Reduction Kinetics of Thermally Reduced Graphene Oxide ...pustaka.unpad.ac.id/wp-content/uploads/2017/11/Abstrak-Reduction... · Universitá di Milano Bicocca, Dipartimento di Scienza

Publikasi di Jurnal Internasional

ISSN : 0255-5476, ISBN-13: 978-3-03835-547-2

Reduction Kinetics of Thermally Reduced

Graphene Oxide Thin Films

Materials Science Forum 827, 317-320 (2015)

Fitrilawati, Norman Syakir, Annisa Aprilia,

Zhouyang Liu, Xinliang Feng and Christoph

Bubeck

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Materials Science Forum

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Home > Our library > Materials Science Forum > Functional Properties of Modern Materials

Functional Properties of Modern Materials

978-3-03835-547-2

Risdiana, Kuwat Triyana and Agustinus Agung Nugroho

Selected, peer reviewed papers from the 2nd International Conference on Functional Materials Science (ICFMS 2014), November 12-13, 2014, Lombok, Indonesia

406

2015

Materials Science Forum Vol. 827

softcover

table of contents

Description:

Collection of selected, peer reviewed papers from the 2nd International Conference on Functional Materials Science. The 66 papers are grouped as follows: Chapter 1: Materials in Environmental Engineering; Chapter 2: Materials in Biomedical Engineering; Chapter 3: Materials for Devices of Conversion and Storage of Energy; Chapter 4: Ferromagnetic and Superconducting Materials; Chapter 5: Materials for Sensors; Chapter 6: Researching and Designing of Fabrication Technologies; Chapter 7: Applied Research Techniques of Phenomena in Solid State Materials

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p.13

p.19

p.25

p.31

p.37

p.43

p.49

Home > Our library > Materials Science Forum > Functional Properties of Modern Materials > ToC

Table of contents



Papers published in this volume:

Preface, Conference Organizers and Organizing Committee

Deposition of Ag 2~6 mol%-Doped ZnO Photocatalyst Thin Films by Thermal Spray Coating Method for E.coli Bacteria DegradationHeri Sutanto, Iis Nurhasanah, Eko Hidayanto

Photocatalytic Activities of Electrospun TiO /Styrofoam Composite Nanofiber Membrane in Degradation of Waste WaterAbdul Rajak, Muhammad Miftahul Munir, Abdullah Mikrajuddin, Khairurrijal

Magnetic Composite Fe O /CuO/TiO Nanoparticles: Preparation, Characterization and Photocatalytic ActivityShofianina Jalaludin, Sarah A. Arifin, Rosari Saleh

Photocatalytic Activity of Fe-Doped ZnO/Montmorillonite Nanocomposite for Degradation of Malachite GreenNur Afifah, Nadia Febiana Djaja, Rosari Saleh

Comparative Study of Photocatalytic Activity of Ni-Doped ZnO and Zeolite Supported Ni-Doped ZnO Prepared by Co-Precipitation MethodRaynaldi Philipus, Annisa Noorhidayati, Nadia Febiana Djaja, Rosari Saleh

Comparative Study on Photocatalytic Performance of (La,Fe) and (Ce,Fe)-Codoped ZnO NanoparticlesNadia Febiana Djaja, Rosari Saleh

Preparation, Characterization and Photocatalytic Activity of Multifunctional Fe O /ZnO/CuO Hybrid NanoparticlesArdiansyah Taufik, Iqriah Kalim, Rosari Saleh

Photocatalytic Activity of Zeolite Supported Transition Metal-(Co and Cr ) Doped ZnO: Comparative StudyAnnisa Noorhidayati, Mia Putri Rahmawati, Nadia Febiana Djaja, Rosari Saleh

Preparation, Characterization of Fe O /TiO /CuO Nanohybrid and its Potential Performance for Chromium Removal from Aqueous SolutionSarah A. Arifin, Shofianina Jalaludin, Rosari Saleh

1 2 3 4 5 … > >>

2

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Periodical:

Volume:

p.56

p.62

p.67

p.75

p.81

p.87

p.91

p.95

p.99

p.105


Table of contents




UV-Light Absorption and Photocatalytic Properties of Zn-Doped CeO Nanopowders Prepared by Ultrasound IrradiationAula Fitra Efendi, Iis Nurhasanah

Growth and UV Absorption of 5 mol% Zn-Doped CeO Nanoparticle Synthesized with a Simple Precipitation ProcessIis Nurhasanah, Aula Fitra Efendi, Heri Sutanto, Priyono

Synthesis, Characterization and Photocatalytic Performance of ZnO/TiO and ZnO/TiO /CuO NanocompositeAlfred Albert, Rosari Saleh

Preparation and Characterization of Magnetic Carbonate Apatite/Chitosan/Alginate Composite ScaffoldDecky Jusiana Indrani, Bambang Sunendar Purwasasmita, Wisnu Ari Adi, Jojor Simanjuntak

Bone Scaffold Based on Biopolymer/Carbonate Apatite by Freeze Drying Method: Synthesis, Characterization, and In Vitro CytotoxicityAbdul Halim Daulay, Decky Jusiana Indrani, Muhammad Rifqi Aufan, Aditianto Ramelan, Mardjono Siswosuwarno, Bambang Sunendar Purwasasmita

Sintering Behavior and Diametral Tensile Strength Properties of Hydroxyapatite-Zirconia CompositesEko Pujiyanto, Pringgo Widyo Laksono, Sagiran

Electrospun Polyvinylpyrrolidone as a Carrier for Leaves Extracts of Anredera cordifolia

(Ten.) SteenisAde Yeti Nuryantini, Dhewa Edikresnha, Muhammad Miftahul Munir, Khairurrijal

Fabricating Polyvinyl Alcohol Fibers with Evenly Distributed Nano SilverHarsojo, Anna Layla, Kuwat Triyana, Harini Sosiati

Characterization of Optical and Structure Properties of PolydimethylsiloxanesHanif Sulistiya Nusa, Widi Astuti, Arief Sjamsulaksan Kartasasmita, Rova Virgana, Norman Syakir, Ayi Bahtiar, Lusi Safriani, Risdiana

Measurement of Glucose in Blood Using a Simple Non Invasive MethodMuhammad Sainal Abidin, Abdul Rajak, Rahmat Awaludin Salam, Muhammad Miftahul Munir, Khairurrijal

< 1 2 3 4 5 … > >>

2

2

2

2


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Periodical:

Volume:

p.113

p.119

p.125

p.131

p.135

p.140

p.146

p.151

p.156

p.162


Table of contents




AC-MnO -CNT Composites for Electrodes of Electrochemical SupercapacitorsAgus Subagio, Priyono, Pardoyo, Aswardi, R. Yudianti, A. Subhan, E. Taer

Optical, Structural and Morphological Properties of Ternary Thin Film Blend of P3HT:PCBM:ZnO NanoparticlesAyi Bahtiar, Siti Halimah Tusaddiah, Wendy Paramandhita S. Mustikasari, Lusi Safriani, Mariah Kartawidjaja, Kei Kanazawa, Ippei Enokida, Yukio Furukawa, Isao Watanabe

Conduction Properties of PTMSPMA-PEO and its Application as Polymer Electrolyte in LiFePO BatteriesSahrul Hidayat, Orina Amelia, Iman Rahayu, Fitrilawati

μSR Study of Charge Carrier Motion in Active Layer P3HT:ZnO:PCBM Hybrid Solar CellsLusi Safriani, Risdiana, Ayi Bahtiar, Annisa Aprilia, I. Kawasaki, Isao Watanabe

The Effect of Sintering and Soaking Temperature on the Dye-Sensitized Solar Cell PerformanceTika Paramitha, Tifa Paramitha, Agus Purwanto

Study on Carbon-Coated LiMn Fe Ni PO (0 ≤ x ≤ 0.15) as Cathode Material for Lithium Ion BatteriesJoko Triwibowo, Jan Setiawan, Raden Ibrahim Purawiardi, Bambang Prihandoko

Effect of LiFePO Cathode Thickness on Lithium Battery PerformanceAriska Rinda Adityarini, Eka Yoga Ramadhan, Endah Retno Dyartanti, Agus Purwanto

Effect of TiO on Duck Eggshell Membrane as Separators in Supercapacitor ApplicationsD. Dahlan, N. Sartika, Astuti, E.L. Namigo, E. Taer

Enhancement of Lithium Battery Performance by Thickness Anode Film ModificationRani Cahyani Fajaryatun, Therecia Wulan Sukardi, Arif Jumari, Agus Purwanto

Study of Interfacial Charge Transfer Loss in Hybrid Solar Cells by Impedance SpectroscopyRahmat Hidayat, Yolla Sukma Handayani, Priastuti Wulandari

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4

0.7 0.3-x x 4

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Periodical:

Volume:

p.168

p.174

p.180

p.186

p.192

p.203

p.208

p.213

p.219

p.223


Table of contents




Study of Charge Carrier Dynamics of P3HT:PCBM Blend for Active Material Solar Cell Using Muon Spin RelaxationA. Bahtiar, Lusi Safriani, Annisa Aprilia, Risdiana, Harsojo, Triwikantoro, Darminto, Agustinus Agung Nugroho, Hanjie Guo, Ikuto Kawasaki, Isao Watanabe

Microscopic Characterization of Cellulose Nanocrystals Isolated from Sisal FibersHarini Sosiati, Mu'minul Muhaimin, Purwanto, Dwi Astuti Wijayanti, Harsojo, Soekrisno, Kuwat Triyana

Effects of Gamma Radiation on Electrical Conductivity of PVA-CH CompositesSusilawati, Aris Doyan

Synthesis and Characterization of Carbon-Coated LiFePO with Various Carbon Sources as Cathode Material for Lithium Ion Batteries through a Solid-State ProcessJoko Triwibowo, Irvan Alamsyah, Jan Setiawan

Optical Property Enhancement of Silica-Modified Polyaniline Grown on Glass Substrate via Incorporation of Zinc Sulfide into the Polymer MatrixMelchor Jocanain Potestas, Arnold C. Alguno, Reynaldo M. Vequizo, Bianca Rae B. Sambo, Majvell Kay G. Odarve

Explorative Synthesis of Magnetic Ca-Fe-O Compounds by Mixing Precipitated CaCOfrom Limestone and Iron Sand Extracted – Fe O .H OMastuki, Malik Anjelh Baqiya, Darminto

Simulation Analysis of Damage Mechanism on Ferritic Material SA-213 T22 Type Using Finite Element Method ProgramCukup Mulyana, Otong Nurhilal, Adhitya Rusel Syah, Nendi Suhendi

Nano-Structural Studies on Fe O Particles Dispersing in a Magnetic Fluid Using X-Ray Diffractometry and Small-Angle Neutron ScatteringAhmad Taufiq, Sunaryono, Edy Giri Rachman Putra, Suminar Pratapa, Darminto

Synthesis of Cobalt Ferrite Particles by Utilized Sol-Gel MethodTogar Saragi, Siti Nurjannah, Ricca Novia, Norman Syakir, Edward Simanjuntak, Lusi Safriani, Risdiana, Ayi Bahtiar

The Orientation Study of Ba-Sr Hexaferrite Particles by Parallel Magnetic Field PressAgus Sukarto Wismogroho, Wahyu Bambang Widayatno, Toto Sudiro, Didik Aryanto

<< < … 2 3 4 5 6 … > >>

4

3

2 3 2

3 4



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Periodical:

Volume:

p.229

p.235

p.240

p.243

p.251

p.257

p.262

p.266

p.271

p.279


Table of contents




Various Magnetic Properties of Magnetite Nanoparticles Synthesized from Iron-Sands by Coprecipitation Method at Room TemperatureSunaryono, Ahmad Taufiq, Mashuri, Suminar Pratapa, M. Zainuri, Triwikantoro, Darminto

Effect of Pb Substitution on Superconducting and Normal State Electrical Properties of Bi Sr CaCu O NanopowdersFahmi Astuti, Malik Anjelh Baqiya, Darminto

Electronic Structure of Muonated La CuOAinul Fauzeeha Rozlan, Shukri Sulaiman, M.I. Mohamed-Ibrahim, Isao Watanabe

Study of Thermal Conductivity due to Spins in One-Dimensional Spin Systems AFeX(A=Rb, Cs; X=Cl, Br)Riesma Tasomara, T. Kawamata, Y. Matsuoka, H. Sudo, K. Naruse, M. Ohno, H. Nagasawa, Y. Hagiya, T. Sasaki, Risdiana, Yoji Koike

SnO Films Decorated by Au Clusters and their Gas Sensing PropertiesGhenadii Korotcenkov, Vladimir Brinzari, S.H. Han, L.B. Gulina, V.P. Tolstoy, B.K. Cho

Modification of Polystyrene Morphology and its Influence to the Coated Zinc Phthalocyanine Layer and Frequency Change in QCM SensorMasruroh, D.J.D.H. Djoko, Lalu A. Didik, Eka Rachmawati, Fadli Robiandi, Masdiana Padaga, S.P. Sakti

Effect of Nb O Addition to the Electrical Properties of Fe TiO Ceramics-Based NTC ThermistorWiendartun, Risdiana, Fitrilawati, Rustam E. Siregar

Functionality of ZnPc Thin Film Deposited on Polystyrene Interlayer for Immobilization of Biomolecules in QCM Based BiosensorD.J. Djoko H. Santjojo, Masruroh, Sri Widyarti, Fadli Robiandi

Fabrication of Photonic Crystal Based on Polystyrene ParticlesLusi Safriani, Ian Sopian, Tuti Susilawati, Sahrul Hidayat

Synthesis of Styrofoam Fibers Using Rotary Forcespinning TechniqueAhmad Fauzi, Dhewa Edikresnha, Muhammad Miftahul Munir, Khairurrijal

<< < … 3 4 5 6 7 >

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3

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2 5 2 5



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Periodical:

Volume:

p.285

p.290

p.294

p.300

p.306

p.311

p.317

p.321

p.326

p.332


Table of contents




Study on Phase, Molecular Bonding, and Bandgap of Reduced Graphene Oxide Prepared by Heating Coconut ShellAnanda Yogi Nugraheni, Muhammad Nasrullah, Fandi Angga Prasetya, Fahmi Astuti, Darminto

Study of Raman Spectroscopy on Graphene Phase from Heat Treatment of Coconut (Cocus nucifera) ShellFandi Angga Prasetya, Muhammad Nasrullah, Ananda Yogi Nugraheni, Darminto

Characterization of Al-Si-Mg/Al O Nanocomposite Produced by Stir Casting MethodAnne Zulfia, J. Salahuddin, Hafeizh E. Ahmad

Fe-Si-Al Alloys Prepared by a Spark Plasma Sintering TechniqueToto Sudiro, Kemas Ahmad Zaini Thosin, Didik Aryanto, Agus Sukarto Wismogroho, Kazuya Kurokawa

Synthesis of Amylopectin Macro-Initiator for Graft Copolymerization of Amylopectin-g-Poly(Methyl Methacrylate) by ATRP (Atom Transfer Radical Polymerization)Aniek S. Handayani, Is Sulistyati Purwaningsih, Muhamad Chalid, Emil Budianto, Dedi Priadi

Preparation and Characterization of Ni/Zr-Saponite as Catalyst in Catalytic Hydrogen Transfer Reaction of IsopulegolIs Fatimah, Dwiarso Rubiyanto, Thorikul Huda

Reduction Kinetics of Thermally Reduced Graphene Oxide Thin FilmsFitrilawati, Norman Syakir, Annisa Aprilia, Zhou Yang Liu, Xin Liang Feng, Christoph Bubeck

Electrospun Nanofibers Based on Polyvinyl Alcohol/Chitosan and its Stability in KOH SolutionKuwat Triyana, M. Solihul Mu’min, Kuni Faizah, Yusril Yusuf, Ahmad Kusumaatmaja, Harsojo

Study of Alkalization to the Crystallinity and the Thermal Behavior of Arenga Pinnata “Ijuk” Fibers-Based Polylactic Acid (PLA) BiocompositeMuchamad Chalid, Evana Yuanita, Juniko Pratama

Preparation of Zn-ZrO Nanocomposite Coating by DC and Pulsed Current Electrodeposition Technique with Low Current DensityAsep Ridwan Setiawan, Marsetio Noorprajuda, Aditianto Ramelan, Rochim Suratman

<< < … 3 4 5 6 7 >

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p.341

p.347

p.355

p.360

p.366

p.371

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Table of contents




Electron Microscopy Study of Grain Boundary Behavior in Pb-Free Solder Materials for Mitigation of WhiskersNoriyuki Kuwano, Sadanori Horikami, Marina Linus

Muon Site Estimations by DFT Calculations in Metal and Insulating SystemsIsao Watanabe, E. Suprayoga, N. Adam, S.S. Mohm-Tajudin, A.F. Rozlan, D. Puspita, R. Asih, F. Astuti, M.D. Umar, J. Angel, S. Sulaiman, M.I. Mohamed-Ibrahim

Electronic Structure of Muonated Me P[Pd(dmit) ]Shukri Sulaiman, S.N.A. Ahmad, M.I. Mohamed-Ibrahim, Isao Watanabe

Phonon Properties of Co:TiO Single CrystalH. Setiadi, A. Prasetyo, V. Suendo, Agustinus Agung Nugroho

Failure Analysis Study of Dissimilar Metal Weld SA-213 T22 and SA-213 TP304H at Boiler Tube Steam Power GenerationCukup Mulyana, Aswad Hi Saad, Mariah Kartawidjaja, Agtri Henboral

The Effect of Graphite and NBR on the Hardness of Fly-Ash/Phenolic Composite for Brake Lining ApplicationShirley Savetlana, Gusri Akhyar Ibrahim

Effect of Soaking Time in Alkali Solution on the Interfacial Shear Strength of Cantala Fiber/Recycled HDPE CompositesWisnu R. Wijang, Heru Sukanto, Miftahul Anwar

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Reduction Kinetics of Thermally Reduced Graphene Oxide Thin Films

Fitrilawati1,a, Norman Syakir1, Annisa Aprilia1, Zhouyang Liu2,

Xinliang Feng2 and Christoph Bubeck2 1Department of Physics University of Padjadjaran, Jl Raya Jatinangor Km 21 Sumedang

West Java Indonesia

2Max Planck Institute for Polymer Research, Ackermannweg 10, 55128 Mainz, Germany

[email protected]

Keywords: graphene oxide, reduced graphene oxide, thermal reduction, spin coating.

Abstract. We report an experimental study of thermal reduction of graphene oxide (GO) under

nitrogen flow. Ultrathin films of GO were prepared on quartz glass substrates by spin-coating from

3 mg/ml aqueous solutions of GO. These films were annealed at 50 °C under vacuum overnight

before thermal reduction. The films were exposed to temperatures of 100 °C, 150 °C, 200 °C, 300

°C, 400 °C, 500 °C and 800 °C under nitrogen flowing. We used UV-Vis absorption spectroscopy

to monitor the change of absorption spectra caused by thermal reduction. We observed a significant

change of absorption spectra due to formation of reduced graphene oxide (RGO). We found that

thermal reduction started already at 100 °C, but proceeded significantly faster at heating

temperatures higher than 200 °C.

Introduction

Graphene is attracting a lot of attention due to its promising properties for electronic devices [1].

There are several methods in preparing graphene, such as micromechanical exfoliation [1],

chemical vapor deposition (CVD) [2], epitaxial growth [3], and the reduction of graphene oxide

(GO) [4,5]. Amongst the methods, the reduction of GO is a low-cost approach to prepare graphene-

based materials in a large scale, since GO is commercially available.

Single sheets of graphene oxide are prepared by oxidation of graphite in the presence of strong

acids and oxidants, followed by a subsequent exfoliation of GO sheets under ultrasonication

treatment. An illustration of GO structure is shown in Fig. 1. The GO sheets are decorated with

oxygen-containing functional groups such as carboxylic, hydroxylic and epoxidic groups. The GO

contains both sp2-

and sp3-

hybridized carbon atoms. Therefore, GO is nearly electrically insulating.

Thermal reduction can remove the oxygen-containing groups from GO and can heal the defects of

the conjugated π-electron system of GO. A schematic view of the conversion of GO to RGO is

shown in Fig. 1, which illustrates the recovery of sp2-binding sites in RGO. The restoration of sp

2-

carbon sites and the recovery of the conjugated π-electron system is indicated by the strongly

increasing UV-Vis absorption spectra of RGO.

Figure 1. Schematic structures of graphene oxide (GO) and reduced graphene oxide (RGO) [5].

Materials Science Forum Vol 827 (2015) pp 317-320 Submitted: 2014-11-08© (2015) Trans Tech Publications, Switzerland Revised: 2015-03-26doi:10.4028/www.scientific.net/MSF.827.317 Accepted: 2015-04-20

All rights reserved. No part of contents of this paper may be reproduced or transmitted in any form or by any means without the written permission of TransTech Publications, www.ttp.net. (ID: 111.223.255.4-25/05/15,07:05:35)

http://dx.doi.org/10.4028/www.scientific.net/MSF.827.317

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