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7/27/2019 Ppt Fabrication Nanocomposit
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Conclusion
References
mailto:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]7/27/2019 Ppt Fabrication Nanocomposit
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ABSTRACT
Conclusion
References
Simple mixing and hot pressing methods were used to make highstrength and light-weight composite from oil palmempty fruit bunches (OPEFB)
using PVAc as an adhesive and silica nanoparticles as a filler. The mechanical
strength of the composite was examined in term of compressive strength. The
simple mixing method was used to mix composition with PVAc and silica
nanoparticles. Silica nanoparticles were added as filler.
At pressing pressure of 100 MPa, pressing temperature of 300
o
C, andpressing time of 20 minutes, we found compressive strength of 11,35 MPa. Data
analysis of XRD showed that the used silica nanoparticles were in amorphous
phase or had broad pattern. The compressive strength data showed that the
composites were stronger than the composites made by Masturi and
Kumagizuri, and also stronger than the ordinary wood-based composites. Thus,
the composites are feasible to be used to replace wood-based composites,
especially in furnishings.
7/27/2019 Ppt Fabrication Nanocomposit
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INTRODUCTION
South Sumatera is one of the three major palm tree producing provinces inIndonesia.
OPEFB is one of oil palm mill residue wastes.
Nanocomposite material consists of two or more organic/inorganic in somecombination form separated at least by a molecule and has at least one-dimensional nano size [3].
The addition of silica nanoparticles will reinforce the mechanical strength of the
composite. s
Conclusion
References
7/27/2019 Ppt Fabrication Nanocomposit
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EXPERIMENTAL
we used OPEFB brought from Tanjung Siapi-api, South Sumatera, Indonesia.LOCATION
The measurement of composite compressive strength was performed using a
Torsee (Tokyo Testing Machine MFG, Ltd.).The size of silica nanoparticles was measured using a scanning electron
microscope (SEM JEOL JSM-6360LA) and its crystallization was determined by X-ray diffraction (XRD).
TOOLS
OPEFB were dried and cut into small pieces.
Polyvinyl acetate (PVAc; FOXTM) was used as an adhesive. In specific mass, it wasdissolved in 8 mL of water and stirred for 10 minutes by using magnetic stirrer.
OPEFB was then put into the PVAc solution and mixed. The mixture was then putinto a cylindrical mold and hot-pressed at varied pressing temperature, time, andpressures.
The fabricated samples had diameter of 26 mm and height of 25 27 mm
STEPS
Conclusion
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7/27/2019 Ppt Fabrication Nanocomposit
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RESULT AND DISCUSSION
Optimum Fraction of POEFB and PVAc
SEM and XRD Features
Compressive Strength: Addition of SilicaNanoparticles
Variation of Pressing Pressure
Conclusion
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7/27/2019 Ppt Fabrication Nanocomposit
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RESULT AND DISCUSSION
50.00
55.00
60.00
65.00
70.00
75.00
80.00
85.00
0.001 0.003 0.005 0.007 0.009
CompressiveStrength(MPa)
POEFB Fraction (w/w)
Optimum Fraction of POEFB and PVAC
Conclusion
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7/27/2019 Ppt Fabrication Nanocomposit
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RESULT AND DISCUSSIONSEM and XRD Features
Conclusion
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7/27/2019 Ppt Fabrication Nanocomposit
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RESULT AND DISCUSSION
50.00
60.00
70.00
80.00
90.00
100.00
110.00
0.001 0.003 0.005 0.007 0.009
Compressivestreng
ht(MPa)
Fraction of silica (w/w)
Compressive Strength: Addition of Silica
Nanoparticles
Conclusion
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7/27/2019 Ppt Fabrication Nanocomposit
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RESULT AND DISCUSSION
40
60
80
100
120
140
40 50 60 70 80 90 100
PressingPressure(MPa)
Compressive Stress (MPa)
150 C
125 C
175 C
200 C
225 C
Variation of Pressing Pressure
Conclusion
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7/27/2019 Ppt Fabrication Nanocomposit
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CONCLUSION
1 We succeeded in making composites with simple mixing and hot pressing methods by using OPEFB,
PVAc, and silica nanoparticles.
2
Mass fraction of PVAc/OPEFB of 13 : 2 has compressive strength of 82,88 MPa.
Composite with high compressive strength of 100,39 MPa was obtained using silica nanoparticles ata pressing pressure of 80 MPa, pressing temperature of 150 oC, and pressing time of 20 minutes.When the pressing pressure of 100 MPa was applied, the compressing strength increased untilreached a saturation value at 115,35 MPa. The same condition occured by varying pressing time.
3
These results are better than those of Masturiof home-waste composite[7]in which its compressivestrength is 84,37MPa and also better than Kumagai and Sasaki of rice husk composite reached 55,7MPa[10].
Thus, the composite is feasible to replace wood-based composite, especially in furnishing.
Conclusion
References
7/27/2019 Ppt Fabrication Nanocomposit
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ReferencesI. Sriyanti., Mikrajuddin, Khairurijal dan L. Marlina. Fabrikasi materialnanokomposit yang kuat, ringan dan murah dengan memanfaatkan serbukkayu dan matriks resin. Laporan Hibah Pekerti Tahun I. Lembaga PenelitianUniversitas Sriwijaya: Unpublished.
Mikrajuddin, A.,Okuyama K. Zinc oxide nanoparticles prepared by a simpleheating: effect of polymer addition and polymer absence on morphology.Proceedings ITB on Enggineering Science, 35B (2004) 140-152.
Stephanie, Yoshimichi,Ohki, Takahiro Imai, Toshikatsu Tanaka, JosefKindersberger. Tree initiation characteristic of epoxy resin/claynanocomposites. J IEEE Transactions on Dielectrics and ElectricalInsulation, 16.5(8) (2009) 1473.
Morgan, A. B., Gilman, J. Characterization of polymer-layered silicate (clay)
nanocomposites by transmission electron microscopy and X-ray diffraction:a comparative study. J. App. Polym. Sci. 87, (2003) 1329-1338.
etc
Conclusion
References