14
Disclosure to Promote the Right To Information Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public. इंटरनेट मानक !ान $ एक न’ भारत का +नम-णSatyanarayan Gangaram Pitroda “Invent a New India Using Knowledge” प0रा1 को छोड न’ 5 तरफJawaharlal Nehru “Step Out From the Old to the New” जान1 का अ+धकार, जी1 का अ+धकारMazdoor Kisan Shakti Sangathan “The Right to Information, The Right to Live” !ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता ह Bharthari—Nītiśatakam “Knowledge is such a treasure which cannot be stolen” IS 15608 (2005): Cream Bleach [PCD 19: Cosmetics]

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Page 1: IS 15608 (2005): Cream Bleach - Public.Resource.Org · IS 15608:2005 the specifications if the composite sample passes all thetests, asper Table 1 and Table2. 6 TEST METHODS Test

Disclosure to Promote the Right To Information

Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public.

इंटरनेट मानक

“!ान $ एक न' भारत का +नम-ण”Satyanarayan Gangaram Pitroda

“Invent a New India Using Knowledge”

“प0रा1 को छोड न' 5 तरफ”Jawaharlal Nehru

“Step Out From the Old to the New”

“जान1 का अ+धकार, जी1 का अ+धकार”Mazdoor Kisan Shakti Sangathan

“The Right to Information, The Right to Live”

“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता है”Bhartṛhari—Nītiśatakam

“Knowledge is such a treasure which cannot be stolen”

“Invent a New India Using Knowledge”

है”ह”ह

IS 15608 (2005): Cream Bleach [PCD 19: Cosmetics]

Page 2: IS 15608 (2005): Cream Bleach - Public.Resource.Org · IS 15608:2005 the specifications if the composite sample passes all thetests, asper Table 1 and Table2. 6 TEST METHODS Test
Page 3: IS 15608 (2005): Cream Bleach - Public.Resource.Org · IS 15608:2005 the specifications if the composite sample passes all thetests, asper Table 1 and Table2. 6 TEST METHODS Test
Page 4: IS 15608 (2005): Cream Bleach - Public.Resource.Org · IS 15608:2005 the specifications if the composite sample passes all thetests, asper Table 1 and Table2. 6 TEST METHODS Test

IS 15608:2005

T?av7mF

YFw@iM– Milk

Indian Standard

CREAM BLEACH — SPECIFICATION

Ics 70.100.70

0 BIS 2005

BUREAU OF INDIAN STANDARDSMANAK 13HAVAN, 9 BAHADUR SHAH ZAFAR MARG

NEW DELHI 110002

November 2005 Price Group 4

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Cosmetics Sectional Committee, PCD 19

FOREWORD

This Indian Standard was adopted by the Bureau of Indian Standards, after the draft finalized by the CosmeticsSectional Committee had been approved by the Petroleum, Coal and Related Products Division Council.

Cream bleach is a two component product one containing hydrogen peroxide in a cosmetically acceptable formsuch as cream, lotion, etc. The second component contains activator essentially in a powder or cream form whichwhen mixed with a cream reacts and Iibrates the necessary quantity of nascent oxygen for action. Additionally,it may contain soothing anti-inflammatory, cooling applications and optionally it may contain instruction sheet,spatula, tray, etc, to facilitate application of product.

Cream bleach and activator are extemporaneously mixed in the proportion advised by ‘the manufacturer andapplied. Such application is held on the skin/hair for a period as specified and rinsed off, adequate precautions inrespect of product suitability on customer is to be taken.

No stipulation has been made in this standard regarding composition of cream bleaches. The manufacturer has achoice of using variety of raw materials and combination there of. However, it is necessary that the raw materialsused are such that in the concentration in which they would be present in the finished cosmetic formulation afterinteract ion with other raw materials, are free from any harmfid effects. For evaluating the safety of a newformulation, reference may be madetoIS4011 :1997 ‘Methods of test for safety evaluation of cosmetics (secondrevision)’.

A scheme for labelling environment friendly product as known as ECO-Mark was introduced at the instance ofthe Ministry of Environment and Forests (MEF), Government of India. The ECO-Mark is being administered bythe Bureau of Indian Standards (BIS) under the Bureau of Indian Standards Act, 1986 as per the ResolutionNo. 71 dated21 February 1991 and No. 768 dated 24 August 1992 published in the Gazette of the Governmentof India. For a product to be eligible for marking with ECO logo it shall also carry the Standard Mark of BISbesides meeting additional environment friendly requirements. .For this purpose, the Standard Mark of BIS wouldbe a single mark being a combination of the”BISmonogram and the ECO logo. Requirements for ECO,friendlinesswil] be additional, manufacturing units will be free to opt for Standard Mark alone also.

The composition of the Committee responsible for the formulation of this standard is given in Annex H,

For the -purpose of deciding whether a particular requirement of this standard is complied with, the final value,observed or calculated, expressing the result of a test or analysis, shall be rounded off in accordance withIS 2:1960 ‘Rules for rounding off numerical values (revise~’. The number of significant places retained in therounded off value should be the same as that of the specified value in this standard.

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-IS 15608:2005

Indian Standard

CREAM BLEACH — SPECIFICATION

1 SCOPE

1.1 This standard prescribes the requirement and themethods of sampling and tests for cream bleach.

1.2 Cosmetic preparations which are fluid at ambienttemperature, classified generally as lotions, milks, etc,and skin creams generally vanishing cream, coldcream, cleanzing cream, moisturizing cream, sportscream, foundation cream, hand cream, emollient creamand general purpose cream are excluded from the scopeof this standard.

2 REFERENCES

The following standards contain provisions, whichthrough reference, in this text, constitute provisions ofthis standard. At the time of publication, the editionsindicated were valid. All standards are subject torevision and parties to agreements based on thisstandard are encouraged to investigate the possibilityof applying the most recent editions of the standardsindicated below:

IS No.

1070:19922088:1983

3958:1984

4707

(Part 1): 2001

(Part 2): 2001

14648:1999

Title

Reagent grade water (third revision)

Methods for determination of arsenic(second rxwision)

Methods of sampling cosmetics@rs~revision)

Classification of cosmetics rawmaterials and ad@ncts:Dyes, colour and pigments (secondrevision)

List of raw materials generallynot recognized as safe for use incosmetics (second revision)

Methods of tests for microbiologicalexamination ‘ofcosmetics

3 REQUIREMENTS

3.1 Description

Cream bleach is normally supplied in two packs, onecontaining cream and the other containing cream orpowder activator in duo pack form. Cream bleach shallbe white or coloured, perfumed and smooth creamhaving uniform consistency. Powder activator may bewhite or coloured and may be perfumed.

3.2 Ingredients

Unless specified otherwise, all the raw materials used

in the manufacture of cream bleach shall conform tothe requirements prescribed in the relevant IndianStandards, where such standards exist.

3.3 The dyes and pigments used in manufacture ofcream bleach shall comply with the provisions ofIS 4707 (Part 1).

Ingredients other than colours, dyes and pigments usedin formulation of cream bleach shall comply with theprovisions of IS 4707 (Part 2).

3.4 The cream shall comply with the requirementsgiven in Table 1, when tested as prescribed inCO14 ofTable 1 and activator (powder/cream) shall complywith the requirements given in Table 2.

4 PACKING AND MARKING

4.1 Packing

4.1.1 The cream bleach and activator shall be packed.in suitable well closed, air-tight container and both shallbe given together with instruction sheet, spatula insuitable cartons.

4.2 Marking

4.2.1 The containers shall be legibly marked with thefollowing information:

a)

b)

c)

d)

e)

f)

g)h)

j)

k)

Name of the product;

Active content of the~roduct (percent contentof hydrogen peroxide);

Manufacturer’s name, address andlorrecognized trade-mark, if any;

Net mass of the material;

Batch number, in code or otherwise to enablethe lot of manufacture to be traced back fromrecords;

For external use only;

Instructions for use;

Other statutory requirements, if any;

‘Best use before. . . .‘ (month and year to bedeclared by the manufacturer);

NOTE — This requirement is exempted in case ofl

1) Small packings of 10 g or 25.ml, and

2) Products with shelf life of more than 24months; and

List of key ingredients.

NOTE — This is exempted in case of pack sizes of30 g/60 ml or less,

1

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IS 15608:2005

Table 1 Requirements for Cream

(Clauses 3.4 and 5.3)

S1No. Characteristics Requirements Method of Test, Ref to Annex

(1) (2) (3) (4)

O pH 2.5 to 4.5 A

ii) Assay (as hydrogen peroxide), percent by mass 3.5 to 5.5 B

Table 2 Requirements for Activator Powder/Cream

(Clauses 3.4 and 5.3)

N Characteristics Requirements Method of Test, Ref toNo. ~~

Powder Cream Annex IS No,F + YAmmonia Oxygen

Based Generating

(1) (2) (3) (4) (5) (6) (7)

i) PH of 10 per cent aqueous solution 7-11 10-13 8-1 I A —

ii) Assay:a) As ammonium bicarbonate, percent by L5 . 4 c —

mass, Mirrb) As oxygen content, pereent by mass, Max — 3.5 — D —

iii) Total fatty substance, percent by mass, Mrr — — 5.0 E —

iv) Heavy metals (as Pb), parts per million, Max 20 20 20 F —

v) Arsenic (as AszOl), parts per million, Max 2 2 2 G —

v) Total plate count, cfu/g, Mu 1000 1000 1000 . 14648

NOTES

1 If individual raw material have been tested for heavy metals and arsenic then finished raw material may not be tested again for theserequirements.

2 When the cream bleach and activator are mixed, total hydrogen peroxide percent by mass in the mixture sbordd not be more [IIm 4.

3 pH of the mixed produet should be 6-9.5.4 When both the bleach and iictivator are cream, proper Iabelling to this effect should be ensured by the manufacturer.

4.3 BIS Certification Marking

The containers may also be marked with the StandardMark.

4.3.1 The use of the Standard Mark is governed by theprovisions of the Bureau ofIndian Standards Act, 1986

and the Rules and Regulations made thereunder. Thedetails of conditions under which the licence for theuse of the Standard Mark may be granted tomanufacturers or producers maybe obtained from theBureau of Indian Standards.

4.4 Caution

Hydrogen peroxide may cause skin irritation incerta”mcases, so a preliminary test according to theaccompanying direction should first be made(see 4.4. 1). The material should not be used forbleaching around the eyes.

Each package shall contain instructions in English andlocal language on the folIowing lines for carrying outthe test.

4.4.1 Hydrogen peroxide containing preparations maycause serious inflammation of the skin in some casesand so a preliminary test should always be carried outto determine whether or not special sensitivity exists.For carrying out the test, cleanse a small area of skinbehind the ear or upon the inner surface of the forearm,using either soap and water or alcohol. Apply a smallquantity of cream bleach as prepared for use to thearea and allow it to dry. After 10-15 minor as directedby the manufacturer, wash the area gently with soapand water. If no irritation or inflammation is apparent,it maybe assumed that no hypersensitivity to the creambleach exists. The test should, however, be carried outbefore each and every application.

5 SAMPLING

5.1 Representative }amples of the material shall bedrawn as prescribed in IS 3958.

5.2 Test for all the characteristics shall be carried outon the composite sample.

5.3 The material shall be taken to have conformed to

2

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IS 15608:2005

the specifications if the composite sample passes allthetests, asper Table 1 and Table2.

6 TEST METHODS

Test for the requirements shall be carried out asprescribed in Annexes A to G.

7 QUALITY OF REAGENTS

Unless specified otherwise, pure chemicals and distilledwater (see 1S 1070) shall be employed in the tests.

NOTE — ‘Pure chemicals’ shall mean the chemicals that donot contain impurities which affects the results of analysis.

ANNEX A

[Table 1, S1 No. (i), Table 2, Sl No. (i) and Clause 6]

DETERMINATION OF@

A-1 APPARATUS 50 ml beaker. Determine the pH of cream bleach at

A caIibratedpH meter, equipped with a combined glass 27* 2°C using thepH meter. Weigh accurately about

electrode.10 + ].0 g of activator powder in 250 ml beaker.Add 100 ml water, stir for 5 min. Determine the pH

A-2 PROCEDURE of suspen-sion at 27 + 2°C using the

Weigh accurately about 40 + 1.0 g of the cream in pH meter.

ANNEX B

[Table 1, S7 No. (ii) and Clause 6]

DETERMINATION OF HYDROGEN PEROXIDE PERCENT BY MASS (ASSAY)

B-1 REAG-ENTS

-B-l.l Potassium Permanganate (0. IN) — Dissolve3.3 g of potassium permanganate in 1000 ml distilledwater, heat it on water bath for 1 h, allow to stand for2 days, filter through glass wool or filter paper No. 1and standardize the solution.

B-1. 1.1 Procedure for Standardization

Weigh accurately about 200 mg of sodium oxalate,previously dried at 11O“C to constant weight anddissolve it in 250 ml of water. Add 7 mI of concentratedsulphuric acid, heat to about 70”C and titrate with 0.1 Npotassium permanganate solution, with constant stirringuntil ‘a pale pink colour, which persist for 15 s isproduced. The temperature at any stage of the titrationshould not be less than 60”C. Calculate the normality.

Each 6.7 mg of sodium oxalate is equivalent to 1 mlof 0.1 N potassium permanganate.

B-1.2 Sulphuric Acid (20 Percent) — Take 700 mlof ice cold distilled water in 1000 ml volumetric flask,add slowly along walls 200 ml of concentratedsulphuric acid, cool and make the volume up to1000 ml mark with distilled water.

B-1.3 Concentrated Sulphuric Acid

B-1.4 Sodium Oxalate — A.R. grade.

B-2 PROCEDURE (ASSAY)

Weigh accurately about 1.0 g cream in 100 ml beaker.Add distilled water slowly and disperse the cream.Transfer the contents of the beaker quantitativ.elyto a 250 ml conical flask with the aid of water. Add20 ml of 20 percent sulphuric acid solution andshakee vigorously. Titrate the contents of the flaskwith 0.1 N potassium permanganate solution. Theend point is reached when faint pink colour persistsfor 15 s.

B-3 CALCULATION

Content of H20Zpercent by mass=VXNX1.701

w

where

V = volume of KMnOd required for titration,

N = normality of KMnO,, and

W = weight of the cream taken for titration.

3

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1S 15608:2005

ANNEX C

[Table 2, S1 No. (ii)(a) and Clause 6]

DETERMINATION OF AMMONIUM BICARBONATE, PERCENT BYMASS FROM ACTIVATOR

C-1 REAGENTS

C-1.1 Sodium Hydroxide (1 N) — Dissalve 42 g ofsodium hydroxide in 1 000 ml volumetric flask using500 ml distilled water, cool to room temperature andmake the volume with distilled water to 1 000 ml.

C-1.2 Sulphuric Acid (1 N) — Take ice cold 700 mldistilled water in 1000 ml volumetric flask, add slowlyalong walls 54 ml of concentrated sulphuric acid, cooland make up volume up to 1000 ml mark with distilledwater.

C-1.3 Methyl Red Solution — Dissolve 0.1 g ofmethyl red in 100 ml of 60 percent rectified spirit.

C-2 STANDA-RDIZATION

Weigh accurately about 5.0 .g of potassium hydrogenphthalate, previously powdered and dried at 120°C for2 h and dissolve in 75 ml of water. Add 0.1 ml ofphenolphthalein solution and titrate with the lN sodiumhydroxide solution until pink colour is produced.

Each mI of 1 N sodium hydroxide is equivalent to0.2042 g of potassium hydrogen phthalate.

C-3 PROCEDURE

Weigh accurately about 1.0 g activator (previouslydried at 60°C for 15 rein) in 250 ml conical flrtsk anddissolve in 23 mI distilled water, add 25 ml of 1 N

sulphuric acid and boil for 10 min replacing any ‘lossof volume with distilled water. Cool the solution.Titrate the contents .of the flask with 1 N sodiumhydroxide by using methyl red as indicator. End pointreaches when colour changes from red to yellow. Carryout blank in similar manner with 25 ml of 1 N sulphuricacid without substance.

C-4 CALCULATION

Calculate ammonium bicarbonate content Tercent bymass by following formula. Each ml of 1 N sodiumhydroxide is equivalentbicarbonate.

Consumed reading =

Volume of 1 N NaOH =consumed

to 0.07906 g of ammonium

Blank reading – Samplereading

1 N NaOH consumed inblank – 1 N NaOH consumedin test

Content of ammonium=V XN x7.906

bicarbonate by mass M

where

v=N=

~=

volume of 1N sodium hydroxide consumed;

normality of 1 N sodium hydroxide; and

mass of activator, in g.

ANNEX D

[Table 2, S1 No. (ii)(b) and Clause 6]

DETERMINATION OF OXYGEN CONTENT PERCENT BYMASS FROM ACTIVATOR

D-1 REAGENTS

D-1.1 Sodium Thiosulphate (0.1 N)— Dissolve 25 gof sodium thiosulphate and 200 mg of sodiumcarbonate in 1 000 ml volumetric flask and make thevolume with distilled water.

D-1.2 Hydrochloric Acid (2 N) — Take 700 ml ofice Co]d distilled water in 1 000 ml volumetric flask,add slowly along walls 170 ml of concentratedhydrochloric acid, cool and volume up to 1 000 mlmark with distilled water.

4

D-1.3 Buffer (@ 6.85) — Dissolve 14.4 g disodiumhydrogen orthophosphate and 5.726 g potassiumdihydrogen orthophosphate -in 500 ml distilled water.

D-2 PROCEDURE

Weigh accurately about 0.25 g powder and transfer itinto an iodine flask containing 20 ml buffer pH 6.85and 5 ml of 2 N hydrochloric acid. Then add 5 g ofpotassium iodide into it. Shake the solution well andkeep it in dark place for20 min. Add 20 ml of distilledwater in it and titrate it with 0.1 N sodium thiosulphate.

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IS -15608:.2005

End point reaches when yellowish brown colour Burette Reading x 0.0008 x Exactdisappears. normality of 0.1 N Na2S203 x 100

D-3 CALCULATION Weight ofpowder taken, in gram x 0.1

Calculate percentage of oxygen content by the Each ml of 0.1 N sodium thiosulphate is equivalent to

following formula: 0.0008 g of oxygen

ANNEX E

[Table 2, S1No. (iii) and Clause 6]

DETERMINATION OF TOTAL FATTY SUBSTANCE CONTENT

E-1 ‘PRINCIPLE OF THE METHOD

The emulsion is broken with dilute mineral acid andthe fatty matter is extracted with petroleum ether. It isweighed after removal of the solvent.

E-2 REAGENTS

E-2.1 Dilute Hydrochloric Acid — 1:1 (v/v).

E-2.2 Petroleum Ether (6fJ-80°C)

E-2.3 Methyl Orange Indicator Solution — Dissolve0.1 g of methyl orange in 100 ml of water.

E-2.4 Sodium Sulphate (Anhydrous) — Desiccated.

E-3 PROCEDURE

Weigh accurately about 2 g of the material into aconical flask, add 25 ml of dilute hydrochloric acid,fit a reflux condenser into the flask, and boil thecontents until the solution is perfectly clear. Pour thecontents of the flask into a 300 ml separating funneland allow it to cool to room temperature, Rinse theconical flask with 50 ml of petroleum ether in portionsof 10 ml. Pour the petroleum ether rinsings into the

separating funnel, shake the separating funnel well andleave until the layers separate. Separate out the aqueousphase and shake it out with 50 ml portions of petroleumether twice. Combine all the ether extracts and washthem with water until free of acid (when tested withmethyl orange indicator solution). Filter the petroleumether extracts through a filter paper containing sodiumsulphate (anhydrous) into a conical flask which hasbeen previously dried at a temperature of 90 + 2°Cand then weigh. Wash the sodium sulphate on the filterwith petroleum ether and combine the washings withfiltrate. Distil off the petroleum ether and dry thematerial remaining in the flask at a temperature of90* 2°C to constant mass.

E-4 CALCULATION

100 M,Total fatty substance, percent by mass = ~

2

where

Ml= mass of the residue, in g; and

M2= mass of the material taken for-the test, in g.

ANNEX F

[Table 2, S1 No. (iv) and Clause 6]

DETERMINATION OF-HEAVY METALS

F-1 OUTLINE OF THE METHOD F-2.2 Weighing Scale — 0.0001 g accuracy.

The colour produced with thioacetamide reagent in test F-2.3 Volumetric Flasks — 100 ml capacity.

solution is matched against that obtained with standard F-2.4 Platinum Cruciblelead solution.

F-2.5 Pipette — 2, 10 ml.F-2 AP-PARATUS

F-3 REAGENTSF-2. 1 Nessler Cylinders — 50 ml capacity. F-3.1 Concentrated Hydrochloric Acid

5

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IS 15608:2005

F-3.2 Concentrated Nitric Acid

F-3.3 FIydrofluoric Acid

F-3.4 Dilute Acetic Acid — 6 M (342 ml of glacialacetic acid diluted to 1 OOOmlwith water).

F-3.5 Glycerol Mixture — Take 15 ml of 1M sodiumhydroxide and add 5 ml water and 20 ml of 85 percentglycerol. Mix well.

F-3.6 Thioacetanride Reagent — Weigh 80 mg ofthioacetamide and add 2 ml water to it. Shake todissolve. Add 10 ml glycerol mixture, heat on waterbath for 20 s, cool and use immediately.

F-3.7 Lead Nitrate Stock Solution (100 ppm as Pb)— Dissolve 0.1599 g of lead nitrate in water containing1 ml of nitric acid and makeup the solution to 1000 ml.

F-3.8 Standard Lead Solution (10 ppm as Pb) —

Dilute 10 ml of lead nitrate stock solution with waterto 100 ml. Each ml is equivalent to 0.01 mg of Pb.

F-3.9 Acetate Buffer (3.5 pH) — Dissolve 25 g ofammonium acetate in 25 ml water and add 38 ml of7 M hydrochloric acid. Adjust the@I to 3.5 either with2 M hydrochloric acid or 6M ammonia and dilute to100 ml with water.

F-4 PROCEDURE

F-4.1 Place 2 g of cream bleach sample accuratelyweighed in a platinum dish and incinerate for about2 h at 525 to 550”C. Cool and add 1-2 ml of

hydrochloric acid and 0.5 ml nitric acid and evaporateto dryness on the steam bath. Dissolve the residue in5 ml hot water, evaporate to dryness and treat it withhydrofluoric acid. Evaporate again to dryness. Diluteit with water (about 50 ml). Filter the solution, ifnecessaxy,with suction through a fine fritted glass filterand dilute the filtrate and wash it to 100 ml in agraduated flask. This solution shall be used for testsgiven in F-4.2 and G-3 as test solution.

F-4.2 Transfer 25 ml of test solution preparedin F-4.1 in a 50 ml Nessler cylinder, add further 2 mlof test solution and 2 ml acetate buffer @H = 3.5) andmix well. Add 1.2 ml of thioacetamide reagent, mixand immediately dilute with water to 50 ml and allowto stand for 2 min.

F-4.3 In the second Nessler cylinder, place 1 mlstandard lead solution (see F-3.8) and add 2 ml oftest solution. Dilute with water to 25 ml, and add2 ml acetate buffer (pH 3.5). Mix, add 1.2 ml ofthioacetamide reagent, and immediately dilute withwater to 50 ml. Allow to stand for 2 min. Compare thecolour produced in the two Nessler cylinders.

F-5 R-ESULT

The limit prescribed in Table 1 shall be taken as nothaving been exceeded, if the intensity of colourproduced in the test solution is not greater than thatproduced in the second Nessler cylinder which is acontrol test.

ANNEX G

[Table 2, S1 No. (v) and Clause 6]

DETE-RMINATION OF ARSENIC

G-1 PRINCIPLE

-Arsenic present in a solution of the material is reducedto arsine, which is made to react with mercuric bromidepaper. The stain produced is compared with a standardstain.

G-2 REAGENT

G-2.1 Mixed Acid — Dilute one volume ofconcentrated sulphuric acid with four volumes of water.Add 10 g of sodium chloride for each 100 ml of thesolution.

G-2.2 -Ferric Ammonium Sulphate Solution —Dissolve 64 g of ferric ammonium sulphate in watercontaining 10 ml of mixed acid and makeup to one litre.

G-2.3 Concentrated Hydrochloric Acid — See1S 265.

G-2.4 Stannous Chloride Solution — Dissolve 80 gof stannous chloride (SnClz2HzO) in 100 ml ofwater containing 5 ml of concentrated hydrochloricacid.

G-3 PROCEDURE

Carry out the test as prescribed in IS 2088, adding intothe -Gutzeit bottle, 2 ml of ferric ammonium sulphatesolution, 0.5 ml of stannous chloride solution and 25 mlof sample solution as prepared in F-4. 1.

For comparison, prepare a stain using 0.001 mg ofarsenic trioxide.

6

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ANNEX H

(Foreword)

COMMITTEE COMPOSITION

Cosmetics Sectional Committee, PCD 19

Organization

Directorate General of Health Services, New Delhi

All India Small Scale Cosmetic Manufacturer’s Association,Mumbai

Balsara Home Products, Mumbai

Bengal Chemicals & Pharmaceuticals Ltd, Kolkata

Cavinkare Ltd, Chennai

Centrrd “Drugs Laboratory, Kolkata

Central India Pharmacopoeia Laboratory, Ghaziabad

Ciba Speciality Chemicals Private Limited, Gurgaon

Colgate-Palmolive (India) Ltd, Mumbai

Consumer J3ducation and Research Centre, Ahmedabad

Consumer Guidance Society, Mumbai

Dabur Research Foundation, Sahibabad

Food & Drugs Control Administration, Gandhinagar, Gujarat

Food & Drugs Admini$tration, Maharashtra

Galaxy Surfactants Limited, Mumbai

Godrej Consumer Products Ltd, Mumbai

Hhdustan Lever Research Centre, Mumbai

Hygienic Research hrstitute, Mumbai

Indian Soaps and Toiletries Members Association, Mumbai

Johnson & Johnson Ltd, Mumbai

Lady Amritbai Doga College, Nagpur

L’Oreal India Pvt Ltd, Umbergaon, Gujarat

Maharishi Ayurved Products, Noida (lJ.P.)

Marico India Ltd, Mumbai

Mayar India Limited, Delhi

Procter & Gamble India Ltd, Mumbai

Representative(s)

SHRIASHWINJKUMAR(Chairman)

SHRI M. B. DESAISHRJB. M. CHOPRA(Alternate 1)

Smu S. CHAITEJLJSE(,4/terna(e 11)

DR K. C. GOUNDEN

DR SAJAL K. ROY CHOWDHURY

DR A. K. MANOAL (Alternate)

DR M. P. PRASAD

DR G. V. RAO (Alfertrate)

DR M. K. MAZOMDER

DR A. C. DASGUPTA(,41ternafe)

DR SANTOSH.K. TALWARDR SUKOMALDAS(Alternate)

!+uURAJW.HIYER

DR RAJ KOHLISmu SIJNILAGOARWAL(Alternate)

DR C. J. SHISHOO

Smrr Y. S. YELLORE(Alternate)

DR A. R. SHENOY

Smrr N. G. WAGLE(Alternate)

DR N. M. SUNDER

DR B. N. PATELSsnuMA’rrR. B, DESAI(,41/errrafe)

SHRJA. RAMAKRISHNANSmu K. B. SHENDE(Alternate)

SHRJU. SHSKARSsuu GOPIRAMAN(Alternate)

SHRJA. RANGARAIANDR ([email protected](A//ernate)

SHRJV. R. DHANUKASHRJN. S. BULANJ(Alternate)

SHRJM. B. DESAI

SHRJMANISHK. CHHABRA(Alternate)

SHRJR. HAJUHARAN

DR PRASHANTABHYANKARDR V. R. BAMBULKAR(Alternate)

DR (SSUUMATJ)S. B. KULKARNI

SHRJR. JAYARAJ

DR S. C. SAXSNASHIUD. K. SHRJVASTAVA(Alternate)

SHRJR. MOHILE!$rrsrBENEDICTM. (Alternate)

DR S. ADHIKARI

SHJUMATJSHWSTAPURANDARE

7

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IS 15608:2005

Organization

Shinrgar Ltd, Mumbai

BIS Directorate General

Representative(s)

SHRIV. K. SINGH

SHRIMATISWATI SINGH(Alternate)

DR(SHRIM&TI)VIJAYMALrK,Director and Head (PCD)[Representing Director General (Ex-oficio A4ernber)]

Member Secretary

SHRIMATIKAGAMANIT.Assistant Director (PCD), BIS

Composition of Decorative and Miscellaneous Cosmetics Subcommittee, PCD 19:4

MmlustanLever Research Centre, Mumbai

Balsara Home Products, Mumbai

Central Indian Pharmacopoeia Laboratory, Ghaxiabad

Colgate Palmolive (lndia) L]mited, Mumbai

Consumer Education and Research Centre, Ahmedabad

Consumer Guidance Society, Mumbai

Dabur Research Foundation, Sahibabad

Fern Care Pharma, Mumbai

Food & Drugs Control Administration, Gandhinagar, Gujarat

Food & Drugs Administration, Maharashtra

Glaxosmith Beecham Asia Private Limited, Gurgaon

Godrej Soaps Limited, Mumbai

Johnson & Johnson Ltd, Mumbai

Keel Colours Pvt Ltd, Mumbai

Mayar India Ltd, Delhi

Nogi & Company Pvt Ltd, Mumbai

Procter & Gamble India Ltd, Mumbai

Shhgar Ltd, Mumbai -

Wyeth Lederle Ltd, Mumbai

SHSUS. M. SHANRAGH(Convener)Smu AIAYVASHI(Alternate)

DR K. C. GOUNDE~

DR SUKOMALDAS

SHRJH. S. GOEL(Alternate)

DR SUNIL AGRAWAL

DR SHASHNKPONTSS(Alternate)

SHRI S. YELLOKE

DR FALGUNI“MAZUMOAR(Alternate)

DR A. R. SHENOY

SHRSN. G. WAGLE (A1/ernate)

DR N. M. SUNDER

SHRSDHIRAI KHATrAR (Alternate)

SHSUARUN DESHFANDE

Smu H. V. KOLTE (Alterrrale)

DR R. B. DESAI

SHIUH. B. CHAUDHASU(Alternate)

Smu A. RAMAKSUSHNAN

Smu K. B. SHE~DE(Alternate)

DR MAHESHC. BURSHE

SHM A. RANGARAJAN

DR (SHRIMA@ ROW THAKKAR(Allerrrate)

DR P. N. ARHYANKAR

Saw V. R. BAMMLXAR(Alternate)

SHRI D. DESAI

DR S. ADHI~ARI

DR R. D. PANDIT

Smu M. S. AMRARDEKAR(Alternate)

SHRIMATISHWETAPURANDARE

Sam VINAY KUMAR SINGH

Ms SWATHISINGH(Alternate)

SHSUM. V. BULEULE

SHRSS. R. KULSHRESHTHA(Alternate)

8

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Bureau of Indian Standards

BIS is a statutory institution established under the Bureau of Indian Standar& Act, 1986 to promoteharmonious development of the activities of standardization, marking and quality certification of goods andattending to connected matters in the country.

Copy-right

BIS has the copyright of all its publications. No part of these publications may be-reproduced in any formwithout the prior permission in writing of BIS. This does not preclude the free use, in the course of implementingthe standard, of necessary details, such as symbok and sizes, type or grade designations. Enquiries relating tocopyright be addressed to the Director (Publications), BIS.

Rewiew of Indian Standards

Amendments are issued to standards as the need arises on the basis of comments. Standards are also reviewedperiodically; a standard along with amendments is reatl%med when such review indicates that no changes are-needed; if the review indicates that changes are needed, it is taken up for revision. Users of Indian Standardsshould ascertain that they are in possession of the latest amendments or edition by referring to the latest issue of‘BIS Catalogue’ and ‘Standards: Monthly Additions’.

This Indian Standard has been developed from Dot: No. PCD 19 (2200).

Amendments Issued Since Publication

Amend No. Date of Issue Text Affected

BUREAU OF INDIAN STANDARDS

Headquarters:

Manak Bhavan, 9 Bahadur Shah Zafar Marg, New Delhi 110002Telephones: 23230131,23233375,2323 9402 website: www.bis.org.in

Regional Offices: Telephones

Central :

Eastern :

Northern :

Southern :

Western :

Branches :

Manak Bhavan, 9 Bahadur Shah Zafar Marg{

23237617NEW DELHI 110002 23233841

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SCO 335-336, Sector 34-A, CHANDIGARH 160022{

26038432609285

C.1.T. Campus, IV Cross Road, CHENNAI 600113{

22541216,2254144222542519,22542315

Manalcalaya, E9 MIDC, Marol, Andheri (East){

28329295,28327858MUMBAI 400093 28327891,28327892

AHMEDABAD. BANGALORE. BHOPAL. 13HUBANESHWAR.COIMBATORE. FARIDABAD.GHAZIABAD. GUWAHATI. HYDERABAD. JAIPUR. KANPUR. LUCKNOW. NAGPUR.NALAGARH. PATNA. PUNE. RAJKOT. THIRUVANANTHAPURAM. VISAKHAPATNAM.

Printed at Simco Printing Press, Be.lhi