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ICP Test Report Certification Packet
Company name : Littelfuse, Inc.
Product Series: 5x20 Fuse
Product #: 215xxxXP
Issue Date: December 3, 2012
It is hereby certified by Littelfuse, Inc. that there is neither RoHS (EU Directive 2002/95/EC,
2011/65/EU)-restricted substance nor such use, for materials to be used for unit parts, for
packing/packaging materials, and for additives and the like in the manufacturing processes.
In addition, it is hereby reported to you that the parts and sub-materials, the materials to be used
for unit parts, the packing/packaging materials, and the additives and the like in the manufacturing
processes, are all composed of the following components.
Issued by:
(1) Parts, sub-materials and unit parts
This document covers the 5x20 Fuse RoHS-Compliant series products manufactured by
Littelfuse, Inc.
< Raw Materials Used
Please see Table 1
(2) The ICP data on all measurable substances
Please see appropriate pages as identifed in Table 1
Remarks:
Form 585-047 Rev. A 2/21/06
2
Table 1: List of Raw Materials covered by this report Total Parts Raw Material Part Number Raw Material Description Page(s)
1 C910510/ 910-553 Cap (Copper Shell)
Base & Plating 3-6
2 910-556 Cap Base
Cap Plating 7-10 11-13
3 YJ50/YJM (909-449) Ceramic Body 14-24
4 11-0595 (082xxx) Tinned Wire – Cu99.9MSn 25-31
5 0042xx Tinned Wire – Cu Clad (CuNi44 Sn) 32-38
6 687xxx-001 Silver Plated Wire- Ag-Cu Sn Plated 39-44
7 648901 Yarn 45-53
8 YT-09 (195116) Flux 54-68
9 YTW102 (692539-002) Solder 69-73
10 YTW206 (692529) Solder 74-78
11
C030204, 934-073, 934-077, 934-078, 934-084,934-085, 934-089 C030210
Overcap – Fuses Copper Shell (base and plating)
79-82
12 EP608 (087355) HMA-Glue (Epoxy Adhesive) 83-94
13 091250 Sand Filler 95-101
14 091251 Sand Filler 102-108
15 091254 Sand Filler 109-117
16 425900 Ink-Orange 118-128
17 425901 Ink- Red 129-139
18 425902 Ink-Black 140-150
19 425903 Ink-Yellow 151-161
20 425904 Ink-Blue 162-172
21 425906 Ink-Brown 173-183
22 425907 Ink-Green 184-194
23 425909 Ink-Grey 195-205
24 425911 Ink-Violet 206-216
25 425913 Pale Blue Ink 217-227
26 C610(909-532) Ceramic Tube KER610 228-251
nov'TEST REPORT
NO.jA002E11121307'1R02 DaG:Dec.t5,2Oi1 page 1 of4Custom6i Suzhou FuHong Eteclronic IndustialCo., L6.AddT€sg: NO.89 WEIDU ROAD, WANGTINGTOWN. XIANGCHENG oIsTRIcT. sUzHoU. CHINAReport on tie subnitied samptes.id to beSample name: Copper shellModsl: /
Materlal: /D€cripiion: /Buyer: /Supplier: /
SamPle rcceiwd date: Elec.'13,2011T€dng poriod: From Dec.13,2011 lo Dec.15,2o.l1
T€lino Reou6tedAs sp€cified by client, to detemine the L€ad, Cadmium, Mercury & Hexavat€nt Chromilm content an the slbmified sampte inaccordance wilh Dircctive 200295/EC (RoHS).
Te.Uno method:
T€sling liem Measuring instrument MQLLead (Pb) IEC 62321:2008, section I rcP-oEs 2mg/kgcadmium (cd) IEC 62321:20t,3, s€clion 9 tcPoEs 2 mg/kgllercury (Hg) IEC 62321:2008, section 7 lcPoEs 2 mg/kgChromrum (Cr l'1) IEC 62321:2008, Annex B 0 o2mgkg'
---FOR FURTHER DETAILS, PLEASE REFERTOTHE FOLLOWNG PAGE(ST**'
leg-' 0.02 mg/kg reGrc lo the MQL of sampte extraction tiquid.
99!9!cis!i-When tesled as specined the submi(ed sample compli€d wilh the rcquirements of commission Decision of 18 Aug 2005amending Directive 2002/95/EC notilied undef document 2005/618/EC.
Pro,ect Leader /{bjA-L(Engine€r) J 4
lnsoected bv
,**'*''*,n-, [,[rlg-,i ti-Y\
,ffi:::j:,,44
SHENZHEnl AOVTESTINC TECHNO!OGY CO..L.TD,KUI\ISIIAI\I BRANCIi Holline86.512.5510 8000
nov.NO,: A002E11121307-1 R02
TEST REPORT
Tesled by ICP-OES
Add the digestion sotutioni thevessel is healed until the sampl€has b€€n dissolved
Weigh the sample into
F*_-l-Content (Melal substEle)
Add the digeslion solutjon, ctose
the micfowave ves:€|.
F;;1.-and l\Iercury Content (Plaling)
To Detenn exavalenl Chromium Content (bojting- wateF extraction): (Metat substrate)
The sample is digesred in the
mrcrowave oven iollowing a sp€citic
decomposilion program.
Tesl lh€ s€mple solution and the 0.02mg/kg standard solution by UV-VIS.
Hotline86-512-5510 8000
To
+Cooling the vessel, fltet washed and
filled to the ma* with distilled wat€r.
Remove the sample, and coolthe beaker to room lemperature,and do the color leadion
sample in the beaker.Heat 50 mL of Dl waler in the
beaker to boiling ior 10 min
To Delemine
___+l coorins. rirtei washed and lilled l_-_----|l resteo oy l+fl_*lI
t o t he ma*w i th D twa te r . I l r n " r ,u rn "n , I l " * ' I
SHENZHsN AOV TG6TING ICCHITOI"OGY CO.,L'O.KUNAHAN BRANCH a
nov'NO.i 4002E11121307-rR02
5. To O€temine Hexavalent Chromium
,':"j":::i v^02
Place 1-5
TEST REPORToste:oec15,2011
Contentin colorless and cotorcd cnromaE coating on metats(Plaljng)
5 2 Eoiling- wat6F extraction
Tako the (50+5) cm'?
sample in the beaker.
S!IENZHEN AOV'CSTING IECIINOIOGY CO..ITD,KUNSHAN gNANCH Hotlinea6-512-5510 8000
lf the tesl rcsult is posilive,
the sample is considercd tohave hexavalenl chromilm
Compare the
and lhe 0.02 mg/(qstanda.d solution
Eoiling- wateF ext€ctjonprccedurc shall be used to
lfthere is int€rference or it is hard to decide whetherthe sampl€ have tie h€xavatent chromium
Remove tie sample, and cool
lhe beaksr to room tempeEture,
and do the color reaolion
Heat 50 mlof Dlwaier in the
beaker lo boiling for 10 min
Test the sample solution and the 0.02mg/kg standard solution by UV,VIS.
T€t Re6ult3:
Unit RoHS
Limil
Result
Substrate Plating'
Lead (Pb) mg/Kg 1000 N.O. N.O.Cadmium (cd) mg/Kg 100 N.D, N.D.lvercury (Hg) mgn(]s 1000 N.D. N.D.chromium (Crl'I) mg/Kg 1000 Negalive Negative
nov-TEST REPORT
NO 4002E11121307.rR02
'The new RoHS directive 201 1/65/EU, on Jul. 21 , 201 1 come into lorce on Jan. 03, 20 1 3 the fomat imptementation. Direclive2002,95/EC shall be rcpeated simuttaneousty.
-specimens, which requested to determine Lead, cadmium and l,rercury conteni, have been dissorved comprererv
-N.D.=not detected(
GTI #,ffiffi,HTest Report
Report No. RLSZE0o1492l00002
Applicart DONGGUAN CITY XNHAI METAL PRODUCTS CO.'LTD
Address I 'ST WEIMING ROAD HENGZENG AV.XINAN COMMUI"IIryTOWN DONGGUAN CITY GUANGDONG PROVINCE
The following samplqs) and samPle informttion wavwere submitt€d rnd idbehaH of the clientSample NameMateridlSample Received DateTesting Period
T€st Requ€st€d
T€st Method
As specified by client, to test Lead(Pb), Cadrnium(Cd),Hexavalent Chromium(Cr(Vl)) in the submitted sample(s).
Test Result(s) Please refer io the following page(s).
age I of4
GAN
by/on the
lc
033098
Glnfdd&Chil
a
BASE OF CAPBRASS H65Nov. 16,2012Nov. 16, 2012 to Nov. 19, 2012
Di.d !y
Appt@dR
c!!rnE rEslrNg INrEtNAlloNAl cottonNlol{comot.r4lc6ti D755,33tSii'ra cdmplsrn1E ft sll- .orip s ll@cx'e ftn
Rcvicr€d by
DdcNov. 19,
No. I
Cdlldi€Iffi (S*)Co-Lrt Eofi,li LinNlti{ Zfla BD'a ru Dntrrt
@4 0 0 - 0 7 8 E . 3 ! 3
IEC 62121:2008 Ed.l Sec.9
IEC 612r:2008 Ed.l S€. 9
IEc 62321:2008 Ed.t Sec-7
IEC 62121:2C108 Ed.l Annex B
picL L
$6i.d ttu4!.
GTI
cl{ra[ r
I F_}'H.mrylTest RePort
Report No. R1S2E001492100002
T€rr R€rrlt(sl
Page 2 of4
Tested ltem(s) Result
Lead(Pb) 13 mgllg
Cadmium (Cd) N.D.
Mercury(Hg) N.D,
Hexavalent Chrom ium(c r(v l)) Negative
Tested Sample/Part D€scriptioD Metal base
Note: The sample had bden di,csolved totally tested for Lead, Cadmium'-MDL = Method Detection Linit-N.D. = Not Detected (
o
GTI F_i,H"m,m
Report No RIS2E001492100002
Test Process
1. Lmd(Pb),Cadmiun(cd)
2, Mercury(Hg)
3. Hexavalent Chromiun(C(Vl))
Test Report
ctuTtt t !st | o rNlElr lal toNAL cottolal lof lconormLnrcr l l 0755-!36S:7i0 Compi:r .r E_m6r .4mcir rr t t . l ' ren c 'n
Page 3 of4
@.iif;".,,,
Weigh saraple ed place it m amicrowave digE'stion ves s el
Sdecl a test sallplc
m.aswing about 50t5cnf
AElyred ty UV-V1s
a
GTI #,mffi,^)#Test Report
Report No. RLS2E001492100002
Photo(s) of the sample(s)
*** End of rcport ***
The test aeport is effective only with both signatue and sp€cialized stamp. The result(sreport refer only to the sarnple(s) tested. Without written approval of CTI, thisreDroduced exceDt in full.
Pag. 4 of 4
shown in thiscan't be
ccNlaE ta i r |NG tNlERNAlto l tA l co l to l^r ioNComorarnr carr 0755-33681100 Complsrn l E-r3r l conpia 'urdcI Nen com E n ra , , . , ' i i , . i . f l i Ld
O;';;,;",,,.,,,
a
GTI #,HMJ"M
Sample Received DateTesting Period
T€st Requested
Test Mothod
Test ReportReport No. RLSZE001492I0O00I
Applicant DONGGUAN CITY XINHAI METAL PRODUCTS CO.,LDAddress I 'ST WEIMING ROAD HENGZENG AV.XINAN COMMLINITY
TOWN DONGGUAN CITY CUANGDONG PROVINCE
The following samplqs) and sample informatiotr was/were submitted andbehalf of the clientSample Name SILVER COLOR PLATING OF CAPMaterial El€ctrolytic Nickel
Page I of3
by/on the
Nov. 16;2012Nov. 16, 2012 to Nov. 19, 2012
As specifled by client, to test Lead(Pb), Cadmium(cd),Hexavalent Chrcmium(Cr(Vl)) in the subrnitted sample(s).
T€st Resul(s) Please refer to the following page(s).
elclliod by
4rt ov.dty
Rrvi.&dby
D& Nov. 19,
No. I
a
1033098
Cd!f!di! I@bd (Sedd Co-bf Ea8wdbtil Zoc Bs'- ToDitti:t' Cu-fiL.& 6na
cIt l rE ra5TrN6,NlEtNArroNl! cotPol^l lo l lcodpLi hr cari 0 7 55-l3li I I / i)0 c ompld ril E -fi3r1 I cohpia rl@cl' ce.l .ofr
.a00.6t t6- ! l l
T€st Itein(s)
Ref€r to IEc 62321:2008 Ed.t
R€fer to IEc 62321:2008 Ed.l
Refe. to IEC 62321 :2008 Ed. I
IEC 62321:2008 Ed.l Annex B
teic.l ltu|gr.
E 03 ! { 4? . r r c f l i n n
o
GTI lt.)m.ffiirmTest Report
Report No. RLSzE001492l0000l
Test€d Sample/Prrt Desc ption silvery plating
Not€: The wasb€d plrtirg had beon dissolv€d totally test€d for Lead,Mercury.-MDL = Method Detection Limit-N.D. = Not Detected (
o
GTI #-),m.ffi^'Y!Test Report
Report No. RLSZE00I492I00001 P€e3o f3
Photo(s) ofthe sample(s)
+** End of repon ***
The t€st rcport is elfective onty with both signature and specialized stamp. The shown in thisreport ref€r only to the samplds) test€d. Witlod witten apProval of CTl, thisreorcduced exceot in full.
can't be
ct,{nt f t l f l tG rNIElr{ArrotrAt cot?olAI loNcanro aLnl cair !f55-3308r fao lompla'nl E m$l coc'piii rlrc].l' ce1l c.rr
,aa 0 0 - 6 1 8 8 . 1 3 3
scsI
Test ReportPOLYFIL AGOBERALLMENDSTMSSE 2OA,
was/w6re submitted and identified by/on behalfofthe client as:
Validit nownForQueStiPlease Co ith scs
No. : CE/2011/84950 D e | 2011112101
CH€3OO ZUG / SWITZERLAND
Cu99.9MSn'1'14595
2011t1lt25201 1t11/25 rO 201I |1',01
Page: 1 or 7
rr|| [ltt!|||tlt[t
The following sample(s)
S€mple DescriptionBuyer/Order No.Sample Receiving DateTesting Period
lest Result(a) Plea6eefer to next page(s).
prqt iadsd Ds Gn ,epd eind bComFiy -r ,: !;t lLr. . . i ; l :r l i l l{ i l rt lrd r qti ' r^rl l i9i: l+,11\- em+,i , -,:r. ift",rl.
.ysuq8d b b cs€rcond rbns d ssubrd lo Tems ad cd@ l.l:
o n L y a i d w l h L n h . t m B d c | € d l n !
E d ftr|tld
clsnH L.Do'|b.t - Trhd
Test ReportPOLYFILAGOBERALLI\4ENDSTRASSE
T66i R.6ultls)
PART t.lAME No.1
No.: CE/2011/84950 Dale :2O114ZO1
2OA, CH63OO ZUG / SWITZERLAND
Page'.2 of 7
t I] t l
SILVER COLORED METAL WIRE (INCLUDING THE PLATING LAYER)
Te3t lt6m(s) Unit Method MDLR.3ultNo,l
Cadmium (Cd) mg/KgWith reterence to IEC 62321r 2008 andperfomed by ICP-AES.
n.d.Lead (Pb) mgKg 24Mercury (Hg) mS/kS n.d.Hexavalent Chromium Cr(Vl) With reference to IEC 62321: 2008 and
pedormed by Boiling \r€ter ext€ctionMethod.#
Negative
Sum of PBBS
mgikS With reference to IEC 62321: 2008 andperfomed by GC/MS.
n.d.Monobromobiphenyl 5 n.d.Dibromobiphenyl 5 n.d.Tribromobiphenyl 5 n.d.Tetrabromobiphenyl 5 n.o.Pontabromobiphenyl n.d,Hexabrcmobiphenyl 5 n.o.Heptabromobiphenyl n.d.Octabromobiphenyl 5 n.d.Nonabrornobiphenyl 5 n.d.Dec€bromobiphenyl 5 n .d .Sum of PBOEa n.d.Monobromodiphenyl ether n.d.Dibromodiphenyl ether 5 n.o.Tribromodipheny! ethe. 5 n.d.Tetrabromodiphenyl ether n.d.Pentabromodiphenyl ether n.d.Hexabrcmodiohenvl ether 5 n.d.Heptabromodiphenyl ether 5 n.o,Octabromodiphenyl ether n.o,Nonabromodiphenyl ether 5 n.d.Decabromodiphenyl ether 5 n.d.
eGlG{d rh s ied @d €nrclb Bpdcn€ry 'l+ !r ! rlrl . .n 1!ts,:r1,rtilr. ;l'!l* rrn . imri+Al'r-\r jrl4.f4! 1r€11hsdocmdssdby'h€c.mpany&bldlobcffi6|codibGo's*to. e.d'mc romal dmstu suq
d ^ t ' n d w l h L n h r m B d c r . d ! n d p o B d r t s t o G c s r a n d r h 3 d Mldrrgh6add]Ed'on6un6lh6'm
t',i!r: :d, dri:_ 11rs6rorPre
Test Report No. : CE/2011/84950 Date | 2011h21O1 Page: 3 of 7tl]tIlltltfltttltPOLYFILAG
OBERALLMENDSTRASSE 2OA, CH€3OO ZUG / SWITZERLAND
Test ltem(s) Unit method MDL ResultNo.1
HalogenHalogen-Fluorine (F)(CAS No.: 14762-94-8)
mg/Kg With reference to BS EN M5A2,2007.Analysis was perfomed by lC.
50 n,o,
HalogenChlodne (Cl)(CAS No.: 22537-1s1)
50 n.d.
Halogen-Brcmine (Br)(CAS No.r 10097-32-2)
50 n.d.
Halogen-lodine (l)(CAS No.i 14362-44-8)
50 n.d.
Note :1. mg/kg = ppm : 0.1wf/6 = 1o00ppm2. n.d. = Not Detected3. MDL = Method Detection Limit4 - " - "=No tRegu la led5. '" = Qualitative analysis (No unit)6. # = a. Positive means the presence of CrVl on the tested areas
b. Negative mgans the absence of C l on the tested areasThe dgteci€d concentration in boiling-lvater-ext€ction solution is equalor greaterthan 0.02 mg/kg with 50 cm,tested areas.
7. The sample(€) was/wer6 analyzed on behalfof the applicant as mixing sample in one testing. The above result(s)was^^/€re only giv€n as the informality value.
'nrhstar€Fnd€f ontrorbsmpq3)Idd rhEbd,etsn6ndbGComFny f l t r , l r i 9 ! r . , r l i ] l : r r ! l { : : l : : ; l i ' ! i : l j i A r i i F -5 ! , [ 1 ' e t r ; ' f ' , , ' l ] l t ) [ l i 1 'n3dumd ts6su6d ' l hscomtsny5u*db t csccond1 t r sds
sib iv 6 10 6 o er 5d b6 @mntft,ltrrsandd odd3undrth€ta mol & €pdud depr 'n ju r, ftd
+l r l *J l : r (+s610r ) re t7e f +sitlfuirL!{:,r rr ir: i - i.hsror IlF
Test Report No. : CE201'1/84950 OaL .2011h2,01 Pager 4
according to belo\ / flo /
POLYFILAGOBERALLMENDSTRASSE 2OA, CH63OO ZUG / SWITZERLAND
1) These sample6were da66olved totally by pre-conditioning methoda Cf' test method excluded )
Name of the pe6on who made measurement: Climbg€at YangName ofthe pe6on in charge of measurement: Troy Chang3)
ICP-AES
Sample Material Dige€tion Acid
S1eel, copper, aluminum, sold€r Aqua regia, HNO3, HCl, HF, HrO,
Glass HNO3/HF
cold, platinum, palladium, ceramic Aqua regia
Silver HNO3
Plastic H2SO1, HrOr, HNq, HCI
Othe.s Any acid to totral digestion
ii. irei,.or if *q oy t . cop-r " ,g .oo-maa"J ' * .6b i " - ' *dco^d ' * "6 .Edrcn ico@isbdM!os@]bi.*ddb" -'d l,nsdd 6 *,* i5r
*l iq:i";* @"* -;d.." **o.ooissr,s.ry - r"
"rd;^ a * -nd .
rtf:r:: r1lirtii+ 1l i s6 io,t,e tTe t r s lo:)2e 'r7 ffiar(om
Acid digestion by suitable aciddepended on difierent samplemderial (as belo\ , iable)
Micro\rave digestion with
HNO/HCVHF
Heat to appropriat€
temperature to e,\tract
Cool, filter digestate
through filter1) Alkal iFusion2) HCltodissolve
at 540 nm by UV-VIS
Test ReportPOLYFILAGOBERALLI\4ENDSTRASSE 2OA,
No. : CE2011184950 Oale'. 201 lh2lo1
CH43OO ZUG / SWITZERLAND
Page: 5 of 7
t l | l [ ] | | I t t | l
PBB/PBDE1) lllanE of the person2) MnE of the person
analytical FLOW cHARTwho nEde npasurenEnt: Ronran Wongin charge of nEasurenent Troy Chang
Scrcen analysis
" " " " " 1 " " " " " "
Sanple extraction/So*rlet rEthod
ConcentratdDiluteE)dracbd solution
First testing process -----t
Optional screen process -.--
Confinmtion process - .>
-s."pb---_-]--------r-------[S-r-tp]-j-a"arn"-_l-----r----
Ft ler
Analysis by GC/liS
cm€ry r r ' r j l j r ) t r . : r i l i " . : . l ! i * i , ; i i l ' r l t : e l . t i l : i l r t / . 1 \ ' l r Fn . r ' j : 1 . ' t l 6+
to €sd'o'c ramd dm6tu suq
d^t ,nd vihin rb rmis ot cr€d s i3'lbr.ohbadd€donsu.ddsera od b. repdued eiceol itul wiher
! idsnrzorNe-tu!acirrrer/*l:r/f,!.r +!!4J1i:irlre 02)r!e
I
Test ReportPOLYFIL AGOBERALLMENDSTRASSE
No. : CE/2011/84950 Daie | 2011h21O1
2OA. CH-6300 ZUG / SWITZERLAND
Analytical flow chart of halogen content
1) Name of the p€rson who lmde rneasuredEntr Rita Chen2) llan€ of the person in charge of nEasurerEdt: Troy Chang
Page: 6 of 7
comoad N]r]F,j!:ir.. I tiir lt{!l; ;]]rltl.1!- . r. irtsih-{} I 11 FiT . f!l r19i!+l
fi"JHl"l;liiii',i!',i.iwi;c"ry"';ti"-"c*""tc"t.^a sriu*-t i*n d..",; ''jbl.n bi... .d c.d*" 6, €. a " ' ' i i a - - o e , " a a . ^ * * ' ; . n b a d " i s d l b d i b m a i o ; d k . d h ;
; ; ; q ; ; ; ; oo ,4a t ; . : 6 . ? .€6@- -hsd ; "db . - "b1 .
r L - I I i d l L a i
Sarple pretreatrnent / Separation
Weighting and putting safipte in cell
Orygen Bomb Cofibustion / Absorption
Dilution to fixed volurne
Analysisw€s perfornEd by lC
Test Report No. : CE/2011/84950 D€te 2011h2101 Paget 7 of 7tl] tlt II][]lPOLYFILAG
OBEMLLMENDSTRASSE 2OA, CH63OO ZUG / SWITZERLAND
* The teeted sample / pa is maaked by an arrow if ifs shown on ih€ pholo. '
" End of Report -
€(s) r6rd Th€ r6d rop.n @nd b rccomtsry rirl,,iirar.rr'ir,'r,:111!!1, iilrRj:itr r.il1' l:!11.!-em+iI, ra r';)n:ll 'Thsih{.d"**dbylh6c"np.nysub'db6G4€Ejcond1bngo{sld ,M6.6al &dmsfu' sub]rendir,e'@ d ru d dbn s€s ibrh€! n reieds rhe cmp8.r's t ndn$ 3r rhe-y .d fu " t h " i . 6dc " " c ' * dDc . {5ny r ' j e cdnF i ys9s . s$;nshisandobroa,o3@do,rbta mdsrepd@sxepr'nlu.wM,sio,MtenaFro!3 drhecompanv a
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00300774
PREPARED AND CHECKED BY: AUTHORIZED BY: FOR INTERTEK TESTING SERVICES FOR INTERTEK TESTING SERVICES LTD., SHANGHAI LTD., SHANGHAI
MYRA LV JACOB LIN CHEMICAL LAB SENIOR MANAGER GENERAL MANAGER
PAGE 1 OF 7
APPLICANT: LITTELFUSE,INC. DATE: FEB 02, 2012 800 E. NORTHWEST HWY ATTN: A. CESISTA/ K. BACILA
SAMPLE DESCRIPTION: One(1) submitted sample said to be Wire with plating. Part Description : Wire(Elschukon). Part Number : 004206. Date Sample Received : Jan.17, 2012. Date Test Started : Jan.17, 2012. ***********************************************************************
TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
**********************************************************************TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00300774
TESTS CONDUCTED
PAGE 2 OF 7
(Ⅰ) Test Result Summary :
Result (ppm) Testing Item
(1)
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content 20 Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg with 50cm2)
Negative (< 0.02)(#)
Result (ppm)
Testing Item (2)
Heavy Metal
Cadmium (Cd) content/PLATING ND Lead (Pb) content/PLATING 238 Mercury (Hg) content/PLATING ND Chromium VI (Cr6+) content (mg/kg with 50cm2)/PLATING
Negative (< 0.02)(#)
Tested components:
(1) Substrate (2) Plating
Remarks: ppm = Parts per million = mg/kg ND = Not detected # = Due to the insufficient sample area, reduced total
sample surface of 10 cm2 was used and the dilution factor was adjusted accordingly.
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation was not found at the time of testing.
Responsibility Of Chemist :Dent Fang / Ken He **********************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00300774
TESTS CONDUCTED
PAGE 3 OF 7
(Ⅱ) RoHS Requirement: Restricted Substances Limits Cadmium (Cd) Content 0.01% (100ppm)Lead (Pb) Content 0.1% (1000ppm)Mercury (Hg) Content 0.1% (1000ppm)Chromium VI (Cr6+) Content 0.1% (1000ppm)Polybrominated Biphenyls (PBBs) 0.1% (1000ppm)Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. **********************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00300774
TESTS CONDUCTED
PAGE 4 OF 7
(Ⅲ) Test Method:
Testing Item Testing Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer.
0.02 mg/kg with
50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample
Date Sample Received :JAN.17, 2012 Testing Period :JAN.17, 2012 TO JAN.21, 2012 **********************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00300774
TESTS CONDUCTED
PAGE 5 OF 7
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard: IEC 62321 edition 1.0:2008
**********************************************************************TO BE CONTINUED
sampling/grinding or cutting
weigh sample and for different
material, digest the sample with
make up with deionized water
Cd/Pb/Hg
analyzed by ICP-OES
weigh sample and add alkaline solution
definite temp.
make up with deionized water and add diphenyl-
carbazide solution
Cr6+
weigh sample and add organic
soxhlet extraction or
solvent extraction
concentrate the extract and make up with organic
PBBs/PBDEs
analyzed by UV-VIS
analyzed by GC-MSD
spot test
get 50cm2 samples
boiling water extraction
metalpolymers / electronics
negative*2confirm the tested samples are totally
dissolved No
cool and filter the extract
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00300774
TESTS CONDUCTED
PAGE 6 OF 7
REMARKS:
*1: List of appropriate acid: Material Acid added for digestion
Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
**********************************************************************TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00300774
TESTS CONDUCTED
PAGE 7 OF 7
**********************************************************************
END OF REPORT
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00300757
PREPARED AND CHECKED BY: AUTHORIZED BY: FOR INTERTEK TESTING SERVICES FOR INTERTEK TESTING SERVICES LTD., SHANGHAI LTD., SHANGHAI
MYRA LV JACOB LIN CHEMICAL LAB SENIOR MANAGER GENERAL MANAGER
PAGE 1 OF 6
APPLICANT: LITTELFUSE,INC. DATE: FEB 02, 2012 800 E. NORTHWEST HWY ATTN: A. CESISTA/ K. BACILA
SAMPLE DESCRIPTION: One(1) submitted sample said to be Wire with plating. Part Description : Wire(Polyil). Part Number : 687279-001. Date Sample Received : Jan.17, 2012. Date Test Started : Jan.17, 2012. ***********************************************************************
TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
*********************************************************************** To Be Continued
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00300757
TESTS CONDUCTED
PAGE 2 OF 6
(Ⅰ) Test Result Summary :
Result (ppm) Testing Item
(1)
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content (mg/kg with 50cm2) Negative (< 0.02)(#)
Result (ppm)
Testing Item (2)
Heavy Metal
Cadmium (Cd) content/Plating ND Lead (Pb) content/Plating 72 Mercury (Hg) content/Plating ND Chromium VI (Cr6+) content (mg/kg with 50cm2)/Plating
Negative (< 0.02)(#)
Tested components:
(1) Substrate (2) Plating
Remarks: ppm = Parts per million = mg/kg ND = Not detected # = Due to the insufficient sample area, reduced total
sample surface of 10 cm2 was used and the dilution factor was adjusted accordingly.
mg/kg with 50cm2 = milligram per kilogram with 50 square centimetre
Negative = A negative test result indicated positive observation was not found at the time of testing.
Responsibility Of Chemist :Dent Fang / Ken He
Date Sample Received :Jan.17, 2012 Testing Period :Jan.21, 2012 ***********************************************************************
To Be Continued
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00300757
TESTS CONDUCTED
PAGE 3 OF 6
(Ⅱ) RoHS Requirement: Restricted Substances Limits Cadmium (Cd) Content 0.01% (100ppm)Lead (Pb) Content 0.1% (1000ppm)Mercury (Hg) Content 0.1% (1000ppm)Chromium VI (Cr6+) Content 0.1% (1000ppm)Polybrominated Biphenyls (PBBs) 0.1% (1000ppm)Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material.
(Ⅲ) Test Method:
Testing Item Testing Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex B, by boiling water extraction and determined by UV-Vis spectrophotometer.
0.02 mg/kg with
50cm2
Remark: Reporting limit = Quantitation limit of analyte in sample ***********************************************************************
To Be Continued
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00300757
TESTS CONDUCTED
PAGE 4 OF 6
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard: IEC 62321 edition 1.0:2008
*********************************************************************** To Be Continued
sampling/grinding or cutting
weigh sample and for different
material, digest the sample with
make up with deionized water
Cd/Pb/Hg
analyzed by ICP-OES
weigh sample and add alkaline solution
definite temp.
make up with deionized water and add diphenyl-
carbazide solution
Cr6+
weigh sample and add organic
soxhlet extraction or
solvent extraction
concentrate the extract and make up with organic
PBBs/PBDEs
analyzed by UV-VIS
analyzed by GC-MSD
spot test
get 50cm2 samples
boiling water extraction
metalpolymers / electronics
negative*2confirm the tested samples are totally
dissolved No
cool and filter the extract
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00300757
TESTS CONDUCTED
PAGE 5 OF 6
REMARKS: *1: List of appropriate acid:
Material Acid added for digestion
Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected.
*********************************************************************** To Be Continued
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00300757
TESTS CONDUCTED
PAGE 6 OF 6
***********************************************************************
End Of Report
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299962
PREPARED AND CHECKED BY: AUTHORIZED BY: FOR INTERTEK TESTING SERVICES FOR INTERTEK TESTING SERVICES LTD., SHANGHAI LTD., SHANGHAI
MYRA LV STEPHEN TSANG CHEMICAL LAB SENIOR MANAGER GENERAL MANAGER
PAGE 1 OF 9
APPLICANT: LITTELFUSE,INC. DATE: JAN 18, 2012 800 E. NORTHWEST HWY ATTN: A. CESISTA/ K. BACILA
SAMPLE DESCRIPTION: One(1) submitted sample said to be White yarn. Part Description : YARN. Part Number : 648901. Date Sample Received : Jan.11, 2012. Date Test Started : Jan.11, 2012. ***********************************************************************
TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
**********************************************************************TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299962
TESTS CONDUCTED
PAGE 2 OF 9
1 (I) Test Result Summary :
Testing Item Result (ppm)
Halogen Content Fluorine (F) 820 Chlorine (Cl) ND Bromine (Br) ND Iodine (I) ND
Remarks: ppm = Parts per million based on weight of tested sample =
mg/kg ND = Not detected
Responsibility Of Chemist :Ken He
(II) Test Method:
Testing Item Testing Method Reporting Limit
Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample **********************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299962
TESTS CONDUCTED
PAGE 3 OF 9
(III) Measurement Flowchart:
Test For Halogen Content Reference Standard: EN 14582
**********************************************************************TO BE CONTINUED
add absorbent in a combustion flask & place weighed sample in equipment
fill the combustion flask with oxygen
ignite then leave the flask at room temperature
transfer the absorbent into a volumetric flask
make up with deionized water
sampling/grinding or cutting
analyzed by ion chromatography
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299962
TESTS CONDUCTED
PAGE 4 OF 9
2 (I) Test Result Summary :
Testing Item Result (ppm)
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
**********************************************************************TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299962
TESTS CONDUCTED
PAGE 5 OF 9
Remarks: ppm = Parts per million = mg/kg ND = Not detected
Responsibility Of Chemist :Dent Fang / Ken He
(II) RoHS Requirement:
Restricted Substances Limits Cadmium (Cd) Content 0.01% (100ppm)Lead (Pb) Content 0.1% (1000ppm)Mercury (Hg) Content 0.1% (1000ppm)Chromium VI (Cr6+) Content 0.1% (1000ppm)Polybrominated Biphenyls (PBBs) 0.1% (1000ppm)Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. **********************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299962
TESTS CONDUCTED
PAGE 6 OF 9
(III) Test Method:
Testing Item Testing Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample
DATE SAMPLE RECEIVED : JAN.11, 2012 TESTING PERIOD : JAN.11, 2012 TO JAN.13, 2012
**********************************************************************TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299962
TESTS CONDUCTED
PAGE 7 OF 9
(IV) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard: IEC 62321 edition 1.0:2008
**********************************************************************
TO BE CONTINUED
sampling/grinding or cutting
weigh sample and for different
material, digest the sample with
make up with deionized water
Cd/Pb/Hg
analyzed by ICP-OES
weigh sample and add alkaline solution
definite temp.
make up with deionized water and add diphenyl-
carbazide solution
Cr6+
weigh sample and add organic
soxhlet extraction or
solvent extraction
concentrate the extract and make up with organic
PBBs/PBDEs
analyzed by UV-VIS
analyzed by GC-MSD
spot test
get 50cm2 samples
boiling water extraction
metalpolymers / electronics
negative*2confirm the tested samples are totally
dissolved No
cool and filter the extract
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299962
TESTS CONDUCTED
PAGE 8 OF 9
REMARKS:
*1: List of appropriate acid: Material Acid added for digestion Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected. **********************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299962
TESTS CONDUCTED
PAGE 9 OF 9
**********************************************************************
END OF REPORT
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
PREPARED AND CHECKED BY: AUTHORIZED BY: FOR INTERTEK TESTING SERVICES FOR INTERTEK TESTING SERVICES LTD., SHANGHAI LTD., SHANGHAI
MYRA LV STEPHEN TSANG CHEMICAL LAB SENIOR MANAGER GENERAL MANAGER
PAGE 1 OF 15
APPLICANT: LITTELFUSE,INC. DATE: JAN 18, 2012 800 E. NORTHWEST HWY ATTN: A. CESISTA/ K. BACILA
SAMPLE DESCRIPTION: One (1) submitted sample said to be Orange Liquid. Part description : FLUX. Part number : 195116. Date sample received : Jan.11, 2012. Date test started : Jan.11, 2012. ***********************************************************************
TESTS CONDUCTED: AS REQUESTED BY THE APPLICANT, FOR DETAILS REFER TO ATTACHED PAGE(S)
*********************************************************************** TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
PREPARED AND CHECKED BY: AUTHORIZED BY: FOR INTERTEK TESTING SERVICES FOR INTERTEK TESTING SERVICES LTD., SHANGHAI LTD., SHANGHAI
MYRA LV STEPHEN TSANG CHEMICAL LAB SENIOR MANAGER GENERAL MANAGER
PAGE 2 OF 15
CONCLUSION:
TESTED SAMPLE/ COMPONENT
STANDARD RESULT
TESTED COMPONENT OF SUBMITTED SAMPLE
PHTHALATES CONTENT REQUIREMENT IN ANNEX XVII ITEMS 51 & 52 OF THE REACH REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009(FORMERLY KNOWN AS DIRECTIVE 2005/84/EC)
PASS
TESTED SAMPLE/COMPONENT STANDARD RESULT
TESTED COMPONENT OF SUBMITTED SAMPLE
US CONSUMER PRODUCT SAFETY IMPROVEMENT ACT 2008 TITLE I, SEC 108 REQUIREMENT ON PHTHALATES
PASS
**********************************************************************
**********************************************************************
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
TESTS CONDUCTED
PAGE 3 OF 15
1 PHTHALATE CONTENT TEST
WITH REFERENCE TO EN14372, BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY (GC-MS) ANALYSIS.
LIMIT(%,W/W) TESTED COMPOUND RESULT (%,W/W)
(MAX.) DIBUTYL PHTHALATE (DBP) ND --- DI(2-ETHYL HEXYL) PHTHALATE(DEHP) ND --- BENZYL BUTYL PHTHALATE (BBP) ND ---
SUM OF THREE PHTHALATES ND 0.1
REMARK:THE ABOVE LIMIT WAS QUOTED ACCORDING TO ANNEX XVII ITEMS 51 & 52 OF THE REACH REGULATION (EC) NO. 1907/2006 & AMENDENT NO.552/2009 (FORMERLY KNOWN AS DIRECTIVE 2005/84/EC) FOR PHTHALATE CONTENT IN TOYS AND CHILDREN CARE ARTICLES.
DETECTION LIMIT = 0.01%(W/W) ND = NOT DETECTED
*********************************************************************** TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
TESTS CONDUCTED
PAGE 4 OF 15
2 (Ⅰ) Test Result Summary :
Result (ppm) Testing Item
Halogen Content Fluorine (F) ND Chlorine (Cl) 8200 Bromine (Br) ND Iodine (I) ND
Remarks: ppm = Parts per million based on weight of tested sample =
mg/kg ND = Not detected
Responsibility Of Chemist :Ken He
(Ⅲ) Test Method:
Testing Item Testing Method Reporting Limit
Halogen Content With reference to EN 14582:2007 by combustion flask with oxygen and determined by ion chromatography
50 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample **********************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
TESTS CONDUCTED
PAGE 5 OF 15
(Ⅳ) Measurement Flowchart:
Test For Halogen Content Reference Standard: EN 14582
**********************************************************************TO BE CONTINUED
add absorbent in a combustion flask & place weighed sample in equipment
fill the combustion flask with oxygen
ignite then leave the flask at room temperature
transfer the absorbent into a volumetric flask
make up with deionized water
sampling/grinding or cutting
analyzed by ion chromatography
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
TESTS CONDUCTED
PAGE 6 OF 15
3 (Ⅰ) Test Result Summary :
Testing Item Result (ppm)
Heavy Metal
Cadmium (Cd) content ND Lead (Pb) content ND Mercury (Hg) content ND Chromium VI (Cr6+) content ND
Polybrominated Biphenyls (PBBs) Monobrominated Biphenyls (MonoBB) ND Dibrominated Biphenyls (DiBB) ND Tribrominated Biphenyls (TriBB) ND Tetrabrominated Biphenyls (TetraBB) ND Pentabrominated Biphenyls (PentaBB) ND Hexabrominated Biphenyls (HexaBB) ND Heptabrominated Biphenyls (HeptaBB) ND Octabrominated Biphenyls (OctaBB) ND Nonabrominated Biphenyls (NonaBB) ND Decabrominated Biphenyl (DecaBB) ND
Polybrominated Diphenyl Ethers (PBDEs) Monobrominated Diphenyl Ethers (MonoBDE) ND Dibrominated Diphenyl Ethers (DiBDE) ND Tribrominated Diphenyl Ethers (TriBDE) ND Tetrabrominated Diphenyl Ethers (TetraBDE) ND Pentabrominated Diphenyl Ethers (PentaBDE) ND Hexabrominated Diphenyl Ethers (HexaBDE) ND Heptabrominated Diphenyl Ethers (HeptaBDE) ND Octabrominated Diphenyl Ethers (OctaBDE) ND Nonabrominated Diphenyl Ethers (NonaBDE) ND Decabrominated Diphenyl Ether (DecaBDE) ND
**********************************************************************TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
TESTS CONDUCTED
PAGE 7 OF 15
Remarks: ppm = Parts per million = mg/kg ND = Not detected
Responsibility Of Chemist :Dent Fang / Ken He
(Ⅱ) RoHS Requirement: Restricted Substances Limits Cadmium (Cd) Content 0.01% (100ppm)Lead (Pb) Content 0.1% (1000ppm)Mercury (Hg) Content 0.1% (1000ppm)Chromium VI (Cr6+) Content 0.1% (1000ppm)Polybrominated Biphenyls (PBBs) 0.1% (1000ppm)Polybrominated Diphenyl Ehters (PBDEs) 0.1% (1000ppm)
The above limits were quoted from 2002/95/EC and amendment 2005/618/EC for homogeneous material. **********************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
TESTS CONDUCTED
PAGE 8 OF 15
(Ⅲ) Test Method:
Testing Item Testing Method Reporting Limit
Cadmium (Cd) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Lead (Pb) content
With reference to IEC 62321 edition 1.0:2008 in clause 8/9/10, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Mercury (Hg) content
With reference to IEC 62321 edition 1.0:2008 in clause 7, by microwave digestion until the tested samples are totally dissolved and determined by ICP-OES.
2 ppm
Chromium VI (Cr6+) content
With reference to IEC 62321 edition 1.0:2008 in annex C, by alkaline digestion and determined by UV-Vis spectrophotometer.
1 ppm
Polybrominated Biphenyls (PBBs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Polybrominated Diphenyl Ethers (PBDEs)
With reference to IEC 62321 edition 1.0:2008 in annex A, by solvent extraction and determined by GC-MSD and further HPLC confirmation when necessary.
5 ppm
Remark: Reporting limit = Quantitation limit of analyte in sample ***********************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
TESTS CONDUCTED
PAGE 9 OF 15
(Ⅳ) Measurement Flowchart:
Test For Cd/Pb/Hg/Chromium (VI)/PBBs/PBDEs Contents Reference Standard: IEC 62321 edition 1.0:2008
**********************************************************************
TO BE CONTINUED
sampling/grinding or cutting
weigh sample and for different
material, digest the sample with
make up with deionized water
Cd/Pb/Hg
analyzed by ICP-OES
weigh sample and add alkaline solution
definite temp.
make up with deionized water and add diphenyl-
carbazide solution
Cr6+
weigh sample and add organic
soxhlet extraction or
solvent extraction
concentrate the extract and make up with organic
PBBs/PBDEs
analyzed by UV-VIS
analyzed by GC-MSD
spot test
get 50cm2 samples
boiling water extraction
metalpolymers / electronics
negative*2confirm the tested samples are totally
dissolved No
cool and filter the extract
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
TESTS CONDUCTED
PAGE 10 OF 15
REMARKS:
*1: List of appropriate acid: Material Acid added for digestion
Polymers HNO3,HCl,HF,H2O2,H3BO3 Metals HNO3,HCl,HF Electronics HNO3,HCl,H2O2,HBF4
*2: If the result of spot test is positive, Chromium VI would be determined as detected. **********************************************************************
TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
TESTS CONDUCTED
PAGE 11 OF 15
(Ⅳ) Measurement Flowchart:
Test For Halogen Content Reference Standard: EN 14582
add absorbent in a combustion flask & place weighed sample in equipment
fill the combustion flask with oxygen
ignite then leave the flask at room temperature
transfer the absorbent into a volumetric flask
make up with deionized water
sampling/grinding or cutting
analyzed by ion chromatography
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
TESTS CONDUCTED
PAGE 12 OF 15
4 PHTHALATE CONTENT TEST
WITH REFERENCE TO ASTM D3421, BY GAS CHROMATOGRAPHY-MASS
SPECTROMETRY (GC-MS) ANALYSIS.
RESULT (%, w/w) LIMIT (%, w/w) (MAX.) DIBUTYL PHTHALATE (DBP) ND 0.1 DI(2-ETHYL HEXYL) PHTHALATE (DEHP) ND 0.1 BENZYL BUTYL PHTHALATE (BBP) ND 0.1
REMARK:THE ABOVE LIMIT WAS QUOTED ACCORDING TO US CONSUMER
PRODUCT SAFETY IMPROVEMENT ACT 2008 FOR PROHIBITION ON SALE OF CERTAIN PRODUCTS CONTAINING SPECIFIED PHTHALATES.
DETECTION LIMIT = 0.01% (w/w) ND = NOT DETECTED
*********************************************************************** TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
TESTS CONDUCTED
PAGE 13 OF 15
MEASUREMENT FLOWCHART: TEST FOR PHTHALATES CONTENTS
*********************************************************************** TO BE CONTINUED
Weigh sample and place in a thimble
Extracted by Soxhlet extraction with organic solvent
Concentrate the extract
Analyze by GC-MSD
Make up with organic solvent
Transfer the extract into a volumetric flask
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
TESTS CONDUCTED
PAGE 14 OF 15
5 TEST RESULT SUMMARY:
TESTING ITEM RESULT(ppm)
HBCD (HEXABROMOCYCLODODECANE) ND
REMARKS: ppm = PARTS PER MILLION = mg/kg ND = NOT DETECTED (B) TEST METHOD :
TESTING ITEM TESTING METHOD REPORTING
LIMIT
HBCD (HEXABROMOCYCLODODECANE)
WITH REFERENCE TO USEPA 3540C, BY SOLVENT EXTRACTION AND DETERMINED BY GC/MS
10 ppm
DATE SAMPLE RECEIVED : JAN.11, 2012 TESTING PERIOD : JAN.11, 2012 TO JAN.16, 2012
*********************************************************************** TO BE CONTINUED
Intertek Testing Services Ltd., ShanghaiTFH Division Block B, Jinling Business Square,No.801 Yi Shan Road, Shanghai, China, 200233 Tel: +86 21 6120 6565 Fax: +86 21 6127 9740 www.intertek.com www.intertek.com.cn China Toll-Free: 800 999 1338
TEST REPORT NUMBER: SHAH00299991
TESTS CONDUCTED
PAGE 15 OF 15
***********************************************************************
END OF REPORT
Test R€port No. SHAEC1216714750 Date: 25 Sep 2012 Page 'l ofsZHEJIANG ASIA GENERAL SOLDERING&BRAZING MATERIAL CO., LTDXIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CITY, ZHEJIANG, PROVINCE, CHINA
Thg following sample(s) was/were submitted and identifed on beharf of the dients as : LEAD-FREE soLDERWIRE
SGS Job No. :Part No. (P/N) :Composition :Date of Sample Received :Testing Period :Te6t Requested :
Test Method :
Test Results :Conclusion :
sP12-028285 - SHYTWl02 (692s39-002)
Sn2.0CuRE21 9ep 2012
21 Sep 2012 - 25 Sep 2012Selected test(s) as requested by dient.Please refer to next page(s).
Please ref€r to ne\4 page(s).
Based on the performed tests on submitted samples, lhe results of Lead,Mercury, Cadmium, Hexavalent cfiromium, polybrominated biphenyls (pBB),Polybrominated diphenylethe6 (PBDE) compty with the timib as set by RoHSDireclive 2011/6yEU Annex ll; recasting 2OO2|95/EC.
k'{l efir C.nddd.l6.rno odd- osLd, w.r.l'lr 6Mnd kt n lle u! a.Ddr'rE iq Eldimo o.uffi . w*dh,|od ..d..llfu.h-.Aldfiriirmr;iitrffia
!l|dn. rry ndr..rttr' rtr'eddr d*dihndofidd
Signed for and on b€half ofscs-cgTc Ltd.
,z?r"'-Fan Jinqjie, JJApproved Sign€tory
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ry bh rmpr.(r, rnbd .
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tn€Fa)filG60lEEiE-ArOSI9 *n.nrslcdnrllj{E-ar)6140,,0a tt{fi-21l6ao@ .tdir&lilcn
Man!6r or rh€ sqs olo!! (scs sA)
Test Report No. SHAEC1216714750 Date: 25 Sep 201 2 Page 2 of 5Test Results :
Test Part Desciiotion :
Sp€oim€n llo. SGS Sampl€ lD Dcc,ipdon1 SHA12-167147.043 Sitvery wire
RemarlG :(1) 1 mgftg= 1 PPm=0.0001%(2) IVDL = Method Detedion Limit(3) ND = Not Detected ( < l\4DL )(4) "-" = Not Regulated
RoHS Dir€divo 201 1/85/EU
Test l\rethod: With referenc€ to IEC 6232'1:2008(1) Determination ofCadmium by ICP-OES.(2) Determination of Lead by tCp-OES.(3) Determination of Mercury by |CP-OES.(4) Determination of Hexavalent Chromium by Spot test / Cotodmetric Method using UV-Vis.(5) Determination of PBBS / PBDES by GC-MS.
Te6t ltem(s)
Cadmium (Cd)
Lead (Pb)Mercury (Hg)Hexavalenl Chromium (Cr(Vl))Sum of PBBSMonobromobiphenylDibromobiphenylTribromobiphenylTetrabrcmobiphenylPentabromobiphenyl
HeptabromobiphenylOclabromobiphenylNonabromobiphenylDecabromobiphenylSum of PBDESMonobromodiphenyl ether
!!!it Ud!10O mS/kS1000 mSikg1To 'nT
1000 mdkg- mgKg
mgKg- mgKg- mgKg- mg/Kg
ms/Ksmg/Kgmg/KgmS/kS
- mgKs1000 mdkS
- meyKg
l\4DL @32 N D2 1682 N DO Negative- N D
5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D- N D
5 N D
rn .dothr,$rLbhdtuFl
i'drbdn'l''hcd'c'|i&dcmdr.& qi.r rdta dsn-r dnr ncr .|'ld Fdr b. hnr.dmm.rr.ddaDlhMllln.d'lddtl.'
c!dr-/. ndhl. .rtrrhd
h dr hi rPd Dt' cir b,h. rm, .b, hro .
.mb.r ol rh. scs Goup {8Gs€ }
t'inr$r$fedrdrr6nl,gEidaorr 2o@3]+l..t.t.lr6ldrl33oClstn ll:M
lElE{S-Al6ia02563lElEls-a!ffiIg 9w.64a.mrL{6-nl6|102ra rrlr{6-?r)5ae3 .€.d't!0.tM
Test ReportTest ltem(s)
Dibromodiphenyl etherTribromodiphenyl etherTetrabromodiphenyl etherPsntabromodiphenyl elherH€xabromodiphenyl etherHeptabromodiphenyl etherOctabomodiphenyl etherNonabromodiphenyl elherDecabromodiphenyl ether
No. SHAEC1216714750 Datei 25 Sep 2012 Page 3 of 5
Lldl udtms/Ksmg/Kgmg/rgmS/kgmg/Kgmg/Kgmg/Kgm9Kgmdkg
upt555555555
a3NDN DN DN DNDNDNDNDNO
Notes :(1) The maximum permissible limit is quoted from directive 201 1/65/EU, Annex ll(2) "spottest:
Negative = Abs€nce of Cr(Vl) coating, Positive = Presence of Cr(Vt) coating;Cfhe tested sample should be further vedfied by boiling-wateFextraction method if the spot test resultis Negative or cannot be confirmed,)o Boiling-wateFextraction:Negative = Absence of Cf(Vl) coatingPosilive = Presence of Cr(Vl) coating; the detected concenhation in boiling-water-extraclion solution isequal or greater than 0.02 mg/kg with 50 cm. sample surtac€ area.For@rosion protection coalings on metals: Infofmation on sto€ge conditions and production date ofthe tested sample is unavailable and thus results of Cr(Vl) represent status ofthe sample at the timeof testing.
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Test ReDort No. SHAEC1216714750 Date: 25 Sep 2012 Page 4 of 5
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ATTACHMENTS
RoHS Tesflng Ftow Chart1) Name of the person who made testing: Jan Shi^/oyo Wangr'A en Xao,cary Xuz) N€me or tne person in charge of testing: Jeff Zhang/ceorge Xu/ Linda Lir) Inese sampres w€re dissotved tota v bv ore-conditioning method according to belowflow chart. (Cr6'and PBBS/PBDES test method exctudedi
ratUlle.|lrto tr.hrt*€rthccfar zci@33+l..ti.tiEEtufta9+sltt tt: 2r@s
lElE(6?r)6140at63tE!Et6{l)0'tE17t m.6r€..mEtB-?)6r102r1 iL(ri-?r)A!G3 .tasr'..Cc.6
Pb/Cd/Hg PBBs/PBDEs
Acid digestion withmicrowave/ hotplate Nonmetallic
matedal
1) Alkali Fusion /DryAshing
2) Acid to dissolve Filtration and pHadjustment
Adding 1,5-diphenylc€rb€zide
for colordevelopment
Addang 1,5-diphenylcarbazide
for colordevelopment
A red colorindicatesthe
pre6ence of cr6*. lfnecess€ry,confirm with
rd.r[f,t Ddod@nFr!. Thb drsrud d!.r b.6rmdr..d *ror 6 nrr,$,l.d N.ris,.4jwr d tn.c.ffiv
Urmllr ol |h. AgA elou! (gGS SA)
Test Report
Sample photo:
No. SHAEC1216714750 Date:25 Sep 2012 Page 5 of 5
sHA12-167147.043
SGS authenticate the photo on original report only
"' End of Report "*
tt-!,ruaYanbrrrr&id,$.'icti 2tEf3+r'rr.*Jr8ltlsae'{33|t 3L M
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lrom!.r ol rh.8og Group (8G€S )
T€st Report No. SHAEC1216714738 Date: 25 Sep 201 2 Page 1 ol5
ZHEJIANG ASIA GENERAL SOLDERING&BRAZING MATERIAL CO., LTD
XIHU INDUSTRIAL PARK, SANDUN, HANGZHOU CIry' ZHEJIANG, PROVINCE' CHINA
The following 6ample(s) was/were submitted and identified on behalf of the clients as : LEAD-FREE SoLDER
WIRE
SGS Job No. :
Part No. (PN) :
Compositlon :
Date of Sampl€ Received :
Testing Period :
Test R€quested :
Test Method :
T€st Resulb :
Condusion :
Signed for and on b€half ofscs-csTc Ltd.
sP12-028285 - SH
YTW2O6
sno.3Ag0.7ouce
21 Sep 2012
21 s,ep 2012 - 25 SeP 2012
Selected test(s) as requested by client
Please refer to next Page(s)
Please refer to next Page(s).Baa€d on the perfomed tests on submitted samples' the results of Lead'I\rercury, Cadmium, Hexavalent chomium, Polybrorninated biphenyls (PBB)'
Polybrominated diphenyl ethe6 (PBDE) comply with the limits as set by RoHS
Di.ective 201 1/65/EU Annex ll; recasting 200295/EC
/Qv''Fan Jingiie, JJApproved Signatory
.n#ffiffiirmr r* u-ra -td *vot rmrr.t.t t*
tirtDafi$EE|ihtltrorr zxtaoil.t.|.*f,Ertr€€.lt$l ll@3
tErEl@llitldt6!E{ti"clt06t'9 ffior*ofrxr.c+rti el Kr(,-tt)Eaffi 1j!ltor-
iLnlirotllt SOS Otbt4 (aGS 8A)
T€6t Report
Test Results :
Test Pert De€criotion ;
S@rn6n No, SGS Sampl€ lD D6ctiptioi1 SHA12-167147.035 Silvery wire
Rgmarks :(1) 1 mg/kg= I PPm=00001%(2) MDL = Method Deteclion Limit
(3) ND = Not D€teded ( < lrDL )(4) '-' = Not Regulated
RoHS DllBdivs 201 l/85/EU
Test Llethod
No. SHAEC1216714734 Date: 25 Sep 2012 Page 2 o15
with reference to lEc 6232 1 :2008(1) Determination of cadmium by ICP-oEs.(2) Dete.mination of Lead by ICP-oEs(3) Determination of Mercrlry by ICP-OES.(4) Determination of Hexavalent Chromium by Spot test / Colorimetric l\,ethod using UV-Vis(5) Detemination of PBBS i PBoES by GC-[IS.
Test ltem{s)
Cadmium (Cd)
Lead (Pb)
Mercury fig)Hexavalent Chromium (Ci(VD)
Sum of PBBSMonobromobiphenylDibromobiphenylTribromobiph€nylTetrabrornobiphenylPentabromobiPhenYlHe/€bromobiphenylHeptabromobiPhenylOctabromobiphenylNonabromobiPhenylDecabromobiPhenYlSum oI PBDESMonobromodiphenyl ether
Limit UlE l\rDL
100 mdkg 2
1000 ms/kg 2
1000 ms/kS 2o
1000 mS.ftS- mS/kS 5- mdkg 5- mdkS s- mSikS 5- mdks 5- ms/kg 5- mg/kg 5- mdkS 5- msikg 5- mdks 5
1m0 mgftS- mg/KS 5
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ND50ND
N€gativeNDNDNDNDNDNDNDNDNDNDNDNDND
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lr.nD.t o1$.8Gg OrouP (8cgs )
Tes{ Report
Test ltem(s)Dibromodiphenyl etherTribromodiphenyl etherTetrabromodiphenyl etherPentabromodiphenyl elherHexabromodiphenyl etherHeptabromodiphenyl etherOc-tabromodiphenyl etherNonabro.nodiphenyl etherD€cabromodiphenyl ether
thi!
t'ilt,b.aYrbto drchrbrd,Swaon !e3a+1
No. SHAEC1216714738 Date: 25 Sep 2012
UdT MDt @mdkS 5 NDmdkS 5 NDmdkS 5 NDmdkg 5 NOmS/kg 5 NDmSikS 5 NDmg/kg 5 NDmS/kS 5 NDmgkg 5 ND
I ErE {O-Zr)OtrOO*FA)ala@!.a
Page 3 of 5
raEFaFffiTl|{j{l.?J)6r@
Notes :(1) The maximum permissible limit is quoted from diredive 2011/65/EU, Annex ll(2) ospot{est:
Negative = Absence of Cr(Vl) coating, Positive = Presence of Cr(Vl) coating;CIhe tested sample should be fudher verifed by boiling-waterextraction method if the spot test resultis Negative or cannot be confirmed.)oBoiling-wateFextraction:Negative = Ahsence of Cr(Vl) coatingPositive = Pesence of Cr(Vl) coating; the detected concentration in boiling-water-ext€ction solution isequal or greater than 0.02 mgl(q with 50 cm'z sample surtace area.For corrosion protection coatings on metals: Information on storage conditions and produclion date ofthe tested sample is unavailable and thus results of Cr(Vl) represent status of lhe sample at the timeof testing.
M.m!.rorh.scsGtuc(acgs )
Test Report No. SHAEC1216714734 Date: 25 S€p 2012 Page 4 of 5
' l ' ;-;Ltidbd$rffi '-d6.h*lhE.,nrdri*6
ATTACHMENTS
RoHS Te€ting Flow Chart
1) Name of the person who madetesting: Jan Shi/Yoyo Wang/Allen Xiao/Gary xu2i Name of the berson in charge of testing: Jeff Zhang/George Xu/ Linda Liiiiii,"i !!rir!!,i. aissoried totarry 6'y pre-condit-roningherhod accorcting to berowflow chart. (Cf
'
and PBBdPBDES test method excluded)
tr
Sample Prcparation
Sample Measurement
Acid digestion withmicrow€ve/ hotplate
Concentration/Dilution of extraclion
solution
'1) Alkali Fusion /DryAshing
2) Acid to dissolve
Adding 1,sdiphenylcarbazide
for colordevelopment
A red colorindicatesthe
presence of cP'.neceas€ry,confirm with
Pbrcd,Hg PB86fPBDE8
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Test Report
Sample photo:
No. SHAECl2'16714738 Date: 25 Sep 201 2 Page 5 of 5
sHA12-167147.035
SGS authenticato the photo on original report only'* End of Report ""
(d-l!r. .Dor d6.ccil-iibhihr.ldcn.h,
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l|.fiDcrolm. SOS Gtu,D |SOSS ]
nov'TEST REPORT
NO.:4002E11121307-2R02 Oa!aiDec15,2o11 page 1 of4
Customer: Suzhou FuHong Electrcnic IndustfialCo, Ltd.Addrgs8: NO.89WEl DU ROAD, WANGTING TOWN, XTANGCHENG D|STR|CT, SUZHOU, CHTNAReport on th6 3ubmitted ssmple said io beSample name: Fusos copper shellllodol: /
Material: /D$cription: /Buyea: /supplier: /
Sa|nple recelved date: Dec.13,2011Tcatlng p€riod: Frcm Dec.13,2011 to Dec.15,2011
T€tino Reau6tedAs specined by client, to delermine the L€ad, Cadmium, Mercrry & Hexavatent Chrcmium content in the submitted sampte inaccordance wilh Direclive 2002/95/EC (RoHS).
Tcstind method:
Testing llem [,leasudng inslrument MQLLead (Pb) EC 62321: 2008, seclion 9 ICP-OES 2mglkg
cadmium (Cd) EC 62321: 2008, section I ICP€ES 2 mg/kgMercury (Hg) EC 62321r 2008, section 7 rcP-oEs 2 mg/kgChrom'um (Cr l'I) EC 62321:2008, Annex I 0.02mg,a(g'
ILS, PLEASE REFER TOTHE FOLLOWING PAGE(S)'**'
lsg-'0.02 mg/kg returs 10 lhe MQLofsample extEction tiquid.
99!s!.c!i9!j-ffien tesied as specifred the submitted sample complied with the requircments of commission Decision of 18 Aug 2005amending Directive 2002l95/EC nolified lnderdocument 2005/618/EC
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S}'EI{ZN€N AOV TGSTING T€CHNOlOGY CO.,L'D.KUNSHAN EiANCH Hotllne86-512-5510 8000
6novNO.: 4002E11121307-2R02
TEST REPORT
Add the digestion solution; thevessel is heated Lrntil lhe sampl€ Add HrO, u nlil the sampl€ is clear
F;;1.-F;;,",..;-1.-{Melal subslrat€)
Add lhe digestion solution, clos€
the macrowave vess€|.
Cooling the vessel, fllleri washed and
filled to the mark with distilled water.
The sample is digested in the
micrcwave oven following a specific
decomposilion program.
and l\rercury Content: (Praring)
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I to the mark with Dtwater I I r*r.r*t | | -.- |
STIENZH€N AOV TESIING T€CIII{OLOGY CO.,lIO,KUII9HAN BFANCH
Hdpi/j,w.o{,6n
Hotline86-512"s510 8oO0
Cooling the vessel, filter washed and
filled to the mark with distilled water.
Remove the sample, and coollhe beaker lo rcom tempefalure,and do 1ie color reaction
Heal 50 mL ofDlwaterin lhe
beakerto boiling for 10 min
Test the sample solution and lhe 0.02mg/kg standard solution by UV-VIS.
To Detemine
nov.NO.: 4002E11121 307-2R02
5. To Detemine Hexavalent Chromium- '' ',.'1re$eo ovr I r
s.t sw-resi (M&
TEST REPORTDate: Dec.15, 2011
Contentln colorless and colored ctlromate coaling on
Page 3 ol4
metals: (Plating)
lflhe lest resull is positive,
the sample is considered 1o
have hexavalenl chromium
and the 0.02 mg/kg
Boiling- waieF extractionprocedure shall be used to
lfthe€ isrnterference orI rs hard to decide *terhellhe sample have the hexavalent chrcmium
5 2 Boiling- wEter- en€ction
Take the (5015) cm'z
sample in the beaker.
Srmple d93cription:
SH!NZHEN AOV TESTING TCCTNOIqGY CO.,L}D,KUNSHAN BFANCH nHot l ine86'512^5510 8000
Remove he sample, and cool
lhe beaker 1o room temperature,
and do the color reaction
Heat 50 mlof Olwater in the
beaker lo boiling for 10 min
Test the sample solution and the 0.02
mg/kg standard solution by UV-VIS.
Copper shell subslrateLead wle Platrng 24 Copper shell Plaling
Unil RoHS
Limit 2-3 24"Lead (Pb) mg/Kg 1000 N.D. 2.5 40.0 N.D.Cadmium {Cd) mg/kg 100 N,D. N.D. N.D. N.D.Msrorry (Hs) mg/kg 1000 N.D, N.D, N.D. N.D.Chromium (Crvl) mg/Kg 1000 Negative Negative Negalive Negative
nov.TEST REPORT
NO.r A002E11121307-2R02 Dat€iOec15,2011
-The new RoHS di.ective 2011/65/EU, on Jul 21, 2011 come into force, on Jan. 03, 2013 the fomat imotementation. Dircctive
2002l95/EC shall be reoealed simultaneouslv.
Sp€cim€ns, wnicn requested to determine Lead, Cadmium and l4ercury Conlent, have been dissotved comptetety.-mg/kg=ppm
-N.D.=not detected(
BEIJING HYSTIC NEW MATERIALS CO,, LTD.
5 SHUANGYUAN ROAD, BADACHU HIGH.TECH ZONE,BEIJING,100041, cHtNA
Test Report
l\rodel No. :
Date of Sample Received :Testing Period :Test Requested :
Test Method :
Test Results :
Conclusion i
O\ N6'(
The following sample(s) was^^/ere submitted and identified on behalf of the ctients as : EpOXy ADHESTVE
SGS Job No. : TP12-004950 - TJ
EP6O8
3l Mat 2012
31 Mat 2012 - 09 Apt 2012Selecled test(s) as requested by client.
Please refer to next page(s).
Please refer to next page(s).
Based on the perfomed tesb on submitted samples, the resutts of Lead,Mercury, Cadmium, Hexavalent chromium, Polybrominated biphenyts (PBB),Polybrominated diphenyl ethers (PBDE) comply with the limits as set by RoHSDirective 2011/65/EU Annex ll; recasting 2002/95/EC.
Signed for and on behalf ofscs-csTc Ltd.
No. TSNEC1200272601 Date: 09 Apr 2012 Page 1 of I
r 13t2?66233000 I l|t2ri5e95?52 {r*cr !$.ohr 136 266233000 r 136-?a2546?52 e s!.c\ia@6!3@
Aimy WangApproved Signatory
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Memberol rh. SGSGolp{SGS SAI
Te€t Report No. TSNEC1200272601 Date: 09 Apr 20 1 2 Page 2 ol8Test Results :
Test Part Description :
Sp€d.n€n No. SGS Ssmple lD D€6criplion1 TSN12-002726.001 ivory-white paste
Remarks :(1) 1mg/kg= 1 ppm = 0.0001%(2) IIDL = Method Detection Limit(3) ND = Not Deteded ( < MDL )(4) "-' = 1o1 q"nu,","o
RoHS Dirodive 201 t/66/EU
Test Method : With reference to |EC62321:2008(1) Determination ofCadmium by tCP-OES.(2) Determination of Lead by ICP-OES.(3) Detemination of l,rercury by ICP-OES.(4) Determination of Hexavalent Chrcmium by Colo metric Method using UV-Vis(5) Detemination of PBBS / PBDES content by GC-MS.
Test ltem(s)Cadmium (Cd)Lead (Pb)lllercury (Hg)Hexavalent Chromium (Cr(Vl))Sum of PBBSIvlonobromobiphenylDibromobiphenylTribromobiphenylTetrabromobiphenylPentabromobiphenylHexabromobiphenylHeptabromobiphenylOclabromobiphenylNonabromobiphenyl
DecabromobiphenylSum of PBDESMonobromodiphenyl ether
tinit Ud!100 mg/kg1000 mS/kS1000 mS/KS1000 mS/kS1000 mdks
- mg/Kg- mg/Kg- mg/Kg- mg-fts' mgKg- mgKS- ms/Ks- mg/kg- mgKg- m9x9
1000 ms/ks- mg/Kg
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MDt 0p12 N O2 N D2 N D2 N D- N D
5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D5 N D
ND5 N D
;trvdGhFo&de,sr,E^rh.;d.i@br.^ {1d".'db.tr' bt6$n;tonl!N{h'i rh rnir t r rd r . 6i1rir h 6 do.vnld d.di'ci't6rr.nE i DaDbh" -d d e
h,q!aoit" rc'rdn dr s.iod.d'
I 136 2aBA80CC | 0G42529s29 f,nqc'i!9s@rI {3f2r66?8806 l1e2?26&12 s sss.f'[email protected]
Membero, rbe SGS Group (SGS SA)
Test Report
Tost ltem(s)Dibromodiphenyl elherTdbromodiphenyl elherTelrab.omodiphenyl etherPentabromodiphenyl elh€rHexabromodiphenyl etherHeptabromodiphenyl etherOctabromodiphenyl etherNonabromodiphenyl etherDecabromodiphenyl elher
Notes :
No. TSNEC1200272601 Date: 09 Apr 2012 Page 3 of 8
trd!
(1) The maximum permissibte limit is quoted from directive 2011/65/EU. Annex lt.
Horebrpmocrrdododecane THBCDD)
Test lvlethod : With reference to IEC 62321:2008, anatysis was p€rfomed by GC-N4S.
udtms/Kgmg/KgmS/kSms/Ksmg/kgmg/Kgm9KSmgKsmgKs
UlitmgKg
MDt555555555
@1N DN DNDNDNDNDNDNDND
pp1N D
T€st ltem(s)Hexabromocyclododecane (HBCDD)
Notes :
Test ltem(s)Dibutyl Phthalate (DBP)B€nzylbutyl Phthalate (BBP)Bis (2-elhylhexyD Phthalale (DEHP)
Notes :
!d! MDt 0p1% (w4,,/) 0.003 ND% (ww) 0.003 ND% (Ww) 0.003 ND
MDI1 0
(1) Reference Information: Diredive 201 1/6S/EU recasting RoHS directive 200?J9S/EC:Hexabromocydododec€ne (HBCDD) is considered as a priority for riskevaluation and substancerestriclion.
Phthalatss
Test l\Iethod: With reference to EN14372:2004, anatysis was performed by co-tvts.
(1) Reference Infomation: Directive 2011/65/EU recasting RoHS directive 200295/EC:Bis (2-ethylhexyl) phthaiate (DEHP), Butyl benzyt phthatate (BBP) and oibutyt phthatate (DBp) areconsidered as a pdority for riskevaluation and subslance restiction.
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Test ReportResult shown is
No. TSNEC1200272601
of the total weight of wet sample
Date: 09 Apr 201 2 Page 4 of I
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Test ReDort No. TSNEC1200272601 Date: 09 Apr 2012 Page 5 of 8
ATTACHMENTS
cd/Pb/Hg/Cf'lPBB5&PBOES Flow Chart
Name of lhe person who made tesl ing: Aer0n Wang/Jason Li /Angel l Yao
Name ofthe percon in charge oftest ing: Cindy Yin/Rel ZhuThsse samples wsrs dissolved tolal ly by pre-condi l ioning melhod according to
below l low chari . (C16* and PBBS/PBDES test melhod excluded)
ill;l,ffi;i;lii'#:;' i;;;;i'-,iiiliir ii'iiii;'";l;;n *a ro 1t:.,.trere1"l:,11e191191':ll1"l:11*:::::L:11.,1:1:":i:YlTi."ii i i; ;ii; ;'. ti;;:'ii.c"npi'ivt or..p*rurv "tid."di^, ; rn! dod@dca'mri . '#li*lr,:*r";*iitikl.*ri:ni*l:"ll*t:iim::,ttiil:r:r.""i?i"::::'ii,llii:::lligiirliii:?';"'tiiii'i:il*"'
scsManeion.No 41,Ti6 5U Av€rueTEOA.Ianjri ChiM 3COa57
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Sample Preparation
Sample lVeasuremenl
Acid digest ion wi lhmicrcwave/ holplale
Sample solvent Adding digest ion reagent
Heating io 9tF95'C forextractionConcentral ion/
Di lut ion ofextract ions0iuIt0n
ResiduBSolution Fi l t ral ion and pHadjustmenl
1) Akali Fusion IDry Ashin g2) Acid todissolve
Adding 1 ,5'diphenylcarbazide fo!
coloi development
Fb/Cd/Hg PEB'PEDE5
Membero , lne SCS Group (SGS SA)
Test Report
ATTACHMENTS
' l ) Name ofthe percon
2) Nams of lhe person
No. TSNEC1200272601 Date: 09 Apr 2012 Page 6 ofB
HECDD Tosting Flow Chaft
who made test ing: Marine Sunin charge oftest ingr Rex Zhu
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Mebberol rh6 scs Grouo (SGS SAI
Sample cutt ing/preparation
Sample measurement
Solvenl exhaction
ConcBntral iodDilut ion
Test Report
ATTACHMENTS
Phthalde Testng Floli, chaft
1) Nams of lhe pelson who made lest ingi Maina Sun
2) Name ofthe person in charge oftesl ing: Rsx Zhu
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Mbfrberoilh6 SGs 6roup {SGs 5A)
No. TSNEC1200272601 Date: 09 Apr 2012 Page 7 of I
Solvenl exhacl ion
Conc entralion/Dil ution
Fihralion
Test Report
Sample photo:
TSN12-002726.001
SGS authenticate the photo on original repoionly
'*. End of Report '-
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No. TSNEC1200272601 Date: 09 Apr 20 1 2 Page 8 of 8
scs Malior.No 4l,rno 5h aleFJ. rEDA qan 'n chrB 3m'5'
+!.xt6e;r*iteEtt16llCscs*! {|:30q9l
Test Report
BEIJING HYSTIC NEW