J46192-1 Nj Full Package Final Report

J46192-1 Nj_Full_Package Final ReportFor: Conestoga-Rovers & Associates, Inc.
2055 Niagara Falls Blvd., Suite 3 Niagara Falls, NY 14304
Attention: Ms. Sue Scrocchi
_____________________________________________
Approved for release. Jamie Capaci Project Manager I 10/31/2012 3:16 PM
Jamie Capaci Project Manager I
[email protected] 10/31/2012
cc: Chris Barton
The test results in this report meet all NELAP requirements unless specified within the case narrative. Pursuant to NELAP, this report may not be reproduced, except in full, without the written approval of the laboratory. All questions regarding this report should be directed to the TestAmerica Edison Project Manager.
TestAmerica Edison Certifications and Approvals: Connecticut: CTDOH #PH-0200, New Jersey: NJDEP (NELAP) #12028, New York: NYDOH (NELAP) #11452, NYDOH (ELAP) #11452, Pennsylvania: PADEP (NELAP) 68-00522 and Rhode Island: RIDOH LAO00132
TestAmerica Laboratories, Inc.
Tel (732) 549-3900 Fax (732) 549-3679 www.testamericainc.com
10/31/2012Page 1 of 813
Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Report Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
Executive Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 7
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11
GC/MS VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73
Method 8260 DEL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 73 Method 8260 DEL QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 74 Method 8260 DEL Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 85 Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 134
Method 8260 DEL ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 134 Method 8260 DEL CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 158
Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 168 Method 8260 DEL Tune Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 168 Method 8260 DEL Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 177 Method 8260 DEL LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 182 Method 8260 DEL MS/MSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 187
10/31/2012Page 2 of 813
Table of Contents Method 8260 DEL Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 197 Method 8260 DEL Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 199
Inorganic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 203
Met Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 204
Met Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 205
Met QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 213 Met ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 213 Met Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 222 Met ICSA/ICSAB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 233 Met MS/MSD/PDS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 237 Met Dup/Trip . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 242 Met LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 245 Met Serial Dilution . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 250
Met MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 255
Met Raw Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 283
Met Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 801
Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 813
10/31/2012Page 3 of 813
Report Number: 460-46192-1
This case narrative is in the form of an exception report, where only the anomalies related to this report, method specific performance
and/or QA/QC issues are discussed. If there are no issues to report, this narrative will include a statement that documents that there are
no relevant data issues.
It should be noted that samples with elevated Reporting Limits (RLs) as a result of a dilution may not be able to satisfy customer reporting
limits in some cases. Such increases in the RLs are unavoidable but acceptable consequence of sample dilution that enables
quantification of target analytes or interferences which exceed the calibration range of the instrument.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 10/19/2012; the samples arrived in good condition, properly preserved and on ice. The temperature of the
coolers at receipt was 4.0 C.
Note: All samples which require thermal preservation are considered acceptable if the arrival temperature is within 2C of the required
temperature or method specified range. For samples with a specified temperature of 4C, samples with a temperature ranging from just
above freezing temperature of water to 6C shall be acceptable. Samples that are hand delivered immediately following collection may not
meet these criteria, however they will be deemed acceptable according to NELAC standards, if there is evidence that the chilling process
has begun, such as arrival on ice, etc.
DISSOLVED METALS
Samples 460-46192-1 through 460-46192-4 were analyzed for Dissolved metals in accordance with EPA SW-846 Method 6010B. The
samples were prepared on 10/24/2012 and analyzed on 10/24/2012 and 10/25/2012.
Sample 460-46192-1(5X) required dilution prior to analysis. The reporting limits have been adjusted accordingly.
No difficulties were encountered during the dissolved metals analyses.
All quality control parameters were within the acceptance limits.
TOTAL METALS
Samples 460-46192-1 through 460-46192-4 were analyzed for total metals in accordance with EPA SW-846 Method 6010B. The samples
were prepared and analyzed on 10/24/2012.
No difficulties were encountered during the metals analyses.
DISSOLVED MERCURY
Samples 460-46192-1 through 460-46192-4 were analyzed for dissolved mercury in accordance with EPA SW-846 Methods 7470A. The
samples were prepared and analyzed on 10/26/2012.
No difficulties were encountered during the dissolved mercury analyses.
TOTAL MERCURY
Samples 460-46192-1 through 460-46192-4 were analyzed for total mercury in accordance with EPA SW-846 Methods 7470A. The
samples were prepared and analyzed on 10/23/2012 and 10/24/2012.
No difficulties were encountered during the Hg analyses.
VOLATILE ORGANIC COMPOUNDS (GC-MS)
10/31/2012Page 4 of 813
Method 8260B. The samples were analyzed on 10/25/2012.
The matrix spike / matrix spike duplicate (MS/MSD) recoveries and %RPD for batch 133510 were outside control limits for multiple
analytes. The associated laboratory control sample (LCS) recoveries met acceptance criteria.
No other difficulties were encountered during the volatiles analyses.
All other quality control parameters were within the acceptance limits.
10/31/2012Page 5 of 813
Client Sample IDLab Sample ID Client Matrix Sampled Received
Date/Time Date/Time
460-46192-1 WG-17338-101812-MW29-MM-
460-46192-2 WG-17338-101812-MW28-MM-
460-46192-3 WG-17338-101812-MW35-MM-
460-46192-4 WG-17338-101812-MW27-MM-
460-46192-4MS WG-17338-101812-MW27-MM-
460-46192-4MSD WG-17338-101812-MW27-MM-
460-46192-4DU WG-17338-101812-MW27-MM-
460-46192-5 TB-17338-101812-263 Water 10/18/2012 0000 10/19/2012 1845
TestAmerica Edison 10/31/2012Page 6 of 813
EXECUTIVE SUMMARY - Detections
Analyte Result
Qualifier
1.0 ug/L 8260B2.6cis-1,2-Dichloroethene
1.0 ug/L 8260B5.9Ethylbenzene
1.0 ug/L 8260B3.6Cyclohexane
1.0 ug/L 8260B11Benzene
1.0 ug/L 8260B3.5Methylcyclohexane
1.0 ug/L 8260B1.5Toluene
Analyte Result
Qualifier
1.0 ug/L 8260B0.097 JIsopropylbenzene
40.0 ug/L 6010B6.3 JNickel
30.0 ug/L 6010B22.6 JZinc
Analyte Result
Qualifier
10.0 ug/L 6010B6.6 JSelenium
Analyte Result
Qualifier
30.0 ug/L 6010B45.4Zinc
METHOD SUMMARY
Preparation MethodMethodLab LocationDescription
Metals (ICP) TAL EDI SW846 6010B
Preparation, Total Metals TAL EDI SW846 3010A
Metals (ICP) TAL EDI SW846 6010B
Preparation, Total Metals TAL EDI SW846 3010A
Sample Filtration TAL EDI FILTRATION
Mercury (CVAA) TAL EDI SW846 7470A
Preparation, Mercury TAL EDI SW846 7470A
Mercury (CVAA) TAL EDI SW846 7470A
Preparation, Mercury TAL EDI SW846 7470A
Sample Filtration TAL EDI FILTRATION
Lab References:
METHOD / ANALYST SUMMARY
Method Analyst Analyst ID
Tupayachi, Audberto ATSW846 8260B
Staib, Thomas TSSW846 7470A
Client Sample ID:
Lab Sample ID:
0.060 U 1.00.0601,1,1-Trichloroethane
0.22 U 1.00.22Dichlorodifluoromethane
0.10 U 1.00.10Chloromethane
31 1.00.14Vinyl chloride
0.18 U 1.00.18Bromomethane
0.40 U 1.00.401,2-Dibromo-3-Chloropropane
0.21 U 1.00.211,2-Dichlorobenzene
0.15 U 1.00.15Trichlorofluoromethane
0.090 U 1.00.0901,1-Dichloroethene
0.090 U 1.00.0901,2-Dichloropropane
0.080 U 1.00.0801,1,2-Trichloro-1,2,2-trifluoroethane
2.7 U 5.02.7Acetone
0.17 U 1.00.17Chloroethane
0.13 U 1.00.131,1-Dichloroethane
Analytical Data
Client Sample ID:
Lab Sample ID:
0.34 U 1.00.341,2,4-Trichlorobenzene
Analytical Data
Client Sample ID:
Lab Sample ID:
Analytical Data
Client Sample ID:
Lab Sample ID:
0.18 U 1.00.18cis-1,2-Dichloroethene
Analytical Data
Client Sample ID:
Lab Sample ID:
Analytical Data
Client Sample ID:
Lab Sample ID:
Analytical Data
Client Sample ID:
Lab Sample ID:
Analytical Data
Client Sample ID:
Lab Sample ID:
Analytical Data
Client Sample ID:
Lab Sample ID:
Analytical Data
Client Sample ID:
Lab Sample ID:
Analytical Data
Client Sample ID:
Lab Sample ID:
Analytical Data
Client Sample ID:
Lab Sample ID:
Analytical Data
Client Sample ID:
Lab Sample ID:
Analytical Data
Client Sample ID:
Lab Sample ID:
Analytical Data
Client Sample ID:
Lab Sample ID:
Analytical Data
Client Sample ID:
Lab Sample ID:
10/24/2012 0759
0.82 U 5.00.82Cadmium
7.4 U 10.07.4Antimony
0.78 U 2.00.78Beryllium
5.2 U 10.05.2Thallium
5.0 U 40.05.0Nickel
1.3 U 10.01.3Silver
3.7 U 5.03.7Arsenic
7.8 U 25.07.8Copper
4.0 U 5.04.0Lead
10/24/2012 0957
0.82 U 5.00.82Cadmium
5.0 U 40.05.0Nickel
1.3 U 10.01.3Silver
3.7 U 5.03.7Arsenic
7.8 U 25.07.8Copper
4.0 U 5.04.0Lead
5.8 U 30.05.8Zinc
Analytical Data
Client Sample ID:
Lab Sample ID:
606 2005.9Barium
104000 5000305Calcium
36600 15073.6Iron
10/24/2012 0957
257000 250004100Sodium
10/23/2012 1650
0.16 U 0.200.16Mercury
7470A Mercury (CVAA)-Dissolved
7470A Instrument ID:
10/26/2012 1717
0.16 U 0.200.16Mercury
Analytical Data
Client Sample ID:
Lab Sample ID:
10/24/2012 0759
0.82 U 5.00.82Cadmium
6.3 J 40.05.0Nickel
1.3 U 10.01.3Silver
10/24/2012 0957
0.82 U 5.00.82Cadmium
6.4 J 40.05.0Nickel
1.3 U 10.01.3Silver
3.7 U 5.03.7Arsenic
7.8 U 25.07.8Copper
4.0 U 5.04.0Lead
22.6 J 30.05.8Zinc
5.8 U 10.05.8Selenium
4.5 U 10.04.5Chromium
Analytical Data
Client Sample ID:
Lab Sample ID:
5240 5000525Potassium
433 2005.9Barium
30400 5000305Calcium
13100 15073.6Iron
10/23/2012 1650
0.16 U 0.200.16Mercury
10/26/2012 1717
0.16 U 0.200.16Mercury
Analytical Data
Client Sample ID:
Lab Sample ID:
10/24/2012 0759
0.82 U 5.00.82Cadmium
19.7 J 40.05.0Nickel
1.3 U 10.01.3Silver
3.7 U 5.03.7Arsenic
7.8 U 25.07.8Copper
4.0 U 5.04.0Lead
5.8 U 30.05.8Zinc
5.8 U 10.05.8Selenium
10/24/2012 0957
0.82 U 5.00.82Cadmium
20.9 J 40.05.0Nickel
1.3 U 10.01.3Silver
3.7 U 5.03.7Arsenic
7.8 U 25.07.8Copper
4.0 U 5.04.0Lead
5.8 U 30.05.8Zinc
6.6 J 10.05.8Selenium
Analytical Data
Client Sample ID:
Lab Sample ID:
5330 5000525Potassium
301 2005.9Barium
48200 5000305Calcium
10/23/2012 1650
0.16 U 0.200.16Mercury
10/26/2012 1717
0.16 U 0.200.16Mercury
Analytical Data
Client Sample ID:
Lab Sample ID:
10/24/2012 0759
0.82 U 5.00.82Cadmium
26.0 J 40.05.0Nickel
1.3 U 10.01.3Silver
3.7 U 5.03.7Arsenic
7.8 U 25.07.8Copper
4.0 U 5.04.0Lead
10/24/2012 0957
0.82 U 5.00.82Cadmium
26.8 J 40.05.0Nickel
1.3 U 10.01.3Silver
3.7 U 5.03.7Arsenic
7.8 U 25.07.8Copper
4.0 U 5.04.0Lead
Analytical Data
Client Sample ID:
Lab Sample ID:
4970 J 5000525Potassium
108 J 2005.9Barium
10/24/2012 1700
0.16 U 0.200.16Mercury
10/26/2012 1717
0.53 0.200.16Mercury
Quality Control Results
Surrogate Recovery Report
DCA TOL BFB
%Rec %Rec %Rec
460-46192-4 MS WG-17338-101812-M
WaterClient Matrix:
WaterClient Matrix:
4-Bromofluorobenzene 100 70 - 130
Cas Number Analyte RT Est. Result Qual
Tentatively Identified Compound None
Water
1.0
Client Matrix:
20.0 18.8 94 61 - 144Vinyl chloride
20.0 18.9 94 55 - 153Bromomethane
20.0 19.0 95 70 - 1161,2-Dibromo-3-Chloropropane
20.0 19.2 96 82 - 1221,2-Dichlorobenzene
20.0 17.2 86 69 - 147Trichlorofluoromethane
20.0 19.7 99 56 - 1391,1-Dichloroethene
20.0 19.2 96 80 - 1201,2-Dichloropropane
20.0 18.4 92 47 - 1391,1,2-Trichloro-1,2,2-trifluoroethane
20.0 19.4 97 45 - 156Acetone
20.0 21.2 106 58 - 139Carbon disulfide
20.0 18.7 94 50 - 151Methyl acetate
20.0 18.8 94 79 - 119Methylene Chloride
20.0 18.6 93 75 - 122trans-1,2-Dichloroethene
20.0 19.2 96 80 - 120Chlorodibromomethane
20.0 17.7 89 71 - 115Methyl tert-butyl ether
20.0 18.6 93 69 - 145Chloroethane
20.0 18.8 94 78 - 1221,1-Dichloroethane
20.0 19.3 97 80 - 120cis-1,2-Dichloroethene
20.0 17.9 89 65 - 1142-Butanone (MEK)
20.0 19.3 96 82 - 123Chloroform
20.0 19.2 96 79 - 126Ethylbenzene
20.0 19.1 95 58 - 133Cyclohexane
20.0 19.2 96 73 - 120Carbon tetrachloride
20.0 19.7 98 83 - 124Benzene
20.0 19.2 96 74 - 1181,2-Dichloroethane
20.0 20.5 102 78 - 119Trichloroethene
20.0 19.1 96 61 - 129Methylcyclohexane
20.0 19.5 98 79 - 119Dichlorobromomethane
20.0 18.9 95 80 - 120cis-1,3-Dichloropropene
20.0 18.2 91 53 - 1204-Methyl-2-pentanone (MIBK)
20.0 19.5 97 80 - 120Toluene
20.0 18.8 94 78 - 118trans-1,3-Dichloropropene
20.0 19.3 96 79 - 1191,1,2-Trichloroethane
20.0 19.0 95 68 - 139Tetrachloroethene
20.0 18.4 92 53 - 1212-Hexanone
20.0 18.9 95 78 - 1181,2-Dibromoethane
20.0 19.4 97 81 - 121Chlorobenzene
60.0 57.4 96 76 - 121Xylenes, Total
20.0 19.2 96 69 - 112Styrene
20.0 18.9 95 73 - 123Bromoform
20.0 19.0 95 80 - 125Isopropylbenzene
20.0 18.0 90 74 - 1261,1,2,2-Tetrachloroethane
20.0 19.2 96 81 - 1261,3-Dichlorobenzene
Water
1.0
Client Matrix:
Surrogate % Rec Acceptance Limits
4-Bromofluorobenzene 101 70 - 130
Dilution:
Dilution:
Water
1.0
1.0
10/25/2012 1321
73 120 74 - 128 49 30 F F1,1,1-Trichloroethane
63 106 46 - 145 51 30 FDichlorodifluoromethane
67 112 58 - 146 50 30 FChloromethane
70 115 61 - 144 49 30 FVinyl chloride
77 118 55 - 153 42 30 FBromomethane
71 115 70 - 116 47 30 F1,2-Dibromo-3-Chloropropane
74 118 82 - 122 45 30 F F1,2-Dichlorobenzene
97 162 69 - 147 50 30 FTrichlorofluoromethane
69 107 56 - 139 44 30 F1,1-Dichloroethene
77 121 80 - 120 45 30 F F1,2-Dichloropropane
69 115 47 - 139 49 30 F1,1,2-Trichloro-1,2,2-trifluoroethane
74 103 45 - 156 32 30 FAcetone
70 114 58 - 139 47 30 FCarbon disulfide
54 84 50 - 151 42 30 FMethyl acetate
74 118 79 - 119 47 30 F FMethylene Chloride
67 109 75 - 122 47 30 F Ftrans-1,2-Dichloroethene
74 119 80 - 120 46 30 F FChlorodibromomethane
68 108 71 - 115 45 30 F FMethyl tert-butyl ether
90 138 69 - 145 42 30 FChloroethane
69 113 78 - 122 48 30 F F1,1-Dichloroethane
74 117 80 - 120 45 30 F Fcis-1,2-Dichloroethene
68 107 65 - 114 45 30 F2-Butanone (MEK)
73 122 82 - 123 50 30 F FChloroform
74 120 79 - 126 47 30 F FEthylbenzene
79 122 58 - 133 43 30 FCyclohexane
75 121 73 - 120 47 30 FCarbon tetrachloride
76 117 83 - 124 42 30 F FBenzene
71 112 74 - 118 44 30 F F1,2-Dichloroethane
75 119 78 - 119 45 30 F FTrichloroethene
96 135 61 - 129 33 30 FMethylcyclohexane
80 127 79 - 119 45 30 FDichlorobromomethane
73 115 80 - 120 45 30 F Fcis-1,3-Dichloropropene
69 108 53 - 120 44 30 F4-Methyl-2-pentanone (MIBK)
Dilution:
Dilution:
Water
1.0
1.0
10/25/2012 1321
74 119 80 - 120 46 30 F FToluene
73 117 78 - 118 46 30 F Ftrans-1,3-Dichloropropene
76 117 79 - 119 42 30 F F1,1,2-Trichloroethane
75 119 68 - 139 46 30 FTetrachloroethene
67 115 53 - 121 53 30 F2-Hexanone
72 115 78 - 118 46 30 F F1,2-Dibromoethane
75 121 81 - 121 47 30 F FChlorobenzene
74 119 76 - 121 46 30 F FXylenes, Total
75 120 69 - 112 46 30 FStyrene
71 116 73 - 123 48 30 F FBromoform
74 119 80 - 125 47 30 F FIsopropylbenzene
70 116 74 - 126 49 30 F F1,1,2,2-Tetrachloroethane
68 106 66 - 120 44 30 F1,2,4-Trichlorobenzene
Surrogate Acceptance LimitsMS % Rec MSD % Rec
1,2-Dichloroethane-d4 (Surr) 92 91 70 - 130
4-Bromofluorobenzene 97 101 70 - 130
Toluene-d8 (Surr) 100 100 70 - 130
Water
Method: 8260B
Preparation: 5030B
Units: ug/L460-46192-4 460-46192-4MS Lab Sample ID: MSD Lab Sample ID:
Matrix Spike/
Analysis Date:
Prep Date:
Leach Date:
10/25/2012 1321
0.060 U 20.0 20.0 14.6 24.0F F1,1,1-Trichloroethane
0.22 U 20.0 20.0 12.7 21.2 FDichlorodifluoromethane
0.10 U 20.0 20.0 13.4 22.3 FChloromethane
0.14 U 20.0 20.0 14.0 23.1 FVinyl chloride
0.18 U 20.0 20.0 15.3 23.6 FBromomethane
0.40 U 20.0 20.0 14.2 22.9 F1,2-Dibromo-3-Chloropropane
0.21 U 20.0 20.0 14.9 23.6F F1,2-Dichlorobenzene
0.15 U 20.0 20.0 19.5 32.4 FTrichlorofluoromethane
0.090 U 20.0 20.0 13.7 21.5 F1,1-Dichloroethene
0.090 U 20.0 20.0 15.3 24.2F F1,2-Dichloropropane
0.080 U 20.0 20.0 13.9 22.9 F1,1,2-Trichloro-1,2,2-trifluoroethane
2.7 U 20.0 20.0 14.8 20.5 FAcetone
0.13 U 20.0 20.0 14.1 22.8 FCarbon disulfide
0.34 U 20.0 20.0 10.9 16.7 FMethyl acetate
0.18 U 20.0 20.0 14.7 23.7F FMethylene Chloride
0.13 U 20.0 20.0 13.5 21.7F Ftrans-1,2-Dichloroethene
0.20 U 20.0 20.0 14.9 23.8F FChlorodibromomethane
0.14 U 20.0 20.0 13.7 21.5F FMethyl tert-butyl ether
0.17 U 20.0 20.0 18.0 27.5 FChloroethane
0.13 U 20.0 20.0 13.8 22.6F F1,1-Dichloroethane
0.18 U 20.0 20.0 14.9 23.4F Fcis-1,2-Dichloroethene
2.3 U 20.0 20.0 13.6 21.4 F2-Butanone (MEK)
0.080 U 20.0 20.0 14.7 24.4F FChloroform
0.21 J 20.0 20.0 15.1 24.3F FEthylbenzene
0.16 U 20.0 20.0 15.8 24.5 FCyclohexane
0.060 U 20.0 20.0 14.9 24.2 FCarbon tetrachloride
0.080 U 20.0 20.0 15.2 23.4F FBenzene
0.19 U 20.0 20.0 14.3 22.5F F1,2-Dichloroethane
0.090 U 20.0 20.0 15.0 23.9F FTrichloroethene
0.14 U 20.0 20.0 19.2 26.9 FMethylcyclohexane
0.12 U 20.0 20.0 16.0 25.3 FDichlorobromomethane
0.18 U 20.0 20.0 14.6 23.0F Fcis-1,3-Dichloropropene
0.99 U 20.0 20.0 13.9 21.6 F4-Methyl-2-pentanone (MIBK)
0.15 U 20.0 20.0 14.9 23.8F FToluene
0.24 U 20.0 20.0 14.6 23.3F Ftrans-1,3-Dichloropropene
0.19 U 20.0 20.0 15.3 23.3F F1,1,2-Trichloroethane
0.10 U 20.0 20.0 14.9 23.8 FTetrachloroethene
0.50 U 20.0 20.0 13.4 23.0 F2-Hexanone
0.28 U 20.0 20.0 14.4 23.0F F1,2-Dibromoethane
0.11 U 20.0 20.0 15.1 24.3F FChlorobenzene
0.95 J 60.0 60.0 45.4 72.6F FXylenes, Total
0.12 U 20.0 20.0 15.0 24.0 FStyrene
0.19 U 20.0 20.0 14.2 23.2F FBromoform
Water
Method: 8260B
Preparation: 5030B
Units: ug/L460-46192-4 460-46192-4MS Lab Sample ID: MSD Lab Sample ID:
Matrix Spike/
Analysis Date:
Prep Date:
Leach Date:
10/25/2012 1321
0.080 U 20.0 20.0 14.7 23.8F FIsopropylbenzene
0.16 U 20.0 20.0 14.0 23.2F F1,1,2,2-Tetrachloroethane
0.34 U 20.0 20.0 13.6 21.1 F1,2,4-Trichlorobenzene
WaterClient Matrix:
Water
1.0
Client Matrix:
Water
1.0
44.8 500 544.8 100 75 - 125Zinc
5.8 U 2000 1916 96 75 - 125Selenium
4.5 U 200 203.7 102 75 - 125Chromium
85400 20000 105200 99 75 - 125 4Sodium
4800 J 20000 24450 98 75 - 125Potassium
107 J 2000 2181 104 75 - 125Barium
41300 20000 62270 105 75 - 125Calcium
262 1000 1283 102 75 - 125Iron
4.0 U 500 500.2 100 75 - 125Vanadium
27600 20000 47660 101 75 - 125Magnesium
621 2000 2865 112 75 - 125Aluminum
1360 500 1867 102 75 - 125Manganese
22.4 J 500 524.2 100 75 - 125Cobalt
Water
1.0
Lab Sample ID:
Water
1.0
Lab Sample ID:
44.8 500 513.3 94 75 - 125Zinc
5.8 U 2000 1806 90 75 - 125Selenium
4.5 U 200 190.3 95 75 - 125Chromium
85400 20000 102100 84 75 - 125Sodium
4800 J 20000 23240 92 75 - 125Potassium
107 J 2000 2061 98 75 - 125Barium
41300 20000 60260 95 75 - 125Calcium
262 1000 1215 95 75 - 125Iron
4.0 U 500 470.3 94 75 - 125Vanadium
27600 20000 45590 90 75 - 125Magnesium
621 2000 2458 92 75 - 125Aluminum
1360 500 1797 88 75 - 125Manganese
22.4 J 500 495.3 95 75 - 125Cobalt
ug/LUnits:
Water
45.1544.8 0.8 20Zinc
8618085400 0.9 20Sodium
4172041300 1 20Calcium
254.5262 3 20Iron
2803027600 2 20Magnesium
624.7621 0.7 20Aluminum
13761360 1 20Manganese
ug/LUnits:
Water
Cadmium 0.82 U 4.1 UNC 10
Antimony 7.4 U 36.8 UNC 10
Beryllium 0.78 U 3.9 UNC 10
Thallium 5.2 U 26.2 UNC 10
Nickel 26.0 J 28.12 JNC 10
Silver 1.3 U 6.7 UNC 10
Arsenic 3.7 U 18.6 UNC 10
ug/LUnits:
Water
Copper 7.8 U 39.2 UNC 10
Lead 4.0 U 20.1 UNC 10
Zinc 44.8 46.75 JNC 10
Selenium 5.8 U 28.8 UNC 10
Chromium 4.5 U 22.3 UNC 10
Sodium 85400 84800 0.69 10
Potassium 4800 J 4798 JNC 10
Barium 107 J 106.4 JNC 10
Calcium 41300 41030 0.56 10
Iron 262 368 UNC 10
Vanadium 4.0 U 20.2 UNC 10
Magnesium 27600 27590 0.09 10
Aluminum 621 621.0 JNC 10
Manganese 1360 1377 1.5 10
Cobalt 22.4 J 22.70 JNC 10
WaterClient Matrix:
Water
1.0
Client Matrix:
Water
1.0
45.4 500 544.7 100 75 - 125Zinc
6.6 J 2000 2007 100 75 - 125Selenium
4.5 U 200 203.2 102 75 - 125Chromium
89400 20000 113700 122 75 - 125 4Sodium
4970 J 20000 25470 103 75 - 125Potassium
108 J 2000 2242 107 75 - 125Barium
43000 20000 66460 117 75 - 125Calcium
73.6 U 1000 1039 104 75 - 125Iron
4.0 U 500 507.1 101 75 - 125Vanadium
28100 20000 49300 106 75 - 125Magnesium
72.1 U 2000 1995 100 75 - 125Aluminum
1400 500 1969 113 75 - 125Manganese
23.6 J 500 540.8 103 75 - 125Cobalt
Water
1.0
Lab Sample ID:
Water
1.0
Lab Sample ID:
45.4 500 510.8 93 75 - 125Zinc
6.6 J 2000 1875 93 75 - 125Selenium
4.5 U 200 190.1 95 75 - 125Chromium
89400 20000 106700 87 75 - 125Sodium
4970 J 20000 23780 94 75 - 125Potassium
108 J 2000 2095 99 75 - 125Barium
43000 20000 62160 96 75 - 125Calcium
73.6 U 1000 968.7 97 75 - 125Iron
4.0 U 500 473.6 95 75 - 125Vanadium
28100 20000 46270 91 75 - 125Magnesium
72.1 U 2000 1862 93 75 - 125Aluminum
1400 500 1852 90 75 - 125Manganese
23.6 J 500 503.7 96 75 - 125Cobalt
ug/LUnits:
Water
45.6345.4 0.4 20Zinc
9125089400 2 20Sodium
4375043000 2 20Calcium
2864028100 2 20Magnesium
14301400 2 20Manganese
ug/LUnits:
Water
Cadmium 0.82 U 4.1 UNC 10
Antimony 7.4 U 36.8 UNC 10
Beryllium 0.78 U 3.9 UNC 10
Thallium 5.2 U 26.2 UNC 10
Nickel 26.8 J 25.89 JNC 10
Silver 1.3 U 6.7 UNC 10
Arsenic 3.7 U 18.6 UNC 10
ug/LUnits:
Water
Copper 7.8 U 39.2 UNC 10
Lead 4.0 U 20.1 UNC 10
Zinc 45.4 47.06 JNC 10
Selenium 6.6 J 28.8 UNC 10
Chromium 4.5 U 22.3 UNC 10
Sodium 89400 89400 0.01 10
Potassium 4970 J 5020 JNC 10
Barium 108 J 107.5 JNC 10
Calcium 43000 42700 0.67 10
Iron 73.6 U 368 UNC 10
Vanadium 4.0 U 20.2 UNC 10
Magnesium 28100 28320 0.78 10
Aluminum 72.1 U 361 UNC 10
Manganese 1400 1435 2.3 10
Cobalt 23.6 J 23.51 JNC 10
WaterClient Matrix:
Client Matrix:
Water
1.0
ug/LUnits:
Water
ug/LUnits:
Water
Mercury 0.16 U 0.80 UNC 10
WaterClient Matrix:
Client Matrix:
Water
1.0
ug/LUnits:
Water
ug/LUnits:
Water
Mercury 0.16 U 0.80 UNC 10
WaterClient Matrix:
Client Matrix:
Water
1.0
ug/LUnits:
Water
Mercury 0.53 0.80 UNC 10
DATA REPORTING QUALIFIERS
Lab Section Qualifier Description
MS/MSD Recovery or RPD exceeds the control limitsF
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value.
J
Metals
Indicates the analyte was analyzed for but not detected.U
MS, MSD: The analyte present in the original sample is 4 times greater
than the matrix spike concentration; therefore, control limits are not
applicable.
4
Result is less than the RL but greater than or equal to the MDL and the
concentration is an approximate value.
J
QC Association Summary
Lab Sample ID Client Sample ID Client Matrix Method Prep Batch
Report
Basis
Method Blank Water 8260BMB 460-133510/4 T
WaterWG-17338-101812-MW29-MM-250 8260B460-46192-1 T
WaterWG-17338-101812-MW28-MM-260 8260B460-46192-2 T
WaterWG-17338-101812-MW35-MM-261 8260B460-46192-3 T
WaterWG-17338-101812-MW27-MM-262 8260B460-46192-4 T
Matrix Spike Duplicate Water 8260B460-46192-4MSD T
WaterTB-17338-101812-263 8260B460-46192-5 T
Report
Basis
Metals
Method Blank Water 7470AMB 460-133263/11-A T
WaterWG-17338-101812-MW29-MM-250 7470A460-46192-1 T
WaterWG-17338-101812-MW28-MM-260 7470A460-46192-2 T
WaterWG-17338-101812-MW35-MM-261 7470A460-46192-3 T
Matrix Spike Water 7470A460-46246-I-1-F MS T
Analysis Batch:460-133302
Method Blank Water 460-1332637470AMB 460-133263/11-A T
Water 460-133263WG-17338-101812-MW29-MM-250 7470A460-46192-1 T
Water 460-133263WG-17338-101812-MW28-MM-260 7470A460-46192-2 T
Water 460-133263WG-17338-101812-MW35-MM-261 7470A460-46192-3 T
Matrix Spike Water 460-1332637470A460-46246-I-1-F MS T
Prep Batch: 460-133330
WaterWG-17338-101812-MW29-MM-250 3010A460-46192-1 T
WaterWG-17338-101812-MW28-MM-260 3010A460-46192-2 T
WaterWG-17338-101812-MW35-MM-261 3010A460-46192-3 T
WaterWG-17338-101812-MW27-MM-262 3010A460-46192-4 T
Method Blank Water 3010AMB 460-133340/1-B D
WaterWG-17338-101812-MW29-MM-250 3010A460-46192-1 D
WaterWG-17338-101812-MW28-MM-260 3010A460-46192-2 D
WaterWG-17338-101812-MW35-MM-261 3010A460-46192-3 D
WaterWG-17338-101812-MW27-MM-262 3010A460-46192-4 D
WaterWG-17338-101812-MW27-MM-262 7470A460-46192-4 T
TestAmerica Edison
Report
Basis
Metals
Method Blank Water 460-1334457470AMB 460-133445/11-A T
Water 460-133445WG-17338-101812-MW27-MM-262 7470A460-46192-4 T
Duplicate Water 460-1334457470A460-46192-4DU T
Method Blank Water 460-1333306010BMB 460-133330/1-A T
Lab Control Sample Water 460-1333656010BLCS 460-133365/2-A T
Method Blank Water 460-1333656010BMB 460-133340/1-B D
Water 460-133330WG-17338-101812-MW29-MM-250 6010B460-46192-1 T
Water 460-133365WG-17338-101812-MW29-MM-250 6010B460-46192-1 D
Water 460-133330WG-17338-101812-MW28-MM-260 6010B460-46192-2 T
Water 460-133365WG-17338-101812-MW28-MM-260 6010B460-46192-2 D
Water 460-133330WG-17338-101812-MW35-MM-261 6010B460-46192-3 T
Water 460-133365WG-17338-101812-MW35-MM-261 6010B460-46192-3 D
Water 460-133330WG-17338-101812-MW27-MM-262 6010B460-46192-4 T
Duplicate Water 460-1333306010B460-46192-4DU T
Water 460-133365WG-17338-101812-MW27-MM-262 6010B460-46192-4 D
Duplicate Water 460-1333656010B460-46192-4DU D
Method Blank Water 7470AMB 460-133760/1-B D
WaterWG-17338-101812-MW29-MM-250 7470A460-46192-1 D
WaterWG-17338-101812-MW28-MM-260 7470A460-46192-2 D
WaterWG-17338-101812-MW35-MM-261 7470A460-46192-3 D
WaterWG-17338-101812-MW27-MM-262 7470A460-46192-4 D
TestAmerica Edison
Report
Basis
Metals
Method Blank Water 460-1337667470AMB 460-133760/1-B D
Water 460-133766WG-17338-101812-MW29-MM-250 7470A460-46192-1 D
Water 460-133766WG-17338-101812-MW28-MM-260 7470A460-46192-2 D
Water 460-133766WG-17338-101812-MW35-MM-261 7470A460-46192-3 D
Water 460-133766WG-17338-101812-MW27-MM-262 7470A460-46192-4 D
Duplicate Water 460-1337667470A460-46192-4DU D
Report Basis
D = Dissolved
T = Total
TestAmerica Edison
Laboratory Chronicle
10/19/2012 18:45
Lab ID:
460-46192-1 WG-17338-101812-MW29-MM-250
P:3010A 460-46192-D-1-B 460-133489 460-133330 10/24/2012 07:59 MCTAL EDI1
A:6010B 460-46192-D-1-B 460-133489 460-133330 10/24/2012 17:51 CDCTAL EDI1
P:3010A 460-46192-E-1-B 460-133489 460-133365 10/24/2012 09:57 MCTAL EDI1
A:6010B 460-46192-E-1-B 460-133489 460-133365 10/24/2012 20:02 CDCTAL EDI1
P:3010A 460-46192-E-1-B ^5 460-133561 460-133365 10/24/2012 09:57 MCTAL EDI5
A:6010B 460-46192-E-1-B ^5 460-133561 460-133365 10/25/2012 11:49 CDCTAL EDI5
P:7470A 460-46192-D-1-A 460-133302 460-133263 10/23/2012 16:50 TSTAL EDI1
A:7470A 460-46192-D-1-A 460-133302 460-133263 10/23/2012 20:35 TSTAL EDI1
P:7470A 460-46192-E-1-D 460-133790 460-133766 10/26/2012 17:17 TSTAL EDI1
A:7470A 460-46192-E-1-D 460-133790 460-133766 10/26/2012 20:20 TSTAL EDI1
10/19/2012 18:45
Lab ID:
460-46192-2 WG-17338-101812-MW28-MM-260
P:3010A 460-46192-D-2-B 460-133489 460-133330 10/24/2012 07:59 MCTAL EDI1
A:6010B 460-46192-D-2-B 460-133489 460-133330 10/24/2012 18:10 CDCTAL EDI1
P:3010A 460-46192-E-2-B 460-133489 460-133365 10/24/2012 09:57 MCTAL EDI1
A:6010B 460-46192-E-2-B 460-133489 460-133365 10/24/2012 20:06 CDCTAL EDI1
P:7470A 460-46192-D-2-A 460-133302 460-133263 10/23/2012 16:50 TSTAL EDI1
A:7470A 460-46192-D-2-A 460-133302 460-133263 10/23/2012 20:42 TSTAL EDI1
P:7470A 460-46192-E-2-D 460-133790 460-133766 10/26/2012 17:17 TSTAL EDI1
A:7470A 460-46192-E-2-D 460-133790 460-133766 10/26/2012 20:21 TSTAL EDI1
10/19/2012 18:45
Lab ID:
460-46192-3 WG-17338-101812-MW35-MM-261
P:3010A 460-46192-D-3-B 460-133489 460-133330 10/24/2012 07:59 MCTAL EDI1
A:6010B 460-46192-D-3-B 460-133489 460-133330 10/24/2012 18:14 CDCTAL EDI1
P:3010A 460-46192-E-3-B 460-133489 460-133365 10/24/2012 09:57 MCTAL EDI1
A:6010B 460-46192-E-3-B 460-133489 460-133365 10/24/2012 20:10 CDCTAL EDI1
P:7470A 460-46192-D-3-A 460-133302 460-133263 10/23/2012 16:50 TSTAL EDI1
A:7470A 460-46192-D-3-A 460-133302 460-133263 10/23/2012 20:44 TSTAL EDI1
P:7470A 460-46192-E-3-D 460-133790 460-133766 10/26/2012 17:17 TSTAL EDI1
A:7470A 460-46192-E-3-D 460-133790 460-133766 10/26/2012 20:23 TSTAL EDI1
A = Analytical Method P = Prep Method TestAmerica Edison
10/31/2012Page 68 of 813
10/19/2012 18:45
Lab ID:
460-46192-4 WG-17338-101812-MW27-MM-262
P:3010A 460-46192-D-4-A 460-133489 460-133330 10/24/2012 07:59 MCTAL EDI1
A:6010B 460-46192-D-4-A 460-133489 460-133330 10/24/2012 17:37 CDCTAL EDI1
P:3010A 460-46192-E-4-D 460-133489 460-133365 10/24/2012 09:57 MCTAL EDI1
A:6010B 460-46192-E-4-D 460-133489 460-133365 10/24/2012 19:47 CDCTAL EDI1
P:7470A 460-46192-D-4-D 460-133468 460-133445 10/24/2012 17:00 TSTAL EDI1
A:7470A 460-46192-D-4-D 460-133468 460-133445 10/24/2012 20:32 TSTAL EDI1
P:7470A 460-46192-E-4-J 460-133790 460-133766 10/26/2012 17:17 TSTAL EDI1
A:7470A 460-46192-E-4-J 460-133790 460-133766 10/26/2012 20:12 TSTAL EDI1
10/19/2012 18:45
Lab ID:
460-46192-4 WG-17338-101812-MW27-MM-262
P:3010A 460-46192-D-4-C MS 460-133489 460-133330 10/24/2012 07:59 MCTAL EDI1
A:6010B 460-46192-D-4-C MS 460-133489 460-133330 10/24/2012 17:44 CDCTAL EDI1
P:3010A 460-46192-E-4-F MS 460-133489 460-133365 10/24/2012 09:57 MCTAL EDI1
A:6010B 460-46192-E-4-F MS 460-133489 460-133365 10/24/2012 19:55 CDCTAL EDI1
P:7470A 460-46192-D-4-F MS 460-133468 460-133445 10/24/2012 17:00 TSTAL EDI1
A:7470A 460-46192-D-4-F MS 460-133468 460-133445 10/24/2012 20:36 TSTAL EDI1
P:7470A 460-46192-E-4-L MS 460-133790 460-133766 10/26/2012 17:17 TSTAL EDI1
A:7470A 460-46192-E-4-L MS 460-133790 460-133766 10/26/2012 20:18 TSTAL EDI1
10/19/2012 18:45
Lab ID:
460-46192-4 WG-17338-101812-MW27-MM-262
10/31/2012Page 69 of 813
10/19/2012 18:45
Lab ID:
460-46192-4 WG-17338-101812-MW27-MM-262
10/19/2012 18:45
Lab ID:
460-46192-4 SD WG-17338-101812-MW27-MM-262
P:3010A 460-46192-D-4-A SD
A:6010B 460-46192-D-4-A SD
P:3010A 460-46192-D-4-A
A:6010B 460-46192-D-4-A
P:3010A 460-46192-E-4-D SD
A:6010B 460-46192-E-4-D SD
P:3010A 460-46192-E-4-D
A:6010B 460-46192-E-4-D
P:7470A 460-46192-D-4-D SD
A:7470A 460-46192-D-4-D SD
P:7470A 460-46192-E-4-J SD
A:7470A 460-46192-E-4-J SD
10/19/2012 18:45
Lab ID:
460-46192-5 TB-17338-101812-263
10/31/2012Page 70 of 813
Lab ID:
MB N/A
P:3010A MB 460-133330/1-A 460-133489 460-133330 10/24/2012 07:59 MCTAL EDI1
A:6010B MB 460-133330/1-A 460-133489 460-133330 10/24/2012 18:06 CDCTAL EDI1
P:3010A MB 460-133340/1-B 460-133489 460-133365 10/24/2012 09:57 MCTAL EDI1
A:6010B MB 460-133340/1-B 460-133489 460-133365 10/24/2012 19:36 CDCTAL EDI1
P:7470A MB 460-133263/11-A 460-133302 460-133263 10/23/2012 16:50 TSTAL EDI1
A:7470A MB 460-133263/11-A 460-133302 460-133263 10/23/2012 19:54 TSTAL EDI1
P:7470A MB 460-133445/11-A 460-133468 460-133445 10/24/2012 17:00 TSTAL EDI1
A:7470A MB 460-133445/11-A 460-133468 460-133445 10/24/2012 20:28 TSTAL EDI1
P:7470A MB 460-133760/1-B 460-133790 460-133766 10/26/2012 17:17 TSTAL EDI1
A:7470A MB 460-133760/1-B 460-133790 460-133766 10/26/2012 20:08 TSTAL EDI1
Lab ID:
LCS N/A
P:3010A LCS 460-133330/2-A 460-133489 460-133330 10/24/2012 07:59 MCTAL EDI1
A:6010B LCS 460-133330/2-A 460-133489 460-133330 10/24/2012 17:55 CDCTAL EDI1
P:3010A LCS 460-133365/2-A 460-133489 460-133365 10/24/2012 09:57 MCTAL EDI1
A:6010B LCS 460-133365/2-A 460-133489 460-133365 10/24/2012 19:40 CDCTAL EDI1
P:7470A LCS 460-133263/12-A 460-133302 460-133263 10/23/2012 16:50 TSTAL EDI1
A:7470A LCS 460-133263/12-A 460-133302 460-133263 10/23/2012 19:56 TSTAL EDI1
P:7470A LCS 460-133445/12-A 460-133468 460-133445 10/24/2012 17:00 TSTAL EDI1
A:7470A LCS 460-133445/12-A 460-133468 460-133445 10/24/2012 20:30 TSTAL EDI1
P:7470A LCS 460-133766/12-A 460-133790 460-133766 10/26/2012 17:17 TSTAL EDI1
A:7470A LCS 460-133766/12-A 460-133790 460-133766 10/26/2012 20:10 TSTAL EDI1
Lab ID:
MS N/A
10/31/2012Page 71 of 813
Lab ID:
DU N/A
Lab ID:
SD N/A
A:7470A 460-46246-I-1-D SD
10/31/2012Page 72 of 813
8260 (Delaware)
SDG No.:
#Lab Sample IDClient Sample ID # #DCA TOL BFB
460-46192-1WG-17338-101812-MW 29-MM-250
460-46192-4 MSWG-17338-101812-MW 27-MM-262 MS
TOL = Toluene-d8 (Surr) 70-130
10/31/2012Page 74 of 813
FORM III
TestAmerica Edison
Bromomethane 20.0 18.9 55-15394
1,2-Dibromo-3-Chloropropane 20.0 19.0 70-11695
1,2-Dichlorobenzene 20.0 19.2 82-12296
Trichlorofluoromethane 20.0 17.2 69-14786
1,1-Dichloroethene 20.0 19.7 56-13999
1,2-Dichloropropane 20.0 19.2 80-12096
trans-1,2-Dichloroethene 20.0 18.6 75-12293
Chlorodibromomethane 20.0 19.2 80-12096
Chloroethane 20.0 18.6 69-14593
1,1-Dichloroethane 20.0 18.8 78-12294
cis-1,2-Dichloroethene 20.0 19.3 80-12097
Chloroform 20.0 19.3 82-12396
Ethylbenzene 20.0 19.2 79-12696
Cyclohexane 20.0 19.1 58-13395
Benzene 20.0 19.7 83-12498
1,2-Dichloroethane 20.0 19.2 74-11896
Trichloroethene 20.0 20.5 78-119102
Methylcyclohexane 20.0 19.1 61-12996
Dichlorobromomethane 20.0 19.5 79-11998
cis-1,3-Dichloropropene 20.0 18.9 80-12095
Toluene 20.0 19.5 80-12097
trans-1,3-Dichloropropene 20.0 18.8 78-11894
1,1,2-Trichloroethane 20.0 19.3 79-11996
Tetrachloroethene 20.0 19.0 68-13995
2-Hexanone 20.0 18.4 53-12192
1,2-Dibromoethane 20.0 18.9 78-11895
Chlorobenzene 20.0 19.4 81-12197
FORM III 8260B
# Column to be used to flag recovery and RPD values
10/31/2012Page 75 of 813
FORM III
TestAmerica Edison
10/31/2012Page 76 of 813
FORM III
TestAmerica Edison
20.0 12.7 46-145Dichlorodifluoromethane 630.22 U
20.0 13.4 58-146Chloromethane 670.10 U
20.0 14.0 61-144Vinyl chloride 700.14 U
20.0 15.3 55-153Bromomethane 770.18 U
20.0 14.2 70-1161,2-Dibromo-3-Chloropropane 710.40 U
20.0 14.9 82-1221,2-Dichlorobenzene 740.21 U F
20.0 19.5 69-147Trichlorofluoromethane 970.15 U
20.0 13.7 56-1391,1-Dichloroethene 690.090 U
20.0 15.3 80-1201,2-Dichloropropane 770.090 U F
20.0 13.9 47-1391,1,2-Trichloro-1,2,2-trifluor oethane
20.0 14.1 58-139Carbon disulfide 700.13 U
20.0 10.9 50-151Methyl acetate 540.34 U
20.0 14.7 79-119Methylene Chloride 740.18 U F
20.0 13.5 75-122trans-1,2-Dichloroethene 670.13 U F
20.0 14.9 80-120Chlorodibromomethane 740.20 U F
20.0 13.7 71-115Methyl tert-butyl ether 680.14 U F
20.0 18.0 69-145Chloroethane 900.17 U
20.0 13.8 78-1221,1-Dichloroethane 690.13 U F
20.0 14.9 80-120cis-1,2-Dichloroethene 740.18 U F
20.0 13.6 65-1142-Butanone (MEK) 682.3 U
20.0 14.7 82-123Chloroform 730.080 U F
20.0 15.1 79-126Ethylbenzene 740.21 J F
20.0 15.8 58-133Cyclohexane 790.16 U
20.0 14.9 73-120Carbon tetrachloride 750.060 U
20.0 15.2 83-124Benzene 760.080 U F
20.0 14.3 74-1181,2-Dichloroethane 710.19 U F
20.0 15.0 78-119Trichloroethene 750.090 U F
20.0 19.2 61-129Methylcyclohexane 960.14 U
20.0 16.0 79-119Dichlorobromomethane 800.12 U
20.0 14.6 80-120cis-1,3-Dichloropropene 730.18 U F
20.0 13.9 53-1204-Methyl-2-pentanone (MIBK) 690.99 U
20.0 14.9 80-120Toluene 740.15 U F
20.0 14.6 78-118trans-1,3-Dichloropropene 730.24 U F
20.0 15.3 79-1191,1,2-Trichloroethane 760.19 U F
20.0 14.9 68-139Tetrachloroethene 750.10 U
20.0 13.4 53-1212-Hexanone 670.50 U
20.0 14.4 78-1181,2-Dibromoethane 720.28 U F
20.0 15.1 81-121Chlorobenzene 750.11 U F
60.0 45.4 76-121Xylenes, Total 740.95 J F
FORM III 8260B
10/31/2012Page 77 of 813
FORM III
TestAmerica Edison
20.0 14.2 73-123Bromoform 710.19 U F
20.0 14.7 80-125Isopropylbenzene 740.080 U F
20.0 14.0 74-1261,1,2,2-Tetrachloroethane 700.16 U F
20.0 13.6 66-1201,2,4-Trichlorobenzene 680.34 U
FORM III 8260B
10/31/2012Page 78 of 813
FORM III
TestAmerica Edison
20.0 23.1 30 61-144Vinyl chloride 49115 F
20.0 23.6 30 55-153Bromomethane 42118 F
20.0 22.9 30 70-1161,2-Dibromo-3-Chloropropane 47115 F
20.0 23.6 30 82-1221,2-Dichlorobenzene 45118 F
20.0 32.4 30 69-147Trichlorofluoromethane 50162 F
20.0 21.5 30 56-1391,1-Dichloroethene 44107 F
20.0 24.2 30 80-1201,2-Dichloropropane 45121 F
20.0 22.9 30 47-1391,1,2-Trichloro-1,2,2-trifluor oethane
49115 F
20.0 22.8 30 58-139Carbon disulfide 47114 F
20.0 16.7 30 50-151Methyl acetate 4284 F
20.0 23.7 30 79-119Methylene Chloride 47118 F
20.0 21.7 30 75-122trans-1,2-Dichloroethene 47109 F
20.0 23.8 30 80-120Chlorodibromomethane 46119 F
20.0 21.5 30 71-115Methyl tert-butyl ether 45108 F
20.0 27.5 30 69-145Chloroethane 42138 F
20.0 22.6 30 78-1221,1-Dichloroethane 48113 F
20.0 23.4 30 80-120cis-1,2-Dichloroethene 45117 F
20.0 21.4 30 65-1142-Butanone (MEK) 45107 F
20.0 24.4 30 82-123Chloroform 50122 F
20.0 24.3 30 79-126Ethylbenzene 47120 F
20.0 24.5 30 58-133Cyclohexane 43122 F
20.0 24.2 30 73-120Carbon tetrachloride 47121 F
20.0 23.4 30 83-124Benzene 42117 F
20.0 22.5 30 74-1181,2-Dichloroethane 44112 F
20.0 23.9 30 78-119Trichloroethene 45119 F
20.0 26.9 30 61-129Methylcyclohexane 33135 F
20.0 25.3 30 79-119Dichlorobromomethane 45127 F
20.0 23.0 30 80-120cis-1,3-Dichloropropene 45115 F
20.0 21.6 30 53-1204-Methyl-2-pentanone (MIBK) 44108 F
20.0 23.8 30 80-120Toluene 46119 F
20.0 23.3 30 78-118trans-1,3-Dichloropropene 46117 F
20.0 23.3 30 79-1191,1,2-Trichloroethane 42117 F
20.0 23.8 30 68-139Tetrachloroethene 46119 F
20.0 23.0 30 53-1212-Hexanone 53115 F
20.0 23.0 30 78-1181,2-Dibromoethane 46115 F
20.0 24.3 30 81-121Chlorobenzene 47121 F
60.0 72.6 30 76-121Xylenes, Total 46119 F
FORM III 8260B
10/31/2012Page 79 of 813
FORM III
TestAmerica Edison
FORM III 8260B
10/31/2012Page 80 of 813
Lab Name:
SDG No.:
WaterMatrix:
0.18(mm)
LAB SAMPLE ID
10/25/2012 07:40e09399.dLCS 460-133510/3
Analysis Batch No.: 133133
173 Less than 2.0 % of mass 174 1.5 (1.6)1
174 50.0 - 120.00 % of mass 95 94.7
175 5.0 - 9.0 % of mass 174 7.2 (7.6)1
176 95.0 - 101.0 % of mass 174 91.7 (96.8)1
177 5.0 - 9.0 % of mass 176 5.9 (6.4)2
1-Value is % mass 174 2-Value is % mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:
GC/MS VOA INSTRUMENT PERFORMANCE CHECK
TestAmerica Edison
ANALYZED TIME
FORM V
BROMOFLUOROBENZENE (BFB)
Lab Name:
SDG No.:
Analysis Batch No.: 133510
173 Less than 2.0 % of mass 174 0.7 (0.7)1
174 50.0 - 120.00 % of mass 95 94.2
175 5.0 - 9.0 % of mass 174 7.3 (7.8)1
176 95.0 - 101.0 % of mass 174 89.5 (95.0)1
177 5.0 - 9.0 % of mass 176 5.1 (5.7)2
1-Value is % mass 174 2-Value is % mass 176
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:
GC/MS VOA INSTRUMENT PERFORMANCE CHECK
TestAmerica Edison
ANALYZED TIME
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY
Lab Name: Job No.:
Lab File ID (Standard): e09398.d
Instrument ID: VOAMS5 GC Column: Rtx-VMS ID: 0.18(mm)
Heated Purge: (Y/N) N
FB CBZ DCB
4.09
3.09
7.45
6.45
10.97
9.97
LCS 460-133510/3 987382 923531 586471 3.60 6.95 10.47
MB 460-133510/4 909949 852084 547163 3.60 6.95 10.47
460-46192-5 TB-17338-101812-263 888044 828973 545730 3.60 6.95 10.47
460-46192-4 WG-17338-101812-MW27- MM-262
460-46192-2 WG-17338-101812-MW28- MM-260
460-46192-3 WG-17338-101812-MW35- MM-261
460-46192-1 WG-17338-101812-MW29- MM-250
460-46192-4 MS WG-17338-101812-MW27- MM-262 MS
961371 902268 594984 3.60 6.95 10.47
460-46192-4 MSD WG-17338-101812-MW27- MM-262 MSD
960482 915949 594794 3.60 6.95 10.47
CCV 460-133510/21 914316 867035 591131 3.60 6.95 10.47
FB = Fluorobenzene
CBZ = Chlorobenzene-d5
DCB = 1,4-Dichlorobenzene-d4
FORM VIII 8260B
Client Sample ID:
Level: (low/med) Low
CAS NO. COMPOUND NAME RESULT Q MDLRL
1.0 0.060U71-55-6 1,1,1-Trichloroethane 0.060
1.0 0.22U75-71-8 Dichlorodifluoromethane 0.22
1.0 0.10U74-87-3 Chloromethane 0.10
1.0 0.18U74-83-9 Bromomethane 0.18
1.0 0.40U96-12-8 1,2-Dibromo-3-Chloropropane 0.40
1.0 0.21U95-50-1 1,2-Dichlorobenzene 0.21
1.0 0.15U75-69-4 Trichlorofluoromethane 0.15
1.0 0.090U75-35-4 1,1-Dichloroethene 0.090
1.0 0.090U78-87-5 1,2-Dichloropropane 0.090
1.0 0.080U76-13-1 1,1,2-Trichloro-1,2,2-trifluoroethan e
1.0 0.13U156-60-5 trans-1,2-Dichloroethene 0.13
1.0 0.20U124-48-1 Chlorodibromomethane 0.20
1.0 0.17U75-00-3 Chloroethane 0.17
1.0 0.13U75-34-3 1,1-Dichloroethane 0.13
1.0 0.18156-59-2 cis-1,2-Dichloroethene 2.6
1.0 0.080U67-66-3 Chloroform 0.080
1.0 0.10100-41-4 Ethylbenzene 5.9
1.0 0.16110-82-7 Cyclohexane 3.6
1.0 0.08071-43-2 Benzene 11
1.0 0.090U79-01-6 Trichloroethene 0.090
1.0 0.14108-87-2 Methylcyclohexane 3.5
1.0 0.12U75-27-4 Dichlorobromomethane 0.12
1.0 0.18U10061-01-5 cis-1,3-Dichloropropene 0.18
1.0 0.15108-88-3 Toluene 1.5
1.0 0.24U10061-02-6 trans-1,3-Dichloropropene 0.24
Client Sample ID:
1.0 0.10U127-18-4 Tetrachloroethene 0.10
5.0 0.50U591-78-6 2-Hexanone 0.50
1.0 0.28U106-93-4 1,2-Dibromoethane 0.28
1.0 0.11U108-90-7 Chlorobenzene 0.11
1.0 0.12U100-42-5 Styrene 0.12
1.0 0.19U75-25-2 Bromoform 0.19
1.0 0.080J98-82-8 Isopropylbenzene 0.79
1.0 0.16U79-34-5 1,1,2,2-Tetrachloroethane 0.16
1.0 0.34U120-82-1 1,2,4-Trichlorobenzene 0.34
TENTATIVELY IDENTIFIED COMPOUNDS
Client Sample ID:
Number TICs Found: TIC Result Total: 00
QRTCOMPOUND NAME RESULTCAS NO.
TestAmerica
Concentration Formula: Amt * DF * 5/Vo * CpndVariable
Name Value Description -------------- -------------- -----------------------
Cpnd Variable Local Compound Variable
CONCENTRATIONS
========================== ==== == ====== ====== ======== ======= =======
4 Vinyl Chloride 62 1.029 1.028 (0.286) 199821 31.2406 31
28 MTBE 73 2.016 2.022 (0.560) 7459 0.52141 0.52(a)
36 cis-1,2-Dichloroethene 96 2.656 2.650 (0.738) 12691 2.59086 2.6
44 Cyclohexane 56 2.790 2.784 (0.775) 30031 3.61284 3.6
48 Benzene 78 3.260 3.260 (0.469) 209177 10.9183 11
$ 47 1,2-Dichloroethane-d4 (SUR) 65 3.363 3.363 (0.934) 268325 50.7169 51
* 52 Fluorobenzene 96 3.601 3.595 (1.000) 894460 50.0000
56 Methyl cyclohexane 83 3.729 3.729 (1.036) 25700 3.54014 3.5
$ 65 Toluene-d8 (SUR) 98 5.107 5.107 (0.734) 893412 50.0781 50
66 Toluene 91 5.162 5.162 (0.742) 32397 1.50535 1.5
* 78 Chlorobenzene-d5 117 6.954 6.954 (1.000) 826320 50.0000
81 Ethylbenzene 106 7.064 7.064 (1.016) 44537 5.89334 5.9
82 m+p-Xylene 106 7.277 7.277 (1.046) 49413 5.07440 5.1
84 o-Xylene 106 7.856 7.863 (1.130) 27212 2.79539 2.8
88 Isopropylbenzene 105 8.344 8.344 (1.200) 18075 0.79402 0.79(a)
$ 89 Bromofluorobenzene (SUR) 174 8.710 8.710 (0.832) 442726 51.2450 51
10/31/2012Page 88 of 813
CONCENTRATIONS
========================== ==== == ====== ====== ======== ======= =======
QC Flag Legend
a - Target compound detected but, quantitated amount Below Limit Of Quantitation(BLOQ).
10/31/2012Page 89 of 813
Sample Info: 460-46192-A-1 Operator: GC/MS VOAMS5
10/31/2012Page 90 of 813
4 Vinyl Chloride
28 MTBE
36 cis-1,2-Dichloroethene
81 Ethylbenzene
44 Cyclohexane
48 Benzene
56 Methyl cyclohexane
66 Toluene
82 m+p-Xylene
84 o-Xylene
88 Isopropylbenzene
Client Sample ID:
1.0 0.18U74-83-9 Bromomethane 0.18
1.0 0.17U75-00-3 Chloroethane 0.17
1.0 0.18U156-59-2 cis-1,2-Dichloroethene 0.18
1.0 0.080U67-66-3 Chloroform 0.080
1.0 0.10J100-41-4 Ethylbenzene 0.37
1.0 0.16U110-82-7 Cyclohexane 0.16
1.0 0.080J71-43-2 Benzene 0.12
1.0 0.14U108-87-2 Methylcyclohexane 0.14
1.0 0.15U108-88-3 Toluene 0.15
Client Sample ID:
5.0 0.50U591-78-6 2-Hexanone 0.50
1.0 0.28U106-93-4 1,2-Dibromoethane 0.28
1.0 0.11U108-90-7 Chlorobenzene 0.11
1.0 0.12U100-42-5 Styrene 0.12
1.0 0.19U75-25-2 Bromoform 0.19
1.0 0.080J98-82-8 Isopropylbenzene 0.097
Client Sample ID:
TestAmerica
CONCENTRATIONS
========================== ==== == ====== ====== ======== ======= =======
* 52 Fluorobenzene 96 3.595 3.595 (1.000) 871328 50.0000
$ 65 Toluene-d8 (SUR) 98 5.107 5.107 (0.734) 888323 49.3523 49
* 78 Chlorobenzene-d5 117 6.954 6.954 (1.000) 833697 50.0000
81 Ethylbenzene 106 7.058 7.064 (1.015) 2796 0.36671 0.37(a)
82 m+p-Xylene 106 7.277 7.277 (1.046) 14986 1.52535 1.5
88 Isopropylbenzene 105 8.344 8.344 (1.200) 2234 0.09727 0.097(aH)
* 108 1,4-Dichlorobenzene-d4 152 10.465 10.466 (1.000) 532289 50.0000
M 121 Xylene (Total) 100 14986 1.52535 1.5(a)
QC Flag Legend
10/31/2012Page 105 of 813
QC Flag Legend
10/31/2012Page 106 of 813
10/31/2012Page 107 of 813
81 Ethylbenzene
48 Benzene
82 m+p-Xylene
88 Isopropylbenzene
Client Sample ID:
1.0 0.18U74-83-9 Bromomethane 0.18
1.0 0.17U75-00-3 Chloroethane 0.17
1.0 0.080U67-66-3 Chloroform 0.080
1.0 0.10J100-41-4 Ethylbenzene 0.28
1.0 0.16U110-82-7 Cyclohexane 0.16
1.0 0.080J71-43-2 Benzene 0.45
1.0 0.090J79-01-6 Trichloroethene 0.87
1.0 0.15U108-88-3 Toluene 0.15
Client Sample ID:
5.0 0.50U591-78-6 2-Hexanone 0.50
1.0 0.28U106-93-4 1,2-Dibromoethane 0.28
1.0 0.11U108-90-7 Chlorobenzene 0.11
1.0 0.12U100-42-5 Styrene 0.12
1.0 0.19U75-25-2 Bromoform 0.19
1.0 0.080U98-82-8 Isopropylbenzene 0.080
Client Sample ID:
TestAmerica
CONCENTRATIONS
========================== ==== == ====== ====== ======== ======= =======
* 52 Fluorobenzene 96 3.601 3.595 (1.000) 921729 50.0000
54 Trichloroethene 95 3.747 3.741 (1.041) 4762 0.86977 0.87(a)
$ 65 Toluene-d8 (SUR) 98 5.107 5.107 (0.734) 916272 50.6989 51
* 78 Chlorobenzene-d5 117 6.954 6.954 (1.000) 837087 50.0000
81 Ethylbenzene 106 7.064 7.064 (1.016) 2178 0.28450 0.28(a)
82 m+p-Xylene 106 7.277 7.277 (1.046) 12975 1.31531 1.3
M 121 Xylene (Total) 100 12975 1.31531 1.3(a)
QC Flag Legend
10/31/2012Page 115 of 813
10/31/2012Page 116 of 813
81 Ethylbenzene
48 Benzene
54 Trichloroethene
82 m+p-Xylene
Client Sample ID:
1.0 0.18U74-83-9 Bromomethane 0.18
1.0 0.17U75-00-3 Chloroethane 0.17
1.0 0.080U67-66-3 Chloroform 0.080
1.0 0.10J100-41-4 Ethylbenzene 0.21
1.0 0.16U110-82-7 Cyclohexane 0.16
1.0 0.080U71-43-2 Benzene 0.080
1.0 0.15U108-88-3 Toluene 0.15
Client Sample ID:
5.0 0.50U591-78-6 2-Hexanone 0.50
1.0 0.28U106-93-4 1,2-Dibromoethane 0.28
1.0 0.11U108-90-7 Chlorobenzene 0.11
1.0 0.12U100-42-5 Styrene 0.12
1.0 0.19U75-25-2 Bromoform 0.19
Client Sample ID:
TestAmerica
CONCENTRATIONS
========================== ==== == ====== ====== ======== ======= =======
* 52 Fluorobenzene 96 3.601 3.595 (1.000) 909494 50.0000
$ 65 Toluene-d8 (SUR) 98 5.107 5.107 (0.734) 900809 49.7913 50
* 78 Chlorobenzene-d5 117 6.954 6.954 (1.000) 837961 50.0000
81 Ethylbenzene 106 7.064 7.064 (1.016) 1617 0.21100 0.21(a)
82 m+p-Xylene 106 7.277 7.277 (1.046) 9360 0.94786 0.95(a)
M 121 Xylene (Total) 100 9360 0.94786 0.95(a)
QC Flag Legend
10/31/2012Page 124 of 813
10/31/2012Page 125 of 813
81 Ethylbenzene
82 m+p-Xylene
Client Sample ID:
1.0 0.18U74-83-9 Bromomethane 0.18
1.0 0.17U75-00-3 Chloroethane 0.17
1.0 0.080U67-66-3 Chloroform 0.080
1.0 0.10U100-41-4 Ethylbenzene 0.10
1.0 0.16U110-82-7 Cyclohexane 0.16
1.0 0.080U71-43-2 Benzene 0.080
1.0 0.15U108-88-3 Toluene 0.15
Client Sample ID:
5.0 0.50U591-78-6 2-Hexanone 0.50
1.0 0.28U106-93-4 1,2-Dibromoethane 0.28
1.0 0.11U108-90-7 Chlorobenzene 0.11
1.0 0.12U100-42-5 Styrene 0.12
1.0 0.19U75-25-2 Bromoform 0.19
Client Sample ID:
TestAmerica
CONCENTRATIONS
========================== ==== == ====== ====== ======== ======= =======
22 Methylene Chloride 49 1.864 1.864 (0.518) 6755 0.96729 0.97(a)
* 52 Fluorobenzene 96 3.601 3.595 (1.000) 888044 50.0000
$ 65 Toluene-d8 (SUR) 98 5.107 5.107 (0.734) 898197 50.1852 50
* 78 Chlorobenzene-d5 117 6.954 6.954 (1.000) 828973 50.0000
QC Flag Legend
10/31/2012Page 131 of 813
10/31/2012Page 132 of 813
22 Methylene Chloride
GC/MS VOA INITIAL CALIBRATION DATA
TestAmerica Edison 460-46192-1
N
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID: 1Level IC 460-133133/3 e09277.d 2Level IC 460-133133/4 e09278.d 3Level ICIS 460-133133/2 e09273.d 4Level IC 460-133133/5 e09279.d 5Level IC 460-133133/6 e09280.d 6Level IC 460-133133/7 e09281.d
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVE TYPE
MIN RRF
LVL 6
0.1000 30.00.2211
0.1000 30.00.4291
Vinyl chloride 0.3688 0.3581 0.3275 0.3099 0.3315 Ave 6.7 0.3220
0.1000 30.00.3363
0.99000.1829
0.1000 30.00.1987
0.1000 30.00.3242
0.1000 30.00.1893
Carbon disulfide 0.7986 0.7632 0.6881 0.6789 0.7655 Ave 7.1 0.7980
0.1000 30.00.7487
0.1000 30.00.2232
Methylene Chloride 0.4517 0.3798 0.3490 0.3396 0.3260 Ave 13.5 0.3226
0.1000 30.00.3615
0.1000* 30.00.0241
0.1000 30.00.2322
Methyl acetate 0.0530 0.0517 0.0462 0.0473 0.0491 Ave 5.6 0.0522
0.1000* 30.00.0499
Methyl tert-butyl ether 0.7983 0.7461 0.7241 0.7432 0.7725 Ave 5.1 0.8293
0.1000 30.00.7689
0.1000 30.00.4820
FORM VI 8260B
Note: The m1 coefficient is the same as Ave RRF for an Ave curve type.
10/31/2012Page 134 of 813
N
CURVE TYPE
MIN RRF
LVL 6
0.1000 30.00.2593
0.1000 30.00.4160
0.1000 30.00.4475
Carbon tetrachloride 0.3185 0.3206 0.2780 0.3006 0.3488 Ave 10.6 0.3748
0.1000 30.00.3236
0.1000 30.00.3901
2-Butanone (MEK) 0.0288 0.0297 0.0397 0.0410 0.0463 LinF 0.9993 0.0479
0.99000.0476
0.1000 30.01.2206
0.1000 30.00.3659
0.1000 30.00.3699
0.1000 30.00.2791
0.1000 30.00.2827
0.1000 30.00.3556
0.1000 30.00.5277
0.1000 30.01.4384
0.1000 30.00.3717
4-Methyl-2-pentanone (MIBK) 0.3405 0.3098 0.2925 0.3010 0.3227 Ave 7.7 0.3573
0.1000 30.00.3206
0.1000 30.00.4827
0.1000 30.00.2298
0.1000 30.00.3371
0.1000 30.00.2914
FORM VI 8260B
10/31/2012Page 135 of 813
N
CURVE TYPE
MIN RRF
LVL 6
0.1000 30.00.2453
0.1000 30.01.0088
0.1000 30.00.5455
m-Xylene & p-Xylene 0.7084 0.6864 0.6532 0.6414 0.7308 Ave 4.9 0.6888
0.1000 30.00.6848
0.1000 30.00.6635
0.1000 30.00.2514
0.1000 30.01.1284
0.1000 30.01.6411
0.1000 30.00.6066
0.1000 30.01.3588
0.1000 30.01.4198
0.1000 30.01.2940
0.1000 30.00.1029
0.1000 30.00.7588
1,2-Dichloroethane-d4 (Surr) 0.2689 0.2712 0.2619 0.2683 0.2676 Ave 3.8 0.2918
0.1000 30.00.2716
Toluene-d8 (Surr) 1.0511 1.0461 1.0491 1.0610 1.0113 Ave 2.3 1.0013
0.1000 30.01.0367
0.1000 30.00.8468
FORM VI 8260B
10/31/2012Page 136 of 813
N
Calibration Files:
LEVEL: LAB SAMPLE ID: LAB FILE ID: Level 1 IC 460-133133/3 e09277.d Level 2 IC 460-133133/4 e09278.d Level 3 ICIS 460-133133/2 e09273.d Level 4 IC 460-133133/5 e09279.d Level 5 IC 460-133133/6 e09280.d Level 6 IC 460-133133/7 e09281.d
ANALYTE CURVE TYPE
CONCENTRATION (UG/L)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 6
Dichlorodifluoromethane AveFB 5652 27039 87989 213774 958172 2641093
1.00 5.00 20.0 50.0 200 500
Chloromethane AveFB 10499 49748 179016 427508 1883260 5289390
1.00 5.00 20.0 50.0 200 500
Vinyl chloride AveFB 7792 38066 144221 340692 1486824 4315724
1.00 5.00 20.0 50.0 200 500
Bromomethane LinFFB 6221 25258 87741 201169 888247 2414765
1.00 5.00 20.0 50.0 200 500
Chloroethane AveFB 5098 21966 82894 195756 803698 +++++
1.00 5.00 20.0 50.0 200 +++++
Trichlorofluoromethane AveFB 7451 37823 147057 347725 1312784 3936688
1.00 5.00 20.0 50.0 200 500
1,1-Dichloroethene AveFB 4360 22226 74767 197642 794898 2604993
1.00 5.00 20.0 50.0 200 500
Carbon disulfide AveFB 16873 81132 303028 746243 3433007 10693293
1.00 5.00 20.0 50.0 200 500
1,1,2-Trichloro-1,2,2-trifluoroetha ne
1.00 5.00 20.0 50.0 200 500
Methylene Chloride AveFB 9543 40381 153721 373280 1462225 4322633
1.00 5.00 20.0 50.0 200 500
Acetone AveFB 2578 6955 11217 26042 113798 317359
5.00 15.0 20.0 50.0 200 500
trans-1,2-Dichloroethene AveFB 4899 25787 94047 243580 1051302 3341417
1.00 5.00 20.0 50.0 200 500
Methyl acetate AveFB 1119 5492 20338 52038 220167 699726
1.00 5.00 20.0 50.0 200 500
Methyl tert-butyl ether AveFB 16868 79316 318920 816984 3464387 11113713
1.00 5.00 20.0 50.0 200 500
1,1-Dichloroethane AveFB 10649 52949 200872 520402 2094218 6610081
1.00 5.00 20.0 50.0 200 500
cis-1,2-Dichloroethene AveFB 5979 28082 109361 270211 1119261 3548938
1.00 5.00 20.0 50.0 200 500
FORM VI 8260B 10/31/2012Page 137 of 813
FORM VI
N
ANALYTE CURVE TYPE
Cyclohexane AveFB 9071 44349 157862 415149 1925338 6490239
1.00 5.00 20.0 50.0 200 500
Chloroform AveFB 9596 47073 191977 485952 2011060 6182871
1.00 5.00 20.0 50.0 200 500
Carbon tetrachloride AveFB 6730 34080 122450 330472 1564485 5022722
1.00 5.00 20.0 50.0 200 500
1,1,1-Trichloroethane AveFB 8031 39740 154868 412044 1881521 5902931
1.00 5.00 20.0 50.0 200 500
2-Butanone (MEK) LinFFB 3043 9468 17466 45083 207809 641434
5.00 15.0 20.0 50.0 200 500
Benzene AveCBZ 22501 111968 443002 1097892 4875952 15292699
1.00 5.00 20.0 50.0 200 500
1,2-Dichloroethane AveFB 8018 38025 157546 389707 1650219 5068256
1.00 5.00 20.0 50.0 200 500
Methylcyclohexane AveFB 8593 40133 143545 368564 1627062 5507619
1.00 5.00 20.0 50.0 200 500
Trichloroethene AveFB 6124 29991 109657 278396 1276244 4229174
1.00 5.00 20.0 50.0 200 500
1,2-Dichloropropane AveFB 5891 29564 120103 295330 1291486 4154314
1.00 5.00 20.0 50.0 200 500
Dichlorobromomethane AveFB 6721 35047 152171 375130 1735496 5524121
1.00 5.00 20.0 50.0 200 500
cis-1,3-Dichloropropene AveCBZ 8993 47081 195397 480591 2150085 6946495
1.00 5.00 20.0 50.0 200 500
Toluene AveCBZ 27081 135172 526606 1278522 5711343 17384836
1.00 5.00 20.0 50.0 200 500
Tetrachloroethene AveCBZ 7195 34799 130089 329329 1475873 4581393
1.00 5.00 20.0 50.0 200 500
4-Methyl-2-pentanone (MIBK) AveCBZ 30775 84312 111145 281868 1294026 4234091
5.00 15.0 20.0 50.0 200 500
trans-1,3-Dichloropropene AveCBZ 7554 40569 181114 443675 2061669 6716304
1.00 5.00 20.0 50.0 200 500
1,1,2-Trichloroethane AveCBZ 3902 21156 86718 205930 924389 2974610
1.00 5.00 20.0 50.0 200 500
Chlorodibromomethane AveCBZ 5251 27987 127105 310646 1462961 4655038
1.00 5.00 20.0 50.0 200 500
1,2-Dibromoethane AveCBZ 5133 26080 110235 262595 1192992 3664694
1.00 5.00 20.0 50.0 200 500
2-Hexanone AveCBZ 23192 63434 95948 220487 1012683 2860968
5.00 15.0 20.0 50.0 200 500
Chlorobenzene AveCBZ 19181 92558 374897 889738 4073934 12076194
1.00 5.00 20.0 50.0 200 500
FORM VI 8260B 10/31/2012Page 138 of 813
FORM VI
N
ANALYTE CURVE TYPE
Ethylbenzene AveCBZ 10253 49684 192639 473826 2254445 6909087
1.00 5.00 20.0 50.0 200 500
m-Xylene & p-Xylene AveCBZ 25611 124543 496459 1201209 5861845 16326844
2.00 10.0 40.0 100 400 1000
o-Xylene AveCBZ 12165 61421 244886 586427 2778797 7906278
1.00 5.00 20.0 50.0 200 500
Bromoform AveCBZ 3672 20340 94905 232249 1193442 3386225
1.00 5.00 20.0 50.0 200 500
Styrene AveCBZ 19573 100902 423418 1004339 4892888 13848523
1.00 5.00 20.0 50.0 200 500
Isopropylbenzene AveCBZ 30452 152621 599386 1475964 7014081 18694381
1.00 5.00 20.0 50.0 200 500
1,1,2,2-Tetrachloroethane AveDCB 6618 33482 147424 337007 1615148 4392112
1.00 5.00 20.0 50.0 200 500
1,3-Dichlorobenzene AveDCB 15932 77593 321356 774407 3491238 9243627
1.00 5.00 20.0 50.0 200 500
1.00 5.00 20.0 50.0 200 500
1.00 5.00 20.0 50.0 200 500
1,2-Dibromo-3-Chloropropane AveDCB 1094 5446 24955 58145 277143 772181
1.00 5.00 20.0 50.0 200 500
1,2,4-Trichlorobenzene AveDCB 9750 43086 184728 425017 1819367 4960064
1.00 5.00 20.0 50.0 200 500
1,2-Dichloroethane-d4 (Surr) AveFB 284034 288310 288382 294972 300073 390976
50.0 50.0 50.0 50.0 50.0 50.0
Toluene-d8 (Surr) AveCBZ 949983 948992 996798 993419 1013962 1186675
50.0 50.0 50.0 50.0 50.0 50.0
4-Bromofluorobenzene AveDCB 478286 478323 499558 503114 549858 575768
50.0 50.0 50.0 50.0 50.0 50.0
Curve Type Legend: Ave = Average ISTD LinF = Linear ISTD forced zero
FORM VI 8260B 10/31/2012Page 139 of 813
Data File: /chem/VOAMS5.i/8260DE/10-22-12/22oct12.b/e09273.d Report Date: 23-Oct-2012 02:21
TestAmerica
AMOUNTS
========================== ==== == ====== ====== ======== ======= =======
4 Vinyl Chloride 62 1.028 1.028 (0.286) 144221 20.0000 19
6 Bromomethane 94 1.181 1.181 (0.328) 87741 20.0000 18
5 Chloroethane 64 1.236 1.236 (0.344) 82894 20.0000 20
7 Trichlorofluoromethane 101 1.297 1.297 (0.361) 147057 20.0000 20
14 Freon TF 101 1.571 1.571 (0.437) 87510 20.0000 18
15 1,1-Dichloroethene 96 1.553 1.553 (0.432) 74767 20.0000 18
16 Acetone 58 1.894 1.894 (0.527) 11217 20.0000 21
18 Carbon Disulfide 76 1.565 1.565 (0.435) 303028 20.0000 18
27 Methyl Acetate 74 1.961 1.961 (0.546) 20338 20.0000 18
22 Methylene Chloride 49 1.858 1.858 (0.517) 153721 20.0000 19
28 MTBE 73 2.022 2.022 (0.562) 318920 20.0000 19
25 trans-1,2-Dichloroethene 96 1.949 1.949 (0.542) 94047 20.0000 18
30 1,1-Dichloroethane 63 2.309 2.309 (0.642) 200872 20.0000 19
36 cis-1,2-Dichloroethene 96 2.650 2.650 (0.737) 109361 20.0000 19
10/31/2012Page 140 of 813
AMOUNTS
========================== ==== == ====== ====== ======== ======= =======
45 Carbon Tetrachloride 117 2.931 2.931 (0.815) 122450 20.0000 17
48 Benzene 78 3.260 3.260 (0.469) 443002 20.0000 19
49 1,2-Dichloroethane 62 3.412 3.412 (0.949) 157546 20.0000 20
* 52 Fluorobenzene 96 3.595 3.595 (1.000) 1101033 50.0000
54 Trichloroethene 95 3.741 3.741 (1.041) 109657 20.0000 18
56 Methyl cyclohexane 83 3.729 3.729 (1.037) 143545 20.0000 18
57 1,2-Dichloropropane 63 4.192 4.192 (1.166) 120103 20.0000 19
68 Bromodichloromethane 83 4.272 4.272 (1.188) 152171 20.0000 19
67 cis-1,3-Dichloropropene 75 4.906 4.906 (0.705) 195397 20.0000 19
70 4-Methyl-2-Pentanone 43 5.625 5.625 (0.809) 111145 20.0000 18
$ 65 Toluene-d8 (SUR) 98 5.107 5.107 (0.734) 996798 50.0000 51
66 Toluene 91 5.162 5.162 (0.742) 526606 20.0000 19
64 trans-1,3-Dichloropropene 75 5.650 5.650 (0.812) 181114 20.0000 20
69 1,1,2-Trichloroethane 83 5.826 5.826 (0.838) 86718 20.0000 20
71 Tetrachloroethene 166 5.582 5.582 (0.803) 130089 20.0000 18
73 2-Hexanone 43 6.674 6.674 (0.960) 95948 20.0000 20
74 Dibromochloromethane 129 6.015 6.015 (0.865) 127105 20.0000 20
77 1,2-Dibromoethane 107 6.259 6.259 (0.900) 110235 20.0000 20
* 78 Chlorobenzene-d5 117 6.954 6.954 (1.000) 950107 50.0000
79 Chlorobenzene 112 6.972 6.972 (1.003) 374897 20.0000 20
81 Ethylbenzene 106 7.064 7.064 (1.016) 192639 20.0000 18
82 m+p-Xylene 106 7.277 7.277 (1.046) 496459 40.0000 38
84 o-Xylene 106 7.856 7.856 (1.130) 244886 20.0000 19
85 Styrene 104 7.942 7.942 (1.142) 423418 20.0000 29
86 Bromoform 173 7.911 7.911 (1.138) 94905 20.0000 20
88 Isopropylbenzene 105 8.344 8.344 (1.200) 599386 20.0000 19
92 1,1,2,2-Tetrachloroethane 83 9.112 9.112 (0.871) 147424 20.0000 20
105 1,3-Dichlorobenzene 146 10.325 10.325 (0.987) 321356 20.0000 20
* 108 1,4-Dichlorobenzene-d4

Documents

J46192-1 Nj Full Package Final Report