























Water 8015B 117567320-20109-8 DU-5-20160705 Total/NA





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Prep Batch: 121672


Solid 3550B 117428320-20109-2 - RE DU-3-2-20160705 Total/NA





Solid 8015B 121672320-20109-2 - RE DU-3-2-20160705 Total/NA



Metals













Solid Increment, Prep320-20107-A-6-L MS Matrix Spike Total/NA

Solid Increment, Prep320-20107-A-6-M MSD Matrix Spike Duplicate Total/NA

Prep Batch: 117503


Water 7470A320-20109-8 DU-5-20160705 Total/NA



Water 7470A320-20190-A-1-B MS Matrix Spike Total/NA

Water 7470A320-20190-A-1-C MSD Matrix Spike Duplicate Total/NA






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Metals (Continued)






Solid Increment, prep320-20109-6 DU-2A-20160705 Total/NA

Solid Increment, prep320-20109-7 DU-2B-20160705 Total/NA


Solid Increment, prep320-20109-1 MS DU-3-1-20160705 Total/NA

Solid Increment, prep320-20109-1 MSD DU-3-1-20160705 Total/NA



Water 7470A 117503320-20109-8 DU-5-20160705 Total/NA

Water 7470A 117503MB 320-117503/25-A Method Blank Total/NA

Water 7470A 117503LCS 320-117503/26-A Lab Control Sample Total/NA

Water 7470A 117503320-20190-A-1-B MS Matrix Spike Total/NA

Water 7470A 117503320-20190-A-1-C MSD Matrix Spike Duplicate Total/NA

Prep Batch: 119391














Prep Batch: 119509


Solid 7471A 117428320-20109-1 DU-3-1-20160705 Total/NA



Solid 7471A 117428320-20109-4 DU-4-20160705 Total/NA


Solid 7471A 117428320-20109-6 DU-2A-20160705 Total/NA

Solid 7471A 117428320-20109-7 DU-2B-20160705 Total/NA


Solid 7471AMB 320-119509/11-A Method Blank Total/NA

Solid 7471ALCS 320-119509/12-A Lab Control Sample Total/NA

Solid 7471A 117435320-20107-A-6-L MS Matrix Spike Total/NA

Solid 7471A 117435320-20107-A-6-M MSD Matrix Spike Duplicate Total/NA

Prep Batch: 119581


Water 3010A320-20109-8 DU-5-20160705 Total/NA



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Metals (Continued)




Water 3010A320-20109-8 MS DU-5-20160705 Total/NA

Water 3010A320-20109-8 MSD DU-5-20160705 Total/NA

















Solid 7471A 119509320-20109-6 DU-2A-20160705 Total/NA

Solid 7471A 119509320-20109-7 DU-2B-20160705 Total/NA


Solid 7471A 119509MB 320-119509/11-A Method Blank Total/NA

Solid 7471A 119509LCS 320-119509/12-A Lab Control Sample Total/NA

Solid 7471A 119509320-20107-A-6-L MS Matrix Spike Total/NA

Solid 7471A 119509320-20107-A-6-M MSD Matrix Spike Duplicate Total/NA




Water 6010B 119581320-20109-8 DU-5-20160705 Total/NA







Water 6010B 119581320-20109-8 MS DU-5-20160705 Total/NA

Water 6010B 119581320-20109-8 MSD DU-5-20160705 Total/NA

General Chemistry








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General Chemistry (Continued)









Solid D 2216 117428320-20109-1 DU-3-1-20160705 Total/NA



Solid D 2216 117428320-20109-4 DU-4-20160705 Total/NA


Solid D 2216 117428320-20109-6 DU-2A-20160705 Total/NA

Solid D 2216 117428320-20109-7 DU-2B-20160705 Total/NA


Solid D 2216660-74532-A-6 DU Duplicate Total/NA


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Client Sample ID: DU-3-1-20160705 Lab Sample ID: 320-20109-1Matrix: SolidDate Collected: 07/05/16 09:30


Prep 5035 FRD07/12/16 13:24 TAL SAC117535

Type

Batch

Method

Batch

Prep Type LabAnalystRun

Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 132.54 g 150 mL

Analysis 8260B/CA_LUFTM

S

1 117842 07/14/16 18:26 SS TAL SACTotal/NA 1 mL 50 mL

ISM Prep Increment, prep 117636 07/13/16 08:18 VY1 TAL SACTotal/NA

Prep 3550B 118337 07/18/16 11:09 M1A TAL SACTotal/NA 30.22 g 3 mL

Analysis 8015B 1 120305 08/01/16 14:32 HKP TAL SACTotal/NA


Prep 3050B 119391 07/26/16 07:00 NIM TAL SACTotal/NA 9.99 g 500 mL

Analysis 6010B 2 119908 07/28/16 12:12 TWR TAL SACTotal/NA

ISM Prep Increment, Prep 117428 07/12/16 08:17 VY1 TAL SACTotal/NA

Analysis D 2216 1 118572 07/19/16 18:15 EP1 TAL SACTotal/NA



ISM Prep Increment, Prep VY107/12/16 08:17 TAL SAC117428

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA


Analysis 8270C SIM 1 119388 07/26/16 00:50 MEO TAL SACTotal/NA





Prep 7471A 119509 07/26/16 18:20 SFM TAL SACTotal/NA 10.09 g 500 mL

Analysis 7471A 1 119738 07/27/16 14:09 SFM TAL SACTotal/NA



Prep 5035 FRD07/12/16 13:24 TAL SAC117535

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil



S











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Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA






ISM Prep Increment, Prep RE 117428 07/12/16 08:17 VY1 TAL SACTotal/NA

Prep 3550B RE 121672 08/11/16 10:11 NGK TAL SACTotal/NA 30.67 g 3 mL

Analysis 8015B RE 1 122880 08/18/16 16:23 RS1 TAL SACTotal/NA






Prep 5035 FRD07/12/16 13:24 TAL SAC117535

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil



S













Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA










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Client Sample ID: DU-4-20160705 Lab Sample ID: 320-20109-4Matrix: SolidDate Collected: 07/05/16 10:40


Prep 5035 FRD07/12/16 13:24 TAL SAC117535

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil



S













Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA











Prep 5035 FRD07/12/16 13:24 TAL SAC117535

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil



S











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Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA









Client Sample ID: DU-2A-20160705 Lab Sample ID: 320-20109-6Matrix: SolidDate Collected: 07/05/16 11:30


Prep 5035 FRD07/12/16 13:24 TAL SAC117535

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil



S













Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA





Analysis 8015B 1 121363 08/09/16 14:00 AVM TAL SACTotal/NA





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Client Sample ID: DU-2B-20160705 Lab Sample ID: 320-20109-7Matrix: SolidDate Collected: 07/05/16 11:45


Prep 5035 FRD07/12/16 13:24 TAL SAC117535

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil



S













Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA









Client Sample ID: DU-5-20160705 Lab Sample ID: 320-20109-8Matrix: WaterDate Collected: 07/05/16 12:30



S

SS07/14/16 21:261 TAL SAC117842

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA 50 mL 50 mL

Prep 3510C 117570 07/12/16 16:02 NGK TAL SACTotal/NA 874.2 mL 1 mL

Analysis 8270C SIM 1 118918 07/21/16 23:01 ONL TAL SACTotal/NA

Prep 3510C 117567 07/12/16 15:58 SJR TAL SACTotal/NA 900.5 mL 3 mL


Prep 3010A 119581 07/27/16 07:00 NIM TAL SACTotal/NA 50 mL 50 mL


Prep 7470A 117503 07/20/16 08:34 SFM TAL SACTotal/NA 30 mL 30 mL



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Prep 5035 FRD07/12/16 13:24 TAL SAC117535

Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil



S













Type

Batch

Method

Batch


Prepared

or Analyzed

Initial

Amount Amount

Final Batch

NumberFactor

Dil

Total/NA












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Laboratory: TestAmerica SacramentoAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.


A2LA 2928-01DoD ELAP 01-31-17

Alaska (UST) State Program 10 UST-055 12-18-16


Arkansas DEQ State Program 6 88-0691 06-17-17


Colorado State Program 8 CA00044 08-31-16

Connecticut State Program 1 PH-0691 06-30-17

Florida NELAP 4 E87570 06-30-17


Illinois NELAP 5 200060 03-17-17

Kansas NELAP 7 E-10375 08-31-17

Louisiana NELAP 6 30612 06-30-17

Maine State Program 1 CA0004 04-18-18

Michigan State Program 5 9947 01-31-18

Nevada State Program 9 CA00044 07-31-17

New Jersey NELAP 2 CA005 06-30-17

New York NELAP 2 11666 04-01-17

Oregon NELAP 10 4040 01-29-17

Pennsylvania NELAP 3 68-01272 03-31-17

Texas NELAP 6 T104704399 07-31-17


USDA Federal P330-11-00436 12-30-17

USEPA UCMR Federal 1 CA00044 11-06-16

Utah NELAP 8 CA00044 02-28-17

Virginia NELAP 3 460278 03-14-17


West Virginia (DW) State Program 3 9930C 12-31-16

Wyoming State Program 8 8TMS-L 01-29-17







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Method SummaryTestAmerica Job ID: 320-20109-1Client: Element Environmental, LLC


Method Method Description LaboratoryProtocol

SW8468260B/CA_LUFTM

S

Volatile Organic Compounds by GC/MS TAL SAC

SW8468270C SIM Semivolatile Organic Compounds (GC/MS SIM) TAL SAC

SW8468015B Diesel Range Organics (DRO) (GC) TAL SAC

SW8466010B Metals (ICP) TAL SAC



ASTMD 2216 Percent Moisture TAL SAC

Protocol References:

ASTM = ASTM International

SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.




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320-20109-1 DU-3-1-20160705 Solid 07/05/16 09:30 07/08/16 09:20

320-20109-2 DU-3-2-20160705 Solid 07/05/16 09:45 07/08/16 09:20

320-20109-3 DU-3-3-20160705 Solid 07/05/16 10:00 07/08/16 09:20

320-20109-4 DU-4-20160705 Solid 07/05/16 10:40 07/08/16 09:20

320-20109-5 DU-6-20160705 Solid 07/05/16 11:00 07/08/16 09:20

320-20109-6 DU-2A-20160705 Solid 07/05/16 11:30 07/08/16 09:20

320-20109-7 DU-2B-20160705 Solid 07/05/16 11:45 07/08/16 09:20

320-20109-8 DU-5-20160705 Water 07/05/16 12:30 07/08/16 09:20

320-20109-9 DU-1-20160705 Solid 07/05/16 13:20 07/08/16 09:20


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Login Number: 20109


Creator: Turpen, Troy

List Source: TestAmerica Sacramento

List Number: 1

N/ARadioactivity wasn't checked or is </= background as measured by a survey meter.

TrueThe cooler's custody seal, if present, is intact. Seal






TrueCOC is present.




FalseThere are no discrepancies between the containers received and the COC. Refer to Job Narrative for details.














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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Seattle5755 8th Street EastTacoma, WA 98424Tel: (253)922-2310



Attn: Matt Neal





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Table of Contents



Page 2 of 53TestAmerica Seattle

8/22/2016

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1


Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5



Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38


Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46


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Job ID: 580-61481-1

Laboratory: TestAmerica Seattle

Narrative


Comments


Receipt

The samples were received on 8/3/2016 9:40 AM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 2.9º C.

GC/MS VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

GC/MS Semi VOA Method(s) 8270C SIM: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch 440-348082 and analytical batch 440-348390. The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch.


GC VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

GC Semi VOA Method(s) 8015B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries and precision for preparation batch 580-224304 and 580-224734 and analytical batch 580-224710 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample / laboratory sample control duplicate (LCS/LCSD) precision was within

acceptance limits.

Method(s) 8015B: The following samples contained a hydrocarbon pattern in the diesel range; however, the elution pattern was later than the typical diesel fuel pattern used by the laboratory for quantitative purposes: DU-3-1-20160801 (580-61481-1), DU-3-2-20160801 (580-61481-2) and DU-3-3-20160801 (580-61481-3).

Method(s) 8015B: The continuing calibration verification (CCV) associated with batch 440-348086 recovered above the upper control limit

for C10-C28. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. The following sample is impacted: (CCV 440-348086/35).


preparation batch 440-347843 and analytical batch 440-348086.The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch.


Metals



Organic Prep Method(s) 3510C: The following sample was prepared outside of preparation holding time due to oversight by the lab. The sample status

was at "Shipd" until 8/9/16 which is one day after holding time had expired. Sample was extracted on 8/9/16. DU-5-20160801 (580-61481-8).

Method(s) 3520C: The following sample(s) was received with less than 2 days remaining on the holding time or less than one shift (8

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Laboratory: TestAmerica Seattle (Continued)

hours) remaining on a test with a holding time of 48 hours or less. As such, the laboratory had insufficient time remaining to perform the

analysis within holding time: 3520C/8270_SIM PAH DU-5-20160801 (580-61481-8).


VOA Prep



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Qualifiers

GC/MS Semi VOA



Qualifier

GC Semi VOA



Qualifier

F2 MS/MSD RPD exceeds control limits



Metals



applicable.

Qualifier


Glossary



Abbreviation

%R Percent Recovery












NC Not Calculated



QC Quality Control






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GRO (C4-C12) ND 10 7.0 mg/Kg 08/01/16 09:00 08/08/16 14:43 100




Dibromofluoromethane (Surr) 87 08/01/16 09:00 08/08/16 14:43 10055 - 140

Toluene-d8 (Surr) 107 08/01/16 09:00 08/08/16 14:43 10060 - 140













1.8 0.55 ug/Kg 08/11/16 14:46 08/13/16 18:55 1☼Chrysene ND



1.8 0.18 ug/Kg 08/11/16 14:46 08/13/16 18:55 1☼Fluorene ND




1.8 0.36 ug/Kg 08/11/16 14:46 08/13/16 18:55 1☼Pyrene ND

Terphenyl-d14 110 68 - 138 08/11/16 14:46 08/13/16 18:55 1



HI Diesel Range Organics (>C12-C24) ND 9.1 4.5 mg/Kg ☼ 08/12/16 08:19 08/12/16 21:12 1


16 4.6 mg/Kg 08/12/16 08:19 08/13/16 01:22 1HI Residual Range Organics (>C24-C32)

20 F1 F2

o-Terphenyl (Surr) 77 37 - 127 08/12/16 08:19 08/12/16 21:12 1


o-Terphenyl (Surr) 77 08/12/16 08:19 08/13/16 01:22 137 - 127


Arsenic 23 5.8 0.62 mg/Kg 08/11/16 11:47 08/11/16 16:37 4


0.97 0.087 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Barium 4.8

1.9 0.095 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Cadmium 0.52 J

2.5 0.36 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Chromium 85

4.8 1.4 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Copper 15

2.9 0.19 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Lead 0.79 J

9.7 0.39 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Selenium 1.2 J

4.8 1.1 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Silver ND

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Strontium 2400 9.7 0.78 mg/Kg 08/11/16 11:47 08/11/16 16:37 4


9.7 0.20 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Tin 0.47 J

2.9 0.46 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Titanium 480

3.9 0.62 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Zinc 39


Mercury ND 0.013 0.0040 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:15 1





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GRO (C4-C12) ND 9.8 6.9 mg/Kg 08/01/16 09:15 08/08/16 15:13 100





Toluene-d8 (Surr) 106 08/01/16 09:15 08/08/16 15:13 10060 - 140













1.8 0.55 ug/Kg 08/11/16 14:46 08/13/16 20:11 1☼Chrysene ND



1.8 0.18 ug/Kg 08/11/16 14:46 08/13/16 20:11 1☼Fluorene ND




1.8 0.35 ug/Kg 08/11/16 14:46 08/13/16 20:11 1☼Pyrene ND

Terphenyl-d14 120 68 - 138 08/11/16 14:46 08/13/16 20:11 1






21

o-Terphenyl (Surr) 78 37 - 127 08/12/16 08:19 08/12/16 22:20 1


o-Terphenyl (Surr) 79 08/12/16 08:19 08/13/16 01:45 137 - 127


Arsenic 23 5.9 0.63 mg/Kg 08/11/16 11:47 08/11/16 16:56 4


0.99 0.089 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Barium 5.1

2.0 0.097 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Cadmium 0.77 J

2.6 0.36 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Chromium 89

4.9 1.4 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Copper 16

3.0 0.19 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Lead 0.64 J

9.9 0.40 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Selenium 1.2 J

4.9 1.1 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Silver ND

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Strontium 2300 9.9 0.79 mg/Kg 08/11/16 11:47 08/11/16 16:56 4


9.9 0.21 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Tin 0.38 J

3.0 0.47 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Titanium 600

4.0 0.63 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Zinc 42


Mercury ND 0.014 0.0041 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:22 1





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GRO (C4-C12) ND 8.7 6.1 mg/Kg 08/01/16 09:30 08/08/16 15:44 100





Toluene-d8 (Surr) 107 08/01/16 09:30 08/08/16 15:44 10060 - 140













1.8 0.55 ug/Kg 08/11/16 14:46 08/13/16 20:37 1☼Chrysene ND



1.8 0.18 ug/Kg 08/11/16 14:46 08/13/16 20:37 1☼Fluorene ND




1.8 0.36 ug/Kg 08/11/16 14:46 08/13/16 20:37 1☼Pyrene ND

Terphenyl-d14 115 68 - 138 08/11/16 14:46 08/13/16 20:37 1






27

o-Terphenyl (Surr) 70 37 - 127 08/12/16 08:19 08/12/16 22:43 1


o-Terphenyl (Surr) 79 08/12/16 08:19 08/13/16 02:08 137 - 127


Arsenic 23 6.0 0.64 mg/Kg 08/11/16 11:47 08/11/16 17:01 4


1.0 0.090 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Barium 5.6

2.0 0.098 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Cadmium 0.76 J

2.6 0.37 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Chromium 94

5.0 1.4 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Copper 16

3.0 0.19 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Lead 0.40 J

10 0.40 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Selenium ND

5.0 1.1 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Silver ND

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Strontium 2300 10 0.80 mg/Kg 08/11/16 11:47 08/11/16 17:01 4


10 0.21 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Tin 0.41 J

3.0 0.47 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Titanium 670

4.0 0.64 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Zinc 43


Mercury ND 0.014 0.0041 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:25 1





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GRO (C4-C12) ND 9.2 6.4 mg/Kg 08/01/16 09:45 08/08/16 16:14 100





Toluene-d8 (Surr) 107 08/01/16 09:45 08/08/16 16:14 10060 - 140













1.9 0.56 ug/Kg 08/11/16 14:46 08/13/16 21:02 1☼Chrysene ND



1.9 0.19 ug/Kg 08/11/16 14:46 08/13/16 21:02 1☼Fluorene ND




1.9 0.36 ug/Kg 08/11/16 14:46 08/13/16 21:02 1☼Pyrene ND

Terphenyl-d14 102 68 - 138 08/11/16 14:46 08/13/16 21:02 1





16 4.6 mg/Kg 08/12/16 08:19 08/13/16 02:31 1HI Residual Range Organics

(>C24-C32)

ND

o-Terphenyl (Surr) 72 37 - 127 08/12/16 08:19 08/12/16 23:06 1


o-Terphenyl (Surr) 77 08/12/16 08:19 08/13/16 02:31 137 - 127


Arsenic 23 5.8 0.62 mg/Kg 08/11/16 11:47 08/11/16 17:11 4


0.97 0.087 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Barium 5.1

1.9 0.095 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Cadmium 0.74 J

2.5 0.36 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Chromium 84

4.9 1.4 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Copper 15

2.9 0.19 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Lead 0.55 J

9.7 0.39 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Selenium 1.2 J

4.9 1.1 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Silver ND

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Strontium 2500 9.7 0.78 mg/Kg 08/11/16 11:47 08/11/16 17:11 4


9.7 0.20 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Tin 0.25 J

2.9 0.46 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Titanium 590

3.9 0.62 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Zinc 40


Mercury ND 0.014 0.0041 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:27 1





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GRO (C4-C12) ND 8.8 6.2 mg/Kg 08/01/16 11:00 08/08/16 16:44 100





Toluene-d8 (Surr) 103 08/01/16 11:00 08/08/16 16:44 10060 - 140













1.9 0.57 ug/Kg 08/11/16 14:46 08/13/16 21:28 1☼Chrysene ND



1.9 0.19 ug/Kg 08/11/16 14:46 08/13/16 21:28 1☼Fluorene ND




1.9 0.37 ug/Kg 08/11/16 14:46 08/13/16 21:28 1☼Pyrene ND

Terphenyl-d14 106 68 - 138 08/11/16 14:46 08/13/16 21:28 1



HI Diesel Range Organics (>C12-C24) ND 10 4.9 mg/Kg ☼ 08/12/16 08:19 08/12/16 23:29 1



4.6 J

o-Terphenyl (Surr) 72 37 - 127 08/12/16 08:19 08/12/16 23:29 1


o-Terphenyl (Surr) 83 08/12/16 08:19 08/13/16 02:53 137 - 127


Arsenic 22 5.9 0.63 mg/Kg 08/11/16 11:47 08/11/16 17:15 4


0.98 0.088 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Barium 5.1

2.0 0.096 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Cadmium 0.73 J

2.5 0.36 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Chromium 88

4.9 1.4 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Copper 15

2.9 0.19 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Lead 0.40 J

9.8 0.39 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Selenium 0.97 J

4.9 1.1 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Silver ND

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Strontium 2400 9.8 0.78 mg/Kg 08/11/16 11:47 08/11/16 17:15 4


9.8 0.21 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Tin 0.37 J

2.9 0.46 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Titanium 550

3.9 0.63 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Zinc 39


Mercury ND 0.014 0.0042 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:29 1





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GRO (C4-C12) ND 9.2 6.5 mg/Kg 08/01/16 11:30 08/08/16 17:15 100





Toluene-d8 (Surr) 105 08/01/16 11:30 08/08/16 17:15 10060 - 140







1.9 0.22 ug/Kg 08/11/16 14:46 08/13/16 21:53 1☼Anthracene 2.0






1.9 0.56 ug/Kg 08/11/16 14:46 08/13/16 21:53 1☼Chrysene ND



1.9 0.19 ug/Kg 08/11/16 14:46 08/13/16 21:53 1☼Fluorene ND




1.9 0.36 ug/Kg 08/11/16 14:46 08/13/16 21:53 1☼Pyrene ND

Terphenyl-d14 96 68 - 138 08/11/16 14:46 08/13/16 21:53 1






(>C24-C32)

ND

o-Terphenyl (Surr) 63 37 - 127 08/12/16 08:19 08/13/16 00:14 1


o-Terphenyl (Surr) 80 08/12/16 08:19 08/13/16 03:16 137 - 127


Arsenic 27 5.9 0.63 mg/Kg 08/11/16 11:47 08/11/16 17:19 4


0.99 0.089 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Barium 4.9

2.0 0.097 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Cadmium 0.60 J

2.6 0.36 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Chromium 66

4.9 1.4 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Copper 15

3.0 0.19 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Lead 0.79 J

9.9 0.40 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Selenium ND

4.9 1.1 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Silver ND

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Strontium 2700 9.9 0.79 mg/Kg 08/11/16 11:47 08/11/16 17:19 4


9.9 0.21 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Tin ND

3.0 0.47 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Titanium 540

4.0 0.63 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Zinc 32


Mercury ND 0.014 0.0042 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:32 1





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GRO (C4-C12) ND 9.9 7.0 mg/Kg 08/01/16 11:45 08/08/16 17:45 100





Toluene-d8 (Surr) 108 08/01/16 11:45 08/08/16 17:45 10060 - 140













1.8 0.53 ug/Kg 08/11/16 14:46 08/13/16 22:19 1☼Chrysene ND



1.8 0.18 ug/Kg 08/11/16 14:46 08/13/16 22:19 1☼Fluorene ND




1.8 0.34 ug/Kg 08/11/16 14:46 08/13/16 22:19 1☼Pyrene ND

Terphenyl-d14 117 68 - 138 08/11/16 14:46 08/13/16 22:19 1






(>C24-C32)

ND

o-Terphenyl (Surr) 76 37 - 127 08/12/16 08:19 08/13/16 00:37 1


o-Terphenyl (Surr) 80 08/12/16 08:22 08/13/16 03:38 137 - 127


Arsenic 26 5.9 0.63 mg/Kg 08/11/16 11:47 08/11/16 17:24 4


0.99 0.089 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Barium 4.6

2.0 0.097 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Cadmium 0.60 J

2.6 0.36 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Chromium 75

5.0 1.4 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Copper 14

3.0 0.19 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Lead 0.40 J

9.9 0.40 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Selenium 0.68 J

5.0 1.1 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Silver ND

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Strontium 2600 9.9 0.79 mg/Kg 08/11/16 11:47 08/11/16 17:24 4


9.9 0.21 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Tin 0.29 J

3.0 0.47 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Titanium 480

4.0 0.64 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Zinc 35


Mercury ND 0.014 0.0042 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:06 1





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1-Methylnaphthalene ND H 0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1


0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 12-Methylnaphthalene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Acenaphthene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Acenaphthylene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Anthracene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Benzo[a]anthracene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Benzo[a]pyrene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Benzo[b]fluoranthene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Benzo[g,h,i]perylene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Benzo[k]fluoranthene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Chrysene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Dibenz(a,h)anthracene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Fluoranthene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Fluorene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Indeno[1,2,3-cd]pyrene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Naphthalene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Phenanthrene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Pyrene ND H



Nitrobenzene-d5 66 08/10/16 09:36 08/11/16 22:14 146 - 109

Terphenyl-d14 62 08/10/16 09:36 08/11/16 22:14 128 - 124



-C4-C12

ND 50 25 ug/L 08/10/16 06:41 1





DRO (C9-C25) ND H 0.50 0.10 mg/L 08/09/16 13:20 08/10/16 20:18 1


0.50 0.10 mg/L 08/09/16 13:20 08/10/16 20:18 1RRO (C24-C40) ND H

n-Octacosane 51 45 - 120 08/09/16 13:20 08/10/16 20:18 1



Arsenic ND 0.010 0.0050 mg/L 08/18/16 09:05 08/20/16 16:15 1


0.010 0.0050 mg/L 08/18/16 09:05 08/19/16 00:11 1Barium 0.0079 J

0.0050 0.0020 mg/L 08/18/16 09:05 08/19/16 00:11 1Cadmium ND

0.0050 0.0025 mg/L 08/18/16 09:05 08/19/16 00:11 1Chromium 0.031

0.010 0.0050 mg/L 08/18/16 09:05 08/19/16 00:11 1Copper 0.0069 J

0.0050 0.0025 mg/L 08/18/16 09:05 08/19/16 00:11 1Lead ND

0.010 0.0061 mg/L 08/18/16 09:05 08/19/16 00:11 1Selenium ND

0.010 0.0050 mg/L 08/18/16 09:05 08/19/16 00:11 1Silver ND

0.020 0.010 mg/L 08/18/16 09:05 08/19/16 00:11 1Strontium 0.031

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Method: 6010B - Metals (ICP) - Total Recoverable (Continued)RL MDL

Tin ND 0.10 0.012 mg/L 08/18/16 09:05 08/19/16 00:11 1


0.0050 0.0025 mg/L 08/18/16 09:05 08/19/16 00:11 1Titanium 0.53

0.020 0.010 mg/L 08/18/16 09:05 08/19/16 00:11 1Zinc ND


Mercury ND 0.00020 0.00010 mg/L 08/09/16 19:08 08/10/16 16:35 1


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GRO (C4-C12) ND 9.9 6.9 mg/Kg 08/01/16 13:30 08/08/16 18:15 100





Toluene-d8 (Surr) 105 08/01/16 13:30 08/08/16 18:15 10060 - 140













1.8 0.53 ug/Kg 08/11/16 14:46 08/13/16 22:45 1☼Chrysene ND



1.8 0.18 ug/Kg 08/11/16 14:46 08/13/16 22:45 1☼Fluorene ND




1.8 0.34 ug/Kg 08/11/16 14:46 08/13/16 22:45 1☼Pyrene ND

Terphenyl-d14 115 68 - 138 08/11/16 14:46 08/13/16 22:45 1






(>C24-C32)

ND

o-Terphenyl (Surr) 79 37 - 127 08/12/16 08:19 08/13/16 01:00 1


o-Terphenyl (Surr) 80 08/12/16 08:22 08/13/16 04:22 137 - 127


Arsenic 8.6 5.7 0.61 mg/Kg 08/11/16 11:47 08/11/16 17:28 4


0.96 0.086 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Barium 5.8

1.9 0.094 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Cadmium 0.16 J

2.5 0.35 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Chromium 28

4.8 1.4 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Copper 8.5

2.9 0.18 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Lead ND

9.6 0.38 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Selenium ND

4.8 1.1 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Silver ND

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Strontium 2800 9.6 0.77 mg/Kg 08/11/16 11:47 08/11/16 17:28 4


9.6 0.20 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Tin 0.30 J

2.9 0.45 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Titanium 210

3.8 0.61 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Zinc 11


Mercury ND 0.012 0.0037 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:08 1





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Client Sample ID: Method BlankLab Sample ID: MB 440-347464/10Matrix: Solid Prep Type: Total/NAAnalysis Batch: 347464

RL MDL

GRO (C4-C12) ND 10 7.0 mg/Kg 08/08/16 12:12 100

MB MB



MB MB


87 08/08/16 12:12 100Dibromofluoromethane (Surr) 55 - 140

105 08/08/16 12:12 100Toluene-d8 (Surr) 60 - 140


RL MDL

GRO (C4-C12) ND 10 7.0 mg/Kg 08/08/16 09:40 100

MB MB



MB MB



106 08/08/16 09:40 100Toluene-d8 (Surr) 60 - 140

Client Sample ID: Lab Control SampleLab Sample ID: LCS 440-347464/7Matrix: Solid Prep Type: Total/NAAnalysis Batch: 347464

GRO (C4-C12) 50.0 46.2 mg/Kg 92 60 - 130

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

102

LCS LCS


86Dibromofluoromethane (Surr) 55 - 140

104Toluene-d8 (Surr) 60 - 140

Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 440-347464/8Matrix: Solid Prep Type: Total/NAAnalysis Batch: 347464

GRO (C4-C12) 50.0 47.3 mg/Kg 95 60 - 130 2 25

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Surrogate

101

LCSD LCSD




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RL MDL


MB MB











ND 0.501.7 ug/Kg 08/11/16 14:46 08/13/16 17:38 1Chrysene



ND 0.171.7 ug/Kg 08/11/16 14:46 08/13/16 17:38 1Fluorene




ND 0.321.7 ug/Kg 08/11/16 14:46 08/13/16 17:38 1Pyrene

Terphenyl-d14 119 68 - 138 08/13/16 17:38 1

MB MB

Surrogate

08/11/16 14:46



1-Methylnaphthalene 333 325 ug/Kg 97 71 - 118

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Acenaphthene 333 319 ug/Kg 96 68 - 116

Acenaphthylene 333 354 ug/Kg 106 68 - 120

Anthracene 333 371 ug/Kg 111 73 - 125

Benzo[a]anthracene 333 353 ug/Kg 106 66 - 119

Benzo[a]pyrene 333 346 ug/Kg 104 72 - 124

Benzo[b]fluoranthene 333 360 ug/Kg 108 63 - 121

Benzo[g,h,i]perylene 333 328 ug/Kg 99 63 - 124

Benzo[k]fluoranthene 333 295 ug/Kg 89 63 - 129

Chrysene 333 287 ug/Kg 86 69 - 120

Dibenz(a,h)anthracene 333 349 ug/Kg 105 70 - 125

Fluoranthene 333 334 ug/Kg 100 65 - 125

Fluorene 333 381 ug/Kg 114 66 - 121

Indeno[1,2,3-cd]pyrene 333 333 ug/Kg 100 65 - 121

Naphthalene 333 334 ug/Kg 100 70 - 112

Phenanthrene 333 336 ug/Kg 101 73 - 106

Pyrene 333 326 ug/Kg 98 64 - 120

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Terphenyl-d14 68 - 138

Surrogate

115

LCS LCS



1-Methylnaphthalene 333 329 ug/Kg 99 71 - 118 1 11

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Acenaphthene 333 340 ug/Kg 102 68 - 116 6 12

Acenaphthylene 333 375 ug/Kg 113 68 - 120 6 12

Anthracene 333 372 ug/Kg 112 73 - 125 0 12

Benzo[a]anthracene 333 363 ug/Kg 109 66 - 119 3 14

Benzo[a]pyrene 333 358 ug/Kg 107 72 - 124 3 12

Benzo[b]fluoranthene 333 362 ug/Kg 109 63 - 121 1 14

Benzo[g,h,i]perylene 333 338 ug/Kg 101 63 - 124 3 14

Benzo[k]fluoranthene 333 318 ug/Kg 95 63 - 129 8 15

Chrysene 333 296 ug/Kg 89 69 - 120 3 12

Dibenz(a,h)anthracene 333 358 ug/Kg 107 70 - 125 3 13

Fluoranthene 333 340 ug/Kg 102 65 - 125 2 13

Fluorene 333 396 ug/Kg 119 66 - 121 4 13

Indeno[1,2,3-cd]pyrene 333 354 ug/Kg 106 65 - 121 6 15

Naphthalene 333 336 ug/Kg 101 70 - 112 1 12

Phenanthrene 333 338 ug/Kg 101 73 - 106 0 11

Pyrene 333 334 ug/Kg 100 64 - 120 2 12


Surrogate

111

LCSD LCSD



1-Methylnaphthalene ND 366 342 ug/Kg 93 71 - 118☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Acenaphthene ND 366 367 ug/Kg 100 68 - 116☼

Acenaphthylene ND 366 406 ug/Kg 111 68 - 120☼

Anthracene ND 366 410 ug/Kg 112 73 - 125☼

Benzo[a]anthracene ND 366 398 ug/Kg 109 66 - 119☼

Benzo[a]pyrene ND 366 376 ug/Kg 103 72 - 124☼

Benzo[b]fluoranthene ND 366 374 ug/Kg 102 63 - 121☼

Benzo[g,h,i]perylene ND 366 354 ug/Kg 97 63 - 124☼

Benzo[k]fluoranthene ND 366 320 ug/Kg 87 63 - 129☼

Chrysene ND 366 319 ug/Kg 87 69 - 120☼

Dibenz(a,h)anthracene ND 366 371 ug/Kg 101 70 - 125☼

Fluoranthene ND 366 377 ug/Kg 103 65 - 125☼

Fluorene ND 366 437 ug/Kg 119 66 - 121☼

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Indeno[1,2,3-cd]pyrene ND 366 359 ug/Kg 98 65 - 121☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Naphthalene ND 366 367 ug/Kg 100 70 - 112☼

Phenanthrene ND 366 370 ug/Kg 101 73 - 106☼

Pyrene ND 366 365 ug/Kg 100 64 - 120☼


Surrogate

114

MS MS



1-Methylnaphthalene ND 364 358 ug/Kg 99 71 - 118 5 40☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Acenaphthene ND 364 363 ug/Kg 100 68 - 116 1 40☼

Acenaphthylene ND 364 407 ug/Kg 112 68 - 120 0 40☼

Anthracene ND 364 407 ug/Kg 112 73 - 125 1 40☼

Benzo[a]anthracene ND 364 399 ug/Kg 110 66 - 119 0 40☼

Benzo[a]pyrene ND 364 377 ug/Kg 104 72 - 124 0 40☼

Benzo[b]fluoranthene ND 364 384 ug/Kg 106 63 - 121 3 40☼

Benzo[g,h,i]perylene ND 364 359 ug/Kg 99 63 - 124 1 40☼

Benzo[k]fluoranthene ND 364 322 ug/Kg 89 63 - 129 1 40☼

Chrysene ND 364 317 ug/Kg 87 69 - 120 1 40☼

Dibenz(a,h)anthracene ND 364 370 ug/Kg 102 70 - 125 0 40☼

Fluoranthene ND 364 377 ug/Kg 104 65 - 125 0 40☼

Fluorene ND 364 438 ug/Kg 121 66 - 121 0 40☼

Indeno[1,2,3-cd]pyrene ND 364 361 ug/Kg 99 65 - 121 0 40☼

Naphthalene ND 364 374 ug/Kg 103 70 - 112 2 40☼

Phenanthrene ND 364 371 ug/Kg 102 73 - 106 0 40☼

Pyrene ND 364 364 ug/Kg 100 64 - 120 0 40☼


Surrogate

111

MSD MSD



RL MDL


MB MB









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RL MDL

Benzo[g,h,i]perylene ND 0.20 0.10 ug/L 08/10/16 09:36 08/11/16 16:02 1

MB MB



ND 0.100.20 ug/L 08/10/16 09:36 08/11/16 16:02 1Chrysene



ND 0.100.20 ug/L 08/10/16 09:36 08/11/16 16:02 1Fluorene




ND 0.100.20 ug/L 08/10/16 09:36 08/11/16 16:02 1Pyrene


MB MB

Surrogate

08/10/16 09:36


63 08/10/16 09:36 08/11/16 16:02 1Nitrobenzene-d5 46 - 109

85 08/10/16 09:36 08/11/16 16:02 1Terphenyl-d14 28 - 124



Analyte

LCS LCS


Spike

Added

%Rec.

Limits



Anthracene 1.00 0.728 ug/L 73 56 - 120






Chrysene 1.00 0.779 ug/L 78 65 - 120



Fluorene 1.00 0.798 ug/L 80 53 - 120


Naphthalene 1.00 0.704 ug/L 70 46 - 120


Pyrene 1.00 0.782 ug/L 78 63 - 120


Surrogate

69

LCS LCS




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Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD



Anthracene 1.00 0.721 ug/L 72 56 - 120 1 35






Chrysene 1.00 0.764 ug/L 76 65 - 120 2 35



Fluorene 1.00 0.785 ug/L 78 53 - 120 2 35


Naphthalene 1.00 0.717 ug/L 72 46 - 120 2 35


Pyrene 1.00 0.755 ug/L 75 63 - 120 4 35


Surrogate

69

LCSD LCSD






RL MDL


-C4-C12

ND 50 25 ug/L 08/09/16 18:32 1

MB MB



MB MB




-C4-C12

800 810 ug/L 101 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

111

LCS LCS


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Client Sample ID: Matrix SpikeLab Sample ID: 440-154665-D-3 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 347941


-C4-C12

ND 800 820 ug/L 102 65 - 140

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Surrogate

107

MS MS


Client Sample ID: Matrix Spike DuplicateLab Sample ID: 440-154665-D-3 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 347941


-C4-C12

ND 800 849 ug/L 106 65 - 140 4 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Surrogate

111

MSD MSD




RL MDL

HI Diesel Range Organics (>C12-C24) ND 25 12 mg/Kg 08/12/16 08:19 08/12/16 20:03 1

MB MB


ND 1450 mg/Kg 08/12/16 08:19 08/12/16 20:03 1HI Residual Range Organics

(>C24-C32)

o-Terphenyl (Surr) 79 37 - 127 08/12/16 20:03 1

MB MB

Surrogate

08/12/16 08:19



HI Diesel Range Organics

(>C12-C24)

503 444 mg/Kg 88 62 - 118

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

HI Residual Range Organics

(>C24-C32)

503 522 mg/Kg 104 77 - 144


Surrogate

87

LCS LCS


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(>C12-C24)

503 441 mg/Kg 88 62 - 118 1 16

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


(>C24-C32)

503 527 mg/Kg 105 77 - 144 1 16


Surrogate

85

LCSD LCSD




(>C12-C24)

ND F2 191 157 mg/Kg 82 62 - 118☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


(>C24-C32)

20 F1 F2 191 192 mg/Kg 90 77 - 144☼


Surrogate

81

MS MS




(>C12-C24)

ND F2 190 129 F2 mg/Kg 68 62 - 118 20 16☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


(>C24-C32)

20 F1 F2 190 158 F1 F2 mg/Kg 72 77 - 144 20 16☼


Surrogate

65

MSD MSD



RL MDL

DRO (C9-C25) ND 0.50 0.10 mg/L 08/09/16 12:28 08/10/16 17:57 1

MB MB


ND 0.100.50 mg/L 08/09/16 12:28 08/10/16 17:57 1RRO (C24-C40)

n-Octacosane 73 45 - 120 08/10/16 17:57 1

MB MB

Surrogate

08/09/16 12:28


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C10-C28 1.00 0.498 J mg/L 50 40 - 115

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

54

LCS LCS



C10-C28 1.00 0.570 mg/L 57 40 - 115 14 25

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Surrogate

62

LCSD LCSD




RL MDL

Arsenic ND 3.0 0.32 mg/Kg 08/11/16 11:47 08/11/16 16:28 1

MB MB


ND 0.0450.50 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Barium

ND 0.0491.0 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Cadmium

ND 0.181.3 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Chromium

ND 0.722.5 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Copper

ND 0.0961.5 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Lead

ND 0.205.0 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Selenium

ND 0.562.5 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Silver


ND 0.115.0 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Tin

ND 0.241.5 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Titanium

ND 0.322.0 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Zinc


Arsenic 200 198 mg/Kg 99 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 200 200 mg/Kg 100 80 - 120

Cadmium 5.00 4.87 mg/Kg 97 80 - 120

Chromium 20.0 18.8 mg/Kg 94 80 - 120

Copper 25.0 25.1 mg/Kg 100 80 - 120

Lead 50.0 48.1 mg/Kg 96 80 - 120

Selenium 200 195 mg/Kg 97 80 - 120

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Silver 30.0 28.1 mg/Kg 94 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Tin 250 242 mg/Kg 97 80 - 120

Titanium 250 242 mg/Kg 97 80 - 120

Zinc 200 196 mg/Kg 98 80 - 120


Arsenic 200 194 mg/Kg 97 80 - 120 2 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Barium 200 193 mg/Kg 97 80 - 120 4 20

Cadmium 5.00 4.78 mg/Kg 96 80 - 120 2 20

Chromium 20.0 18.0 mg/Kg 90 80 - 120 4 20

Copper 25.0 24.6 mg/Kg 98 80 - 120 2 20

Lead 50.0 47.4 mg/Kg 95 80 - 120 1 20

Selenium 200 192 mg/Kg 96 80 - 120 2 20

Silver 30.0 27.6 mg/Kg 92 80 - 120 2 20

Tin 250 238 mg/Kg 95 80 - 120 2 20

Titanium 250 236 mg/Kg 94 80 - 120 3 20

Zinc 200 194 mg/Kg 97 80 - 120 2 20


Arsenic 23 96.9 124 mg/Kg 104 80 - 120

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 4.8 96.9 99.5 mg/Kg 98 80 - 120

Cadmium 0.52 J 2.42 3.03 mg/Kg 104 80 - 120

Chromium 85 9.69 92.1 4 mg/Kg 76 80 - 120

Copper 15 12.1 26.6 mg/Kg 96 80 - 120

Lead 0.79 J 24.2 24.2 mg/Kg 97 80 - 120

Selenium 1.2 J 96.9 97.2 mg/Kg 99 80 - 120

Silver ND 14.5 14.3 mg/Kg 98 80 - 120

Tin 0.47 J 121 120 mg/Kg 99 80 - 120

Titanium 480 121 594 mg/Kg 92 80 - 120

Zinc 39 96.9 139 mg/Kg 103 80 - 120


Arsenic 23 94.0 126 mg/Kg 109 80 - 120 2 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium 4.8 94.0 99.3 mg/Kg 100 80 - 120 0 20

Cadmium 0.52 J 2.35 3.20 mg/Kg 114 80 - 120 5 20

Chromium 85 9.40 95.3 4 mg/Kg 113 80 - 120 3 20

Copper 15 11.8 26.3 mg/Kg 97 80 - 120 1 20

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Lead 0.79 J 23.5 24.3 mg/Kg 100 80 - 120 0 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Selenium 1.2 J 94.0 98.9 mg/Kg 104 80 - 120 2 20

Silver ND 14.1 13.9 mg/Kg 99 80 - 120 3 20

Tin 0.47 J 118 121 mg/Kg 103 80 - 120 1 20

Titanium 480 118 612 4 mg/Kg 110 80 - 120 3 20

Zinc 39 94.0 142 mg/Kg 109 80 - 120 2 20


RL MDL

Barium ND 0.010 0.0050 mg/L 08/18/16 09:05 08/18/16 23:57 1

MB MB


ND 0.00200.0050 mg/L 08/18/16 09:05 08/18/16 23:57 1Cadmium

ND 0.00250.0050 mg/L 08/18/16 09:05 08/18/16 23:57 1Chromium

ND 0.00500.010 mg/L 08/18/16 09:05 08/18/16 23:57 1Copper

ND 0.00250.0050 mg/L 08/18/16 09:05 08/18/16 23:57 1Lead

ND 0.00610.010 mg/L 08/18/16 09:05 08/18/16 23:57 1Selenium

ND 0.00500.010 mg/L 08/18/16 09:05 08/18/16 23:57 1Silver

ND 0.0100.020 mg/L 08/18/16 09:05 08/18/16 23:57 1Strontium

ND 0.0120.10 mg/L 08/18/16 09:05 08/18/16 23:57 1Tin

ND 0.00250.0050 mg/L 08/18/16 09:05 08/18/16 23:57 1Titanium

ND 0.0100.020 mg/L 08/18/16 09:05 08/18/16 23:57 1Zinc


RL MDL

Arsenic ND 0.010 0.0050 mg/L 08/18/16 09:05 08/20/16 16:03 1

MB MB



Arsenic 1.00 0.905 mg/L 91 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 1.00 0.923 mg/L 92 80 - 120

Cadmium 1.00 0.927 mg/L 93 80 - 120

Chromium 1.00 0.921 mg/L 92 80 - 120

Copper 1.00 0.924 mg/L 92 80 - 120

Lead 1.00 0.953 mg/L 95 80 - 120

Selenium 1.00 0.868 mg/L 87 80 - 120

Silver 0.500 0.450 mg/L 90 80 - 120

Strontium 1.00 0.915 mg/L 91 80 - 120

Tin 1.00 0.908 mg/L 91 80 - 120

Titanium 1.00 0.944 mg/L 94 80 - 120

Zinc 1.00 0.894 mg/L 89 80 - 120

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Arsenic 1.00 0.937 mg/L 94 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Matrix SpikeLab Sample ID: 440-155280-I-4-B MSMatrix: Water Prep Type: Total RecoverableAnalysis Batch: 350369 Prep Batch: 350111

Arsenic 0.10 B 1.00 1.10 mg/L 99 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 0.022 1.00 0.974 mg/L 95 75 - 125

Cadmium ND 1.00 0.905 mg/L 91 75 - 125

Chromium 0.12 1.00 1.08 mg/L 96 75 - 125

Copper ND 1.00 1.13 mg/L 113 75 - 125

Lead ND L 1.00 0.970 mg/L 97 75 - 125

Selenium ND 1.00 0.935 mg/L 93 75 - 125

Silver ND 0.500 0.536 mg/L 107 75 - 125

Strontium 14 1.00 15.7 4 mg/L 215 75 - 125

Tin ND 1.00 0.916 mg/L 92 75 - 125

Titanium 0.019 1.00 1.04 mg/L 103 75 - 125

Zinc ND 1.00 0.947 mg/L 95 75 - 125


Arsenic 0.11 1.00 1.10 mg/L 99 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 440-155280-I-4-C MSDMatrix: Water Prep Type: Total RecoverableAnalysis Batch: 350369 Prep Batch: 350111

Arsenic 0.10 B 1.00 1.08 mg/L 98 75 - 125 1 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium 0.022 1.00 0.955 mg/L 93 75 - 125 2 20

Cadmium ND 1.00 0.919 mg/L 92 75 - 125 2 20

Chromium 0.12 1.00 1.09 mg/L 97 75 - 125 1 20

Copper ND 1.00 1.08 mg/L 108 75 - 125 5 20

Lead ND L 1.00 0.917 mg/L 92 75 - 125 6 20

Selenium ND 1.00 0.908 mg/L 91 75 - 125 3 20

Silver ND 0.500 0.520 mg/L 104 75 - 125 3 20

Strontium 14 1.00 15.5 4 mg/L 198 75 - 125 1 20

Tin ND 1.00 0.881 mg/L 88 75 - 125 4 20

Titanium 0.019 1.00 0.998 mg/L 98 75 - 125 5 20

Zinc ND 1.00 0.930 mg/L 93 75 - 125 2 20

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Arsenic 0.11 1.00 1.13 mg/L 102 75 - 125 3 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD



RL MDL

Mercury ND 0.00020 0.00010 mg/L 08/09/16 19:08 08/10/16 16:19 1

MB MB



Mercury 0.00800 0.00803 mg/L 100 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Matrix SpikeLab Sample ID: 440-154741-M-1-C MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 348253 Prep Batch: 347966

Mercury ND 0.00800 0.00827 mg/L 103 70 - 130

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 440-154741-M-1-D MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 348253 Prep Batch: 347966

Mercury ND 0.00800 0.00814 mg/L 102 70 - 130 2 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD



RL MDL

Mercury ND 0.012 0.0036 mg/Kg 08/11/16 13:23 08/12/16 09:58 1

MB MB



Mercury 0.100 0.0857 mg/Kg 86 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

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Method: 7471A - Mercury (CVAA) (Continued)


Mercury 0.100 0.0842 mg/Kg 84 80 - 120 2 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Mercury ND 0.113 0.106 mg/Kg 94 80 - 120☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Mercury ND 0.115 0.103 mg/Kg 89 80 - 120 4 20☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Client Sample ID: DU-3-1-20160801Lab Sample ID: 580-61481-1 DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 224669


Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD

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Prep 5035 08/01/16 09:00 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Analysis 8260B/CA_LUFTMS 100 347464 08/08/16 14:43 WC TAL IRVTotal/NA

ISM Prep Increment, Prep 224304 08/08/16 11:02 HJM TAL SEATotal/NA

Prep 3546 224734 08/12/16 08:19 J1J TAL SEATotal/NA

Analysis 8015B 1 224710 08/13/16 01:22 CJ TAL SEATotal/NA


Prep 3050B 224649 08/11/16 11:47 PAB TAL SEATotal/NA

Analysis 6010B 4 224725 08/11/16 16:37 HJM TAL SEATotal/NA


Analysis D 2216 1 224669 08/11/16 14:28 CBS TAL SEATotal/NA



ISM Prep Increment, Prep 08/08/16 11:02 HJM224304 TAL SEA

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA

Prep 3546 224674 08/11/16 14:46 CBS TAL SEATotal/NA

Analysis 8270C SIM 1 224832 08/13/16 18:55 D1R TAL SEATotal/NA





Prep 7471A 224662 08/11/16 13:23 PAB TAL SEATotal/NA

Analysis 7471A 1 224756 08/12/16 10:15 FCW TAL SEATotal/NA



Prep 5035 08/01/16 09:15 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA










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Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











Prep 5035 08/01/16 09:30 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA









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Prep 5035 08/01/16 09:45 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











Prep 5035 08/01/16 11:00 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA










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Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











Prep 5035 08/01/16 11:30 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA









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Prep 5035 08/01/16 11:45 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











Prep 3520C 08/10/16 09:36 BMN348082 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA


Analysis 8015B 1 347941 08/10/16 06:41 IM TAL IRVTotal/NA

Prep 3510C 347843 08/09/16 13:20 AP TAL IRVTotal/NA



Analysis 6010B 1 350369 08/19/16 00:11 ND TAL IRVTotal Recoverable




Analysis 7470A 1 348253 08/10/16 16:35 B1H TAL IRVTotal/NA

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Prep 5035 08/01/16 13:30 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











TAL SEA = TestAmerica Seattle, 5755 8th Street East, Tacoma, WA 98424, TEL (253)922-2310

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Laboratory: TestAmerica SeattleAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.


Alaska (UST) UST-02210State Program 03-02-17


L-A-B DoD ELAP L2236 01-19-19

L-A-B ISO/IEC 17025 L2236 01-19-19

Montana (UST) State Program 8 N/A 04-30-20

Oregon NELAP 10 WA100007 11-06-16


USDA Federal P330-14-00126 04-08-17








Alaska CA0153110State Program 06-30-17



California State Program 9 CA ELAP 2706 06-30-18



Kansas NELAP Secondary AB 7 E-10420 07-31-16 *

Nevada State Program 9 CA015312016-2 07-31-17 *



Oregon NELAP 10 4028 01-29-17

USDA Federal P330-09-00080 07-08-18


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580-61481-1 DU-3-1-20160801 Solid 08/01/16 09:00 08/03/16 09:40

580-61481-2 DU-3-2-20160801 Solid 08/01/16 09:15 08/03/16 09:40

580-61481-3 DU-3-3-20160801 Solid 08/01/16 09:30 08/03/16 09:40

580-61481-4 DU-4-20160801 Solid 08/01/16 09:45 08/03/16 09:40

580-61481-5 DU-6-20160801 Solid 08/01/16 11:00 08/03/16 09:40

580-61481-6 DU-2A-20160801 Solid 08/01/16 11:30 08/03/16 09:40

580-61481-7 DU-2B-20160801 Solid 08/01/16 11:45 08/03/16 09:40

580-61481-8 DU-5-20160801 Water 08/01/16 12:00 08/03/16 09:40

580-61481-9 DU-1-20160801 Solid 08/01/16 13:30 08/03/16 09:40

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Login Number: 61481


Creator: Gonzales, Steve

List Source: TestAmerica Seattle

List Number: 1








TrueCOC is present.











TrueSample Preservation Verified.







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Login Number: 61481


Creator: Salas, Margarita


List Creation: 08/06/16 10:12 AMList Number: 2








TrueCOC is present.



N/AIs the Field Sampler's name present on COC? Received project as a subcontract.















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Login Number: 61481


Creator: Ornelas, Olga










TrueCOC is present.


















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ANALYTICAL REPORTTestAmerica Laboratories, Inc.TestAmerica Seattle5755 8th Street EastTacoma, WA 98424Tel: (253)922-2310



Attn: Matt Neal





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Table of Contents



Page 2 of 53TestAmerica Seattle

8/22/2016

Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1


Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3

Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5



Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 38


Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 45

Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 46


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Job ID: 580-61481-1

Laboratory: TestAmerica Seattle

Narrative


Comments


Receipt

The samples were received on 8/3/2016 9:40 AM; the samples arrived in good condition, properly preserved and, where required, on ice.

The temperature of the cooler at receipt was 2.9º C.

GC/MS VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

GC/MS Semi VOA Method(s) 8270C SIM: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch 440-348082 and analytical batch 440-348390. The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch.


GC VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.

GC Semi VOA Method(s) 8015B: The matrix spike / matrix spike duplicate (MS/MSD) recoveries and precision for preparation batch 580-224304 and 580-224734 and analytical batch 580-224710 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated laboratory control sample / laboratory sample control duplicate (LCS/LCSD) precision was within

acceptance limits.

Method(s) 8015B: The following samples contained a hydrocarbon pattern in the diesel range; however, the elution pattern was later than the typical diesel fuel pattern used by the laboratory for quantitative purposes: DU-3-1-20160801 (580-61481-1), DU-3-2-20160801 (580-61481-2) and DU-3-3-20160801 (580-61481-3).

Method(s) 8015B: The continuing calibration verification (CCV) associated with batch 440-348086 recovered above the upper control limit

for C10-C28. The samples associated with this CCV were non-detects for the affected analytes; therefore, the data have been reported. The following sample is impacted: (CCV 440-348086/35).


preparation batch 440-347843 and analytical batch 440-348086.The laboratory control sample (LCS) was performed in duplicate to provide precision data for this batch.


Metals



Organic Prep Method(s) 3510C: The following sample was prepared outside of preparation holding time due to oversight by the lab. The sample status

was at "Shipd" until 8/9/16 which is one day after holding time had expired. Sample was extracted on 8/9/16. DU-5-20160801 (580-61481-8).

Method(s) 3520C: The following sample(s) was received with less than 2 days remaining on the holding time or less than one shift (8


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Laboratory: TestAmerica Seattle (Continued)

hours) remaining on a test with a holding time of 48 hours or less. As such, the laboratory had insufficient time remaining to perform the

analysis within holding time: 3520C/8270_SIM PAH DU-5-20160801 (580-61481-8).


VOA Prep



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Qualifiers

GC/MS Semi VOA



Qualifier

GC Semi VOA



Qualifier

F2 MS/MSD RPD exceeds control limits



Metals



applicable.

Qualifier


Glossary



Abbreviation

%R Percent Recovery












NC Not Calculated



QC Quality Control






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GRO (C4-C12) ND 10 7.0 mg/Kg 08/01/16 09:00 08/08/16 14:43 100





Toluene-d8 (Surr) 107 08/01/16 09:00 08/08/16 14:43 10060 - 140













1.8 0.55 ug/Kg 08/11/16 14:46 08/13/16 18:55 1☼Chrysene ND



1.8 0.18 ug/Kg 08/11/16 14:46 08/13/16 18:55 1☼Fluorene ND




1.8 0.36 ug/Kg 08/11/16 14:46 08/13/16 18:55 1☼Pyrene ND

Terphenyl-d14 110 68 - 138 08/11/16 14:46 08/13/16 18:55 1






20 F1 F2

o-Terphenyl (Surr) 77 37 - 127 08/12/16 08:19 08/12/16 21:12 1


o-Terphenyl (Surr) 77 08/12/16 08:19 08/13/16 01:22 137 - 127


Arsenic 23 5.8 0.62 mg/Kg 08/11/16 11:47 08/11/16 16:37 4


0.97 0.087 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Barium 4.8

1.9 0.095 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Cadmium 0.52 J

2.5 0.36 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Chromium 85

4.8 1.4 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Copper 15

2.9 0.19 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Lead 0.79 J

9.7 0.39 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Selenium 1.2 J

4.8 1.1 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Silver ND

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Strontium 2400 9.7 0.78 mg/Kg 08/11/16 11:47 08/11/16 16:37 4


9.7 0.20 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Tin 0.47 J

2.9 0.46 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Titanium 480

3.9 0.62 mg/Kg 08/11/16 11:47 08/11/16 16:37 4Zinc 39


Mercury ND 0.013 0.0040 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:15 1





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GRO (C4-C12) ND 9.8 6.9 mg/Kg 08/01/16 09:15 08/08/16 15:13 100





Toluene-d8 (Surr) 106 08/01/16 09:15 08/08/16 15:13 10060 - 140













1.8 0.55 ug/Kg 08/11/16 14:46 08/13/16 20:11 1☼Chrysene ND



1.8 0.18 ug/Kg 08/11/16 14:46 08/13/16 20:11 1☼Fluorene ND




1.8 0.35 ug/Kg 08/11/16 14:46 08/13/16 20:11 1☼Pyrene ND

Terphenyl-d14 120 68 - 138 08/11/16 14:46 08/13/16 20:11 1






21

o-Terphenyl (Surr) 78 37 - 127 08/12/16 08:19 08/12/16 22:20 1


o-Terphenyl (Surr) 79 08/12/16 08:19 08/13/16 01:45 137 - 127


Arsenic 23 5.9 0.63 mg/Kg 08/11/16 11:47 08/11/16 16:56 4


0.99 0.089 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Barium 5.1

2.0 0.097 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Cadmium 0.77 J

2.6 0.36 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Chromium 89

4.9 1.4 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Copper 16

3.0 0.19 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Lead 0.64 J

9.9 0.40 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Selenium 1.2 J

4.9 1.1 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Silver ND

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Strontium 2300 9.9 0.79 mg/Kg 08/11/16 11:47 08/11/16 16:56 4


9.9 0.21 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Tin 0.38 J

3.0 0.47 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Titanium 600

4.0 0.63 mg/Kg 08/11/16 11:47 08/11/16 16:56 4Zinc 42


Mercury ND 0.014 0.0041 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:22 1





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GRO (C4-C12) ND 8.7 6.1 mg/Kg 08/01/16 09:30 08/08/16 15:44 100





Toluene-d8 (Surr) 107 08/01/16 09:30 08/08/16 15:44 10060 - 140













1.8 0.55 ug/Kg 08/11/16 14:46 08/13/16 20:37 1☼Chrysene ND



1.8 0.18 ug/Kg 08/11/16 14:46 08/13/16 20:37 1☼Fluorene ND




1.8 0.36 ug/Kg 08/11/16 14:46 08/13/16 20:37 1☼Pyrene ND

Terphenyl-d14 115 68 - 138 08/11/16 14:46 08/13/16 20:37 1






27

o-Terphenyl (Surr) 70 37 - 127 08/12/16 08:19 08/12/16 22:43 1


o-Terphenyl (Surr) 79 08/12/16 08:19 08/13/16 02:08 137 - 127


Arsenic 23 6.0 0.64 mg/Kg 08/11/16 11:47 08/11/16 17:01 4


1.0 0.090 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Barium 5.6

2.0 0.098 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Cadmium 0.76 J

2.6 0.37 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Chromium 94

5.0 1.4 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Copper 16

3.0 0.19 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Lead 0.40 J

10 0.40 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Selenium ND

5.0 1.1 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Silver ND

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Strontium 2300 10 0.80 mg/Kg 08/11/16 11:47 08/11/16 17:01 4


10 0.21 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Tin 0.41 J

3.0 0.47 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Titanium 670

4.0 0.64 mg/Kg 08/11/16 11:47 08/11/16 17:01 4Zinc 43


Mercury ND 0.014 0.0041 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:25 1





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GRO (C4-C12) ND 9.2 6.4 mg/Kg 08/01/16 09:45 08/08/16 16:14 100





Toluene-d8 (Surr) 107 08/01/16 09:45 08/08/16 16:14 10060 - 140













1.9 0.56 ug/Kg 08/11/16 14:46 08/13/16 21:02 1☼Chrysene ND



1.9 0.19 ug/Kg 08/11/16 14:46 08/13/16 21:02 1☼Fluorene ND




1.9 0.36 ug/Kg 08/11/16 14:46 08/13/16 21:02 1☼Pyrene ND

Terphenyl-d14 102 68 - 138 08/11/16 14:46 08/13/16 21:02 1






(>C24-C32)

ND

o-Terphenyl (Surr) 72 37 - 127 08/12/16 08:19 08/12/16 23:06 1


o-Terphenyl (Surr) 77 08/12/16 08:19 08/13/16 02:31 137 - 127


Arsenic 23 5.8 0.62 mg/Kg 08/11/16 11:47 08/11/16 17:11 4


0.97 0.087 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Barium 5.1

1.9 0.095 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Cadmium 0.74 J

2.5 0.36 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Chromium 84

4.9 1.4 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Copper 15

2.9 0.19 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Lead 0.55 J

9.7 0.39 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Selenium 1.2 J

4.9 1.1 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Silver ND

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Strontium 2500 9.7 0.78 mg/Kg 08/11/16 11:47 08/11/16 17:11 4


9.7 0.20 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Tin 0.25 J

2.9 0.46 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Titanium 590

3.9 0.62 mg/Kg 08/11/16 11:47 08/11/16 17:11 4Zinc 40


Mercury ND 0.014 0.0041 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:27 1





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GRO (C4-C12) ND 8.8 6.2 mg/Kg 08/01/16 11:00 08/08/16 16:44 100





Toluene-d8 (Surr) 103 08/01/16 11:00 08/08/16 16:44 10060 - 140













1.9 0.57 ug/Kg 08/11/16 14:46 08/13/16 21:28 1☼Chrysene ND



1.9 0.19 ug/Kg 08/11/16 14:46 08/13/16 21:28 1☼Fluorene ND




1.9 0.37 ug/Kg 08/11/16 14:46 08/13/16 21:28 1☼Pyrene ND

Terphenyl-d14 106 68 - 138 08/11/16 14:46 08/13/16 21:28 1



HI Diesel Range Organics (>C12-C24) ND 10 4.9 mg/Kg ☼ 08/12/16 08:19 08/12/16 23:29 1



4.6 J

o-Terphenyl (Surr) 72 37 - 127 08/12/16 08:19 08/12/16 23:29 1


o-Terphenyl (Surr) 83 08/12/16 08:19 08/13/16 02:53 137 - 127


Arsenic 22 5.9 0.63 mg/Kg 08/11/16 11:47 08/11/16 17:15 4


0.98 0.088 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Barium 5.1

2.0 0.096 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Cadmium 0.73 J

2.5 0.36 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Chromium 88

4.9 1.4 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Copper 15

2.9 0.19 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Lead 0.40 J

9.8 0.39 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Selenium 0.97 J

4.9 1.1 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Silver ND

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Strontium 2400 9.8 0.78 mg/Kg 08/11/16 11:47 08/11/16 17:15 4


9.8 0.21 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Tin 0.37 J

2.9 0.46 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Titanium 550

3.9 0.63 mg/Kg 08/11/16 11:47 08/11/16 17:15 4Zinc 39


Mercury ND 0.014 0.0042 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:29 1





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GRO (C4-C12) ND 9.2 6.5 mg/Kg 08/01/16 11:30 08/08/16 17:15 100





Toluene-d8 (Surr) 105 08/01/16 11:30 08/08/16 17:15 10060 - 140







1.9 0.22 ug/Kg 08/11/16 14:46 08/13/16 21:53 1☼Anthracene 2.0






1.9 0.56 ug/Kg 08/11/16 14:46 08/13/16 21:53 1☼Chrysene ND



1.9 0.19 ug/Kg 08/11/16 14:46 08/13/16 21:53 1☼Fluorene ND




1.9 0.36 ug/Kg 08/11/16 14:46 08/13/16 21:53 1☼Pyrene ND

Terphenyl-d14 96 68 - 138 08/11/16 14:46 08/13/16 21:53 1






(>C24-C32)

ND

o-Terphenyl (Surr) 63 37 - 127 08/12/16 08:19 08/13/16 00:14 1


o-Terphenyl (Surr) 80 08/12/16 08:19 08/13/16 03:16 137 - 127


Arsenic 27 5.9 0.63 mg/Kg 08/11/16 11:47 08/11/16 17:19 4


0.99 0.089 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Barium 4.9

2.0 0.097 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Cadmium 0.60 J

2.6 0.36 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Chromium 66

4.9 1.4 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Copper 15

3.0 0.19 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Lead 0.79 J

9.9 0.40 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Selenium ND

4.9 1.1 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Silver ND

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Strontium 2700 9.9 0.79 mg/Kg 08/11/16 11:47 08/11/16 17:19 4


9.9 0.21 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Tin ND

3.0 0.47 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Titanium 540

4.0 0.63 mg/Kg 08/11/16 11:47 08/11/16 17:19 4Zinc 32


Mercury ND 0.014 0.0042 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:32 1





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GRO (C4-C12) ND 9.9 7.0 mg/Kg 08/01/16 11:45 08/08/16 17:45 100





Toluene-d8 (Surr) 108 08/01/16 11:45 08/08/16 17:45 10060 - 140













1.8 0.53 ug/Kg 08/11/16 14:46 08/13/16 22:19 1☼Chrysene ND



1.8 0.18 ug/Kg 08/11/16 14:46 08/13/16 22:19 1☼Fluorene ND




1.8 0.34 ug/Kg 08/11/16 14:46 08/13/16 22:19 1☼Pyrene ND

Terphenyl-d14 117 68 - 138 08/11/16 14:46 08/13/16 22:19 1






(>C24-C32)

ND

o-Terphenyl (Surr) 76 37 - 127 08/12/16 08:19 08/13/16 00:37 1


o-Terphenyl (Surr) 80 08/12/16 08:22 08/13/16 03:38 137 - 127


Arsenic 26 5.9 0.63 mg/Kg 08/11/16 11:47 08/11/16 17:24 4


0.99 0.089 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Barium 4.6

2.0 0.097 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Cadmium 0.60 J

2.6 0.36 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Chromium 75

5.0 1.4 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Copper 14

3.0 0.19 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Lead 0.40 J

9.9 0.40 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Selenium 0.68 J

5.0 1.1 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Silver ND

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Strontium 2600 9.9 0.79 mg/Kg 08/11/16 11:47 08/11/16 17:24 4


9.9 0.21 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Tin 0.29 J

3.0 0.47 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Titanium 480

4.0 0.64 mg/Kg 08/11/16 11:47 08/11/16 17:24 4Zinc 35


Mercury ND 0.014 0.0042 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:06 1





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1-Methylnaphthalene ND H 0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1


0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 12-Methylnaphthalene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Acenaphthene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Acenaphthylene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Anthracene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Benzo[a]anthracene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Benzo[a]pyrene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Benzo[b]fluoranthene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Benzo[g,h,i]perylene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Benzo[k]fluoranthene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Chrysene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Dibenz(a,h)anthracene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Fluoranthene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Fluorene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Indeno[1,2,3-cd]pyrene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Naphthalene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Phenanthrene ND H

0.20 0.10 ug/L 08/10/16 09:36 08/11/16 22:14 1Pyrene ND H



Nitrobenzene-d5 66 08/10/16 09:36 08/11/16 22:14 146 - 109

Terphenyl-d14 62 08/10/16 09:36 08/11/16 22:14 128 - 124



-C4-C12

ND 50 25 ug/L 08/10/16 06:41 1





DRO (C9-C25) ND H 0.50 0.10 mg/L 08/09/16 13:20 08/10/16 20:18 1


0.50 0.10 mg/L 08/09/16 13:20 08/10/16 20:18 1RRO (C24-C40) ND H

n-Octacosane 51 45 - 120 08/09/16 13:20 08/10/16 20:18 1



Arsenic ND 0.010 0.0050 mg/L 08/18/16 09:05 08/20/16 16:15 1


0.010 0.0050 mg/L 08/18/16 09:05 08/19/16 00:11 1Barium 0.0079 J

0.0050 0.0020 mg/L 08/18/16 09:05 08/19/16 00:11 1Cadmium ND

0.0050 0.0025 mg/L 08/18/16 09:05 08/19/16 00:11 1Chromium 0.031

0.010 0.0050 mg/L 08/18/16 09:05 08/19/16 00:11 1Copper 0.0069 J

0.0050 0.0025 mg/L 08/18/16 09:05 08/19/16 00:11 1Lead ND

0.010 0.0061 mg/L 08/18/16 09:05 08/19/16 00:11 1Selenium ND

0.010 0.0050 mg/L 08/18/16 09:05 08/19/16 00:11 1Silver ND

0.020 0.010 mg/L 08/18/16 09:05 08/19/16 00:11 1Strontium 0.031

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Method: 6010B - Metals (ICP) - Total Recoverable (Continued)RL MDL

Tin ND 0.10 0.012 mg/L 08/18/16 09:05 08/19/16 00:11 1


0.0050 0.0025 mg/L 08/18/16 09:05 08/19/16 00:11 1Titanium 0.53

0.020 0.010 mg/L 08/18/16 09:05 08/19/16 00:11 1Zinc ND


Mercury ND 0.00020 0.00010 mg/L 08/09/16 19:08 08/10/16 16:35 1


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GRO (C4-C12) ND 9.9 6.9 mg/Kg 08/01/16 13:30 08/08/16 18:15 100





Toluene-d8 (Surr) 105 08/01/16 13:30 08/08/16 18:15 10060 - 140













1.8 0.53 ug/Kg 08/11/16 14:46 08/13/16 22:45 1☼Chrysene ND



1.8 0.18 ug/Kg 08/11/16 14:46 08/13/16 22:45 1☼Fluorene ND




1.8 0.34 ug/Kg 08/11/16 14:46 08/13/16 22:45 1☼Pyrene ND

Terphenyl-d14 115 68 - 138 08/11/16 14:46 08/13/16 22:45 1






(>C24-C32)

ND

o-Terphenyl (Surr) 79 37 - 127 08/12/16 08:19 08/13/16 01:00 1


o-Terphenyl (Surr) 80 08/12/16 08:22 08/13/16 04:22 137 - 127


Arsenic 8.6 5.7 0.61 mg/Kg 08/11/16 11:47 08/11/16 17:28 4


0.96 0.086 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Barium 5.8

1.9 0.094 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Cadmium 0.16 J

2.5 0.35 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Chromium 28

4.8 1.4 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Copper 8.5

2.9 0.18 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Lead ND

9.6 0.38 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Selenium ND

4.8 1.1 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Silver ND

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Strontium 2800 9.6 0.77 mg/Kg 08/11/16 11:47 08/11/16 17:28 4


9.6 0.20 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Tin 0.30 J

2.9 0.45 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Titanium 210

3.8 0.61 mg/Kg 08/11/16 11:47 08/11/16 17:28 4Zinc 11


Mercury ND 0.012 0.0037 mg/Kg ☼ 08/11/16 13:23 08/12/16 10:08 1





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RL MDL

GRO (C4-C12) ND 10 7.0 mg/Kg 08/08/16 12:12 100

MB MB



MB MB



105 08/08/16 12:12 100Toluene-d8 (Surr) 60 - 140


RL MDL

GRO (C4-C12) ND 10 7.0 mg/Kg 08/08/16 09:40 100

MB MB



MB MB



106 08/08/16 09:40 100Toluene-d8 (Surr) 60 - 140

Client Sample ID: Lab Control SampleLab Sample ID: LCS 440-347464/7Matrix: Solid Prep Type: Total/NAAnalysis Batch: 347464

GRO (C4-C12) 50.0 46.2 mg/Kg 92 60 - 130

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

102

LCS LCS




Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 440-347464/8Matrix: Solid Prep Type: Total/NAAnalysis Batch: 347464

GRO (C4-C12) 50.0 47.3 mg/Kg 95 60 - 130 2 25

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Surrogate

101

LCSD LCSD




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RL MDL


MB MB











ND 0.501.7 ug/Kg 08/11/16 14:46 08/13/16 17:38 1Chrysene



ND 0.171.7 ug/Kg 08/11/16 14:46 08/13/16 17:38 1Fluorene




ND 0.321.7 ug/Kg 08/11/16 14:46 08/13/16 17:38 1Pyrene

Terphenyl-d14 119 68 - 138 08/13/16 17:38 1

MB MB

Surrogate

08/11/16 14:46




Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Acenaphthene 333 319 ug/Kg 96 68 - 116

Acenaphthylene 333 354 ug/Kg 106 68 - 120

Anthracene 333 371 ug/Kg 111 73 - 125

Benzo[a]anthracene 333 353 ug/Kg 106 66 - 119

Benzo[a]pyrene 333 346 ug/Kg 104 72 - 124

Benzo[b]fluoranthene 333 360 ug/Kg 108 63 - 121

Benzo[g,h,i]perylene 333 328 ug/Kg 99 63 - 124

Benzo[k]fluoranthene 333 295 ug/Kg 89 63 - 129

Chrysene 333 287 ug/Kg 86 69 - 120

Dibenz(a,h)anthracene 333 349 ug/Kg 105 70 - 125

Fluoranthene 333 334 ug/Kg 100 65 - 125

Fluorene 333 381 ug/Kg 114 66 - 121

Indeno[1,2,3-cd]pyrene 333 333 ug/Kg 100 65 - 121

Naphthalene 333 334 ug/Kg 100 70 - 112

Phenanthrene 333 336 ug/Kg 101 73 - 106

Pyrene 333 326 ug/Kg 98 64 - 120

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Surrogate

115

LCS LCS




Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Acenaphthene 333 340 ug/Kg 102 68 - 116 6 12

Acenaphthylene 333 375 ug/Kg 113 68 - 120 6 12

Anthracene 333 372 ug/Kg 112 73 - 125 0 12

Benzo[a]anthracene 333 363 ug/Kg 109 66 - 119 3 14

Benzo[a]pyrene 333 358 ug/Kg 107 72 - 124 3 12

Benzo[b]fluoranthene 333 362 ug/Kg 109 63 - 121 1 14

Benzo[g,h,i]perylene 333 338 ug/Kg 101 63 - 124 3 14

Benzo[k]fluoranthene 333 318 ug/Kg 95 63 - 129 8 15

Chrysene 333 296 ug/Kg 89 69 - 120 3 12

Dibenz(a,h)anthracene 333 358 ug/Kg 107 70 - 125 3 13

Fluoranthene 333 340 ug/Kg 102 65 - 125 2 13

Fluorene 333 396 ug/Kg 119 66 - 121 4 13

Indeno[1,2,3-cd]pyrene 333 354 ug/Kg 106 65 - 121 6 15

Naphthalene 333 336 ug/Kg 101 70 - 112 1 12

Phenanthrene 333 338 ug/Kg 101 73 - 106 0 11

Pyrene 333 334 ug/Kg 100 64 - 120 2 12


Surrogate

111

LCSD LCSD




Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Acenaphthene ND 366 367 ug/Kg 100 68 - 116☼

Acenaphthylene ND 366 406 ug/Kg 111 68 - 120☼

Anthracene ND 366 410 ug/Kg 112 73 - 125☼

Benzo[a]anthracene ND 366 398 ug/Kg 109 66 - 119☼

Benzo[a]pyrene ND 366 376 ug/Kg 103 72 - 124☼

Benzo[b]fluoranthene ND 366 374 ug/Kg 102 63 - 121☼

Benzo[g,h,i]perylene ND 366 354 ug/Kg 97 63 - 124☼

Benzo[k]fluoranthene ND 366 320 ug/Kg 87 63 - 129☼

Chrysene ND 366 319 ug/Kg 87 69 - 120☼

Dibenz(a,h)anthracene ND 366 371 ug/Kg 101 70 - 125☼

Fluoranthene ND 366 377 ug/Kg 103 65 - 125☼

Fluorene ND 366 437 ug/Kg 119 66 - 121☼

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Indeno[1,2,3-cd]pyrene ND 366 359 ug/Kg 98 65 - 121☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Naphthalene ND 366 367 ug/Kg 100 70 - 112☼

Phenanthrene ND 366 370 ug/Kg 101 73 - 106☼

Pyrene ND 366 365 ug/Kg 100 64 - 120☼


Surrogate

114

MS MS




Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Acenaphthene ND 364 363 ug/Kg 100 68 - 116 1 40☼

Acenaphthylene ND 364 407 ug/Kg 112 68 - 120 0 40☼

Anthracene ND 364 407 ug/Kg 112 73 - 125 1 40☼

Benzo[a]anthracene ND 364 399 ug/Kg 110 66 - 119 0 40☼

Benzo[a]pyrene ND 364 377 ug/Kg 104 72 - 124 0 40☼

Benzo[b]fluoranthene ND 364 384 ug/Kg 106 63 - 121 3 40☼

Benzo[g,h,i]perylene ND 364 359 ug/Kg 99 63 - 124 1 40☼

Benzo[k]fluoranthene ND 364 322 ug/Kg 89 63 - 129 1 40☼

Chrysene ND 364 317 ug/Kg 87 69 - 120 1 40☼

Dibenz(a,h)anthracene ND 364 370 ug/Kg 102 70 - 125 0 40☼

Fluoranthene ND 364 377 ug/Kg 104 65 - 125 0 40☼

Fluorene ND 364 438 ug/Kg 121 66 - 121 0 40☼

Indeno[1,2,3-cd]pyrene ND 364 361 ug/Kg 99 65 - 121 0 40☼

Naphthalene ND 364 374 ug/Kg 103 70 - 112 2 40☼

Phenanthrene ND 364 371 ug/Kg 102 73 - 106 0 40☼

Pyrene ND 364 364 ug/Kg 100 64 - 120 0 40☼


Surrogate

111

MSD MSD



RL MDL


MB MB









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RL MDL

Benzo[g,h,i]perylene ND 0.20 0.10 ug/L 08/10/16 09:36 08/11/16 16:02 1

MB MB



ND 0.100.20 ug/L 08/10/16 09:36 08/11/16 16:02 1Chrysene



ND 0.100.20 ug/L 08/10/16 09:36 08/11/16 16:02 1Fluorene




ND 0.100.20 ug/L 08/10/16 09:36 08/11/16 16:02 1Pyrene


MB MB

Surrogate

08/10/16 09:36


63 08/10/16 09:36 08/11/16 16:02 1Nitrobenzene-d5 46 - 109

85 08/10/16 09:36 08/11/16 16:02 1Terphenyl-d14 28 - 124



Analyte

LCS LCS


Spike

Added

%Rec.

Limits



Anthracene 1.00 0.728 ug/L 73 56 - 120






Chrysene 1.00 0.779 ug/L 78 65 - 120



Fluorene 1.00 0.798 ug/L 80 53 - 120


Naphthalene 1.00 0.704 ug/L 70 46 - 120


Pyrene 1.00 0.782 ug/L 78 63 - 120


Surrogate

69

LCS LCS




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Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD



Anthracene 1.00 0.721 ug/L 72 56 - 120 1 35






Chrysene 1.00 0.764 ug/L 76 65 - 120 2 35



Fluorene 1.00 0.785 ug/L 78 53 - 120 2 35


Naphthalene 1.00 0.717 ug/L 72 46 - 120 2 35


Pyrene 1.00 0.755 ug/L 75 63 - 120 4 35


Surrogate

69

LCSD LCSD






RL MDL


-C4-C12

ND 50 25 ug/L 08/09/16 18:32 1

MB MB



MB MB




-C4-C12

800 810 ug/L 101 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

111

LCS LCS


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Client Sample ID: Matrix SpikeLab Sample ID: 440-154665-D-3 MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 347941


-C4-C12

ND 800 820 ug/L 102 65 - 140

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Surrogate

107

MS MS


Client Sample ID: Matrix Spike DuplicateLab Sample ID: 440-154665-D-3 MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 347941


-C4-C12

ND 800 849 ug/L 106 65 - 140 4 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Surrogate

111

MSD MSD




RL MDL

HI Diesel Range Organics (>C12-C24) ND 25 12 mg/Kg 08/12/16 08:19 08/12/16 20:03 1

MB MB


ND 1450 mg/Kg 08/12/16 08:19 08/12/16 20:03 1HI Residual Range Organics

(>C24-C32)

o-Terphenyl (Surr) 79 37 - 127 08/12/16 20:03 1

MB MB

Surrogate

08/12/16 08:19




(>C12-C24)

503 444 mg/Kg 88 62 - 118

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


(>C24-C32)

503 522 mg/Kg 104 77 - 144


Surrogate

87

LCS LCS


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(>C12-C24)

503 441 mg/Kg 88 62 - 118 1 16

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


(>C24-C32)

503 527 mg/Kg 105 77 - 144 1 16


Surrogate

85

LCSD LCSD




(>C12-C24)

ND F2 191 157 mg/Kg 82 62 - 118☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


(>C24-C32)

20 F1 F2 191 192 mg/Kg 90 77 - 144☼


Surrogate

81

MS MS




(>C12-C24)

ND F2 190 129 F2 mg/Kg 68 62 - 118 20 16☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


(>C24-C32)

20 F1 F2 190 158 F1 F2 mg/Kg 72 77 - 144 20 16☼


Surrogate

65

MSD MSD



RL MDL

DRO (C9-C25) ND 0.50 0.10 mg/L 08/09/16 12:28 08/10/16 17:57 1

MB MB


ND 0.100.50 mg/L 08/09/16 12:28 08/10/16 17:57 1RRO (C24-C40)

n-Octacosane 73 45 - 120 08/10/16 17:57 1

MB MB

Surrogate

08/09/16 12:28


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C10-C28 1.00 0.498 J mg/L 50 40 - 115

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Surrogate

54

LCS LCS



C10-C28 1.00 0.570 mg/L 57 40 - 115 14 25

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Surrogate

62

LCSD LCSD




RL MDL

Arsenic ND 3.0 0.32 mg/Kg 08/11/16 11:47 08/11/16 16:28 1

MB MB


ND 0.0450.50 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Barium

ND 0.0491.0 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Cadmium

ND 0.181.3 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Chromium

ND 0.722.5 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Copper

ND 0.0961.5 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Lead

ND 0.205.0 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Selenium

ND 0.562.5 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Silver


ND 0.115.0 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Tin

ND 0.241.5 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Titanium

ND 0.322.0 mg/Kg 08/11/16 11:47 08/11/16 16:28 1Zinc


Arsenic 200 198 mg/Kg 99 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 200 200 mg/Kg 100 80 - 120

Cadmium 5.00 4.87 mg/Kg 97 80 - 120

Chromium 20.0 18.8 mg/Kg 94 80 - 120

Copper 25.0 25.1 mg/Kg 100 80 - 120

Lead 50.0 48.1 mg/Kg 96 80 - 120

Selenium 200 195 mg/Kg 97 80 - 120

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Silver 30.0 28.1 mg/Kg 94 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Tin 250 242 mg/Kg 97 80 - 120

Titanium 250 242 mg/Kg 97 80 - 120

Zinc 200 196 mg/Kg 98 80 - 120


Arsenic 200 194 mg/Kg 97 80 - 120 2 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD

Barium 200 193 mg/Kg 97 80 - 120 4 20

Cadmium 5.00 4.78 mg/Kg 96 80 - 120 2 20

Chromium 20.0 18.0 mg/Kg 90 80 - 120 4 20

Copper 25.0 24.6 mg/Kg 98 80 - 120 2 20

Lead 50.0 47.4 mg/Kg 95 80 - 120 1 20

Selenium 200 192 mg/Kg 96 80 - 120 2 20

Silver 30.0 27.6 mg/Kg 92 80 - 120 2 20

Tin 250 238 mg/Kg 95 80 - 120 2 20

Titanium 250 236 mg/Kg 94 80 - 120 3 20

Zinc 200 194 mg/Kg 97 80 - 120 2 20


Arsenic 23 96.9 124 mg/Kg 104 80 - 120

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 4.8 96.9 99.5 mg/Kg 98 80 - 120

Cadmium 0.52 J 2.42 3.03 mg/Kg 104 80 - 120

Chromium 85 9.69 92.1 4 mg/Kg 76 80 - 120

Copper 15 12.1 26.6 mg/Kg 96 80 - 120

Lead 0.79 J 24.2 24.2 mg/Kg 97 80 - 120

Selenium 1.2 J 96.9 97.2 mg/Kg 99 80 - 120

Silver ND 14.5 14.3 mg/Kg 98 80 - 120

Tin 0.47 J 121 120 mg/Kg 99 80 - 120

Titanium 480 121 594 mg/Kg 92 80 - 120

Zinc 39 96.9 139 mg/Kg 103 80 - 120


Arsenic 23 94.0 126 mg/Kg 109 80 - 120 2 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium 4.8 94.0 99.3 mg/Kg 100 80 - 120 0 20

Cadmium 0.52 J 2.35 3.20 mg/Kg 114 80 - 120 5 20

Chromium 85 9.40 95.3 4 mg/Kg 113 80 - 120 3 20

Copper 15 11.8 26.3 mg/Kg 97 80 - 120 1 20

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Lead 0.79 J 23.5 24.3 mg/Kg 100 80 - 120 0 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Selenium 1.2 J 94.0 98.9 mg/Kg 104 80 - 120 2 20

Silver ND 14.1 13.9 mg/Kg 99 80 - 120 3 20

Tin 0.47 J 118 121 mg/Kg 103 80 - 120 1 20

Titanium 480 118 612 4 mg/Kg 110 80 - 120 3 20

Zinc 39 94.0 142 mg/Kg 109 80 - 120 2 20


RL MDL

Barium ND 0.010 0.0050 mg/L 08/18/16 09:05 08/18/16 23:57 1

MB MB


ND 0.00200.0050 mg/L 08/18/16 09:05 08/18/16 23:57 1Cadmium

ND 0.00250.0050 mg/L 08/18/16 09:05 08/18/16 23:57 1Chromium

ND 0.00500.010 mg/L 08/18/16 09:05 08/18/16 23:57 1Copper

ND 0.00250.0050 mg/L 08/18/16 09:05 08/18/16 23:57 1Lead

ND 0.00610.010 mg/L 08/18/16 09:05 08/18/16 23:57 1Selenium

ND 0.00500.010 mg/L 08/18/16 09:05 08/18/16 23:57 1Silver

ND 0.0100.020 mg/L 08/18/16 09:05 08/18/16 23:57 1Strontium

ND 0.0120.10 mg/L 08/18/16 09:05 08/18/16 23:57 1Tin

ND 0.00250.0050 mg/L 08/18/16 09:05 08/18/16 23:57 1Titanium

ND 0.0100.020 mg/L 08/18/16 09:05 08/18/16 23:57 1Zinc


RL MDL

Arsenic ND 0.010 0.0050 mg/L 08/18/16 09:05 08/20/16 16:03 1

MB MB



Arsenic 1.00 0.905 mg/L 91 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Barium 1.00 0.923 mg/L 92 80 - 120

Cadmium 1.00 0.927 mg/L 93 80 - 120

Chromium 1.00 0.921 mg/L 92 80 - 120

Copper 1.00 0.924 mg/L 92 80 - 120

Lead 1.00 0.953 mg/L 95 80 - 120

Selenium 1.00 0.868 mg/L 87 80 - 120

Silver 0.500 0.450 mg/L 90 80 - 120

Strontium 1.00 0.915 mg/L 91 80 - 120

Tin 1.00 0.908 mg/L 91 80 - 120

Titanium 1.00 0.944 mg/L 94 80 - 120

Zinc 1.00 0.894 mg/L 89 80 - 120

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Arsenic 1.00 0.937 mg/L 94 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits


Arsenic 0.10 B 1.00 1.10 mg/L 99 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Barium 0.022 1.00 0.974 mg/L 95 75 - 125

Cadmium ND 1.00 0.905 mg/L 91 75 - 125

Chromium 0.12 1.00 1.08 mg/L 96 75 - 125

Copper ND 1.00 1.13 mg/L 113 75 - 125

Lead ND L 1.00 0.970 mg/L 97 75 - 125

Selenium ND 1.00 0.935 mg/L 93 75 - 125

Silver ND 0.500 0.536 mg/L 107 75 - 125

Strontium 14 1.00 15.7 4 mg/L 215 75 - 125

Tin ND 1.00 0.916 mg/L 92 75 - 125

Titanium 0.019 1.00 1.04 mg/L 103 75 - 125

Zinc ND 1.00 0.947 mg/L 95 75 - 125


Arsenic 0.11 1.00 1.10 mg/L 99 75 - 125

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Arsenic 0.10 B 1.00 1.08 mg/L 98 75 - 125 1 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD

Barium 0.022 1.00 0.955 mg/L 93 75 - 125 2 20

Cadmium ND 1.00 0.919 mg/L 92 75 - 125 2 20

Chromium 0.12 1.00 1.09 mg/L 97 75 - 125 1 20

Copper ND 1.00 1.08 mg/L 108 75 - 125 5 20

Lead ND L 1.00 0.917 mg/L 92 75 - 125 6 20

Selenium ND 1.00 0.908 mg/L 91 75 - 125 3 20

Silver ND 0.500 0.520 mg/L 104 75 - 125 3 20

Strontium 14 1.00 15.5 4 mg/L 198 75 - 125 1 20

Tin ND 1.00 0.881 mg/L 88 75 - 125 4 20

Titanium 0.019 1.00 0.998 mg/L 98 75 - 125 5 20

Zinc ND 1.00 0.930 mg/L 93 75 - 125 2 20

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Arsenic 0.11 1.00 1.13 mg/L 102 75 - 125 3 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD



RL MDL

Mercury ND 0.00020 0.00010 mg/L 08/09/16 19:08 08/10/16 16:19 1

MB MB



Mercury 0.00800 0.00803 mg/L 100 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

Client Sample ID: Matrix SpikeLab Sample ID: 440-154741-M-1-C MSMatrix: Water Prep Type: Total/NAAnalysis Batch: 348253 Prep Batch: 347966

Mercury ND 0.00800 0.00827 mg/L 103 70 - 130

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits

Client Sample ID: Matrix Spike DuplicateLab Sample ID: 440-154741-M-1-D MSDMatrix: Water Prep Type: Total/NAAnalysis Batch: 348253 Prep Batch: 347966

Mercury ND 0.00800 0.00814 mg/L 102 70 - 130 2 20

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD



RL MDL

Mercury ND 0.012 0.0036 mg/Kg 08/11/16 13:23 08/12/16 09:58 1

MB MB



Mercury 0.100 0.0857 mg/Kg 86 80 - 120

Analyte

LCS LCS


Spike

Added

%Rec.

Limits

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Method: 7471A - Mercury (CVAA) (Continued)


Mercury 0.100 0.0842 mg/Kg 84 80 - 120 2 20

Analyte

LCSD LCSD


Spike

Added

%Rec.

Limits LimitRPD

RPD


Mercury ND 0.113 0.106 mg/Kg 94 80 - 120☼

Analyte

MS MS


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits


Mercury ND 0.115 0.103 mg/Kg 89 80 - 120 4 20☼

Analyte

MSD MSD


Spike

Added

Sample

Result

Sample

Qualifier

%Rec.

Limits LimitRPD

RPD


Client Sample ID: DU-3-1-20160801Lab Sample ID: 580-61481-1 DUMatrix: Solid Prep Type: Total/NAAnalysis Batch: 224669


Analyte

DU DU


Sample

Result

Sample

Qualifier LimitRPD

RPD

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Prep 5035 08/01/16 09:00 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











Prep 5035 08/01/16 09:15 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA










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Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











Prep 5035 08/01/16 09:30 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA









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Prep 5035 08/01/16 09:45 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











Prep 5035 08/01/16 11:00 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA










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Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











Prep 5035 08/01/16 11:30 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA









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Prep 5035 08/01/16 11:45 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











Prep 3520C 08/10/16 09:36 BMN348082 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA


Analysis 8015B 1 347941 08/10/16 06:41 IM TAL IRVTotal/NA

Prep 3510C 347843 08/09/16 13:20 AP TAL IRVTotal/NA



Analysis 6010B 1 350369 08/19/16 00:11 ND TAL IRVTotal Recoverable




Analysis 7470A 1 348253 08/10/16 16:35 B1H TAL IRVTotal/NA

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Prep 5035 08/01/16 13:30 ATL347564 TAL IRV

Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA













Type

Batch Batch


Prepared

or Analyzed

Batch

Number

Dilution

Factor

Total/NA











TAL SEA = TestAmerica Seattle, 5755 8th Street East, Tacoma, WA 98424, TEL (253)922-2310

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Laboratory: TestAmerica SeattleAll certifications held by this laboratory are listed. Not all certifications are applicable to this report.


Alaska (UST) UST-02210State Program 03-02-17


L-A-B DoD ELAP L2236 01-19-19

L-A-B ISO/IEC 17025 L2236 01-19-19

Montana (UST) State Program 8 N/A 04-30-20

Oregon NELAP 10 WA100007 11-06-16


USDA Federal P330-14-00126 04-08-17








Alaska CA0153110State Program 06-30-17



California State Program 9 CA ELAP 2706 06-30-18



Kansas NELAP Secondary AB 7 E-10420 07-31-16 *

Nevada State Program 9 CA015312016-2 07-31-17 *



Oregon NELAP 10 4028 01-29-17

USDA Federal P330-09-00080 07-08-18


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580-61481-1 DU-3-1-20160801 Solid 08/01/16 09:00 08/03/16 09:40

580-61481-2 DU-3-2-20160801 Solid 08/01/16 09:15 08/03/16 09:40

580-61481-3 DU-3-3-20160801 Solid 08/01/16 09:30 08/03/16 09:40

580-61481-4 DU-4-20160801 Solid 08/01/16 09:45 08/03/16 09:40

580-61481-5 DU-6-20160801 Solid 08/01/16 11:00 08/03/16 09:40

580-61481-6 DU-2A-20160801 Solid 08/01/16 11:30 08/03/16 09:40

580-61481-7 DU-2B-20160801 Solid 08/01/16 11:45 08/03/16 09:40

580-61481-8 DU-5-20160801 Water 08/01/16 12:00 08/03/16 09:40

580-61481-9 DU-1-20160801 Solid 08/01/16 13:30 08/03/16 09:40

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Login Number: 61481


Creator: Gonzales, Steve

List Source: TestAmerica Seattle

List Number: 1








TrueCOC is present.











TrueSample Preservation Verified.







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Login Number: 61481


Creator: Salas, Margarita


List Creation: 08/06/16 10:12 AMList Number: 2








TrueCOC is present.


















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Login Number: 61481


Creator: Ornelas, Olga










TrueCOC is present.


















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Sea Engineering, Inc. b

APPENDIX B: BLACK POT BEACH GRAIN SIZE ANALYSIS DATA SHEET

Client: Sea Engineer259-7566 Log # : 32381Job # : Black Pot

Date Sampled: not reported Date Received: CL/DC

Size Fraction Data Sheet

Size (mm) >4.00 4.00-2.00 2.00-1.00 1.00-.500 .500-.355 .355-.250 .250-.125 .125-.075 .075-.063 .063-.044 .044-.031 .031-.022 .022-.016.016-.0078

.0078-.0039

.0039-.00195

.00195-.00098

.00098-.00049 <.00049 Total

phi -2 -1 0 1 3 4.5 5 5.5 6 7 8 9 10 11 12+

2A 0.00 0.09 0.24 0.49 0.64 2.88 69.66 14.41 0.17 0.11 0.00 0.10 0.00 0.14 0.00 0.02 0.04 0.10 0.02 89.11

0.00% 0.10% 0.27% 0.55% 0.72% 3.23% 78.17% 16.17% 0.19% 0.12% 0.00% 0.11% 0.00% 0.16% 0.00% 0.02% 0.04% 0.11% 0.02% 100.00%

2B 0.17 0.22 0.12 1.15 2.05 6.89 53.13 7.67 0.27 0.07 0.17 0.16 0.04 0.07 0.12 0.02 0.11 0.18 0.00 72.61

0.23% 0.30% 0.17% 1.58% 2.82% 9.49% 73.17% 10.56% 0.37% 0.10% 0.23% 0.22% 0.06% 0.10% 0.17% 0.03% 0.15% 0.25% 0.00% 100.00%

3 0.04 0.00 0.04 0.21 0.75 4.78 75.27 16.26 0.57 0.27 0.08 0.27 0.00 0.82 0.16 0.07 0.14 0.45 0.18 100.36

0.04% 0.00% 0.04% 0.21% 0.75% 4.76% 75.00% 16.20% 0.57% 0.27% 0.08% 0.27% 0.00% 0.82% 0.16% 0.07% 0.14% 0.45% 0.18% 100.00%

4 0.00 0.00 0.09 0.64 1.26 4.57 64.00 12.39 0.20 0.05 0.08 0.05 0.06 0.06 0.00 0.00 0.10 0.34 0.11 84.00

0.00% 0.00% 0.11% 0.76% 1.50% 5.44% 76.19% 14.75% 0.24% 0.06% 0.10% 0.06% 0.07% 0.07% 0.00% 0.00% 0.12% 0.40% 0.13% 100.00%

5 0.00 0.08 0.21 0.75 1.25 3.34 48.67 6.18 0.08 0.03 0.03 0.06 0.00 0.00 0.01 0.00 0.00 0.15 0.08 60.92

0.00% 0.13% 0.34% 1.23% 2.05% 5.48% 79.89% 10.14% 0.13% 0.05% 0.05% 0.10% 0.00% 0.00% 0.02% 0.00% 0.00% 0.25% 0.13% 100.00%

4 Dup 0.00 0.00 0.07 0.66 1.26 4.63 64.08 12.36 0.17 0.05 0.08 0.05 0.06 0.06 0.00 0.00 0.10 0.34 0.11 84.08

0.00% 0.00% 0.08% 0.78% 1.50% 5.51% 76.21% 14.70% 0.20% 0.06% 0.10% 0.06% 0.07% 0.07% 0.00% 0.00% 0.12% 0.40% 0.13% 100.00%

Notes (These are not usually included in the data report.) Samples wet sieved with 0.63 mm then fines decanted after 48 hr settling. Minimal fines in samples limits the accuracy of the silt and clay method (hence some 0 values).

Attn: ANDY/CHRIS Sample type: sand

2 4

Date/Analyst: various

Government & Nonprofit

Black Pot Beach Park Coastal Assessment