Metrohm inline sample preparation

IC Sample Preparation*ic_sampl_prep_26062003_e.ppt
*ic_sampl_prep_26062003_e.ppt
Big particles are flushed away
and do not clog the membrane
High flow on the sample side
Low flow on the acceptor side
Strong concentration gradient
No equilibrium concentration
Cellulose acetate membrane
Sample volume 10 mL
Equilibrium concentration
No filtration, no pre concentration
Unique technique, that had significantly improves the field of application for IC
Inline sample preparation
1
Acetate
2.3
2
Formate
22.0
3
Chloride
13.0
4
Carbonate
n.q.
5
Nitrate
4.5
6
Phosphate
16.0
7
Sulfate
8.5
8
Oxalate
12.0
ppt
Inline sample preparation
Metrosep Dual 2
E
E
B
377.unknown
1
Formate
n.q.
2
Chloride
0.03
3
Nitrite
n.q.
4
Bromide
0.95
5
Nitrat
0.04
6
Carbonate
n.q.
7
Sulfate
0.13
ppm
Tartaric-/dipicolinic acid; 4.0/0.75 mmol/L; 7 mol HCl, 10 µL loop
# 1: Transfer of 2 mL ultrapure water to the preconcentrator
Blank value
# 2: Transfer of 2 mL ultrapure water to the preconcentrator. Valve B is thrown from fill to inject and back once
Calibration level 1
# 3: Transfer of 2 mL ultrapure water to the preconcentrator. Valve B is thrown from fill to inject and back twice
Calibration level 2
# 4: Transfer of 2 mL ultrapure water to the preconcentrator. Valve B is thrown from fill to inject and back three times
Calibration level 3, etc

Metrohm inline sample preparation

Text of Metrohm inline sample preparation

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