ICP Test Report Certification Packet - littelfuse.com/media/electronics_technical/icp_test... · 'The new RoHS directive 201 1/65/EU, on Jul. 21 , 201 1 come into lorce on Jan. 03,

1

ICP Test Report Certification Packet

Company name : Littelfuse, Inc. Product Series: 5x20 Cartridge Product #: 234xxxP Series Issue Date: January 27, 2012 It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC)-restricted substance nor such use, for materials to be used for unit parts, for packing/packaging materials, and for additives and the like in the manufacturing processes. In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing processes, are all composed of the following components.

Issued by:

<Global EHS Engineer>

(1) Parts, sub-materials and unit parts This document covers the 5x20 Cartridge RoHS-Compliant series products manufactured by Littelfuse, Inc. ＜ Raw Materials Used

Please see Table 1 (2) The ICP data on all measurable substances Please see appropriate pages as identifed in Table 1

Remarks：

Form 585-047 Rev. A 2/21/06

2

Table 1: List of Raw Materials covered by this report

Total Parts Raw Material Part Number Raw Material Description Page(s) 1 C910541 Cap 3-6 2 909532 Body-Ceramic Tube 7-29 3 C909543, C909542 Body-Soda Lime Glass 30-33 4 11-0595 (082xxx-001) Element – Cu99.9MSn 34-40 5 687xxx-001 Element - Sn Plated Ag Cu 41-50 6 648xxx-001 Tinned Wires 41-50 7 YTW102 (692535-002) Solder 51-55

8 3M 3779-PG (087244) HMA 56-60, 61-64

9 934-077 (C030208), C030210 Overcap (Cap base and plating) 65-68 10 934-077 (C030208), C030210 Overcap (Wire base and plating) 65-68 11 091251 Filler-Sand 69-74 12 425901 Ink-Red 75-89 13 425902 Ink-Black 90-104 14 425903 Ink-Yellow 105-119 15 425904 Ink-Blue 120-133 16 425906 Ink-Brown 134-148 17 425907 Ink-Green 149-163 18 425909 Ink-Grey 164-178

nov'TEST REPORT

NO.jA002E11121307'1R02 DaG:Dec.t5,2Oi1 page 1 of4Custom6i Suzhou FuHong Eteclronic IndustialCo., L6.AddT€sg: NO.89 WEIDU ROAD, WANGTINGTOWN. XIANGCHENG oIsTRIcT. sUzHoU. CHINAReport on tie subnitied samptes.id to beSample name: Copper shellModsl: /

Materlal: /D€cripiion: /Buyer: /Supplier: /

SamPle rcceiwd date: Elec.'13,2011T€dng poriod: From Dec.13,2011 lo Dec.15,2o.l1

T€lino Reou6tedAs sp€cified by client, to detemine the L€ad, Cadmium, Mercury & Hexavat€nt Chromilm content an the slbmified sampte inaccordance wilh Dircctive 200295/EC (RoHS).

Te.Uno method:

T€sling liem Measuring instrument MQL

Lead (Pb) IEC 62321:2008, section I rcP-oEs 2mg/kgcadmium (cd) IEC 62321:20t,3, s€clion 9 tcPoEs 2 mg/kgllercury (Hg) IEC 62321:2008, section 7 lcPoEs 2 mg/kg

Chromrum (Cr l'1) IEC 62321:2008, Annex B 0 o2mgkg'

---FOR FURTHER DETAILS, PLEASE REFERTOTHE FOLLOWNG PAGE(ST**'

leg-' 0.02 mg/kg reGrc lo the MQL of sampte extraction tiquid.

99!9!cis!i-When tesled as specined the submi(ed sample compli€d wilh the rcquirements of commission Decision of 18 Aug 2005amending Directive 2002/95/EC notilied undef document 2005/618/EC.

Pro,ect Leader /{bjA-L(Engine€r) J 4

lnsoected bv

,**'*''*,n-, [,[rlg-,i ti-Y\

,ffi:::j:,,44

SHENZHEnl AOVTESTINC TECHNO!OGY CO..L.TD,KUI\ISIIAI\I BRANCIi Holline86.512.5510 8000

nov.NO,: A002E11121307-1 R02

TEST REPORT

Tesled by ICP-OES

Add the digestion sotutioni thevessel is healed until the sampl€has b€€n dissolved

Weigh the sample into

F*_-l-Content (Melal substEle)

Add the digeslion solutjon, ctose

the micfowave ves:€|.

F;;1.-and l\Iercury Content (Plaling)

To Detenn exavalenl Chromium Content (bojting- wateF extraction): (Metat substrate)

The sample is digesred in the

mrcrowave oven iollowing a sp€citic

decomposilion program.

Tesl lh€ s€mple solution and the 0.02mg/kg standard solution by UV-VIS.

Hotline86-512-5510 8000

To

+Cooling the vessel, fltet washed and

filled to the ma* with distilled wat€r.

Remove the sample, and coolthe beaker to room lemperature,and do the color leadion

sample in the beaker.Heat 50 mL of Dl waler in the

beaker to boiling ior 10 min

To Delemine

___+l coorins. rirtei washed and lilled l_-_----|l resteo oy l+fl_*l

I t o t he ma*w i th D twa te r .

I l r n " r ,u rn "n , I l " * ' I

SHENZHsN AOV TG6TING ICCHITOI"OGY CO.,L'O.KUNAHAN BRANCH a

nov'NO.i 4002E11121307-rR02

5. To O€temine Hexavalent Chromium

,':"j":::i v^02

Place 1-5

TEST REPORToste:oec15,2011

Contentin colorless and cotorcd cnromaE coating on metats(Plaljng)

5 2 Eoiling- wat6F extraction

Tako the (50+5) cm'?

sample in the beaker.

S!IENZHEN AOV'CSTING IECIINOIOGY CO..ITD,KUNSHAN gNANCH Hotlinea6-512-5510 8000

lf the tesl rcsult is posilive,

the sample is considercd tohave hexavalenl chromilm

Compare the

and lhe 0.02 mg/(qstanda.d solution

Eoiling- wateF ext€ctjonprccedurc shall be used to

lfthere is int€rference or it is hard to decide whetherthe sampl€ have tie h€xavatent chromium

Remove tie sample, and cool

lhe beaksr to room tempeEture,

and do the color reaolion

Heat 50 mlof Dlwaier in the

beaker lo boiling for 10 min

Test the sample solution and the 0.02mg/kg standard solution by UV,VIS.

T€t Re6ult3:

Unit RoHS

Limil

Result

Substrate Plating'

Lead (Pb) mg/Kg 1000 N.O. N.O.Cadmium (cd) mg/Kg 100 N.D, N.D.lvercury (Hg) mgn(]s 1000 N.D. N.D.

chromium (Crl'I) mg/Kg 1000 Negalive Negative

nov-TEST REPORT

NO 4002E11121307.rR02

'The new RoHS directive 201 1/65/EU, on Jul. 21 , 201 1 come into lorce on Jan. 03, 20 1 3 the fomat imptementation. Direclive2002,95/EC shall be rcpeated simuttaneousty.

-specimens, which requested to determine Lead, cadmium and l,rercury conteni, have been dissorved comprererv

-N.D.=not detected(<tltoL)-MOL=ntethod Ouantitation Limit-Negative=Absence of Cr (VIir

PositivF Presence ofCr (\ll)i

Unc€rlain= can not verify whetlerthe sampte have Hexavatent Chromium by spoltest.(The test€d sample should be fufthet verified by boiling-waler-€nraction method if the spot test resutt |s uncertain ornegalive. )

-'The tesl is based on lhe following assumption:The sampte ptating is a singte tayefand each paft is uniform. The tesr resuttmaybe cannotsland br lhe physicaltruth ofsampte ptating.

Photograph ofSample

Coppershell

SHENZHEN AOVT€STING TECHNOLOGYCO.,IID,XUNSHAN ARANCTI e!:-"Jllls,.**

Validit nownFor Qu€5llPlease Co ith scs

t:|l l llllnTest RePortCERAMTEC GMBH

The following samPle(3)

Sample DescriptionStybr'ltem No.Sample Receiving DdeTesting Period

No.: CEI2of n1777 O./(e | 2O11t02122 Page | 1 of 23

was/weE submitted and ideniified by/on behalf of the client as:

CERAMIC TUBEc61020111021142011 IOZ 1 4 rO 201 1 l12l22

Please refer to next Page(s).

Bas€d uDon the performed tests by submitted sample6 the test re6ults of C?dTiT ..Lead, Mercury, Hexavalent Chromium Cr(Vl) PBBS and PBDES comply wltn tne llmls or

RoHS Directive 200295/EC and its slbs€quent amendments'

Test Result(s)

Conclusion

u::::jYi.,rf:'T:11r":ii'il"T[:iT'T:1.:i--,:{1:11!Y,lii.ti"'"1*-:"]*l:j::T:::l1 ::*'-'**--"'^"#imr;#r*.i"";:m,r,'r"'*.'*":*rrlft*:nTc*"'"1'l'#aif*1"?'Y:ffiffiiil;"[fli:",r#r."il:'ffBilil:iil#iliaji-,.'.iJi."",ii]:,i"ao";i;;xrearr"."eryr'oo*ornloei;in;;d"sodb,,dma6d"".!hi,.; ; " . . " ; ; . . . . . ' ' ' - ' . * * . - " - * . * r . " " c " - - " " '; ; . ; ; . . ; - ; ; r * , . * * * *a - d@ivs - " . - n ' - r i : . * ; * * " * " ' . ' '

' r i i l " :

i r ' 1 ' r LsMo? t r s "

g$d for.tld

Ct-r ..1L&..1btv-TrF.l

Test Report No. : CE12O11121777 D e:2011102122 Page 2of23

CERAMTEC GMBH|l||1[rrl0lllllrlll

Test Result{sl

PART MME No.1 GRAY CERAMIC

Te6t lt6m (s): Unit Method MDLResult LimitNo,t

cadmium (Cd)

LeaJ]FE'-

Mercury (Hg)

m9Kg Wlifi'Erenerence to lEc 6232 ! i 2008 andperformed by ICP-AES.

2 n.d. 100

m!/Kg W;ifrErencelo IEC 62321: 2008 andperformed by ICP{ES.

2 100 1000

Wii[reference to lec 62321: 2008 andpedormed by lcPaES.

2 n.d. 1000mgl(g

WiiFreference o tec 02321: 2008 andpeformed by uV-VlS.

n.d. 1000Hetavalent Chromium Cr(Vl) bYalkaline extraction

m9/Kg

Folychlodnated Biphenyls (PCB8)(CAS No.:001336-36-3)

mgikg rl/itlt reGrence to US EPA 3540C methodAnalysis was performed bY GC/MS.

n.d.

Polychlodnated NaPhthalen€(PCNs)

mg/k9 WiiF reference to Us EPA 3540c method.Analysis u,as performed bY GC/MS

5 n.d.

Polychlorinated TelphenYls(PCTs)

mdks Fittr reference to US EPA 3g0C methodAnalysis ,,.€s perform€d by GC/MS

0.5 n.d.

Alkanes, C10-13, chloro (ShodChain Chlorinated Paraffins) (CASNo. | 08553H,L4)

WiFh reference to uS EPA 3540c methodAnalysis $ras pedormed bY GC/MS

0.01 n.d.

Formaldehyde (CAS No.: 000050-004)

mg/Kg wttr reference to lso tz2m-1e008'|Analysis raEs performed by HPLC/DAD

3 n.o_

PVC Analysis was performed bY FTIR andFLAME T€st.

Negative

Pedluorooctane sulfonates(PFOS)PFOS - AcidPFOS - Metal saltPFOS -Amide

mg/Kg with reference to US EPA 3540C: 1 996method for PFOS Content. Analysi6 wasperfoFned by LC/MS.

1 0 n.o.

PFOA (CAS No.: 000335$71) mg/Kg With reference to US EPA 3540C: 1 996method for PFOA Content- Analy6is waspedormed by LC/[,S.

1 0 n.o_

Menbedm,!G5creuP665er

Test Report No. I CE12O11121777 Dale: 20111O2J22 Paoe: 3of 23

CERAMTEC GMBH l]mtt|l|||l|r[r

Te6t ltem (s): Unit Me{hod MDLRe.ult

LimitNo.1

Monomethyl dibromodiphenylmethane (DBBT)

mgftg With reference to US EPA 8270D method.Analysis was perfomed by GC/MS.

0.5 n.d.

Monomethyl dichlolodiphenylmethane (Ugilec'l21)

mg/Kg With reference to uS EPA 8270D method.Analysis was performed by GC/MS.

0.5 n.d.

Monomethyl te'trachlorodiphenylmethane (Ugilec141)

mg/Kg With reference to US EPA 82700 m€thod.Analysis ,.,ras perform€d by GC/MS.

0.5 n.d.

Organic.tin compoundsTributyl Tin (TBT) (CAS No.:00068E-73-3)

mg./Kg With reference to DIN 38407-13. Analysiswas performed by GC/FPD.

0.03 n.d.

Triphenyl Tjn (TphT) (CAS No.:000668-34-8)

mg/Kg With reference to olN 38407-13. Analysiswas oerformed bv GC/FPD.

0.03 n-d.

Halon6Halon-1211(CAS No.: 000353-59-3)

mg/kg With Gference to IJS EPA 5021 m6thod.Analysis was performed by GC/MS.

1 n.d.

Halon-1301(CAS No.: 000075$3-8)

mg/Kg With reference to US EPA 5021 method.Analysis was performed by GC/MS.

I n.d.

Halon-2402(CAS No.:000124-73-2)

mg/Kg With reference to US EPA 5021 method.Analysis wE6 performed by GC/MS.

I n.o.

HaloqenHalogen-Fluorine (F) (CAS No.:014762-94-8)

mgikg With reference to BS EN A5A2'.2OO7 .Analysis was performed by lC.

50 n.d.

Halogen4hlorine (Cl) (CAS No.:022537-15-1)

mg/Kg With reference to BS EN ft54220o7.Analysis ,r/as perfo.med by lC.

50 n.d.

Halogen-Bromine (Br) (CAS No.:01 0097-32-2)

mg/Kg With reference to BS EN 14582:2007.Analysis was performed by lC.

50 n.o.

Halogen-lodine (l) (CAS No.:01436244-8)

mSikS With reference to BS EN 14582'2007 .Analysis was perfomed by lC.

50 n.d.

o 6 J l . j e d r h s € $ € p d e | d e r c

Test Report No.: CH2O11t21n7 Dale:201110222 Page: 4 of 23

CERAMTEC GMBHrt] [tllu|Illllll

T€6t ltem (slr Unit Method MDLResuli LimitNo,1

Asb€toeAclinolite (CAS No.: 077536€6-a)

ffio6Gl6RiTo;TiZ1Ztit

To Wiih refer€nce to NIOSH 9000 methodAnalysis w€s performed bY XRD

1 Negative

o/o WlGlarence to NIoSH 9000 methodAnalysis was performed bY XRD

,t Negative

AnthQhy ite (CAS No.: 077536-67€)

o/o with reterbnce to Ntostt 9000 methodAnalysis was perfomed bY XRD

I Negative

Chrysotile (CAS No.: 012001-2$51 '/o wttr referenc; to NIOSH 9000 methodAnalysi6 was Performed bY XRD

Negative

Oocidolite (CAS No.: 012001-2&4)

% Wlifr-reference to NlosH 9000 method.Analysis was performed bY )(RD

Negative

Tremolite (CAS No.; 07753+684) % Wlih-Erence to l.llosH 9000 method.Analysis was pedomed bY XRD

Negative

PhthalatesBBP (Berizyl butyl phthalato) (cAsNo.:000085$8-7)

% Wiif,reference to EN 14372 Analysis wasperformed by GC/MS.

0.003 n.o.

DEHP (Di- (2-ethylheryDphthalate) (CAS No.: 000117€1-7)

Wittr reference to EN 14372. Analysis waspeformed by GC/MS.

0.003 n.o.

DICrP (Di-isodecyl phthalate) (CASNo.:02676'l-4Go)

Wil6Fference to EN 14372. Analvsis waspedormed by Go/MS.

0.01 n.d.

DINP (Di-isononyl phthalate) (CASNo.:028553-12{)

% Wiith reference to Ett 14372. Analysis waspedormed by GC/MS.

0.01 n.o-

ENOP (Di-n-octyl Phthalate) (CASNo.:000117€4-0)

o/o With reference to EN 14372. Analysis waspedormed by GC/MS.

0.003 n,o.

oBP (Dibutt phthalate) (cAs No.000084-74-2)

% Wittr reterence to gH t472. Analysis wasperformed by GC/MS.

0.003 n.d.

i f h 3 c d € p & d a o n ' b f i m p b ] 3 ) l a s 1 t s ] h 6 . : a e ' o d € m d b @ l d u

ffi**":m;.*,""*r'rx,t$":6:xx4,g$5E.###:iiliili:#ffil;##i'i;;ffi11,1",-#Hlrl"T#ifrll.fl$ris#ililrysilfis*ii'ijsr,^!i!;64iliE$m:1*,frru:g,:rU*n:n:l,m*i*nr*;:m*il*n",:m-rj*:m*i!r:i';rx::i:fl ff :H;[: v$9il,.*TTs"I;3trfl"J:^,

Test Report No. I CH2011121n7 Date: 20111O2n2 Page : 5 of 23

CERAMTEC GMBH

Tosl ltem (e): Unit Method fiIDLR€ault LimitI'lo.l

Sum ot PBBS

mgkg With referenc€ to IEC 62321 : 2008 andpe.formed by GC/MS.

n,o, '1000

Monobromobiphenyl 5 n.o.Dibromobiphenyl 5 n-d.Tribromobiphenyl 5 n.d.Tet€bromobiphenvl n.d.Pentabromobiphenyl 5 n.d.Hexabrcmobiphenyl 5 n.d.Heptabromobiphenyl 5 n.d.Octabromobiphenyl n.o.Nonabromobiphenyl 5 n-d.Decabromobiphenyl 5 n.d.Sum of PBDE5 n.d. 1000Monobrcmodiphenyl ether n.d.Dibromodiphenyl ether 5 n.d.Triblomodiohenvl ether 5 n.d.Tetrabromodiohenvl ether 5 n.d.Pentabromodiphenyl ether n.o,Hexabromodiohenvl ether n.o.Heptabromodiphenyl ether n.o.OctabrornodiDhenvl ether n.d-Nonabroinodiohenvl ether n.d.Decabromodiohenvl ether n.d.EO1): 4-AMINODIPHENYL (CAS No.:000092s7-1)

mg/x{l With reference to LFGB 82.02-2. Analy6iswas performed by GC/MS-

n.cl.

2): BENZIDINE (CAS No.: 00092-87-5)

mg/Kg With reference to LFGB 82.02-2. Analysiswas performed by GC/MS.

3 n.o.

3): 4-CHLORO-O-TOLUIDINE(CAS No.: 00009S9-2)

mg/Kg With reference to LFGB 82.02-2. Analysisr,r€s performed by GC/[,S.

n.d.

4): 2-I'IAPHTHYLAMINE (CASNo.: 000091-59-8)

mS/kS With reference to LFGB 82.02-2. Analysislras performed by GC/MS.

3 n.d.

5): O-AMINOAZOTOLUENE (CASNo.: 000097-56-3)

mg/(g With reference to LFGB 82.02-2. Analysis,va6 perfomed by GC/MS.

n.d.

o(sl bd.d rh e bd €pod eimr b. recdDao 4 r r; !i :{u. i-n:!r rr,{lf rilir.ll,rii nF :*r..+.f d!: .-! r il j. I Jr ri 1llfttsdomsnr s s€dbyb6cmFry'or drdoic romo' do.!re s suqd

Ie@dGd€rcepi'nj!

idutL zoi€ N€{Lpe.o L,d]n- ' ' ] .1] :

scsTest Report No. : CEJ201121777 Dale:2011t0i,22 page:6of23

CERAMTEC GMBH ll]tI|t|||||ttltt!

Test ltem (3): Unit Mothod MDL ReaultLimitNo.l

b): z:AMtNo-4-NtTROTOLUENE(CAS No.: 000099-55-8)

mg/Kg With reference to LFGB 82.02?lAi;ii;i;wEs perfomed by GC/MS.

n.d.

7): P-CHLOROAN|L|NE (CAS flo-00010647{)

mgkg With reference to LFGB 82.02-2. Anatysiswas perform€d by GC/MS.

n.d.

E): 2,+DTAMtNOANtSOLE (CASNo.:000615-05-4)

mg/Kg with reference to LFGB 82.02-2. Analysisrnas perfomed by GC/MS.

n.d.

9): 4,4'-DIAMINODIPHENYLMETHANE(CAS No.: 000'101-77-9)

mS/kg With reference to LFGB 82.02-2.jndysis-was performed by GC/IMS.

3 n.d.

'lo): 3,3 -DtcHLOROBENZtDtNE(CAS No.: 000091-94-1)

mg/xg With reference to LFGB 8rj-. Anatysswas perfomed by GC/MS.

3 n.o.

1 1): 3,3'-DIMETHOXYBENZID|NE(CAS No.: 00011990-4)

mgiks With reference to LFGB 82.02-2. Analysis\Nas performed by GC/[,I|S.

3 n.d.

12): 3,3:DIMETHYLBENZtDtNE(CAS No.: 00011$93-7)

mgkg With referenc€ to LFGB 82.02-2. Anatysiswas performed by cC/[rS.

3 n.d-

13): 3,3 -DlMETHYL4,4 -DIAMINODIPHENYLMETHANE(CAS No.: 000838-88-0)

mg/Kg With reference to LFGB 82.02-2. Anaitsiswas performed by GC/MS.

3 n.d.

14)r P-CRESIDINE (2-METHOXY-s-METHYLANILINE) (CAS No.:000120-71-8)

mg/K9 With reference to LFGB 82.02-2. Analysisi/as perfomed by GC/MS.

3 n.cl.

15): 4,4'-METHYLENE-B|S- (2-CHLOROANILINE) (CAS No.:0001 01 -1,f-4)

mg/kg With r€ference to LFGB 82.02-2. Anatysis$ras pedormed by co/lrs.

3 n.d.

16): 4,4'-OXYDIANILINE (CASNo.: 000101-80-4)

mg/Kg with reference to LFGB 82.02-2. Anatysiswas pedormed by GC/MS.

3 n-d.

17): 4,4'-THIODIANILINE (CASNo-:000139€5-1)

mg/Kg With reference to LFGB 82.02-2. Anatysisw€3 pertormed by GC/MS.

3 n.o.

18): o-TOLUIDINE (CAS No.:000095-s34)

mg/Kg With reference to LFGB 82.02-2. Analy6iswas perfomed by GC/MS.

3 n.d.

'19): 2,4-TOLUYLENEDIAMINE(CAS No.: 000095-80-7)

mg/Kg With reference to LFGB 82.02-2. Anat6isrvas perfomed by GC/MS.

3 n.o,

20): 2,4,s-TRIMETHYLANILINE(CAS No.: 000137-17-7)

mg/Kg With reference to LFGB 82.02-2_ Analysiswas pertomed by GC/MS.

3 n.d.

i ' tr| isEd€pd6ldlodylohesanple13)l6'drh3'a*GFietrd!eF4: r r / s , r r1 i i . t , ;h r r r . ! . r " . r l i r . : ! , r ! : ly s 6 l d b 6 G e i 6 d c s d l o r e d s s

btsFdld'rupl]nil lhhdpior

&meror rh€ scs cblp 665 sAl

Test Report No. : CEaU1D1777 Oale :2OjjtOZ2z page : 7of 23CEMMTEC GMBH lmfllr||fimrl|r

Test lten (s): Unit Method MDL ResultLimit1{o.t

2r)r o-ANtstDtNE (CAS No.l000090{4-0)

mg/K9 With reference to LFGBE.ou. Ana'liiwas perfomed by GC/MS.

n.d.

zz): r"-AMtNoAZoEENZENE(CAS No.: 00006M9-3)

mS/kg With reference to LFGB 82.o2-Zlnatysisrvas performed by GC/MS.

n.d.

zJ): 2,4-xYLrutNE (cAs No.:000095$8-1)

mg/kg With reference to LFGB 82.02-2_ Analysis^/a6 perfomed by GC/MS.

n.o,

24): 2,6-XYLIDINE (CAS No.:000087€2-7)

mg/l(g With efer€nce to LFGB 82.02-2. Anatysisas performed by GC/MS.

n.d.

CFC's (ChloJofl uorocarbon3)Group IChlorof luorocarbon-1 1 (CAS No. :000075€9.4)

mg/Kg With reference to US EpA 5021 methodAnalysis was pertormed by GC/MS_

1 n.d,

Chlorofluoroca6on-12 (CAS No.:000075-71-8)

m9/l(g With reference to US EpA 50216ethod-Analysis was perfomed by GC/MS.

1 n.d.

Chlorcf luorocarbon-1 1 3 (CAS No.:000076-1 3-1 )

mdks With reference to US EpA 5021 methodAnalysis r{as performed by GC/[jS.

1 n.d.

thlorotluorocarbon-l 14 (CAS No.i000076-14-2)

mg/kg With reference to US EPA 5021 method.Analysis \ras performed by GC/IrS.

1 n-d.

Chlorof luorccarbon-1 15 (CAS No.00007c15J)

mg/Kg With rcference to US EpA 5021 methodAnalysis was perform€d by GC/MS.

I n.o.

Group lllChlorofluorocarbon- 1 3 (CAS No. :000075-72-9)

mg/Kg With reference to US EpA 5021 method.Analysis was performed by GC/MS.

1 n,d,

Chlorcfluoroca6on-1 1 1 (CAS No.:000354-56-3)

mg/Kg Wilh reterence to US EPA 5021 method.Analysis was pertomed by GC/MS.

1 n.d.

uhrorofl uorocaruon-1'12 (CAS No.:000076-12-0)

mS/kg Wath reference to US EPA 5021 method.qnalysis was perfonhed by GC/MS.

I n.d.

Chlorof luorocarbon-21 1 (CAS No.:oo0422-7851

mS/kS With reference to US EPA 5021 method.Analysis wa6 perfomed by GC/MS.

1 n.d.

Chlorofl uoocarbon-212 (CAS No.:003182-20-1)

mdkg With r€ference to uS EPA 5021 method-qnalysis was perfomed by GC/MS.

1 n.d.

Chlorof luorocarbon-2 1 3 (CAS No.:002354-06-5)

mg/kS With reference to US EPA 5021 method.qnalysis w€s performed by GC/MS.

1 n.d.

Chlorcfluorocarbon-214 (CAS No.:0292ss-31 -0)

mgKg With reference to IJS EPA 5021 method.qnalysis wEs performed by GC/MS.

I n.d.

Test Report No. : CEt2011t21777 Oale :2011|t0i,22 page | 8 of 23

CERAMTEC GMBH l [tltu[luttl

Test ltom (s): Unit irethod MOL ResultLimitNo.1

Chlorofluorocarbon-2 t 5 (CAS ltto:0042594}2t

mg/Kg With referenc€ to US EpA 502i method.Analysis ,,vas performed by GC/[,S.

n.d.

Chlorof luorocarbon-216 (CAS No. :000661-97-2)

mg/Kg With reference to US EFA 502 1mElFodAnalysis was performed by GC/MS_

n,o,

Chlorof luorocarbon-21 2 (CAS No-000422-866)

mg/kg with reference to us EpA 5021 nrethodAnalysis was performed by GC/MS.

n.d.

CHCa (Chlorinate hydrocarbon)1 ,1 , 1 ,2-Te'trachloroethane (CASNo.: 000630-20-6)

mg/Kg With reference to US EPA 5021 methodAnalysis ,,rras performed by GC/MS.

n.d.

1, 1, 1-Trichloro€thane (CAS No.:000071-556)

mg/kg With reference to US EpA 502.1 m6i6o<t-Analysis vr€6 performed by GC/MS.

n.d.

1, 1,2,2-Tetrachloroethane (CASNo. : 00007$345)

mdkg With reference to US EPA 5021 methodAnalysis wEs perfo.med by GC/lrS.

n.d-

1, r,Z- Inchloroethane (CAS No.:0000794G5)

mg/Kg With reference to US EpA 5021 method.Analysis u/as performed by cc/l\rs.

n.d.

1,1-Dichloroethane (CAS No.:00007r3+3)

mg/Kg With reference to US EPA 5021 method.Analysis was performed by GC/MS.

n.o.

1,'1-Dichloroethene (CAS No.:00007t35-4)

mg/Kg Wth reference lo US EPA 5021 methodAnalysis was performed by GC/MS.

n.d.

1,1-Dichloropropene (CAS No.:000563-s8€)

mg/kg with reference to us EPA 5021 method.qnavsis was pertormed by GC/MS.

n.d.

'1,2,3-Trichloropropane (CAS No.:000096-184)

mg/Kg With reference to US EPA 5021 method.qnalysis was perfomed by GC/MS.

n.d.

1,2-Dichloro€thane (CAS No.:0001 07-06-2)

mSikS With reference to US EPA 5021 method.qnaryds was performed by GC/MS.

1 n.d.

1,2-Dichloropropane (CAS No.:000078-87-5)

mSikg With reference to US EPA 5021 method.Analysis was performed by GC/MS.

n.d.

'1,3-Dichloropropane (CAS No.:000142-28-9)

mg/tg Wilh reference to US EPA 502'1 method.Analysis ,,rras performed by GC/MS.

n.d.

2,2-Dichloropropane (CAS No. :000594-20-7)

mg/Kg With reference to US EPA 5021 method.Analysis \r/as performed by GC/MS.

n.d.

Carbon tetr€chloride (CAS No.:000056-23-5)

mg/Kg With reference to US EPA 502'1 method.Analysis was performed by GC/MS.

n.o.

Chloroethane (CAS No.: 000075-00-3)

mg/Kg Wth refcr€nce lo US EPA 5021 method.Analysis was performed by GC/MS.

n.o.

' f : . : ; ' : r t i J 1 * j , i t r r i l ! . , : r j i r r l . 1 1 ; r j ' . j - , , i j L

6l ..cts c iomd d6!mm. {bJel

t . r q h b a n d o b i g a l o n s m d b e l € i , , d - d l F E b .

Test Report No. : CEl2011l21TI7 Date :2l1jto2t22 page : 9 of 23

CERAMTEC GMBH lll ||I]l||ttlll

Tsst ltem (6): Unit Method MDL ResultLimit

No.1Chloroforn (CAS No.: 000067-6G3)

msikg With reference to US EPA 5021 method.Analysis wEs performed by GC/MS.

1 n.d.

Chloromethane (CAS No.:000074€7-3)

mg/Kg With reference to l-JS EpA-O2Gethod-Analysis was performed by GC/MS_

n.d.

cis-1,2-Dichloroethene (CAS No.:000156-59-2)

mg/Kg Wath reference to US EPA 5021 melhod.Analysis was performed by GC/MS.

n.d.

cie1,3-Dichloropropene (CAS No_:010061-01-5)

mSikS With r€ference to US EpA 5021 methodAnalysis vr€s performed by GC/MS.

n.d.

Hexachlorobutadieno (CAS No.:0000876E3)

mg./kg With reference to US EpA 5021 methodAnalysis uras performed by GC/[/|S.

n-d.

Methylene Chloride (CAS No.:000075-0$.2)

mg/kg With reference to US EPA 5021 methodAnalysis ,r€s performed by GC/MS.

n.o.

Tetrachloroethene (CAS No.l000127-184)

mg/Kg With fefe.€nce lo uS EPA 5021 mJthodAnalysis was perlomed by GC/MS.

n.d.

trans-1,2-Dichloroe{hene (CASNo.:00015660-5)

mSikS With reference to US EPA 5021 nrettrodAnalysis wEs perfomed by GC/MS.

n.d.

trans- 1,3-Dichloropropene (CASNo.: 010061{26)

mdkg With refe€nce to US EPA 5021 m€thod.Analysis wae performed by GC/lrS.

n-d.

Trichloro€thylene (CAS No.:000079-01€)

mg/Kg With reference to US EPA 5021 method.Analysis was performed by cc/lrs.

n.o.

HCFCs(Hydrochlorofl uorocalbons)HCFC-21 (CAS No.i 000075.43-4)mg/kg With referenc€ to US EPA 5021 method.

Analysis r€s performed by GC/l!lS.n.d.

HCFC-22 (CAS No.: 000075.45€) mg/Kg With reference to US EPA 5021 method.Analysis wEs performed by cC/[iS.

n.o.

HCFC-31 (CAS No.: 000593-70-4)mg/Kg With referenc€ to US EPA 5021 method.Anelysis was performed by cC/[rS.

n.o.

HCFC-121 (CAS No.: 000354-14-3)

mg/Kg With reference to US EPA 502'1 method.Analysis ,,vas perform€d by cC/lIS.

n.o.

HCFC-'122 (CAS No.: 000354-2'1-2)

mgkg With referenc€ to US EPA 5021 method.Analysis was performed by GC/MS.

n-d.

HCFCI23 (CAS No.: 000306-8$2)

mgKg With reference to US EPA 5021 method.Analysas w€s performed by GC/MS.

n.d.

bF) ra*d ths bn @d €ind be @{ r l i r . t : i ! , l r i q i t i l r , . a r t , . i . r i - r i r 1 r . 1 r t l l

s6Fd b b Goio€l coid't'on3 ol s*

ciec6 h cm@ny s 6tu ^6 a $e he or b ibdsl oidry ddwhn turmb dcrsncffrd

bacp.oduddspl'niu|triMplol

Test Report No. : CEJ2011121727 Dale : 2011/02n2 Page : 10 of 23CERAMTEC GMBH

tlllttf]lrttl|l

Test ltem (s): Unit Method rNDL

1

R€ultLimitNo.1

0)rzq tuAD No.: u02u37_E9- mg/Kg With reference to US Efi-SdliTEifid.

Analysis was oerformed bv .:crusn.d.

Hcrc-r at lcnSNol-663EEl2El4)

mg/(g vytrfl rererence rc ulj Et,A 5021 method.Analysis $/Es Derformed bv cc/Ms

1 n.d.

HcFc-132b (cAS Noj oolE6:6E:7)

mg/kg vvtrn rererence ro u5 EpA 502.1 method.Analysis w€s Derformed bv cC/Ms

'I n.d.

HcFc-l 3sa (Cns NolhidTffi7')

mg/kg vvnn fercr€nce to us EpA 5021 method.Analysis w€s performed bv GC/MS

1 n.d.

HcFc-141b (cAs Norlo17i7fr:6)

mg/Kg vym rererence lo us tpA 502.1 method.Analysis was perfomed bv cc/Ms

n.d.

HcFc-142b (cAs Noja00o75$:3)

mg/kg YYM rErerence rc uu EpA 5021 method.Analysis \'!€s performed bv GC/MS

n.d.

HCFC-221 (CAS No. : -00+22-7d-4)

mg/kg wrln rererence to us EpA 5021 method.Analysis ! ras pedormed bv GC/MS.

n.0.

HcFc-222 (c^s Noj-ooa2Z]5l1 )

mdks w|In rererence to us EPA 5021 method.Analysie ,,i€s performed by GC/MS.

1 n,d.

HGFC-223 (CAS No.j 000422-526)

mg/kg w|In rererence to us EpA 5021 method_Analysis wEs perfomed by GC/MS.

1 n.d.

HCFC-224 (CAS tto.: 0OO+Zz++8)

mg/Kg With reterence to us EpA S62lEEiidAnalysis v/a6 perfomed bv GC/MS.

1 n.d.

HCFC-22sca (CAS Noj Oodtt564)

mg/kS wm rererence to US EpA 5021 method.Analysis was performed by GC/MS.

I n.o,

nvru-zrcco (uAs No.t uoo507-5s-1)

mg/xg With reference to US EpA 502ii6if,6d-Analysis w6s performed by GC/[r|S.

1 n.d.

HCFC-226 (CAS No.: OO0a3n-AZ8)

mg/Kg wm rererence to US EpA 5021 method.Analysis was perfomed by GC/MS.

1 n.d.

HCFC-231 (CAS No.: 0OO42r++3)

mSikS With ref€rence to US EpA 5021 method.Analysis wEs performed by cc/t!ts.

'I n.d.

Frur-u-2JZ ((;AS No.: 00046G8$ mg/kg With reference to US EFA-SE2lGetrod-Analysis was performed by GC/MS.

1 n.d.

Fi(,FU-ZJJ (UAs NO,: 00712t84_0)

mg(g With reference to USEFAEd2TEEIh-6E.Analysis wEs performed by GC/|\4S.

n.d.

HCFC-23 (CAS No.: 000425-94- mg/kg With reference to US EpA 5O2i methodAnalysis was performed by GC/MS.

n.d.

4l:;ilil*'l'11* 1*',".?lt |Tr::trq"'1:ijIrifl:i.t,r'r:d,lf :il"F^*-'b"p-f :"J";:,"'-';tr"'l IlAf "J :""11: :.'"';i.::"""';t : "'[ti*#*iH;.;,:lj:l:*s:.^,rsl*$$i:ti:ffi:-&sjF,,;,ffifl,trff::;**.,H.TrAfi:t;ff{:jr,tr#r1fl"",:,,r*1,}mfs;tr5:"J;"tu;u1try:R::*1Ttr:##ffi#ffid,"8#*firuilrffis#frtrfjltrinffi"iff"HrffiT.::1r"r#l

Test Report No. I CE|2O11l217TI Date:2O11t0iJ22P a g e : t l o f 2 3

CERA[.l!TEC GMBHllr [ttl|fittttft

Tost ltom (s): unit Irrethod MDL RosultLimitNo.1HCFC-235 (CAS No.:-0G60€-

4)mgKg with reference to USEpA sm1;Efr&

Analysis ,,vas performed by GC/MS.n.o.

HCFC-241 (CAS No.: 00066&223)

mgks wln rererence to US EpA 5021 method.Analysis rr/as performed by GC/MS.

1 n.d.

HCFC-242 (CAS No.:-0046G6- mg/kg Wilh reference to US EpATdZiEEifr6SlAnalysis wEs performed by GC/IMS.

'I n.d.

HCFC-243 (CAS No.: 00M60-G9. mg/Kg w|m ercrence to US EpA 5021 method.qnalysis we6 pertomed by GC/MS.

I n.d.

mdkg With reference to US EpA Sd2l6Ehod-Analysis wes performed by GC/MS.

I n,d.

HCFC-251 (CAS No.: 000421<!0)

mg/r(g Wrlh referenco to US EpA 5021 methodAnaly6is wEs perfomed by GC/[IS.

1 n-d.

HCFC-252 (CAS No.: 000819-0G1 )

mg/Kg With reference to US EpA SbIlGEiEd.Analysis was pertomed by GC/MS.

1 n.d.

HoFC-2$ lCns No.: bootoo-d mgikg With reference to US EpA 5mt methodAnalysis ,.vas p€rformed by GC/MS.

1 n.d.

nvru-zo | (uAtj No,: uuu420L97-3)

mg/kg With reference to USEFAT62ITdE6E.Analysis wEs performed by GC/MS.

1 n.d-

HCFC-262 (CAS No.: 00M21-OZ03)

mg/Kg With reference to US EpA SOZlEEf,di.-Analysis was performed by GC/MS.

n.d.

HCFC-271 (CAS No.: O()043G5S-7')

mg/kg With reference to US EPA S02 1 methodqnarysi6 wE6 performed by GC/MS.

n.d.

Noto :1. mg/kg = ppm ; 0.1wt% = 100oppm2. n.d. = Not Detected3. [rDL = lrothod Deteclion Limit4 . " - "=No tRegu la ted5. * = Quatitative anatysis (No Unit)6. Negative = und€tectabtc / Positive = Detectabte7. Asbestos : Negative = "< 1.0 7o,,, po€itive = "> 1_O %'

l : i l i , i l i i r $ r r i L r r l ; i r { r i . , : i t r j _ i . r i i ; : l

oe,mor a.**iom-l_'o;;ffi;';;;;l#;*",.,"! mHo" ",,"b,,y.I sd*d,b, dm, o^ 6nBrcd h-ffi €d! re compa;,3;*.,s r ne,ne d BnEtosrdm ' ay ri* corum,3 $s csFBbhy," b,6c,*, _d h,. a*;;;i;*;;;";;i;;;i;;;. G"*"r* i_..*.".",,

Test ReportCERAMTEC GMBH

PFOS Reference Information : Dir€ctive Am6/l2ZEC(1) May not be plac€d on the market or used as a substiance of constituent of preparations in € concentration equal to orhigherthan 0.005 % by mass.(2) May not be placed on the maftet in s€mi-finish€d products or adicles, or parts thereof, if the concentration of PFOSis equalto or higherthan 0.1 % by mass carcurated with reference to the mass of strucru€Iy or mlcrc€tructurallydistinct pads that contain PFos or, for textiles orother coated materials, ifthe amount of pFos is equalto or hlgherthan 1pg/m2 of the coated material.

e(s) €led rh s €d €pr. eid e €r!-n r . rl,i,l:.-:lj1!,rr::Fa :ts.,1.r 1-r:.-a r i- ; i Jf r3.irl:

mt 'id tr'h i rhe rn b d c| enrs Nid

No. I CEl2O11l21n7 Oate: 2011102n2 Page : 12 of 23

rl][tIt llttIt!

Test Report No.: CEn011/21n7Oa1.e :2011102122Page : 13 of 23cERAt\rTEC GMBH |l rl][ttlr

'1) These samptes were dissolved totally by pre-conditioning method according to betow flow chart.I ur lest method exctuded )2) Name ofthe person who mado me€surement Climbgreatyang3) Name of the person in charge of measurement: Troy Chang

ICP.AES

Sample Matedal Digestion Acjd

Seel, copper, aluminum, solder Aqua regia, HNO3, HCI, HF, HrO,

Glass HNO3/HF

Gold, platinum, palladium, ceramic Aqua regiaSilver HNO3

Plastic H,SO1, HrOr, HNO3, HCI

Others Any acid to total digestion

nm rhsred €pon6raronybh.3.m9 du*d ere$ntqr kbolrpno,wntrenFmsmordarr-nr- 'etir.tr;4,!!.Bqi ,,;[t!-f ,.!ri] Tt _ T i,1,ri'\,:.

y sub jdbbGs i sdco id l omdsd

b..ndrbadobrsro$un6r6ar6 oeGprdud 3spr nidr ffiodpnor

Sample Measurement

Acid digestion by suit€bte aciddepended on differenl samolemateri€l (a6 below tabte)

Micrcwav€ digestion with

HNO3/HCyHFAdd appropdate smount ofdigestion reagent

Heat lo appropriate

temperature to exlElct

Cool, filt€r digest€te

through filter1) Alkal iFusion2) HClto dissolve

measure the absorbance

at 540 nm by UV-VIS

Mem&,dm€sdsd @p{ r . ! s l

Test Report No. I CEJ2O11U7T7 D*e 2011t02122 page:14ot 29CERAfuITEC GIVBH

Chlorinated Flame retardant anal!|tical flow chart'1) Name oflhe person who made measurement BaryTseng2) Name of the person in charge of measuemenl: Troy Changr Reierence method: US EpAO27OD, US EpA3S4Or Te6l ltems: PCBS, pCNs, pCTs, Mirex, Cp, MCCP

Data

[lr]fltf,t Iltttt!

ersl lesed rh s €s €@n eid e rc

Ths darud 3 suedbylfu cmFryrdddoi. ronar dureds suqd me hn Afti'tr 3 dhrd 'o s€ | m blon or abrt

udo i3 l 5dysecoPsys !d .G+

Test Report No.: CEn011n1T77Date | 2O11102122Page : 15 of 23

CERA['TEC GMBH tl||i tItl||ttll|]

Analysis flow chart for determination of pVC in material1) Name of the person who made measurement Eva Chao2) Name ofthe person in chsrge ofmeasurement Shinjyh Chen

b€kMa imareu f f i b suqd me hm A tun rd6d ravn ro i e rnb l so r ab r9

oiib ! 3ro rc 6m'idsstumn

sample pr+treatment

Sample anel]|zed by FTIR

Check wave-number of C-Clbonding

Test Report No.: CH2O11121777OaL:201110222 P a g e : 1 6 o f 2 3

CERAMTEC GMBH [t|| l|lttl[rtltll

Analytical flow chart ofSoxhlet extraction (LC/MS) procedure'1) Name ofthe person who made measurem€nt: Lydia Fu

2) Name of the person in charge of measur€ment: Shinjyh Chen

lTest ltems: PFOS/PFOA . Benzotriazole

Sample pretreatm€nuseparation

I

Data

eis)'.dd rh 3 b* cFd enid be €! : i t i r r i i t * r r ! , . J i i r + r { r d r . : i l , . , . i , . i "

, o . e M m a , o m a | d u n H b s l b , * l f u f t i l h l n A G d o ^ ' d € w i l o h e ' h i a i d o l ] a b l JLd.mniebnddllBddmcsG&

Mcnh.orse5cs6ro!p6GssAr


No. : CEl2O11n17nDale: 2011t02n2 Page : 17 of 23

Analtrtical flow chart of Soxhlet extraction (GC/MS) procedure

1) Name ofthe person who made measurement: Lydia Fu

2) Name of the person in charge of measurement: Shinjyh Chen

I Test ltems: Phthalate . Benzotriazole , HBCDD , Np . DBBT ,

Organic phosphoru6 compounds

UAEI

rt tl|l[tflttl

c a h € ! . J . , , t : . , \ ' r , ; : l r r j , i . x j r . i r : t r : P n r f i , . | t . l - \ _ F h : ' r . r l r F i j t

m | y a n d { ' b n | h e | f , c d c l e n | s f t ts n m e D b € l d $ e c o m @ ^ ! A n , B u i o E d a b E b i

rorgory or ra s.aDi or rhe odem or a

d s f u z o t u N r i L F . , q L d r i . . . i : - i ) , ; t t .

Mcnbd df he scs 6dup lsr sAl

Test Report No.: CE12011/21n7 DaIe | 2Oi1tOZ22 Page : 18 of 23CERAMTEC G[IBH

llt| [tlt]flttlttl

r )2)

Analytical flow chart of Organic-Tin contentName of the person who made measurement cinny ChenName of the person in charge of measurement: T.oy Chang

Data

i n h s ' . d l 6 p o d e l o d y b l & s . n p li n L . ! . , ! l ; 1 i 1 1 , { ! L n r i r " * a ; i a { l i : s r : . . I ; . j r i . [ ] l

ysgtdbbG6i66 chdlomd ss6r edmc tomardclmd:. elqer anedhm Aratuoi sdl:MbhetmdonorLabr!.

i d 4 r , u o i q N r ! L F i . 1 , L 4 e ] i i 1 . , ] i I

Test Report No. : CED011|21V7 Dz,!e : 2OiitOZ22 Page : tg of 23CERA['TEC GMBH

Analytical flow chart of hatogen contant1) Name of lhe person who made mea6urement Rita Chen2) Name of lhe person in charge of measurement: Troy Chang

r|||||ttflflnrlt

Sample pretreatment / Separation

Weighting and putting sampte in ce

Oxygen Eomb Combustion / Absorption

Dilution to fixed volume

Analysis was performed by lC

@dld.e|epl]^ ico rpa ry : r , , , i r ' ; : r : : . r : , r i r r 4 ! r , ! i r n ; : : r x r i , { ! r " . r i , t . , ! : l

ro. eM'mn rond d€unbb suter turun,hh Abd; r d.wn ro be ,mrar m or rab lry

Test Report No. : CEt2011t21T?7 Date : 2011to2t22Page : 20 ol 23CERAMTEC GMBH

;$l[!tt][fltttt

Analysis flow chart for determination of Asbestos1) Name of the person who made measurement Victor Kao2) Name of the person in charge of measurement Wendy Wd

Not containing Asb6tos/Negative

,n 0i6hn. ,omd d&n'b sq< o-,.* a **.a".,,a""iiirii;;;iffi;ffi;';ira"^ b ,i" i,b!." o, ab,ry

*ru" "er.*rd

ri" c".ery *y,*".-,*. r.a *"aoroae",ryreirceu*oiri6o "an""iln"

ii ''' ,

XRD Qualitative analysis by X-ray diflactionmethod

Diff.action peak ofasbestos is absent

Asbestos ldentification byoptical miqoscopy

Test Report No. : CEqU1P1777 Date : 2O11\OZ22Page:21 ol 23CERAMTEC GMBH Irl][ll [tl[ttl

1 )

2')

Analt{ical ftow chartName of the person who made measurementj Roman WonoName ofthe person in charge of measuranent Troy Changf

r Test ltems: PBEI/PBDE, TBBp-A-bisFirsl lesting process -----f Optionatscrcen process -.._. Confirmation orocess _ .>

Screen analysisr@t

lssue Report

lll.iff,#i?;,jll1*:Hi;:.:11jg1fl:"r"9T..jlTiJ::1::T.d*;;"'ir;;;:;;;;t;Hffiilfi",i,,,i',:.]tiilt'il_ii"',fri"'il,ir"iilfl]iill::#:H jl:s::fl,:ll*:i:*itr j":l*-t:?:*r::g:yltq:i,;;c,;;fi;;;:;:;;-":i;;;i$:t:i;,,,.""**,_..*_""s",;il;^{i,11_?l*":";;tf;*^..;:.T-"1..1t:I1e_:r:r;;;;:;.--';;;."'".-f:".",fi;,"..":;:i;.;,:li::.:ff1T;.;;

I Sampte extracion metnoA __l

V

I Concentrate/Dilde Extracted sotution I!'

I Firter -l

+I Anaty6is by cciMs

]V

: " " " " " " " " " r " " " ' . . . . . . . - - - r

Test Report No. I CED011l21n7 Dale: 2011tO?,22Page : 22 of 23

CERAMTEC GI\4BH rl|u l||at [t

Analytical flow chart of volatile organic compounds (VOCS)

1) Reference method : US EPA 50212) Name of the person who made measurement : Dalkiyen3) Name of the pe6on in charge of measurement : Shinjyh Chen

Sample pretreatrnent

Take sample and put it intoheadspace glas6ware,


No. : CE12O11121777Oale .201110?,22Page.23 ot 23

rllfl||t||[ttttt!

'* End of Report "

y s u b j d b b G s m d c o f u d o m d s e

be.epdu€de€pllfu!whodpnq

2L777

TeSt Report No.: GZt 1o6o8jgt5/cHEM oate:JUN24,2o1tXIAMEN LICHUN ELECTRONIC ELEI!,IENT CO., LTD42.2 XINGLIN WEST RD,361002 JIMEI DISTRICT, XIAIV]EN FUJIAN. P,R.C

Page 1 ol 4

..4 f*..st hLlcrrr.rtra!|'.|ffcts-..!**htr'.

The following sample(s) wavwere submitted and identitied on behaff ofthe applic€nt as soDA Lrt4E GLAss ruBE

SGS Job No.SGS Internal Referenco No.Clienl Rererence In{ormationDate ol Sample ReceivedTesting Pedod

Test Requesled

Test l\,lethod

xM13205987EC

3.6.4.6,5.2.6.3.10.3JUN 23 ,2011JUN 23,201t TO JIJN 24,2011

Selected tesl (s) as req.iested by client.

Please refer to nexl page(s).

Please rofer lo next page(s).

Based on lhe performed lests on submitted sampte(s), the results comptywllh the RoHS Directive 200Z9'EC and its subsequenl amendments.

Tesl Rosull(s)

Conclusion

Signed lor and on behalf ofSGS-CSTC Ltd.

rdta..dlt'd'.rl|..d!ft..3r6.tr.P.r.dl-rli.hrd. .r|rrx..'. Hrrni|'.i'tr.r'.rr|.lrt|.*i , n**q,n s"..!.116r.....nr.hdl *.rrr.s.d criG!*

Approved Signatory

r|||t.roafi. scs tl'.ta lscll S^l

Test Report No.: GZl 10608131s/CHE[,{ Date: JUN 24, 2011 Page 2 ol 4Test Rosults:Description for specimen 1 : Transparent glass tube

RoHS Direc{w 2002/9tEc

Test ltem(s)

Cadmium (Cd)Lead (Pb)lrercury (Hg)Hexavalent Chromjum {CrVl) bvalkaline extractionSum of PBBSMonobromobiphenylDibromobiphenylTribromobiphenylTelrabromobiphenylPentabromobiphenylHexabromobiph€nyiHeptabromobiphenytOclabromobiphenylNonabromobiphenylDecabromobiphenylSum of PBDESMonobromodiphenyl etherDibromodiphenyl etherTdbromodjphenyl etherTetrabromodiphenyl etherPenlabromodiphenyl etherHexabromodiphonyl etherHeptabromodiphonyl elherOctabromodiphenyl gtherNonabromodiphsnyl etherDecabromodiphenyl ether

Note:1. mg/kg = ppm2. N.D. = Not Detected (< [,tDL)3. I\,DL = Method Detection Limil4. "-" = Not regulated

Test Method (Ref erence)

iEC 62321: 2008, ICP-OESIEC 62321: 2008, lCp-OESIEC 62321: 2008, ICP-OES

IEC 62321:2008, UV-Vis

IEC 62321: 2008, GC-MSIEC 62321r 2008, GC-MSIEC 62321:2008, GC-MSIEC 62321: 2008, GC-[,|SIEC 62321:2008, GC-MSIEC 62321: 2008, GC,MSIEC 62321: 2008, GC-MSIEC 62321i 2008, cC-[rSIEC 62321: 2008, GC-ltlSIEC 62321:2008, GC-MS

IEC 62321: 2008, GC-MSIEC 62321: 2008, GC-MSIEC 62321: 2008, GC-MSIEC 62321:2008, GC-IISIEC 62321:2008, co-t SIEC 62321:2008, GC-t SIEC 62321:2008, GC-MSIEC 62321:2008, GC-MSIEC 62321:2tr08, GC-MSIEC 62321: 2008, GC,MS

Unit

mgKgm9Kgmg/kgmgikS

mg/KgmgKgmS/kSmg/xgng&gmgKgmdksm9KgmeyxgmgikgMEKgmgKgmgKgMEK9m9KgMEKgmg/kgmg/kgmg/kgmg/Kgmg/KgmgKg

Result

N.D.203N.D.

N.D.

N.D.N.D,N . D ,N.D.N.D.N.D.N.D,N,D.N,D.N-D.N.D.N.D,N.D,N.D.N.D.N,D.N.D.N.D.N.D.N.D.N.D.N.D,

[rOL Limit2 1002 10002 t0002 1000- 10005555

55555- 10005555555

5

is itsr|ill|lecllnry*.-'* affiIt.r .l|ll*tt8t+a*itri!11 lt.tc

.d!iq!!4rd.n'|ir..-K..rhriEr

' d*-t a*uli. ,G tb aFrt r* m5$b[-rdcr-r r-{.r4, ,4 rboq{. rr.s.rrrt bb.crd-a*:|t -.t!! r_a'r ..!.t -.!'rq-Iffi!-4..'M@ rr.r '.h.r.t olr.r.a.lr'|a..*rrn||$+-Ea.e'rL14r.brFc4Fkr.trcls.n

tP.{|rE!a l|.l!|le nr ..ll4r6dr&E.tdiirF,*

r.|rO.rollE aOSOrqF laoAg )

Test Report No.: GZl 10608131s/CHEMDate: JUN 24, 2011 Page 3 of 4

ATTACHMENTSRoHSTesting Ftow Chart

1) Name of the p€rson who made testing: Belta Wang / Cutey yu / Ross Zhan2) Name of the p€rcon in charge of testing: Adams y! / Ryan yang3) These samples were dissolved lolally by pre-condjtioning method according to below flow chart

(Cr6+ and PBBS/PBoES tesi method exctudec

Acid digestion withmicrowave/ hotplate

ConcenlratiorVDilution of extraction

solution

l) Alkali Fusion /DryAshing

2) Acid todissolve

Filfation andpH adjustment

Adding l ,sdiphonylc€rbazide

developmentAdding 1,$diphenylcarbazidefor colordevelopment indicales the

presence of cfo.. lfnecessary, conitm

Pb/Cd/Hg PBBS/PBDES

Negative

rr-{'ddErrtfr-

lb'.r-rrr-at!a.o.rrrt

r.tit aqadrrrr.l. tuF.4F d.lrCrQ.{.

Test Report No.: G21106081315/CHEMDate:JUN 24,201i page 4 of 4

Sample photo

SGS authenticate the photo on oiginat repon only

"' End of Repoi "'

rrta',....qt4{. tuFh.4Fr.t.td cri.4.

,r0aa3 t F{4lllt5l5 l xe{!6115 nr6ss

rnolrol !F aoa olb|' l8oaaA)

scsI

Test ReportPOLYFIL AGOBERALLMENDSTMSSE 2OA,

was/w6re submitted and identified by/on behalfofthe client as:

Validit nownForQueStiPlease Co ith scs

No. : CE/2011/84950 D e | 2011112101

CH€3OO ZUG / SWITZERLAND

Cu99.9MSn'1'14595

2011t1lt25201 1t11/25 rO 201I |1',01

Page: 1 or 7

rr|| [ltt!|||tlt[t

The following sample(s)

S€mple DescriptionBuyer/Order No.Sample Receiving DateTesting Period

lest Result(a) Plea6eefer to next page(s).

prqt iadsd Ds Gn ,epd eind bComFiy -r ,: !;t lLr. . . i ; l :r l i l l{ i l rt lrd r qti ' r^rl l i9i: l+,11\- em+,i , -,:r. ift",rl.

.ysuq8d b b cs€rcond rbns d ssubrd lo Tems ad cd@ l.l:

o n L y a i d w l h L n h . t m B d c | € d l n !

E d ftr|tld

clsnH L.Do'|b.t - Trhd

Test ReportPOLYFILAGOBERALLI\4ENDSTRASSE

T66i R.6ultls)

PART t.lAME No.1

No.: CE/2011/84950 Dale :2O114ZO1

2OA, CH63OO ZUG / SWITZERLAND

Page'.2 of 7

t I] t l

SILVER COLORED METAL WIRE (INCLUDING THE PLATING LAYER)

Te3t lt6m(s) Unit Method MDLR.3ultNo,l

Cadmium (Cd) mg/KgWith reterence to IEC 62321r 2008 andperfomed by ICP-AES.

n.d.Lead (Pb) mgKg 24Mercury (Hg) mS/kS n.d.Hexavalent Chromium Cr(Vl) With reference to IEC 62321: 2008 and

pedormed by Boiling \r€ter ext€ctionMethod.#

Negative

Sum of PBBS

mgikS With reference to IEC 62321: 2008 andperfomed by GC/MS.

n.d.Monobromobiphenyl 5 n.d.Dibromobiphenyl 5 n.d.Tribromobiphenyl 5 n.d.Tetrabromobiphenyl 5 n.o.Pontabromobiphenyl n.d,Hexabrcmobiphenyl 5 n.o.Heptabromobiphenyl n.d.Octabromobiphenyl 5 n.d.Nonabrornobiphenyl 5 n.d.Dec€bromobiphenyl 5 n .d .Sum of PBOEa n.d.Monobromodiphenyl ether n.d.Dibromodiphenyl ether 5 n.o.Tribromodipheny! ethe. 5 n.d.Tetrabromodiphenyl ether n.d.Pentabromodiphenyl ether n.d.Hexabrcmodiohenvl ether 5 n.d.Heptabromodiphenyl ether 5 n.o,Octabromodiphenyl ether n.o,Nonabromodiphenyl ether 5 n.d.Decabromodiphenyl ether 5 n.d.

eGlG{d rh s ied @d €nrclb Bpdcn€ry 'l+ !r ! rlrl . .n 1!ts,:r1,rtilr. ;l'!l* rrn . imri+Al'r-\r jrl4.f4! 1r€11hsdocmdssdby'h€c.mpany&bldlobcffi6|codibGo's*to. e.d'mc romal dmstu suq

d ^ t ' n d w l h L n h r m B d c r . d ! n d p o B d r t s t o G c s r a n d r h 3 d Mldrrgh6add]Ed'on6un6lh6'm

t',i!r: :d, dri:_ 11rs6rorPre

Test Report No. : CE/2011/84950 Date | 2011h21O1 Page: 3 of 7

tl]tIlltltfltttltPOLYFILAGOBERALLMENDSTRASSE 2OA, CH€3OO ZUG / SWITZERLAND

Test ltem(s) Unit method MDLResultNo.1

HalogenHalogen-Fluorine (F)(CAS No.: 14762-94-8)

mg/Kg With reference to BS EN M5A2,2007.Analysis was perfomed by lC.

50 n,o,

HalogenChlodne (Cl)(CAS No.: 22537-1s1)

50 n.d.

Halogen-Brcmine (Br)(CAS No.r 10097-32-2)

50 n.d.

Halogen-lodine (l)(CAS No.i 14362-44-8)

50 n.d.

Note :1. mg/kg = ppm : 0.1wf/6 = 1o00ppm2. n.d. = Not Detected3. MDL = Method Detection Limit4 - " - "=No tRegu la led5. '" = Qualitative analysis (No unit)6. # = a. Positive means the presence of CrVl on the tested areas

b. Negative mgans the absence of C l on the tested areasThe dgteci€d concentration in boiling-lvater-ext€ction solution is equalor greaterthan 0.02 mg/kg with 50 cm,tested areas.

7. The sample(€) was/wer6 analyzed on behalfof the applicant as mixing sample in one testing. The above result(s)was^^/€re only giv€n as the informality value.

'nrhstar€Fnd€f ontrorbsmpq3)Idd rhEbd,etsn6ndbGComFny f l t r , l r i 9 ! r . , r l i ] l : r r ! l { : : l : : ; l i ' ! i : l j i A r i i F -5 ! , [ 1 ' e t r ; ' f ' , , ' l ] l t ) [ l i 1 'n3dumd ts6su6d ' l hscomtsny5u*db t csccond1 t r sds

sib iv 6 10 6 o er 5d b6 @mntft,ltrrsandd odd3undrth€ta mol & €pdud depr 'n ju r, ftd

+l r l *J l : r (+s610r ) re t7e f +sitlfuirL!{:,r rr ir: i - i.hsror

IlF

Test Report No. : CE201'1/84950 OaL .2011h2,01 Pager 4

according to belo\ / flo /

POLYFILAGOBERALLMENDSTRASSE 2OA, CH63OO ZUG / SWITZERLAND

1) These sample6were da66olved totally by pre-conditioning methoda Cf' test method excluded )

Name of the pe6on who made measurement: Climbg€at YangName ofthe pe6on in charge of measurement: Troy Chang3)

ICP-AES

Sample Material Dige€tion Acid

S1eel, copper, aluminum, sold€r Aqua regia, HNO3, HCl, HF, HrO,

Glass HNO3/HF

cold, platinum, palladium, ceramic Aqua regia

Silver HNO3

Plastic H2SO1, HrOr, HNq, HCI

Othe.s Any acid to totral digestion

ii. irei,.or if *q oy t . cop-r " ,g .oo-maa"J ' * .6b i " - ' *dco^d ' * "6 .Edrcn ico@isbdM!os@]bi.*ddb" -'d l,nsdd 6 *,* i5r

*l iq:i";* @"* -;d.." **o.ooissr,s.ry - r"

"rd;^ a * -nd .

rtf:r:: r1lirtii+ 1l i s6 io,t,e tTe t r s lo:)2e 'r7 ffiar(om

Acid digestion by suitable aciddepended on difierent samplemderial (as belo\ , iable)

Micro\rave digestion with

HNO/HCVHF

Heat to appropriat€

temperature to e,\tract

Cool, filter digestate

through filter1) Alkal iFusion2) HCltodissolve

at 540 nm by UV-VIS

Test ReportPOLYFILAGOBERALLI\4ENDSTRASSE 2OA,

No. : CE2011184950 Oale'. 201 lh2lo1

CH43OO ZUG / SWITZERLAND

Page: 5 of 7

t l | l [ ] | | I t t | l

PBB/PBDE1) lllanE of the person2) MnE of the person

analytical FLOW cHARTwho nEde npasurenEnt: Ronran Wongin charge of nEasurenent Troy Chang

Scrcen analysis

" " " " " 1 " " " " " "

Sanple extraction/So*rlet rEthod

ConcentratdDiluteE)dracbd solution

First testing process -----t

Optional screen process -.--

Confinmtion process - .>

-s."pb---_-]--------r-------[S-r-tp]-j-a"arn"-_l-----r----

Ft ler

Analysis by GC/liS

cm€ry r r ' r j l j r ) t r . : r i l i " . : . l ! i * i , ; i i l ' r l t : e l . t i l : i l r t / . 1 \ ' l r Fn . r ' j : 1 . ' t l 6+

to €sd'o'c ramd dm6tu suq

d^t ,nd vihin rb rmis ot cr€d s i3'lbr.ohbadd€donsu.ddsera od b. repdued eiceol itul wiher

! idsnrzorNe-tu!acirrrer/*l:r/f,!.r +!!4J1i:irlre 02)r!e

I

Test ReportPOLYFIL AGOBERALLMENDSTRASSE

No. : CE/2011/84950 Daie | 2011h21O1

2OA. CH-6300 ZUG / SWITZERLAND

Analytical flow chart of halogen content

1) Name of the p€rson who lmde rneasuredEntr Rita Chen2) llan€ of the person in charge of nEasurerEdt: Troy Chang

Page: 6 of 7

comoad N]r]F,j!:ir.. I tiir lt{!l; ;]]rltl.1!- . r. irtsih-{} I 11 FiT . f!l r19i!+l

fi"JHl"l;liiii',i!',i.iwi;c"ry"';ti"-"c*""tc"t.^a sriu*-t i*n d..",; ''jbl.n bi... .d c.d*" 6, €. a " ' ' i i a - - o e , " a a . ^ * * ' ; . n b a d " i s d l b d i b m a i o ; d k . d h ;

; ; ; q ; ; ; ; oo ,4a t ; . : 6 . ? .€6@- -hsd ; "db . - "b1 .

r L - I I i d l L a i

Sarple pretreatrnent / Separation

Weighting and putting safipte in cell

Orygen Bomb Cofibustion / Absorption

Dilution to fixed volurne

Analysisw€s perfornEd by lC

Test Report No. : CE/2011/84950 D€te 2011h2101 Paget 7 of 7

tl] tlt II][]lPOLYFILAGOBEMLLMENDSTRASSE 2OA, CH63OO ZUG / SWITZERLAND

* The teeted sample / pa is maaked by an arrow if ifs shown on ih€ pholo. '

" End of Report -

€(s) r6rd Th€ r6d rop.n @nd b rccomtsry rirl,,iirar.rr'ir,'r,:111!!1, iilrRj:itr r.il1' l:!11.!-em+iI, ra r';)n:ll 'Thsih{.d"**dbylh6c"np.nysub'db6G4€Ejcond1bngo{sld ,M6.6al &dmsfu' sub]rendir,e'@ d ru d dbn s€s ibrh€! n reieds rhe cmp8.r's t ndn$ 3r rhe-y .d fu " t h " i . 6dc " " c ' * dDc . {5ny r ' j e cdnF i ys9s . s$;nshisandobroa,o3@do,rbta mdsrepd@sxepr'nlu.wM,sio,MtenaFro!3 drhecompanv a

Validit nownFor QuegllPlea€e Co ith scs

,Fl|s,#+Test ReportELSCHI'{Oi' ELEKTROSChUTZ(OVPONEMENBAU CVBHGEI'ERBESTMSSE 87, D-98669 VEILSMRF. GERVANT

trTi{*&efi*8P 't*, -a ts *P +*:t a*l},r *rs+Ti de t r t i f i€d by lo ! !eb . l f o f the c l ienr as) :

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& S 3 + * ( s . . p l . D e s c r i p t i o . )11"9"4f i (sryl€/ I tem No. ),FA El (corntry of o. is in){ i?t A lq (sanp I e Receivins Date):Il:{,Jk lE1(resr i ir Pe'i od)

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2 0 1 2 / t / 1

2 0 L 2 / I / 4 T O 2 0 1 2 / 0 I / I I

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O!-rLd bDo.rtlft -TdDd

c o m q i l t : , . 1 i r , l ' - i ' i , . r - : l f , i j ' i r . I l i l r l : r . ' r ' i , ! : '[email protected]€rcddrdi3orse'epin€doleder,,v' 'bdeoi.eq

p o j b ' I } c l o c c | e d a . d h s d d J n

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(NW4D

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,F{'d,#+Test Report

i t IS(N6. ) : cE/2012l10834

ELSCIIU(OTI ELEKMOSCiIUTZKO}TIONENTBNMU GMBHGESSRBESTRASSE 87, D 98669 \'EIISMRF, CERN,{IY

idLg*(Test Re.u l ts l

;FJiT4,'i (PART NANE) NO.1 :

q s ( D a L e ) : u o l 2 l o t / t l n * ( p a 8 e ) : 2 o I r 0

llfllflNl[lttutl

'e,).1ift6fr?,+n& (e4t,?) (*14*t) (Mr)GD ALL @LoR t!tE-rA! lvrRE( INCLIJDING THE PLATING LAYM) (1! TPES) )

comranY r i I i l r r ' l r ' i i , . ' i r l ; l n i i :r y sub ]d l o6cene6cdd | t o^3ds

r r ,u : . i t : r r i rJ r , , r . s6Lo?r rq

jrl ttt E +&(Uni t )

,{fi,rx t;i.ttrlEIE{T(mL)

,*1f,(Resq l t )

N o . 1tA / cadmiun (cd) ++IEc 62321t 2008rt1, ,r(&Alt

A€*4+**f tE;*d,i*,r|. / nitr'.e fe rence ro IEC 62321: 2008 a idper fo rned by ICP-A 'S.

tE / r.ad (Pb) ++rFE 62321,, 2oo8tti, /64*A€*,.f +*+lrt r*A*,!i. / wirh.e fe r€nce ro IEC 6?321: 2008 andperforn€d by ICP-AXS.

68

* . / vercury (Hs) t-+rFN 623211 2008t:1, ,xdA**A€t.6+*4trb*Al*,r,. / lvi thre f€ renc€ ro IEC 62321: 2008 andperforn€d by ICP AXS.

n1!r$ / Hexaralent chro6iun cr(v l ) t-trFr 62321: 2oo$rit , ,]lih'K+* .* l * ; r l . / i r i rh ie f erence to tEc62321, 200A and per forned byB o i t i n s ' a i € r € x t r a c t i o n l t e t h o d . #

An+B,*& / Per f l uo!ooctanesul fonates (PFOS-ACid, veta l sa l r ,

4+us EPA 3510c, 1996rii, ,(rirE,?ff l(+dis;r'lafi.+Edda*./ S i t ! re fe rence io US EPA 3540C:1996 ne thod lo r PFOS Co! renr ,Ana lys is vas pe . fo .ned by tC lMS.

l 0

an+6(r4) / PFoA (cAs No.: 335-6?-1 )

4+us EPA 3b1oc, r996til, ,x,t€,? { f, rt&l*,fl }n+d.(r*) 6t/ r / i th refefence io us EPA 3510c1996 ncthod for PFoA content .Analys is {as pei forned 6y rc /MS.

t 0

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rfla#+Test ReportE-scllUKOIl ELE(TROSCHUTZI(oIPONENTEN&{U GItsHCEWE&BESTRASSE 87, D 98669 VEITSDoRF, GERII,AI\'Y

*4(No. ) : cE/2012l10834 a&(Date) : 20r2/or/r2 F*.(par€) : 3 of ro

ul||||al][tllml

*litit E(TeEt I tGos)

+4t(utri t )

,{etti(ucthod)

tr*,ltrltrE{t0{DL)

sjF

N o . 1t* l t**F / su! or PBE6

+41F. 62321. 2aa9t)*, ,)rfulaEfid,/f -*d,&xi. / rt / i th.ererenc€ro IEC 62321. 2008 and p€r fornedby CC/MS-

- i l# jS / Monobromohi ph€ny l

:ArS. i i / Dibronobj lh€ny L=.ill6i*. / Tr i broeobi phenytq t A # S / r e t r a b r o m o b i p h e , v Ii *S1i / P." rabromob iph.nv L, r i lSX. / Hexabronob i phehy l

+,1#X / HeDtabromobi Dhenvl, \ iA#*. / octabronohi ph€nyt

,L, {dX / Nonabronobi ph€nyl

+t tSX / Dec,b.onobi pbenvl

ttlt*r|trfr / suo of PBDEg- , *S fAd / Monobronod i pher r l e theri -_A#X6t / DibronodiDhenr l e ther:Als ' ta t / I r ibroaodiDlenvl etherq A S * a t / T e t r a b r o m o d i p h e n y L e t h e rA*#*at / Pen r abromodi ohenvl etheriA ls t ld / H€xabronod iDhenvL e ther- t 4 # E A d i H € p t a b r o d o d i p h e n y l e t h e r, \ t l t f i i i$ / octabromodiDhenvl ethern*dS&. i NonabronodiDhenvl ether

+*#tr ie / DecabrosodiDhenyl e th€.

i * / l la logeo

At (n) / Ealos€.-Fluo. in€ (F) (cAsN o . : 1 4 7 6 2 - 9 1 - 8 )

n8/k8

++Bs EN r4FB2,?!Jo7, ,/,*L+Ett&i*1. r , l i t t ' re f €rence to BS s*I 4 5 8 2 : 2 0 0 7 . A n a l y s i s s a s

5 0

&+ (S,) / Halosen-chlor ine (c l ) (cAS

No. : 22537- I5- I )5 0

6* ( ; * ) / Halogen-Brosi .e (8. ) (cAs{ o . : r 0 0 9 7 - 3 2 - 2 )

50

& * ( 4 ) / H a l o s € n - I o d i n e ( I ) ( c a s

! o . : 1 4 3 6 2 - 4 4 - 8 )5 0

nPb(s) bdad *€ ra$ Gpod enior br . , l r . , r i 1 . , . ! l 1 r r . : r , . r l r f l ! .

rh s dofumeil ts 'sued 6y $e co6p'9 u b j . c l l o ] € m s 6 i d c o i d l o n s i o r E A h e f r o n € d a w i l o h s ] m { d o n d : b l l y

! idr( d zoiq N?! riiF clr tiiwd r]i : r!rt r r! r:{i!.l,rrh}s6iorr,

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E-sCIruIOU ELB<TROSCHUTZKOIIPOIIENTINB,{U GMBHGESERBESTRASSE 87, D-98669 VEItsDoRF, GIRMANry

AA\Date) : 20r2/0r/r2 Fg.(pase) : a of 10

tI|||l||lt][trt|l!

f , l i (Note):r . n s l k 8 : P p n ; 0 . l n t % : 1 0 0 0 P P n2 . n . d . = N o r D e t e c r e d ( , f t . A * )

3. MDL = Merhod Dere.r ion Lioi t ( t* . l* tFl tsfE.t i )

4. ' - ' : Noi Res'1.r .d (**n*. i4.)

5 . . . : Q u a l i r a t i v e a n a l y s i s ( N o U n i t ) . t , E r > r 4 G R + A )6 . # : a . P o s i r i v e m e a n s r b e p r e s € n c e o f C r V I o n t h e t e s r e d a r e 2 s

( po s i r i ve i.6n,l:d, E&jA ;Fl r|l ,r.ll J} )b. Nesat ive means th€ abs€nce o f C.VI on t le tesred areas( Nega r i ve A + jr,l:i, E }{ ^.fi '4l r,j ,rllj* )

T l e d € t e c t e d c o d c e n t . a t i o n i n 6 . i r i n s _ q a r e r - e x t r a c i i o n s o l u r i o n i s e q u a L o r g r e a t e . t h a r o , o 2 o g l k g w i t hs0 csr tesred ar"a" , / i t8 i i ;AA=o.02 na/ks u i ih 50 cm? ( tested areas)

7- *tsiitrl:{€I,'A f ;6^*,tEAtslit ' lE*f tli&A)rl:t}: *.ir1ti.4 f tEfl+-+iJ{ t.l+&.(Tn€ sanp les vas /sere ana lyzed on b€na l f o f rhe app l ican l as n ix ing sanp le i . one resr ing . T le abover e s u l l s s a s / - € r e o n l y g i v € n a s r h € i n f o . n a l i r y v a l u e . )

8. ttr)*E+4c.f\2orzlor / rr ir ' t t *gcE/20t2/ tos3l&+.(This repor t s !persedes the previors dd.uDent bear ing rhe resr repor t number CE/2012l10834 vhi .h vasi s s u € d o n 2 0 1 2 l 0 1 / 1 1 . )

Plost+ f in (R. f . ' .nce InJoraa! ion) | )A+ 2006/r22/M (Dl tecr i rc 2oo6/ t22/w,(r) Ji&( 4;rfl +t4_Ld.&n r{.++**rlf d.aefl rt+€g;ia+,a*.rJi+o. oo5%.

(May no t be p laced on rhe oarke t o r used as a subs taace or cons t i tuent o f Drepara i ions in a conc€n! ra ! ionequa l to o r h igher than 0 .005 % hy hass . )

(2r r hy4rr &*fi 8!at+d.s{.ff tr"d.4b4; 1Rri+t+}3EH*.4{ pFoss49€-.r*fi}a&hii€}g4pFos6i,tA++t A,Ao. t%, fi,rt,{'sd.*{tt$*rtr, j'*.P!osAA}.{tf f 5g+,i4,*. ji'ifrug/.r.( N a y n o t b e P l a c e d o n r h € n a r k e t i n s e E i - f i n i s h e d p r o d u c t s o r a r r i c l e s , o r p a r t s r h € r e o f , i f t h e

conc€n1.a t ion o f PFOS is equa l to o f h iChe. than 0 .1 % by nass ca lcu la red v i rh r€ fe rence to the nass o I

s t r u c t u r a l l y o . m i c r o s t r u c t u r a l l y d i s t i d c i p a ! t s t h a t c o n t a i n P F O S o r , f o r t € x t i l e s o r o t l e r c o a t e d

nater ia ls , i f the a ' ioun t o f P IOS is equa l to o r I igher than 1Ug/n? o f the coated narer iaL . )

cmoanyr : f r111r ! L l l i . , r i , j . , ln l r . i i : i . t r i l i , , ! ,L l \ i . r 4 . r i r , r t r , , ! .

fil-d,+E+i t6(No.) : cEl2012l I0834 Aq(Date) , 2012/01/12 F]R(p,s") : 5 of t0

t||uI| ]||lr]|lt

Test ReportELSCI1UKOM ELEKTROSCHU']'ZKONPONENTENBAU CMBHGEIERBESTRASSE 8?, D-98669 \'EILSDORF, CETMI\Y

t lB4 l t (s iy le / I !€n No. )( A - 1 ) 1 0 1 - - 2 ? 1 . 0 - - - - t i n n e d c o p p e r w i . e - C u , S n - %( A - 2 ) 1 0 1 - - 2 8 3 . 0 - - - - t i n n e d . o p p e r c l a d w i r e - E l . o n 3 0 , S n - - %( A - 3 ) 1 0 1 - 2 7 2 . 0 - - - - t i n n e d c o p p e r c l a d w i r c - E l c o n F , S n - - %

( A - 4 ) 1 0 1 _ _ 2 8 1 . 0 - - - - t i n n e d c o p p e r c l a d w i . e - E l c o n D , s n - - %( A - 5 ) 1 0 1 - - 2 2 1 , . 0 - - - - t i n n e d c o p p e r n i c k e l a l l o y u i . e - C u N i { 4 , S n - - %( A - 6 ) 1 0 1 - - 2 4 - . O - - - - r i n n e d s i l v e r p i a t e d c o p p € r F i r e - c ! , A s - - % , s n - - %( A - ? ) l 0 l _ - 2 5 7 , 0 - - - t i n n e d b r a s s v i r e - C t 8 0 2 n 2 0 , S n - - %( A - 8 ) I 0 l - - 2 3 2 . 0 - - r i n n e d s i l v e r c o p p e r a i t o y v i r € - A s c u 5 0 , S n %( A - 9 ) 1 0 1 - - 2 3 4 . 0 - - - - t i . n € d s i l v e r c o p p e r a L L o y w i r € - A s c u g o , s n - - % ( E l c u g o , s i - % )( A - 1 0 ) 1 0 r - - 2 5 5 . - - - - t i n n e d c o p p e . z i n c a L l o y p i r e - C u 7 0 2 n 3 0 , S n - - %( A - 1 1 ) 1 0 1 - - 2 2 9 . - - - - - t i n n e d c o p p € r n i c k e l a L L o y r i r e - C ! N i 1 2 , S n - - ,

( A _ 1 2 ) 1 0 1 - - 2 3 5 . - - - - - t i n n e d s i l v € r . o p p e r a L L o y v i r e - A g 7 2 c u 2 8 , s n - - ,

( A - 1 3 ) r 0 1 - 2 3 r . - - - - - t i n n e d s i t v e r w i r e - A 8 1 0 0 0 , s n - %( A - 1 4 ) r 0 1 2 3 6 . - - - - - t i n n e d s i t v e r c o p p e r a l l o y

" i r e - A s 4 5 c u 5 5 . s n - - % ( A g c u s 5 , S n )

P]BG) bsbd rh 3 bi cPod €nnd ec m p a i y ; , . r , l l r ' r : i : , l . l j , l i l r + r . r i l l + ! r , ] ] . r 4 , L | \ i .

p o i g b ' t } 6 l o b c l € d a o d h s d g m

,Ff 'd,*E+Test Report

i tS(No. ) : cE/ 2Or2l10834

EI-SCHLXOM ELEKTROSCHUTZ.(OVPOMNTENBAU CVBIIGEFMBESTMSSE 87, D-98669 VEIT^SDORF, GEL\!AIry

a*(Date) : 2ar2/a1/L2 F*(P.8.)

|r []t fllr

43)

illi,rTdt )i.a tr ai*r+ ' tls e, tt*tt . ( ilt jtjrt i{t* ff + ) / Thes€ sampt€€ we€dissolvEd lolalt by pHonditioning method accoftting 10 betM no/r ch€rt. ( CP test m€thod excluded )ir, d^ I : lr.Ett / Name of the pe6on wio ftade m€surement ctimbs€ar yans)rlll fi I ^ : tl,l|^ / Name or the p€Bon in chaBe ol measu€ment Troy Chans

rgrt'rst*,*+*4.Jt,rlfl / ICP-AES

*.sltrf / sample Matedal tXib*&&t / oiqestion Add

S1eel. coooer. aluminum. solder.at! sr!, !at, i.f.*, !*.+ /Aquareqia, HNOr BCl, HF, H,O,4&,1Rt / HNO:,/HF

Gold. Dlatinum, Dalladium. c6'dmic

.t&, ttr.+, drn, 4.t / Hzsor H:o, HNo:, HCIrF \4+t;r&7?aa4 | Any acid lo lotal dbestion

4 a t e d b 1 6 G e i e € r c o d r o i s o t s

3 p o l g b ' t y 6 l o ' 9 c ' d ' d d h 6 e !

t{.'1.*{*.9 / Cutting . Peporation

dq$slil / sample Me*uemenr

fti{ r E *.s n{ { 6,} !! f,.0 *i3li,I &(r,T*.rf +) / rdd dtg€slion by suitaue acid dep€nded ddiffe€nt sampls materiat (as betowtabte)

d &/I &/i. s.*at&tit ib /Micwve digestian wnh HNoJHct/HF

,, t*4iitE& j!ti l{ it ++. / Heat ro appropnab

AftlirQ*{'s / Cool,nllel digeclale omugh liher

e\*ei l f ,e /Add

/*t lX-a A,kk1+t ' ttl*eatta 54onm At4

ab6dban@ al 540 nm byUV.VIS

1) &8fi;4 /AlkaliFudon2) i*t8t+ / HCllo dissoh€

,t{'d,+E+Test ReportET.SCHU(OM ELH(TRG5CHU1'ZKOMA)NEMENBAU GI{BHGEAERBESTI.ASSE 87, D.98669 VEILSDORF. GERVAIY

i t4(No. ) : CE/2012lr0834 A*(Dare) . 2072/07/ t2 F*(P.g.)

tmrum tlltmr

t*i+/ t*i&g,.&*,€ll / PBB/PBDE analytlcal FLOw CHARTr ;il$r'.t : 4iir# / Name oflh€ peEon who made measurcment: Roman Wongr FIE\ A l/\ : 'E-** / Name of the person in chaEe of measurement Troy Chang?r^,rli{fll / First testing proc€€s ---------+1ti*la$*€,+ / oplional sc€en [email protected]{1 ,l / Conf nnalion DrcGs - . - .)

Sc.een analys's/ ir$ "+4

I Sample ext€c1ion Sa;+*.-/ |I Soxhlei method *1.++t* |

Concenvate/Dilute Extracl€d solutionsfrR;i*ffif

Filter / +F enli&

Analysis by GCAIS / *,IAEf|ii'*it+4

p3(s)bsrad rb s rad Gponenior bc o m e a n v ! : ' , 1 , r . 1 i ) r r . l , a r r , : . . r i i i : ! l - l i , , . r , ' r \ l ! .

rl|a*E+Test Report

*tq(No.) : cEl2012/ lo83a

ELSCIIU(OM ELEKTROSCHUTZKOMPONENTENBAU CMBHCEIERBESTRASSE 8?, D-98669 I'EIISDORF, GERM,{NY

A*$are) | 2.r12/or/r2 q&(pase) : 8 " f l0

lflmf]t lttlfil

I

I

f *+*tr;t€f / Analytical flow chad of hatogen content

irl-J,/.F : tt,g+ / Narne of the pe6:on who made measurement Rita Chenlll$A t,t. : Ji.*q / Name of the person in charge of measurement: Troy Chang

*+nfr6N{r IAnalysis was performed by IC

c o m r a t u t , . ) ) i , t . , , t I t ' r , , r . : j r i r l r : l i r 1 . ' i r ' r lT h s f u m e . l s ' $ u e d b y 6 e c o m p a n i 9 b ] e d l o ' B G e n e l a c o | d t o i s d s ! 8 l o l a c 3 s f t a l W s g s c o m [ e m

suq6d ro r.ms aid coid$o.s ro, E abnron 6 dawi ro rh. miaioi or abit

!hds(D|7omN4'!pd(ur!w!i/N

,t{-d#+itt6(Yo. ) : cE/ 20r2/r0834 *(D"r") , 2or2/ot/12 FjF.(pase) : 9 or to

lfll[l] [ttl|||l

Test ReportELSCHUKOM ELE(TROSCHUTZKONPONENTENBAU GMBHGEi'ERBESIIASSE 87, D-98669 IIEII,SDORF, GRMA\Y

*{+F)ffX,ar /Analytical flow chat of 50)6tet extraction (LC/MS) procedu.e

r i{l- F : ff 41, / Name of the person who made me€surement: Roman Wongr fl:{A t,\ : tFr'34 / Name of the person in charge of measurementt Troy Chang

( rdn,i E: aF.+*,*rn/an+t(*) , **:"+fitb+& /Test ltem3: PFOS/PFOA ' Benzotriazole)

,tf / Daia

!bG) r8*d rh s bd r4or ennd e' r _ l l r , . r i r l / : r f i i r . ! 7 i l f r r t ) r 4 r L r r r , l n .

s p o ^ s b ' t y 6 l o l s c s i l a i d s 6 d d m

,F{a+E+i g g ( \ o . ) : c E . 2 0 l 2 t 0 8 t {

Test Report!I-SCHLT]<OiI ELEKTROSCHUTZ{OTPONENTENMU GTtsHGEWERBESTR/SSE 87, D 98669 VEILSDORF, GIII,\IANY

*(Date) , 2012/01/12 F*. (Pase) : 10 of 10

rfl[tl lllttflu

' ,R.H ft'tfrt*+ ' flAi&lFl*''l.{ls/S.t+. .(The tes t€d saDple / pa . t i s mrked by a t r a r ro , i I i t , s shoen on th€ photo . )

. . +t+r+4,(End of Report) **

, , r " . l r : l r ' l i 1 , . ! i 1 : i , i r . 1 i l r | r n .rh s dodmeil a sd byse.omo'iysuhedb 6 &iera' codd r ois or s

, 4 ' " N r1 r . ' . r j , l 600

10834

r0834

Test Report

SGS Job No. :

l,Iodel No. I

Composition :

Date of Sample Received :

Testing Period :

Test Requested :

Test Method :

Test Results :

Condusion :

No. SHAEC1116009838 Date: 14 Oct 2011 Page 1of 5

ZHEJIANG ASIA GENERAL SOLDERING & BRAZING MATERIAL CO.,LTDXIHU INDUSTRIAL PARK,SANDUN,HANGZHOU CITY.ZHEJIANG PROVINCE.CHINA

The following sample(s) was/u/ere submitted and identifed on b€hatf of the clients as : LEAD-FREE SOLDERWRE

sP11-030781 -SH

YTW102(692535-00 t,692535-002,692535-003)

Sn2.0CuRE

09 Oct 2011

09Oc t2011-13Oc t2011

Selecied test(s) as requested by client.

Please refer to next page(s).

Please lefer lo next page(s).

Based on the performed tests on submitted samples, the results of Lead,Mercury, Cadmium, Hexavalent chromium, Polybrominated biphenyls (PBB),Polybrominated diphenylethers (PBDE) comply wilh the limits as set by RoHSDiredive 201 1/65/EU Annex ll; recasting 200295/EC.

Signed for and on behalf ofSGgCSTC Lrd.

,zQr''Fan Jingjie, JJApproved Signatory

cdEd ar-r b tu ondr co'v,uo. ds.dd rnd .,.,h.r, .nr| . m q!$' 4 tarrbr. j hdA/hw er.oiw!!-!44!d!trNd;fi;L-;ii;;'tu;a-e-a;fr;;;; 'tu; DA;;F. i*!tEa@r:419!s4!sja!.Eii r {.I'-r. i. *oflq,d;iirrii€ b tu. ts c.icrba b Edisr DoMFF . !Etl@[email protected]*hd.arhl*r!rd.d.a'.dLdtdrdiffidRhf,i$rrss.c4m"/. I'drie' nhrm'd$.hado'.*. i'.nvd.d, ,b. rh.c!.lar rd. '.r.ddDri rb|bc||fndnui.d..dil6 d o9n;";;;d;;d;'d t$aidqiagDi.f . ntu'nm'it ad b FFd,{d.€!r h tun *'hod F!sFtbtu6db@h'd

Lun .hMri*hrntsnhtudrbib.6!i.(r)in!.

fArhthn9l|red&|,a.{9r9roh @lnt.!:.ltral&1830+$ lrl2@3

lEt(H1)8'lqA r$EF-?r)04€ryt9 l*.d.aicmHLO-el)611@t Hlj(10-21p15@ .sd'lerFq

r .nbdol tr'. SGS GmrP (gGS SA)

T€st Report No. SHAECl116009838 Date: 14 Ocl2011 Page 2 of 5

Test Results :

Test Part Descriotion :

Sp€dhen tlo. SGS &mdo lD Dscridion1 SHA1 1-160098.033 Sitvery metatwire

Remarks :(1) 1 mg/kg = 1 PPm = 0 0001%(2) MDL = Method Deteciion Limit(3) ND = Not Detected ( < tvDL )(4) "-' = Not Regulated

RoHS Dir€div€ 2011lbs/Eu

Test Method: With reference to IEC 62321:2008(1) Determination ofCadmium by ICP-OES.(2) Determination of Lead by ICP-OES.(3) Determination of Mercury by ICP-OES.(4) Determination of Hexavalent Chromium by Spot test / Colodmetdc Method using IJV-Vis.(5) Determination ofPBBS/ PBDES by GC-MS.

T€st ltem(s)Cadmium (Cd)Lead (Pb)Merorry (Hg)Hexavalent Chromium (Cr(Vl))Sum of PBBSMonobbmobiph€nylDibromobiphenylTribromobiphenylT€trabromobiphenylPentabromobiphenylHexabromobiphenylHeptabrornobiphenylOctabromobiphenylNonabromobiphenylDecabromobiphenylSum of PBDESlllonobromodiphenyl ether

ti!!t Ud!100 mg/kg

1,000 mg/kg1,000 mg/kg

1,000 mg/kg- mgKs- mgKs- mg/Kg- ms/Ks

mdks- ms/KS- ms/Kg- mg/Kg- mgKs- mg/Kg

1,000 mg/kgmg/Kg

MDt 0332 N D2 1672 N DO Negative- N D

5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D. N D

5 N D

dun .h.s6nirdn dr|rrsrrbbsir.Glbbd.

rh!dgr'ibb&-t'|h. ry&uEr b r. or-rcdt'|m.l !.'vr6dh Dcsr{rb.r tGrrr!Ar!!&t!!ll&s0,al@

-*rirEt id&n.h*did.i^dri.ah rdw detudt..dddMliFd6affih.noi.i'rtbs.c!rt,. imne..rhrhdb.a-iEiifi*rhntur rdchdr hdd.!, dE. n.cMrt or.o.4lbrlUr6k c lx{rnuirlh4Mr.6'd-.fi|

t.irdpbaYrtutodxll$ci1d,9rldOlr 20Gt'il 'lt .*Jr6tttragllstl lti 2@3

rEuFa)arlo€!5lrEl€(6-AFffi7t nr.4.$cml!{fi.2t)6l]@Sa Hr06-ql)5a5060 .!$dmGFs

fr.mbor ol U. AOS Goup (8GsS )

Test ReportTest ltem{s)

Dibromodiphenyl etherTdbromodiph€nyl eiherTetrabromodiphenyl eiherPentabromodiphenyl elherHexabromodiphenyl etherHeplabromodiphenyl etherOctabromodiphenyl etherNonabromodiphenyl eiherDecabromodiphenyl elhe.

No. SHAEC1116009834 Date: 14 Oct 2011 Page 3 of 5

Limit ldrm9Kgmdksmgkgmsn<9mg/Kgmg/Ksmg/KgmgK9mgKs

fitED&nrhrrhrD.l4LC'ao de33Sl.-tt.*fiAldt|€€efl+l :*2@r

MDt555555555

033NONDNDNDN DNDNDNDND

Notes :(1) The maximum permis,sibte timjt is quoted from direciive 2011/65/EU, Annex ll(2) o spottest:Negative = Absence of C t coating, positive = presence of CrVl coating;The tested sample shoutd b€ furthor verified by boiting-wateFextraction method if the spot test result isNegative or cannot be confrmed.o Boiling-water-extraction:Negative = Absence of CrVl coating; Positive = presence of CrVt coatingThe detected concentration in boiting-waterextraction solution is equat or greater than O.O2 mg/kg with S0cm2 sample surface area.For corrosion prctection coatings on metals: Infomation on storage conditions and produclion date of thetested sample is unavailable and thus results of Cr(Vl) represent status of the sample at the time oftestino

rE€(6-?1)11{@5! |E€F6-AF{S?! ||r4.rfl.cooH!i&ala11q04 |l0n-21)6aa!d|.3 .r6d'h&9.qr

M6ln!6. or ho 8GS Oro(9 {8OS S.$

Test Report No. SHAEC1116009838 Date: 14 Oct 2011 Page 4 of 5

,rtu.rM h r* bi npd rrrr o r b rr tmpr.(r) 'obd

ATTACHMENTS

RoHS Testing Flow Chart

1) Name of the person who made tesling: Jan Shi/yoyo Wang/A en Xiao/Gary Xuz) Name or me person in charge oftesling: Jefi zhang/George xu/ Elim LinJ) | nese samples w€re dissolved totaltv bv oreconditioning method according lo below flow chart.(Cl6+ and PBBS/PBDES test method'ex;tuoeo,

Sample Preparation

Sample l\Ieasurcment

Acid digestion withmacrowave/ hotplate

1) Alkali Fusion /DryAshing

2) Acid to di66olve

Nonmetallicmaterial

Heating to 90-95Cfor extraction

Adding 1,5-diphenylcarbazide

forcolordevelopment

Adding 1,5-diphenylcarbazide

for colordevelopment

A red colorindicatesthe

presence of Cr6'.necess€ry,

Pb/Cd/Hg PBB9/PBDES

.rbrd n T.m. d c.{drb * uidr Dd'M d fti..dt{rB..d.ol,dl'6:,{61-l-i6-n 66-Ii!1ii'd.-i-dbrr4f,iki.drrdiehxa&hd hrii.^ny[&db eour! ddHEffiEEFii|lsF-Eb afrlrb di-riinh fr l'trrd G.ll|t h*!d.F, td.ihloollaItllsltd*{.rdilkbrd.b!.. .Iihrhffi-i{rb.aturrq..rE rhturr.{6M.n'tuDrdo,rr.clqry.D/$.ffidrtr i{F.bE-yt

JbfBlsraY!$blrri urt4Strtllch 2m33+l 'tl . *iE8Atll89!13t! l* 2@c

rEcFa)6rc45* lE E(S{I6SD tw.ojra@ru{n-21)6L@s1 HirF2l)5a5{rE! . 3i.hi|or4@

M6hblr o, $o SGS Grolp l8GS 5,^)

Test Report

Sample photo:

No. SHAEC1116009838 Date: 14 Oct 20t l Page 5 of 5

SGS authenticate the photo on original r€port only'- End of Report "*

br. o.'|'rc.d!{rd l.d{ prr@d er.t, ud.nbd oqrd d -rrdtr n!414!!49!!qo44_!!!_a!q!aa

tr.hcd.D, ,d. rn.Cdrrvt -r. dn.*llt iblbcrd jdr'Lrn t ucr{a@rd|!.ft460ffi'nsrdb.nrDdo!.dE lhMlrldDdrdqrtls...pDB.roi$r

dub.hMhdrhinrddroi,rb'hrnp.i4lELc.

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[.m!.. otlh. 8GS Orcqp (aOS S )

SGS Job No. :

Date of Sample Received :

Testing Pedod :

Test Requested :

Test llethod :

Test Rosults :

Test Report No. SHAEC1119525001 Date: 07 Dec 2011 Page 1of 5

3M CHINA LII\4ITED

222# T|AN LtN ROAD, SHANGHAT (200233)

The following sample(s) was/were submjtted and identified on behatf of the ctients as j 3M 3779-pc

sP11-036760 - SH

03 Dec 2011

03 Dec 20'11 - 07 Dec 2011

Selected test(s) as requested by ctient.



Signed for and on behalfofscs-csTc Ltd.

. rhlconr.rt dr dMr!,rlty r.brbdM!l![|',1|blt'c]|n|sdon.dedr'4i.lb.'.'fd!cn.gpl|ilu

,.,1s

,rt*{ *

Fan Jingjie, JJApproved Signatory

B dud rr h. 6hF4 4bLd bn c.'6ld hr 61 6rFe Ebtd b rE c.!6h. dodDd,rlFd r hr s n e'@h/orat.{.Mrit,ifi enA n ch^ ro-b-knbrd o;d;; ;6;;-rd;:;;6;;H ff 4fi ;ffi;;6;ii?6; d &; G6i;i$fiiiiuiriiiii?l;;ft'diffii;n; ;r

'rhrconr.rt !h dMllr|lty r.b

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lE&lr+tle$OZs5s lFlE{e-aF4e$Ot ffici.4rj0nH! n1)314&591 Hlr@6-21)646063 . €.!'i'€re.q

Monbor oth. SGS grup (SGg S )

Test Report No. SH4EC1119525001 Date: 07 Dec 201'1 Page 2 of 5

Test Results :

Test Pan Descriotion :

Spodm€n No. SGS Sample lD D66cription1 SHA1 1-195250.001 Ye ow sotid

Remarks :

(1) 1 mg/kg= I PPm =0.0001o/o

(2) MDL = l,tethod Detection Limit(3) ND = Not Detected ( < IIDL )(4) "-" = Not Regulated

RoHS Dir€dive 201 iA5/EU

Test l\rethod: with referenc€ to tEC 62321i2008(1) Delemination ofCadmium by tCP-OES.(2) Determination of Lead by tCp-OES.(3) Determination of Mercury by lCp-OES.(4) Determination of Hexavatent Chromium by Cotodmetric Method using IJV-Vis.(5) Determination of PBBS / PBDES content by GC-MS.

Test ltem(s)Cadmium (Cd)Lead (Pb)Mercury (Hg)Hexavalent Chrcmium (Cr(Vl))Sum of PBBSMonobromobiphenylDibromobiphenylTdbromobiphenylTetrabromobiphenylPentabromobiphenylHexabromobiphenylHeptabromobiphenylOclabromobiphenylNonabrohobjphenyl

Decabromobiph6nylSum of PBDESMonobromodiphenyl ether

ud! udr100 mS/kS

1,000 mg/kg1,000 mg/kg1,000 mg/kg1,000 mg/kg

- mg/Kg- ng/Kg- mg/kgmg/Kg- mgfl(g- mg/kgmg/Kg- mgKg- mgKg- mg/Kg

1,000 mg/kgmg/kg

Ma! 0p12 N D2 N D2 N D2 N D- N D

5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D

5 N D, N D

5 N D

'aad* b rmr h. c@ '. tq ErFioir ooamrb .r n*r.oitu'm .{dM(h_.a&d,& tr &.m b-br lldabr oi$uB4t6-.Bdk,Hie .dndLn.xdhGlffi;;dF;.ffi

,. ih. conDrvr |d. dH.5 1y r.roro C r.d !d fi @iar d6! id.xffiib !.di;b I hi-did.'d.b!l!| |...uid'|h.hEd|on

b hr hd com'rk FrFiori bamrb.r 6Fr.oitu'm.{ddr h_.a&d,t tr &.h b-rrlltub. o

' / D t ' r h . c o n D f y r d . f i H & J | ' L{!hb.id.bft:rr..r und.r rh. hu|. 'd.o!l!|h.uielb.hEd|o

i rtori.r.n!.(.) ' ..bd

Membfi ol h6 SGS G.o{p (SqS S,A)

t'ctElu8Ygrsidd xdr dsid,iuahdol|tl.Ill.*icEturi|3aelts+i ll

lE&E(s-z)61{!2553 ift€(6-21)6€Sl! l*o3e3.hru{6-?11614025e4 NL06-a)5{44653 .t5.diE€F9{q

Test ReportTest ltemls)

Dibromodiphenyl etherTribrcmodiphenyl etherTetrabromodiphenyl etherPentabromodiphenyl elh€rHexabromodiphenyl etherHeptabromodiphenyl etherOclabromodiphenyl elherNonabromodiphenyl etherDecabromodiphenyl elher

Notes :

No. SHAEC1119525001

tuni.!

Date: 07 Dec 2011 Page 3 ofs

Ulit Mgt @lmg/kg 5 NDmg/kg 5 NDmg/kg 5 NDmg/kg 5 NDmg/kg 5 NDmg/kg 5 NDmdkS 5 NDmg/kg 5 NDmdkS 5 ND

(1) The maximum permissible limit is quoted from directive 2011/65/EU, Annex ll

lhrid@'i.n b d.d rrrh. co6Ftry rbj.d b r. qdsrc4rrls!or s.ftronld d,blllgbd io.'n docle'f,a*dn r.m. .nd co{drrN ft. €e

.n o,r€a'br. n!qjr!r! rt. 6i4.!4 r{ @l!4!!'!ilrir€. r.m.6d cotu ft. Ed;d. oo*tub d fr er.s;E m.ndrd.hi. ^ed & tr hh |th. iin'bd-r-d.tudhrii adbrdr.rBMd'.ddturEffiF 6ffirffi;i;6dc[ift htulnlE. ririr, rnrco@$?. ,.rr ridlbfly nbitcjrr rnrco@rf. ,0r ridlb$v I

Ddobrrrrd.uncrh.r.6.cl0n nrr&-{.r. rltull|mod'.s'b{4etfui '6o'$.*d.i ld

i rrcii. hr.(r)L.bd

t'btEr$loYdrnto d&htotttltsllccrir 2t0233FN.lll.iiEEf, dr1330+39| 11 2M3

rEtE{s-21)81,€2553 tEE€(6-2r)6'gS79 t*.Nn.4.Mh!t& 21J6t4@P1 rL{s'?rFLa653 . !s.d'iEo!p9@

Membsr ol tlra SGS Grolp (6GS SA)

Test Report No. SHAEC1119525001 Date: 07 Dec 2011 Page 4 of 5

ATTACIII,|ENTS

Rol-ls Testing Flo\ r Chart

1) Name of the p€rson who made testing: Jan S hi/yolo Wangr'A en Xiaocary Xu2) Name ofthe p€r6on in charg€ ofteging: Jeff Zhang/George Xu/ Etim Lin3) These sam ples were d isso lved t otat ty b y pre-cond iti oning met hoda cDordi ng to be tow ffow chan.

(Cr6+ and PABs/PBDEst6st method exdudeO

Sample Preparalion

Sample Measuremenl

Acid digestion withmicrDwa\€/ hohlate

Concentratio n/Dilutaon ofodradion

solution

1) Alkal iFudon /Ory Ashing

2) Acjdto dissol\E

Metal l icmatedal

Heating to 90-95Cfor extraclion

Filtration and pHadiustnent

Adding 1,SdiphenY€arbazide

de\elopmentAdding ' l ,$

diphentcarbazide

ind icates the

Pb/Cd/Hg PBBs/PBDES

iro -drll!!tub bd &!m.tr6 Ebld b thr md cdhffi 6

[email protected] Er. r.@idb rr BiorqcldhdN'elndd'rid.

ry b rb ..FPr.(.) hrbd

3'hidterdre.d&n ol,nli.dijc|i. 2ocrar34!'lt.*iEgl&l6ao+3*l ll:2o@3

rErE6-?)0110?653 lElE&"rF4o$tg md..!.cmHL(A-2',)01'&Cr r.iL{e-21)s.6dEE3 . rg5ftnD9d

M3mb6r ot rhe SGS Group (SGS SA)

Test Report

Sample pholo:

No. SHAECI' l19s25001 Date: 07 Dec 2011 Page 5 of 5

sHA11n9s250.001

SGS authenticate the photo on original report only

""' End of Report "*

'd4r ilffi b N. nd -Fr nb sry r. tu 3hpr.{.) r..bd

Daqdbr.oddlr obte b h oFdredf r 41 5k6E e6min I .h sr.Birr'hr .{oon.d}hi. Atut{; n dn;lt[aIFd oi ol

BdlgtRia..d hd'dbn E{a otud tu{i. ^ry ber.,d' tunmr I kd hr];Gifii6iEn-&.d|'lnfu-h co.e.hrr r{ns .'hnhdtlAi5rl6dqarbhhrin!d*mtrd!d.F,[email protected]!bbcr.drndh!deun.ntd-3iddoi.nbFtubrntrrdoni ' t r 5 t d ] h ! . l | t i i N b f r [ d d i | ' ' $ l . l | d d f f t r 1 d i n d l b . E 9 F d . o d . r F 9 t | n f u | l ' f | s M 0 d ' | i ' b 'fi/srdi!|@ rhQan.htsry d

3nElEbr3gYitritodxll|loitad,$|Et'otu a@3+l ..ti|.*[Allt$r.lrrtsltl lrt 2@33

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Msnb€i ol dt6 SGS Gble {SqS s,q)

Tast Report No. SHAEC1119525002 Date: 07 Dec 2011 Page 1 of4

3M CHINA LIIVITED

222#T|AN LtN ROAD, SHANGHAT (200233)

The following sample(6) wasi/vere submitted and identified on behalfofthe ctients as :3M 3779-pc

SGS Job No. :Date of Sample ReceivedTesting Pedod :Tesl Requested :

Test Method :

Test Results :

sP11-036760 - SH03 Dec 2011

03Dec2011-07Dec2O11

Selected test(s) as requested by client.



Signed for and on behalfofscs-csTc Ltd.

.--),-

,/t*( Y*

Fan Jingjie, JJApproved Signatory

tiu dud 'r .sd br rh c.6Fn &b!.r b r! o-nr c.i.dEr.r sirdd.qlqs* hr, dodtun.rdt dr nmr.^r @d.d b Eh'. eErd d ,wB Fri/!.r{ .{oen.d.di' ^M-s n dfraltb.I {orol

t'EtuneY$se.dlnde4$.ddonr 2o@3t!'tl.*iEEt r||$sts+l ln:2(0aa

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lrombor ot th€ SCSCloup (SGSaA)

Test Report

Haloo€n

Test lrethod : With

Test ltem{s)Fluorine (F)Chlorine (Cl)Bromine (Br)lodine (l)

No. SHAEC1119525002 Date: 07 Dec 2011 Page 2 of 4

Test Results :

T€st Part Descriotion :

Sp€dm6n No. SGS Samplo lO D€6cfiption1 SHA1l -195250.001 Yellowsolid

Remarks :(1) 1 mg/kg= 1 ppm =0.0001%

(2) MDL = Method Detection Limit

(3) ND = Not Detected ( < MDL )(4) "-" = Not Regulated

reference to EN 14582: 2007, analysis was performed by lon Chromatograph (lC).

Unit

mg/kgmg/kgmg/kgmg/kg

MDL OA50 ND50 ND50 ND50 ND

ftldemd b &.d by rh. c.rtse &q-i b h. ofmrc&dlnld !d@,.,gEo* hd d..4d,r4d b rlm.ir o6idri6 k EMor. D.eMr d mcoMrB.-dM' tu- abdli n a.dr ro *ittdrldon o,t3ltzEnastql/l!l{i!.'gql+ltffill{eq!l.dlgr9 tudnc h'h aryi"k.lhb &ffitL rdrd!E ffi;Eifiaii'*-iiiaiiP|q-T5^46N@htuhtr

d.trtr,rD.cmk_qL. reh.rr.ri.&nds.bt

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Mehbrrot lhe SGS OlouD (SGSSA)

Test Report

ATTACHMENTS

No. SHAEC1'119525002 Date: 07 Dec 201'1 Page 3 of 4

1 ) Name of the person2) Name of the person

Halogen Testing Flow Chart

who made testing: Daisy Gongin charge ofte6ting:Alex Jiang

Sample measurement

Combustion in oxygen boftb

Dissolved in an absorptionsolution

Analyzed by ionchromatography. Double conf km

by other instruments, if

rhbdtuiff | 6rd !r rh conFry rhtd b dr oddr ftrdds3 ar 5!l! rd,,!!!!r'* hn daclhublr 4- b r.nr tn! codfr b ddo. Doo|Eb !t ,N m.qtrr..fl ..

trqld & |d|# .r idt.'@rj!I!4!rt!!!!r!!_s'q!!!r!!t ffis.c.fr4.!4!d!hn ^tuiion a-h ic6nhlbii;i'r

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t'etEl$&lbrsto dxniudtd,gt$afl onr [email protected],t.$llEttftaetst* ll:2Mo

rE!E(S-2r)0t104!& IAEt6?1)6{S',r9 lwcr.3s"co6N!(6.?16r102!04 -L {*-n)6460cs3 . .ssd'mO69q

M6mb6rollheaqsGbup (SGgsr)

T€st Report

Sample photo:

tTr.t:ry::. D-? I'gT.i:?aq!Ke.n: j!L 1cbj

*nrbr .prdd or b. comr.iy.hrw.iMridrndnldrhrnrrr.ih..F r.(.)r..bd.

No. SHAEC1119525002 Date:07 Dec 2011 Page 4 ol4

sHA11-195250.001

SGS authenticate the photo on odginat report onty

"* End of Report '*'

l'Dt!.It6eY.l.iicdunosJdshdtorr 200233tl..ti,*iE8lurt|8ogli3qt lrl:2M3

rEtEl&2r)d14653 lElE6?lje€$da ffi .i..!.cmHli(s-zll6t@ol &ls-?l)se$ ..s.dr&F.6

Mlmb€| ol rh. scs Goup (scs sa)

nov'TEST REPORT

NO.:4002E11121307-2R02 Oa!aiDec15,2o11 page 1 of4

Customer: Suzhou FuHong Electrcnic IndustfialCo, Ltd.Addrgs8: NO.89WEl DU ROAD, WANGTING TOWN, XTANGCHENG D|STR|CT, SUZHOU, CHTNAReport on th6 3ubmitted ssmple said io beSample name: Fusos copper shellllodol: /

Material: /D$cription: /Buyea: /supplier: /

Sa|nple recelved date: Dec.13,2011Tcatlng p€riod: Frcm Dec.13,2011 to Dec.15,2011

T€tino Reau6tedAs specined by client, to delermine the L€ad, Cadmium, Mercrry & Hexavatent Chrcmium content in the submitted sampte inaccordance wilh Direclive 2002/95/EC (RoHS).

Tcstind method:

Testing llem [,leasudng inslrument MQL

Lead (Pb) EC 62321: 2008, seclion 9 ICP-OES 2mglkg

cadmium (Cd) EC 62321: 2008, section I ICP€ES 2 mg/kg

Mercury (Hg) EC 62321r 2008, section 7 rcP-oEs 2 mg/kg

Chrom'um (Cr l'I) EC 62321:2008, Annex I 0.02mg,a(g'

ILS, PLEASE REFER TOTHE FOLLOWING PAGE(S)'**'

lsg-'0.02 mg/kg returs 10 lhe MQLofsample extEction tiquid.

99!s!.c!i9!j-ffien tesied as specifred the submitted sample complied with the requircments of commission Decision of 18 Aug 2005amending Directive 2002l95/EC nolified lnderdocument 2005/618/EC

',:,"il:::i" ryf4lffH*"",",We-i hr n

,3ffi::::1,,44

S}'EI{ZN€N AOV TGSTING T€CHNOlOGY CO.,L'D.KUNSHAN EiANCH Hotllne86-512-5510 8000

6novNO.: 4002E11121307-2R02

TEST REPORT

Add the digestion solution; thevessel is heated Lrntil lhe sampl€ Add HrO, u nlil the sampl€ is clear

F;;1.-F;;,",..;-1.-{Melal subslrat€)

Add lhe digestion solution, clos€

the macrowave vess€|.

Cooling the vessel, fllleri washed and

filled to the mark with distilled water.

The sample is digested in the

micrcwave oven following a specific

decomposilion program.

and l\rercury Content: (Praring)

_____-l coor,ns. nrr", *""n"0 ""0 r"o | ,l o*o -ill_.;*--;-l

I to the mark with Dtwater I I r*r.r*t | | -.- |

STIENZH€N AOV TESIING T€CIII{OLOGY CO.,lIO,KUII9HAN BFANCH

Hdpi/j,w.o{,6n

Hotline86-512"s510 8oO0

Cooling the vessel, filter washed and

filled to the mark with distilled water.

Remove the sample, and coollhe beaker lo rcom tempefalure,and do 1ie color reaction

Heal 50 mL ofDlwaterin lhe

beakerto boiling for 10 min

Test the sample solution and lhe 0.02mg/kg standard solution by UV-VIS.

To Detemine

nov.NO.: 4002E11121 307-2R02

5. To Detemine Hexavalent Chromium- '' ',.'1re$eo ovr I r

s.t sw-resi (M&

TEST REPORTDate: Dec.15, 2011

Contentln colorless and colored ctlromate coaling on

Page 3 ol4

metals: (Plating)

lflhe lest resull is positive,

the sample is considered 1o

have hexavalenl chromium

and the 0.02 mg/kg

Boiling- waieF extractionprocedure shall be used to

lfthe€ isrnterference orI rs hard to decide *terhellhe sample have the hexavalent chrcmium

5 2 Boiling- wEter- en€ction

Take the (5015) cm'z

sample in the beaker.

Srmple d93cription:

SH!NZHEN AOV TESTING TCCTNOIqGY CO.,L}D,KUNSHAN BFANCH nHot l ine86'512^5510 8000

Remove he sample, and cool

lhe beaker 1o room temperature,

and do the color reaction

Heat 50 mlof Olwater in the

beaker lo boiling for 10 min

Test the sample solution and the 0.02

mg/kg standard solution by UV-VIS.

Copper shell subslrateLead wle Platrng 24 Copper shell Plaling

Unil RoHS

Limit 2-3 24"Lead (Pb) mg/Kg 1000 N.D. 2.5 40.0 N.D.Cadmium {Cd) mg/kg 100 N,D. N.D. N.D. N.D.Msrorry (Hs) mg/kg 1000 N.D, N.D, N.D. N.D.Chromium (Crvl) mg/Kg 1000 Negative Negative Negalive Negative

nov.TEST REPORT

NO.r A002E11121307-2R02 Dat€iOec15,2011

-The new RoHS di.ective 2011/65/EU, on Jul 21, 2011 come into force, on Jan. 03, 2013 the fomat imotementation. Dircctive

2002l95/EC shall be reoealed simultaneouslv.

Sp€cim€ns, wnicn requested to determine Lead, Cadmium and l4ercury Conlent, have been dissotved comptetety.-mg/kg=ppm

-N.D.=not detected(<tVoL)-MQL=l'rethod Ouaniilation Limit-Negalive=Abs€nce of Cr (VI);

Posilive=Prcs€nce of Cr (VI)i

Uncedain= c€n noi ve fy whether the sample have Hexavat€nt Chrcm ium by spoliesl.(The tested s€mple should be furlher venfed by boiling-waterextradion method if the spol test result is uncertain or

-'The test is based on the following assumption:The sampte ptating is a singte tayerand each pad is unifom. The test resuttmaybe cannol sland ior rhe physicartruth of sample plating.

Photog.aph ofSample

"'End of Repod"'

S'iE'!ZH€N AOVT€STING TECXNO!OGYCO..lIO,KUNSHAN ABANCH

Hh,:/fuloi6n nHotline86-512-5510 8000

Test Report Number : TWNC00233073

Authorized By: On Behalf Of Intertek Testing Services Taiwan Limited

K. Y. Liang Director

This report shall not be reproduced except in full, without the written approval of the laboratory.

Page 1 of 6 Intertek Testing Services Taiwan Ltd.

8F., No. 423, Ruiguang Rd., Neihu District, Taipei 114, Taiwan, R.O.C. 全國公證檢驗股份有限公司 114台北市內湖區瑞光路 423號 8樓

Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

Applicant: Littelfuse Philippines Inc. Date : Nov 23, 2011 LIMA Technology Center, Lipa City,

Malvar, Batangas

Sample Description:

One (1) group of submitted samples said to be : Part Description : Sand Filler Part Number : 091251 Date Sample Received : Nov 17, 2011 Date Test Started : Nov 18, 2011

Test Conducted :

As requested by the applicant, for details please refer to attached pages.

Number : TWNC00233073

Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

(Ⅰ) Test Result Summary : Result (ppm)

Test Item Light Grey Powder

Heavy Metal

Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND

Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND

Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND

Halogen Content Fluorine (F) ND Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million based on weight of tested sample = mg/kg ND = Not detected

Responsibility of Chemist :Irene Chiou / Kevin Liu / Cathy Chen

Date Sample Received : Nov 17, 2011 Test Period : Nov 18, 2011 To Nov 22, 2011


Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

(Ⅱ) RoHS Requirement: Restricted Substances Limits

Cadmium (Cd) Content 0.01% (100ppm) Lead (Pb) Content 0.1% (1000ppm) Mercury (Hg) Content 0.1% (1000ppm) Chromium VI (Cr6+) Content 0.1% (1000ppm) Polybrominated Biphenyls (PBBs) 0.1% (1000ppm) Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

(Ⅲ) Test Method:

Test Item Test Method Reporting Limit

Cadmium (Cd) content

With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Lead (Pb) content


2 ppm

Mercury (Hg) content

With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.

2 ppm

Chromium VI (Cr6+) content

With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.

1 ppm

Polybrominated Biphenyls (PBBs)

With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.

5 ppm

Polybrominated Diphenyl Ethers (PBDEs)


5 ppm

Halogen Content With reference to EN 14582:2007 by calorimetric bomb with oxygen and determined by ion chromatography

50 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample


Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

(Ⅳ) Measurement Flowchart: Test for Cd/Pb/Hg/Chromium (VI)/PBBS/PBDES Contents Reference Standard: IEC 62321 edition 1.0:2008

Remarks: *1: List of Appropriate Acid：

Material Acid Added for Digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected.

Sample preparation

For different material, digest the sample with appropriate acid*1

Make up with deionized water

Cd/Pb/Hg

Analyzed by ICP-OES

Weigh sample and add alkaline solution

Definite temp. extraction

Make up with deionized water and add diphenyl-carbazide solution

Cool and filter the extract

Cr6+

Weigh sample and add organic solvent

By Soxhlet extraction or Solvent extraction

Concentrate the extract and make upwith organic solvent

PBBs/PBDEs

Analyzed by UV-VIS

Analyzed by GC-MSD

By spot test

Get 50cm2 sample

By boiling water extraction

Metal Polymers / electronics

Negative *2

Confirm the tested samples are totally dissolved

Take sample and immerse into Aqua Regia, start to strip plating layer

Stop the stripping procedure upon color change completely

Take the Aqua solution as plating component and stripped body as substrate component

For non-metal part For metal part


Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

(Ⅳ) Measurement Flowchart:

Test for Halogen Content Reference Standard：EN 14582

End of Report

Add absorbent in a combustion flask & place weighed sample in equipment

Fill oxygen into calorimetric bomb

Ignite then leave the flask at room temperature

Transfer the absorbent into a volumetric flask

Make up with deionized water

Sampling/grinding or cutting

Analyzed by ion chromatography


Test Conducted



Tel: (+886-2) 6602-2888．2797-8885 Fax: (+886-2) 6602-2400．6602-2401

Photo

Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338

TEST REPORT NUMBER: SHAH00287553

PREPARED AND CHECKED BY: AUTHORIZED BY: FOR INTERTEK TESTING SERVICES FOR INTERTEK TESTING SERVICES LTD., SHANGHAI LTD., SHANGHAI

MYRA LV STEPHEN TSANG CHEMICAL LAB SENIOR MANAGER GENERAL MANAGER

PAGE 1 OF 15

APPLICANT: LITTELFUSE,INC. DATE: NOV 01, 2011 800 E. NORTHWEST HWY

ATTN: A. CESISTA/ K. BACILA

SAMPLE DESCRIPTION: One (1) submitted sample said to be: Red ink. Part Description : Ink - red. Part Number : 425901. Date Sample Received : Oct.25, 2011. Date Test Started : Oct.25, 2011. ***********************************************************************

TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)

*********************************************************************** TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 15

1 PHTHALATE CONTENT TEST

WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.

LIMIT(%,W/W) TESTED COMPOUND RESULT (%,W/W)

(MAX.) DIBUTYL PHTHALATE (DBP) ND --- DI(2-ETHYL HEXYL) PHTHALATE(DEHP) ND --- BENZYL BUTYL PHTHALATE (BBP) ND ---

SUM OF THREE PHTHALATES ND 0.1

REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 (FORMERLY KNOWN AS DIRECTIVE 2005/84/EC) FOR PHTHALATE CONTENT IN TOYS AND CHILDREN CARE ARTICLES.

DETECTION LIMIT = 0.01%(W/W) ND = NOT DETECTED % = PERCENTAGE BASED ON DRY WEIGHT OF SAMPLE/COMPONENT

**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 15

MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS

**********************************************************************

TO BE CONTINUED

Weigh sample and place in a thimble

Extracted by Soxhlet extraction with organic solvent

Concentrate the extract

Analyze by GC-MSD

Make up with organic solvent

Transfer the extract into a volumetric flask



TESTS CONDUCTED

PAGE 4 OF 15

2 (I) Test Result Summary :

Testing Item Result (ppm)

Halogen Content Fluorine (F) ND Chlorine (Cl) 720 Bromine (Br) ND Iodine (I) ND

Remarks: ppm = Parts per million based on weight of tested sample =

mg/kg ND = Not detected

Responsibility Of Chemist :Ken He

(II) Test Method:

Testing Item Testing Method Reporting Limit

Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography

50 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 15

(III) Measurement Flowchart:

Test For Halogen Content Reference Standard： EN 14582

**********************************************************************TO BE CONTINUED

add absorbent in a combustion flask & place weighed sample in equipment

fill the combustion flask with oxygen

ignite then leave the flask at room temperature

transfer the absorbent into a volumetric flask

make up with deionized water

sampling/grinding or cutting

analyzed by ion chromatography



TESTS CONDUCTED

PAGE 6 OF 15



Heavy Metal




**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 7 OF 15

Remarks: ppm = Parts per million = mg/kg ND = Not detected

Responsibility Of Chemist :Dent Fang / Ken He

(II) RoHS Requirement:

Restricted Substances Limits Cadmium (Cd) Content 0.01% (100ppm)Lead (Pb) Content 0.1% (1000ppm)Mercury (Hg) Content 0.1% (1000ppm)Chromium VI (Cr6+) Content 0.1% (1000ppm)Polybrominated Biphenyls (PBBs) 0.1% (1000ppm)Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)

The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 8 OF 15

(III) Test Method:




2 ppm

Lead (Pb) content


2 ppm



2 ppm



1 ppm



5 ppm



5 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 9 OF 15

(IV) Measurement Flowchart:

Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard: IEC 62321 edition 1.0:2008

**********************************************************************

TO BE CONTINUED


weigh sample and for different

material, digest the sample with


Cd/Pb/Hg

analyzed by ICP-OES

weigh sample and add alkaline solution

definite temp.

make up with deionized water and add diphenyl-

carbazide solution

Cr6+

weigh sample and add organic

soxhlet extraction or

solvent extraction

concentrate the extract and make up with organic

PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples

boiling water extraction

metalpolymers / electronics

negative*2confirm the tested samples are totally

dissolved No

cool and filter the extract



TESTS CONDUCTED

PAGE 10 OF 15

REMARKS:

*1: List of appropriate acid： Material Acid added for digestion

Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4

*2: If the result of spot test is positive, Chromium VI would be determined as detected. **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 11 OF 15


WITH REFERENCE TO ASTM D3421, BY GAS CHROMATOGRAPHY-MASS

SPECTROMETRY (GC-MS) ANALYSIS.

RESULT (%, w/w) LIMIT (%, w/w) (MAX.) DIBUTYL PHTHALATE (DBP) ND 0.1 DI(2-ETHYL HEXYL) PHTHALATE (DEHP) ND 0.1 BENZYL BUTYL PHTHALATE (BBP) ND 0.1

REMARK：THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER

PRODUCT SAFETY IMPROVEMENT ACT 2008 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES.

DETECTION LIMIT = 0.01% (w/w) ND = NOT DETECTED % = PERCENTAGE BASED ON DRY WEIGHT OF SAMPLE/COMPONENT.

**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 12 OF 15

MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS **********************************************************************

TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 13 OF 15

5 (A) TEST RESULT SUMMARY:

TESTING ITEM RESULT(ppm)

HBCDD (HEXABROMOCYCLODODECANE) ND

REMARKS: ppm = PARTS PER MILLION = mg/kg ND = NOT DETECTED (B) TEST METHOD :

TESTING ITEM TESTING METHOD REPORTING

LIMIT

HBCDD (HEXABROMOCYCLODODECANE)

WITH REFERENCE TO USEPA 3540C, BY SOLVENT EXTRACTION AND DETERMINED BY GC/MS

10 ppm

DATE SAMPLE RECEIVED : OCT.25, 2011 TESTING PERIOD : OCT.25, 2011 TO OCT.31, 2011 **********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 14 OF 15

MEASUREMENT FLOWCHART: TEST FOR HBCDD (Hexabromocyclododecane) CONTENT **********************************************************************

TO BE CONTINUED

Weigh sample and place into a thimble

Soxhlet extraction with organic solvent


Analyze by GC-MSD





TESTS CONDUCTED

PAGE 15 OF 15

**********************************************************************

END OF REPORT





PAGE 1 OF 15

APPLICANT: LITTELFUSE,INC. DATE: OCT 31, 2011 800 E. NORTHWEST HWY ATTN: A. CESISTA/ K. BACILA

SAMPLE DESCRIPTION: One (1) submitted sample said to be Black ink. Part Description : Ink – black. Part Number : 425902. Date Sample Received : Oct.25, 2011. Date Test Started : Oct.25, 2011. ***********************************************************************


**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 15








**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 15


**********************************************************************

TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 4 OF 15







(II) Test Method:



50 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 15



**********************************************************************TO BE CONTINUED










TESTS CONDUCTED

PAGE 6 OF 15



Heavy Metal




**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 7 OF 15






TO BE CONTINUED



TESTS CONDUCTED

PAGE 8 OF 15

(III) Test Method:




2 ppm

Lead (Pb) content


2 ppm



2 ppm



1 ppm



5 ppm



5 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 9 OF 15



**********************************************************************

TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples




dissolved No




TESTS CONDUCTED

PAGE 10 OF 15

REMARKS:




TO BE CONTINUED



TESTS CONDUCTED

PAGE 11 OF 15








**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 12 OF 15


TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 13 OF 15






LIMIT



10 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 14 OF 15


TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 15 OF 15

**********************************************************************

END OF REPORT





PAGE 1 OF 15

APPLICANT: LITTELFUSE,INC. DATE: OCT 31, 2011 800 E. NORTHWEST HWY


SAMPLE DESCRIPTION: One (1) submitted sample said to be Yellow ink. Part Description : Ink – yellow. Part Number : 425903. Date Sample Received : Oct.25, 2011. Date Test Started : Oct.25, 2011. ***********************************************************************


**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 15








**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 15


**********************************************************************

TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 4 OF 15







(II) Test Method:



50 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 15



**********************************************************************TO BE CONTINUED










TESTS CONDUCTED

PAGE 6 OF 15



Heavy Metal




**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 7 OF 15






TO BE CONTINUED



TESTS CONDUCTED

PAGE 8 OF 15

(III) Test Method:




2 ppm

Lead (Pb) content


2 ppm



2 ppm



1 ppm



5 ppm



5 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 9 OF 15



**********************************************************************

TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples




dissolved No




TESTS CONDUCTED

PAGE 10 OF 15

REMARKS:




TO BE CONTINUED



TESTS CONDUCTED

PAGE 11 OF 15








**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 12 OF 15


TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 13 OF 15






LIMIT



10 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 14 OF 15


TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 15 OF 15

**********************************************************************

END OF REPORT





PAGE 1 OF 14



SAMPLE DESCRIPTION: One (1) submitted sample said to be: Blue ink. Part Description : Ink - blue. Part Number : 425904. Date Sample Received : Oct.25, 2011. Date Test Started : Oct.25, 2011. ***********************************************************************


**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 14







DETECTION LIMIT = 0.01%(W/W) ND = NOT DETECTED

**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 14

MEASUREMENT FLOWCHART: TEST FOR PHTHALATES (EN14372) CONTENTS

**********************************************************************TO BE CONTINUED


Extracted by Soxhlet extraction with organic solvent for 6 hours


Analyze by GC-MSD





TESTS CONDUCTED

PAGE 4 OF 14

2 (Ⅰ) Test Result Summary : Testing Item Result (ppm)





Date Sample Received :OCT.25, 2011 Testing Period :OCT.28, 2011

(Ⅱ) Test Method:



50 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample ***********************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 14

(Ⅲ) Measurement Flowchart:


************************************************************************

TO BE CONTINUED










TESTS CONDUCTED

PAGE 6 OF 14

3 (Ⅰ) Test Result Summary :


Heavy Metal




************************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 7 OF 14



Date Sample Received :OCT.28, 2011 Testing Period :OCT.28, 2011

(Ⅱ) RoHS Requirement:


The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.

************************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 8 OF 14

(Ⅲ) Test Method: Testing Item Testing Method Reporting Limit



2 ppm

Lead (Pb) content


2 ppm



2 ppm



1 ppm



5 ppm



5 ppm

Remark: Reporting limit = Quantitation limit of analyte in sample

************************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 9 OF 14

(Ⅳ) Measurement Flowchart:


************************************************************************

TO BE CONTINUED



TESTS CONDUCTED

PAGE 10 OF 14


WITH REFERENCE TO ASTM D3421, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.




DETECTION LIMIT = 0.01% (w/w) ND = NOT DETECTED

**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 11 OF 14

MEASUREMENT FLOWCHART: TEST FOR PHTHALATES (ASTM D3421) CONTENTS

**********************************************************************TO BE CONTINUED


Extracted by Soxhlet extraction with organic solvent for 16 hours


Analyze by GC-MSD





TESTS CONDUCTED

PAGE 12 OF 14






LIMIT



10 ppm

DATE SAMPLE RECEIVED : OCT.25, 2011 TESTING PERIOD : OCT.25, 2011 TO OCT.28, 2011

**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 13 OF 14


TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 14 OF 14

**********************************************************************

END OF REPORT





PAGE 1 OF 15



SAMPLE DESCRIPTION: One (1) submitted sample said to be Brown ink. Part Description : Ink - brown. Part Number : 425906. Date Sample Received : Oct.25, 2011. Date Test Started : Oct.25, 2011. ***********************************************************************


**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 15








**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 15


**********************************************************************

TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 4 OF 15







(II) Test Method:



50 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 15



**********************************************************************TO BE CONTINUED










TESTS CONDUCTED

PAGE 6 OF 15



Heavy Metal




**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 7 OF 15






TO BE CONTINUED



TESTS CONDUCTED

PAGE 8 OF 15

(III) Test Method:




2 ppm

Lead (Pb) content


2 ppm



2 ppm



1 ppm



5 ppm



5 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 9 OF 15



**********************************************************************

TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples




dissolved No




TESTS CONDUCTED

PAGE 10 OF 15

REMARKS:




TO BE CONTINUED



TESTS CONDUCTED

PAGE 11 OF 15








**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 12 OF 15


TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 13 OF 15






LIMIT



10 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 14 OF 15


TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 15 OF 15

**********************************************************************

END OF REPORT





PAGE 1 OF 15

APPLICANT: LITTELFUSE,INC. DATE: NOV 01, 2011 800 E. NORTHWEST HWY


SAMPLE DESCRIPTION: One (1) submitted sample said to be Green ink. Part Description : Ink – green. Part Number : 425907. Date Sample Received : Oct.25, 2011. Date Test Started : Oct.25, 2011. ***********************************************************************


**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 15








**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 15


**********************************************************************

TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 4 OF 15







(II) Test Method:



50 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 15



**********************************************************************TO BE CONTINUED










TESTS CONDUCTED

PAGE 6 OF 15



Heavy Metal




**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 7 OF 15






TO BE CONTINUED



TESTS CONDUCTED

PAGE 8 OF 15

(III) Test Method:




2 ppm

Lead (Pb) content


2 ppm



2 ppm



1 ppm



5 ppm



5 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 9 OF 15



**********************************************************************

TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples




dissolved No




TESTS CONDUCTED

PAGE 10 OF 15

REMARKS:




TO BE CONTINUED



TESTS CONDUCTED

PAGE 11 OF 15








**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 12 OF 15


TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 13 OF 15






LIMIT



10 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 14 OF 15


TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 15 OF 15

**********************************************************************

END OF REPORT





PAGE 1 OF 15



SAMPLE DESCRIPTION: One (1) submitted sample said to be Grey ink. Part Description : Ink - grey. Part Number : 425909. Date Sample Received : Oct.25, 2011. Date Test Started : Oct.25, 2011. ***********************************************************************


**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 2 OF 15








**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 3 OF 15


**********************************************************************

TO BE CONTINUED


Extracted by Soxhletextraction with organic solvent


Analyze by GC-MSD





TESTS CONDUCTED

PAGE 4 OF 15







(II) Test Method:



50 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 5 OF 15



**********************************************************************TO BE CONTINUED










TESTS CONDUCTED

PAGE 6 OF 15



Heavy Metal




**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 7 OF 15






TO BE CONTINUED



TESTS CONDUCTED

PAGE 8 OF 15

(III) Test Method:




2 ppm

Lead (Pb) content


2 ppm



2 ppm



1 ppm



5 ppm



5 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 9 OF 15



**********************************************************************

TO BE CONTINUED





Cd/Pb/Hg

analyzed by ICP-OES


definite temp.


carbazide solution

Cr6+



solvent extraction


PBBs/PBDEs

analyzed by UV-VIS

analyzed by GC-MSD

spot test

get 50cm2 samples




dissolved No




TESTS CONDUCTED

PAGE 10 OF 15

REMARKS:




TO BE CONTINUED



TESTS CONDUCTED

PAGE 11 OF 15








**********************************************************************TO BE CONTINUED



TESTS CONDUCTED

PAGE 12 OF 15


TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 13 OF 15






LIMIT



10 ppm


TO BE CONTINUED



TESTS CONDUCTED

PAGE 14 OF 15


TO BE CONTINUED




Analyze by GC-MSD





TESTS CONDUCTED

PAGE 15 OF 15

**********************************************************************

END OF REPORT

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