RADIATION AND DESIGN BASIS ACCIDENT TESTING OF › docs › ML0706 › ML070600220.pdfSet Lower Autoclave controller to desired setting, manual output at zero. 5. Close two (2) valves

_. . 856 Echo Lake Road P. 0. Box 460 Watertown, CT 06795 Tel: 860-274-6701 Fax: 860-274-5857

RADIATION AND

DESIGN BASIS ACCIDENT TESTING

OF THIN FILM TECHNOLOGY’S BIO-DUR 561

CONDUCTED FOR: Tennessee Valley Authority 1101 Market Street, LP4H Chattanooga, TN 37402-2801

Underwater Construction Corporation 1260 Seminole Drive Indian Harbour Beach, FL 32937

REQUESTED BY:

CONDUCTED BY:

Robert L Phillips, TVA Program Manager Materials and Metallurgical Engineering

Charles A. Vallance, UCC Division Manager

University of Massachusetts Lowell Radiation Laboratory Keeler 8 Long PPG

1 REPORT NO. 05-0209 ISSUED: February 25,2005

THE TECHNICAL DATA PRESENTED IN THIS REPORT ARE BASED UPON TESTING AND ANALYSIS USING THE BEST PROCEDURES AND PRACTICES KNOWN TO KEELER & LONG I PPG AT THE PRESENT TIME. THIS REPORT SHOULD NOT BE INTERPRETED AS A RECOMMENDATION FOR ANY PARTICULAR USE AND IS NOT A REPRESENTATION OR WARRANTY OF PREFORMANCE. THIS REPORT IS INTENDED FOR USE BYA QUALIFIED NUCLEAR COATINGS SPECIALIST.

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I . ,-. . . : .

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0

TVA and UCC DBA Summary DBA Test Conditions K&L PPG Autoclave Calibration K&L PPG Autoclave Operation Procedures

.. -

TVA and UCC: Test Parameters and Correspondence UMLRadiation Laboratory Test Samples Irradiation Report UMLCertificate of Exposure UMtCertificate of Irradiation

_ . _ . ) . _ . . . . . . . . . . . ..

856 Echo Lake Road P. 0. Box 460 Watertown, CT 06795 Tel: 860-274-6701 Fax: 860-274-5057

Keeler & Long PPG NAS Test Facility Date: February 9,2005

Report of Radiation Tolerance And Design Basis Accident Testing

For Tennessee Valley Authority

Browns Ferry Nuclear Power Plant

The Radiation Tolerance Testing was preformed at the University of Massachusetts Lowell Radiation Laboratory. Testing was done in accordance with Tennessee ValIey Authority’s Contract #00010630 faxed on 08/24/04 (Section 2 of this Report) and Undenvater Construction Corporation’s Contract #04- 32Q faxed on 09/17/04 (Section 2 of this Report), UML Radiation Laboratory Document No. uML-12- 08-04PPG/TVA (Section 2 o f this Report), Keeler & Long PPG Purchase Order #700327 (Section 2 of this Report), and the requirements of ASTM D-4082 Test Method for Effects of Radiation on Coatings for Use in Light Water Nuclear Power Plants.

The Design Basis Accident (DBA) Testing was performed at Keeler & Long PPG NAS Testing Facility. This icst ’v‘r7r~ zondnctzd in accordance with Tennessee Valley Authority’s Cor.tract # O W 1063 0 faxc3 03 08/24/04 (Section 2 of this Report) and Underwater Construction Corporation’s Contract #04-32Q.faxed- .. on 09/17/04 (Section 2 of this Report), the requirements of ASTM D3911-03 Standard Test Method for Evaluating Coatings Used in Nuclear Power Plants at Simulated Design Basis Accident (DBA) Conditions, and Keeler & Long PPG Quality Assurance Procedures R&D 1.?3 and R&D 124 (Section 1 of this Report).

Evaluated By:

. . ... .. .

90

90-2 18

856 Echo Lake Road .’ P. 0. Box 460 Watertown, CT 06795 Tel: 860-274-6701 Fax: 860-274-5857

0 Steam Generator preheated for 24 Hours . 040.5 Steam Injected

, Manufacturer: Thin Film Technology

~

21 8

218-116

Keeler & Long PPG Test Report: 05-0209

.< , -. -- 40.5-24.0 Recirculating pump initiated

24.0-20.3 Test ended at 11.5 Days from Start Time

Keeler & Long PPG NAS Test Facility Date: 02/09/05

1 Table 1. DBA Test Solution

Reagent Concentration 1 - I

1 Deionized Water 100%

Table 2. DBA Test Conditions

Time

~ --

Start Time: 9:45 am 7Hours

7 Hours-1 5 Minutes

7HrsM 5Mins- 11.5Days

Temp OF I Pressure (psi) I Comments

90 I 0 1 Autoclave preheated for 24 Hours 1

I 1 -I

h

Evaluated By: a F- Approved By: L--<-S

CALIBRATION OF AUTOCLAVE

PRESSURE:

Before test - calibrate Ashcroft gage to Bristol Babcock Pressure Transmitter Series 2508 158-230- 212-000-100. Then remove Ashcrofl gage and replace with Helicoid pressure gage.

TEMPERATURE:

Remove Thermocouple from top cf Autoclave. Put Thermocouple in oil along wilh GAibrated thermometer and bring to high temperature range of test plus 10'F. If calibration is off, re-calibrate temperature transmitter. Remove Thermocouple Probe and thermometer from oil and clean. Put both in boiling water and repeat procedure. Put both in ice water and repeat procedure. Repeat procedure as necessary if calibration is off.

. .

AUTOCLAVE CALIBRATiON FREQUENCY:

Calibrate temperature and pressure prior to use.

PRESSURE CALLIBRATION

Calibrated Gage Autoclave Recorder SL.

30 psi XP,? 60 mi 59.6 70 Dsi 61. (

AUTOCLAVE CALIBRATION

Calibrated Thermometer Ice Water HoVBoiling Water High Range Oil ---- .3 7 , '7 E -- - f 77,x-

-- 3%

a s -- ._

2xg; 2 .,* -? ..-

Calibrated By:

9 . . 1 --- 1s:ued ,;!.&? --- L lderrtification No. ----

07-29-98 Cii'k: '* H ~ L , R&D-I23 Revised Appr: /j+--- '

Origin CALIBRATION OF AUTOCLAVE 07-23-04 Sheet 1 of- 1 Revision 3 No.,

P&D

1.

2.

3.

4.

5.

6.

7.

8.

9.

10.

11.

12.

13.

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i

j AUTOCLAVE OPERATION PROCEDURES i

Prior to any work ALL lockouts must be in place and in locked position

Autoclave should be dry and clean.

Prepare fresh spray solution ahead of time. Send for independent verification and certification. (When required)

Open two (2) red valves on steam generator site tube

Remove lockout from valve #3 and place in open position

Remove lockouts from valves #4 8 #5 then place in open position

Fill steam generator to indicator line on site tube.

Turn electric control panel switch to on position, adjust steam generator control set point to 212'F

While venting steam generator bring to 212°F.

When steam generator reaches 2 1 P F close valves #l , #2, and #3 on steam generator and replace lockouts

Close two (2) red valves On steam generator site tube

Adjust steam generator set poini to required temperature dependant on initial ramp. DO NOT EXCEED 37S°F OR 170 psi

Fill Autoclave with enough deionized water (or spray solution as specified) to cover lower heating element. '

,. Issued By: p22 --- .

07-29-98 Ch'k NE--3 Identification No.

RBD-124 Revised Appr: @A . I

AUTOCLAVE 12-15-04 OPERATION PROCEDURES Revision No. Sheet 1 o! %

Origin

R & D 3 -

14. Attach test specimens to rack. Place specimen rack in Autoclave.

15. Place lid on P.utoclave apd bolt together.

16. Attach regulated steam line.

17. Attach unregulated steam line. ..*

18. Lockout valves #1 & #2 far safety.

19. Connect air supply line to Autoclave remove lockout #6 and shut valve.

20. Pre-set air pressure line to desired minimum (if required).

2 1. Pre-set steam regulator to desired setting.

22. Connect recirculation pump line to Autoclave and shut valve.

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23. Connect fresh spray solution line to Autoclave shut valve.

24. Preset fresh spray regulator to desired pressure.

25. Put suction hose and by-pass in fresh spray solution container.

26. Connect pressure transmitter line to Autoclave, open valve and attach #8 lockout

27. Connect Thermocouple to Autoclave.

I

28. Put recorder paper in Autoclave recorder.

29. Check Recirculation Pump screens and clean if required.

. Issued By: 07-29-98 Ch'k

___- IdentificatiGn NO.

R&D-I24 Revised Appr:

TO BEGIN TEST:

1. Allow Autoclave to maintain pre-LOCA temperature for one (1) hour minimum (or as specified).

-- A7.3 " M e 4 ht??

2. Fill fresh spray solution bucket per specification and record temperature (If required).

AUTOCLAVE 12-15-04 OPERATION PROCEDURES Revision NO. Origin

3. Set Upper Autoclave controller to desired settings, manual output at zero.

\ Sheet Gf '

4. Set Lower Autoclave controller to desired setting, manual output at zero.

5. Close two (2) valves on Autoclave site tube, then close and lockout #9 valve.

6. Set Upper Autoclave controller to manual at 100% output

7. Set Autoclave recorder to fast speed Tab 2, (If required).

8. Remove #I and #2 lockouts from steam generator.

9. Remove #4 and #5 lockouts and open valves #4 and #5 steam inlets on Autoclave.

I O . When Autoclave temperature reaches 2°F above pre-DBA setting the test is ready to begin

* READY TO BEGIN TEST . ,A;? .. -2- ..-

11 . Open valves #1 and #2 simultaneously on steam generator (NOTE TIME AND DOCUMENT). Note: Some tests may onry require use of one steam line.

12. When Autoclave temperature approaches desired temperature (minus 5-1 O°F of temperature spike), shut unregulated steam line valve #2

13. Bring Autoclave temperature to specification and maintain temperature with steam regulator

14. Set Autoclave Recorder to normal speed Tab 1 (If required) once temperature has stabilized, reducing pressure as necessary to meet specification. Note: Some tests may require air io maintain specified pressure.

15. When Autoclave temperature has stabilized, shut regulated steam inlet valve #I and allow temperature to be maintained by Upper Autoclave Controller.

16. Shut steam generator off. Replace Lockouts on valves #I, #2. #4, and #5.

:ssUc.J ldertiflcation No. 07-29-98

A*.

-7

By: Ch'k v).(&

KMJ-1 L4

Origin

R&D

Revised AUTOCLAVE 12-15-04

Revision No. Sheet 3 of 4 OPERATION PROCEDURES 3

ENDING TEST

33. Shut recirculation pump off, close upper and lower valves.

34. Make sure all valves attached to Autoclave are closed with the exception of the pressure transmitter.

35. Remove regulated steam line.

36. Remove unregulated steam fine.

37. Shut #6 valve and lockout, then remove air supply line.

38. Slowly release pressure from Autoclave by opening valve on air supply line.

39. Remove Autoclave site ttlbe line.

40. Remove pressure transmitter line.

41. Remove recirculation pump line.

42. Remove fresh spray injection line.

43. Stop Autoclave recorder and remove chart paper.

44. Open autoclave and remove test specimens.

TEST COMPLETE

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PEG PACK&€ NO. e- 14-9 B PAGE 7 d / b

k ? k & mcyrC d DBA Testing Work Scope

Specimen Preparation

Note: The term overcoatirecoat refers to overcoating !he simulated (or actual samples) old existing system with the new system to be evaluafed.

The term repair refers to the smaller repair test performed on the panel as described in ANSI N101.2., Section 5 (Although the actual surface prep and repair method and repair area may vary from the method describe in ANSI N101.2, it will be typical of actual plant conditions and shall envelope thq..tehnical requirements outlined in ANSI N101.2.)

TASK DESCRIPTION

AMERON TASKS

a.

b.

C.

d.

e.

f.

9.

Ameron shall prepare carbon steel panels identified on "Phase I, DBA Test Plan Matrix" for each "Base Coating" System identified (1 through 7). Each panel should meet the requirements ol ASTM A36 steel.

Each coating system shall have five panels 4 (2"x4") and 1 (2"x 8" as a Controt and to perform Adhesion testing on one side).

Specimens size shall be approximately 2" X 4" X l/q" or 11B"min.

Specimens shall have approximately 1/4" hole drilled near one end (for hanging).

Ameron shall labeled by stamping, tagging or other suitable means, with the following info derived from the attached "Phase I, DBATesting Matrix": [(Base Sys no., 1-1 2), (overcoat sys no. a- e.), (panel no. 1 - 5) (front or back, I or b) For Example: for Base coaling D6/66 to be overcoathecoat with Amerlock 400NT, Panel No. 1, Front Side would be idenlified as lalf. (this method may be revised if necessary with coordination with TVA).

Ameron shall insure all panels have initial surface prep similar to existing coatings (SSPC SP- 10) near white metal blast wivl a 1 - 3 mil anchor profile prior to application of the 'Base Coating" system.

"Base Coaling" shal be applied and cured following requirements specified in "Phase I, DBA Test Plan Matrix''.

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k.

1.

PEG PACKAGE NO.&&34%3 PAGE 23 d

&fad Repalr areas s I1 e prepped as part of the overcoathecoat application with 1M of one side of the "Base Coating" system removed to bare substrate and prepped in accordance with SSPC SP-11, with a minimum profile of 1 mil. The "Base Coating" shall be feathered, abraded by sanding or other TVA approved method and solved washed prior to overcoathecoat application of the system to be tested. This repair shall be in lieu of the guidelines specified in ANSI N101.2 (a technical justification for this repair method will be provided by TVA as an attachment to the final report).

Base Coating systems to be overcoated lrecoated shall be prepared for repair as described in (h) above and the remaining surface (both sides) shall be abraded by sanding. or other N A approved method, to remove gloss prior to overcoathecoat apptiiation.

Each panel shall either be coated with the initial(exis1ing) coating system as identified on the "Phase I, DBA Testing Matrix" or procure an original sample that has been remove from Unit I Primary Containment and overcoated with the designated "Phase I, DBA Testing Matrix" system.

All overcoathepair systems shall be applied in a single coat at the specified DFT located on the Phase I, DBA Testing Matrix.

Ameron coating systems to be overcoated hepaired shall be abraded to remove gloss and areas that transition from substrate to initial coating shall have a smooth feathered edge prior to overcoatlrepair.

KEELER & LONG TASKS

Base Coating systems to be overcoated lrecoated shall be prepared for repair as described in (b) below and the remaining surface (both sides) shall be abraded by sanding, or other TVA approved method, to remove gloss prior to overcoatlrecoat application.

Repair areas shall be prepped as part of the overcoatlrecoat application with 1/3 of one side of the "Base Coating" system removed to bare substrate and prepped in accordance wilh SSPC SP-11, with a minimum profile of 1 mil. The "Base Coating" shall be feathered, abraded by sanding or other TVA approved method and solvent washed prior to overcoathecoat application of the system to be tested. Thls repair shall be in lieu of the guidelines specified in ANSI N101.2 (a technical justification for this repair method will be provided by TVA as an attachment to the final report).

Keeler and Long shall overcoathepair all of their systems identified in the "Phase I, DBA Testing Matrix".

111.

IV.

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v11.

d. These systems shall be applied in a single coat following the parameters specified in the "Phase I, DBA Testing Matrix".

Repairability

a. Repairability shall be performed as described under Keeler & Long's Tasks, Section II, paragraph (a)

b. Repair shall include coating removal, feather edging existing coating and ' surface prep 8 profile utilizing SSPC-SP 11.

Adhesion .:.> .

Adhesion shall be performed by Keeler & Long (per ANSI N5.12) on the back of Ihe 7 control panels (3 dollies each panel).

Decontamination, Fire Evaluation and Thermal Conductlvitv Testinq

Decontamination, fire evaluation and thermal conductivity testing is not required as all the overcoathecoat systems have already been tested and approved lor these attributes.

Test Parameters

a. Radiation tolerance shall be 1 X 109 Rads total dose, max temp 1800 F. b. Dynamic elevated temperature-pressure test (DBA) may be simulated in either of

Iwo ways. As a continuous function As a step function, as many steps being used as are necessary 10 represent the DBA curve conservatively (ANSI N101.2)

c. Temperature max 3400 F. d. Pressure 70 psig min e. Follow the site specific Harsh Environment Curve (TVA will provide the curve to

Keeler and Long).

Acceptance Crileria

Blistering, Few intact size #4 (ff4, Few) ASTM D714 0 Chalking.,.Heavy chalking shall not be pennitled ASTM D659

Delarninationlpeeling. ..neither delamination nor peeling shall be permitted.

* Flaking ... ASTM D772

NOTE: Any other changes in coating properties not associated with separation or the release of coating shall not be cause for rejection.

PEG PACKAGE NO. d k - h&'@ PAGE ./b of ./g

#=&*tLli m.cw-c A- . VIII. Base Coatins System and Overcoat lRecoat Systems

= Ameron shall prepare the "Base Coating" system with following the requirements listed in the attached table prior to the overcoathecoats systems being applied.

s Keeler and Long and Ameron will prepare the OvercoatlRecoat over their specific coating systems following the requirements listed in the attached table.

Keeler and Long will perform the underwaier coating repair of the UCC candidate coa1i.q system.

IX. Attachments

Attachment 1, PHASE I , DBA TESTING MATRIX Attachment 2, BFN, Harsh Environment Curve

0

a

. .. .. .... . . .. ._^ . ._ . ...... ..

3 50

500

- 4 - 250 W (r 3 I-

2 200 W Q I W +

I50

100

SO

FZGURE: . \ A DBA L O C A AND MSLB

DRYWE L L TEMPERATURE RESPONSE

I I .

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I n

In

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B 0 In I .,...

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I I I i i I I I

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F I G U R E 2 DBA LOCA AND MSLB

WETWELC TEMPERATURE RESPONSE

200 r I I I I J 1 I I I 1 I I 1 I 1 [ 1 I t

*OBA LOCA P E A K TEMP - 177‘F A T 5.33 HOURS *MStB P E A K TEMP = i 7 7 . F A T 4 HOURS I90

4 0 60 100 3

f

. I.<....,"..L...- .

70

60

50

40

30

20

10

0

F I G U R E 3 OBA LOCA AND MSLB

WETWELL PRESSURE RESPONSE

I I I I I I

*DBA LOCA P E A K PRESSURE = 50 7 PSIA A T 6 7 SECONDS -+-MSCB P E A K PRESSURE = 44.8 P S I A A T 6 4 0 SECONDS -

TIME

. . , , .. , ,. . ,I . . . . . ,. .. . ., . , , _ _ , I , . . .. < . . . . . . . . . . %

Subsirate Surface Profile No,

1

lase Coating OvercoatRecoat system Cleanliness mils Coats

Steel SSPC-SPI 1 1.0-3.0 1 .O-3.0 . D6/66 a. Amerlock 400NT 6, I b 1

b. Amerlock 400NT ~ 1 8 6 1 '1 '1

OvercoaVRec Curing Requirements DFTmils

Final cure per Mfg 4 - 8 4 - 8 product requirements

l l 1 .O-3.0 1 <0$3..0 *=:

two week air dry 1 3 - 8 Final cure per Mfg 1 5 - 8 product requirements

I d. I I

!. D6 -- e.

a. K & L 654817107 I' bI I :,+ .I 4s .,-

d b. K & L9600N wlaccelerator I *

. > C.

d. I ' I

1.0-3.0 '1.0-3.0

two week air dry

product requirements >12 5 - 8 Final cure per Mfg

* 1 4 - 8 3 . 400 NT

... I I I Repair: 150° 2 5 for

11 - b I e. a. K & L9600N w/accelerator b. Amercoat 90 c. Arnerlock 400NT w/861

': r: L l .+% k' .I '( *;R

r .

1 .O-3.0 1 .O-3.0

two week air dry 1 5 - 8 Final cure per Mfg 1 4 - 8 product requirements

1.0-3.0 I 1 1 4 - 8 I Repair: 150" +- 5 for

4. 400NT w/861 ..? . ,

.I. ,

._. .., - 1, ,. :..: e.

a. K & L9600N wlaccelerator

c. Amcrcoat 90

, . . * d' , .:-. ','+,. ':a ',,% ( ( fi .,. ,-, ue-. .y$p$

.. - b. Amerlock 400 NT &I '-;3. " 1.0-3.0 1 1 1 - I Repair: 150" t 5 for

1 .O-3.0

-

5 - 8 Final cure per Mt'g 1 product requirements

Repair: 150' 5 for two week air dry

I UCC requirements

7. Vaispar 78 d. ~ - ( , v ,

a. UCC Bio-Dur 561 I

856 Echo Lake Road P. 0. Box 460 Watertown. CT 06795 Tel: 860-274-6701 Fax: 860-274-5857

Manufacturer: Thin Film Technolony Keeler & Lone. I’ PPG h e r o n Test Preformed for T.V.A.

Keeler & Long PPG NAS Test Facility Date: January 11,2005

System Identification: X Steel Concrete Other

Total Dose: 1.015~10~ Dose Rate: 1.26~1 O6 Irradiation Length: 81 1 .O Hours

Keeler & Long PPG Test Report: 05-0209 Uh4L - Radiation Laboratory Document Number: UML-12-08-04/PPGITVA Radiation Tolerance Test Results:

Samde No. Results

6A 1 F (Front) Color changed from white to medium yellow and the repair system color changed from light gray to mustard color. The repair system has dense pinholes or biowholes on surface. Coatings are inlact, no other defects. .-I . =. -.

6AlF (Back)

_..

Color changed from white to medium yellow. Coatings are intact, no other. defects.

Evaluated By: Approved By:

I -

6A2F (Back)

Results

Color changed from white to medium yellow and the repair system color changed from light gray to mustard color. The repair system has dense pinholes sr biowholes on surface. Coatings are intact, no other defects. . , .?< .. -.-. ’

Color changed fiom white to medium yellow. Coatings are intact, no other defects.

Evaluated By: e&


Manufacturer: Thin Film Technolorn Keeler & Long / PPG h e r o n Test Preformed for T.V.A.

System Identification: X Steel Coilcrete Other

Keeler & Long PPG NAS Test Facility Date: Januarv 11.2005

Total Dose: 1 .015~10~ Dose Rate: 1.26~1 O6 Irradiation Length: 8 1 1 .O Hours

Keeler & Long PPG Test Report: 05-0209 UML - Radiation Laboratory Document Number: UML-12-08-04/PPG/A Radiation Tolerance Test Results: a Samule No.

7A1F (Front)

7A1F (Back)

Results

Color changed from white to medium yellow and the repair system color changed from light gray to dark mustard color. The repair system has dense pinholes or blowhales on xrface. Coatings are intact, no other defects. _ _ :< *-. ..

,**

Color changed from white to medium yellow. Coatings are intact, no other defects.

EvaluatedBy: & Approved By:

856 Echo Lake Road P. 0. Box 460 Watertown, CT 06795 Yel: 860-274-6701 Fax: 860-274-5857

Manufacturer: Thin Film Technology Keeler & Long PPG NAS Test Facility Keeler & Long / PPG

h e r o n Date: January 1 1.2005 Test Preformed for T.V.A.

Other Svstem Identification: X Steel Concrete I

Total Dose: 1 . 0 1 5 ~ 1 0 ~ Dose Rate: 1.26~10~ Irradiation Length: 8 1 1 .O Hours

Keeler & Long PPG Test Report: 05-0209 UML - Radiation Laboratory Document Number: UML-12-08-04/PPG/TVA Radiation Tolerance Test Results:

Sample No.

7A2F (Front)

7A2F (Back)

Results

Color changed from white to medium yellow and the repair system color changed from light gray to dark mustard color. The repair system has dense

intact, no other defects. pinholes or blowholes on surface. Coatings are . , .*? . - . .' .

Color changed from white to medium yellow. Coatings are intact, no othwdefects.

6 Evaluated By: a /L Approved By: /%i.Y A4 Y

n M B no 3 3 1 e . m

Mail Invoice TOI TVA X X O U N T S PAYABLE PO BOX 15500 KNOXVILLE TN 37901-5500

P U R C H A S E O R D E R

Fuxcham? Order : 00010630 R e v i 8 ion Re1 ea 88

. Printed : 08/24 /04 Page 2

: 00129

~~~~

TESTING OF PROTECTIVE COATING SYSTEMS SAFETY RELATED APPLICATIONS AS DESCRIBED I N : ATTACHMENT A ATTACHMENT 1 ATTACHMENT 2

Q A l . ..

Purchase O r d e r Total Amount

- ., . . '

TOTAL THZS PO: $24,000.00 . --.

i AUTHORIZED S m A E

Standards and Procedures Text at E a 6

End of Purchase Order * * * * * *

P U R C H A S E O R D E R

Purchase Order : 00010630 Revisian R e l e a s e : 00129 Printed 08/24 /04 Page 1

I please Direct Inguiribs to: Venaort

DAVID E . MCGINNIS JOHN DEaARBA T i t l e : CONTRACT MANAGER Phone: F a : 423/751-3550 . ONE PPG PL 4x2

KEELER & LONG/PPG Ext : ATTN: K & L PPG TWLM 4 23 17 5 1 - 4 9 61

PITTSBURGH PA 15172

.... .

* * * * BLANKET OllDER RELEASE **** .. i - I 1.' .

-I_.----

Payment Tern8 % Days Yet 3 0 bays E R 3 r N Ref Contract!

Primary Ship To:

Attention

Transit ryge C a r r i e r Name FOB €08 Point

SERVICE, FOB N/A

Instxuctiona & N o t e s

ATTACHMENTS: EXTERNAL NOTES & ATTACHMENTS T-NOTES TVA 40738

Headex Terms and Conditions - T e x t at End

?ac standard Name Rev s/P Text Title

KEELER-WACT1 002 S Y ASL RESTRICTION FOR XEELER & LONG/PPG TNOTEWEBPAGE 003 S Y VENDOR INSTRUCTIONS FOR T-NOTE WEB SITE

L i n e Qty UP Itam Description Vni t Price Ex t ensi on

-.. 24 ,000 EA catalog ID: $1.000000 $ 2 4 , 0 0 0 . 0 0 2301 1

NON- TAXABLE QtY: 24,000 Delivery D a t e : C 9 / 3 0 / 0 4

ENGINEERING SERVICES TO PROVIDE DESIGN BASIS ACCIDENT (DBA)

. ..

?.

p

Page 1 of I

DeBarba, John

From: Charles A. Vallance [[email protected]] Sent: To : cc:

Subject: Importance: High

Saturday, January 08,2005 12:29 PM rl ph il li [email protected] Jason Keir; David Horn; Kevin Groom; DeBarba, John; Darrell Moody; Les Ayer; Phil McDermot; Chris Hutt DBA Testing of Service Level 1 Underwater Coatings

To All:

This email will provide a status update and confirmation of the LOCA test criteria. Please advise if there are any questions.

The UCC test panels will complete irradiation on or about Jan 11, 2005. Keeler & Long will begin LOCA testing immediately following post irradiation evaluation. Only UCC panels will undergo LOCA testing at this time.

LOCA Testing will follow the ANSI 101.2 test cuwe for postulated BWR Suppression Chamber vapor phase conditions as shown in Fig. 2 of ANSI 101.2. The UCC panels will placed underwater in the test chamber.

Regards, Charlie

Charles A. Vallance Underwater Construction Corp.

Cell: 321-223-5230 Off: 321-779-9693

...

1/10/2005

mailto:[email protected]

SEP.17.2004 2:5@PM UNDER WATER CONSTRUCTION N0.625 P . 2

omred From; Keeler & Long P.0. Box 460 BCSB Echo L a b RD. Watertow, C".06796

UNDERWATER CONSTRUCTION CORPORATION 110 PLAIN8 ROAD ESSEX,CT 06426

860-787-82S0

Ship To : I

Underwater construction mrporat9an I10 Plains Rd. Essex, CT. D6426 . I

i Atbntion: Leo AyerfQA Dept.

PURCHASE OPPER Account/Job No.: Purchase OrUst No,: 0 1 -04923 04-328

1 Cantad: John Debarber i Tefephone N~.#fJ-2746701

I Ehm: I FOB: 1 T m : NEE 30 UP^ m d p t of Ordw Date Wl7/04 Rtquhd Dab: 9/30/04 Br;tWly prsliiinary rspori

IW QTY Rocdved DESCRIPTION UNIT NO PRICE

Per your approved progmm , Pevfslon 16 dated 5/2000 and TVA Purchase Order 0001 0630 requirements pleese provldo the fdollwbg services:

s24000.00

UCC to prarlde K d w Long hth underwater repair coating to be applbd over DBA Test panels matd with WQUARD 78 (formerly Valspar 78) DEA pan& shall be testrd in accordance with ANSI N101.2 'Supprussion Chamber' Test Cuwe The fullowkng shelf ba documented on the tast repan 3est results, your company name, our Po number, M&TE ID number (If appllcable), signature of person performing the test Certificate of Cmpllance, Indicating wmplience with the requirements ofthis P.O. and signed by your authorked company rep b required

Supplier shall not s u b n t m d without UCC QA approval. Supplier shell prwide right of a w e ~ ~ to authorbd parties of UCC for inspection w audit af kcllttles, products or recards.

Supplier shll provide requested dQCUmBnWOD pnwta or In conjunction wlth dellvcyy ofthis order. Nonconformance's or out-of-tnlerance conditions shell be reportfd to UCC QA pepertment prfor to dispitioning. NOTE: SEND INVOICE TO UCC DATED ON OR BEFORE 9/30104

10 CFR 50 Appendk B and lOCFR Part 21 Is applicable to thi

APPLICABLE WHEN CHECED: I

. .-< .

x MIS IS A QUALITY RELATED P U R C W E ORDER

&imWdpd by nnd D&:

'AN EQUAL OPPORTUMl7YEMFiOY'

PURCHASE ORDER (RELEASE) -.= NUCLEAR SAFETY RELATED SERVICES

PLEAS€ SIGN AND FAX TO: 860-274-5857

Dale: December 7, 2004

Supplier: University of Massachusetts Lowell

Address: One University Avenue

Lowell, Massachusetts 01854 b *

978-934-3374 Phone #: Fax #: 978-459-6561

Service requested: In accordance with pa 700327 perfom radiation test per ASTM D 4082 with a dose rate of IxlObrads/hour

or greater, and a total dose of 1x10' for 8-2"x4"

p a n e l s a s supplied by Underwater Constructors and TVA

and d e l i v e r e d by Keeler & Long PPG ---c-

Requested by: John F. De Barba

The Quality Assurance program and documentation requirements, a s specified below, shall be subject to Purchaser review and acceptance prior to payment of invoice(s). The SellerlContractor shall maintain and implement a Quality Assurance program, allowing access to the facility, and records pertaining to this Purchase Order, for the purpose of QA audits andlar surveillances at mutually agreed times. These audits or surveillances may he requestedhequired by a Keeler & Long PPG customer.

The requirements cf 10 CFR Part 21 sha!l apply to this Purchase Order. _.,* -...

I hereSy accept the requirements listed above:

panel Numbers: 6AlF, 6A2F 7AlF,. 7A2F 7B1F, 7B2F 7C1F, 7C2F /A / x / o r/

/ d e

Identification No. Issued By: i iES

PURCHfisE CWEH (RELEASE) . Revised Appr: ,F?L - QA-6398 02/12/01 Ch'k:

Origin FORM FOR NUCLEAR SAFElY o/ b

RELATED SERVICES Revision No.

!

,

University of Massachusetts

UMASS Lowell Radiiztion Laboratoiy

Test Samples Irradiation Report

For

KEELER & LONG PPG TVA Samples ..-

Y

D

Radiation Laboratory Universitg Of Massachusetts Lowell

Pinanski Building, Room 104 1 University Avenue Lowel, MA 01854 (978) 934-3374

Fax (978) 9344067

APPROVALS:

- .

Quality Assurance Managcr

I DOCUMENT NUMBER: UML-12-08-041PPGKVA U;\.la.u Lowell Ibdzation LaborutoT

Project; IRRADIATION OF TEST SAMPLES

1.0 SCOPE

The University of Massachusetts Lowell Radiation Laboratory (UMLRL) exposed eight - 2" x 4 test panels supplied by Keeler & Long PPG, to (20-60 gamma radiation. The test samples were irradiated to a minimum dose of l.OxlOQ rads using the UMLRL underwater submersible type irradiator.

2.0 BACKGROUND

2.1 Description of Co-60 Irradiator

The Irradiator is housed at the bottom of the thirty-one foot open reactor pool and consists of the following three components:

I

CENTER COBALT SOURCE

CHAMBER COVER

CENTRAL COBALT SOURCE 5- SUBMERSIBLE CHAMBER

- MODFIED FOR

0 Eight frames containing approximately 35,000 Curies of CMO.

an aluminum table stand

a modified aluminum submersible chamber

The C&O frames are fixed in a square geometry on the top of the table unit. The submersible chamber is lowered into the geometric center of the square geometry by use of an aluminum cone bolted at the bottom of the submersible chamber. This cane was designed to mate with a 2 and 3/8 inch diameter hole on the tabletop thereby ensuring reproducibility of chamber position. The submersible chamber cover has been modified to accept a central C0-60 source. The central source is !owered into the modified chamber cover after the chamber is on the tabletop. This center source results in greater dpse unifomity within the chamber.

e

_-

3.0 DESCRIPTION OF TEST SAMPLE LOADING -*

The eight test samples were threaded onto a metal ring at the top level of the aluminum sample holder and individually secured in place. The holder designed to hold the samples at a predetermined height within the submersible chamber, was loaded with the samples prior to insertion into the submersible chamber. Figure 1 shows the test samples secured to the aluminum sample holder after removal from the submersible chamber post the 34day irradiation.

Figure 1.

Page 2 of 7

DOCUMENT NUMBER: UML-12-08-04/PPG/TVA UMoss L0wd.f Ra l lah i I ~ b o r a ~ o t y

Project: IRRADIATION OF TEST SAMPLES

4.0 SAMPLE ORIENTATION AND DOSIMETRY RESULTS 0

A dosimetric analysis was performed to determine the positional dose rate in the submersible chamber when occupied by the coating samples. Alanine Pellet Dosimeters (Batch #T020604) and Bruker reader #0141 were used to measure radiation doses within the submersible chamber. The UMLRL dosimetry system is directly traceable to the National Institute of Standards and Technology (Appendix A) and has been in use at the Radiation Laboratory under the facility's QA program.

Figure 2: Top view of the sample loading scheme within the submersible chamber.

UMLRL dosimetry measurements, performed on December 8, 2004 determined an average dose rate within the chamber of 1.28 Megarads .per hour. The minimum dose rate, measured on the panels, was determined to be 1.26 Megaraddhr. The samples were irradiated for 811 hours to ensure that all samples received a minimum dose of 1 .Ox1 Os. Dose calculations are presented in Appendix C.

. '. . .

Page 3 of 7

National Xnstitu te of Standards and Technology CERTIFICATE of IRRADIATION

DOCUMENT NUMBER: UML-12-08-041PPGTTVA


APPENDIX A - NIST certification.

a

Palgo 4 of 7

i

Dosimeter Type: Gamma Senice Alanine Pellet Batch 020604 - I Dates of Irradiation Dose Rate Irradiation Temperature

24 c

Universig oi'3Iassachusetts LoweU Reference: PO# 0005009165

..I

NIST Rcfercnce: HDMM. Da~abook 1005i104

Panel Numbers: 6A1F, 6A2F. 7A1F, 7A2F. 7B1F, 7B2F. 7ClF. 7C2F

DOCUMENT NUMBER: U ML-12-08-04/PPG/TVA [,lAd&..i ]_nwefl Ruiiuhojt .h//lotnIop


APPENDIX B - The Job Check List traces the progress of the samples through receipt, irradiation, and shipment back to the client.

JOB CHECK LIST

COMPANY: Keeler & Long PPG

ADDRESS: PO Box 460 856 Echo Lake Road Watertown, CT 06795

CONTACT PERSON & PHONE NUMBER: John DeBarba

DATE OF PACKAGE ARRIVAL: December 8,2004

ITEMS : Eight 2" x 4" panels

Check -X- to indicate compliance:

PACKAGING SLIP ACCURATELY REPRESENTS CONTENTS: X

INTEGRITY OF PACKAGE MArNTAINED X

SAMPLES TO BE IRRADIATED ARE UNDAMAGED: .x SAMPLES IRRADIATED AS REQUIRED: X

SAMPLES RE-PACKAGED AM) SHIPPED TO CLIENT X

UNUSUAL OCCURANCES N / A

COMMENTS-N/A

- ~~

Page 5 of 7

DOCUMENT NUMBER: UMC-12-08-O4/PP GmVA (JAjll~lr b i v e l l Radiotion h h o r a / 9 t ~


APPENDIX C - The Irradiation Schedule shows dates and times of irradiation, dose rates and any correction factors used to anive at the final accumulated dose.

IRRADIATION SCHEDULE

8

COMPANY: Keeler & Long PPG PO Box 460 856 Echo Lake Road Watertown, CT 06795

TIME OF SAMPLE IRRADIATION:

START: 12/08/04 11:16 STOP: 12/0SfO4 12:16 START: 12/08/04 13% STOP: 12/20/04 13:06 START: 12/20/04 13:36 STOP: 12/22/04 0950 START: 12/22/04 10:33 STOP: 0 1 /03/05 10:33 START: 01/03/05 11:07 STOP: 0 1/05/05 14:37 START 0 1 /05/05 ' 15 : 14 STOP: 0 111 1/05 09:30

Total Irradiation time = 8 1 1 -00 hours e EQUIPMENT :Bruker readedi0141 Pellet

OPERATIONAL CHECK: X OPERATOR: MM

Total Dose Calculation R, = Dose Rate (Rads/hr) at reference time, 4, D = Total accumulated dose (Rads) from radiation exposure. h = Radiological decay constant for Goa, h = A331 T,,= =1.51E-5 h-' t, = Elapsed d n e from start of dosimetry measurement, tr = Total sample irradiation time T,,2 = half-life of a patticular radioactive elemenr, CoW=5.24 years

(BatchT020604)

. J - . ,

,

D = &e &'(1- e 'I2)

h Dose calculation based on minimum dose rate:

) = 1 .015~ 109Rads 1.51E-5 hr-1(81 I hq 1 . 2 6 ~ lo6 (1-e- 1.5lE-5 hr''

0 e

- Page 6 of 7

DOCUMENT NUMBER: UML-12-08-041PPGTTVA ciA4u.r.r Imwll IEadiation Labor-afoy


CERTIFICATE OF EXPOSURE

COMPANY: Keeler & Long PPG PO Box 460 856 Echo Lake Road Watertown, CT 06795

TEST PROGRAM UML-12-08-04/I’PG/TVA

Dosimetry Equipment: Bruker Biospin go141

Calibration due (NIST) 10/2006 Dosimeters: Alanine Pellets Batch TO20604

Facility: Modified Submersible Chamber Co60 Rack #s D-1, D-2, D-3, D-4

141, 18, 120, 134, Central cylinder # 1 13

Radiation Results

adiation Length: 8 1 1 .O hours

Reviewed by:

@ Page I of 7

..-

i

2oamg %stem K L G S Y ~ ~ ~ W / ~ ! 6%7/07/&w7 /07 SubstralEType am &%K/ Surface Prep. 5;sPC 9-/0 For. X DBA X RADIATION DECON. PHYSICAL CHEMICAL OTHER

Test Repon # C&-O;Io9 *

I .

11.

I l l .

d i i I

i

/ COATING SYSTEM Curing Compound: mils ! PrimerlSurlacer: mils GFT . Inrer mediate: mils EFT i

finish: mils EFT i

A P P LI C AT1 0 N CRITERIA

Number Applied

/

-- ~- -- - -_ -

1 2 /07 7 7 .. * -2

. R 6 0 118 Revised f w r : 7L,

.. L

11/16/93 Origin SP ECl PJlE N PREPARATION DATA SHEET (LABORATORY) Revision No. Sheet 1 ci

R &D 4-

I

Identification No. Issued By: \g,A.U 12/07/77 Ch'k: f*r

A- , R&D 118 Revked Appr: 9~~ - fl . - - SPECIMEN PREPARATION DATA 11/16/93

Origin S H E 9 (LABORATORY) Revision No. Sheet 2 0: L 2 R&D

L I / - .

‘0 UNDERWATER CONSTRUCTION CORPORATlON DBA COATING REPAIR PANEL /APPLICATION DATA SHEET

I 1

1 I .

b 1 I

Page 1

e UNDERWATER CONSTRUCTION CORPORATION TVA TEST PANELS 0 DBA COATING REPAIR PANEL /APPLICATION DATA SHEET UCCJob# 04923 .

Panel Side Panel Repair Material Date Time Pit Measuring & Test Equipment No. Substrate Coating Mixed Applied Applied Depth Mils Type ! SN

Page 1

856 Echo Lake Road P. 0. Box 460 Watertown. CT 06795 Tel: 860-274-6701 Fax; 860-274-5857

Manufacturer: Thin Film Technolonv Keeler & Long PPG NAS Test Facility Keeler & Long / PPG

Ameron Date: lanuary 11.2005 Test Preformed for T.V.A.

Other System Identification: X Steel Concrete

Total Dose: 1.015~10~ Dose Rate: 1 -26x1 O6 Irradiation Length: 8 1 1 .O Hours


Sample No.

6A1F (Front)

6A1F (Back)

Results

Color changed from white to medium yellow and the repair system color changed from light gray to mustard color. The repair system has dense pinholes or biowholes on surface. Coatings are intact, no other defects. . - < ~ :. ..

_..


Evaluated By: &L Approved By:

I


Manufacturer: Thin Film Technolow Keeler & Long PPG NAS Test Facility Keeler & Long / PPG

h e r o n Date: January 11,2005 Test Preformed for T.V.A.


Total Dose: 1 .O 15x1 0’ Dose Rate: 1 . 2 6 ~ 1 O6 Irradiation Length: 8 1 1 .O Hours


Sample No.

6A2F (Front1

6A2F E3ack)

Results

Color changed from white to medium yellow and the repair system color changed from light gray to mustard color. The repair system has dense pinholes ar bIowholes on surface. Coatings are intact, no other defects. - . . , - < .. .% .


Evaluated By: e &z& Approved By: ”


Manufacturer: Thin Film Techno1og;v Keeler & Long PPG Keeler & Long PPG NAS Test Facility h e r o n Date: January 11.2005 Test Preformed for T.V.A.

System Identification: X Steel Comret e Other

Total Dose: 1.015~10~ Dose Rate: 1 . 2 6 ~ 1 0 ~ Irradiation Length 8 1 1 .O Hours

Keeler & Long PPG Test Report: 05-0209 UML - Radiation Laboratory Document Number: UML-IZOS-OP/PPGffVA Radiation Tolerance Test Results: e SamDle No.

7A 1 F (Front)

7AIF (Back]

Results

Color changed fiom white to medium yellow and the repair system color changed from light gray to dark mustard color. The repair system has dense pinholes or blowholes on swface. Coatings are intact, no other defects. _ , .*< =. -


Evaluated By: ea


Manufacturer: Thin Film Techno1oe;v Keeler & Long PPG NAS Test Facility Keeler & Long / PPG

Ameron Date: January 1 1.2005 Test Preformed for T.V.A.

System Identification: X Steel Concrete Otiier

Total Dose: 1 .015~10~ Dose Rate: 1 . 2 6 ~ 1 0 ~ Irradiation Length: 8 1 1 .O Hours


SamDle No.

7A2F (Front)

7A2F (Back)

Results

Color changed from white to medium yellow and the repair system color changed from light gray to dark mustard color. The repair system has dense pinholes or blowholes on surface. Coatings are intact, no other defects.

_ , .-< ~ ... '.

.._- . _ Color changed from white to medium yellow. Coatings are intact, no other-defects.

1- Evaluated By: Approved By:Jd i L 4 ,,A Y


Manufacturer: Thin Film Technolonv Keeler & Long PPG NAS Test Facility Keeler & Low / PPG



Total Dose: 1.015~1 O9 Dose Rate: 1.26~1 O6 Irradiation Length: 8 1 1 .O Hours

Keeler & Long PPG Test Report: 05-0209 UML - Radiation Laboratory Document Number: UML-12-08-04/PPG/T'VA Radiation Tolerance Test Results:

SamDle No.

7B 1 F (Front)

7B 1F Back)

Results

Color changed from white to medium yellow and the repair system color changed from off-white to mustard color. Coatings are intact, no other defects.

Color changed from white to medium yellow and the repair system color chhged from dark gray to a dark greenish brown. Coatings are intact, no other defects.

7-

Evaluated By: a& Approved By: 4-J .J Y ,acciz,- y---


Manufacturer: Thin Film Technology Keeler & Long / PPG h e r o n Date: January 11,2005 Test Preformed for T.V.A.

Keeler & Long PPG NAS Test Facility


Total Dose: 1.015~10~ Dose Rate: 1 .26x106 Irradiation Length: 8 1 1 .O Hours


Sample No.

7B2F (Front)

7B2F (Back)

Results

Color changed from white to medium yellow and the repair system color changed horn off-white to mustard color. Coatings are intact, no other defects.

Color changed fiom white to medium yellow and the repair system color cfi.&ged fiom dark gray to a dark greenish brown. Coatings are intact, no other defects.

Evaluated By: & 6&zL Approved By:

0 856 Echo Lake Road P 0. Box 480 Watertown, CT 06795 Tel: 860-274-6701 Fax: 860-274-5857

Manufacturer: Thin Film Technologv Keeler & Long PPG NAS Test Facility Keeler & Long / PPG

h e r o n Date: January 11.2005 - Test Preformed for T.V.A.


Total Dose: 1 .O 15x1 0' Dose Rate: 1 .26x106 Irradiation Length: 8 1 1 .O Hours

Keeler & Long PPG Test Report: 05-0209 UML - Radiation Laboratory Document Number: UML-12-08-04/PPG/TVA Radiation Tolerance Test Results: 0 Sample No.

7C1F (Front)

0

7C1F (Back)

Results

Color changed from white to medium yellow and the repair system color changed from lemon ice to mustard color. Coatings are intact, no other defects.

Color changed from white to medium yellow and the repair system color cfi'kged from gray to a dark greenish yellow. Coatings are intact, no other defects.

Evaluated By: & 657-

a 856 Echo Lake Road P. 0. Box 460 Watertown, CT 06795 Tel: 860-274-6701 Fax: 860-274-5857


h e r o n Date: January 1 1,2005 Test Preformed for T.V.A.


Total Dose: 1.015~10~ Dose Rate: 1.26~ 1 O6 Irradiation Length: 8 1 1 .O Hours

Keeler & Long PPG Test Report: 05-0209 UML - Radiation Laboratory Document Number: UML-12-08-04/PPG/TVA Radiation Tolerance Test Results: 0 Sample No. -- P esults

7C2F Front) Color changed from white to medium yellow and the repair system color changed from lemon ice to mustard color. Coatings are intact, no other defects.

. * < . -.,

Color changed from white to medium yellow and the repair system color changed from gray to a dark greenish yellow. Coatings are intact, no other defects.

0

7C2F (Back)

Evaluated By: e& Approved By:

~

856 Echo Lake Road P 0. Box 460 Watertown. CT 06795 Tel: 860-274-6701 Fax: 860-274-5857

m

Manufacturer: Thin Film Technology Keeler & Long PPG NAS Test Facility Keeler & L o w / PPG

h e r o n Date: Januw 26,2005 Test Preformed for T.V.A.


Keeler & Long PPG Test Report: 05-0209 Design Basis Accident (DBA) Test Results (4 Hour Evaluation):

e Sample~o . Results

6A1 F (Front1 No. 4 medium blisters on upper part of panel, blisters are intact. No blisters on repair system. Coatings are intact, no other defects.

._ -, 5

6A 1 F (Back) No. 4 fewlmedium blisters (not pronounced) on entire panel, blisters are intact. Coating is intact, no other defects.

*This panel during test was immersed and was irradiated prior to DBA.

Evaluated By: a& Approved By:

*JA


Manufacturer: Thin Film Technoloe;~ Keeler & Long PPG NAS Test Facility Keeler & Long / PPG

h e r o n Date: Januarv 26,2005 Test Preformed for T.V.A.



Sample No. Results

6A2F (FrontJ

6A2F [Back)

No. 4 medium blisters on entire panel, blisters are intact. No blisters on repair system. Coatings are intact, no other defects.

No. 4 few/medium blisters (not pronounced) on entire panel, blisters are intact. Coating is intact, no other defects.

..-

*This panel during test was immersed and was irradiated prior to DBA.

8-56 Fcho Lake Road P. 0. Box 460 Waterlowit. CT 06795 Tel: 860-274-6701 Fax: 860-274-5857


h e r o n Date: J a n w 26,2005 Test Preformed for T.V.A.



Sample No. Results

6A3F (Front)

6A3F (Back)

*This panel during test was immersed.

Color changed from white to medium yellow and the repair system color changed from off-white to light yellow. Coatings are intact, no other defects.

Color changed born white to medium yellow. Coating is intact, no other-defects.

.. 7 . . .

858 Echo Lake Road P. 0. Box 460 Watertown, CT 06795 Tel: 860-274-6701 Fax: 860-274-5857 . .

Manufacturer: Thin Film Technolorzv Keeler & Long PPG NAS Test Facility Keeler & Lonn / PPG

h e r o n Date: Januarv 26.2005 Test Preformed for T.V.A.

System Identification: X Steel . Concrete Other


a SampleNo.

6A4F (Front)

6A4F IBack)


Evaluated By: a&

Results

Color changed from white to medium yellow and the repair system color changed from off-white to light yellow. Coatings are intact, no other defects.

V

Color changed from white to medium yellow. Coating is intact, no other..defects.

.'.I

856 Echo Lake Road P. 0. Box 460 Watertown. CT 08795 Tel: 860-274-6701 Far: 860-274-5857

a

Manufacturer: Thin Film Technologv Keeler & Long PPG NAS Test Facility Keeler & Long / PPG


System Jdentification: X Steel Concrete Other

Keeler & Long PPG Test Report: 05-0209 Design Basis Accident @BA) Test Results (4 Hour Evaluation):

@ S m p l e ~ o . Results

7A 1 F (Front) Color changed from medium yellow to light brown and the repair system color changed from dark mustard to a lighter mustard. No. 4 medium dense blisters on entire panel, blisters are intact. No blisters on repair system. The repair system has a rust spot in center. Some rust spots along edge of panel. Coatings are intact, no other defects.

Color changed from medi-um yellow to light brown. No. 4 medium dense blisters on entire panel, blisters are intact. Rust stain on lower right corner of panel. Coating is intact, no other defects.

.

'' -'

*This panel during test was immersed and irradiated prior to DBA.

Approved By.

7A1F (Back)

Evaluated By: - A 2 2

856 Echo Lake Road P. 0. Box 460 Watertown, CT 06795 fel: 860-274-6701 Fax. 860-274-5857

0

Manufacturer: Thin Film Techno1oe;v Keeler & Long PPG NAS Test Facility Keeler & Long / PPG

Ameron Date: January 26,2005 Test Preformed for T.V.A.

Concrete Other Svstem Identification: X Steel


S a m D l e ~ o . Results

7A2F (Front) Color changed from medium yellow to light brown and the repair system color changed fiom dark mustard to a lighter mustard. No. 4 to No. 6 mediddense blisters on entire panel, blisters are intact. No blisters on repair system. The repair system has a dozen rust spots in center. Coatings are intact, no other defects.

Color changed from medium yellow to light brown. No. 6 and No. 8 dense blisters on entire panel, blisters are intact. Rust stains on upper center and lower left comer of panel. Coating is intact, no other defects.

.. . a.

7A2F (Back)


Evaluated By: a& Approved By: kb-4-

0


a . -

Manufacturer: Thin Film Technolorn Keeler & Long PPG NAS Test Facility Keeler & Lone. / PPG

h e r o n Date: Januarv 26.2005 Test Preformed for T.V.A.



@ SampleNo. Results

7A3F (Front) Color changed from white to light yellow and the repair system color changed from off-white to a darker off-white. Coatings are intact, no other defects.

Color changed from white to light yellow. . ’> . =. ~

No. 8 few blisters in upper left and lower left comers of panel, blisters ,are intact. Coating is intact, no other defects.

e

7A3F (Back)

*This panel during test was immersed. . .

Evaluated By: @A

7A4F (Back)

*This panel during test was imqersed.

Evaluated By: Approved By: 4- &- #&//


e





1) SampleNo. Results I

7BlF Front) Color changed fiom medium yellow to light brown and the repair system color changed from mustard to a darker mustard. No. 8 few blisters, blisters are intact. Some light staining on most of the panel and repair. Coatings are intact, no other defects.

Color changed from medium yellow to light bfown and the repair system color changed fiom dark greenish brown to a medi,vm brown. No. 8 dense blisters on bottom of panel, blisters are intact. Some light staining on most of the panel and repair. Coatings are intact, no other defects

~

*This panel during test was in vapor phase and irradiated prior to DBA.

c

Evaluated By: && Approved By: QC& 0 v

7B1F (Back)


e

Manufacturer: Thin Film Technolorn Keeler & Long PPG NAS Test Facility Keeler & Low / PPG

h e r o n Date: January 26.2005 Test Preformed for T.V.A.



Sample No. Results

7B2F (Front) Color changed from medium yellow to light brown and the repair system color changed from mustard to a darker mustard. No. 8 medium dense on lower half of panel, blisters are intact. No blisters on repair system. Small rust stain on right top of repair system. Coatings are intact, no other defects.

e

-> - . I -

7B2F (Back) Color changed from medium yellow to light brown and the repair system color changed from dark gLeenish brown to a mediiirn brown. No. 8 medium /dense blisters on entire panel, blisters are intact. No blisters on repair system. Coatings are intact, no other defects.

*This panel during test was in vapor phase and irradiated prior to DBA.

-. Evaluated By: &A Approved By: <& & 6’’

a

856 Echo Lake Road P. 0. Box 460 WateRown, CT 06795 Tel: 860-274-6701 Fax: 860-274-5857


h e r o n Date: J a n w 26,2005 Test Preformed for T.V.A.


~ ~ ~~ ~ ~ ~~~

0


@ Samule~o . Results

7B3F (Front) Color changed from white to light yellow and the repair system color changed from off-white to light yellow. Coatings are intact, no other defects.

Color changed from white to light > ellow and the repair system gray color did not change.. Small rust stah on left edge of repair system. Coatings are intact, no other defects.

'< - ='

..'

0

7E3F (Back1

*This panel during test was in vapor phase.

0


@ Samule~o . Results

7B3F (Front) Color changed from white to light yellow and the repair system color changed from off-white to light yellow. Coatings are intact, no other defects.

Color changed from white to light yellow and the repair system gray color did not change.. Small rust stah on left edge of repair system. Coatings are intact, no other defects.

'< - ='

..'

0

e 856 Echo Lake Road P. 0. Box 460 Watertown. CT 06795 Tel: 860-274-6701 Fax: 660-274-5857

Manufacturer: Thin Film Technologv Keeler & Long PPG NAS Test Facility Keeler & Lone. / PPG

h e r o n Date: January 26.2005 Test Preformed for T.V.A.

System Ideatification: X Steel Concrete Other


SampleNo. Results

7B4F (Front) Color changed from white to light yellow and the repair system color changed fitom off-white to light yellow. No.8 few blisters on upper left corner of panel, blisters are intact. No blisters on repair system. Coatings are intact, no other defects.

-* . 7. ~

Color changed from white to light yellow and tile repair system gray color did not change. Small rust stain on right cage of repair system. Coatings are intact, no other defects.

*This panel during test was in vapor phase.

Evaluated By: a& k 7 D-6 A 0 V

,.

7B4F (Back)

Approved By: c





Keeler & Long PPG Test Report: 05-0209 Design Basis Accident @BA) Test Results (4 Hour Evaluation):

7C 1 F (Front)

7C1F (Back’)

Results

Color changed from medium yellow to light brown and the repair system color changed from mustard to a medium brown. No. 6 few/medium blisters on entire panel, blisters are intact. No blisters on repair system. Coatings are intact, no other defects.

,

Color changed from medium yellow to light br&h :’ .- and the repair system color changed from dark greenish yellow to mustard color. No. 6 few/ medium blisters on entirdpanel, blisters are intact. Small rust stain on upper right edge of repair system. Coatings are intact, no other defects.



. .


Ameron Date: J a n w 26.2005 Test Preformed for T.V.A.



Samule No. Results

7C2F Eront)

7C2F [Back)

Color changed from medium yellow to light brown and the repair system color changed from mustard to a medium brown. Rust stain on top edge of repair system. Light yellow stain (possibly from tape) on center of panel and repair system. Coatings are intact, no other defects.

Color chang:d from medium yellow to light brown and the repair system color changed fiom dark"' ' greenish yellow to mustard color. No. 8 few/ medium blisters on panel and right side of repair system, blisters are intact;"smaIl rust stain on left edge of repair system and two spots on bottom center ofpanel. Coatings are intact, no other defects.

%*


Evaluated By: Approved By

856 Echo Lake Road P. 0. BOX 460 Watertown, CT 06795 Tel: 860-274-6701 Fax: 860-274-5857


Ameron Date: January 26,2005 Test Preformed for T.V.A.

0 ther System Identification: X Steel Concrete


SampleNo. Results

7C3F (Front) Color changed from white to light yellow and the repair system color changed from off-white to medium yellow. Coatings are intact, no other defects.

Color changed from white to light yellow and '' ' the repair system color changed from gray to lighter gray. One rust spot on left edge of panel. Coatings are intact, no other defects.

*

0

7C3F (Back)


~


a

Manufacturer: Thin Film Technolonv Keeler & Long PPG NAS Test Facility Keeler & Long; / PPG


System Identificatiox X Steel Concrete Other


a S m p l e ~ o . Results

7C4F (Front) Color changed from white to light yellow and the repair system color changed from off-white to medium yellow. Coatings are intact, no other defects.

Color changed from white to light yellow and c . . the repair system color changed from gray to lighter gray. No. 8 few blisters on edge of panel, blisters are intact. Coatings are infact, no other defects.


Evaluated By: &&

a

7C4F (Back)


Manufacturer: Thin Film Technolo!Zv Keeler & Long PPG NAS Test Facility Keeler & Long / PPG

h e r o n Date: Februarv 9.2005 Test Preformed for T.V.A.

Other Concrete - System Identification: X Steel

Keeler & Long PPG Test Report: 05-0209 Design Basis Accident @BA) Test Results (14 Day Evaluation):

Sample No.

6A1F (Front)

6Al F (Back)

Results

No change from 4 hour evaluation.

No change from 4 hour evaluation. ..*



a

Manufacturer: Thin Film Technology Keeler & Long PPG NAS Test Facility Keeler & Lone: / PPG

h e r o n Date: February 9.2005 Test Prefonned for T.V.A.

Other Svstem Identification: X Steel Concrete

Keeler & Long PPG Test Report: 05-0209 Design Basis Accident (DBA) Test Results (14 Day Evaluation):

Sample No. Results

6A2F (Front)

a No change from 4 hour evaluation.

No change fiom 4 hour evaluatip

Evaluated By: ae

l

I

6A2F Back)

856 Echo Lake Road P. 0. Box 460 Watertown. CT 06795 Tel: 860-274-6701 Far 860-274-5857

e

Manufacturer: Thin Film Technolow Keeler & Long PPG NAS Test Facility Keeler & Long. / PPG

h e r o n Date: February 9,2005 Test Prefonned for T.V.A.

Concrete Other System Identification: X Steel


Sample No. Results

6A3F (Front)

* No change from 4 hour evaluation.

a

:. . *. ..

No change from 4 hour evaluation. ..*

6A3F (Back)



0

Manufacturer: Thin Film Technology Keeler & Long PPG NAS Test Facility Keeler & Lone. / PPG

h e r o n Date: Februaw 9.2005 Test Preformed for T.V.A.



Samde No. Results

6A4F (Front)

e No change fiom 4 hour evaluation.

a

6A4F (Back) No change from 4 hour evaluation. ...

.4 -- Evaluated By: Approved By:

I



h e r o n Date: February 9,2005 Test Preformed for T.V.A.


Keeler & Long PPG Test Report: 05-0209 Design Basis Accident @BA) Test Results (14 Day Evaluation):

Sample No. Results

7AlF (Front) No change from 4 hour evaluation.

7A1F (Back) No change from 4 hour evaluation. ..'

~~


a


h e r o n Date: February 9.2005 Test Preformed for T.V.A.



Sample No. Results

7A2F (Front)

I)


_ , ,.J . .-

No change from 4 hour evaluation. ..* . ;.

7A2F (Back)

Y

856 Echo Lake Road P. 0. BOX 460 Watertown. CT 06795 Tel: 860-274-6701 Fax: 860-274-5857




Keeler & Long PPG Test Report: 054209 Design Basis Accident @BA) Test Results (14 Day Evaluation):

Samde No. Results

7A3F (Front) No Change fiom 4 hour evaluation.

7A3F (Back) No change fiom 4 hour evaluation. :_.

Evaluated By: a Approved By: *

856 Echo Lake Road P. 0. Box460 Watertown. CT 06795 lei: 860-274-6701 fax: 860-274-5857

Manufacturer: Thin Film Technologv Keeler & Long; / PPG h e r o n Date: Februarv 9,2005 Test Preformed for T.V.A.

Keeler & Long PPG NAS Test Facility

System Identification: - X Steel Concrete Other


Sample No.

7A4F (Front)

7A4F Back)

Results


No change from 4 hour evaluatim. ...

Evaluated By: Approved By: -



h e r o n Date: Februaw 9,2005 Test Preformed for T.V.A.



Sample No.

7B1F ('Front)

7B1F (Back)

Results


No change fiom 4 hour evaluation. _..

EvaluatedBy:

~ ~


Manufacturer: Thin Film Technoloav Keeler & Long PPG NAS Test Facility Keeler & Long / PFG

Ameron Date: February 9,2005 Test Preformed for T.V.A.



Sample No. F esults

7B2F Front)

0 No change from 4 hour evaluation.

0

.*I > =.. -

No change from 4 hour evaluation. ,.-

7B2F (Back)

EvaluatedBy: a = HZ2 Approved By. / / ~ - : t ~ :

856 Echo Lake Road P. 0. Box 460 Watettown, CT 06795 Tel: 860-274-6701 Fax: 860-274-5857 a




a

0

2


S a m d e No.

7B3F (Front)

Results


7B3F (Back) No change from 4 hour evaluation. ..- . . ..


856 Echo Lake Road P. 0. Box 460 Watertown, CT 06795 Tel: 860-274-6701 F x . 860-2745857

Manufacturer: Thin Film Technolow Keeler & Long: / PPG h e r o n Date: Februarv 9.2005 Test Preformed for T.V.A.

Reeler & Long PPG NAS Test Facility



- Sample No. Results

7B4F (Front) No change tiom 4 hour evaluation.

7B4F (Back) No change fiom 4 hour evaluation. ,.--

Evaluated By: &&

2

. , .’? \. -.. -

a 856 Echo Lake Road P. 0. Box 460 Watertown, CT 06795 Tel: 860-274-6701 Fax: 860-274-5857

Mkufacturer:.Thiri Film Technoloq ,.’ ‘, ‘ Keeler & Long PPG .Keeler.& Long /2PG Ameron ’ Date: February 9.2005 Test Preformed for T.V.A.

NAS Test Facility



Sample No. Results

7C 1 F Front)

I)

No change fiom 4 hour evaluation.

0

7C 1 F (Back) No change from 4 hour evaluation. ..*



h e r o n Date: Februarv 9.2005 Test Preformed for T.V.A.



Sample No.

7C2F (“Front)

7C2F (Back)

Results


No change from 4 hour evaluation. ’ ,.

Evaluated By: &&


Manufacturer: Thin Film Technology Keeler &'Lone / PPG h e r o n Test Preformed for T.V.A.

Keeler & Long PPG NAS Test Facility Date: February 9,2005

System Identification: X Steel . Concrete Other


Sample No.

7C3F (Front)

Results


7C3F (Back) No change from 4 hour evaluation. ..-



Ameron Date: Februarv 9.2005 Test Preformed for T.V.A.

Concrete Other System Identification: X Steel


a SamDle No. Results

7C4F (Front) No change from 4 hour evaluation.

a

-< . 7. -.

No change from 4 hour evaluation. ...

7C4F (Back)


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Documents

RADIATION AND DESIGN BASIS ACCIDENT TESTING OF › docs › ML0706 › ML070600220.pdfSet Lower Autoclave controller to desired setting, manual output at zero. 5. Close two (2) valves