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Quality Characteristics and Nutritional Profiles of DDGS Dr. Jerry Shurson Department of Animal Science University of Minnesota

2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

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Page 1: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Quality Characteristics and Nutritional Profiles of DDGSDr. Jerry ShursonDepartment of Animal ScienceUniversity of Minnesota

Page 2: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

DDGS Varies in Nutrient Content and Digestibility, Color, and Particle Size Among U.S. Sources

Page 3: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

0.42 – 0.990.75 (19.4)Phosphorus, %0.61 – 1.060.90 (11.4)Lysine, %3504 – 40483810 (3.5)Swine ME, kcal/kg

3.0 – 9.86.0 (26.6)Ash, %5.4 – 10.47.2 (18.0)Crude fiber, %8.8 – 12.410.7 (16.4)Crude fat, %28.7 – 32.930.9 (4.7)Crude protein, %87.3 – 92.489.3Dry matter, %

RangeAverageNutrient

Averages, Coefficients of Variation, and Ranges of Selected Nutrients Among 32 U.S. DDGS Sources (100% Dry Matter Basis)

Page 4: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

How Does DDGS Compare to Soybean Meal?

Page 5: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Variability (CV, %) of Selected Nutrients Among U.S. DDGS Sources vs. U.S. Soybean Meal Sources

9.119.4Phosphorus25.8117.5Calcium7.312.0Tryptophan4.25.8Threonine5.38.5Methionine3.012.1Lysine6.627.2Ash9.518.9Crude fiber30.917.1Crude fat2.34.5Crude proteinSoybean MealDDGSNutrient

Page 6: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Variation in Particle Size Among DDGS Samples Representing 25 U.S. Ethanol Plants

2005

-

200

400

600

800

1,000

1,200

0 5 10 15 20 25 30

Page 7: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Variation in Particle Size Among Soybean Meal Samples Representing 6 U.S. Plants

2005

-

200

400

600

800

1,000

1,200

0 5 10 15 20 25 30

Page 8: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Variation in Bulk Density (Lbs/Cubic Ft.) Among DDGS Samples Representing 25 U.S. Ethanol Plants

1/05

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5

10

15

20

25

30

35

40

0 5 10 15 20 25

Page 9: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Variation in Bulk Density (Lbs/Cubic Ft.) Among Soybean Meal Samples Representing 6 U.S. Plants

2003

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5

10

15

20

25

30

35

40

0 5 10 15 20 25 30

Page 10: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

DDGS Definition and Terminology in the Market

Page 11: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Distillers Products Definitions27.6 Distillers Dried Grains with Solubles is the product obtained after the removal of ethyl alcohol by distillation from the yeast fermentation of a grain or a grain mixture by condensing and drying at least ¾ of the solids of the resultant whole stillageand drying it by methods employed in the grain distilling industry. The predominating grain shall be declared as the first word in the name.

Page 12: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

0

5

10

15

20

25

30

35

Grains Solubles

DM, %CP, %Fat, %CF, %Ash, %Ca, %P, %

Comparison of the Nutrient Content of Corn Distiller’s Grains and Corn Condensed Distiller’s Solubles

Page 13: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

0.620.570.680.890.780.77P, %

0.170.040.510.060.120.07Ca, %

No data0.270.250.230.180.25Trp, %

No data1.101.131.041.011.17Thr, %

No data0.610.660.540.540.62Met, %

No data0.990.830.900.610.92Lys, %

No data37893560No data35773781ME, kcal/kg*

No dataNo data3796No data38084053DE, kcal/kg*

4.283.77.34.65.36.9Ash, %

No data20.221.017.911.812.4ADF, %

15.1010.67.8No data7.96.3Crude fiber, %

9.008.88.915.33.511.3Fat, %

27.029.930.131.629.331.8Protein, %

PelletedDDGS

Whiskey DDGS

Partial De-germed

DDGS

High Fat DDGS“DDGS”

Golden Corn

DDGS

*Calculated energy values for swine

Comparison of Nutrient Composition of Golden DDGS to Other “DDGS Sources” (100% Dry Matter Basis)

Page 14: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Grain Source Affects Nutrient Content and Digestibility

Page 15: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Comparison of Nutrient Composition of Corn DDGS, Sorghum DDGS, and a Corn-Sorghum Blend (As-is basis)

0

5

10

15

20

25

30

35

Protein%

Fat % ADF % Ash %

Corn DDGSSorghum DDGSCorn-Sorghum DDGS

Urriola et al. (2006)

Page 16: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Comparison of Total Lysine, Methionine, Threonine, and Tryptophan of Corn DDGS, Sorghum DDGS, and a Corn-Sorghum Blend of DDGS for Swine

0

0.2

0.4

0.6

0.8

1

1.2

Lys Met Thr Trp

Corn DDGSSorghum DDGSCorn-Sorghum DDGS

Urriola et al. (2006)

Page 17: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Comparison of Lys, Met, Thr, and Trp Digestibilities of Corn DDGS, Sorghum DDGS, and a Corn-Sorghum Blend of DDGS for Swine

0102030405060708090

Lys Met Thr Trp

Corn DDGSSorghum DDGSCorn-Sorghum DDGS

Urriola et al. (2006)

Page 18: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Standardized Ileal Lysine Digestibility Coefficients Among 10 “Golden” Corn DDGS Sources for Swine (Stein et al., 2005)

0

10

20

30

40

50

60

70

DDGS Source

12345678910

%

Page 19: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Differences in Digestible Amino Acid Content Among DDGS Sources for Poultry

0

0.2

0.4

0.6

0.8

1

1.2

Digest. AA (%)

Cys Lys ThrAmino acid

S1S2S3S4S5

Noll et al. (2006)

Page 20: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Prediction of Amino Acid Digestibility Among Sources of DDGS for Swine and Poultry

Page 21: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Lightness 25% Lightness 50% Lightness 75%

Commission of illumination color scale (Minolta):L* = Lightnessa* = rednessb* = yellowness

Hunter Lab and Minolta Color Measurements

Page 22: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Fig. 1. Regression of digestible lys (%) and color (L*, b*)

R2 = 0.71

R2 = 0.74

20

25

30

35

40

45

50

55

60

0.20 0.30 0.40 0.50 0.60 0.70 0.80

Lys (%)

L*, b

* sc

ore L*

b*Linear (L*)Linear (b*)

Source: Dr. Sally Noll (2003)

Page 23: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Prediction of Digestible Lysine from Color (L*, a*, and b*) Among DDGS Sources for Swine

R2 = 0.12, RMSE = 0.10, PC = 1

0.30

0.40

0.50

0.60

0.70

0.80

0.90

0.30 0.40 0.50 0.60 0.70 0.80 0.90

In vitro digestible lysine, %

In v

ivo

dig

estib

le ly

sine

, % .

Urriola et al. (2006)

Page 24: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Prediction of Digestible Lysine from Color L*, a*, and b* (L* < 50 in corn DDGS)

R2 = 0.40, RMSE = 0.07, PC = 1

0.300.350.400.450.500.550.600.650.700.750.80

30.00 35.00 40.00 45.00 50.00 55.00 60.00

Lightness (L*)

In v

ivo

dig

estib

le ly

sine

, %..

Urriola et al. (2006)

Page 25: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

-

10

20

30

40

50

60

400 450 500 550 600 650 700Wavelengh frecuency, nm

Ligh

t int

ensit

y, m

n

0.77% digestible lysine

0.54% digestible lysine 0.33% digestible lysine

Prediction of Digestible Lysine Content of DDGS Using Optical Density

Page 26: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Prediction of Digestible Lysine from Optical Density (400 to 700 nm)

R2 = 0.86, RMSE = 0.05, PC = 14

0.30

0.35

0.40

0.45

0.50

0.55

0.60

0.65

0.70

0.75

0.80

0.30 0.35 0.40 0.45 0.50 0.55 0.60 0.65 0.70 0.75 0.80In vitro digestible lysine, % .

In v

ivo

dig

estib

le ly

sine

, % .

Urriola et al. (2006)

Page 27: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Prediction of Digestible Lysine in DDGS Using Front Face Fluorescence

R2 = 0.98, RMSE = 0.07, PC = 9

0.30

0.35

0.40

0.45

0.50

0.55

0.60

0.65

0.70

0.75

0.80

0.30 0.40 0.50 0.60 0.70 0.80

In vitro digestible lysine, % .

In v

ivo

dig

estib

le ly

sine,

%.

Urriola et al. (2006)

Page 28: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Some of the Nutrient Variability Among DDGS Sources is Due to the Use of Different Laboratory Testing Procedures

Page 29: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Comparison of AOAC Approved Moisture Testing Methods

130-135° C for 1 hour

100-105° C for 3 hours

100-105° C for 4 hours

60-70° C for 24 hours

Page 30: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Variability of Laboratory Results from the Same DDGS Sample Sent to 5 Different Commercial Laboratories

Moisture Fat ProteinLab 1 12.69 13.73 26.00Lab 2 10.48 10.01 26.30Lab 3 10.09 10.04 27.02Lab 4 10.64 8.73 26.13Lab 5 13.30 10.15 26.29NIR 12.60 9.40 25.00

Page 31: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent
Page 32: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

An “Ideal” DDGS Quality Assurance Program for Ethanol Plants

Monitor incoming corn for mycotoxins and reject postive loads

Standardize the amount of solubles added to the grains fraction to produce DDGS

Use minimal drying time and temperature to produce DDGSDryer temperatures range from 445° F to 1150°F

Segregate poor quality DDGS from good quality DDGS when it is producedPrice different qualities accordingly

Provide transparent and frequent nutrient profile information to customers on the DDGS being produced

Specify the testing procedures used to determine nutrient content

Become ISO 9000:2001 and HAACP certified

Page 33: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Physical Characteristics to MonitorBulk densityParticle sizeHunter color scores

L*a*b*

pH

Page 34: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Nutrients to MonitorMoistureCrude proteinCrude fatCrude fiberADFNDFAshSwine DE, ME, NE (calculated)Starch

Page 35: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

MineralsCalciumPhosphorusSulfurChlorideSodium

Page 36: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Amino acidsLysineMethionineThreonineTryptophanCystine

Page 37: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

MycotoxinsAflatoxins

B1, B2, G1, G2

Deoxynivalenol (DON)ZearalenoneFumonisins

B1, B2, B3

Page 38: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

The Value of New Distiller’s By-Products in Swine Diets

Page 39: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Comparison of Mineral Content of Dakota Gold DDGS with High Protein Dakota Gold and Corn Protein Concentrate (100% DM Basis)

0

0.2

0.4

0.6

0.8

1

1.2

Ca, % P, % Na, % S, %

DDGSHP DDGSCPC

Page 40: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Comparison of Nutrient Content of Dakota Gold DDGS with High Protein Dakota Gold and Corn Protein Concentrate (100% DM Basis)

05

101520253035404550

Protein, % Fat, % NDF, % Ash, %

DDGSHP DDGSCPC

Page 41: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Comparison of Amino Acid Content of Dakota Gold DDGS with High Protein Dakota Gold and Corn Protein Concentrate (100% DM Basis)

00.20.40.60.8

11.21.41.61.8

Lys, % Met, % Cys, % Thr, % Trp, %

DDGSHP DDGSCPC

Page 42: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

Opportunity Costs of Corn By-Products in Swine and Poultry Diets

$43.00$75.20$53.00$75.20$80.00Poultry

$61.60$63.40$51.00$78.00$80.00Swine

CPCGlutenolHP DDGS

DDGS Spec. 2

DDGS Spec. 1

Page 43: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent

U of M DDGS Web Sitewww.ddgs.umn.edu

We have developed a DDGS web site featuring:* nutrient profiles and photos of DDGS samples

* research summaries

- swine, poultry, dairy, & beef

- DDGS quality

* presentations given* links to other DDGS related web sites* international audiences

Page 44: 2006 NGFA Quality Characteristics of DDGS...Segregate poor quality DDGS from good quality DDGS when it is produced Price different qualities accordingly Provide transparent and frequent