2016 Collaborative Study of CORESTA Monitor 8 (CM8) · 2016 Collaborative Study of CORESTA Monitor 8 (CM8) for the Determination of Test Piece Weight, TPM, Water, Nicotine, NFDPM,

Routine Analytical Chemistry Sub-Group

Technical Report

2016 Collaborative Study of

CORESTA Monitor 8 (CM8)

for the Determination of Test Piece Weight TPM Water Nicotine NFDPM

Carbon Monoxide and Puff Count Obtained under Mainstream lsquoISOrsquo and lsquoIntensersquo

Smoking Regimes

February 2017

Co-ordinator

Linda A Crumpler Cerulean USA

Authors

Guy Jaccard and Donatien Tafin Djoko

Philip Morris International Switzerland

Table of Contents

Introduction 3 1

Organisation 3 2

21 Participants 3

22 Protocol 4

Raw Data 5 3

Statistical Analysis 19 4

Exclusion of outliers 19 41

411 Numerical outlier technique Cochran amp Grubbs test 19

Repeatability and reproducibility estimation 19 42

Data Representation 21 5

51 ISO smoking regime 22

52 Intense smoking regime 25

Comparison 28 6

61 Comparisons of Linear with Rotary smoking machines for test piece CM8 28

62 Comparison with previous studies 28

Conclusion 31 7

APPENDIX A - List of Participating Laboratories 32

APPENDIX B ndash Experimental Protocol 33

APPENDIX C ndash Departures from Experimental Protocol 34

APPENDIX D ndash Raw Data Set 35

APPENDIX E ndash IUPAC 1994 Harmonized Statistical Procedure 44

APPENDIX F ndash Linear - Rotary Comparisons 45

APPENDIX G ndash Rotary Smoking Machines 52

APPENDIX H ndash Linear Smoking Machines 59

APPENDIX I ndash Equipment Survey 66

RAC-103-CTR CM8 Coll Study 2016 ndash February 2017 377

Introduction 1

The CORESTA Routine Analytical Chemistry Sub-Group has been given the responsibility to

organize the annual testing of the CORESTA Monitor test piece

The 2016 study was designed

to measure mainstream ISO and Intense smoke yields of nicotine-free dry particulate

matter (NFDPM) nicotine and carbon monoxide (CO) to verify the current monitor test

piece CM8

to determine intra- and inter-laboratory variability for the measured ISO and Intense smoke

yields for the CM8

to verify the conditioned weight for the CM8

Organisation 2

21 Participants

In total 25 laboratories participated in the 2016 study Appendix A lists the participating

laboratories in alphabetical order Note the mix of labs between ISO and Intense differed

25 laboratories delivered data for ISO mainstream smoke for the CM8 test piece using 36

smoking machines (20 rotary smoking machines and 16 linear smoking machines)

20 laboratories delivered data for Intense mainstream smoke for the CM8 test piece using 28

One laboratory provided an incomplete data set

Table 1 summarises the number and type of smoking machines used

Table 1 Number of smoking machines

Machine Class ISO Intense

Linear smoking machines 16 13

LX-20 type 2 2

SM450 type 14 11

Rotary smoking machines 20 15

RM20A type 1 1

RM20D type 2 2

RM20H type 5 3

RM200 type 1 1

RM200A type 11 8

Total 36 28

Table 2 summarises the number of datasets provided for the reported parameters

Table 2 Number of datasets obtained

Physical Parameter

WEIGHT 175

Smoking Parameter ISO Intense

TPM 180 140

WATER 180 140

NIC 180 140

NFDPM 180 140

CO 180 140

PUFF 180 140

Total individual data obtained 1080 840

Total individual data expected 1080 840

A laboratory code number has been assigned in confidence by the study co-ordinator to each

of the individual smoking machines used in the study

22 Protocol

Participants were requested to follow the protocol ldquoAnnual Study of the CORESTA Monitor

Test Piece CM8 - 2016 Experimental Protocolrdquo (provided in Appendix B) to analyse the CM8

test pieces and to report the seven parameters listed in Table 3

Table 3 Parameters to be reported

Parameter Number of replicates Unit Code

Conditioned Weight 5 mgtest piece (tp) WEIGHT

Total Particulate Matter 5 mgtest piece (tp) TPM

Water content (smoke) 5 mgtest piece (tp) WATER

Smoke Nicotine 5 mgtest piece (tp) NIC

Nicotine Free Dry

Particulate Matter 5 mgtest piece (tp) NFDPM

Carbon Monoxide 5 mgtest piece (tp) CO

Puff count 5 pufftest piece (tp) PUFF

CM8 test pieces should have been smoked under two different mainstream smoking regimes

with a fixed butt length of 32 mm as defined in the following table

Table 4 Mainstream ISO and Intense (Health Canada Intense or HCI) smoking regime

parameters

Smoking

Regime

Puff Volume

Puff Frequency

Puff Duration

Vent Blocking

ISO 35 60 2 0

Intense (HCI) 55 30 2 100

The CM8 test piece was purchased by the participants individually via Borgwaldt KC or

Cerulean

Raw Data 3

Table 5 gives the results for conditioned weight while Tables 6 to 11 list the results for the

reported parameters for ISO smoking regime Tables 12 to 17 list the results for intense

smoking regime Basic statistics (mean and standard deviation) were applied to summarize the

raw data for each smoking machine used and parameters reported for CM8 test piece At this

stage no outlier statistics were applied Appendix D contains the raw data (single values) for

every measured parameter reported by smoking machine included in the study

Table 5 WEIGHT mean and standard deviation per laboratory code

Lab Code Machine Type Mean SD CV [] Sample size

1A R 96055 2731 0284 5

1B L 96519 3313 0343 5

2A R 94828 2622 0277 5

2B L 95000 5958 0627 5

3 R 90323 3183 0352 5

4A R 96060 2510 0261 5

4B R 96200 6481 0674 5

5A R 96494 1638 0170 5

5B R 95620 2978 0311 5

6A R 96612 4814 0498 5

6B L 96604 2688 0278 5

7A L 95598 3295 0345 5

7B R 95490 3365 0352 5

8 R 96653 2676 0277 5

9A L 95220 2564 0269 5

9B R 95900 2264 0236 5

10 L 96640 2595 0269 5

11 L 95968 8571 0893 5

12A R 95840 4930 0514 5

12B R 96226 2852 0296 5

12C L 95960 2702 0282 5

13A R 95806 2698 0282 5

13B R 95901 5717 0596 5

14 R 96102 3340 0348 5

15 R 95871 4505 0470 5

16 L 96286 4512 0469 5

17 L 95626 3166 0331 5

18 L 95285 3720 0390 5

19 L 95285 3720 0390 5

20 L 95767 5690 0594 5

22A R 96300 1414 0147 5

22B R 96240 1517 0158 5

23 R 94926 3700 0390 5

24 L 95591 5108 0534 5

25 L 96223 5979 0621 5

Table 6 ISO smoking regime TPM mean and standard deviation per laboratory code

Lab Code Machine Type Mean (mgtp) SD CV [] Sample size

1B L 1793 024 132 5

2B L 1765 063 357 5

6B L 1574 061 387 5

7A L 1804 039 214 5

9A L 1698 033 197 5

10 L 1807 048 265 5

11 L 1828 045 248 5

12C L 1728 055 321 5

16 L 1742 010 058 5

17 L 1616 030 187 5

18 L 1772 036 205 5

19 L 1772 036 205 5

20 L 1783 040 224 5

21 L 1832 050 272 5

24 L 1791 033 185 5

25 L 1607 079 494 5

1A R 1749 024 135 5

2A R 1698 028 166 5

3 R 1760 019 107 5

4A R 1723 028 165 5

4B R 1769 038 212 5

5A R 1703 022 127 5

5B R 1724 031 178 5

6A R 1740 031 176 5

7B R 1646 017 103 5

8 R 1737 022 125 5

9B R 1711 025 147 5

12A R 1758 040 227 5

12B R 1790 014 078 5

13A R 1674 017 104 5

13B R 1700 020 115 5

14 R 1746 044 254 5

15 R 1719 041 238 5

22A R 1752 020 115 5

22B R 1731 022 129 5

23 R 1651 037 226 5

Table 7 ISO Smoking regime WATER mean and standard deviation per laboratory code

1B L 161 007 428 5

2B L 145 008 518 5

6B L 118 014 1213 5

7A L 175 006 364 5

9A L 142 011 802 5

10 L 177 010 581 5

11 L 142 009 632 5

12C L 122 008 645 5

16 L 142 012 872 5

17 L 145 026 1823 5

18 L 147 019 1299 5

19 L 147 019 1299 5

20 L 214 013 611 5

21 L 120 024 2024 5

24 L 156 009 551 5

25 L 127 016 1261 5

1A R 215 007 316 5

2A R 174 008 444 5

3 R 196 010 493 5

4A R 197 008 406 5

4B R 213 013 629 5

5A R 197 009 471 5

5B R 192 008 419 5

6A R 227 010 445 5

7B R 184 007 396 5

8 R 206 013 637 5

9B R 203 012 579 5

12A R 250 012 464 5

12B R 244 010 430 5

13A R 205 007 362 5

13B R 204 012 576 5

14 R 228 017 739 5

15 R 188 016 834 5

22A R 219 007 337 5

22B R 215 005 225 5

23 R 179 003 179 5

Table 8 ISO Smoking regime Nicotine mean and standard deviation per laboratory code

1B L 1704 0029 170 5

2B L 1706 0039 227 5

6B L 1624 0048 295 5

7A L 1687 0033 194 5

9A L 1612 0200 1240 5

10 L 1748 0070 401 5

11 L 1691 0028 166 5

12C L 1669 0034 206 5

16 L 1731 0028 159 5

17 L 1674 0046 276 5

18 L 1697 0014 082 5

19 L 1697 0014 082 5

20 L 1734 0021 124 5

21 L 1812 0048 266 5

24 L 1694 0037 217 5

25 L 1743 0154 883 5

1A R 1669 0023 141 5

2A R 1638 0037 224 5

3 R 1652 0018 110 5

4A R 1630 0042 255 5

4B R 1653 0035 214 5

5A R 1612 0023 142 5

5B R 1602 0023 141 5

6A R 1661 0037 225 5

7B R 1564 0022 140 5

8 R 1535 0031 204 5

9B R 1659 0047 285 5

12A R 1719 0024 142 5

12B R 1718 0037 216 5

13A R 1497 0024 163 5

13B R 1546 0013 086 5

14 R 1590 0035 217 5

15 R 1651 0030 181 5

22A R 1612 0011 068 5

22B R 1630 0012 075 5

23 R 1639 0026 159 5

Table 9 ISO smoking regime NFDPM mean and standard deviation per laboratory code

1B L 1462 016 111 5

2B L 1449 053 366 5

6B L 1294 044 344 5

7A L 1460 031 214 5

9A L 1395 011 080 5

10 L 1455 039 269 5

11 L 1518 036 236 5

12C L 1439 049 338 5

16 L 1427 013 092 5

17 L 1304 054 413 5

18 L 1456 020 135 5

19 L 1456 020 135 5

20 L 1395 036 255 5

21 L 1531 057 371 5

24 L 1466 023 154 5

25 L 1306 066 509 5

1A R 1367 020 145 5

2A R 1361 023 169 5

3 R 1398 012 083 5

4A R 1363 024 176 5

4B R 1391 028 201 5

5A R 1347 014 107 5

5B R 1372 023 166 5

6A R 1346 019 142 5

7B R 1305 020 153 5

8 R 1378 026 192 5

9B R 1342 015 114 5

12A R 1337 037 278 5

12B R 1375 018 129 5

13A R 1319 015 112 5

13B R 1341 009 069 5

14 R 1359 028 204 5

15 R 1366 029 214 5

22A R 1371 019 136 5

22B R 1353 024 175 5

23 R 1308 037 283 5

Table 10 ISO Smoking regime CO mean and standard deviation per laboratory code

1B L 1335 020 150 5

2B L 1297 037 288 5

6B L 1260 099 790 5

7A L 1374 034 249 5

9A L 1233 019 153 5

10 L 1219 054 445 5

11 L 1267 044 350 5

12C L 1325 033 248 5

16 L 1307 024 185 5

17 L 1196 029 242 5

18 L 1335 010 072 5

19 L 1335 010 072 5

20 L 1324 033 248 5

21 L 1363 032 238 5

24 L 1263 040 315 5

25 L 1194 069 574 5

1A R 1368 010 076 5

2A R 1308 018 135 5

3 R 1345 023 172 5

4A R 1340 011 079 5

4B R 1394 041 294 5

5A R 1292 028 216 5

5B R 1360 034 251 5

6A R 1372 023 166 5

7B R 1291 013 098 5

8 R 1369 025 183 5

9B R 1276 023 182 5

12A R 1317 034 256 5

12B R 1375 024 175 5

13A R 1334 021 155 5

13B R 1338 030 227 5

14 R 1366 023 167 5

15 R 1377 019 139 5

22A R 1344 016 118 5

22B R 1341 016 116 5

23 R 1334 029 217 5

Table 11 ISO Smoking regime Puff count mean and standard deviation per laboratory code

Lab Code Machine Type Mean (pufftp) SD CV [] Sample size

1B L 796 005 059 5

2B L 806 012 144 5

6B L 814 018 219 5

7A L 789 009 112 5

9A L 781 024 306 5

10 L 802 020 245 5

11 L 784 018 225 5

12C L 794 021 263 5

16 L 850 014 168 5

17 L 774 016 203 5

18 L 787 015 187 5

19 L 787 015 187 5

20 L 769 014 188 5

21 L 808 008 097 5

24 L 792 010 128 5

25 L 751 030 400 5

1A R 767 005 068 5

2A R 727 008 109 5

3 R 779 008 099 5

4A R 748 011 146 5

4B R 758 013 172 5

5A R 782 011 144 5

5B R 766 017 216 5

6A R 773 009 117 5

7B R 716 011 160 5

8 R 754 010 127 5

9B R 755 008 107 5

12A R 755 006 078 5

12B R 771 008 102 5

13A R 740 017 225 5

13B R 769 007 091 5

14 R 761 011 140 5

15 R 750 018 246 5

22A R 757 008 110 5

22B R 759 007 088 5

23 R 732 009 117 5

Table 12 Intense smoking regime TPM mean and standard deviation per laboratory code

1B L 4551 091 200 5

2B L 4391 078 178 5

6B L 3936 067 170 5

9A L 4471 060 134 5

10 L 4667 073 157 5

11 L 5068 136 269 5

12C L 4644 031 066 5

17 L 4346 106 243 5

19 L 4566 087 190 5

20 L 4616 122 265 5

21 L 5008 077 153 5

24 L 4782 094 196 5

25 L 4434 081 182 5

1A R 4168 016 039 5

2A R 4014 024 061 5

3 R 4247 035 083 5

4A R 4097 039 095 5

4B R 4181 064 153 5

5B R 3997 040 101 5

6A R 4076 074 181 5

8 R 4044 043 107 5

9B R 4097 033 080 5

12A R 4125 046 112 5

12B R 4257 039 092 5

15 R 3957 052 131 5

22A R 4046 028 069 5

22B R 4015 045 112 5

23 R 3830 073 192 5

Table 13 Intense smoking regime Water mean and standard deviation per laboratory code

1B L 1237 038 305 5

2B L 999 037 375 5

6B L 906 034 381 5

9A L 1147 043 373 5

10 L 1152 052 453 5

11 L 1488 053 356 5

12C L 1061 019 179 5

17 L 1027 028 274 5

19 L 1095 038 348 5

20 L 1216 083 681 5

21 L 1285 026 206 5

24 L 1235 060 484 5

25 L 1004 031 307 5

1A R 1024 014 138 5

2A R 797 016 197 5

3 R 974 031 317 5

4A R 911 034 368 5

4B R 931 027 287 5

5B R 815 041 507 5

6A R 923 038 411 5

8 R 929 033 354 5

9B R 927 028 301 5

12A R 1004 051 508 5

12B R 935 017 181 5

15 R 823 029 349 5

22A R 953 005 052 5

22B R 926 038 410 5

23 R 1598 065 404 5

Table 14 Intense smoking regime Nicotine mean and standard deviation per laboratory code

1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

Table 15 Intense smoking regime NFDPM mean and standard deviation per laboratory code

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

Table 16 Intense smoking regime CO mean and standard deviation per laboratory code

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

Table 17 Intense smoking regime Puff count mean and standard deviation per laboratory code

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

Statistical Analysis 4

Exclusion of outliers 41

411 Numerical outlier technique Cochran amp Grubbs test

The statistical evaluation of data for this collaborative study followed the methods provided

by ISO 5725-21 For outlier testing the Grubbs and Cochran methods were used

ISO 5725-2 Tests Consistency

Cochranrsquos ndash test Within-laboratory variability Suitable for detecting whether the highest value in a set of laboratory standard deviations is an outlier or not

Grubbsrsquo ndash test Between-laboratory variability Suitable for detecting whether the highest (or lowest) laboratories averages are outliers or not

The protocol ldquoHarmonized statistical procedurerdquo defined by IUPAC (International Union of

Pure and Applied Chemistry) has been applied as well It consists of sequential applications of

the Cochran and Grubbs tests until no further outliers are detected or until a drop of more than

222 (for this study =29) in the original number of laboratories would occur (see flowchart

in Appendix F)

First apply the Cochran outlier test and if an outlying laboratory is identified then a single

value Grubbs test is performed on the individual values of this outlying laboratory (Individual

Grubbs) If no individual value is identified as outlier the outlying laboratory is removed

When an individual value is identified as an outlier only this value is removed

Afterwards single-value Grubbs test is applied and outlying laboratories are removed If no

laboratory is identified as outlier the pair-value test is applied (two values at the same end)

Remove any laboratory(ies) flagged by these tests but stop removal if more than 222 (2 of

9 laboratories) would be removed

The test was performed with both linear and rotary smoking machines together but also with

rotary respectively linear smoking machines separately The results provided in the report for

all smoking machines respectively with linear or rotary only smoking machines are obtained

after exclusion of the outliers for those respective categories

The paired value Grubbsrsquo test is an extension of the single value Grubbs test for pairs of

outliers The use is advised in ISO 5725 to detect pairs of outlier undetectable sequentially by

using single value Grubbs test

The outlying laboratories are provided in the Tables 18 to 23

Repeatability and reproducibility estimation 42

Repeatability and reproducibility limits are calculated for both smoking regimes each

parameter and for both smoking machine types The results are summarized in tables 18 to 23

with all machines grouped respectively with linear or rotary machines only both with ISO

and intense smoking regimes Outlying laboratories are provided in the same tables The

corresponding graphs named ldquoindividual valuesrdquo are given in Part 5 of this report

1 ISO 5725-21994 Accuracy (trueness and precision) of measurement methods and results ndash Part 2 Basic

method for the determination of repeatability and reproducibility of a standard measurement method

Table 18 r amp R estimations for CM8 under ISO smoking regime (all machines)

p n Global Mean Sr CVr[] r SR CVR [] R C GG2 Stragglers Parameter

34 5 959028 4035 0421 11414 6190 0645 17507 NA 3 11 Conditioned weight

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

Table 19 r amp R estimations for CM8 under ISO smoking regime (rotary machines)

20 5 959539 3575 0373 10111 5837 0608 16510 NA 3 NA Conditioned weight

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

20 5 7560 0107 1411 0302 0195 2584 0552 NA NA NA Puff count

Table 20 r amp R estimations for CM8 under ISO smoking regime (linear machines)

15 5 958382 4553 0475 12877 6687 0698 18913 NA NA NA Conditioned weight

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

Table 21 r amp R estimations for CM8 under Intense smoking regime (all machines)

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

Table 22 r amp R estimations for CM8 under Intense smoking regime (rotary machines)

p n Global Mean Sr CVr[] r SR CVR[] R C GG2 Stragglers Parameter

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

Table 23 r amp R estimations for CM8 under Intense smoking regime (linear machines)

p n Global Mean Sr CVr [] r SR CVR[ ] R C GG2 Stragglers Parameter

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Data Representation 5

The following figures show the raw data for CM8 and for all parameters The plots indicate

mean values with 95 confidence interval (CI) highlighted in green (for valid participants) or

in red (for participants detected as outlier) for each smoking machine Laboratories excluded

by outlier statistics are denoted by the name of the test rejecting the laboratory (G for Grubbs

G2 for double Grubbs and C for Cochran) The confidence limits at 95 and 99 for the

difference between the reference value (average of all laboratories) and the average of one

laboratory are plotted in orange and red respectively

51 ISO smoking regime

Figure 1 CM8 Individual observations of conditioned test piece WEIGHT

Straggler value in orange

Figure 2 CM8 Individual observations of mainstream ldquoISOrdquo TPM

Figure 3 CM8 Individual observations of mainstream ldquoISOrdquo WATER

Figure 4 CM8 Individual observations of mainstream ldquoISOrdquo Nicotine

Figure 5 CM8 Individual observations of mainstream ldquoISOrdquo NFDPM

Figure 6 CM8 Individual observations of mainstream ldquoISOrdquo CO

Figure 7 CM8 Individual observations of mainstream ldquoISOrdquo PUFF Count

52 Intense smoking regime

Figure 8 CM8 Individual observations of mainstream ldquoIntenserdquo TPM

Figure 9 CM8 Individual observations of mainstream ldquoIntenserdquo WATER

Figure 10 CM8 Individual observations of mainstream ldquoIntenserdquo Nicotine

Figure 11 CM8 Individual observations of mainstream ldquoIntenserdquo NFDPM

Figure 12 CM8 Individual observations of mainstream ldquoIntenserdquo CO

Figure 13 CM8 Individual observations of mainstream ldquoIntenserdquo PUFF Count

Comparison 6

61 Comparisons of Linear with Rotary smoking machines for test piece CM8

It should be noted that a statistical evaluation of differences in linear and rotary smoking

machine results on the basis of just one product (CM8) could be misleading Furthermore a

simplistic differentiation between linear and rotary smoking machines could also be

misleading as both machine types used in this study comprise different models produced by

different manufacturers Furthermore it has to be noted that each measurement from a rotary

machine represents a single result from a single pad onto which the smoke of twenty (or ten in

intense smoking regime) test pieces is trapped Linear smoking machines require 4 pads to

collect mainstream TPM from the same number of test pieces and hence each measurement

on a linear machine is the average of 4 results This has to be taken into account when

interpreting statistical differences in repeatability between machine classes

Due to the aforementioned reasons a pure statistical comparison seems to have limited value

Graphical comparison of smoke data separated for linear and rotary smoking machines are

available in Appendix F

62 Comparison with previous studies

This section compares the results of this study with previous collaborative studies of different

test pieces conducted by the Routine Analytical Subgroup under the ISO smoking regime It

has to be noted that the number of smoking machines smoking machine types and

participants varies throughout the studies

Table 24 lists the averages reproducibility and repeatability limits for the test pieces CM6

CM7 and CM8 under ISO smoking regime

Table 24 Averages repeatability reproducibility of CORESTA collaborative studies from 2008

to 2016 for different test pieces under ISO smoking conditions

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Test piece CM6 CM6 CM6 CM7 CM7 CM7 CM7 CM8 CM8

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

There is no systematic tendency for the mean values of CM8 between 2014 and 2016 some

parameters decrease slightly but nicotine slightly increases Repeatability and reproducibility

figures are quite stable and comparable to those obtained with the other test pieces taking into

account the slightly higher mean values of TPM and nicotine for CM8 than for the previous

test pieces

Table 25 lists the averages reproducibility and repeatability limits for the test pieces CM7 and

CM8 under intense smoking regime

to 2016 for different test pieces under intense smoking conditions

Intense smoking regime

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

With comparable mean values for CM7 and CM8 with the exception of nicotine higher in the

CM8 the values obtained for repeatability and reproducibility are generally better with CM8

(it shall not be forgotten however that the collaborative tests organized in 2013 and 2016 did

not include the same laboratories)

Table 26 lists the averages reproducibility and repeatability limits of weight

Table 26 Average weight data repeatability and reproducibility for test pieces CM8

Study CM8 2014 CM8 2016

Weight (mgtp) 9610 9590

Repeatability (r) 141 114

Reproducibility (R) 173 175

The data obtained in the two collaborative tests for the test piece conditioned weight are quite

stable in terms of average repeatability and reproducibility

Conclusion 7

In summary the analytical results for the CM8 test piece lead to the conclusion that CM8

remains stable and it can be used as a monitor test piece in smoke analysis

APPENDIX A - List of Participating Laboratories

Altria JTI UK

BAT Germany Karelia Tobacco Co

Borgwaldt ASL KTampG

CIT Monte Paz SA Landewyck Group sarl

Enthalpy Analytical Inc Liggett Group

Essentra Scientific Services MST Vectis

Imperial Tobacco Joure Papierfabrik Wattens

Imperial Tobacco Polaska SA PT HM Sampoerna Tbk

Imperial Tobacco Reemtsma RJ Reynolds Tobacco Company

Imperial Tobacco Seita RPC ndash Americas Souza Cruz

ITC Limited TDR Rovinj Croatia

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

APPENDIX B ndash Experimental Protocol

PT_SS_Collaborative_Proficiency Study Protocol Template_Jan 2016_RAC_REV3pdf

Collaborative Study

ANNUAL STUDY OF THE CORESTA MONITOR TEST PIECE CM8 - 2016

EXPERIMENTAL PROTOCOL

08 January 2016

1 Foreword

This CORESTA protocol describes the elements that the Standards Task Force has identified as important for describing elements of an experimental protocol for a collaborative study or a proficiency study as defined below (Horwitz 862)

bull Collaborative study

ldquoA collaborative study is an interlaboratory study in which each laboratory uses the defined method of analysis to analyse identical portions of homogeneous materials to assess the performance characteristics obtained for that method of analysisrdquo

CORESTA recognizes that collaborative studies require considerable effort and should be conducted only on methods that have received adequate prior testing

bull Proficiency Study

ldquoA proficiency study is an interlaboratory study consisting of one or more assays-conducted by a group of laboratories on one or more identical materials by whatever method is in use in each laboratory for the purpose of comparing the results of each laboratory with those of other laboratories with the objective of evaluating or improving performancerdquo

Proficiency studies often serve as pre-work for selecting a method for a full collaborative study

2 Table of Contents 1 Foreword 2

1 Introduction 4

2 Objectives 4

3 Study Coordinator(s) 4

4 Normative References 4

5 Methods 5

51 General Guidance 5

52 Test Specimen(s) 5

53 Sampling 5

54 Ventilation Zone Blocking 6

55 Butt Marking 6

56 Conditioning 6

57 Test Piece Weight 6

58 Smoking Machine 6

59 Smoking Plans 7

6 Target Variables and Data Reporting 10

7 Study Time Table 11

8 Data Submission 12

9 Explanation of Statistics to be Applied for a Collaborative Study 12

91 Repeatability and Reproducibility Estimation 12

Bibliography 13

Appendix A ndash Systegraveme International (SI) Units and their Symbols 14

1 Introduction The CORESTA Routine Analytical Chemistry Sub Group has been given the responsibility to organize the annual testing of the CORESTA Monitor test piece This year the study will include CM8

2 Objectives This yearrsquos study will have expanded objectives that include smoking the monitor test piece under both ISO and a specified intense smoking regime The study objectives are

bull To measure mainstream smoke yields of nicotine-free dry particulate matter (NFDPM) nicotine and carbon monoxide (CO) when smoked under ISO and a specified intense smoking regime

bull To establish the conditioned weight of CM8 prior to smoking bull To determine intra- and inter-laboratory variability for the measured smoke yields

and to continue this comparison over time bull To obtain statistical information about possible differences in smoke yields from

different smoking machines

3 Study Coordinator(s)

4 Normative References The relevant Standards for ISO smoking are

The relevant Standards for Intense smoking include the ISO Standards above and

Tar and Nicotine and CO T-115e4pdf

Note T-115 has been removed from the Health Canada website and therefore is embedded here

5 Methods

51 General Guidance

As a general guide experiments conducted under each puffing regime should be conducted according to ISO standard requirements Exceptions to this guiding principle include the puffing parameters applied for intense smoking regime the vent blocking applied the number of cigarettes smoked per sample and the butt length for smoking The study (the smoking results) and the daily use of the monitor are based on a fixed butt length of 33 mm

Please note that any operating conditions (a) not specified in the above ISO standards or regarded as optional (b) not specified in the intense method documents provided as guidelines and (c) any circumstances that may have influenced test results should be noted in the test report

Puffing parameter and vent blocking specifications for each puffing regime are summarized in Table 1 Note Although the CORESTA Monitor Test Pieces are unventilated it is advised to follow the Health Canada procedures exactly and tape the filter ventilation zone

Table 1 Smoking Regime Specifications

plusmn plusmn plusmn

52 Test Specimen(s)

53 Sampling The smoking plans will use 200 test pieces for each rotary smoking machine or 220 test pieces for each linear smoking machine included in the study A composite of all packs should be prepared for conditioning according to ISO 82432006 If a substantial period of

time is expected to occur between the times when the test pieces are smoked with the different smoking regimes then two separate composite samples should be prepared one for each smoking regime

54 Ventilation Zone Blocking The blocking of the filter ventilation zone will be achieved by wrapping a single layer of invisible tape 190 mm wide or equivalent around the complete circumference of the filter and tipping paper of the test articles

55 Butt Marking For the purpose of this study the CM8 test pieces will be butt marked to a fixed butt length of 33 mm

56 Conditioning The composite samples shall be conditioned for at least 48 hours but no more than 10 days under the following conditions

Temperature 22 plusmn 1degC Relative humidity 60 plusmn 3

Temperature and relative humidity of the conditioning enclosure shall be checked and recorded for every smoking run

Test cigarettes to be smoked for the determination of NFDPM nicotine and CO should be selected at random from the conditioned cigarettes

Any test pieces with visible defects shall be discarded

57 Test Piece Weight The test articles will be weighed for ISO smoking only since the ventilation zone blocking tape applied for intense smoking may vary between laboratories The weight of the test piece after conditioning is to be determined by weighing all test pieces to be smoked just before they are placed at the smoking machine The result is reported as the mean weight of the 20 test pieces for linear or rotary smoking machine at ISO puffing parameters

58 Smoking Machine Where smoking laboratories have more than one type of smoking machine (ie linear and rotary variants) they are encouraged to include as many types in the study as possible

59 Smoking Plans The smoking plans will incorporate one product (CM8) shown as M in the smoking plans These plans are designed to smoke the CM8 in all ports for each puffing regime spread over a number of days If possible each participating laboratory should use only one operator (for each smoking machine type) throughout the course of the study

For ISO smoking one test result is defined as the mean yield obtained from smoking 20 test pieces in a single smoking machine run therefore from a rotary machine it is the result from one run smoking 20 test pieces and from a linear machine it is the average of four ports smoking five test pieces per port This is repeated on five separate days resulting in 100 test pieces being smoked (Tables 2-3)

For Intense smoking the number of test pieces smoked per filter pad is reduced to avoid overloading the pad As a consequence the number of smoking runsports has to be increased so that the same nominal numbers of test pieces are smoked Thus a test result from a rotary machine is the mean of two runs each of 10 test pieces and from a linear machine it is the average of eight ports smoking three test pieces per port (Tables 4-5)

Note that the side seam of the test pieces should be positioned at random and not in a fixed position since it has been observed that some laboratory staff habitually place cigarettes in a particular orientation Ports not occupied by the test pieces are left blank which may be assigned to any other cigarette that is to be smoked by the laboratory or the ports may be left empty

Table 2 Smoking Plan for 20-port Linear Machines for ISO smoking (5 test pieces per pad)

Table 3 Smoking Plan for 20-port Rotary Machines for ISO smoking (20 test pieces per pad)

Table 4 Smoking Plan for 20-port Linear Machines for Intense smoking (3 test pieces per pad)

Table 5 Smoking Plan for 20-port Rotary Machines for Intense smoking (10 test pieces per pad)

6 Target Variables and Data Reporting The variables to be reported fall into two categories those which will form the basis of the statistical evaluation of the data and those that are ancillary to the test The variables to be reported for statistical analysis are bull Mean weight of the Monitor after conditioning (just prior to smoking) bull Mean puff number per test piece bull Mean TPM per test piece bull Mean nicotine delivery per test piece bull Mean water delivery per test piece bull Mean NFDPM delivery per test piece bull Mean CO delivery per test piece The ancillary variables are bull Date of test bull Type of smoking machine used bull Temperature (Cdeg) and relative humidity (RH) of conditioning enclosure bull Temperature (Cdeg) and relative humidity (RH) of smoking environment bull Atmospheric pressure in the laboratory during smoking bull Ambient air flow in the smoking machine before smoking (mmsec)

Dimensions and rounding of test results Analytical variables

Weight of Monitor mg per test piece

Puff number number

TPM mg per test piece

Nicotine mg per test piece

Water mg per test piece

NFDPM mg per test piece

Carbon Monoxide mg per test piece

Ancillary variables

Date of test DDMMYY

Conditioning temperature degrees Celsius

Conditioning humidity percent RH

Air velocity mms

Laboratory temperature degrees Celsius

Laboratory humidity percent RH

Laboratory barometric pressure

Please note that the rounding of the data to the formats specified above must take place after any calculations that may be involved All calculations will use the laboratory data as recorded using the maximum number of digits available All data arising from this study will be made available to the laboratories participating in the study The distribution of data will be done after collation and statistical evaluation To facilitate the statistical evaluation all data must be reported using the attached spreadsheets and must be submitted via e-mail Please use the attached spreadsheets as provided without changing the format

7 Study Time Table

The smoking should be performed during January and February 2016 Strict adherence to the timeline is very important for the data to be compiled for an initial assessment at the next Sub-Group meeting on April 2016 Data not received by February 26 2016 will be excluded from the formal statistical analysis Please review your data carefully before submitting as the statistical analysis is very labour intensive

The statistical analysis of the results will follow as closely as possible the recommendations of ISO 5725

Should any questions arise please contact the study coordinator Linda Crumpler

All results must be sent via e-mail to

Linda A Crumpler lindacrumplerceruleancom

8 Data Submission

9 Explanation of Minimum Statistics to be Applied for a Collaborative Study

91 Repeatability and Reproducibility Estimation

Bibliography

Chem Pure Appl QUALITY ASSURANCE SCHEMES THE INTERNATIONAL HARMONIZED PROTOCOL FOR THE PROFICIENCY TESTING OF ANALYTICAL CHEMISTRY LABORATORIES (nd) n pag Web

Council of Science Editors 8th ed Np Council of Science Editors nd Print

Form and Style for ASTM Standards West Conshohocken PA ASTM INTERNATIONAL 2015 Print

Horwitz William Protocol for the Design Conduct and Interpretation of Collaborative Studies Pure and Applied Chemistry 606 (1988) 855-64 ShareGate International Union of Pure and Applied Chemistry De Gruyter Jan 1988 Web 30 July 2015

ISO 5725 Standard And Reference Laboratories Errorpdf ISO 5252 ISO 5725 Standard And Reference Laboratories Error (nd) n pag Web

IUPAC 2006 IUPAC Pure and Applied Chemistry 78 145ndash196 Np nd Web 25 Aug 2015

Numbers Units Mathematicial Expressions and Statistics Scientific Style and Format The CSE Manual for Authors Editors and Publishers 8th ed Chicago The University of Chicago 2014 157-91 Print

Appendix A ndash Systegraveme International (SI) Units and their Symbols

SI base units

Base Quantity Name Symbol Length meter m Mass kilogram Kg Time second s Electric current ampere A Temperature kelvin K Amount of substance mole mol Luminous intensity Candela cd

SI derived units

Derived Quantity Name Symbol Equivalent SI Units

Frequency hertz Hz s-1 Force newton N mmiddotkgmiddots-2 Pressure pascal Pa Nm2 Energy joule J Nmiddotm Power watt W Js Electric charge coulomb C smiddotA Electric potential volt V WA Electric resistance ohm Ω VA Celsius temperature Degrees Celsius degC K Unit degree Celsius is equal in magnititude to unit kelvin

SI prefixes

Factor Name Symbol Numerical Value 1012 tera T 1 000 000 000 000 109 giga G 1 000 000 000 106 mega M 1 000 000 103 kilo k 1 000 102 hecto h 100 101 deka da 10 10-1 deci d 01 10-2 centi c 001 10-3 milli m 0001 10-6 micro micro 0000 001 10-9 nano n 0000 000 001 10-12 pico p 0000 000 000 001

1 Foreword

1 Introduction

2 Objectives

4 Normative References

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

54 Ventilation Zone Blocking

55 Butt Marking

56 Conditioning

57 Test Piece Weight

58 Smoking Machine

59 Smoking Plans

6 Target Variables and Data Reporting

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe
RAC-103-CTR_Protocol-CM8-Coll-Study-2016pdf


APPENDIX C ndash Departures from Experimental Protocol

One Laboratory (Lab 9A) smoked 2 cigarettes per port on linear smoking machine for the

analyses performed with intense smoking regime


APPENDIX D ndash Raw Data Set

Table 1 Raw data for CM8 ndash ISO Smoking regime

Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783

Table 2 Raw data for CM8 ndash Intense Smoking regime

Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080

5 8 5A R RM20A 1 NA NA NA NA NA NA

5A R RM20A 2 NA NA NA NA NA NA




9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160

7 12 7A L SM450 1 NA NA NA NA NA NA

7A L SM450 2 NA NA NA NA NA NA



Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count



13 7B R RM200A 1 NA NA NA NA NA NA

7B R RM200A 2 NA NA NA NA NA NA




8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125

13 22 13A R RM20H 1 NA NA NA NA NA NA

13A R RM20H 2 NA NA NA NA NA NA




23 13B R RM20H 1 NA NA NA NA NA NA

13B R RM20H 2 NA NA NA NA NA NA



13B R RM20H M2

5 NA NA NA NA NA NA

14 24 14 R RM200A 1 NA NA NA NA NA NA

14 R RM200A 2 NA NA NA NA NA NA




15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076

16 26 16 L SM450 1 NA NA NA NA NA NA

16 L SM450 2 NA NA NA NA NA NA




17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120


APPENDIX E ndash IUPAC 1994 Harmonized Statistical Procedure

IUPAC 1994 HARMONIZED STATISTICAL PROCEDURE

SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES

DROP LAB UNLESS OVERALL

FRACTION OF LABS DROPPED

WOULD EXCEED 29

DROP INDIVIDUAL VALUE



WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS

OUTLIER ON INDIVIDUAL VALUES

OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO


APPENDIX F ndash Linear - Rotary Comparisons

Figure 1 CM8 under ISO smoking regime ndash r and R values (conditioned weight)

Figure 2 CM8 under ISO smoking regime ndash r and R values (TPM)


Figure 3 CM8 under ISO smoking regime ndash r and R values (Water)

Figure 4 CM8 under ISO smoking regime ndash r and R values (Nicotine)


Figure 5 CM8 under ISO smoking regime ndash r and R values (NFDPM)

Figure 6 CM8 under ISO smoking regime ndash r and R values (CO)


Figure 7 CM8 under ISO smoking regime ndash r and R values (Puff count)

Figure 8 CM8 under intense smoking regime ndash r and R values (TPM)


Figure 9 CM8 under intense smoking regime ndash r and R values (Water)

Figure 10 CM8 under intense smoking regime ndash r and R values (Nicotine)


Figure 11 CM8 under intense smoking regime ndash r and R values (NFDPM)

Figure 12 CM8 under intense smoking regime ndash r and R values (CO)


Figure 13 CM8 under intense smoking regime ndash r and R values (Puff count)


APPENDIX G ndash Rotary Smoking Machines


Figure 1 CM8 Individual observations of mainstream ldquoISOrdquo conditioned WEIGHT





















APPENDIX H ndash Linear Smoking Machines






















RAC-103-STR-CM8 Coll Study 2016 ndash February 2017 6677

APPENDIX I ndash Equipment Survey

Lab Code

Smoking Machine Model Manufacturer

Gas Chromatograph ModelManufacturerColumn Internal Standards

Airlflow Meter ModelManufacturer

NDIR analyser ModelManufacturer

1A RM200A Borgwaldt Agilent 7890A

Nic Column Length 25m id 032mm Film Thickness 03microm Stationary Phase HP-20M Carbowax

Nicotine IS n-Octadecane

Anemometer Type g4403s-113 Schiltknecht

CO-Measuring Unit Model No70700050 Borgwaldt

Water Column Length 15m Film thickness 20microm Stationary Phase HP-PLOTQ

Water IS Ethanol

1B SM450 Cerulean Agilent 7890A


Nicotine IS n-Heptadecane


COA205Cerulean


Water IS Ethanol

2A RM200A Borgwaldt Agilent 68907890

Nic Column Length 25m id 032mm Film Thickness 03microm Stationary Phase Polyethylenglycol (PEG)



Anemometer Type g4403s-181 Schiltknecht Water Column

Length 15m id 032mm Film Thickness 020microm Stationary Phase Polystrene - divinylbenzene

Water IS Ethanol


Lab Code





2B SM450 Cerulean Agilent 68907890


Nicotine ISn-Heptadecane


Cerulean COA205 Water Column Length 15m id 032mm Film Thickness 020microm Stationary Phase Polystrene - divinylbenzene

Water IS Ethanol

3 RM200 Borgwaldt 6890A Agilent

Nicotine Column Length 30m Id 032mm Film Thickness 025microm Stationary Phase Agilent 10191N-113 HP-INNOWAX


80709500Borgwaldt 70700050Borgwaldt Water Column Length 30m id 032 Film Thickness 020microm Stationary Phase JampW 1909 IP-Q04 bonded polystyrene-divinyl benzene (DVB)

Water IS Ethanol


Nic Column Length 5m id 020 Film Thickness 040microm Stationary Phase DB-WAXetr high polarity polyethylene glycol (PEG)


Anemometer Schiltknecht CO-Analyser Borgwaldt

Water Column Length 6 Stainless Steel Packed id 2mm Stationary Phase Porapak Q cross-linked

Water IS Ethanol


Lab Code





4B RM20D Borgwaldt Agilent 6890





Water IS Ethanol

5A RM20 Borgwaldt Agilent 6890 7890

A



Anemometer Type g 4403s-113 Schiltknecht

CO-Analyser Borgwaldt

Water Column Length 6 Stainless Steel Packed id 2mm Stationary Phase JampW Porapak QS 80-100 mesh

Water IS Ethanol

5B RM200A Borgwaldt Agilent 6890 7890

A






Water IS Ethanol


Lab Code





6A RM20D Borgwaldt 7890 B Agilent

Nic Column INNO Steel Packed Length 18m id 20mm Stationary Phase 75 Carbowax 2 KOH 80100 Chromosorb-WAW


Schiltknecht C24 Borgwaldt Water Column INNO Steel packed column Length 360m id 20mm Stationary Phase 6080 Hayesep-Q porous polymer

Water IS Methanol

6B LX20 Borgwaldt 7890 B Agilent




Water IS Methanol

7A SM450 Cerulean Agilent 7890

Nic Column Capillary HP-20M Length 25m id 032mm Film Thickness 030microm Stationary Phase Polyethylene Glycol


Schiltknecht Cerulean COA205 Water Column Capillary Length 15m id 032mm Film Thickness 020microm Stationary Phase HP Plot-Q bonded polystyrene-divinyl benzene (DVB)

Water IS Ethanol


Lab Code





7B RM200A Borgwaldt Agilent 7890



Schiltknecht Borgwaldt Water Column Capillary Length 15m id 032mm Film Thickness 020microm Stationary Phase HP Plot-Q bonded polystyrene-divinyl benzene (DVB)

Water IS Ethanol

8 RM20H Borgwaldt Agilent 6890

Nic Column Length 18m id 2mm Film Thickness Stationary Phase 10 Carbowax 2M 2 KOH


Schiltknecht C24Borgwaldt

Water Column Porapak Q 2m packed

Water IS Ethanol

9A SM450RH Cerulean Agilent 7890

Nic Column Capillary Agilent CP7424 Length id Film Thickness Stationary Phase CP-Wax


ThermoAire3 Schiltknecht Cerulean COA200 Water Column Capillary Agilent CP7554 Length id Film Thickness Stationary Phase PoraPLOT Q

Water IS Ethanol


Lab Code








RM200A Schiltknecht Integrated NDIR analyser Water Column Capillary Agilent CP7554 Length id Film Thickness Stationary Phase PoraPLOT Q

Water IS Ethanol

10 SM450 Cerulean Agilent 7890

Nic Column Capillary Length 5m id 0200mm Film Thickness 040microm Stationary Phase DB-Wax ETR

Nicotine IS Octadecane

ThermoAire2 Schiltknecht Cerulean COA

Water Column Packed 6 ft x 18 in x 21mm 80-100 mesh Porapak Q

Water IS Ethanol


Nic Column Capillary CP WAX 52 CB Length id 053mm Film Thickness 1microm Stationary PhaseCP-Wax

Nicotine IS Decanol

Schiltknecht Cerulean COA205

Water Column Capillary Length id 053mm Film Thickness 20microm Stationary Phase PoraPLOT Q

Water IS Ethanol


Lab Code





12A RM200A Borgwaldt HP 6890

Nic Column Length 30m id 032mm Film Thickness 025microm Stationary PhaseCP-Wax

Nicotine IS Heptadecane

Schiltknecht SibenchSiemens Water Column Capillary Length id 053mm Film Thickness 20microm Stationary Phase PoraPLOT Q

Water IS Methanol

12B RM200A2 Borgwaldt HP 6890




Water IS Methanol

12C KC LX20 Borgwaldt HP 6890

Nic Column Length 30m id 032mm Film Thickness 025microm Stationary Phase CP-Wax

Nicotine ISHeptadecane


Water IS Methanol


Lab Code





13A RM20H Borgwaldt M1 Agilent 7890B

Nic Column Length 5m id Film Thickness 04microm Stationary Phase DB-WAXETR


Schiltknecht g4403S-113

Built in RM20H Water Column Length 30m id Film Thickness 40microm Stationary Phase PoraPLOT Q

Water IS Ethanol

13B RM20H Borgwaldt M2 Agilent 7890B



Schiltknecht g4403s-113


Ethanol

14 RM200A Borgwaldt Nicotine Agilent

6890 Water Agilent 7890

Nic Column Length 30 id 0320mm Film thickness 025 Stationary Phase HP-INNOWAX



Borgwaldt COCO2 Analyser Water Column Length 30m id 0320mm Film Thickness 20microm Stationary Phase HP-PLOTQ

Water IS Ethanol


Lab Code





15 RM200A Borgwaldt Agilent 7890B

Nic Column Length 2m id 18in Film thickness Stationary Phase 80-100 mesh Carbowax 20M 2 KOH

Nicotine IS Quinaldine


Borgwaldt COCO2 Analyser Water Column Length 2m id 18in Film Thickness Stationary Phase 80100 mesh Porapak Q

Water IS Ethanol


Nic Column Length 6ft Stainlees Steel id 18in Film thickness Stationary Phase 80100 mesh2 Versamid + 1 KOH on Chromasorb 750


ThermoAire2 SchiltknechtVMD100 Filtrona

Cerulean COA 205

Water Column Length 6ft Stainlees Steel id 18in Film Thickness Stationary Phase 80100 mesh Porapak Q

Water IS Methanol

17 SM450 Cerulean Agilent 6890N

Nic Column Length 10m id 018mm Film thickness 03microm Stationary Phase DB Wax

Nicotine IS Anethole

VPS 103 Schiltknecht

Cerulean COA 205 Water Column Length 3ft Stainlees Steel id 025in Film Thickness Stationary Phase Haye SepQ 6080 mesh

Water IS Ethanol


Lab Code






Nic Column Length 30m id 053mm Film Thickness 1microm Stationary Phase Restek Stabilwax


ThermoAire2 Schiltknecht Cerulean COA 205

Water Column Supelco 80100 mesh Porapak R 18x 21mm

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Nic Column Polyethylene glycol 20 M + 10 KOH + 2 Chromosorb W80100 AW-DMCS Shimadzu 20 m x 30 m


996 ThermoAire2 Schiltknecht Cerulean COA 205

Water Column PorapakQ 80100 Shimadzu 20m x 30m

Water IS Ethanol 998

20 SM450 Cerulean HP 5890

Nic Column Length 30m id 053mm Film thickness 01microm Stationary Phase Restek Stabilwax


Schiltknecht 1 Air Flow meter

Cerulean COA 205


Water IS Ethanol


Nic Column Length 2mid 2mmFilm thickness Stationary PhaseCarbowax 10 + 2 KOH


435-2Testo Cerulean COA 205 Water Column Length 2m id 2mm Film Thickness Stationary Phase 80100 mesh Porapak QS

Water IS Ethanol


Lab Code





22A RM20H Borgwaldt

Model No 70740010 Agilent 7890A

Nic Column Length 2m id 18 Film thickness 21mm Stationary Phase 10 Carbowax 20M + 2 KOH



70740050Borgwaldt Water Column Length 2m id 18 Film Thickness 20mm Stationary Phase 80100 mesh Porapak Q

Water IS Ethanol

22B RM20D Borgwaldt Model No70750020

Agilent 7890A





Water IS Ethanol

23 RM20H Borgwaldt Agilent 7890B

Nic Column Length 30m id Film thickness 025microm Stationary Phase HP-5MS Crosslinked 5 PHME Siloxane


Schiltknecht Flow Meter Borgwaldt CO Analyzer Water Column Length 30m id Film Thickness 20microm Stationary Phase HP-Plot Q Divenylbenzenestyrene porous polymer

Water IS Ethanol


Lab Code





24 SM450 Cerulean Agilent 7890B

Nic Column Length 15m + 5m guard id 032mm Film thickness 025microm Stationary Phase Restek 10821 Stabilwax-DB


Schiltknecht Messtechnik ThermoAire6

Cerulean COA 205 Water Column Length 10 id 18 Film Thickness Stationary Phase 80100 mesh Porapak-QS

Water IS Ethanol


Nic ColumnSS 18OD Stationary Phase 7 Carbowax 20M 2 KOH 3 OS-138 Chromosorb W-HP 80100 mesh

Nicotine ISAnethole

ThermoAire2 Schiltknecht Cerulean COA 205 Water Column SS 18OD Stationary Phase Porapak QS 80100 mesh

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data

4 Statistical Analysis

41 Exclusion of outliers


42 Repeatability and reproducibility estimation

5 Data Representation



6 Comparison



7 Conclusion










Table of Contents

Introduction 3 1

Organisation 3 2

21 Participants 3

22 Protocol 4

Raw Data 5 3

Statistical Analysis 19 4

Exclusion of outliers 19 41

411 Numerical outlier technique Cochran amp Grubbs test 19

Repeatability and reproducibility estimation 19 42

Data Representation 21 5

51 ISO smoking regime 22

52 Intense smoking regime 25

Comparison 28 6

61 Comparisons of Linear with Rotary smoking machines for test piece CM8 28

62 Comparison with previous studies 28

Conclusion 31 7

APPENDIX A - List of Participating Laboratories 32

APPENDIX B ndash Experimental Protocol 33

APPENDIX C ndash Departures from Experimental Protocol 34

APPENDIX D ndash Raw Data Set 35

APPENDIX E ndash IUPAC 1994 Harmonized Statistical Procedure 44

APPENDIX F ndash Linear - Rotary Comparisons 45

APPENDIX G ndash Rotary Smoking Machines 52

APPENDIX H ndash Linear Smoking Machines 59

APPENDIX I ndash Equipment Survey 66

Introduction 1

piece CM8

yields for the CM8

Organisation 2

21 Participants

LX-20 type 2 2

SM450 type 14 11

RM20A type 1 1

RM20D type 2 2

RM20H type 5 3

RM200 type 1 1

RM200A type 11 8

Total 36 28

Physical Parameter

WEIGHT 175

TPM 180 140

WATER 180 140

NIC 180 140

NFDPM 180 140

CO 180 140

PUFF 180 140

22 Protocol

Nicotine Free Dry

parameters

Smoking

Regime

Puff Volume

Puff Frequency

Puff Duration

Vent Blocking

ISO 35 60 2 0

Cerulean

Raw Data 3

1A R 96055 2731 0284 5

1B L 96519 3313 0343 5

2A R 94828 2622 0277 5

2B L 95000 5958 0627 5

3 R 90323 3183 0352 5

4A R 96060 2510 0261 5

4B R 96200 6481 0674 5

5A R 96494 1638 0170 5

5B R 95620 2978 0311 5

6A R 96612 4814 0498 5

6B L 96604 2688 0278 5

7A L 95598 3295 0345 5

7B R 95490 3365 0352 5

8 R 96653 2676 0277 5

9A L 95220 2564 0269 5

9B R 95900 2264 0236 5

10 L 96640 2595 0269 5

11 L 95968 8571 0893 5

12A R 95840 4930 0514 5

12B R 96226 2852 0296 5

12C L 95960 2702 0282 5

13A R 95806 2698 0282 5

13B R 95901 5717 0596 5

14 R 96102 3340 0348 5

15 R 95871 4505 0470 5

16 L 96286 4512 0469 5

17 L 95626 3166 0331 5

18 L 95285 3720 0390 5

19 L 95285 3720 0390 5

20 L 95767 5690 0594 5

22A R 96300 1414 0147 5

22B R 96240 1517 0158 5

23 R 94926 3700 0390 5

24 L 95591 5108 0534 5

25 L 96223 5979 0621 5

1B L 1793 024 132 5

2B L 1765 063 357 5

6B L 1574 061 387 5

7A L 1804 039 214 5

9A L 1698 033 197 5

10 L 1807 048 265 5

11 L 1828 045 248 5

12C L 1728 055 321 5

16 L 1742 010 058 5

17 L 1616 030 187 5

18 L 1772 036 205 5

19 L 1772 036 205 5

20 L 1783 040 224 5

21 L 1832 050 272 5

24 L 1791 033 185 5

25 L 1607 079 494 5

1A R 1749 024 135 5

2A R 1698 028 166 5

3 R 1760 019 107 5

4A R 1723 028 165 5

4B R 1769 038 212 5

5A R 1703 022 127 5

5B R 1724 031 178 5

6A R 1740 031 176 5

7B R 1646 017 103 5

8 R 1737 022 125 5

9B R 1711 025 147 5

12A R 1758 040 227 5

12B R 1790 014 078 5

13A R 1674 017 104 5

13B R 1700 020 115 5

14 R 1746 044 254 5

15 R 1719 041 238 5

22A R 1752 020 115 5

22B R 1731 022 129 5

23 R 1651 037 226 5

1B L 161 007 428 5

2B L 145 008 518 5

6B L 118 014 1213 5

7A L 175 006 364 5

9A L 142 011 802 5

10 L 177 010 581 5

11 L 142 009 632 5

12C L 122 008 645 5

16 L 142 012 872 5

17 L 145 026 1823 5

18 L 147 019 1299 5

19 L 147 019 1299 5

20 L 214 013 611 5

21 L 120 024 2024 5

24 L 156 009 551 5

25 L 127 016 1261 5

1A R 215 007 316 5

2A R 174 008 444 5

3 R 196 010 493 5

4A R 197 008 406 5

4B R 213 013 629 5

5A R 197 009 471 5

5B R 192 008 419 5

6A R 227 010 445 5

7B R 184 007 396 5

8 R 206 013 637 5

9B R 203 012 579 5

12A R 250 012 464 5

12B R 244 010 430 5

13A R 205 007 362 5

13B R 204 012 576 5

14 R 228 017 739 5

15 R 188 016 834 5

22A R 219 007 337 5

22B R 215 005 225 5

23 R 179 003 179 5

1B L 1704 0029 170 5

2B L 1706 0039 227 5

6B L 1624 0048 295 5

7A L 1687 0033 194 5

9A L 1612 0200 1240 5

10 L 1748 0070 401 5

11 L 1691 0028 166 5

12C L 1669 0034 206 5

16 L 1731 0028 159 5

17 L 1674 0046 276 5

18 L 1697 0014 082 5

19 L 1697 0014 082 5

20 L 1734 0021 124 5

21 L 1812 0048 266 5

24 L 1694 0037 217 5

25 L 1743 0154 883 5

1A R 1669 0023 141 5

2A R 1638 0037 224 5

3 R 1652 0018 110 5

4A R 1630 0042 255 5

4B R 1653 0035 214 5

5A R 1612 0023 142 5

5B R 1602 0023 141 5

6A R 1661 0037 225 5

7B R 1564 0022 140 5

8 R 1535 0031 204 5

9B R 1659 0047 285 5

12A R 1719 0024 142 5

12B R 1718 0037 216 5

13A R 1497 0024 163 5

13B R 1546 0013 086 5

14 R 1590 0035 217 5

15 R 1651 0030 181 5

22A R 1612 0011 068 5

22B R 1630 0012 075 5

23 R 1639 0026 159 5

1B L 1462 016 111 5

2B L 1449 053 366 5

6B L 1294 044 344 5

7A L 1460 031 214 5

9A L 1395 011 080 5

10 L 1455 039 269 5

11 L 1518 036 236 5

12C L 1439 049 338 5

16 L 1427 013 092 5

17 L 1304 054 413 5

18 L 1456 020 135 5

19 L 1456 020 135 5

20 L 1395 036 255 5

21 L 1531 057 371 5

24 L 1466 023 154 5

25 L 1306 066 509 5

1A R 1367 020 145 5

2A R 1361 023 169 5

3 R 1398 012 083 5

4A R 1363 024 176 5

4B R 1391 028 201 5

5A R 1347 014 107 5

5B R 1372 023 166 5

6A R 1346 019 142 5

7B R 1305 020 153 5

8 R 1378 026 192 5

9B R 1342 015 114 5

12A R 1337 037 278 5

12B R 1375 018 129 5

13A R 1319 015 112 5

13B R 1341 009 069 5

14 R 1359 028 204 5

15 R 1366 029 214 5

22A R 1371 019 136 5

22B R 1353 024 175 5

23 R 1308 037 283 5

1B L 1335 020 150 5

2B L 1297 037 288 5

6B L 1260 099 790 5

7A L 1374 034 249 5

9A L 1233 019 153 5

10 L 1219 054 445 5

11 L 1267 044 350 5

12C L 1325 033 248 5

16 L 1307 024 185 5

17 L 1196 029 242 5

18 L 1335 010 072 5

19 L 1335 010 072 5

20 L 1324 033 248 5

21 L 1363 032 238 5

24 L 1263 040 315 5

25 L 1194 069 574 5

1A R 1368 010 076 5

2A R 1308 018 135 5

3 R 1345 023 172 5

4A R 1340 011 079 5

4B R 1394 041 294 5

5A R 1292 028 216 5

5B R 1360 034 251 5

6A R 1372 023 166 5

7B R 1291 013 098 5

8 R 1369 025 183 5

9B R 1276 023 182 5

12A R 1317 034 256 5

12B R 1375 024 175 5

13A R 1334 021 155 5

13B R 1338 030 227 5

14 R 1366 023 167 5

15 R 1377 019 139 5

22A R 1344 016 118 5

22B R 1341 016 116 5

23 R 1334 029 217 5

1B L 796 005 059 5

2B L 806 012 144 5

6B L 814 018 219 5

7A L 789 009 112 5

9A L 781 024 306 5

10 L 802 020 245 5

11 L 784 018 225 5

12C L 794 021 263 5

16 L 850 014 168 5

17 L 774 016 203 5

18 L 787 015 187 5

19 L 787 015 187 5

20 L 769 014 188 5

21 L 808 008 097 5

24 L 792 010 128 5

25 L 751 030 400 5

1A R 767 005 068 5

2A R 727 008 109 5

3 R 779 008 099 5

4A R 748 011 146 5

4B R 758 013 172 5

5A R 782 011 144 5

5B R 766 017 216 5

6A R 773 009 117 5

7B R 716 011 160 5

8 R 754 010 127 5

9B R 755 008 107 5

12A R 755 006 078 5

12B R 771 008 102 5

13A R 740 017 225 5

13B R 769 007 091 5

14 R 761 011 140 5

15 R 750 018 246 5

22A R 757 008 110 5

22B R 759 007 088 5

23 R 732 009 117 5

1B L 4551 091 200 5

2B L 4391 078 178 5

6B L 3936 067 170 5

9A L 4471 060 134 5

10 L 4667 073 157 5

11 L 5068 136 269 5

12C L 4644 031 066 5

17 L 4346 106 243 5

19 L 4566 087 190 5

20 L 4616 122 265 5

21 L 5008 077 153 5

24 L 4782 094 196 5

25 L 4434 081 182 5

1A R 4168 016 039 5

2A R 4014 024 061 5

3 R 4247 035 083 5

4A R 4097 039 095 5

4B R 4181 064 153 5

5B R 3997 040 101 5

6A R 4076 074 181 5

8 R 4044 043 107 5

9B R 4097 033 080 5

12A R 4125 046 112 5

12B R 4257 039 092 5

15 R 3957 052 131 5

22A R 4046 028 069 5

22B R 4015 045 112 5

23 R 3830 073 192 5

1B L 1237 038 305 5

2B L 999 037 375 5

6B L 906 034 381 5

9A L 1147 043 373 5

10 L 1152 052 453 5

11 L 1488 053 356 5

12C L 1061 019 179 5

17 L 1027 028 274 5

19 L 1095 038 348 5

20 L 1216 083 681 5

21 L 1285 026 206 5

24 L 1235 060 484 5

25 L 1004 031 307 5

1A R 1024 014 138 5

2A R 797 016 197 5

3 R 974 031 317 5

4A R 911 034 368 5

4B R 931 027 287 5

5B R 815 041 507 5

6A R 923 038 411 5

8 R 929 033 354 5

9B R 927 028 301 5

12A R 1004 051 508 5

12B R 935 017 181 5

15 R 823 029 349 5

22A R 953 005 052 5

22B R 926 038 410 5

23 R 1598 065 404 5

1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Introduction 1

piece CM8

yields for the CM8

Organisation 2

21 Participants

LX-20 type 2 2

SM450 type 14 11

RM20A type 1 1

RM20D type 2 2

RM20H type 5 3

RM200 type 1 1

RM200A type 11 8

Total 36 28

Physical Parameter

WEIGHT 175

TPM 180 140

WATER 180 140

NIC 180 140

NFDPM 180 140

CO 180 140

PUFF 180 140

22 Protocol

Nicotine Free Dry

parameters

Smoking

Regime

Puff Volume

Puff Frequency

Puff Duration

Vent Blocking

ISO 35 60 2 0

Cerulean

Raw Data 3

1A R 96055 2731 0284 5

1B L 96519 3313 0343 5

2A R 94828 2622 0277 5

2B L 95000 5958 0627 5

3 R 90323 3183 0352 5

4A R 96060 2510 0261 5

4B R 96200 6481 0674 5

5A R 96494 1638 0170 5

5B R 95620 2978 0311 5

6A R 96612 4814 0498 5

6B L 96604 2688 0278 5

7A L 95598 3295 0345 5

7B R 95490 3365 0352 5

8 R 96653 2676 0277 5

9A L 95220 2564 0269 5

9B R 95900 2264 0236 5

10 L 96640 2595 0269 5

11 L 95968 8571 0893 5

12A R 95840 4930 0514 5

12B R 96226 2852 0296 5

12C L 95960 2702 0282 5

13A R 95806 2698 0282 5

13B R 95901 5717 0596 5

14 R 96102 3340 0348 5

15 R 95871 4505 0470 5

16 L 96286 4512 0469 5

17 L 95626 3166 0331 5

18 L 95285 3720 0390 5

19 L 95285 3720 0390 5

20 L 95767 5690 0594 5

22A R 96300 1414 0147 5

22B R 96240 1517 0158 5

23 R 94926 3700 0390 5

24 L 95591 5108 0534 5

25 L 96223 5979 0621 5

1B L 1793 024 132 5

2B L 1765 063 357 5

6B L 1574 061 387 5

7A L 1804 039 214 5

9A L 1698 033 197 5

10 L 1807 048 265 5

11 L 1828 045 248 5

12C L 1728 055 321 5

16 L 1742 010 058 5

17 L 1616 030 187 5

18 L 1772 036 205 5

19 L 1772 036 205 5

20 L 1783 040 224 5

21 L 1832 050 272 5

24 L 1791 033 185 5

25 L 1607 079 494 5

1A R 1749 024 135 5

2A R 1698 028 166 5

3 R 1760 019 107 5

4A R 1723 028 165 5

4B R 1769 038 212 5

5A R 1703 022 127 5

5B R 1724 031 178 5

6A R 1740 031 176 5

7B R 1646 017 103 5

8 R 1737 022 125 5

9B R 1711 025 147 5

12A R 1758 040 227 5

12B R 1790 014 078 5

13A R 1674 017 104 5

13B R 1700 020 115 5

14 R 1746 044 254 5

15 R 1719 041 238 5

22A R 1752 020 115 5

22B R 1731 022 129 5

23 R 1651 037 226 5

1B L 161 007 428 5

2B L 145 008 518 5

6B L 118 014 1213 5

7A L 175 006 364 5

9A L 142 011 802 5

10 L 177 010 581 5

11 L 142 009 632 5

12C L 122 008 645 5

16 L 142 012 872 5

17 L 145 026 1823 5

18 L 147 019 1299 5

19 L 147 019 1299 5

20 L 214 013 611 5

21 L 120 024 2024 5

24 L 156 009 551 5

25 L 127 016 1261 5

1A R 215 007 316 5

2A R 174 008 444 5

3 R 196 010 493 5

4A R 197 008 406 5

4B R 213 013 629 5

5A R 197 009 471 5

5B R 192 008 419 5

6A R 227 010 445 5

7B R 184 007 396 5

8 R 206 013 637 5

9B R 203 012 579 5

12A R 250 012 464 5

12B R 244 010 430 5

13A R 205 007 362 5

13B R 204 012 576 5

14 R 228 017 739 5

15 R 188 016 834 5

22A R 219 007 337 5

22B R 215 005 225 5

23 R 179 003 179 5

1B L 1704 0029 170 5

2B L 1706 0039 227 5

6B L 1624 0048 295 5

7A L 1687 0033 194 5

9A L 1612 0200 1240 5

10 L 1748 0070 401 5

11 L 1691 0028 166 5

12C L 1669 0034 206 5

16 L 1731 0028 159 5

17 L 1674 0046 276 5

18 L 1697 0014 082 5

19 L 1697 0014 082 5

20 L 1734 0021 124 5

21 L 1812 0048 266 5

24 L 1694 0037 217 5

25 L 1743 0154 883 5

1A R 1669 0023 141 5

2A R 1638 0037 224 5

3 R 1652 0018 110 5

4A R 1630 0042 255 5

4B R 1653 0035 214 5

5A R 1612 0023 142 5

5B R 1602 0023 141 5

6A R 1661 0037 225 5

7B R 1564 0022 140 5

8 R 1535 0031 204 5

9B R 1659 0047 285 5

12A R 1719 0024 142 5

12B R 1718 0037 216 5

13A R 1497 0024 163 5

13B R 1546 0013 086 5

14 R 1590 0035 217 5

15 R 1651 0030 181 5

22A R 1612 0011 068 5

22B R 1630 0012 075 5

23 R 1639 0026 159 5

1B L 1462 016 111 5

2B L 1449 053 366 5

6B L 1294 044 344 5

7A L 1460 031 214 5

9A L 1395 011 080 5

10 L 1455 039 269 5

11 L 1518 036 236 5

12C L 1439 049 338 5

16 L 1427 013 092 5

17 L 1304 054 413 5

18 L 1456 020 135 5

19 L 1456 020 135 5

20 L 1395 036 255 5

21 L 1531 057 371 5

24 L 1466 023 154 5

25 L 1306 066 509 5

1A R 1367 020 145 5

2A R 1361 023 169 5

3 R 1398 012 083 5

4A R 1363 024 176 5

4B R 1391 028 201 5

5A R 1347 014 107 5

5B R 1372 023 166 5

6A R 1346 019 142 5

7B R 1305 020 153 5

8 R 1378 026 192 5

9B R 1342 015 114 5

12A R 1337 037 278 5

12B R 1375 018 129 5

13A R 1319 015 112 5

13B R 1341 009 069 5

14 R 1359 028 204 5

15 R 1366 029 214 5

22A R 1371 019 136 5

22B R 1353 024 175 5

23 R 1308 037 283 5

1B L 1335 020 150 5

2B L 1297 037 288 5

6B L 1260 099 790 5

7A L 1374 034 249 5

9A L 1233 019 153 5

10 L 1219 054 445 5

11 L 1267 044 350 5

12C L 1325 033 248 5

16 L 1307 024 185 5

17 L 1196 029 242 5

18 L 1335 010 072 5

19 L 1335 010 072 5

20 L 1324 033 248 5

21 L 1363 032 238 5

24 L 1263 040 315 5

25 L 1194 069 574 5

1A R 1368 010 076 5

2A R 1308 018 135 5

3 R 1345 023 172 5

4A R 1340 011 079 5

4B R 1394 041 294 5

5A R 1292 028 216 5

5B R 1360 034 251 5

6A R 1372 023 166 5

7B R 1291 013 098 5

8 R 1369 025 183 5

9B R 1276 023 182 5

12A R 1317 034 256 5

12B R 1375 024 175 5

13A R 1334 021 155 5

13B R 1338 030 227 5

14 R 1366 023 167 5

15 R 1377 019 139 5

22A R 1344 016 118 5

22B R 1341 016 116 5

23 R 1334 029 217 5

1B L 796 005 059 5

2B L 806 012 144 5

6B L 814 018 219 5

7A L 789 009 112 5

9A L 781 024 306 5

10 L 802 020 245 5

11 L 784 018 225 5

12C L 794 021 263 5

16 L 850 014 168 5

17 L 774 016 203 5

18 L 787 015 187 5

19 L 787 015 187 5

20 L 769 014 188 5

21 L 808 008 097 5

24 L 792 010 128 5

25 L 751 030 400 5

1A R 767 005 068 5

2A R 727 008 109 5

3 R 779 008 099 5

4A R 748 011 146 5

4B R 758 013 172 5

5A R 782 011 144 5

5B R 766 017 216 5

6A R 773 009 117 5

7B R 716 011 160 5

8 R 754 010 127 5

9B R 755 008 107 5

12A R 755 006 078 5

12B R 771 008 102 5

13A R 740 017 225 5

13B R 769 007 091 5

14 R 761 011 140 5

15 R 750 018 246 5

22A R 757 008 110 5

22B R 759 007 088 5

23 R 732 009 117 5

1B L 4551 091 200 5

2B L 4391 078 178 5

6B L 3936 067 170 5

9A L 4471 060 134 5

10 L 4667 073 157 5

11 L 5068 136 269 5

12C L 4644 031 066 5

17 L 4346 106 243 5

19 L 4566 087 190 5

20 L 4616 122 265 5

21 L 5008 077 153 5

24 L 4782 094 196 5

25 L 4434 081 182 5

1A R 4168 016 039 5

2A R 4014 024 061 5

3 R 4247 035 083 5

4A R 4097 039 095 5

4B R 4181 064 153 5

5B R 3997 040 101 5

6A R 4076 074 181 5

8 R 4044 043 107 5

9B R 4097 033 080 5

12A R 4125 046 112 5

12B R 4257 039 092 5

15 R 3957 052 131 5

22A R 4046 028 069 5

22B R 4015 045 112 5

23 R 3830 073 192 5

1B L 1237 038 305 5

2B L 999 037 375 5

6B L 906 034 381 5

9A L 1147 043 373 5

10 L 1152 052 453 5

11 L 1488 053 356 5

12C L 1061 019 179 5

17 L 1027 028 274 5

19 L 1095 038 348 5

20 L 1216 083 681 5

21 L 1285 026 206 5

24 L 1235 060 484 5

25 L 1004 031 307 5

1A R 1024 014 138 5

2A R 797 016 197 5

3 R 974 031 317 5

4A R 911 034 368 5

4B R 931 027 287 5

5B R 815 041 507 5

6A R 923 038 411 5

8 R 929 033 354 5

9B R 927 028 301 5

12A R 1004 051 508 5

12B R 935 017 181 5

15 R 823 029 349 5

22A R 953 005 052 5

22B R 926 038 410 5

23 R 1598 065 404 5

1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Physical Parameter

WEIGHT 175

TPM 180 140

WATER 180 140

NIC 180 140

NFDPM 180 140

CO 180 140

PUFF 180 140

22 Protocol

Nicotine Free Dry

parameters

Smoking

Regime

Puff Volume

Puff Frequency

Puff Duration

Vent Blocking

ISO 35 60 2 0

Cerulean

Raw Data 3

1A R 96055 2731 0284 5

1B L 96519 3313 0343 5

2A R 94828 2622 0277 5

2B L 95000 5958 0627 5

3 R 90323 3183 0352 5

4A R 96060 2510 0261 5

4B R 96200 6481 0674 5

5A R 96494 1638 0170 5

5B R 95620 2978 0311 5

6A R 96612 4814 0498 5

6B L 96604 2688 0278 5

7A L 95598 3295 0345 5

7B R 95490 3365 0352 5

8 R 96653 2676 0277 5

9A L 95220 2564 0269 5

9B R 95900 2264 0236 5

10 L 96640 2595 0269 5

11 L 95968 8571 0893 5

12A R 95840 4930 0514 5

12B R 96226 2852 0296 5

12C L 95960 2702 0282 5

13A R 95806 2698 0282 5

13B R 95901 5717 0596 5

14 R 96102 3340 0348 5

15 R 95871 4505 0470 5

16 L 96286 4512 0469 5

17 L 95626 3166 0331 5

18 L 95285 3720 0390 5

19 L 95285 3720 0390 5

20 L 95767 5690 0594 5

22A R 96300 1414 0147 5

22B R 96240 1517 0158 5

23 R 94926 3700 0390 5

24 L 95591 5108 0534 5

25 L 96223 5979 0621 5

1B L 1793 024 132 5

2B L 1765 063 357 5

6B L 1574 061 387 5

7A L 1804 039 214 5

9A L 1698 033 197 5

10 L 1807 048 265 5

11 L 1828 045 248 5

12C L 1728 055 321 5

16 L 1742 010 058 5

17 L 1616 030 187 5

18 L 1772 036 205 5

19 L 1772 036 205 5

20 L 1783 040 224 5

21 L 1832 050 272 5

24 L 1791 033 185 5

25 L 1607 079 494 5

1A R 1749 024 135 5

2A R 1698 028 166 5

3 R 1760 019 107 5

4A R 1723 028 165 5

4B R 1769 038 212 5

5A R 1703 022 127 5

5B R 1724 031 178 5

6A R 1740 031 176 5

7B R 1646 017 103 5

8 R 1737 022 125 5

9B R 1711 025 147 5

12A R 1758 040 227 5

12B R 1790 014 078 5

13A R 1674 017 104 5

13B R 1700 020 115 5

14 R 1746 044 254 5

15 R 1719 041 238 5

22A R 1752 020 115 5

22B R 1731 022 129 5

23 R 1651 037 226 5

1B L 161 007 428 5

2B L 145 008 518 5

6B L 118 014 1213 5

7A L 175 006 364 5

9A L 142 011 802 5

10 L 177 010 581 5

11 L 142 009 632 5

12C L 122 008 645 5

16 L 142 012 872 5

17 L 145 026 1823 5

18 L 147 019 1299 5

19 L 147 019 1299 5

20 L 214 013 611 5

21 L 120 024 2024 5

24 L 156 009 551 5

25 L 127 016 1261 5

1A R 215 007 316 5

2A R 174 008 444 5

3 R 196 010 493 5

4A R 197 008 406 5

4B R 213 013 629 5

5A R 197 009 471 5

5B R 192 008 419 5

6A R 227 010 445 5

7B R 184 007 396 5

8 R 206 013 637 5

9B R 203 012 579 5

12A R 250 012 464 5

12B R 244 010 430 5

13A R 205 007 362 5

13B R 204 012 576 5

14 R 228 017 739 5

15 R 188 016 834 5

22A R 219 007 337 5

22B R 215 005 225 5

23 R 179 003 179 5

1B L 1704 0029 170 5

2B L 1706 0039 227 5

6B L 1624 0048 295 5

7A L 1687 0033 194 5

9A L 1612 0200 1240 5

10 L 1748 0070 401 5

11 L 1691 0028 166 5

12C L 1669 0034 206 5

16 L 1731 0028 159 5

17 L 1674 0046 276 5

18 L 1697 0014 082 5

19 L 1697 0014 082 5

20 L 1734 0021 124 5

21 L 1812 0048 266 5

24 L 1694 0037 217 5

25 L 1743 0154 883 5

1A R 1669 0023 141 5

2A R 1638 0037 224 5

3 R 1652 0018 110 5

4A R 1630 0042 255 5

4B R 1653 0035 214 5

5A R 1612 0023 142 5

5B R 1602 0023 141 5

6A R 1661 0037 225 5

7B R 1564 0022 140 5

8 R 1535 0031 204 5

9B R 1659 0047 285 5

12A R 1719 0024 142 5

12B R 1718 0037 216 5

13A R 1497 0024 163 5

13B R 1546 0013 086 5

14 R 1590 0035 217 5

15 R 1651 0030 181 5

22A R 1612 0011 068 5

22B R 1630 0012 075 5

23 R 1639 0026 159 5

1B L 1462 016 111 5

2B L 1449 053 366 5

6B L 1294 044 344 5

7A L 1460 031 214 5

9A L 1395 011 080 5

10 L 1455 039 269 5

11 L 1518 036 236 5

12C L 1439 049 338 5

16 L 1427 013 092 5

17 L 1304 054 413 5

18 L 1456 020 135 5

19 L 1456 020 135 5

20 L 1395 036 255 5

21 L 1531 057 371 5

24 L 1466 023 154 5

25 L 1306 066 509 5

1A R 1367 020 145 5

2A R 1361 023 169 5

3 R 1398 012 083 5

4A R 1363 024 176 5

4B R 1391 028 201 5

5A R 1347 014 107 5

5B R 1372 023 166 5

6A R 1346 019 142 5

7B R 1305 020 153 5

8 R 1378 026 192 5

9B R 1342 015 114 5

12A R 1337 037 278 5

12B R 1375 018 129 5

13A R 1319 015 112 5

13B R 1341 009 069 5

14 R 1359 028 204 5

15 R 1366 029 214 5

22A R 1371 019 136 5

22B R 1353 024 175 5

23 R 1308 037 283 5

1B L 1335 020 150 5

2B L 1297 037 288 5

6B L 1260 099 790 5

7A L 1374 034 249 5

9A L 1233 019 153 5

10 L 1219 054 445 5

11 L 1267 044 350 5

12C L 1325 033 248 5

16 L 1307 024 185 5

17 L 1196 029 242 5

18 L 1335 010 072 5

19 L 1335 010 072 5

20 L 1324 033 248 5

21 L 1363 032 238 5

24 L 1263 040 315 5

25 L 1194 069 574 5

1A R 1368 010 076 5

2A R 1308 018 135 5

3 R 1345 023 172 5

4A R 1340 011 079 5

4B R 1394 041 294 5

5A R 1292 028 216 5

5B R 1360 034 251 5

6A R 1372 023 166 5

7B R 1291 013 098 5

8 R 1369 025 183 5

9B R 1276 023 182 5

12A R 1317 034 256 5

12B R 1375 024 175 5

13A R 1334 021 155 5

13B R 1338 030 227 5

14 R 1366 023 167 5

15 R 1377 019 139 5

22A R 1344 016 118 5

22B R 1341 016 116 5

23 R 1334 029 217 5

1B L 796 005 059 5

2B L 806 012 144 5

6B L 814 018 219 5

7A L 789 009 112 5

9A L 781 024 306 5

10 L 802 020 245 5

11 L 784 018 225 5

12C L 794 021 263 5

16 L 850 014 168 5

17 L 774 016 203 5

18 L 787 015 187 5

19 L 787 015 187 5

20 L 769 014 188 5

21 L 808 008 097 5

24 L 792 010 128 5

25 L 751 030 400 5

1A R 767 005 068 5

2A R 727 008 109 5

3 R 779 008 099 5

4A R 748 011 146 5

4B R 758 013 172 5

5A R 782 011 144 5

5B R 766 017 216 5

6A R 773 009 117 5

7B R 716 011 160 5

8 R 754 010 127 5

9B R 755 008 107 5

12A R 755 006 078 5

12B R 771 008 102 5

13A R 740 017 225 5

13B R 769 007 091 5

14 R 761 011 140 5

15 R 750 018 246 5

22A R 757 008 110 5

22B R 759 007 088 5

23 R 732 009 117 5

1B L 4551 091 200 5

2B L 4391 078 178 5

6B L 3936 067 170 5

9A L 4471 060 134 5

10 L 4667 073 157 5

11 L 5068 136 269 5

12C L 4644 031 066 5

17 L 4346 106 243 5

19 L 4566 087 190 5

20 L 4616 122 265 5

21 L 5008 077 153 5

24 L 4782 094 196 5

25 L 4434 081 182 5

1A R 4168 016 039 5

2A R 4014 024 061 5

3 R 4247 035 083 5

4A R 4097 039 095 5

4B R 4181 064 153 5

5B R 3997 040 101 5

6A R 4076 074 181 5

8 R 4044 043 107 5

9B R 4097 033 080 5

12A R 4125 046 112 5

12B R 4257 039 092 5

15 R 3957 052 131 5

22A R 4046 028 069 5

22B R 4015 045 112 5

23 R 3830 073 192 5

1B L 1237 038 305 5

2B L 999 037 375 5

6B L 906 034 381 5

9A L 1147 043 373 5

10 L 1152 052 453 5

11 L 1488 053 356 5

12C L 1061 019 179 5

17 L 1027 028 274 5

19 L 1095 038 348 5

20 L 1216 083 681 5

21 L 1285 026 206 5

24 L 1235 060 484 5

25 L 1004 031 307 5

1A R 1024 014 138 5

2A R 797 016 197 5

3 R 974 031 317 5

4A R 911 034 368 5

4B R 931 027 287 5

5B R 815 041 507 5

6A R 923 038 411 5

8 R 929 033 354 5

9B R 927 028 301 5

12A R 1004 051 508 5

12B R 935 017 181 5

15 R 823 029 349 5

22A R 953 005 052 5

22B R 926 038 410 5

23 R 1598 065 404 5

1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










parameters

Smoking

Regime

Puff Volume

Puff Frequency

Puff Duration

Vent Blocking

ISO 35 60 2 0

Cerulean

Raw Data 3

1A R 96055 2731 0284 5

1B L 96519 3313 0343 5

2A R 94828 2622 0277 5

2B L 95000 5958 0627 5

3 R 90323 3183 0352 5

4A R 96060 2510 0261 5

4B R 96200 6481 0674 5

5A R 96494 1638 0170 5

5B R 95620 2978 0311 5

6A R 96612 4814 0498 5

6B L 96604 2688 0278 5

7A L 95598 3295 0345 5

7B R 95490 3365 0352 5

8 R 96653 2676 0277 5

9A L 95220 2564 0269 5

9B R 95900 2264 0236 5

10 L 96640 2595 0269 5

11 L 95968 8571 0893 5

12A R 95840 4930 0514 5

12B R 96226 2852 0296 5

12C L 95960 2702 0282 5

13A R 95806 2698 0282 5

13B R 95901 5717 0596 5

14 R 96102 3340 0348 5

15 R 95871 4505 0470 5

16 L 96286 4512 0469 5

17 L 95626 3166 0331 5

18 L 95285 3720 0390 5

19 L 95285 3720 0390 5

20 L 95767 5690 0594 5

22A R 96300 1414 0147 5

22B R 96240 1517 0158 5

23 R 94926 3700 0390 5

24 L 95591 5108 0534 5

25 L 96223 5979 0621 5

1B L 1793 024 132 5

2B L 1765 063 357 5

6B L 1574 061 387 5

7A L 1804 039 214 5

9A L 1698 033 197 5

10 L 1807 048 265 5

11 L 1828 045 248 5

12C L 1728 055 321 5

16 L 1742 010 058 5

17 L 1616 030 187 5

18 L 1772 036 205 5

19 L 1772 036 205 5

20 L 1783 040 224 5

21 L 1832 050 272 5

24 L 1791 033 185 5

25 L 1607 079 494 5

1A R 1749 024 135 5

2A R 1698 028 166 5

3 R 1760 019 107 5

4A R 1723 028 165 5

4B R 1769 038 212 5

5A R 1703 022 127 5

5B R 1724 031 178 5

6A R 1740 031 176 5

7B R 1646 017 103 5

8 R 1737 022 125 5

9B R 1711 025 147 5

12A R 1758 040 227 5

12B R 1790 014 078 5

13A R 1674 017 104 5

13B R 1700 020 115 5

14 R 1746 044 254 5

15 R 1719 041 238 5

22A R 1752 020 115 5

22B R 1731 022 129 5

23 R 1651 037 226 5

1B L 161 007 428 5

2B L 145 008 518 5

6B L 118 014 1213 5

7A L 175 006 364 5

9A L 142 011 802 5

10 L 177 010 581 5

11 L 142 009 632 5

12C L 122 008 645 5

16 L 142 012 872 5

17 L 145 026 1823 5

18 L 147 019 1299 5

19 L 147 019 1299 5

20 L 214 013 611 5

21 L 120 024 2024 5

24 L 156 009 551 5

25 L 127 016 1261 5

1A R 215 007 316 5

2A R 174 008 444 5

3 R 196 010 493 5

4A R 197 008 406 5

4B R 213 013 629 5

5A R 197 009 471 5

5B R 192 008 419 5

6A R 227 010 445 5

7B R 184 007 396 5

8 R 206 013 637 5

9B R 203 012 579 5

12A R 250 012 464 5

12B R 244 010 430 5

13A R 205 007 362 5

13B R 204 012 576 5

14 R 228 017 739 5

15 R 188 016 834 5

22A R 219 007 337 5

22B R 215 005 225 5

23 R 179 003 179 5

1B L 1704 0029 170 5

2B L 1706 0039 227 5

6B L 1624 0048 295 5

7A L 1687 0033 194 5

9A L 1612 0200 1240 5

10 L 1748 0070 401 5

11 L 1691 0028 166 5

12C L 1669 0034 206 5

16 L 1731 0028 159 5

17 L 1674 0046 276 5

18 L 1697 0014 082 5

19 L 1697 0014 082 5

20 L 1734 0021 124 5

21 L 1812 0048 266 5

24 L 1694 0037 217 5

25 L 1743 0154 883 5

1A R 1669 0023 141 5

2A R 1638 0037 224 5

3 R 1652 0018 110 5

4A R 1630 0042 255 5

4B R 1653 0035 214 5

5A R 1612 0023 142 5

5B R 1602 0023 141 5

6A R 1661 0037 225 5

7B R 1564 0022 140 5

8 R 1535 0031 204 5

9B R 1659 0047 285 5

12A R 1719 0024 142 5

12B R 1718 0037 216 5

13A R 1497 0024 163 5

13B R 1546 0013 086 5

14 R 1590 0035 217 5

15 R 1651 0030 181 5

22A R 1612 0011 068 5

22B R 1630 0012 075 5

23 R 1639 0026 159 5

1B L 1462 016 111 5

2B L 1449 053 366 5

6B L 1294 044 344 5

7A L 1460 031 214 5

9A L 1395 011 080 5

10 L 1455 039 269 5

11 L 1518 036 236 5

12C L 1439 049 338 5

16 L 1427 013 092 5

17 L 1304 054 413 5

18 L 1456 020 135 5

19 L 1456 020 135 5

20 L 1395 036 255 5

21 L 1531 057 371 5

24 L 1466 023 154 5

25 L 1306 066 509 5

1A R 1367 020 145 5

2A R 1361 023 169 5

3 R 1398 012 083 5

4A R 1363 024 176 5

4B R 1391 028 201 5

5A R 1347 014 107 5

5B R 1372 023 166 5

6A R 1346 019 142 5

7B R 1305 020 153 5

8 R 1378 026 192 5

9B R 1342 015 114 5

12A R 1337 037 278 5

12B R 1375 018 129 5

13A R 1319 015 112 5

13B R 1341 009 069 5

14 R 1359 028 204 5

15 R 1366 029 214 5

22A R 1371 019 136 5

22B R 1353 024 175 5

23 R 1308 037 283 5

1B L 1335 020 150 5

2B L 1297 037 288 5

6B L 1260 099 790 5

7A L 1374 034 249 5

9A L 1233 019 153 5

10 L 1219 054 445 5

11 L 1267 044 350 5

12C L 1325 033 248 5

16 L 1307 024 185 5

17 L 1196 029 242 5

18 L 1335 010 072 5

19 L 1335 010 072 5

20 L 1324 033 248 5

21 L 1363 032 238 5

24 L 1263 040 315 5

25 L 1194 069 574 5

1A R 1368 010 076 5

2A R 1308 018 135 5

3 R 1345 023 172 5

4A R 1340 011 079 5

4B R 1394 041 294 5

5A R 1292 028 216 5

5B R 1360 034 251 5

6A R 1372 023 166 5

7B R 1291 013 098 5

8 R 1369 025 183 5

9B R 1276 023 182 5

12A R 1317 034 256 5

12B R 1375 024 175 5

13A R 1334 021 155 5

13B R 1338 030 227 5

14 R 1366 023 167 5

15 R 1377 019 139 5

22A R 1344 016 118 5

22B R 1341 016 116 5

23 R 1334 029 217 5

1B L 796 005 059 5

2B L 806 012 144 5

6B L 814 018 219 5

7A L 789 009 112 5

9A L 781 024 306 5

10 L 802 020 245 5

11 L 784 018 225 5

12C L 794 021 263 5

16 L 850 014 168 5

17 L 774 016 203 5

18 L 787 015 187 5

19 L 787 015 187 5

20 L 769 014 188 5

21 L 808 008 097 5

24 L 792 010 128 5

25 L 751 030 400 5

1A R 767 005 068 5

2A R 727 008 109 5

3 R 779 008 099 5

4A R 748 011 146 5

4B R 758 013 172 5

5A R 782 011 144 5

5B R 766 017 216 5

6A R 773 009 117 5

7B R 716 011 160 5

8 R 754 010 127 5

9B R 755 008 107 5

12A R 755 006 078 5

12B R 771 008 102 5

13A R 740 017 225 5

13B R 769 007 091 5

14 R 761 011 140 5

15 R 750 018 246 5

22A R 757 008 110 5

22B R 759 007 088 5

23 R 732 009 117 5

1B L 4551 091 200 5

2B L 4391 078 178 5

6B L 3936 067 170 5

9A L 4471 060 134 5

10 L 4667 073 157 5

11 L 5068 136 269 5

12C L 4644 031 066 5

17 L 4346 106 243 5

19 L 4566 087 190 5

20 L 4616 122 265 5

21 L 5008 077 153 5

24 L 4782 094 196 5

25 L 4434 081 182 5

1A R 4168 016 039 5

2A R 4014 024 061 5

3 R 4247 035 083 5

4A R 4097 039 095 5

4B R 4181 064 153 5

5B R 3997 040 101 5

6A R 4076 074 181 5

8 R 4044 043 107 5

9B R 4097 033 080 5

12A R 4125 046 112 5

12B R 4257 039 092 5

15 R 3957 052 131 5

22A R 4046 028 069 5

22B R 4015 045 112 5

23 R 3830 073 192 5

1B L 1237 038 305 5

2B L 999 037 375 5

6B L 906 034 381 5

9A L 1147 043 373 5

10 L 1152 052 453 5

11 L 1488 053 356 5

12C L 1061 019 179 5

17 L 1027 028 274 5

19 L 1095 038 348 5

20 L 1216 083 681 5

21 L 1285 026 206 5

24 L 1235 060 484 5

25 L 1004 031 307 5

1A R 1024 014 138 5

2A R 797 016 197 5

3 R 974 031 317 5

4A R 911 034 368 5

4B R 931 027 287 5

5B R 815 041 507 5

6A R 923 038 411 5

8 R 929 033 354 5

9B R 927 028 301 5

12A R 1004 051 508 5

12B R 935 017 181 5

15 R 823 029 349 5

22A R 953 005 052 5

22B R 926 038 410 5

23 R 1598 065 404 5

1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1A R 96055 2731 0284 5

1B L 96519 3313 0343 5

2A R 94828 2622 0277 5

2B L 95000 5958 0627 5

3 R 90323 3183 0352 5

4A R 96060 2510 0261 5

4B R 96200 6481 0674 5

5A R 96494 1638 0170 5

5B R 95620 2978 0311 5

6A R 96612 4814 0498 5

6B L 96604 2688 0278 5

7A L 95598 3295 0345 5

7B R 95490 3365 0352 5

8 R 96653 2676 0277 5

9A L 95220 2564 0269 5

9B R 95900 2264 0236 5

10 L 96640 2595 0269 5

11 L 95968 8571 0893 5

12A R 95840 4930 0514 5

12B R 96226 2852 0296 5

12C L 95960 2702 0282 5

13A R 95806 2698 0282 5

13B R 95901 5717 0596 5

14 R 96102 3340 0348 5

15 R 95871 4505 0470 5

16 L 96286 4512 0469 5

17 L 95626 3166 0331 5

18 L 95285 3720 0390 5

19 L 95285 3720 0390 5

20 L 95767 5690 0594 5

22A R 96300 1414 0147 5

22B R 96240 1517 0158 5

23 R 94926 3700 0390 5

24 L 95591 5108 0534 5

25 L 96223 5979 0621 5

1B L 1793 024 132 5

2B L 1765 063 357 5

6B L 1574 061 387 5

7A L 1804 039 214 5

9A L 1698 033 197 5

10 L 1807 048 265 5

11 L 1828 045 248 5

12C L 1728 055 321 5

16 L 1742 010 058 5

17 L 1616 030 187 5

18 L 1772 036 205 5

19 L 1772 036 205 5

20 L 1783 040 224 5

21 L 1832 050 272 5

24 L 1791 033 185 5

25 L 1607 079 494 5

1A R 1749 024 135 5

2A R 1698 028 166 5

3 R 1760 019 107 5

4A R 1723 028 165 5

4B R 1769 038 212 5

5A R 1703 022 127 5

5B R 1724 031 178 5

6A R 1740 031 176 5

7B R 1646 017 103 5

8 R 1737 022 125 5

9B R 1711 025 147 5

12A R 1758 040 227 5

12B R 1790 014 078 5

13A R 1674 017 104 5

13B R 1700 020 115 5

14 R 1746 044 254 5

15 R 1719 041 238 5

22A R 1752 020 115 5

22B R 1731 022 129 5

23 R 1651 037 226 5

1B L 161 007 428 5

2B L 145 008 518 5

6B L 118 014 1213 5

7A L 175 006 364 5

9A L 142 011 802 5

10 L 177 010 581 5

11 L 142 009 632 5

12C L 122 008 645 5

16 L 142 012 872 5

17 L 145 026 1823 5

18 L 147 019 1299 5

19 L 147 019 1299 5

20 L 214 013 611 5

21 L 120 024 2024 5

24 L 156 009 551 5

25 L 127 016 1261 5

1A R 215 007 316 5

2A R 174 008 444 5

3 R 196 010 493 5

4A R 197 008 406 5

4B R 213 013 629 5

5A R 197 009 471 5

5B R 192 008 419 5

6A R 227 010 445 5

7B R 184 007 396 5

8 R 206 013 637 5

9B R 203 012 579 5

12A R 250 012 464 5

12B R 244 010 430 5

13A R 205 007 362 5

13B R 204 012 576 5

14 R 228 017 739 5

15 R 188 016 834 5

22A R 219 007 337 5

22B R 215 005 225 5

23 R 179 003 179 5

1B L 1704 0029 170 5

2B L 1706 0039 227 5

6B L 1624 0048 295 5

7A L 1687 0033 194 5

9A L 1612 0200 1240 5

10 L 1748 0070 401 5

11 L 1691 0028 166 5

12C L 1669 0034 206 5

16 L 1731 0028 159 5

17 L 1674 0046 276 5

18 L 1697 0014 082 5

19 L 1697 0014 082 5

20 L 1734 0021 124 5

21 L 1812 0048 266 5

24 L 1694 0037 217 5

25 L 1743 0154 883 5

1A R 1669 0023 141 5

2A R 1638 0037 224 5

3 R 1652 0018 110 5

4A R 1630 0042 255 5

4B R 1653 0035 214 5

5A R 1612 0023 142 5

5B R 1602 0023 141 5

6A R 1661 0037 225 5

7B R 1564 0022 140 5

8 R 1535 0031 204 5

9B R 1659 0047 285 5

12A R 1719 0024 142 5

12B R 1718 0037 216 5

13A R 1497 0024 163 5

13B R 1546 0013 086 5

14 R 1590 0035 217 5

15 R 1651 0030 181 5

22A R 1612 0011 068 5

22B R 1630 0012 075 5

23 R 1639 0026 159 5

1B L 1462 016 111 5

2B L 1449 053 366 5

6B L 1294 044 344 5

7A L 1460 031 214 5

9A L 1395 011 080 5

10 L 1455 039 269 5

11 L 1518 036 236 5

12C L 1439 049 338 5

16 L 1427 013 092 5

17 L 1304 054 413 5

18 L 1456 020 135 5

19 L 1456 020 135 5

20 L 1395 036 255 5

21 L 1531 057 371 5

24 L 1466 023 154 5

25 L 1306 066 509 5

1A R 1367 020 145 5

2A R 1361 023 169 5

3 R 1398 012 083 5

4A R 1363 024 176 5

4B R 1391 028 201 5

5A R 1347 014 107 5

5B R 1372 023 166 5

6A R 1346 019 142 5

7B R 1305 020 153 5

8 R 1378 026 192 5

9B R 1342 015 114 5

12A R 1337 037 278 5

12B R 1375 018 129 5

13A R 1319 015 112 5

13B R 1341 009 069 5

14 R 1359 028 204 5

15 R 1366 029 214 5

22A R 1371 019 136 5

22B R 1353 024 175 5

23 R 1308 037 283 5

1B L 1335 020 150 5

2B L 1297 037 288 5

6B L 1260 099 790 5

7A L 1374 034 249 5

9A L 1233 019 153 5

10 L 1219 054 445 5

11 L 1267 044 350 5

12C L 1325 033 248 5

16 L 1307 024 185 5

17 L 1196 029 242 5

18 L 1335 010 072 5

19 L 1335 010 072 5

20 L 1324 033 248 5

21 L 1363 032 238 5

24 L 1263 040 315 5

25 L 1194 069 574 5

1A R 1368 010 076 5

2A R 1308 018 135 5

3 R 1345 023 172 5

4A R 1340 011 079 5

4B R 1394 041 294 5

5A R 1292 028 216 5

5B R 1360 034 251 5

6A R 1372 023 166 5

7B R 1291 013 098 5

8 R 1369 025 183 5

9B R 1276 023 182 5

12A R 1317 034 256 5

12B R 1375 024 175 5

13A R 1334 021 155 5

13B R 1338 030 227 5

14 R 1366 023 167 5

15 R 1377 019 139 5

22A R 1344 016 118 5

22B R 1341 016 116 5

23 R 1334 029 217 5

1B L 796 005 059 5

2B L 806 012 144 5

6B L 814 018 219 5

7A L 789 009 112 5

9A L 781 024 306 5

10 L 802 020 245 5

11 L 784 018 225 5

12C L 794 021 263 5

16 L 850 014 168 5

17 L 774 016 203 5

18 L 787 015 187 5

19 L 787 015 187 5

20 L 769 014 188 5

21 L 808 008 097 5

24 L 792 010 128 5

25 L 751 030 400 5

1A R 767 005 068 5

2A R 727 008 109 5

3 R 779 008 099 5

4A R 748 011 146 5

4B R 758 013 172 5

5A R 782 011 144 5

5B R 766 017 216 5

6A R 773 009 117 5

7B R 716 011 160 5

8 R 754 010 127 5

9B R 755 008 107 5

12A R 755 006 078 5

12B R 771 008 102 5

13A R 740 017 225 5

13B R 769 007 091 5

14 R 761 011 140 5

15 R 750 018 246 5

22A R 757 008 110 5

22B R 759 007 088 5

23 R 732 009 117 5

1B L 4551 091 200 5

2B L 4391 078 178 5

6B L 3936 067 170 5

9A L 4471 060 134 5

10 L 4667 073 157 5

11 L 5068 136 269 5

12C L 4644 031 066 5

17 L 4346 106 243 5

19 L 4566 087 190 5

20 L 4616 122 265 5

21 L 5008 077 153 5

24 L 4782 094 196 5

25 L 4434 081 182 5

1A R 4168 016 039 5

2A R 4014 024 061 5

3 R 4247 035 083 5

4A R 4097 039 095 5

4B R 4181 064 153 5

5B R 3997 040 101 5

6A R 4076 074 181 5

8 R 4044 043 107 5

9B R 4097 033 080 5

12A R 4125 046 112 5

12B R 4257 039 092 5

15 R 3957 052 131 5

22A R 4046 028 069 5

22B R 4015 045 112 5

23 R 3830 073 192 5

1B L 1237 038 305 5

2B L 999 037 375 5

6B L 906 034 381 5

9A L 1147 043 373 5

10 L 1152 052 453 5

11 L 1488 053 356 5

12C L 1061 019 179 5

17 L 1027 028 274 5

19 L 1095 038 348 5

20 L 1216 083 681 5

21 L 1285 026 206 5

24 L 1235 060 484 5

25 L 1004 031 307 5

1A R 1024 014 138 5

2A R 797 016 197 5

3 R 974 031 317 5

4A R 911 034 368 5

4B R 931 027 287 5

5B R 815 041 507 5

6A R 923 038 411 5

8 R 929 033 354 5

9B R 927 028 301 5

12A R 1004 051 508 5

12B R 935 017 181 5

15 R 823 029 349 5

22A R 953 005 052 5

22B R 926 038 410 5

23 R 1598 065 404 5

1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1B L 1793 024 132 5

2B L 1765 063 357 5

6B L 1574 061 387 5

7A L 1804 039 214 5

9A L 1698 033 197 5

10 L 1807 048 265 5

11 L 1828 045 248 5

12C L 1728 055 321 5

16 L 1742 010 058 5

17 L 1616 030 187 5

18 L 1772 036 205 5

19 L 1772 036 205 5

20 L 1783 040 224 5

21 L 1832 050 272 5

24 L 1791 033 185 5

25 L 1607 079 494 5

1A R 1749 024 135 5

2A R 1698 028 166 5

3 R 1760 019 107 5

4A R 1723 028 165 5

4B R 1769 038 212 5

5A R 1703 022 127 5

5B R 1724 031 178 5

6A R 1740 031 176 5

7B R 1646 017 103 5

8 R 1737 022 125 5

9B R 1711 025 147 5

12A R 1758 040 227 5

12B R 1790 014 078 5

13A R 1674 017 104 5

13B R 1700 020 115 5

14 R 1746 044 254 5

15 R 1719 041 238 5

22A R 1752 020 115 5

22B R 1731 022 129 5

23 R 1651 037 226 5

1B L 161 007 428 5

2B L 145 008 518 5

6B L 118 014 1213 5

7A L 175 006 364 5

9A L 142 011 802 5

10 L 177 010 581 5

11 L 142 009 632 5

12C L 122 008 645 5

16 L 142 012 872 5

17 L 145 026 1823 5

18 L 147 019 1299 5

19 L 147 019 1299 5

20 L 214 013 611 5

21 L 120 024 2024 5

24 L 156 009 551 5

25 L 127 016 1261 5

1A R 215 007 316 5

2A R 174 008 444 5

3 R 196 010 493 5

4A R 197 008 406 5

4B R 213 013 629 5

5A R 197 009 471 5

5B R 192 008 419 5

6A R 227 010 445 5

7B R 184 007 396 5

8 R 206 013 637 5

9B R 203 012 579 5

12A R 250 012 464 5

12B R 244 010 430 5

13A R 205 007 362 5

13B R 204 012 576 5

14 R 228 017 739 5

15 R 188 016 834 5

22A R 219 007 337 5

22B R 215 005 225 5

23 R 179 003 179 5

1B L 1704 0029 170 5

2B L 1706 0039 227 5

6B L 1624 0048 295 5

7A L 1687 0033 194 5

9A L 1612 0200 1240 5

10 L 1748 0070 401 5

11 L 1691 0028 166 5

12C L 1669 0034 206 5

16 L 1731 0028 159 5

17 L 1674 0046 276 5

18 L 1697 0014 082 5

19 L 1697 0014 082 5

20 L 1734 0021 124 5

21 L 1812 0048 266 5

24 L 1694 0037 217 5

25 L 1743 0154 883 5

1A R 1669 0023 141 5

2A R 1638 0037 224 5

3 R 1652 0018 110 5

4A R 1630 0042 255 5

4B R 1653 0035 214 5

5A R 1612 0023 142 5

5B R 1602 0023 141 5

6A R 1661 0037 225 5

7B R 1564 0022 140 5

8 R 1535 0031 204 5

9B R 1659 0047 285 5

12A R 1719 0024 142 5

12B R 1718 0037 216 5

13A R 1497 0024 163 5

13B R 1546 0013 086 5

14 R 1590 0035 217 5

15 R 1651 0030 181 5

22A R 1612 0011 068 5

22B R 1630 0012 075 5

23 R 1639 0026 159 5

1B L 1462 016 111 5

2B L 1449 053 366 5

6B L 1294 044 344 5

7A L 1460 031 214 5

9A L 1395 011 080 5

10 L 1455 039 269 5

11 L 1518 036 236 5

12C L 1439 049 338 5

16 L 1427 013 092 5

17 L 1304 054 413 5

18 L 1456 020 135 5

19 L 1456 020 135 5

20 L 1395 036 255 5

21 L 1531 057 371 5

24 L 1466 023 154 5

25 L 1306 066 509 5

1A R 1367 020 145 5

2A R 1361 023 169 5

3 R 1398 012 083 5

4A R 1363 024 176 5

4B R 1391 028 201 5

5A R 1347 014 107 5

5B R 1372 023 166 5

6A R 1346 019 142 5

7B R 1305 020 153 5

8 R 1378 026 192 5

9B R 1342 015 114 5

12A R 1337 037 278 5

12B R 1375 018 129 5

13A R 1319 015 112 5

13B R 1341 009 069 5

14 R 1359 028 204 5

15 R 1366 029 214 5

22A R 1371 019 136 5

22B R 1353 024 175 5

23 R 1308 037 283 5

1B L 1335 020 150 5

2B L 1297 037 288 5

6B L 1260 099 790 5

7A L 1374 034 249 5

9A L 1233 019 153 5

10 L 1219 054 445 5

11 L 1267 044 350 5

12C L 1325 033 248 5

16 L 1307 024 185 5

17 L 1196 029 242 5

18 L 1335 010 072 5

19 L 1335 010 072 5

20 L 1324 033 248 5

21 L 1363 032 238 5

24 L 1263 040 315 5

25 L 1194 069 574 5

1A R 1368 010 076 5

2A R 1308 018 135 5

3 R 1345 023 172 5

4A R 1340 011 079 5

4B R 1394 041 294 5

5A R 1292 028 216 5

5B R 1360 034 251 5

6A R 1372 023 166 5

7B R 1291 013 098 5

8 R 1369 025 183 5

9B R 1276 023 182 5

12A R 1317 034 256 5

12B R 1375 024 175 5

13A R 1334 021 155 5

13B R 1338 030 227 5

14 R 1366 023 167 5

15 R 1377 019 139 5

22A R 1344 016 118 5

22B R 1341 016 116 5

23 R 1334 029 217 5

1B L 796 005 059 5

2B L 806 012 144 5

6B L 814 018 219 5

7A L 789 009 112 5

9A L 781 024 306 5

10 L 802 020 245 5

11 L 784 018 225 5

12C L 794 021 263 5

16 L 850 014 168 5

17 L 774 016 203 5

18 L 787 015 187 5

19 L 787 015 187 5

20 L 769 014 188 5

21 L 808 008 097 5

24 L 792 010 128 5

25 L 751 030 400 5

1A R 767 005 068 5

2A R 727 008 109 5

3 R 779 008 099 5

4A R 748 011 146 5

4B R 758 013 172 5

5A R 782 011 144 5

5B R 766 017 216 5

6A R 773 009 117 5

7B R 716 011 160 5

8 R 754 010 127 5

9B R 755 008 107 5

12A R 755 006 078 5

12B R 771 008 102 5

13A R 740 017 225 5

13B R 769 007 091 5

14 R 761 011 140 5

15 R 750 018 246 5

22A R 757 008 110 5

22B R 759 007 088 5

23 R 732 009 117 5

1B L 4551 091 200 5

2B L 4391 078 178 5

6B L 3936 067 170 5

9A L 4471 060 134 5

10 L 4667 073 157 5

11 L 5068 136 269 5

12C L 4644 031 066 5

17 L 4346 106 243 5

19 L 4566 087 190 5

20 L 4616 122 265 5

21 L 5008 077 153 5

24 L 4782 094 196 5

25 L 4434 081 182 5

1A R 4168 016 039 5

2A R 4014 024 061 5

3 R 4247 035 083 5

4A R 4097 039 095 5

4B R 4181 064 153 5

5B R 3997 040 101 5

6A R 4076 074 181 5

8 R 4044 043 107 5

9B R 4097 033 080 5

12A R 4125 046 112 5

12B R 4257 039 092 5

15 R 3957 052 131 5

22A R 4046 028 069 5

22B R 4015 045 112 5

23 R 3830 073 192 5

1B L 1237 038 305 5

2B L 999 037 375 5

6B L 906 034 381 5

9A L 1147 043 373 5

10 L 1152 052 453 5

11 L 1488 053 356 5

12C L 1061 019 179 5

17 L 1027 028 274 5

19 L 1095 038 348 5

20 L 1216 083 681 5

21 L 1285 026 206 5

24 L 1235 060 484 5

25 L 1004 031 307 5

1A R 1024 014 138 5

2A R 797 016 197 5

3 R 974 031 317 5

4A R 911 034 368 5

4B R 931 027 287 5

5B R 815 041 507 5

6A R 923 038 411 5

8 R 929 033 354 5

9B R 927 028 301 5

12A R 1004 051 508 5

12B R 935 017 181 5

15 R 823 029 349 5

22A R 953 005 052 5

22B R 926 038 410 5

23 R 1598 065 404 5

1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1B L 161 007 428 5

2B L 145 008 518 5

6B L 118 014 1213 5

7A L 175 006 364 5

9A L 142 011 802 5

10 L 177 010 581 5

11 L 142 009 632 5

12C L 122 008 645 5

16 L 142 012 872 5

17 L 145 026 1823 5

18 L 147 019 1299 5

19 L 147 019 1299 5

20 L 214 013 611 5

21 L 120 024 2024 5

24 L 156 009 551 5

25 L 127 016 1261 5

1A R 215 007 316 5

2A R 174 008 444 5

3 R 196 010 493 5

4A R 197 008 406 5

4B R 213 013 629 5

5A R 197 009 471 5

5B R 192 008 419 5

6A R 227 010 445 5

7B R 184 007 396 5

8 R 206 013 637 5

9B R 203 012 579 5

12A R 250 012 464 5

12B R 244 010 430 5

13A R 205 007 362 5

13B R 204 012 576 5

14 R 228 017 739 5

15 R 188 016 834 5

22A R 219 007 337 5

22B R 215 005 225 5

23 R 179 003 179 5

1B L 1704 0029 170 5

2B L 1706 0039 227 5

6B L 1624 0048 295 5

7A L 1687 0033 194 5

9A L 1612 0200 1240 5

10 L 1748 0070 401 5

11 L 1691 0028 166 5

12C L 1669 0034 206 5

16 L 1731 0028 159 5

17 L 1674 0046 276 5

18 L 1697 0014 082 5

19 L 1697 0014 082 5

20 L 1734 0021 124 5

21 L 1812 0048 266 5

24 L 1694 0037 217 5

25 L 1743 0154 883 5

1A R 1669 0023 141 5

2A R 1638 0037 224 5

3 R 1652 0018 110 5

4A R 1630 0042 255 5

4B R 1653 0035 214 5

5A R 1612 0023 142 5

5B R 1602 0023 141 5

6A R 1661 0037 225 5

7B R 1564 0022 140 5

8 R 1535 0031 204 5

9B R 1659 0047 285 5

12A R 1719 0024 142 5

12B R 1718 0037 216 5

13A R 1497 0024 163 5

13B R 1546 0013 086 5

14 R 1590 0035 217 5

15 R 1651 0030 181 5

22A R 1612 0011 068 5

22B R 1630 0012 075 5

23 R 1639 0026 159 5

1B L 1462 016 111 5

2B L 1449 053 366 5

6B L 1294 044 344 5

7A L 1460 031 214 5

9A L 1395 011 080 5

10 L 1455 039 269 5

11 L 1518 036 236 5

12C L 1439 049 338 5

16 L 1427 013 092 5

17 L 1304 054 413 5

18 L 1456 020 135 5

19 L 1456 020 135 5

20 L 1395 036 255 5

21 L 1531 057 371 5

24 L 1466 023 154 5

25 L 1306 066 509 5

1A R 1367 020 145 5

2A R 1361 023 169 5

3 R 1398 012 083 5

4A R 1363 024 176 5

4B R 1391 028 201 5

5A R 1347 014 107 5

5B R 1372 023 166 5

6A R 1346 019 142 5

7B R 1305 020 153 5

8 R 1378 026 192 5

9B R 1342 015 114 5

12A R 1337 037 278 5

12B R 1375 018 129 5

13A R 1319 015 112 5

13B R 1341 009 069 5

14 R 1359 028 204 5

15 R 1366 029 214 5

22A R 1371 019 136 5

22B R 1353 024 175 5

23 R 1308 037 283 5

1B L 1335 020 150 5

2B L 1297 037 288 5

6B L 1260 099 790 5

7A L 1374 034 249 5

9A L 1233 019 153 5

10 L 1219 054 445 5

11 L 1267 044 350 5

12C L 1325 033 248 5

16 L 1307 024 185 5

17 L 1196 029 242 5

18 L 1335 010 072 5

19 L 1335 010 072 5

20 L 1324 033 248 5

21 L 1363 032 238 5

24 L 1263 040 315 5

25 L 1194 069 574 5

1A R 1368 010 076 5

2A R 1308 018 135 5

3 R 1345 023 172 5

4A R 1340 011 079 5

4B R 1394 041 294 5

5A R 1292 028 216 5

5B R 1360 034 251 5

6A R 1372 023 166 5

7B R 1291 013 098 5

8 R 1369 025 183 5

9B R 1276 023 182 5

12A R 1317 034 256 5

12B R 1375 024 175 5

13A R 1334 021 155 5

13B R 1338 030 227 5

14 R 1366 023 167 5

15 R 1377 019 139 5

22A R 1344 016 118 5

22B R 1341 016 116 5

23 R 1334 029 217 5

1B L 796 005 059 5

2B L 806 012 144 5

6B L 814 018 219 5

7A L 789 009 112 5

9A L 781 024 306 5

10 L 802 020 245 5

11 L 784 018 225 5

12C L 794 021 263 5

16 L 850 014 168 5

17 L 774 016 203 5

18 L 787 015 187 5

19 L 787 015 187 5

20 L 769 014 188 5

21 L 808 008 097 5

24 L 792 010 128 5

25 L 751 030 400 5

1A R 767 005 068 5

2A R 727 008 109 5

3 R 779 008 099 5

4A R 748 011 146 5

4B R 758 013 172 5

5A R 782 011 144 5

5B R 766 017 216 5

6A R 773 009 117 5

7B R 716 011 160 5

8 R 754 010 127 5

9B R 755 008 107 5

12A R 755 006 078 5

12B R 771 008 102 5

13A R 740 017 225 5

13B R 769 007 091 5

14 R 761 011 140 5

15 R 750 018 246 5

22A R 757 008 110 5

22B R 759 007 088 5

23 R 732 009 117 5

1B L 4551 091 200 5

2B L 4391 078 178 5

6B L 3936 067 170 5

9A L 4471 060 134 5

10 L 4667 073 157 5

11 L 5068 136 269 5

12C L 4644 031 066 5

17 L 4346 106 243 5

19 L 4566 087 190 5

20 L 4616 122 265 5

21 L 5008 077 153 5

24 L 4782 094 196 5

25 L 4434 081 182 5

1A R 4168 016 039 5

2A R 4014 024 061 5

3 R 4247 035 083 5

4A R 4097 039 095 5

4B R 4181 064 153 5

5B R 3997 040 101 5

6A R 4076 074 181 5

8 R 4044 043 107 5

9B R 4097 033 080 5

12A R 4125 046 112 5

12B R 4257 039 092 5

15 R 3957 052 131 5

22A R 4046 028 069 5

22B R 4015 045 112 5

23 R 3830 073 192 5

1B L 1237 038 305 5

2B L 999 037 375 5

6B L 906 034 381 5

9A L 1147 043 373 5

10 L 1152 052 453 5

11 L 1488 053 356 5

12C L 1061 019 179 5

17 L 1027 028 274 5

19 L 1095 038 348 5

20 L 1216 083 681 5

21 L 1285 026 206 5

24 L 1235 060 484 5

25 L 1004 031 307 5

1A R 1024 014 138 5

2A R 797 016 197 5

3 R 974 031 317 5

4A R 911 034 368 5

4B R 931 027 287 5

5B R 815 041 507 5

6A R 923 038 411 5

8 R 929 033 354 5

9B R 927 028 301 5

12A R 1004 051 508 5

12B R 935 017 181 5

15 R 823 029 349 5

22A R 953 005 052 5

22B R 926 038 410 5

23 R 1598 065 404 5

1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1B L 1704 0029 170 5

2B L 1706 0039 227 5

6B L 1624 0048 295 5

7A L 1687 0033 194 5

9A L 1612 0200 1240 5

10 L 1748 0070 401 5

11 L 1691 0028 166 5

12C L 1669 0034 206 5

16 L 1731 0028 159 5

17 L 1674 0046 276 5

18 L 1697 0014 082 5

19 L 1697 0014 082 5

20 L 1734 0021 124 5

21 L 1812 0048 266 5

24 L 1694 0037 217 5

25 L 1743 0154 883 5

1A R 1669 0023 141 5

2A R 1638 0037 224 5

3 R 1652 0018 110 5

4A R 1630 0042 255 5

4B R 1653 0035 214 5

5A R 1612 0023 142 5

5B R 1602 0023 141 5

6A R 1661 0037 225 5

7B R 1564 0022 140 5

8 R 1535 0031 204 5

9B R 1659 0047 285 5

12A R 1719 0024 142 5

12B R 1718 0037 216 5

13A R 1497 0024 163 5

13B R 1546 0013 086 5

14 R 1590 0035 217 5

15 R 1651 0030 181 5

22A R 1612 0011 068 5

22B R 1630 0012 075 5

23 R 1639 0026 159 5

1B L 1462 016 111 5

2B L 1449 053 366 5

6B L 1294 044 344 5

7A L 1460 031 214 5

9A L 1395 011 080 5

10 L 1455 039 269 5

11 L 1518 036 236 5

12C L 1439 049 338 5

16 L 1427 013 092 5

17 L 1304 054 413 5

18 L 1456 020 135 5

19 L 1456 020 135 5

20 L 1395 036 255 5

21 L 1531 057 371 5

24 L 1466 023 154 5

25 L 1306 066 509 5

1A R 1367 020 145 5

2A R 1361 023 169 5

3 R 1398 012 083 5

4A R 1363 024 176 5

4B R 1391 028 201 5

5A R 1347 014 107 5

5B R 1372 023 166 5

6A R 1346 019 142 5

7B R 1305 020 153 5

8 R 1378 026 192 5

9B R 1342 015 114 5

12A R 1337 037 278 5

12B R 1375 018 129 5

13A R 1319 015 112 5

13B R 1341 009 069 5

14 R 1359 028 204 5

15 R 1366 029 214 5

22A R 1371 019 136 5

22B R 1353 024 175 5

23 R 1308 037 283 5

1B L 1335 020 150 5

2B L 1297 037 288 5

6B L 1260 099 790 5

7A L 1374 034 249 5

9A L 1233 019 153 5

10 L 1219 054 445 5

11 L 1267 044 350 5

12C L 1325 033 248 5

16 L 1307 024 185 5

17 L 1196 029 242 5

18 L 1335 010 072 5

19 L 1335 010 072 5

20 L 1324 033 248 5

21 L 1363 032 238 5

24 L 1263 040 315 5

25 L 1194 069 574 5

1A R 1368 010 076 5

2A R 1308 018 135 5

3 R 1345 023 172 5

4A R 1340 011 079 5

4B R 1394 041 294 5

5A R 1292 028 216 5

5B R 1360 034 251 5

6A R 1372 023 166 5

7B R 1291 013 098 5

8 R 1369 025 183 5

9B R 1276 023 182 5

12A R 1317 034 256 5

12B R 1375 024 175 5

13A R 1334 021 155 5

13B R 1338 030 227 5

14 R 1366 023 167 5

15 R 1377 019 139 5

22A R 1344 016 118 5

22B R 1341 016 116 5

23 R 1334 029 217 5

1B L 796 005 059 5

2B L 806 012 144 5

6B L 814 018 219 5

7A L 789 009 112 5

9A L 781 024 306 5

10 L 802 020 245 5

11 L 784 018 225 5

12C L 794 021 263 5

16 L 850 014 168 5

17 L 774 016 203 5

18 L 787 015 187 5

19 L 787 015 187 5

20 L 769 014 188 5

21 L 808 008 097 5

24 L 792 010 128 5

25 L 751 030 400 5

1A R 767 005 068 5

2A R 727 008 109 5

3 R 779 008 099 5

4A R 748 011 146 5

4B R 758 013 172 5

5A R 782 011 144 5

5B R 766 017 216 5

6A R 773 009 117 5

7B R 716 011 160 5

8 R 754 010 127 5

9B R 755 008 107 5

12A R 755 006 078 5

12B R 771 008 102 5

13A R 740 017 225 5

13B R 769 007 091 5

14 R 761 011 140 5

15 R 750 018 246 5

22A R 757 008 110 5

22B R 759 007 088 5

23 R 732 009 117 5

1B L 4551 091 200 5

2B L 4391 078 178 5

6B L 3936 067 170 5

9A L 4471 060 134 5

10 L 4667 073 157 5

11 L 5068 136 269 5

12C L 4644 031 066 5

17 L 4346 106 243 5

19 L 4566 087 190 5

20 L 4616 122 265 5

21 L 5008 077 153 5

24 L 4782 094 196 5

25 L 4434 081 182 5

1A R 4168 016 039 5

2A R 4014 024 061 5

3 R 4247 035 083 5

4A R 4097 039 095 5

4B R 4181 064 153 5

5B R 3997 040 101 5

6A R 4076 074 181 5

8 R 4044 043 107 5

9B R 4097 033 080 5

12A R 4125 046 112 5

12B R 4257 039 092 5

15 R 3957 052 131 5

22A R 4046 028 069 5

22B R 4015 045 112 5

23 R 3830 073 192 5

1B L 1237 038 305 5

2B L 999 037 375 5

6B L 906 034 381 5

9A L 1147 043 373 5

10 L 1152 052 453 5

11 L 1488 053 356 5

12C L 1061 019 179 5

17 L 1027 028 274 5

19 L 1095 038 348 5

20 L 1216 083 681 5

21 L 1285 026 206 5

24 L 1235 060 484 5

25 L 1004 031 307 5

1A R 1024 014 138 5

2A R 797 016 197 5

3 R 974 031 317 5

4A R 911 034 368 5

4B R 931 027 287 5

5B R 815 041 507 5

6A R 923 038 411 5

8 R 929 033 354 5

9B R 927 028 301 5

12A R 1004 051 508 5

12B R 935 017 181 5

15 R 823 029 349 5

22A R 953 005 052 5

22B R 926 038 410 5

23 R 1598 065 404 5

1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1B L 1462 016 111 5

2B L 1449 053 366 5

6B L 1294 044 344 5

7A L 1460 031 214 5

9A L 1395 011 080 5

10 L 1455 039 269 5

11 L 1518 036 236 5

12C L 1439 049 338 5

16 L 1427 013 092 5

17 L 1304 054 413 5

18 L 1456 020 135 5

19 L 1456 020 135 5

20 L 1395 036 255 5

21 L 1531 057 371 5

24 L 1466 023 154 5

25 L 1306 066 509 5

1A R 1367 020 145 5

2A R 1361 023 169 5

3 R 1398 012 083 5

4A R 1363 024 176 5

4B R 1391 028 201 5

5A R 1347 014 107 5

5B R 1372 023 166 5

6A R 1346 019 142 5

7B R 1305 020 153 5

8 R 1378 026 192 5

9B R 1342 015 114 5

12A R 1337 037 278 5

12B R 1375 018 129 5

13A R 1319 015 112 5

13B R 1341 009 069 5

14 R 1359 028 204 5

15 R 1366 029 214 5

22A R 1371 019 136 5

22B R 1353 024 175 5

23 R 1308 037 283 5

1B L 1335 020 150 5

2B L 1297 037 288 5

6B L 1260 099 790 5

7A L 1374 034 249 5

9A L 1233 019 153 5

10 L 1219 054 445 5

11 L 1267 044 350 5

12C L 1325 033 248 5

16 L 1307 024 185 5

17 L 1196 029 242 5

18 L 1335 010 072 5

19 L 1335 010 072 5

20 L 1324 033 248 5

21 L 1363 032 238 5

24 L 1263 040 315 5

25 L 1194 069 574 5

1A R 1368 010 076 5

2A R 1308 018 135 5

3 R 1345 023 172 5

4A R 1340 011 079 5

4B R 1394 041 294 5

5A R 1292 028 216 5

5B R 1360 034 251 5

6A R 1372 023 166 5

7B R 1291 013 098 5

8 R 1369 025 183 5

9B R 1276 023 182 5

12A R 1317 034 256 5

12B R 1375 024 175 5

13A R 1334 021 155 5

13B R 1338 030 227 5

14 R 1366 023 167 5

15 R 1377 019 139 5

22A R 1344 016 118 5

22B R 1341 016 116 5

23 R 1334 029 217 5

1B L 796 005 059 5

2B L 806 012 144 5

6B L 814 018 219 5

7A L 789 009 112 5

9A L 781 024 306 5

10 L 802 020 245 5

11 L 784 018 225 5

12C L 794 021 263 5

16 L 850 014 168 5

17 L 774 016 203 5

18 L 787 015 187 5

19 L 787 015 187 5

20 L 769 014 188 5

21 L 808 008 097 5

24 L 792 010 128 5

25 L 751 030 400 5

1A R 767 005 068 5

2A R 727 008 109 5

3 R 779 008 099 5

4A R 748 011 146 5

4B R 758 013 172 5

5A R 782 011 144 5

5B R 766 017 216 5

6A R 773 009 117 5

7B R 716 011 160 5

8 R 754 010 127 5

9B R 755 008 107 5

12A R 755 006 078 5

12B R 771 008 102 5

13A R 740 017 225 5

13B R 769 007 091 5

14 R 761 011 140 5

15 R 750 018 246 5

22A R 757 008 110 5

22B R 759 007 088 5

23 R 732 009 117 5

1B L 4551 091 200 5

2B L 4391 078 178 5

6B L 3936 067 170 5

9A L 4471 060 134 5

10 L 4667 073 157 5

11 L 5068 136 269 5

12C L 4644 031 066 5

17 L 4346 106 243 5

19 L 4566 087 190 5

20 L 4616 122 265 5

21 L 5008 077 153 5

24 L 4782 094 196 5

25 L 4434 081 182 5

1A R 4168 016 039 5

2A R 4014 024 061 5

3 R 4247 035 083 5

4A R 4097 039 095 5

4B R 4181 064 153 5

5B R 3997 040 101 5

6A R 4076 074 181 5

8 R 4044 043 107 5

9B R 4097 033 080 5

12A R 4125 046 112 5

12B R 4257 039 092 5

15 R 3957 052 131 5

22A R 4046 028 069 5

22B R 4015 045 112 5

23 R 3830 073 192 5

1B L 1237 038 305 5

2B L 999 037 375 5

6B L 906 034 381 5

9A L 1147 043 373 5

10 L 1152 052 453 5

11 L 1488 053 356 5

12C L 1061 019 179 5

17 L 1027 028 274 5

19 L 1095 038 348 5

20 L 1216 083 681 5

21 L 1285 026 206 5

24 L 1235 060 484 5

25 L 1004 031 307 5

1A R 1024 014 138 5

2A R 797 016 197 5

3 R 974 031 317 5

4A R 911 034 368 5

4B R 931 027 287 5

5B R 815 041 507 5

6A R 923 038 411 5

8 R 929 033 354 5

9B R 927 028 301 5

12A R 1004 051 508 5

12B R 935 017 181 5

15 R 823 029 349 5

22A R 953 005 052 5

22B R 926 038 410 5

23 R 1598 065 404 5

1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1B L 1335 020 150 5

2B L 1297 037 288 5

6B L 1260 099 790 5

7A L 1374 034 249 5

9A L 1233 019 153 5

10 L 1219 054 445 5

11 L 1267 044 350 5

12C L 1325 033 248 5

16 L 1307 024 185 5

17 L 1196 029 242 5

18 L 1335 010 072 5

19 L 1335 010 072 5

20 L 1324 033 248 5

21 L 1363 032 238 5

24 L 1263 040 315 5

25 L 1194 069 574 5

1A R 1368 010 076 5

2A R 1308 018 135 5

3 R 1345 023 172 5

4A R 1340 011 079 5

4B R 1394 041 294 5

5A R 1292 028 216 5

5B R 1360 034 251 5

6A R 1372 023 166 5

7B R 1291 013 098 5

8 R 1369 025 183 5

9B R 1276 023 182 5

12A R 1317 034 256 5

12B R 1375 024 175 5

13A R 1334 021 155 5

13B R 1338 030 227 5

14 R 1366 023 167 5

15 R 1377 019 139 5

22A R 1344 016 118 5

22B R 1341 016 116 5

23 R 1334 029 217 5

1B L 796 005 059 5

2B L 806 012 144 5

6B L 814 018 219 5

7A L 789 009 112 5

9A L 781 024 306 5

10 L 802 020 245 5

11 L 784 018 225 5

12C L 794 021 263 5

16 L 850 014 168 5

17 L 774 016 203 5

18 L 787 015 187 5

19 L 787 015 187 5

20 L 769 014 188 5

21 L 808 008 097 5

24 L 792 010 128 5

25 L 751 030 400 5

1A R 767 005 068 5

2A R 727 008 109 5

3 R 779 008 099 5

4A R 748 011 146 5

4B R 758 013 172 5

5A R 782 011 144 5

5B R 766 017 216 5

6A R 773 009 117 5

7B R 716 011 160 5

8 R 754 010 127 5

9B R 755 008 107 5

12A R 755 006 078 5

12B R 771 008 102 5

13A R 740 017 225 5

13B R 769 007 091 5

14 R 761 011 140 5

15 R 750 018 246 5

22A R 757 008 110 5

22B R 759 007 088 5

23 R 732 009 117 5

1B L 4551 091 200 5

2B L 4391 078 178 5

6B L 3936 067 170 5

9A L 4471 060 134 5

10 L 4667 073 157 5

11 L 5068 136 269 5

12C L 4644 031 066 5

17 L 4346 106 243 5

19 L 4566 087 190 5

20 L 4616 122 265 5

21 L 5008 077 153 5

24 L 4782 094 196 5

25 L 4434 081 182 5

1A R 4168 016 039 5

2A R 4014 024 061 5

3 R 4247 035 083 5

4A R 4097 039 095 5

4B R 4181 064 153 5

5B R 3997 040 101 5

6A R 4076 074 181 5

8 R 4044 043 107 5

9B R 4097 033 080 5

12A R 4125 046 112 5

12B R 4257 039 092 5

15 R 3957 052 131 5

22A R 4046 028 069 5

22B R 4015 045 112 5

23 R 3830 073 192 5

1B L 1237 038 305 5

2B L 999 037 375 5

6B L 906 034 381 5

9A L 1147 043 373 5

10 L 1152 052 453 5

11 L 1488 053 356 5

12C L 1061 019 179 5

17 L 1027 028 274 5

19 L 1095 038 348 5

20 L 1216 083 681 5

21 L 1285 026 206 5

24 L 1235 060 484 5

25 L 1004 031 307 5

1A R 1024 014 138 5

2A R 797 016 197 5

3 R 974 031 317 5

4A R 911 034 368 5

4B R 931 027 287 5

5B R 815 041 507 5

6A R 923 038 411 5

8 R 929 033 354 5

9B R 927 028 301 5

12A R 1004 051 508 5

12B R 935 017 181 5

15 R 823 029 349 5

22A R 953 005 052 5

22B R 926 038 410 5

23 R 1598 065 404 5

1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1B L 796 005 059 5

2B L 806 012 144 5

6B L 814 018 219 5

7A L 789 009 112 5

9A L 781 024 306 5

10 L 802 020 245 5

11 L 784 018 225 5

12C L 794 021 263 5

16 L 850 014 168 5

17 L 774 016 203 5

18 L 787 015 187 5

19 L 787 015 187 5

20 L 769 014 188 5

21 L 808 008 097 5

24 L 792 010 128 5

25 L 751 030 400 5

1A R 767 005 068 5

2A R 727 008 109 5

3 R 779 008 099 5

4A R 748 011 146 5

4B R 758 013 172 5

5A R 782 011 144 5

5B R 766 017 216 5

6A R 773 009 117 5

7B R 716 011 160 5

8 R 754 010 127 5

9B R 755 008 107 5

12A R 755 006 078 5

12B R 771 008 102 5

13A R 740 017 225 5

13B R 769 007 091 5

14 R 761 011 140 5

15 R 750 018 246 5

22A R 757 008 110 5

22B R 759 007 088 5

23 R 732 009 117 5

1B L 4551 091 200 5

2B L 4391 078 178 5

6B L 3936 067 170 5

9A L 4471 060 134 5

10 L 4667 073 157 5

11 L 5068 136 269 5

12C L 4644 031 066 5

17 L 4346 106 243 5

19 L 4566 087 190 5

20 L 4616 122 265 5

21 L 5008 077 153 5

24 L 4782 094 196 5

25 L 4434 081 182 5

1A R 4168 016 039 5

2A R 4014 024 061 5

3 R 4247 035 083 5

4A R 4097 039 095 5

4B R 4181 064 153 5

5B R 3997 040 101 5

6A R 4076 074 181 5

8 R 4044 043 107 5

9B R 4097 033 080 5

12A R 4125 046 112 5

12B R 4257 039 092 5

15 R 3957 052 131 5

22A R 4046 028 069 5

22B R 4015 045 112 5

23 R 3830 073 192 5

1B L 1237 038 305 5

2B L 999 037 375 5

6B L 906 034 381 5

9A L 1147 043 373 5

10 L 1152 052 453 5

11 L 1488 053 356 5

12C L 1061 019 179 5

17 L 1027 028 274 5

19 L 1095 038 348 5

20 L 1216 083 681 5

21 L 1285 026 206 5

24 L 1235 060 484 5

25 L 1004 031 307 5

1A R 1024 014 138 5

2A R 797 016 197 5

3 R 974 031 317 5

4A R 911 034 368 5

4B R 931 027 287 5

5B R 815 041 507 5

6A R 923 038 411 5

8 R 929 033 354 5

9B R 927 028 301 5

12A R 1004 051 508 5

12B R 935 017 181 5

15 R 823 029 349 5

22A R 953 005 052 5

22B R 926 038 410 5

23 R 1598 065 404 5

1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1B L 4551 091 200 5

2B L 4391 078 178 5

6B L 3936 067 170 5

9A L 4471 060 134 5

10 L 4667 073 157 5

11 L 5068 136 269 5

12C L 4644 031 066 5

17 L 4346 106 243 5

19 L 4566 087 190 5

20 L 4616 122 265 5

21 L 5008 077 153 5

24 L 4782 094 196 5

25 L 4434 081 182 5

1A R 4168 016 039 5

2A R 4014 024 061 5

3 R 4247 035 083 5

4A R 4097 039 095 5

4B R 4181 064 153 5

5B R 3997 040 101 5

6A R 4076 074 181 5

8 R 4044 043 107 5

9B R 4097 033 080 5

12A R 4125 046 112 5

12B R 4257 039 092 5

15 R 3957 052 131 5

22A R 4046 028 069 5

22B R 4015 045 112 5

23 R 3830 073 192 5

1B L 1237 038 305 5

2B L 999 037 375 5

6B L 906 034 381 5

9A L 1147 043 373 5

10 L 1152 052 453 5

11 L 1488 053 356 5

12C L 1061 019 179 5

17 L 1027 028 274 5

19 L 1095 038 348 5

20 L 1216 083 681 5

21 L 1285 026 206 5

24 L 1235 060 484 5

25 L 1004 031 307 5

1A R 1024 014 138 5

2A R 797 016 197 5

3 R 974 031 317 5

4A R 911 034 368 5

4B R 931 027 287 5

5B R 815 041 507 5

6A R 923 038 411 5

8 R 929 033 354 5

9B R 927 028 301 5

12A R 1004 051 508 5

12B R 935 017 181 5

15 R 823 029 349 5

22A R 953 005 052 5

22B R 926 038 410 5

23 R 1598 065 404 5

1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1B L 1237 038 305 5

2B L 999 037 375 5

6B L 906 034 381 5

9A L 1147 043 373 5

10 L 1152 052 453 5

11 L 1488 053 356 5

12C L 1061 019 179 5

17 L 1027 028 274 5

19 L 1095 038 348 5

20 L 1216 083 681 5

21 L 1285 026 206 5

24 L 1235 060 484 5

25 L 1004 031 307 5

1A R 1024 014 138 5

2A R 797 016 197 5

3 R 974 031 317 5

4A R 911 034 368 5

4B R 931 027 287 5

5B R 815 041 507 5

6A R 923 038 411 5

8 R 929 033 354 5

9B R 927 028 301 5

12A R 1004 051 508 5

12B R 935 017 181 5

15 R 823 029 349 5

22A R 953 005 052 5

22B R 926 038 410 5

23 R 1598 065 404 5

1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1B L 3484 0055 158 5

2B L 3434 0048 141 5

6B L 3342 0051 153 5

9A L 3494 0089 255 5

10 L 3578 0226 633 5

11 L 3620 0082 225 5

12C L 3402 0024 070 5

17 L 3622 0075 208 5

19 L 3520 0012 035 5

20 L 3552 0230 647 5

21 L 3712 0030 082 5

24 L 3524 0061 174 5

25 L 2986 0052 173 5

1A R 3385 0020 060 5

2A R 3317 0030 090 5

3 R 3479 0023 067 5

4A R 3369 0037 109 5

4B R 3340 0053 160 5

5B R 1677 0025 148 5

6A R 3390 0066 195 5

8 R 2967 0044 149 5

9B R 3410 0048 142 5

12A R 3452 0030 085 5

12B R 3520 0068 192 5

15 R 3333 0099 296 5

22A R 3222 0051 159 5

22B R 3210 0049 151 5

23 R 6610 0108 163 5

1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1B L 2965 054 183 5

2B L 3048 092 301 5

6B L 2696 035 131 5

9A L 2975 038 129 5

10 L 3157 047 148 5

11 L 3218 082 255 5

12C L 3243 015 047 5

17 L 3157 079 250 5

19 L 3119 084 268 5

20 L 3045 056 185 5

21 L 3351 066 198 5

24 L 3195 050 158 5

25 L 3132 054 174 5

1A R 2806 018 065 5

2A R 2885 012 043 5

3 R 2925 040 135 5

4A R 2849 021 074 5

4B R 2917 035 119 5

5B R 3013 023 077 5

6A R 2811 036 129 5

8 R 2819 021 074 5

9B R 2832 032 115 5

12A R 2776 048 171 5

12B R 2970 026 086 5

15 R 2800 035 124 5

22A R 2770 025 091 5

22B R 2768 049 178 5

23 R 1570 060 384 5

1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1B L 2478 034 137 5

2B L 2472 027 111 5

6B L 2367 039 165 5

9A L 2423 065 270 5

10 L 2373 018 077 5

11 L 2568 029 114 5

12C L 2497 028 113 5

17 L 2321 032 139 5

19 L 2488 022 086 5

20 L 2489 056 227 5

21 L 2523 045 177 5

24 L 2470 052 211 5

25 L 2399 089 369 5

1A R 2505 033 131 5

2A R 2485 037 149 5

3 R 2605 031 119 5

4A R 2513 031 125 5

4B R 2542 047 185 5

5B R 2480 022 088 5

6A R 2570 024 092 5

8 R 2532 047 185 5

9B R 2457 044 181 5

12A R 2506 023 093 5

12B R 2523 018 069 5

15 R 2547 039 154 5

22A R 2470 034 138 5

22B R 2466 032 130 5

23 R 2508 030 119 5

1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1B L 1138 022 191 5

2B L 1154 019 162 5

6B L 1170 008 068 5

9A L 1095 013 114 5

10 L 1138 023 199 5

11 L 1127 016 138 5

12C L 1115 022 199 5

17 L 1110 009 079 5

19 L 1059 011 101 5

20 L 1087 019 176 5

21 L 1121 019 169 5

24 L 1106 027 248 5

25 L 1102 012 105 5

1A R 1111 018 159 5

2A R 1059 014 130 5

3 R 1152 013 110 5

4A R 1078 008 070 5

4B R 1105 016 143 5

5B R 1134 030 267 5

6A R 1136 004 034 5

8 R 1075 015 142 5

9B R 1077 006 054 5

12A R 1102 020 186 5

12B R 1097 016 148 5

15 R 1084 010 091 5

22A R 1112 016 147 5

22B R 1106 014 122 5

23 R 1066 009 088 5

in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










in Appendix F)

36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










36 5 17331 0371 2139 1049 0689 3976 1949 NA NA 25 TPM

36 5 1809 0124 6835 0350 0382 21087 1079 NA NA 17 Water

36 5 1657 0033 1994 0093 0071 4306 0202 9A-25 NA 10 Nicotine

36 5 13864 0313 2260 0886 0674 4864 1907 NA NA 25 NFDPM

36 5 13239 0279 2106 0789 0536 4046 1515 6B-25 NA NA CO

36 5 7722 0136 1765 0386 0292 3779 0825 NA NA 25 Puff count

20 5 17240 0283 1644 0802 0455 2641 1288 NA NA NA TPM

20 5 2067 0103 4973 0291 0221 10696 0625 NA NA NA Water

20 5 1624 0029 1802 0083 0062 3843 0177 NA NA NA Nicotine

20 5 13550 0232 1710 0655 0324 2392 0917 NA NA NA NFDPM

20 5 13421 0243 1811 0688 0387 2883 1095 NA NA NA CO

16 5 17445 0457 2620 1293 0901 5167 2549 NA NA NA TPM

16 5 1487 0146 9791 0412 0279 18748 0789 NA NA 20 Water

16 5 1705 0038 2217 0107 0055 3219 0155 9A-25 NA NA Nicotine

16 5 14257 0392 2751 1109 0791 5551 2238 NA NA NA NFDPM

16 5 12910 0359 2780 1015 0672 5207 1901 6B NA 25 CO

16 5 7926 0166 2095 0470 0264 3336 0748 NA NA 16 Puff count

28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










28 5 43083 0693 1609 1960 3348 7771 9470 NA NA NA TPM

28 5 10008 0345 3451 0977 1341 13402 3793 20 23-11 NA Water

28 5 3400 0054 1581 0152 0179 5278 0508 20 23-5B NA Nicotine

28 5 29646 0493 1662 1394 1778 5997 5029 NA 23 NA NFDPM

28 5 24881 0367 1476 1039 0707 2842 2000 25 NA NA CO

15 5 40767 0464 1138 1312 1194 2930 3378 NA NA NA TPM

15 5 9193 0310 3368 0876 0722 7851 2041 NA 23 NA Water

13 5 3338 0052 1552 0147 0150 4500 0425 NA 23-5B 15-8 Nicotine

15 5 28530 0319 1116 0901 0826 2894 2335 NA 23 NA NFDPM

15 5 25139 0340 1352 0961 0510 2028 1442 NA NA NA CO

15 5 10995 0153 1387 0431 0302 2748 0855 NA NA 5B Puff count

13 5 45755 0887 1938 2508 3014 6588 8526 NA NA NA TPM

13 5 11425 0448 3919 1267 1581 13842 4473 NA NA NA Water

13 5 3512 0056 1599 0159 0118 3352 0333 20 25 NA Nicotine

13 5 30847 0629 2038 1778 1755 5688 4963 NA NA NA NFDPM

13 5 24515 0455 1856 1287 0811 3309 2294 NA NA 25 CO

Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Comparison 6

ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










ISO smoking regime

Year 2008 2010 2011 2011 2012 2013 2014 2014 2016

Average

TPM (mgtp) 1754 1737 1743 1637 1628 1616 1615 1757 1733

WATER (mgtp)

187 181 184 178 175 171 171 184 181

NICOTINE (mgtp)

1390 1366 1362 1236 1221 1221 1204 1650 1657

NFDPM (mgtp)

1428 1418 1421 1334 1329 1323 1325 1406 1386

CO (mgtp) 1483 1456 1442 1293 1284 1276 1283 1342 1324

PUFF (tp) 915 909 900 836 836 832 823 770 772

Repeatability (r)

TPM (mgtp) 083 081 094 093 080 085 087 106 105

WATER (mgtp)

043 040 047 041 041 039 036 039 035

NICOTINE (mgtp)

0080 0074 0084 0075 0066 0076 0075 0119 0093

NFDPM (mgtp)

071 063 080 077 078 072 072 082 089

CO (mgtp) 082 092 095 095 078 075 079 105 079

PUFF (tp) 037 039 033 038 034 031 036 030 039

Reproducibility (R)

TPM (mgtp) 177 154 172 177 167 161 193 189 195

WATER (mgtp)

111 109 098 097 103 098 101 112 108

NICOTINE (mgtp)

0131 0150 0173 0150 0143 0146 0155 0197 0202

NFDPM (mgtp)

180 153 192 188 173 185 216 197 191

CO (mgtp) 164 196 183 194 175 161 197 202 152

PUFF (tp) 088 082 069 086 093 091 082 075 083

test pieces

Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Year 2013 2016

Test piece CM7 CM8

Average

TPM (mgtp) 4156 4308

WATER (mgtp)

1033 1001

NICOTINE (mgtp)

2493 3400

NFDPM (mgtp)

2839 2965

CO (mgtp) 2472 2488

PUFF (tp) 1179 1108

Repeatability (r)

TPM (mgtp) 238 196

WATER (mgtp)

123 098

NICOTINE (mgtp)

0152 0152

NFDPM (mgtp)

157 139

CO (mgtp) 130 104

PUFF (tp) 052 047

Reproducibility (R)

TPM (mgtp) 1053 947

WATER (mgtp)

477 379

NICOTINE (mgtp)

0313 0508

NFDPM (mgtp)

566 503

CO (mgtp) 301 200

PUFF (tp) 127 092

Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Study CM8 2014 CM8 2016

Conclusion 7

Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Altria JTI UK

ITG Brands

Japan Tobacco Inc

JTI Germany

CM8 ISO Regime Only

Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Collaborative Study

08 January 2016

1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1 Foreword

1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










1 Introduction 4

2 Objectives 4

5 Methods 5

53 Sampling 5

55 Butt Marking 6

56 Conditioning 6

59 Smoking Plans 7

Bibliography 13

5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










5 Methods

51 General Guidance

52 Test Specimen(s)

Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Puff number number

Ancillary variables

Date of test DDMMYY

Air velocity mms

7 Study Time Table

8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










8 Data Submission

Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Bibliography

SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










SI base units

SI derived units

SI prefixes

1 Foreword

1 Introduction

2 Objectives

5 Methods

51 General Guidance

52 Test Specimen(s)

53 Sampling

55 Butt Marking

56 Conditioning

58 Smoking Machine

59 Smoking Plans

7 Study Time Table

8 Data Submission


Bibliography


CORESTA
Piegravece jointe








Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

12A R

RM200 A

2 9620 1811 256 1738 1381 1340 763

12A R

RM200 A

3 9560 1725 255 1715 1299 1290 753

12A R

RM200 A

4 9530 1765 231 1747 1359 1340 753

12A R

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760


Lab Count

Machine

Count

Lab Cod

e

Machine

Class

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080






9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160





Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count








8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125










13B R RM20H M2

5 NA NA NA NA NA NA






15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076






17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111






19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061


Lab Count

Machine Count

Lab

Code

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120




SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

(C)

COCHRAN

OUTLYING LAB

(G)

SINGLE

GRUBBS

OUTLIER

(G2)

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES



WOULD EXCEED 29




WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

YES

YES

YES

YES

NO

NO

NO

NO

(Gi)SINGLE GRUBBS


OF COCHRAN OUTLYING

LAB

YES



WOULD EXCEED 29

NO






































































Lab Code











Water IS Ethanol





COA205Cerulean


Water IS Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Water IS Ethanol






Water IS Ethanol


Lab Code










Water IS Ethanol


A






Water IS Ethanol


A






Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol





Water IS Ethanol


Lab Code









Water IS Ethanol






Water IS Ethanol



Nicotine IS Decanol



Water IS Ethanol


Lab Code









Water IS Methanol





Water IS Methanol





Water IS Methanol


Lab Code










Water IS Ethanol






Ethanol







Water IS Ethanol


Lab Code










Water IS Ethanol





Cerulean COA 205


Water IS Methanol






Water IS Ethanol


Lab Code










Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297










Cerulean COA 205


Water IS Ethanol





Water IS Ethanol


Lab Code





22A RM20H Borgwaldt






Water IS Ethanol


Agilent 7890A





Water IS Ethanol





Water IS Ethanol


Lab Code










Water IS Ethanol



Nicotine ISAnethole


Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795

Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757

Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

RM200 A

2 9620 1811 256 1738 1381 1340 763

RM200 A

3 9560 1725 255 1715 1299 1290 753

RM200 A

4 9530 1765 231 1747 1359 1340 753

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748

Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760

Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080

9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125

13B R RM20H M2

5 NA NA NA NA NA NA

15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076

17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111

19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120

SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

COCHRAN

OUTLYING LAB

SINGLE

GRUBBS

OUTLIER

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES

WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

(Gi)SINGLE GRUBBS

OF COCHRAN OUTLYING

WOULD EXCEED 29

Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

1 1 1A R RM200A 1 9609 1723 206 1657 1351 1357 770

1A R RM200A 2 9650 1776 221 1701 1385 1364 774

1A R RM200A 3 9584 1762 216 1678 1378 1385 762

1A R RM200A 4 9583 1725 221 1638 1340 1365 767

1A R RM200A 5 9602 1757 211 1670 1380 1369 762

2 1B L SM450 1 9640 1752 151 1673 1433 1321 801

1B L SM450 2 9630 1806 162 1749 1469 1308 797

1B L SM450 3 9702 1795 158 1709 1467 1343 799

1B L SM450 4 9620 1803 165 1701 1468 1351 790

1B L SM450 5 9668 1810 169 1686 1472 1354 792

2 3 2A R RM200A 1 9490 1682 176 1652 1341 1296 729

2A R RM200A 2 9497 1748 179 1689 1400 1317 737

2A R RM200A 3 9512 1692 172 1641 1356 1286 718

2A R RM200A 4 9471 1680 161 1593 1360 1311 720

2A R RM200A 5 9444 1690 180 1614 1349 1331 731

4 2B L SM450 1 9450 1787 151 1710 1465 1330 801

2B L SM450 2 9440 1768 141 1715 1455 1336 796

2B L SM450 3 9490 1737 138 1702 1428 1246 796

2B L SM450 4 9540 1851 155 1755 1520 1296 817

2B L SM450 5 9580 1680 140 1647 1375 1278 820

3 5 3 R RM200 1 8994 1782 202 1679 1413 1350 789

3 R RM200 2 9071 1756 197 1644 1394 1377 774

3 R RM200 3 9007 1743 180 1648 1398 1335 778

3 R RM200 4 9040 1776 205 1657 1405 1349 784

3 R RM200 5 9051 1742 197 1630 1382 1313 770

4 6 4A R RM200A 1 9630 1694 196 1611 1337 1337 740

4A R RM200A 2 9580 1692 198 1569 1337 1328 740

4A R RM200A 3 9580 1730 184 1670 1379 1356 740

4A R RM200A 4 9610 1753 206 1665 1381 1344 760

4A R RM200A 5 9630 1745 199 1633 1383 1335 760

7 4B R RM20D 1 9620 1702 199 1598 1343 1338 750

4B R RM20D 2 9620 1790 224 1665 1400 1447 760

4B R RM20D 3 9720 1785 199 1692 1417 1376 780

4B R RM20D 4 9600 1783 216 1668 1400 1415 750

4B R RM20D 5 9540 1785 227 1643 1394 1392 750

5 8 5A R RM20A 1 9655 1726 205 1620 1358 1333 784

5A R RM20A 2 9675 1686 201 1603 1330 1272 778

5A R RM20A 3 9635 1697 185 1632 1357 1262 795

Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757

Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

RM200 A

2 9620 1811 256 1738 1381 1340 763

RM200 A

3 9560 1725 255 1715 1299 1290 753

RM200 A

4 9530 1765 231 1747 1359 1340 753

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748

Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760

Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080

9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125

13B R RM20H M2

5 NA NA NA NA NA NA

15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076

17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111

19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120

SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

COCHRAN

OUTLYING LAB

SINGLE

GRUBBS

OUTLIER

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES

WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

(Gi)SINGLE GRUBBS

OF COCHRAN OUTLYING

WOULD EXCEED 29

Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

5A R RM20A 4 9637 1724 204 1628 1357 1295 788

5A R RM20A 5 9646 1679 189 1576 1332 1301 765

9 5B R RM200A 1 9535 1723 199 1590 1365 1322 767

5B R RM200A 2 9577 1702 189 1609 1352 1387 767

5B R RM200A 3 9607 1777 203 1636 1411 1383 789

5B R RM200A 4 9540 1709 188 1600 1361 1323 767

5B R RM200A 5 9551 1711 184 1576 1369 1386 742

6 10 6A R RM20D 1 9709 1696 212 1628 1322 1342 785

6A R RM20D 2 9608 1721 223 1616 1337 1385 760

6A R RM20D 3 9671 1754 237 1692 1348 1361 775

6A R RM20D 4 9614 1773 230 1698 1373 1401 771

6A R RM20D 5 9704 1755 234 1673 1354 1373 776

11 6B L LX20 1 9675 1473 097 1546 1221 1085 801

6B L LX20 2 9642 1605 112 1654 1327 1308 826

6B L LX20 3 9699 1564 118 1613 1284 1275 819

6B L LX20 4 9654 1627 132 1666 1329 1325 834

6B L LX20 5 9632 1602 130 1642 1307 1307 791

7 12 7A L SM450 1 9583 1849 184 1715 1493 1379 795

7A L SM450 2 9516 1748 167 1663 1415 1324 788

7A L SM450 3 9538 1786 178 1663 1442 1378 783

7A L SM450 4 9565 1813 176 1665 1470 1420 800

7A L SM450 5 9597 1824 172 1730 1479 1368 778

13 7B R RM200A 1 9510 1641 184 1570 1300 1290 718

7B R RM200A 2 9550 1663 174 1590 1330 1286 733

7B R RM200A 3 9560 1621 187 1530 1281 1287 710

7B R RM200A 4 9527 1644 194 1560 1294 1280 702

7B R RM200A 5 9598 1660 182 1570 1321 1313 717

8 14 8 R RM20H 1 9624 1700 204 1546 1340 1327 754

8 R RM20H 2 9652 1746 201 1525 1392 1389 768

8 R RM20H 3 9680 1739 195 1521 1392 1382 752

8 R RM20H 4 9685 1748 228 1584 1361 1381 753

8 R RM20H 5 9685 1754 199 1502 1405 1364 741

9 15 9A L SM450 1 9490 1732 143 1762 1412 1230 775

9A L SM450 2 9550 1714 146 1689 1399 1264 765

9A L SM450 3 9545 1711 158 1689 1384 1233 773

9A L SM450 4 9505 1645 132 1261 1387 1217 823

9A L SM450 5 9520 1689 130 1658 1393 1219 768

16 9B R RM200A 1 9590 1748 215 1675 1366 1309 753

9B R RM200A 2 9610 1678 189 1599 1329 1277 743

9B R RM200A 3 9610 1705 200 1724 1333 1258 758

9B R RM200A 4 9585 1707 195 1631 1349 1287 757

Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

RM200 A

2 9620 1811 256 1738 1381 1340 763

RM200 A

3 9560 1725 255 1715 1299 1290 753

RM200 A

4 9530 1765 231 1747 1359 1340 753

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748

Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760

Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080

9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125

13B R RM20H M2

5 NA NA NA NA NA NA

15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076

17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111

19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120

SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

COCHRAN

OUTLYING LAB

SINGLE

GRUBBS

OUTLIER

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES

WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

(Gi)SINGLE GRUBBS

OF COCHRAN OUTLYING

WOULD EXCEED 29

Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

9B R RM200A 5 9555 1715 215 1666 1334 1251 765

10 17 10 L SM450 1 9657 1785 175 1693 1441 1160 800

10 L SM450 2 9664 1765 160 1835 1422 1165 790

10 L SM450 3 9627 1870 185 1813 1504 1243 835

10 L SM450 4 9698 1768 178 1700 1420 1240 785

10 L SM450 5 9675 1845 185 1698 1490 1285 798

11 18 11 L SM450 1 9581 1876 156 1715 1549 1292 803

11 L SM450 2 9572 1807 134 1665 1507 1203 765

11 L SM450 3 9743 1764 136 1658 1462 1256 765

11 L SM450 4 9572 1830 138 1700 1522 1264 790

11 L SM450 5 9516 1865 145 1718 1548 1322 795

12 19 12A R RM200

A 1 9560 1778 260 1711 1347 1344 747

RM200 A

2 9620 1811 256 1738 1381 1340 763

RM200 A

3 9560 1725 255 1715 1299 1290 753

RM200 A

4 9530 1765 231 1747 1359 1340 753

RM200 A

5 9650 1713 246 1685 1299 1272 757

20 12B R RM200A 1 9610 1793 250 1724 1371 1358 775

12B R RM200A 2 9617 1808 237 1743 1397 1352 765

12B R RM200A 3 9673 1792 255 1753 1362 1369 783

12B R RM200A 4 9605 1790 229 1713 1390 1412 765

12B R RM200A 5 9608 1769 247 1658 1356 1384 767

21 12C L LX20 1 9610 1750 133 1652 1453 1352 804

12C L LX20 2 9560 1665 114 1638 1387 1270 758

12C L LX20 3 9600 1777 117 1703 1490 1319 812

12C L LX20 4 9630 1671 120 1642 1388 1338 798

12C L LX20 5 9580 1775 128 1709 1476 1344 797

13 22 13A R RM20H 1 9556 1673 210 1486 1314 1330 732

13A R RM20H 2 9620 1682 212 1510 1319 1350 733

13A R RM20H 3 9560 1668 193 1478 1327 1320 733

13A R RM20H 4 9571 1649 204 1476 1297 1310 770

13A R RM20H 5 9596 1696 206 1533 1337 1360 733

23 13B R RM20H 1 9658 1726 222 1570 1347 1350 777

13B R RM20H 2 9595 1686 196 1540 1336 1350 765

13B R RM20H 3 9535 1715 208 1541 1353 1330 775

13B R RM20H 4 9633 1682 199 1538 1329 1290 770

13B R RM20H 5 9531 1689 193 1543 1342 1370 760

14 24 14 R RM200A 1 9611 1789 243 1604 1386 1379 767

14 R RM200A 2 9626 1679 200 1552 1324 1327 752

14 R RM200A 3 9553 1728 231 1563 1341 1379 748

Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760

Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080

9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125

13B R RM20H M2

5 NA NA NA NA NA NA

15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076

17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111

19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120

SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

COCHRAN

OUTLYING LAB

SINGLE

GRUBBS

OUTLIER

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES

WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

(Gi)SINGLE GRUBBS

OF COCHRAN OUTLYING

WOULD EXCEED 29

Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

14 R RM200A 4 9625 1754 239 1594 1356 1381 762

14 R RM200A 5 9637 1780 229 1639 1387 1365 774

15 25 15 R RM200A 1 9623 1750 201 1636 1385 1371 761

15 R RM200A 2 9558 1765 205 1668 1393 1409 758

15 R RM200A 3 9556 1713 188 1631 1362 1375 762

15 R RM200A 4 9647 1709 167 1695 1372 1375 753

15 R RM200A 5 9550 1660 179 1624 1319 1357 718

16 26 16 L SM450 1 9606 1752 163 1770 1412 1315 870

16 L SM450 2 9634 1748 134 1741 1439 1334 840

16 L SM450 3 9663 1726 139 1735 1413 1276 855

16 L SM450 4 9676 1745 143 1706 1432 1321 850

16 L SM450 5 9564 1739 132 1703 1437 1287 833

17 27 17 L SM450 1 9525 1593 165 1670 1261 1198 770

17 L SM450 2 9603 1658 128 1610 1369 1233 788

17 L SM450 3 9573 1615 118 1728 1325 1205 773

17 L SM450 4 9536 1583 180 1655 1237 1190 750

17 L SM450 5 9576 1633 133 1708 1329 1153 788

18 28 18 L SM450 1 9573 1772 149 1708 1453 1337 800

18 L SM450 2 9500 1750 144 1695 1437 1331 765

18 L SM450 3 9542 1757 142 1677 1447 1330 795

18 L SM450 4 9546 1747 123 1712 1453 1350 795

18 L SM450 5 9481 1835 176 1693 1489 1325 778

19 29 19 L SM450 1 9573 1772 149 1708 1453 1337 800

19 L SM450 2 9500 1750 144 1695 1437 1331 765

19 L SM450 3 9542 1757 142 1677 1447 1330 795

19 L SM450 4 9546 1747 123 1712 1453 1350 795

19 L SM450 5 9481 1835 176 1693 1489 1325 778

20 30 20 L SM450 1 9597 1828 204 1744 1449 1360 775

20 L SM450 2 9475 1745 204 1700 1371 1286 746

20 L SM450 3 9610 1747 213 1728 1361 1312 768

20 L SM450 4 9598 1773 214 1756 1383 1306 785

20 L SM450 5 9603 1822 236 1742 1412 1357 773

21 31 21 L SM450 1 NA 1823 109 1767 1538 1352 795

21 L SM450 2 NA 1881 091 1752 1615 1391 810

21 L SM450 3 NA 1751 109 1850 1456 1317 808

21 L SM450 4 NA 1848 148 1841 1517 1358 815

21 L SM450 5 NA 1857 142 1849 1531 1397 813

22 32 22A R RM20H 1 9650 1747 220 1620 1365 1350 756

22A R RM20H 2 9630 1760 227 1600 1373 1357 747

22A R RM20H 3 9630 1732 222 1600 1350 1317 752

22A R RM20H 4 9630 1782 219 1620 1401 1352 760

Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080

9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125

13B R RM20H M2

5 NA NA NA NA NA NA

15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076

17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111

19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120

SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

COCHRAN

OUTLYING LAB

SINGLE

GRUBBS

OUTLIER

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES

WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

(Gi)SINGLE GRUBBS

OF COCHRAN OUTLYING

WOULD EXCEED 29

Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Count

Machine

Lab Cod

Machine

Machine Type

Run No

Conditioned

Weight (mgtp)

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff Count

22A R RM20H 5 9610 1737 207 1620 1368 1342 769

33 22B R RM200A 1 9650 1725 208 1640 1353 1339 758

22B R RM200A 2 9620 1720 217 1610 1342 1328 757

22B R RM200A 3 9620 1705 221 1630 1321 1324 755

22B R RM200A 4 9610 1762 216 1640 1382 1360 770

22B R RM200A 5 9620 1745 213 1630 1369 1353 753

23 34 23 R RM20H 1 9440 1685 180 1620 1343 1370 720

23 R RM20H 2 9542 1696 175 1680 1353 1360 730

23 R RM20H 3 9505 1633 179 1622 1291 1319 740

23 R RM20H 4 9482 1613 177 1623 1274 1304 731

23 R RM20H 5 9494 1626 183 1651 1280 1318 741

24 35 24 L SM450 1 9614 1793 154 1700 1469 1258 800

24 L SM450 2 9568 1736 145 1633 1428 1238 785

24 L SM450 3 9545 1814 161 1698 1484 1278 785

24 L SM450 4 9480 1792 154 1733 1465 1220 783

24 L SM450 5 9589 1820 168 1705 1482 1323 805

25 36 25 L SM450 1 9676 1591 116 1592 1317 1125 761

25 L SM450 2 9604 1492 113 1572 1223 1130 719

25 L SM450 3 9534 1598 149 1924 1256 1201 719

25 L SM450 4 9618 1707 139 1818 1386 1289 772

25 L SM450 5 9679 1647 118 1809 1348 1223 783

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

1 1 1A R RM200A 1 4157 1005 3395 2813 2512 1134

1A R RM200A 2 4187 1037 3405 2809 2528 1103

1A R RM200A 3 4184 1013 3393 2831 2480 1123

1A R RM200A 4 4150 1029 3376 2783 2463 1107

1A R RM200A 5 4166 1035 3353 2795 2542 1089

2 1B L SM450 1 4487 1194 3460 2947 2450 1162

1B L SM450 2 4573 1252 3500 2970 2489 1147

1B L SM450 3 4537 1220 3490 2967 2464 1137

1B L SM450 4 4695 1294 3560 3045 2533 1141

1B L SM450 5 4463 1227 3410 2894 2456 1103

2 3 2A R RM200A 1 4005 792 3365 2877 2423 1062

2A R RM200A 2 4017 805 3310 2882 2519 1040

2A R RM200A 3 4021 807 3324 2882 2488 1067

2A R RM200A 4 3981 772 3289 2880 2490 1052

2A R RM200A 5 4048 811 3299 2907 2505 1075

4 2B L SM450 1 4379 962 3450 3071 2452 1152

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080

9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125

13B R RM20H M2

5 NA NA NA NA NA NA

15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076

17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111

19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120

SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

COCHRAN

OUTLYING LAB

SINGLE

GRUBBS

OUTLIER

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES

WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

(Gi)SINGLE GRUBBS

OF COCHRAN OUTLYING

WOULD EXCEED 29

Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

2B L SM450 2 4353 1053 3370 2964 2520 1132

2B L SM450 3 4518 979 3440 3195 2460 1178

2B L SM450 4 4394 1023 3500 3021 2460 1141

2B L SM450 5 4309 980 3410 2987 2469 1167

3 5 3 R RM200 1 4255 1021 3499 2885 2573 1165

3 R RM200 2 4246 982 3467 2918 2653 1131

3 R RM200 3 4225 937 3444 2944 2589 1153

3 R RM200 4 4301 967 3497 2984 2616 1153

3 R RM200 5 4207 961 3488 2898 2595 1158

4 6 4A R RM200A 1 4129 947 3411 2841 2500 1090

4A R RM200A 2 4091 925 3335 2833 2531 1080

4A R RM200A 3 4033 860 3328 2840 2464 1075

4A R RM200A 4 4114 928 3396 2846 2529 1075

4A R RM200A 5 4121 898 3376 2886 2541 1070

7 4B R RM20D 1 4102 907 3272 2868 2534 1120

4B R RM20D 2 4241 966 3366 2938 2624 1100

4B R RM20D 3 4214 935 3369 2942 2536 1115

4B R RM20D 4 4228 945 3398 2943 2510 1110

4B R RM20D 5 4124 903 3296 2892 2509 1080

9 5B R RM200A 1 4036 881 1705 2985 2490 1111

5B R RM200A 2 4019 824 1675 3023 2465 1121

5B R RM200A 3 3974 795 1679 3012 2509 1126

5B R RM200A 4 3938 772 1638 3001 2453 1187

5B R RM200A 5 4018 804 1687 3046 2484 1125

6 10 6A R RM20D 1 3979 884 3279 2767 2562 1138

6A R RM20D 2 4137 944 3394 2854 2570 1132

6A R RM20D 3 4041 889 3445 2792 2543 1141

6A R RM20D 4 4063 922 3401 2801 2569 1132

6A R RM20D 5 4161 975 3435 2843 2608 1137

11 6B L LX20 1 3910 887 3350 2688 2322 1178

6B L LX20 2 3993 919 3400 2734 2353 1175

6B L LX20 3 4019 959 3380 2722 2365 1174

6B L LX20 4 3863 892 3280 2643 2366 1163

6B L LX20 5 3895 871 3300 2695 2429 1160

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125

13B R RM20H M2

5 NA NA NA NA NA NA

15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076

17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111

19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120

SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

COCHRAN

OUTLYING LAB

SINGLE

GRUBBS

OUTLIER

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES

WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

(Gi)SINGLE GRUBBS

OF COCHRAN OUTLYING

WOULD EXCEED 29

Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

8 14 8 R RM20H 1 4081 953 2992 2828 2574 1101

8 R RM20H 2 3991 875 2922 2824 2481 1066

8 R RM20H 3 4069 951 2924 2825 2497 1062

8 R RM20H 4 4076 945 2970 2834 2587 1073

8 R RM20H 5 4003 919 3025 2782 2520 1074

9 15 9A L SM450 1 4401 1110 3440 2947 2512 1104

9A L SM450 2 4529 1160 3430 3026 2360 1111

9A L SM450 3 4486 1196 3610 2929 2389 1094

9A L SM450 4 4523 1173 3570 2994 2471 1083

9A L SM450 5 4415 1095 3420 2977 2381 1083

16 9B R RM200A 1 4127 939 3407 2862 2433 1072

9B R RM200A 2 4135 945 3478 2842 2509 1072

9B R RM200A 3 4093 931 3343 2828 2496 1084

9B R RM200A 4 4068 878 3401 2849 2446 1076

9B R RM200A 5 4063 943 3422 2778 2402 1083

10 17 10 L SM450 1 4625 1168 3500 3109 2351 1169

10 L SM450 2 4600 1066 3980 3134 2393 1109

10 L SM450 3 4620 1145 3450 3128 2366 1129

10 L SM450 4 4728 1176 3450 3205 2364 1133

10 L SM450 5 4764 1203 3510 3210 2391 1150

11 18 11 L SM450 1 5166 1530 3640 3272 2547 1113

11 L SM450 2 5152 1504 3560 3292 2564 1123

11 L SM450 3 5032 1463 3630 3206 2562 1139

11 L SM450 4 5147 1535 3740 3238 2619 1148

11 L SM450 5 4844 1408 3530 3084 2550 1114

12 19 12A R RM200A 1 4107 1025 3461 2735 2506 1118

12A R RM200A 2 4182 987 3422 2853 2519 1126

12A R RM200A 3 4160 1078 3436 2739 2530 1078

12A R RM200A 4 4114 989 3498 2775 2468 1085

12A R RM200A 5 4065 941 3442 2779 2508 1104

20 12B R RM200A 1 4274 936 350 29880 2538 1088

12B R RM200A 2 4308 945 358 30050 2530 1122

12B R RM200A 3 4256 938 358 29600 2497 1104

12B R RM200A 4 4201 906 353 29420 2514 1082

12B R RM200A 5 4247 949 342 29560 2537 1088

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125

13B R RM20H M2

5 NA NA NA NA NA NA

15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076

17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111

19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120

SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

COCHRAN

OUTLYING LAB

SINGLE

GRUBBS

OUTLIER

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES

WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

(Gi)SINGLE GRUBBS

OF COCHRAN OUTLYING

WOULD EXCEED 29

Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

21 12C L LX20 1 4690 1082 339 32680 2486 1122

12C L LX20 2 4622 1046 343 32330 2530 1139

12C L LX20 3 4654 1078 340 32360 2494 1110

12C L LX20 4 4642 1060 337 32450 2518 1080

12C L LX20 5 4612 1039 342 32310 2458 1125

13B R RM20H M2

5 NA NA NA NA NA NA

15 25 15 R RM200A 1 3949 827 3220 2800 2538 1085

15 R RM200A 2 3933 845 3234 2764 2502 1079

15 R RM200A 3 4041 856 3414 2843 2606 1101

15 R RM200A 4 3961 797 3375 2827 2562 1079

15 R RM200A 5 3902 791 3423 2769 2526 1076

17 27 17 L SM450 1 4280 1054 3590 4540 2350 1101

17 L SM450 2 4400 1049 3650 4540 2285 1124

17 L SM450 3 4323 995 3580 4540 2313 1105

17 L SM450 4 4498 1039 3740 4540 2359 1108

17 L SM450 5 4229 999 3550 4540 2298 1111

19 29 19 L SM450 1 4657 1142 3520 3162 2463 1061

Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120

SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

COCHRAN

OUTLYING LAB

SINGLE

GRUBBS

OUTLIER

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES

WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

(Gi)SINGLE GRUBBS

OF COCHRAN OUTLYING

WOULD EXCEED 29

Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Count

Machine Count

Machine Class

Machine Type

Run No

TPM (mgtp)

Water (mgtp)

Nicotine (mgtp)

NFDPM (mgtp)

CO (mgtp)

Puff count

19 L SM450 2 4526 1120 3520 3054 2501 1053

19 L SM450 3 4446 1085 3530 3008 2468 1073

19 L SM450 4 4561 1042 3530 3166 2497 1064

19 L SM450 5 4642 1086 3500 3205 2512 1045

20 30 20 L SM450 1 4612 1199 3480 3065 2472 1085

20 L SM450 2 4519 1127 3190 3074 2410 1076

20 L SM450 3 4474 1154 3610 2959 2476 1080

20 L SM450 4 4754 1273 3760 3105 2544 1120

20 L SM450 5 4722 1326 3720 3024 2544 1073

21 31 21 L SM450 1 5070 1282 3750 3413 2536 1136

21 L SM450 2 5029 1284 3710 3374 2511 1098

21 L SM450 3 4874 1259 3670 3248 2455 1126

21 L SM450 4 5029 1329 3730 3326 2577 1105

21 L SM450 5 5038 1272 3700 3396 2536 1141

22 32 22A R RM20H 1 4059 959 3205 2780 2511 1137

22A R RM20H 2 4019 957 3155 2746 2485 1097

22A R RM20H 3 4086 948 3295 2809 2478 1098

22A R RM20H 4 4022 949 3215 2752 2456 1115

22A R RM20H 5 4043 954 3240 2766 2420 1113

33 22B R RM200A 1 3995 938 3205 2737 2450 1119

22B R RM200A 2 3956 935 3135 2707 2455 1116

22B R RM200A 3 4005 871 3220 2812 2476 1084

22B R RM200A 4 4059 974 3220 2763 2435 1106

22B R RM200A 5 4062 912 3270 2823 2518 1107

23 34 23 R RM20H 1 3859 1602 6575 1599 2551 1076

23 R RM20H 2 3940 1630 6750 1636 2527 1067

23 R RM20H 3 3820 1656 6465 1517 2491 1053

23 R RM20H 4 3771 1616 6585 1496 2496 1062

23 R RM20H 5 3759 1489 6675 1603 2477 1074

24 35 24 L SM450 1 4741 1200 3510 3190 2431 1110

24 L SM450 2 4688 1177 3450 3166 2424 1110

24 L SM450 3 4776 1202 3620 3213 2454 1096

24 L SM450 4 4938 1315 3530 3270 2550 1068

24 L SM450 5 4769 1282 3510 3137 2493 1144

25 36 25 L SM450 1 4423 1002 3030 3117 2437 1091

25 L SM450 2 4431 1021 3050 3106 2463 1097

25 L SM450 3 4343 969 2930 3082 2401 1107

25 L SM450 4 4410 981 2970 3133 2246 1096

25 L SM450 5 4565 1046 2950 3224 2448 1120

SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

COCHRAN

OUTLYING LAB

SINGLE

GRUBBS

OUTLIER

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES

WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

(Gi)SINGLE GRUBBS

OF COCHRAN OUTLYING

WOULD EXCEED 29

Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










SCREEN OUT NON

VALID DATA

START OF LOOP

CALCULATE PRECISION

MEASURES

COCHRAN

OUTLYING LAB

SINGLE

GRUBBS

OUTLIER

PAIRED

GRUBBS

OUTLIER

END REPORT

ORIGINAL amp LAST

COMPUTED

PRECISION

MEASURES

WOULD EXCEED 29

ANY LABS

DROPPED IN

THIS LOOP

(Gi)SINGLE GRUBBS

OF COCHRAN OUTLYING

WOULD EXCEED 29

Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

COA205Cerulean

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

Nicotine IS Decanol

Water IS Ethanol

Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Methanol

Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

Ethanol

Water IS Ethanol

Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

Cerulean COA 205

Water IS Methanol

Water IS Ethanol

Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

19 SM450 Cerulean 598 2200 8821

int297

Cerulean COA 205

Water IS Ethanol

Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

22A RM20H Borgwaldt

Water IS Ethanol

Agilent 7890A

Water IS Ethanol

Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Lab Code

Water IS Ethanol

Nicotine ISAnethole

Water IS Ethanol

1 Introduction

2 Organisation

21 Participants

22 Protocol

3 Raw Data








6 Comparison



7 Conclusion










Documents

2016 Collaborative Study of CORESTA Monitor 8 (CM8) · 2016 Collaborative Study of CORESTA Monitor 8 (CM8) for the Determination of Test Piece Weight, TPM, Water, Nicotine, NFDPM,