UNITED STATES ENVIRONMENTAL PROTECTION AGENCY y · 2017-08-31 · UNITED STATES ENVIRONMENTAL PROTECTION AGENCY PHO'*-0 y REGION 7 25 FUNSTON ROAD KANSAS CITY, KANSAS 66115 gin©?Jakdte

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY

PHO'*-0y

REGION 725 FUNSTON ROAD

KANSAS CITY, KANSAS 66115gin©?Jakdte toy

ff]p> * _A3

DATE:a/9 /%9.

MEMORANDUM

SUBJECT: Data Transmittal for Activity #Site Description:

FROM:

TO:

Andrea Jirka Chief, Laboratory Branch, ENSV

Robert L. MorbyChief, Superfund Branch, WSTM

Attached is the data transmittal for the above referenced

site. This should be considered a ___ Partial or Complete

data transmittal (completes transmittal of ). If

you have any questions or comments, please contact Dee Simmons at

236-3881.

Attachments

cc: Data FilesAnn Melia, E&E/FIT

/

30305824

111 lllllll!Superfund

FT ELD SHEETU.S, EMv I RONMENTAL PRQTE'OT I ON AGENCY , REST ON ‘M 1

ENVIRONMENTAL SERVICES DIN. 25 FUNS70N RD. KANSAS CITY, KS 661.15

s Sits Name: WATERLOO COAL GAS ; Location: WATERLOO I A

Site Number: Site Corje:

!_• d .L i e I I \ B

Sample Number:: 1 L '1 (^0/ SSMQ #:

Media DUST „

Sample split

(Lirele one):RIN3ATE , SEDIMENT,,

(circle one): CjM-p

MATER

NO

OTHER:

Sample Container Tag Color- Preservative : Anal va-is Requested

2-40 ML VIAL. r j.. IMF ■Oh8 OZ.JAR S OZ.JAR

GREENPURPLE

CYANIDE BN A

Depth : .. Pan #: _ ... All quote; ]

Samp] era :......£ft.\C........ ......... .....

COMMENTS OF FIELD PERSONNEL

j i t & :rip tion LocAt\o>^ \&

IBM.PC

u.. s..I RONMENTAI.

■IV I RONM SERVICE

FIELD SHEET■I T ft L P R 0 ! E C T 10 N ft 6 E N C Y , R E G I □ i J V DIV. 25 R.JIM8TON RD. KANSAS CITY 115

Site Name Localion

WATERLOO Clift WATERLOG I ft

Lj H •: S.i. t.e Number ; Site Code:

: Collected 10 : J.iL. Day : Tim Leader HESS

C_" a mi pie

Samd1e Med iDUST

s a ii i p 1 e SpJ x

Sample C o n t a

2--40 Ml... "I8 OZ . JAR8 GZ „ J R R

jrnber: TKSBS^J

( c i r c 1 e o n e ) : RINSATE, SEDIMENT,

(circle one

: Taq Color : Pre

L I ME GREEN

SMG ft:

WATER, OTHER:

NO

Ana I i ' 0 q f

Depth : £ f© 6.

Samp 1 ere:

an # : A1iquot


site Description

IBM--PC

Location

FIELD SHEETU .S. E NI R 0 NIIE H T A l... F' E 0 TEC T I Q N ACE I! C Y „ R EC TO U V 1 I

ENVIRONMENTAL. SERVICES DIV. 25 FUNSTON RD, KANSAS CITY, t 661.15

; Site Name:: Location:

WH TER LOO (...UHL • ’ A.WATERLOO 1A

Site Number:Site Code:

: Collected: YR: 88 MO: |X. Day T i m e : L e a d e r : E , H E S S

: Samp] e Number : TK988^3 SMO #:

Saitipl e lied la (circle one ) :CcO i'l^ DUST,, RI NS ATE, SEDIMENT, WATER, OTHER:

Sample Split (circle one) : .r) NO

....... . .

bdiiipJ 8 '.'ontainer : Too Color :: Preservative : Anal yeie !"•'! 0 q U. tf ti-1.'. t_v cJ

2.40 Mi... ' 'Imi8 QZ.JAR 8 Li /. i.i AR

I... . OF

OF'FEN oiTO"'!.. E

VO ACYANIDEENA

Depth: Pan #: _ __ A1iqucts:_ /

a m p 1 e r a : __...fc’iMc...Hess... .. _... ....

C 0 FI M E N T 5 0 F" F J E L D P E R S 0 N N E!...

Site Description LeeA"P OAi

IBM.PC

FIELD SHEET1.1 „ S „ ENVI R0NI iENTftL PR01'ECT I0N ABENCY , REG I. 0N V I I

ENVIRONMENTAL SERVICES DIV. 2D FUNSTON R.0, KANSAS CITY, KS 66115

5its Mams: WATERLOO COAL GAS Location: WATERLOO IA

Site Number: Site Code:

Collected: YR : S3 MG : jX. Day : Time : jSjpL Leader: E „ HE!

Sample Number; TK9B8$S^y Slu #;

»le Media (circle one): rvuiY. DUST, RING ATE, SEDIMENT, WATER, OTHER;.

!amp]e Split (circle one); (Ec NO

..: Sample Contoj. ner T a q C o 1 o r :: i-' r ess r v stive : Ana 1 vs is Requ.ee ted ;

: 2.40 Mi... VIA!.. LIME : ; VGA; 3 OZ JAR BREEN : : CYANIDE7. U ‘ .] -i J AR PURPLE :: :: BN A

De Ran #:pth ;.^4t>6

amp]ere: ..Eric Bevs

All quote ;

B ofe» Qstec&Ji.

COMMENTS OE FIELD PERSOMNEi..

sits Description:

IBM.PC

FIELD SHEETU.S., ENVIRONMENTAL PROTECTION AGENCY, REGION VII

ENVIRONMENTAL SERVICES DIV. 25 FUNSTON RD „ KANSAS CITY, K3 661.15

; Site Name: WATERLOO COAL GAS : Location: WATERLOO IA

Site Number: Site Lode:

Collected: YR: SO MO: M. Day:

S a mple N u m b e r : T K 9 B 3 ST

Me Media (circle one):JlLj) DUST, RI NS ATE, SEDIMENT,

Sample Split (circle one): Q/ESj

Time: Leader: E.HESS

SMO # :

WATER , OTHER :.... ......

NO

Sample Container : Tag Color :: Preservative : Ana. lye is Requested

2 .40 ML VIAL0 OZ.JAR3 OZ.JAR

i... I ME

GREENPURPLE

VGACYANIDESNA

Depth Pan # :

SamplersCric_Hess

Aliquot (

COMMENTS OF FIELD PER SONNE!...

s i t e D e s c r i p t i o n lotATl

IBM.PC

U.5 - ENVIRONMENTAL I RON ME NT AL SERVICES DIV

FIELD SHEETF::' R 01 E C T 10 N ABE N C'V , REGION VI I 2D FI JNS T ON RD. KANSAS CITY, t 11 5

: Bite Name: WATERLOO COAL Of: Loc a t i on : W ATERL..00 IA

.i.te Number: Site Code:

Collected: YR : S3 NO : Q,. Dav : (f | T

Sample N i. j m b e r : T K 915 8 0<j5 £>

.ime Leader: E . HI-Ss

SNO #:

Sample Media (circle one):DUST, RINSATE, SEDIMENT, WATER, OTHER:

NOSample Split (circle are)

Sa.rrip 1.e Container fag Co 1 or : r ressrvativg : Analysis

40 Ml... VI OZ . JAR U Z . '. I A R

GREENPURPLE

CYANIDE BN A

j

Depth:

Samp1«

an #: , t a

_5©!o_ Ovic/Geii

COMMENTS OF FIELD PERSONNEL..

Site Description 1©cm-i©o 3b

IBM.PC

IJ .. S .. ENv I rgnmentai [ R 0 M !1 E: N T A I... S E R V IC E S DI'

FIELD SHEETPROTECTION AGENCY, REGION VII25 FUNSTON RD. KANSAS CITY, KS 661.15

6ita Mams: WATERLOO COf Location: WATERI....iJ0 IA


Col I sc ted :

::.t)n .j .1. tr i -ihi J.ji.-.-f r

MO : \2,. Day : Time: \(M^ Leader: E . HESS

TK?BS^7 SMO # :

SamipN 'u 1] D ,

Media (circle onej;DUST, RINSATE, SEDIMENT, WATER, OTHER

6 a i i 1 p1e S plit (circIe NO

Tag Color :: Preservative : Analyst

2.40 Mi... VIALy u * . J r-R CYANIC

BN A

ed

Depth : fc''. Pan # :........ Aliquots:

Samplers :.....B©t> 0\JCrfc.l!r..........


Site Description LocATfoO Ms

IB |-1-PC

EN\U.S. ENVIRONMENTAL

IRONMENTAL SERVICES DIV

FIELD SHEETPROTECTION AGENCY, REGION VII25 FUNSTON RD. KANSAS CITY, KS

: Site Name: WATERLOO COAL GA: L o c a t ion : W A T E R I.... 0 0 IA

.1 te Number: Site Code:

Go 11ected: Yh ™: |3L Uav U- T .i m ..eaaer

S ampl e N u rn b e r : TI

pie

■i p 1 e

Ned is.

DUST ,

S p lit

(c: i rc 1 e one ) : RINSATE, SEDIMENT,

(circle one)

bMu #:

WATER, OTHER:

NO

E , HE

Sample Container : Tag Color Preservati An

2-40 ML VIAL 8 OZ.JAR b O l u 2 A R

L I ME

GREENPURPI..E

VGACYANIDE BN A

Depth Pan # A1 i quc

Samp 1ers:

COMMENTS OF FIELD PERSONNEL.

>i t Description LocAT toO

I.J.S. ENVIRONME IRONMENTAL SERVICE?

FIELD SHEETTAI._ PROTECTION AGENCY, REGION VII DIV. 25 RJN3TGN RD. KANSAS CITY, I 1.15

” ,j.t te NaiiiVr:: : Location

hater

HATERLu ' A Site Number;

Site Code:

Co 1 .1 ec ted : YR : 38 MO ; Day : "F

Sample Number: TI<9B8^0^

Sample Media (circle one):''Tot}. DUST, RINSATE, SEDIMENT

,i m e Leader; E.HESS

SMlJ # :

Sample Split (circle one)

WATER,

NO

OTHER

itaine r ■ a +■ Ana I

GREENPURPLE

VGAY A N I D E

n l\! A

1)e p t i"i: JO. F’ an I):

Samp 1 ers:...... ..........tfesY.

A1 iquot \


pt ion LfcCATIOJ^ 58,

IBM.PC

ENV I RONMENTALE N VIE G NIIE N T A L S E R VIC E S DIV

FIELD SHEET

PRGTECT I 0N ABE!NCY ,, REG 10N V I I .25 FUNSION RD. KANSAS CITY, KS 66115

: bits I'laiTie: WATE!vLOQ CUAL 6 A: Location: WAT E R0 G IA


uo i t!i_ i.eu : t r\ : oo uu : ouy :

Sample Number : TK9B8^ |$

i xme : sprjXnf- Ledusr • ■ ntoa

SNO # ;

lied ia DUST ,

(c: i r c 1 e o n e ) :RINSATE, SEDIMENT, WATER, OTHER:

S a in pie b p I it (ci r els one! NO

m p 1. e C o n t aine r ;• Tag Color rressrvative : Ana Iysis Re qu ested

2-40 M i... VIAL. : i... IMF :: : OCA8 GZ .JAR : GREEN : : CYANIDEy \ j l . JAR ; PURPLE :: :: BN A

D/ pin: P a n # a

Samp3.er^ r Eiztc-

A1 iquote: K*.


b i t e 15 e s crip t i o n LocAT/o/o 5 3:

IBM.PC

FIELD SHEETU . S . ENVTR0NHIDHTAL PR0TECT 10N AGENCY, REGION HU

ENVIRONMENTAL SERVICES DIV. 2D FI. INS TON RD „ KANSAS CITY, KS 661.15

: Sits Marne: WATERLOG COAL GAS : Location: WATERLOO IA

bite Number: Site Code:

Collected: YR : 88 MO : |2_ Day : .$2. Time:/.(jJ/SL. Leader: E.HESi

Sample Number: TK9UF;{pf |

le Media (circle one):

SMO #;

DUST, RINSATE, SEDIMENT, WATER, OTHER:

Sample split, (circt :;ne ) : rib NO

m p ]. e Coritai nor : Taq Co ) or •; F'reservative : Analysis Requested s

2-40 Hi... V I A1... : I... THE : VGAS GZ JAR : GREEN : : CYANIDE8 GZ L.i A R : PURPLE : :: BN A

Depth: O Pan tt : _____ A1 iqu.ots:

Samplers:___ _VatTV „ RoUERTV.. ____


3ite Description: LocATfoU £>S

IBM-PC

U.S. ENVIRONMENTAL -JVIRONMENTAL SERVICES DIV

FIELD SHEET PROTECTION AGENT 25 FUNSTON RD.

, RFC I Oil VII i‘i i I hi S C I 1 V , K t: .11 5

* Site N a ill A

: LocationWATERLOO COA WATERLOO IA

3 A i: ito Number: Site Code:

Collected: YR : 88 MO: XZ Day ■■(pz Time: 4^3^.

Sample NLimber: TK9B8^ | %, SMO #:

Sample Media (c: i rc .1 e one ) :(Trilj): DUST,, RI NSATE, SEDINENT , WATER, OT

Sample split (circ1e one): Y ES

11 a i n e r or’ Preservative : Analysis

2.40 Mi... VIAIG OZ.JAR 8 OZ.JAR

GREENPURPLE

CYANIDE BN A

d

Depth:

Samp] ei-

A 1 i. q u. o t 5


>ite Description:LocA-nou T S

JaiMe* L

?.0. Z\S7

loo ,Toto^ SfTlW

IBM.PC

u. s „ IRONMENTAI.

ENVIRONMENTAL SERVICES DIV

FIELD SHEETPROTECTION AGENCY, REGION VII25 FUIM3T0N RD. KANSAS CITY, KS 66115

: Site Name: Location

L'Jf-1 rERLUL) U'.'riL AM WATERLOO IA

its Number; Site Code:

Collects d: YR: 88 M Q:[X Time Leader: E.HESS

mp 1 © id urn her : TK9BSp»3 SMO #:

Med .1 a (c i rc .1 e one) :DUST, R I NS ATE, SEDIMENT, WATER, OTH

SP1 1.1 (c ire 1 e one) : (ois) NO

on t a i n e r : Taq Color' : Preservative :

i... V IA i... « i... IMF :: ;AR ; GREEN : :AR PURFT..E ::

Ana lysis Requested

VGACYANIDE BN A

D'-pti.: Ran ti :......... Aliquots:..

Samp lers :... ..PaT7Y_.RsBefeT*...........


S i t e D e s c r i p t i o n Location 8S

IBM-PC

IJ. S El l'-' IRGNMENTAL SE

FIELD SHEETR 0 N M E N T A I... P R 0 "I E C TI ON A 6 E N C Y , REGION VII VICES DIV. 25 FUNSTON RD. KANSAS CITY, KE 1 .15

3 .1. L e N a m a : N A I E K!.._ U lL c; c a t i o n : W A T E R I.... 01"

COAL 6t; IA


Collected: YR : S3 MO:J2L Day ;

Sample Number : T Kc? 0^ 11|= 11$T .i m e : /1 w(D L e a d e r

SMO #:

E.HESS

Sample Media (circle one):(OJIUS DUST, RI NS ATE, SEDIMENT, WATER, OTHER:

Sample split (. circle one) : NO

ntdJ.ner Taq Color e i Ana 1 vale Requested

* 2.40 Hi... VIAL. : 1... IMF:

“ 3 OZ.JAR : GREF.N3 OZ.JAR s PURF

CYANIDE BN A

Li r» Pan # Allquot 5

Samp lore :............. .<4 •..jfrifcVTV


s i t e D e s c r i p t i o r (Oa

IBM.PC

LdcATJojO

FIELD SHEETU.S. ENVIRONMENTAL PROTECTION AGENCY, REGION VIl ■

ENVIRONMENTAL SERVICES DIV. 25 FUNSTON RD. KANSAS CITY, KS'66115'

3 i t s Name: WATERLOO C u A L G A S Loc a-t i on : WATERLOO IA


Collected: YR: SS MO: |£L_ Dav: <t>2. Time: (MS' Leader: E.HESS

Sample Number: TK9B3^ SMO #:

1 e Med ia (circle one ) :^DlO DUST, RINSATE, SEDIMENT, WATER, OTHER:___________

Sample split ( c i r c 1 e o n e ) : (Y E S NO

: Sample Container 3 T-aa Color ;; preservative : Analysis Reqij.ested

2-40 ML VIAI 3 OZ.JAR 3 OZ.JAR

!. [ME GREEN n ipRLE

VGACYANIDE BN A

Depth: Ran # :_________ A1 iqlaots : ^

Samplers: PaTTV.RsftEJLt!*


Site Description l0CAT/0A^

IBM-PC

U.S. ENVIRONMENTAL ENVIRONMENTAL SERVICES DIV

FIELD SHEETPROTECTION AGENCY., REGION VII. *25 FUNSTON RD. KANSAS CITY, KS 661i5

: Sits Name: WATERLOO COAL oAS: Location : WATERLOO IA


Collected: YR: 88 MO: \*L Dav : fftt Time : \\\tj> Leader: E . HESS

Sample Number: TK9B8^ltSMO #:

Samp1e Media (circle one):£o?£, DUST, RINSATE, SEDIMENT, WATER, OTHER:

Sample Split (circle one) NO

: Sample Container : 'Tag Color : Preservative : Analysis Requested

2-40 ML VIAL : LIME : VO A■2j L; Z ■ J (“iF* : GREEN ; : CYANIDES OZ.JAR : PURPLE ; : BN A

Rep t h : Pan # : .....

Samplers :______ ElR' C,___ VV0S.S>

A1 iquot


Site Description LocAtioJO

IBM-PC

FIELD SHEETU.S. EN VIRONMENTAL PROTECT I ON AGENCY , REGION VIL 1

ENVIRONMENTAL SERVICES DIV. 25 FUNSTON RD. KANSAS CITY, KS 66115

Sits Name: GATERL0u CUAL GAS Location: WATERLOO IA


Collected: YR: 88 MO: D a v: Time: \YL& Leader: E. HESS

Sample Number: TK9B8^|*? SMO #:

Sample Media (circle one):flUlt), DUST, RING ATE, SEDIMENT, WATER, OTHER:___________

Sample Split (circle one): NO

: sample Container Tag Color : Kreservative : Analysis Requested

2-40 ML VIAL 3 OZ.JAR S 0L .JAR

L.1 MEGREENPURPLE

VO ACYANIDE BN A

Depth:

Samplers:

Pan # : A1 i q lio t s :

COMMENTS OF FIELD PERSONNEL,

Site Description Loc.at/ojo

U.S. ENVIRONMENTAL ENVIRONMENTAL SERVICES DIV

FIELD SHEETPROTECTION AGENCY', REGION VIT25 FUN5T0N RD. KANSAS CITY, KS 66115

: Sits Name: WATERLOO COAL GAS : Loca-tion: WATERLOO IA

Site Number; Site Code:

Coll cted: YR : 06 Mi s: f%_ Day : Time : | [M 0 Leader

Sample Number: TK9E<8 |^ SMO #:

1 e Media DUST,

(circle one): RINSATE, SEDIMENT,

Samp1e split (circ1e one)

WATER, OTHER:.

NO

HESS

i Sample Container ; lYg Color : preservative : Anal e q u e s t e d

2-40 ML VIAL S OZ.JAR S OZ.JAR

lime

GREENPURPLE

VOACYANIDE BN A

Depth : Pan #:________ Aliquots:

Samp 1 ere :______ __________.ô8EED»


Site Description Loct\Tio& 13 S

IBM-F'C

ENVIRONMENT ALENVIRONMENTAL SERVICES DIV

FIELD SHEETPROTECTION AGENCY., REGION VIL 125 FUNSTON RD. KANSAS CITY, KS 66115

: Sits Name: WATERLOO COAL GAS Site Number:: Location: WATERLOO IA Site Code:

: Collected: YR: 88 MO: | Dav: Time: (MS' Leader: E.HESS

SMO #:

WATER, OTHER:_

NO

Sample Number: TK9B5(j$J^

■Sample Media (circle one):£oTl), DUST, RINSATE, SEDIMENT,

Sample split (circle one): fYES

: sanip 1 e Cunt.ainei’ lor : Preservative : Analysis Requested :

-40 ML VIAL : LIME• J OZ.JAR : GREENs OZ.JAR : PURPLE

VGACYAN IDE BN A

Depth: Pan #: _

Samplers: ___£Tttlc

A1iquote:


Site Description: LocAtioO

IBM-PC

IJ. s.RONMENTAI.

ENVIRONMENTAL SERVICES 0 f.'

FIELD SHEETPROTECTION AGENCY, REGION VII25 FUNSTON RD. KANSAS CITY, £>6115

: Site Name: WATERLOO COAL... GA: Location : WATERLOO IA

it.e Number: Site Code:

: Co I 1ected : YR :

bample N um t

NO : Q,.

- : TK9Bi

ime : Le

SNO #:

amp I e IL ,

amp 1 ■:

Media (circle DUST, RINSAT

S plit (circle

OTHER

HI

mple Container :: Tag Color : Preservative : Analysis Requested

: LIME ICE C :: GREEN ; ICE ' MaO# A

: PURPLE ; ICE £•

2.40ML VIALS1 L CUB I 80 0Z .JUG

Depth:___

Samp j ere:

VO ACYAN IDE BN A

Pan A1 i. quote : _

a4rsT-Z

C 0 H M E N T S 0 F F I EI....D P EPS O N N E L

Site Description: CO«-Verloo hAuAicfp W LOeW CtOMLO')

'&f/r Z/nttf */3 Gftv)

. d?i\.y.... Cy**'$c - _U*iL VV^ siCu... ut ... /©df ^ _

&/

IBM-PC

FIELD SHEETL.J. S . E N VIR 0 N i i E N T A I.... p R G T E C T I ON AGE i IC Y , REGION VII

ENVIRONMENTAL SERVICES DIV. 25 FUNSTON RD. KANSAS CITY, KS 66115

; Site Name: WATERLOO CO A!... GAS : Location: WATERLOO IA


Co 11 ec ted : YR : 38 iiO : J 2. Day : f Time :____ Leader : E . HESS

8am|j 1 e NuiTibsr : TKV 8P

Sample Media (circle one'!:B 0 I L D U ST, RI N S A T E , S E D I h i E N T ,

II a Hi pie S p lit ( c i r c I e o ne; ; TO

SMO #;

WATERJ

NO

OTHER:

Sa!np1e Container i: T a q C o J o :: Preservative : An a 1 ys i

2-40ML DIALS : I...IME ICE 6,.,. : VGA1 L. CUB I : GREEN : ICE 8 ,. ; CYANIDE80 0Z.JL1B r. PURPLE :: ICE & . . : BN A

Depth P a n if A1 i q i.j. o t s :

Oadip 1 ere :

C 0 i i M E N T S 0 F F IE I , D P E R S 0 N N E I...

Site Description Fie\9 BWW

:

I Bivl ™ PC

A N A L Y SIS TYPE: CYAN 11) E

TITLE tk?B7,tk9e TK9B8..AD: EPA

|i AMPLE PiREGION VIJEP : ANAL YS T /E N TR Y K LC

MATRIX: SEDIMENT METHOD: 3301803 REVIEWER:

UNI TS CASE : DATE :

MG/KG

0.1./0 DATA

SAMPLE NO. RESULT DILUTION VOLUME WET WEIGHT % SOLIDS

TK9B8001 1 . 0

CYANIDEANALYSIS TYI:>!

TITLE: AB: El SAMPLE

TK9B7,TK9B0 ‘A REGION Oil PREP : ANALYST/ENTRY: KI..C

MATRIX: SEDIMENT METHOD: 3351803 REVIEWER:DATA FILE: KLC

UNITSr'Acrr .

DATE

MG/KG

01/1 0/S?

SAMPLE NO RESULT DILUTION VOLUME WET WEIGHT SOL IDS

TK9B8002 IS , 1 . 0TK9B30 0 3 SS . 1 . 0TK9B8004 2 S 0 . 1 . 0TK9B8006 16 0 ■ 1,, 0TK9B8007 1.1. , 1. . 0TK9BOOOO 0,0 1,, 0TK 91580 0 9 130 . 1 . 0TK9B80i0 24 . 1, 0TK9B0 0 IJ. 31 . 1 , 0T l< V B 8 0 .1.2 , 00 1,, 0TK9B8013 77 1 . 0TK7B3014 1,0 1, 0TK9BS0 IS 4 . S 1 . 0

TK9BS0 1 i, ISO , 1, 0TK9B0017 '•> 1 , 0TK9B801S 4,0 1, 0TK9BS01? 4, e i . 0

TITLE: TK9B7 LAB: EPA REG SAMPLE PREP:

SAMPLE NO.

TK9B8005

ANALYSTS TYPE: CYANIDE

,TK 9BO MATRIX: SEDIMENT UNITS: MO/KGTON Oil METHOD: 335IS03 A CASE :

DATE:.. ANALYST/ENTRY: KLC REVIEWER:DATA FILE: KL.C

Oi/i i/S(:

RESULT DILUTION VOLUME WET WEIGHT X SOLIDI

PS, i.0

CYANIDEANALYSIS TYP

TITLE: TK9B8 MATRIX: WATER..AD: ERA REGION VII METHOD: 33S1.U03

PIAMPLE P R EP : \£r__ ANALYST/ENTRY: KLC REVIEWER :

DATA FILE: KLC

UNITS; HO/I... CASE :DATE: 0 i/0 S/89

SAMPLE NO,

TK9B8102

RESULT

,0 030 U

DILUTION

.1. , 0

ANALYSTS TYPE: CYANIDE

TITLE h[...AD : SAMP I.

: TK9D8ERA REGION LIT E P E E P : _ ^ ANALYST/ENTRY:

MATRIX: WATER METHOD: 33SiWO 3

KLC REVIEWER:DATA FILE: KLYf

UNITS: MG /I CASE :DATE: 0i/0'

SAMPLE NO. 3ULT DILUTION

TK9B810SE 0 0 3 0 U i , 0

3/09

VOLATILESANALYSIS T'Y'PEr

i i ! i...L "H j I::.K ER vUL.A i I i....EH LAB? RED HEN TIT EPA

Hi"' L.L:. I-'1-' I:::.!- “ AN AL Y i /h.N ! K VV......

MATE IX. WhTER I'■'!!::: I HUB !; 3 LHv.'

DNE REv I EERIERDATA FILE ? D11

SAMPLES

L i-iU R Li l i E i H •, N I:::.

PPOMOMETHANEvinvl ChlorideCHlOROETHANEi"‘IE"EHV!...Ehil::: (EH HER I DE

ALE 70!PLL,Ti"i H i...i ■ ■! :: i;....!'" .1. : E.

1 , :i ..D T UHL ORijHERE

1 „ !. L- 1... ,■■■!!... E'!" ■.'■ i ■! '■■■; N.H .!. :...

1;j: ■ ■AhL'I ilH

i-PR0!:■;-■■■ HRl-TR

LITi....L!p:J?:: i

■■■■ HjT Ai'-.ipi'.'i:::’

j , :: ..T A I OH:...C A;:"! A1"! A A NR

i! .j'.'v.J'' ’... !. ^r. .;

RLE: it: 1 -.Li- iL.C);;:;:OHEEri-EOTE , -t- t r:Aj.. opnr;oE'ail r

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ANALYSIS TYPE: SEMIVOLAT1LES-PAGE 1

TLE: WATERLOO AB: TMA/NORCAL

COAL GAS MATRIX:METHOD:

SEDIMENT9303M02

UNITSCASE:

UG/KG11157

SAMPLE PREP: ANALYST/ENTRY: 1PLC REVIEWER: arny______ DATE : 02/02/8!

SAMPLES TK9B8001

DATA FILE :

TK9B8002

P64

TK9B8003 TK9B8004

PHENOL 12000 U 12000 U 11000 U 12000 UBIS(2-CHL0R0ETHYL) ETHER 12000 U 12000 U 11000 u 12000 U2-CHL0R0PHEN0L 12000 U 12000 U 11000 U 12000 u1.3 DICHLOROBENZENE 12000 U 12000 U 11000 U 12000 u1,4 DICHLOROBENZENE 12000 U 12000 U 11000 U 12000 uBENZYL ALCOHOL 12000 U 12000 U 11000 U 12000 u1.2 DICHLOROBENZENE 12000 U 12000 U 11000 u 12000 u2-METHYLPHENOL 12000 U 12000 U 11000 U 12000 uBIS <2-CHLOROISOPROPYL)ETHER 12000 U 12000 U 11000 U 12000 U4-METHYLPHENOL 12000 u 12000 U 11000 U 12000 uN-N1TROSO-DIPROPYLAMINE 12000 u 12000 U 11000 U 12000 uHEXACHLOROETHANE 12000 u 12000 U 11000 U 12000 uN1TROBENZENE 12000 u 12000 U 11000 U 12000 uISOPHORONE 12000 u 12000 U 11000 U 12000 u2-NITRGPHENOL 12000 u 12000 U 11000 U 12000 u2.4-DIMETHYLPHENOL 12000 u 12000 U 11000 U 1 2000 uBENZOIC ACID 60000 u 57000 U 53000 U 59000 u

(2-CHLOROETHOXY) METHANE DICHLOROPHENOL

12000 u 12000 U 11000 U 12000 u12000 u 12000 U 11000 U 12000 u

1,2.4-TRI CHLOROBENZENE 12000 u 12000 U 11000 U 12000 uNAPHTHALENE 1300 M 770 M 11000 U 3800 M4-CHLOROANILINE 12000 u 12000 U 11000 u 12000 uHEXACHLOROBUTAD1ENE 12000 u 12000 U 11000 u 12000 u4-CHLORO-3-METHYLPHENOL 12000 u 12000 U 11000 u 12000 u2-METHYLNAPHTHALENE 2400 M 12000 U 11000 u 9600 MHEXACHLOROCYCLOPENTADIENE 12000 U 12000 U 11000 u 12000 u2.4,6-TRICHLOROPHENOL 12000 U 12000 U 11000 u 12000 u2,4,5-TRICHLOROPHENOL 60000 U 57000 U 53000 u 59000 u2-CHLORONAPHTHALENE 12000 u 12000 U 11000 u 12000 u2-NITROANILINE 60000 u 57000 U 53000 u 59000 uDIMETHYLPHTHALATE 12000 u 12000 u 11000 u 12000 uACENAPHTHYLENE 3300 M 1200 M 11000 u 1 2000 u3-NITROANILINE 60000 U 57000 U 53000 u 59000 uACENAPHTHENE 12000 U 12000 U 11000 u 3300 M2.4-DINITR0PHEN0L 60000 U 57000 U 53000 u 59000 u4-NITROPHENOL 60000 U 57000 U 53000 u 59000 uDlBENZOFURAN 12000 u 12000 U 11000 U 1500 M2. 4-DINITROTOLUENE 12000 u 12000 u 11000 u 12000 U

ANALYSIS TYPE: SEMIVOLATILES-PAGE 2

FlTLE: WATERLOO COAL GAS

LAB: TMA/NORCALSAMPLE PREP: ANALYST/ENTRY

MATRIX: SEDIMENT METHOD: 9303M02

PLC REVIEWER: ,~,_r_nvDATA FILE : P65

UNITS: UG/KG CASE: 11157DATE: 02/03/89

SAMPLES TK9B8001 TK9B8002 TK9B8003 TK9B8004

2.6-DINITROTOLUENE 12000 U 12000 U 11000 U 12000 UDIETHYLPHTHALATE 12000 U 12000 U 11000 U 12000 U4-CHLOROPHENYL PHENYL ETHER 12000 U 12000 U 1 1000 U 12000 UFLUORENE 2300 M 12000 U 11000 U 6800 M4-NITROANILINE 60000 U 57000 U 53000 U 59000 U4.6-DINITR0-2-METHYLPHEN0L 60000 U 57000 U 53000 U 59000 UN-NITROSODIPHENYLAMINE 12000 U 12000 U 11000 U 12000 U4-BROMOPHENYL PHENYL ETHER 12000 U 12000 U 11000 U 12000 UHEXACHL0R0BEN2ENE 12000 U 12000 U 11000 U 12000 UPENTACHLOROPHENOL 60000 U 57000 U 53000 U 59000 UPHENANTHRENE 11000 M 830 M 11000 U 61000ANTHRACENE 1900 M 12000 U 11000 U 12000 UDI-N-BUTYLPHTHALATE 12000 U 12000 U 11000 U 12000 UFLUORANTHENE 5800 M 1500 M 650 M 6900 MPYRENE 10000 M 3800 M 6500 M 1 1000 MBUTYL BENZYL PHTHALATE 12000 U 12000 U 11000 U 12000 U3.3’ DICHLOROBENZIDINE 25000 U 24000 U 22000 U 24000 U^^JZO ( A ) ANTHRACENE 12000 U 12000 U 11000 U 12000 U

(2-ETHYLHEXYL)PHTHALATE 12000 U 12000 u 11000 u 12000 UCHRYSENE 4200 M 2100 M 1700 M 14000 JDI -N- OCTYL PHTHALATE 12000 U 12000 U 11000 U 12000 UBENZO(B)FLUORANTHENE 1600 M 1500 M 860 M 6300 MBENZO(K)FLUORANTHENE 2500 M 2200 M 590 M 4500 MBENZO(A;PYRENE 2800 M 2100 M 980 M 5300 MINDENO(1.2,3-CD)PYRENE 12000 U 12000 U 11000 U 2100 MD1BENZO(A.H)ANTHRACENE 12000 U 12000 U 11000 U 12000 UBENZO(G,H.I)PERYLENE 1400 M 12000 U 11000 U 12000 U


■ TLE: WATERLOO COAL GAS MATRIX: SEDIMENT UNITS : UG/KGLAB: TMA/NORCAL METHOD: 9303M02 CASE: 11157SAMPLE PREP : ANALYST/ENTRY: PLC REVIEWER: PnCOY DATE: 02/02/

DATA FILE : P64


PHENOL 24000 U 24000 u 13000 u 24000 UBIS(2-CHL0R0ETHYL) ETHER 24000 U 24000 U 13000 u 24000 u2-CHLOROPHENOL 24000 U 24000 U 13000 u 24000 U1.3 DICHLOROBENZENE 24000 U 24000 U 13000 U 24000 u1,4 DI CHLOROBENZENE 24000 U 24000 U 13000 u 24000 uBENZYL ALCOHOL 24000 U 24000 U 13000 u 24000 u1.2 DICHLOROBENZENE 24000 U 24000 u 13000 U 24000 u2-METHYLPHENOL 24000 U 24000 u 13000 U 24000 uBIS(2-CHL0R0ISOPROPYL)ETHER 24000 U 24000 U 13000 U 24000 u4-METHYLPHENOL 24000 U 24000 U 13000 U 24000 uN-N1TROSO-DIPROPYLAMINE 24000 U 24000 U 13000 u 24000 uHEXACHLOROETHANE 24000 U 24000 U 13000 u 24000 uNITROBENZENE 24000 U 24000 u 13000 u 24000 uISOPHORONE 24000 U 24000 U 13000 u 24000 u2-NITROPHENOL 24000 U 24000 U 13000 u 24000 u2.4-DIMETHYLPHENOL 24000 U 24000 U 13000 u 24000 uBENZOIC ACID 120000 u 120000 U 62000 u 110000 u

2-CHL0R0ETH0XY ) METHANE 24000 u 24000 U 13000 u 24000 uDICHLOROPHENOL 24000 U 24000 U 13000 u 24000 u

1,2.4-TRI CHLOROBENZENE 24000 u 24000 U 13000 u 24000 uNAPHTHALENE 51000 13000 M 13000 u 1300004-CHLOROANILINE 24000 U 24000 U 13000 u 24000 uHEXACHLOROBUTADIENE 24000 u 24000 u 13000 u 24000 u4-CHLORO-3-METHYLPHENOL 24000 u 24000 U 13000 u 24000 u2-METHYLNAPHTHALENE 22000 M 9900 M 13000 u 170000HEXACHLOROCYCLOPENTADIENE 24000 U 24000 U 13000 u 24000 u2.4,6-TRICHLOROPHENOL 24000 u 24000 u 13000 u 24000 u2,4,5-TRICHLOROPHENOL 120000 U 120000 u 62000 u 110000 u2-CHL0R0NAPHTHALENE 24000 u 24000 U 13000 u 24000 u2-NITROANILINE 120000 u 120000 U 62000 u 110000 uDIMETHYLPHTHALATE 24000 u 24000 u 13000 u 24000 uACENAPHTHYLENE 34000 77000 13000 u 24000 u3-NITROANILINE 120000 u 120000 U 62000 u 110000 uACENAPHTHENE 24000 u 1900 M 13000 u 15000 M

2,4-DIN1TROPHENOL 120000 u 120000 U 62000 u 110000 u4-NITROPHENOL 120000 u 120000 U 62000 u 110000 uDIBENZOFURAN 3600 M 2400 M 13000 u 12000 M

2,4-DINITROTOLUENE 24000 u 24000 u 13000 u 24000 u

ANALYSIS TYPE: SEM1VOLATILES-PAGE 2

UTLE: WATERLOO AB: TMA/NORCAL


SEDIMENT 9303M02

UN I TS CASE :

UG/KG11157

SAMPLE PREP: ANALYST/ENTRY: PLC REV I EWER: DATE: 02/03/89DATA FILE : P65


2,6-DINITROTOLUENE 24000 U 24000 U 13000 U 24000 UDIETHYLPHTHALATE ' 24000 U 24000 U 13000 U 24000 U4-CHLOROPHENYL PHENYL ETHER 24000 U 24000 U 13000 U 24000 UFLUORENE 7800 M 4800 M 13000 U 330004-NITROANILINE 120000 U 120000 U 62000 U 1 10000 U4.6-DINITR0-2-METHYLPHEN0L 120000 U 120000 U 62000 U 110000 UN-NITROSODIPHENYLAMINE 24000 U 24000 U 13000 U 24000 U4-BR0M0PHENYL PHENYL ETHER 24000 U 24000 U 13000 U 24000 uHEXACHLOROBENZENE 24000 U 24000 U 13000 U 24000 uPENTACHLOROPHENOL 120000 U 120000 U 62000 U 1 10000 uPHENANTHRENE 98000 J 35000 J 13000 U 690.00ANTHRACENE 24000 U 24000 U 13000 U 4600 MD 1 -N-BUTYLPHTHALATE 24000 U 24000 u 13000 U 24000 UFLUORANTHENE 97000 68000 13000 U 4600 MPYRENE 220000 J 150000 J 1800 M 8000 MBUTYL BENZYL PHTHALATE 24000 U 24000 u 13000 U 24000 U3.3’ DICHLOROBENZIDINE 48000 U 48000 u 25000 U 47000 U^feJZO(A)ANTHRACENE 160000 J 24000 u 13000 U 4200 M1R ( 2-ETHYLHEXYL ) PHTHALATE 5700 M 24000 u 13000 U 24000 UCHRYSENE 24000 U 140000 J 1200 M 4400 MDI -N-OCTYL PHTHALATE 24000 U 24000 u 13000 U 24000 UBENZO(B)FLUORANTHENE 75000 69000 13000 U 2600 MBENZO(K)FLUORANTHENE 56000 J 59000 J 13000 U 24000 UBENZO(A)PYRENE 69000 89000 13000 U 24000 UI NDENO(1.2,3-CD)PYRENE 32000 J 47000 J 13000 U 24000 UDIBENZO(A.H)ANTHRACENE 24000 U 24000 u 13000 U 24000 UBENZO(G,H.I)PERYLENE 57000 J 140000 J 13000 u 24000 U

ANALYSIS TYPE: SEMIVDLATILES-PAGE 1

■i TLE: WATERLOO COAL GAS MATRIX: SEDIMENT UNITS: UG/KGT.AB: TMA/NORCAL SAMPLE PREP: ANALYST/ENTRY:

METHOD: 9303M02PLC REVIEWER: p.roy

CASE: 11157DATE: 02/02/89

DATA FILE : P64


PHENOL 23000 U 24000 U 24000 U 23000 UBISC2-CHL0R0ETHYL) ETHER 23000 U 24000 U 24000 U 23000 U2-CHL0R0PHEN0L 23000 U 24000 U 24000 U 23000 U1.3 DICHLOROBENZENE 23000 U 24000 U 24000 U 23000 U1,4 DICHLOROBENZENE 23000 U 24000 U 24000 U 23000 UBENZYL ALCOHOL 23000 U 24000 U 24000 U 23000 U1.2 DICHLOROBENZENE 23000 U 24000 U 24000 U 23000 U2-METHYLPHENQL 23000 U 24000 U 24000 U 23000 UBIS(2-CHL0R0ISOPROPYL)ETHER 23000 U 24000 U 24000 U 23000 U4-METHYLPHENOL 23000 U 24000 U 24000 U 23000 UN-NITROSO-DIPROPYLAMINE 23000 U 24000 U 24000 U 23000 UHEXACHLOROETHANE 23000 U 24000 U 24000 U 23000 UNITROBENZENE 23000 U 24000 U 24000 U 23000 UISOPHORONE 23000 U 24000 U 24000 U 23000 U2-N1TROPHENOL 23000 U 24000 U 24000 U 23000 U2.4-DIMETHYLPHENOL 23000 U 24000 U 24000 U 23000 UBENZOIC ACID 110000 U 120000 U 110000 U 110000 U

(2-CHL0R0ETH0XY) METHANE 23000 U 24000 U 24000 U 23000 U1R D I CHLOROPHENOL 23000 U 24000 U 24000 U 23000 U1.2,4-TRI CHLOROBENZENE 23000 U 24000 U 24000 U 23000 UNAPHTHALENE 23000 U 24000 U 24000 U 23000 u4-CHLOROANILINE 23000 U 24000 U 24000 U 23000 uHEXACHLOROBUTADIENE 23000 U 24000 U 24000 U 23000 u4-CHL0R0-3-METHYLPHEN0L 23000 U 24000 U 24000 U 23000 u2-METHYLNAPHTHALENE 23000 U 24000 U 24000 U 23000 uHEXACHLOROCYCLOPENTADIENE 23000 U 24000 U 24000 u 23000 u2.4,6-TR1CHLOROPHENOL 23000 U 24000 U 24000 u 23000 u2,4.5-TRICHLOROPHENOL 110000 u 120000 u 110000 u 110000 u2-CHLORONAPHTHALENE 23000 u 24000 u 24000 u 23000 u2-NITROANILINE 110000 u 120000 u 110000 u 110000 uDIMETHYLPHTHALATE 23000 u 24000 u 24000 u 23000 uACENAPHTHYLENE 670 M 24000 u 1400 M 23000 u3-NITROANILINE 110000 U 120000 u 110000 U 110000 uACENAPHTHENE 23000 U 24000 u 24000 U 23000 u2,4-D1NITROPHENOL 110000 U 120000 u 110000 u 110000 u4-NITROPHENOL 110000 U 120000 u 110000 u 110000 uDIBENZOFURAN 23000 u 24000 u 24000 u 23000 u2,4-DINITROTOLUENE 23000 u 24000 u 24000 u 23000 u


% TLE: WATERLOO AB: TMA/NORC-AL


SEDIMENT9303M02

UNITS: UG/KG CASE: 11157

SAMPLE PREP: ANALYST/ENTRY: PLC REVIEWER: DATE: 02/03A

SAMPLES TK9B8009

DATA FILE :

TK9B8010

P65

TK9B8011 TK9B801:r*»

2.6-DINITR0T0LUENE 23000 U 24000 U 24000 U 23000 UD!ETHYLPHTHALATE 23000 U 24000 U 24000 U 23000 U4-CHLOROPHENYL PHENYL ETHER 23000 U 24000 u 24000 U 23000 UFLUORENE 23000 U 24000 u 24000 U 23000 u4-NITROANILINE 110000 U 120000 u 110000 U 110000 u4,6-DINITR0-2-METHYLPHEN0L 110000 U 120000 u 110000 U 110000 uN-N1TROSODI PHENYLAM INE 23000 U 24000 u 24000 U 2300 0 u4-BROMOPHENYL PHENYL ETHER 23000 U 24000 u 24000 U 23000 uHEXACHL0R0BEN2ENE 23000 u 24000 u 24000 U 23000 uPENTACHLOROPHENOL 110000 u 120000 u 110000 U 1 10000 uPHENANTHRENE 23000 u 24000 u 1300 M 23000 uANTHRACENE 23000 u 24000 u 24000 U 23000 uDI-N-BUTYLPHTHALATE 23000 u 24000 u 24000 U 23000 uFLUORANTHENE 860 M 24000 u 1800 M 23000 uPYRENE 1000 M 1800 M 3300 M 23000 uBUTYL BENZYL PHTHALATE 23000 U 24000 u 24000 U 23000 u3.3’ DICHLOROBENZIDINE 47000 U 48000 u 47000 U 47000 u4felZO ( A ) ANTHRACENE

(2-ETHYLHEXYL)PHTHALATE23000 U 1200 M 24000 U 23000 u23000 U 24000 U 24000 U 23000 u-

CHRYSENE 1200 M 24000 U 2500 M 23000 uDI -N- OCTYL PHTHALATE 23000 U 24000 U 24000 U 23000 uBENZO(B)FLUORANTHENE 23000 U 24000 U 24000 U 23000 uBENZO CK>FLUORANTHENE 23000 U 24000 u 24000 U 23000 uBENZO(A)PYRENE 23000 U 24000 u 24000 U 23000 uINDENO(1,2,3-CD)PYRENE 23000 U 24000 u 24000 U 23000 uDIBENZO(A,H)ANTHRACENE 23000 U 24000 u 24000 U 23000 uBENZO(G,H,I)PERYLENE 23000 U 24000 u 24000 U 23000 u


TLE: WATERLOO COAL GAS 'AB: TMA/NORCAL

MATRIX: SEDIMENT METHOD: 9303M02

UNITSCASE

UG/KG 11157

SAMPLE PREP: ANALYST/ENTRY: PLC REVIEWER: .o, rrw_____ DATE: 02/02 /I

SAMPLES TK9B8013

DATA FILE

TK9B80

:

14

P64

TK9B8015 TK9B8016

PHENOL 23000 U 25000 u 25000 U 23000 UBIS(2-CHL0R0ETHYL) ETHER 23000 U 25000 u 25000 U 23000 u2-CHL0R0PHEN0L 23000 U 25000 u 25000 U 23000 U1.3 DICHLOROBENZENE 23000 U ^ 25000 u 25000 U 23000 U1,4 DICHLOROBENZENE 23000 U 25000 u 25000 U 23000 UBENZYL ALCOHOL 23000 U 25000 u 25000 U 23000 U1.2 DICHLOROBENZENE 23000 U 25000 u 25000 U 23000 U2-METHYLPHENOL 23000 U 25000 u 25000 U 23000 UBIS(2-CHLOROISOPROPYL)ETHER 23000 U 25000 u 25000 U 23000 U4-METHYLPHENOL 23000 U 25000 u 25000 U 23000 UN-NITROSO-DIPROPYLAMINE 23000 U 25000 u 25000 U 23000 UHEXACHLOROETHANE 23000 u 25000 u 25000 U 23000 uNITROBENZENE 23000 u 25000 u 25000 U 23000 UISOPHORONE 23000 u 25000 u 25000 U 23000 u2-NITROPHENOL 23000 u 25000 u 25000 u 23000 u2.4-DIMETHYLPHENOL 23000 u 25000 u 25000 U 23000 uBENZOIC ACID 110000 u 120000 u 120000 u 110000 u

(2-CHL0R0ETH0XY) METHANED I CHLOROPHENOL

23000 u 25000 u 25000 U 23000 u23000 u 25000 u 25000 U 23000 u

1,2,4-TRI CHLOROBENZENE 23000 u 25000 u 25000 U 23000 uNAPHTHALENE 23000 u 25000 u 25000 U 2200 M4-CHLOROANILINE 23000 u 25000 u 25000 u 23000 UHEXACHLOROBUTADIENE 23000 u 25000 u 25000 u 23000 U4-CHLORO-3-METHYLPHENOL 23000 u 25000 u 25000 u 23000 u2-METHYLNAPHTHALENE 23000 u 25000 u 25000 u 23000 uHEXACHLOROCYCLOPENTADIENE 23000 u 25000 u 25000 u 23000 u2.4,6-TRICHLOROPHENOL 23000 u 25000 u 25000 u 23000 u2.4.5-TR1CHLOROPHENOL 110000 u 120000 u 120000 u 110000 u2-CHL0R0NAPHTHALENE 23000 u 25000 u 25000 u 23000 u2-N1TROANILINE 110000 u 120000 u 120000 u 110000 uDIMETHYLPHTHALATE 23000 u 25000 u 25000 u 23000 uACENAPHTHYLENE 23000 u 25000 u 1700 M 1600 M3-NITROANILINE 110000 u 120000 u 120000 u 110000 UACENAPHTHENE 23000 u 25000 u 25000 u 23000 u2,4-DINITR0PHEN0L 110000 u 120000 u 120000 u 110000 u4-NITROPHENOL 110000 u 120000 u 120000 u 110000 uDIBENZOFURAN 23000 u 25000 u 25000 u 23000 u2,4-DINITROTOLUENE 23000 u 25000 u 25000 u 23000 u


ITLE: WATERLOO AB: TMA/NORCAL


SEDIMENT9303M02

UNITS CASE :

UG/KG 1 1157

SAMPLE PREP: ANALYST/ENTRY: PLC REV I EWER: p rrw DATE: 02/03/iDATA FILE P65

SAMPLES TK9B8013 TK9B8014 TK9B80 15 TK9B8016

2,6-DIN1TROTOLUENE 23000 U . 25000 U 25000 U 23000 UDIETHYLPHTHALATE 23000 U 25000 U 25000 U 23000 U4-CHLOROPHENYL PHENYL ETHER 23000 U 25000 U 25000 U 23000 UFLUORENE 23000 U 25000 U 25000 U 23000 u4-N1TROANILINE 110000 U 120000 U 120000 U 110000 u4.6-DIN ITR0-2-METHYLPHEN0L 110000 U 120000 U 120000 U 110000 uN-NITROSODI PHENYLAM INE 23000 U 25000 U 25000 U 23000 u4-BROMQPHENYL PHENYL ETHER 23000 U 25000 U 25000 U 23000 uHEXACHLOROBENZENE 23000 U 25000 U 25000 U 23000 uPENTACHLOROPHENOL 110000 U 120000 U 120000 U 1 10000 uPHENANTHRENE 23000 u 25000 U 25000 U 23000 uANTHRACENE 23000 u 25000 U 25000 U 2200 MD I -N-BUTYLPHTHALATE 23000 u 25000 U 25000 U 23000 UFLUORANTHENE 650 M 25000 U 2600 M 2400 MPYRENE 1100 M 1000 M 3400 M 4700 MBUTYL BENZYL PHTHALATE 23000 U 25000 U 25000 U 23000 U3.3’ DICHLOROBENZIDINE 47000 U 50000 U 50000 U 47000 U^ksIZO ( A ) ANTHRACENE 23000 U 25000 U 25000 U 3400 M^Ps (2-ETHYLHEXYL)PHTHALATE

23000 U 25000 U 25000 U 23000 UCHRYSENE 23000 U 25000 U 3400 M 3500 MDI -N-OCTYL PHTHALATE 23000 U 25000 U 890 M 23000 UBENZO(B)FLUORANTHENE 23000 u 25000 U 1900 M 2800 MBENZO(K)FLUORANTHENE 23000 u 25000 U 1900 M 2800 MBENZO(A)PYRENE 23000 u 25000 U 1400 M 2200 MINDENO(1.2.3-CD)PYRENE 23000 u 25000 U 25000 U 3200 MDIBENZO(A,H)ANTHRACENE 23000 u 25000 U 25000 U 23000 UBENZO(G.H,I)PERYLENE 23000 u 25000 U 25000 U 23000 U

ANALYSIS TYPE: SEMIVQLATILES-PAGE 1

^■TLE: WATERLOO COAL GAS MATRIX: SEDIMENT^XAB: TMA/NORCAL

METHOD: 9303M02SAMPLE PREP: ANALYST/ENTRY: PLC REV I EWER ; I'T, c n x

DATA FILE : >64

SAMPLES TK9B8017 TK9B8018 TK9B8019

PHENOL 23000 U 26000 U 22000 UBIS(2-CHL0R0ETHYL) ETHER 23000 U 26000 U 22000 U2-CHLOROPHENOL 23000 U 26000 u 22000 u1,3 DICHLOROBENZENE 23000 U 26000 u 22000 U1,4 DICHLOROBENZENE 23000 U 26000 u 22000 UBENZYL ALCOHOL 23000 U 26000 u 22000 U1,2 DI CHLOROBENZENE 23000 U 26000 u 22000 u2-METHYLPHENOL 23000 u 26000 u 22000 UB1S(2-CHL0R01SOPROPYL)ETHER 23000 u 26000 u 22000 U4-METHYLPHENOL 23000 u 26000 u 22000 uN-N1TROSO-DIPROPYLAMINE 23000 u 26000 u 22000 UHEXACHLOROETHANE 23000 u 26000 u 22000 UNITROBENZENE 23000 u 26000 u 22000 UISOPHORONE 23000 u 26000 u 22000 U2-NITROPHENOL 23000 u 26000 u 22000 U2,4-DIMETHYLPHENOL 23000 u 26000 u 22000 UBENZOIC ACID 110000 u 130000 u 110000 UaK(2-CHL0R0ETH0XY) METHANE 23000 u 26000 u 22000 UV* DICHLOROPHENOL 23000 u 26000 u 22000 U1,2,4-TRI CHLOROBENZENE 23000 u 26000 u 22000 UNAPHTHALENE 5900 M 26000 u 22000 U4-CHLOROANILINE 23000 u 26000 u 22000 uHEXACHLOROBUTAD1ENE 23000 u 26000 u 22000 u4-CHLORO-3-METHYLPHENOL 23000 u 26000 u 22000 u2-METHYLNAPHTHALENE 4500 M 26000 u 22000 uHEXACHLOROCYCLOPENTADIENE 23000 U 26000 u 22000 u2,4,6-TRICHLOROPHENOL 23000 u 26000 u 22000 u2,4,5-TRICHLOROPHENOL 110000 u 130000 u 110000 u2-CHLORONAPHTHALENE 23000 u 26000 u 22000 u2-NITROANILINE 110000 u 130000 u 110000 uDIMETHYLPHTHALATE 23000 u 26000 u 22000 uACENAPHTHYLENE 54000 26000 u 22000 u3-NITROANILINE 110000 u 130000 u 110000 uACENAPHTHENE 23000 u 26000 u 22000 u2,4-DINITROPHENOL 110000 u 130000 u 110000 u4-NITROPHENOL 110000 u 130000 u 110000 uDIBENZOFURAN 2600 M 26000 u 22000 u2,4-DINITROTOLUENE 23000 U 26000 u 22000 u

UNITS CASE : DATE:

UG/KG1115702/02/89


UNITS CASE : DATE:

SAMPLES TK9B8017 TK9B8018 TK9B80 19

2.6-DINITR0T0LUENE 23000 U 26000 U 22000 UDIETHYLPHTHALATE 23000 U 26000 U 22000 U4-CHLOROPHENYL PHENYL ETHER 23000 U 26000 U 22000 UFLUORENE 3900 M 2100 M 22000 U4-NITROANILINE 110000 U 130000 U 110000 U4,6-DINITRO-2-METHYLPHENOL 110000 U 130000 U 110000 UN-NITROSODI PHENYLAM INE 23000 U 26000 U 22000 u4-BROMOPHENYL PHENYL ETHER 23000 U 26000 U 22000 uHEXACHLOROBENZENE 23000 U 26000 U 22000 uPENTACHLOROPHENOL 110000 U 130000 U 110000 uPHENANTHRENE 37000 J 9700 M 1900 MANTHRACENE 23000 U 26000 U 22000 uDI-N-BUTYLPHTHALATE 23000 U 26000 U 22000 UFLUORANTHENE 88000 J 37000 2500 MPYRENE 200000 J 93000 J 3300 MBUTYL BENZYL PHTHALATE 23000 U 26000 u 22000 U2^3’ D1CHLOROBENZIDINE 47000 U 52000 u 44000 UHZO (A) ANTHRACENE 23000 U 26000 u 22000 UWs (2-ETHYLHEXYL)PHTHALATE

23000 U 26000 u 22000 UCHRYSENE 85000 J 50000 J 22000 UDI-N-OCTYL PHTHALATE 23000 U 26000 u 22000 UBENZO(B)FLUORANTHENE 57000 17000 M 22000 U

BENZO(K)FLUORANTHENE 41000 J 20000 M 1300 MBENZO(A)PYRENE 69000 23000 M 22000 UINDENO(1.2,3-CD)PYRENE 28000 15000 M 22000 UDIBENZO(A.H)ANTHRACENE 23000 U 26000 U 22000 UBENZO(G.H,I)PERYLENE 96000 J 49000 J 22000 U

’ITLE: WATERLOO

LAB: TMA/NORCAL SAMPLE PREP:

COAL GAS

ANALYST/ENTRY: PLC

MATRIX: SEDIMENT METHOD: 9303M02 REVIEWER: p.rrwDATA FILE : P65

*

UG/KG1115702/03/89

TENTATIVELY IDENTIFIED COMPOUNDS

TITLE: WATERLOO COAL GAS LAB: TMA/NORCAL ANALYST/ENTRY: PLC

MATRIX: SEDIMENT METHOD: 9303M02 REVIEWER:DATA FILE : P66


SAMPLE NO COMPOUND NAME FRACTION EST. CONCENTRATION

TK9B8001POLYAROMATIC HYDROCARBON BNA 6000 JN

TK9B8002NOTHING SIGNIF CANT FOUND BNA

TK9B8003NOTHING S GNIFICANT FOUND BNA

TK9B8004NOTHING SIGN FICANT FOUND BNA

TK9B8005ETHENYLMETHYL BENZENE BNA 80000 JNPHENYLNAPHTHALENE BNA 30000 JNMETHYLPYRENE BNA 20000 JNSUBSTITUTED ALKENE BNA 90000 JN

3 SUBSTITUTED BENZENES BNA 10000-50000 JN3 SUBSTITUTED ALKANES BNA 10000-30000 JN3 POLYAROMATIC HYDROCARBONS BNA 10000-60000 JN2 SUBSTITUTED AROMATICS BNA 10000-60000 JN3 UNKNOWNS BNA 10000-20000 JN



* THIS IS A CRUDE ESTIMATION BASED ON RESPONSE RELATIVE TO AN INTERNAL STANDARD. AN AUTHENTIC STANDARD HAS NOT BEEN RUN.

** THE COMPOUNDS WERE IDENTIFIED USING A LIBRARY SEARCH ROUTINE AUTHENTIC STANDARDS HAVE NOT BEEN ANALYZED TO VERIFY COMPOUND MASS SPECTRA AND RETENTION TIMES.


TITLE: WATERLOO COAL GAS LAB: TMA/NORCAL ANALYST/ENTRY: PLC

MATRIX: SEDIMENT METHOD: 9303M02 REVIEWER: p.ro^DATA FILE : P66


SAMPLE NO. COMPOUND NAME FRACTION EST. CONCENTRATION

TK9B8008ALKENE

3 SUBSTITUTED BENZENES5 SUBSTITUTED NAPHTHALENES6 ALKANES 5 UNKNOWNS

BNA 50000 JN BNA 10000-40000 JN BNA 40000-300000 JN BNA 10000-200000 JN BNA 30000-200000 JN

TK9B8009NOTHING SIGNIFICANT FOUND BNA


TK9B8011ETHENYLMETHYL BENZENE SUBSTITUTED ALKENE UNKNOWN

BNABNABNA

30000 JN 30000 JN 100000 JN

TK9B8012CARBOXYLIC ACID BNA 100000 JN




THIS IS A CRUDE ESTIMATION BASED STANDARD. AN AUTHENTIC STANDARD

ON RESPONSE RELATIVE HAS NOT BEEN RUN.

#* THE COMPOUNDS WERE IDENTIFIED USING A LIBRARY SEARCH AUTHENTIC STANDARDS HAVE NOT BEEN ANALYZED TO VERIFY MASS SPECTRA AND RETENTION TIMES.

TO AN INTERNAL

ROUTINECOMPOUND


TITLE: WATERLOO COAL GAS MATRIX: SEDIMENT UNITS;: UG/KGLAB: TMA/NORCAL METHOD: 9303M02 CASE : 11157ANALYST/ENTRY: PLC REVIEWER:

DATA FILE : P66'DATE : 02/02/89

SAMPLE NO. COMPOUND NAME FRACTION EST. CONCENTRATION

TK9B8016ETHENYLEMTHYL BENZENE BNA 200000 JNSUBSTITUTED ALKENE BNA 200000 JN

8 SUBSTITUTED BENZENES BNA 10000-50000 JNOXYGEN SUBSTITUTED BENZENE BNA 40000 JN

TK9B8017ALKENE BNA 10000 JNSUBSTITUTED BENZENE BNA 8000 JN

12 POLYAROMATIC HYDROCARBONS BNA 10000-100000 JN3 UNKNOWNS BNA 30000-100000 JN

TK9B80183 METHYLPYRENES BNA 5000-7000 JN3 POLYAROMATIC HYDROCARBONS BNA 10000-20000 JN3 UNKOWNS BNA 9000-40000 JN

TK9B8019NOTHING SIGNIFICANT FOUND BNA *

* THIS IS A CRUDE ESTIMATION BASED ON RESPONSE RELATIVE TO AN INTERNAL STANDARD. AN AUTHENTIC STANDARD HAS NOT BEEN RUN.

*# THE COMPOUNDS WERE IDENTIFIED USING A LIBRARY SEARCH ROUTINE. AUTHENTIC STANDARDS HAVE NOT BEEN ANALYZED TO VERIFY COMPOUND MASS SPECTRA AND RETENTION TIMES.

ANALYSIS TYPE: SEMIVGLATILE5-PA6E i

TITLEi WATERLOO COAL GAS matrix: WATER UNITSAAB! EPA REGION VII Kfc method: 6251W00 /)/ case:SAMPLE PREP: _ ANALYST /'ENTRY l MLG REVIEWER t date:

DATA FILE: MGS

TK9B8102 TK9B6105F

PHENOL 10.U 10.uBIS<2-CHL0R0ETHYL) ETHER 10.U 10.u2-CHL0R0FHEN0L 10.U 10,u1,3 DICHLOROBENZENE 10.U 10.u1,4 DICHLOROBENZENE 10.U 10.uBENZYL ALCOHOL 10 . U 10.u1,2 DICHLOROBENZENE 10.U 10.u2-METHYLFHENOL 10.u 10.uBIS <2-CHL0R0ISOPROPYL)ETHER 10.u 10.u4-METHYLPHENOL 10.u 10.uN-NITROSO-DIPROPYLAMINE 10.u 10,uHEXACHLOROETHANE 10.u 10.uNITROBENZENE 10.u 10.uISuPHORONE 10.u 10.u2-NITROPHENOL 10.u 10.u2,4-DIMETHYLPHENOL 10. u 10.uBENZOIC ACID 50.U 50.UBIS(2-CHL0RGETH0XY) METHANE 10.u 10.u2,4 DICHLOROPHENOL 10.u 10.u1,2,4-TRICHLOROBENZENE 10.u 10.uAtHTHALENE 10. u 10.uWCHLOROANILINE 10.u 10.uHEXACHLOROBUTADIENE 10.u 10.u4-CHL0R0-3-METHYLPHENOL 10.u 10.u2-METHYLNAPHTHALENE 10.u 10.uHEXACHLORQCYCLOFENTADIENE 10.u 10.u2,4,6-TRICHLOROPHENOL 10.u 10.u2,4»5-TRICHL0R0PHENOL 50.U 50.U2-CHLORONAPHTHALENE 10.U 10.u2-NITROANILINE 50.U 50.UDIMETHYLF'HTHALATE 10.U 10.uACENAPHTHYLENE 10.u 10,u3-NITROANILINE 50.U 50.UACENAFHTHENE 10.u 10.u2,4-DINITROFHENOL 50.U 50.U4-NITROPHENOL 50.U 50,UDIBENZOFURAN 10.u 10.u2,4-DINITROTOLUENE 10.u 10.u

** note: N/A MEANS NOT ANALYZED **I HEANS ANALYZED BUT INVALID DATA ***

i UG/L

01/31/89

ANALY5I5 TYPE l 5EHIVOLATILES-PAGE 2

TITLEi WATERLOO COAL GAS matrix: water UNITS^kib: epa region vii rAfe METHOD: 6251W00 /)/ case:Wimple prep: _ __ _ analyst/entry: mlg reviewer: date:

DATA FILE: HG7

TK9B8102 TK9B8105F

2»6-DINITR0T0LUENE 10,U 10.UDIETHYLPHTHALATE 10.U 10.U4-CHLORCJPHENYL PHENYL ETHER 10.U 10.UFLUORENE 10.U 10.U4-NITROANILINE 50.U 50.UAf6-DINITR0-2-METHYLPHEN0L 50.U 50.UN-NITR050DIPHENYLAMINE 10.U 10.U4-BR0M0PHENYL PHENYL ETHER 10.U 10.UHEXACHLGROBENZENE 10.U 10.UPENTACHLGROPHENOL 50.U 50.UPHENANTHRENE 10 ,U 10.UANTHRACENE 10.U 10.UDI-N-BUTYLPHTHALATE 10.U 10.UFLUORANTHENE 10.U 10.uPYRENE 10.U • 10.uBUTYL BENZYL PHTHALATE 10.u 10.u3,3' DICHLORGBENZIDINE 20. U 20.UBENZO<A)ANTHRACENE 10.U 10,UBIS(2-ETHYLHEXYL)PHTHALATE 10.U 110.CHRYSENE 10.u 10.u^N-OCTYL PHTHALATE 10.u 10.uiS^ZO(B)FLUORANTHENE 10.u 10.uBENZO(K)FLUORANTHENE 10.u 10.uBENZO(A)F'YRENE 10 .u 10,uINDENO (1 t 2 » 3-CD ) F’YRENE 10.u 10.uDIBENZO<A,H)ANTHRACENE 10.u 10.uBENZO(G » H »I)PERYLENE 10.u 10.u

** note: **#

N/AI

MEANS NOT ANALYSED * *MEANS ANALYZED BUT INVALID DATA ***

UG/L

01/31/69


TITLE; TK9B8 WATERLOO COAL GAS LAB: ERA REGION VIIANALYST/ENTRY: MLG

MATRIX: WATERMETHOD: 625IWOO REVIEWER:DATA FILE : MG 1

UNITS: LJ6/L CASE;DATE: 01/3:1/8

SAMPLE NO.

TK9B8102NOTHING

TK9BS105FMOTH ING

COMPOUND NAME

SIGNIFICANT FOUND

SIGNIFICANT FOUND

FRACTION EST. CONCENTRATION

BN A

BN A

* THIS IS A CRUDE ESTIMATION BASED ON RESPONSE RELATIVE TO AN INTERNA-.. STANDARD. AN AUTHENTIC STANDARD HAS NOT BEEN RUN.

** THE COMPOUNDS WERE IDENTIFIED USING A LIBRARY SEARCH ROUTINE.. AUTHENTIC STANDARDS HAVE NOT BEEN ANALYZED TO VERIFY COMPOUND NASS SPECTRA AND RETENTION TINES.

ANALYSIS TYPE: VOLATILES

'ITLE: SEDIMENT FOR VOLATILES MATRIX: SEDIMENT„AB: REGION VII ERA METHOD: 6241S00SAMPLE PREP: " ANALYST/ENTRY: DME REVIEWER:

DATA FILE : D10 Jjsf

UNITS: UG/K6 CASE:DATE:

SAMPLES TK9BS001 TK9B8£ 02 TK9B80J2 3 TK9B8004

CHLOROMETHANE 12 U 12 U 12 U 30 (JBROMOMETHANE U U U C." CZ'%J -..J uVINYL CHLORIDE 14 U 14 U 14 U :!■ w' IJCHLOROETHANE 14 U 14 U 14 U ..... u:r•2- _J UMETHYLENE CHLORIDE 10 U 1 0 U 60 U 190ACETONE 10 U 10 U 10 U our UCARBON DISULFIDE 5, 0 IJ 5. 0 U 5. 0 U 13 lj1,1-DICHLOROETHENE 5.0 U 5.0 IJ 5.0 Ll 13 U1,1 DICHLOROETHANE 5. 0 U 5.0 U 5.0 U 13 u1,2,.DICHLOROETHEIME 5. 0 U 5.0 U 5. 0 U 13 uCHLOROFORM 5.0 U 5.0 Ll 5. 0 U 13 IJ1,2,DICHLOROETHANE 5.0 U 5.0 U 5.0 L! 13 u2-BUTANONE 10 U 10 U 10 U 25 u1,1, 1--TR1 CHLOROETHANE 5.0 IJ 5. © U 5. 0 U 13 LiCARBON TETRACHLORIDE 5.0 U 5.0 U 5.0 U 13 uVINYL ACETATE 10 U 10 U 10 IJ ir' IJBR0M0D I CP1L0R0METHANE 5. 0 IJ 5. © U 5.0 U 13 IJ

2 - D I C H L 0 R 0 P R 0 R A N E 5.0 U 5. © U 5.0 Ll 13 IJm2- 1.3-D ICHLOROPROPENE 5. © IJ 5. © U 5.0 U 13 IJTRICHLOROETHENE 5.0 LI 5.0 U 5.0 IJ 13 IJBENZENE 5. © IJ 5. 0 IJ 21 13 ijDIBROMOCHLOROMETHANE 5. 0 IJ 5. 0 U 5. 0 u 13 u1,1,2-TRICHLOROETHANE 5. © LI 5. © U 5. 0 u 13 uTRANS-1,3-D ICHLOROPROPENE 5.0 IJ 5.0 U 5. © Ll 13 IJERGMOPORM 5. 0 LI 5. 0 U 5.0 [J 13 u4-METHYL-2.PENTANONE 10 IJ 10 IJ 10 U cr IJ2--HEX ANONE 10 U 10 IJ 10 IJ o c:- IJ1,1,2,2-TETRACHL0R0ETHANE 5. © U 5. 0 LI 5.0 U 13 LJTETRACHLOROETHENE 5. 0 U 5. © IJ 5. 0 u 13 UTOLUENE 5.0 U 5. 0 U i-'iO ,»LCHLOROBENZENE 5. 0 IJ 5.0 U 5 „ 0 u 13 UETHYL BENZENE 5. © IJ 5. 0 U 5.0 u 13 USTYRENE 5. 0 IJ 5.0 U 5. © Ll 13 uTOTAL XYLENES 5.0 u 5.0 LI 7.0 13 Li

V

ANALYSIS TYPE VOLATILES

^■riTLE: SEDIMENT FOR VOLATILES

î_AB: REGION VII ERA

SAMPLE PREP:^y. i .ANALYST/ENTRY: DME

MATRIX: SEDIMENT UNITS: UG/|;fe

METHOD: 6241S00 /2,_ CASE:REVIEWER: DATE: 12/14/88DATA FILE : D10 .. \ .


CHLOROMETHANE 12 U 12 LI 12 U 60 UBROMOMETHANE U nn U -C. -iL LI 1 10 UVINYL CHLORIDE 14 U 14 IJ 14 U 70 UCHLOROETHANE 14 U 14 U 14 U 70 UMETHYLENE CHLORIDE 30 U 10 U 10 LI 50 L.lACETONE 10 U 10 U 1 0 IJ 50 IJCARBON DISULFIDE 5. 0 1.) 5. 0 U 5.0 U : r.::'

jL-—1 IJ1,1-DICHLUROETHENE 5. 0 IJ 5. 0 U 5. 0 U ur U1,1 DICHLOROETHANE 5.0 IJ 5. 0 U 5. 0 U ir; L.I1.2,-DICHLOROETHENE 5.0 U 5.0 u 5.0 IJ •—i ::r

-:’l •. J uCHLOROFORM 5. 0 U 5.0 IJ 5. 0 U 2 3 U1,2.DICHLOROETHANE 5.0 IJ 5.0 IJ 5.0 U 23 U2-BUTANONE 10 u 10 IJ 10 U 5 u1,1,1-TRICHLOROETHANE 5.0 IJ 5.0 u 5.0 U IJCARBON T E T R A C HL 0RIDE 5.0 u 5. 0 LI 5. 0 U in:; I..JVINYL ACETATE 10 IJ 10 LI 10 IJ 50 uBRGM0DI ChiL.OROMETHANE 5. 0 IJ 5.0 U 5.0 U cr IJ

2—D I CHLOROPROPAME ^Pl.S-1.3-DICHL0R0PR0PENE

5.0 IJ 5.0 IJ 5.0 U 25 Li5. A U 5.0 U 5.0 IJ 23 I...I

TRICHLOROETHENE 5.0 LI 5. 0 LI 5. 0 U •~I fVJ-.ill IJ

BENZENE 500 5. 0 U 5. 0 u 620DIBROMQCHLOROMETHANE 5. 0 IJ 5.0 U 5.0 IJ u1,1,2-TRICHLOROETHANE 5. 0 IJ 5.0 IJ 5.0 u cr I...ITRANS-1,3-DICHLOROF'ROPENE 5. 0 U 5.0 IJ 5.0 IJ i::.~

oi. wJ LIBROMOFORM 5. g U 5. 0 U 5.0 u . nr IJ

4-METHYL-2-PENTAN0NE 10 Ll 10 IJ 10 u 50 IJ2--HEX ANONE 10 U 10 IJ 10 u 50 L.l1,1,2,2-TETRACHL0R0ETHANE 5. 0 IJ 5.0 U 5.0 IJ •—» ur

/.._i IJ

TETRACHLOROETHENE 5. 0 U 5. 0 IJ 5. 0 u ■—i cr UTOLUENE 87 5.0 U 5.0 LI T i'7'jCHLOROBENZENE 5. 0 U 5. 0 LI 5. 0 IJ ■~i rr

oiL -..J IJETHYL BENZENE 65 5.0 U 5.0 IJ 13200STYRENE 5. 0 U 5. 0 IJ 5.0 LI rr; IJTOTAL XYLENES 19 5.0 U 5. 0 U 770


|T I TLE : SEDIMENT FOR VOLATILESLAB; REGION VII EPASAMPLE PREP; ANALYST/ENTRY:

MATRIX: SEDIMEN METHOD: 624 IS®0

DME REVIEWER: __DATA FILE : D10

UNITS; UG/CASE; *' UJ°

DATE; 12/14/88

SAMPLES TK9B31009 TK9B8010 TK9B8011 1 K 9 B o 0 1 *•'

‘r •CHLOROMETHANE 12 U 12 U 12 U 12 UBROMOMETHANE U *L. Xi. U IJ ••“•l •” UVINYL CHLORIDE 14 u 14 U 14 U 14 UCHLOROETHANE 14 u 14 U 14 IJ 14 LiMETHYLENE CHLORIDE 10 u 10 U 15 U 12 Uacetone 10 u 10 U 10 U 10 IJCARBON DISULFIDE 5.0 u 5.0 LI 5.0 U 5.0 U1„1-DICHLOROETHENE 5. 0 IJ 5. 0 U 5.0 IJ 5. 0 U1„1 DICHLOROETHANE 5. 0 u 5. 0 LJ 5. 0 IJ 5 „ 0 LJ1,2,~DICHLOROETHENE 0.0 !J 5.0 IJ 5.0 IJ 5.0 IJCHLOROFORM 5. 0 IJ 5.0 U 5. 0 IJ 5. 0 U1,2,DICHLOROETHANE 5. 0 u 5.0 U 5.0 IJ 5. 0 IJ2-BUTANONE 1 0 u 1 0 IJ 10 u 1 0 i.jI,!,1-TRICHLOROETHANE 5.0 IJ 5. 0 Ll 5.0 IJ 5. 0 IJC A R B 0 N T El T FS A L H L GRIDE 5.0 LI 5. 0 IJ 5,0 u 5. 0 IJVINYL ACETATE 10 U 10 U 10 Ll 10 IJB R 0 r 10 D I C H L 0 R 0 M E T H A N E 5. 0 IJ 5. 0 LJ- 5. 0 Ll 5 0 u

2 —DICHLGROPROPANE 5.0 u 5. 0 LJ 5.0 U cr •_J D uS-1,3 -D ICHLOROPROPENE 0. 0 IJ 5. 0 Ll 5.0 U . I'-;'-1 U

IRICHLOROETHENE 5.0 LI 5.0 U 5.0 Ll 5.0 IJBENZENE 5. 0 LJ 5. 0 U 5.0 U 5.0 uDIBROMOCHLOROMETHANE 5. 0 IJ 5.0 L! 5.0 U 5, 0 LJ1,1.2--TR I CHLOROETHANE 5. 0 IJ 5.0 IJ 5.0 U 5. 0 LJTRANS-1,3-D ICHLOROPROPENE 5.0 U 5.0 U 5. 0 U 5. 0 LJBROMOFORM 5. 0 LI 5. 0 U 5. 0 IJ 5.0 LJ4-METHYL-2-PENTANONE 10 LI 10 U 10 U 10 LJ2-HEXANOME 10 U 10 U 10 U 10 IJ1,1,2,2-TETRACHL0R0ETHANE 5. 0 U 5.0 U 5.0 U 5. 0 LJTETRACHLORQETHENE 5. 0 IJ 5. 0 IJ 5. 0 U 5.0 LiTOLUENE 9. 0 5,0 U 5.0 U 5. 0 LJCHLOROBENZENE 5. 0 Ll 5. 0 U 5. 0 U 5.0 UETHYL BENZENE 49 5. 0 U 5.0 U 5. 0 uSTYRENE 5. 0 U 5. 0 U 5. 0 U 5. 0 uTOTAL XYLENES 16 5.0 IJ 5.0 Ll 5. 0 u


'ITLE: SEDIMENT FOR VOLATILES rLAB: REGION VII ERA

MATRIX: SEDIMENT UNITS: UB/fc&METHOD: 6241S00 /7 _ CASE:

SAMPLE PREP: „ ANALYST/ENTRY: DME REVIEWER: DATE: 12/14/88DATA FILE : D 1 0 .;/

SAMPLES TK9B3013 TK:9BB014 TK9B801 5 TK9B8016

CHLOROMETHANE 12 U 12 U 12 LI 12 UBROMOMETHANE U U 'T' •**? U uVINYL CHLORIDE 14 U 14 IJ 14 U 1-1 UCHLOROETHANE 14 U 14 u 14 U 1 4 UMETHYLENE CHLORIDE 14 U 14 u 14 IJ 14 UACETONE 10 U 10 IJ 10 LI 10 IJCARBON DISULFIDE 5. 0 U 5. 0 u 5. A U b „ 0 U1 , 1-DICHLORGETHENE 5-0 U 5.0 LI 5 „ 0 U b. I-:!-' LJ1,1 DICHLOROETHANE 5.0 IJ 5.0 IJ 5. 0 IJ b. 0 !J1,2,-DICHLORGETHENE 5.0 IJ 5. 0 IJ 5. 0 U 5. 0 IJCHLOROFORM 5- 0 U 5. 0 U 5.0 IJ 5 - 0 IJ1,2,DICHLOROETHANE 5.0 IJ 5. 0 U 5.0 IJ 5. 0 u2-BUTAHONE 10 LI 10 IJ 10 U 10 IJ1,1,1-TRICHLOROETHANE 5 „ 0 U 5. 0 u 5.0 IJ 5. 0 IJCARBON TETRACHLORIDE 5- 0 U 5« 0 IJ 5. 0 u 5.0 uVINYL ACETATE 10 U 10 LI 10 u 1 0 IJBROMODICHLOROMETHANE 5. 0 U 5. 0 IJ 5. 0 u 5. 0 IJ

2—DICHLOROPROPANE 5. 0 U 5. 0 IJ 5.0 LI 5. O uWts-1,3-DICHL0RDPR0PEME 5.0 U 5. 0 U 5. 0 U 5. 0 uTRICHLORGETHENE 5. 0 U 5.0 U 5 - 0 LI 5. 0 uBENZENE 5. 0 IJ 5. A U 5. 0 U 5.0 uDIBRGMOCHLOROMETHANE 5. 0 U 5.0 IJ 5.0 U 5,0 IJ1,1,2-TRICHLOROETHANE 5. 0 LI 5.0 LI 5.0 U 5. 0 uTRANS -1,3--DICHL0R0PR0PENE 5 - 0 U 5.0 U 5. 0 U 5. 0 IJBROMOFORM 5. 0 U 5.0 LI 5.0 u 5.0 U4—METHYL—2—F’ENT ANONE 10 IJ 10 U 10 u 10 U2—HEXANDNE 10 U 10 U 1 0 IJ 10 IJ1 , 1,2,2-TETRACHL0R0ETHANE 5.0 IJ 5.0 IJ 5.0 IJ 5. 0 ijTETRACHLOROETHENE 5.0 U 5.0 LI 5. 0 u 5.fJ UTOLUENE , 5.0 LI 5. 0 U 5.0 u 5.0 LlCHLOROBENZENE 5. 0 LI 5.0 IJ 5.0 u 5.0 UETHYL BENZENE 5. 0 LI b. k) IJ 5.0 IJ 5.0 IJSTYRENE 5. 0 U 5. 0 U 5.0 IJ 5. 0 IJTOTAL XYLENES 5.0 U 5.0 u 5. 0 u 5.0 LJ


ITLE: SEDIMENT FOR LAE: REGION VII EPA

SAMPLE F’l

'OLATILES MATRIX: SEDIMENTMETHOD: 6241S00

ANALYST/ENTRY: DME REVIEWER:DATA FILE : D 1 0 -.2 j.

SAMPLES TK9B8:017 TL:9B801S TK9B8019

CHLQROMETHANE 12 U 12 U 12 UBROMOMETHANE jL. U 2- jL. U UVINYL CHLORIDE 14 IJ 14 IJ 14 UCHLQROETHANE 14 u 14 u 14 UM E T H Y l.. E N E C H L 0 RID E 10 u 10 u 10 UACETONE 1 0 u 10 Ll 1 0 UCARBON DISULFIDE 5.0 u 5. 0 U 5. 0 u1 , 1-DICHL.ORQETHENE 5.0 u 5.0 U 5. 0 IJ1.1 DICHLQROETHANE 5. 0 IJ 5. 0 IJ 5.0 u1.2. --DICHLOROETHENE 5.0 u 5. 0 IJ 5.0 uCHLOROFORM 5.0 IJ 5 - !i-‘ LI 5. 0 u1,2.DICHLOROETHANE 5.0 u 5.0 Ll 5.0 u2-BUTANONE 10 u 10 IJ 10 IJ1,1,1-TRICHLOROETHANE 5.0 u 5. 0 U 5.0 LlCARBON TETRACHLORIDE 5. 0 IJ 5.0 IJ 5. 0 UVINYL ACETATE 10 u 10 IJ 1 0 U

BROMODICHLOROMETHANE 5. 0 u 5.0 U 5.0 U^2 — DICHLOROPROPANE 5.0 LI 5. 0 U 5. 0 Llls-1.3-DICHL0RDPR0PENE 5, 0 u 5. 0 U 5. 0 LlTCICHLOROETHENE ■ 5.0 u 5. 0 U 5.0 U

BENZENE 5. 0 IJ 5. 0 U 5. 0 UDIBRDMOCHLOROMETHANE 5. 0 LI b » ! ■: u 5. 0 Ll1,1,2-TP ICHLOROETHANE 5.0 U 5. 0 Ll 5. 0 UTRANS-1.3- D ICHLOROPROPENE 5.0 U b. it ' u 5. 0 U

BROMOFORM 5. 0 U 5.0 Ll 5.0 U

4 - M E T H Y L. - 2 -PE N T A N 0 N E 10 LI 10 U 10 U

2—HEXANONE 10 LI 10 U 10 IJ1,1,2,2-TETRACHL0R0ETHANE 5,0 U 5. 0 U 5.0 UTETRACHLOROETHENE 5.0 U 5.0 IJ 5.0 uTOLUENE 5.0 IJ 5.0 Ll 5.0 IJ

CHLOROBENZENE 5. 0 LI 5. 0 IJ 5. 0 IJ

ETHYL BENZENE 5. 0 U 5. 0 U b. U) Ll

STYRENE 5. 0 LI 5.0 IJ 5.0 Ll

TOTAL XYLENES 5.0 IJ 5.0 Ll 5.0 U

UNITS: UG/(C.k CASE;DATE: 12/14/E


TITLE: WATER FOR VOLATILES MATRIX: WATER UNITSLAB: REGION VII ERA METHOD: 62 41 W00 CASE:SAMPLE PREP: ANALYST/EN" 'RY: DME REVIEWER:

DATA FILE : DllDATE:

SAMPLES TK9B8102 TK9BB1 05 F

CHLOROMETHANE 12 Ll 12 U ABROMOMETHANE r-i /—.»L. all. U UVINYL CHLORIDE 14 U 14 LICHLOROETHANE 14 U 14 UMETHYLENE CHLORIDE 10 U 10 U

ACETONE 10 U 10 UCARBON DISULFIDE 5.0 U 5.0 U1 . 1 - D I C H L. 0 R 0 E T H E N E 5.0 U 5. 0 U

1,1 D1CHLOROETHANE 5. 0 U 5.0 IJ

1,2,-DICHLOROETHENE 5. 0 U 5.0 U

CHLOROFORM 5.0 U 5.0 U1,2,DICHLOROETHANE 5.0 u 5. 0 U

2—BUT A NON El 10 U 10 U1,1,1~TRICHLOROETHANE 5 KI 0 U 5.0 IJC A R B 0 N T E T R A C H i... 0 RIDE 5. 0 L.I 5.0 U

VINYL ACETATE 10 LI 10 U

BRGMODICHLOROMETHANE 5.0 LI 5.0 u

1,2-DICHL0R0PR0PANE 5,0 U 5. 0 LI

CIS-1„3-DICHL0R0PR0PENE 5.0 U 5.0 U

TRICHLOROETHENE 5.0 IJ 5.0 LI

ênzene 5.0 u 5.0 U

B R 0 M 0 C H L 0 R 0 M E T14 A N E 5.0 U 5.0 IJ

T,1,2-TRICHLOROETHANE 5.0 LJ 5. 0 LITRANS-1,3-DICHL0R0PRQPENE 5.0 IJ 5.0 IJBROMOFORM 5. 0 IJ 5, 0 U4—M E T H Y L—2—P E N T A N 0 N E 10 u 10 U

2-HEXANONE 10 IJ 10 U

1,1,2,2-TETRACHL0R0ETHANE 5.0 u 5.0 LI

T E! T R A C H L 0 R 0 E T H E N E 5.0 IJ 5 - 0 U

TOLUENE 5.0 IJ 5.0 IJ

CHLOROBENZENE 5. 0 u 5. 0 U

ETHYL. BENZENE 5.0 IJ 5. 0 u

STYRENE 5. 0 IJ 5. 0 u

TOTAL XYLENES 5.0 u 5.0 LI

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12/14/88

ecology and environment, inc.CLOVERLEAF BUILDING 3, 6405 METCALF, OVERLAND PARK, KANSAS 66202, TEL. 913/432-9961

International Specialists in the Environment

MEMORANDUM

TO: Andrea Jirka, PhD, Chief, LABOTHRU: Paul Doherty, DPO

FROM: Peggy Cox, TATTHRU: Audra Gier, ATATLO^^

Joe Chandler, TATI^?

DATE: February 2, 1989

SUBJECT: Review of data for WATERLOO COAL GAS TDD# T07-8810-044 PAN# T07-Z054-QSG

These data were reviewed according to the "Laboratory Data Validation Functional Guidelines for Evaluating Organic Analyses," February 1, 1988 revision and the "Laboratory Data Validation Functional Guidelines for Evaluating Pesticides and PCBs."

The following comments and attached data sheets are a result of Ecology & Environment, Inc.'s review of the above mentioned data from the contract laboratory.

CASE NO.: 11157 LABORATORY: TMA/NORCALCONTRACT NO.: 68-W8-0009 METHOD NO.: 9303M02SITE: WATERLOO COAL GAS EPA ACTIVITY : TK9B8REVIEWER: P. COX MATRIX: SOIL

SMO SAMPLE NOS. EPA SAMPLE NOS.

GF797 GF807 TK9B8001 TK9B3011GF798 GF808 TK9B8002 TK9B8012GF7 99 GF809 TK9B8003 TK9B8013GF800 GF810 TK9B8004 TK9B8014GF801 GF811 TK9B8005 TK9B8015GF802 GF812 TK9B8006 TK9B8016GF803 GF813 TK9B8007 TK9B8017GF804 GF814 TK9B8008 TK9B8018GF805 GF815 TK9B8009 TK9B8019 .GF806 TK9B8010

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recycled paper

GENERAL

/\

Case 11157 contained 19 soil samples analyzed for base/neutrals and acids at the medium level concentration. Laboratory did not report tentatively identified compounds (TICS) on Form IF for several samples. Since identification and concentrations of the tentatively identified compounds were not known, instruction was to report them wifeh^fiothing significant 'found.

HOLDING TIMES and PRESERVATION

No technical holding times or required preservation are specified for soil samples.

GC/MS TUNING

All GC/MS tunings and mass calibrations were within quality control limits for all associated data.

INITIAL and CONTINUING CALIBRATION

Pyrene, benzo(a)anthracene, chrysene, indeno(1,2,3-cd)pyrene along with other compounds were outside quality control limits for percent relative standard deviation (%RSD) on the initial calibration. Several compounds including phenanthrene, anthracene, benzo(k)fluoranthene, dibenz(a,h)anthracene, and benzo(g,h,i)perylene were outside quality control limits for percent difference (%D) on the continuing calibrations. All sample data was qualified by the calibration rules.

INTERNAL STANDARD RESPONSE

All internal standard response areas were within a factor of 2 when comparing samples and their associated continuing calibration response areas.

BLANKS

Two method blanks were analyzed for base/neutrals and acids and no compounds were reported.

SURROGATE RECOVERY

All compounds were recovered within quality control limit requirements.

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MATRIX SPIKE/MATRIX SPIKE DUPLICATE

A matrix spike/matrix spike duplicate was analyzed for base/neutrals and acids and 2,4-dinitrotoluene was outside quality control limit requirements for percent recovery on the matrix spike and matrix spike duplicate and 2-chlorophenol was outside control limits for percent recovery on the matrix spike. Uo data was qualified by the matrix spike/matrix spike duplicate.

PERFORMANCE EVALUATION SAMPLE

No performance evaluation sample was submitted to the laboratory for analysis.

COMPOUND IDENTIFICATION and QUANTITATION

All samples were correctly identified by mass spectra submitted for each positive sample response.

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