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4 U.S. Gownmeat Rlntlns offtco: laataos-O~OAIOI 2.1
REPORT # 71
LABORATORY ANALYSIS ON
NAVAL SAMPLES
(A/E CONTRACT N 6 2 4 7 0 - 8 4 - B - 6 9 3 2 ) - - .- .P .,- -
J T C REPORT # 85-208
PREPARED FOR:
DEPARTMENT O F THE NAVY
ATLANTIC D I V I S I O N
NAVAL F A C I L I T I E S ENGINEERING COMMAND
NORFOLK, VA 2 3 5 1 1
PREPARED BY:
JTC ENVIRONMENTAL CONSULTANTS, INC.
4 RESEARCH PLACE, S U I T E L - 1 0
ROCKVILLE, MARYLAND 2 0 8 5 0
MAY 28, 1985
Ann E. R o s e c r a n c e / L a b o r a t o r y D i r e c t o r ' CLW
0 0 ~ 0 0 0 0 5 1 5 7
C t W ~ 0 0 0 0 0 5 1 5 8
JTC E n v i r o n m e n t a l C o n s u l t a n t s , Inc.
~a r s 3 - ~ $ - $ 5 ~ e ~ o r t NO . 7 1 t o N a v a l Facilities E n g i n e e r i n g Command, N o r f o l k , Virginia
J T C D a t a R e p o r t No. 85-208 Table / Date o f Sample R e c e i p t 5-17-85
N A V Y
SAMPLE
I D
JTC
SAMPLE
ID 4 ~ 0 & A
0
484 8% (2-520 B Cattu Phnacr
486 U-6572. A 11
B 11 3
12-08-73 A JI
fie& TL . 6 I! J 3 ,
-. ANALYSIS PARAMETER
see a h c~edl
S htct
I!
I!
I r
I I
I \
2%. this %I.
- f.
0
4 '3 3
0 0 0 0 0 0 5 1 5 9 J T C ENVXRONMENTU CONSULTI\NTS, I N C .
P R I O R I T Y POLLUTI\NT ANALYSIS DATA SHEET
VOLATILE FRnCTXON
-
JK SWPLE # 1 ; r - u 8 ( ~ q A PROJECT NO. NF-12
NAVY SAMPLE # 4 8 3 w DATE RECEIVED 51 \) \ 85 METHOD NO. 624 DETECTION ~AIMXT 10 u g / l i t :
-- - - - .7,43iL - -
PZ$RAME!I!ER RESULT PARAMETER RESULT ug/li t . ugIlXt
2V acrdrein N . D . 32V 1,2-dichloropropane N-D.
3V acrylonitrile N . D.
4v. benzene N . D .
6V carbon tetrachloride NiD.
7V chlorobenzwe N. D.
' 10V 1 r 2-dichloroethane N.D.
LlV 1, I., 1- tz ich lo~- ethane N - D .
13V 1, 1-dichloroethrtne N.D.
14V 1,1,2-trichloro- ethane N.D.
1 S V 1,1,2,2-tetra- chloroethane N.D.
16V c h l o r o e t h a n e N . D .
19V 2-chloroethylvinyl ether N . D .
2 3 V c h l o r o f o r m Lf c 6'-
33V 1,3-dichloropro- pylene N . D ,
38V ethylbenzene N.D. C
44v m e t h v l e n e chloride N . D ,
45V m e t h y l chloride N-D. '
.46V methyl bromide N.D.
4 8V dichlorobromo- , g.2 * m e t h a n e m.
49V trichlorof luoro- m e t h a n e N . D .
50V dichlorodi f luoro- m e t h a n e N . D .
.-' a I 51V c h l o r o d i b r o m o m e t h a n e
BSV tetrachloxoethylene N.D.
86V to luenc N. D.
30V 1 , 2 - t r a n s - d i c h l o r o - 88v vinyl chloride N. D.
c t h y l c n e N.D.
, 0 ~ 0 0 0 0 5 1 6 0 YTC E N V I R O N M E N T A L CONSULTWTS, XNC.
? R I O R I T Y POLLUTMT I\NALYSIS DATA S N G E T
VOLATILE FRACTION
-
JTC SAMPLE # PROJECT NO. NF-12 - NAW SAMPLE # 4 8 3 w /O DATE RECEIVED 51131 85
METHOD NO, 624 DETECTION ~ I M I T 10 ug/lit
PqRAMETER RESULT ug/lit
2~ acrolein N.D.
4 V . benzene N.D.
6V carbon tetrachloride NiD.
7V chloxobenzqe N.D.
t ' 10V I, 2-dichloroethane N O D o
IIv l,l, 1-trichloA- 5+ 8 * ethane 4kB.
13V 1,l-dichloroethane N.D.
14V 1,1,2-trichloro- ethane N.D.
1SV 1,1,2,2-tetra- chloroethane N.D.
16V chloroethane N.D.
19V 2-chloroethylvinyl ether N.D,
23V chloroform I + xnr.
30V 1,2-trans-dichloro- ethylene N.D.
-- - - .- - -
PARAMETER RESULT . ug71i.t
32V 1,2-dichloropropane N.D.
38V ethylbenzene N,D, *
44V methylene chloride NOD-
4SV methyl chloride N.D.'
. 4 6V methyl bromide N.D.
4 8V dichlorobromo- 37 methane *
49V trichlorofluoro- methane N . D .
50V dichlorodifluoro- methane N . D .
51V chlorodibromomethane
8SV tetrachloroethylene N.D.
06V toluene N.D.
U7v trichloroethylene N. D.
08V vinyl chloride N.D.
CLW 0 0 0 0 0 0 5 1 6 1
J T C E N V I R O N M E N T A L , cONSULTWTS, XNC. P R I O R I T Y POLLUTANT ANALYSIS DATA S ~ ~ E E T
VOLATILE FiWCTXON
JTC SAMPLE # /a-0870 f l PROJECT NO. NF-12
NAVY SAMPLE # 2-J Lf bd DATE RECEIVED- 51 131 5
METKOD NO. 624 DETECTION ~ I M I T 10 u g / l i t
PaRAMETER RES U LT ug/lit:
2V a c m l e i n N.D.
3V a c r y l o n i t r i l e N.D-
4 V . benzene N-D.
6 V carbon t e t rach lor ide N : D.
7 V chlorobenzwe . N.D.
IlV 1,1, l-hichlok- 6 a b * ethane M.
1 3 V 1,l-dichloroethrzne N.D.
1 4 V 1 0 112-tr ichloro- ethane N . D .
15V 1,1 ,2 ,2-tetra- chloroethane N . D .
1 6 V chloroethane N. D.
19V 2-chloroethylvinyl e ther N.D.
2 3 V chloroform (4.5 &.
.-m - - - --- .
PARAMETER RESULT . ug11Lt
32V 1,2-dichloropropane N.D.
3 3 V 103-dichloropro- pylene N.D,
3 8 V ethvlbenzene N , D ,
44V methylene ch lor ide N.D.
4SV methyl chloride N.D.'
. 4 6V methyl bxotd.de N.D.
48V dichlorobromo- methane I7 M.
49V t r i c h l o r o f luoro- methane N.D.
50V dichlorodi f luoro- methane N . D .
5lV chlorodibromomethaneY am-.
85V te trachloroethylene N . D .
86v to luene N . D .
B 7 V trichloroethylene N.D.
30V 1,2-trans-dichloro- 88v vinyl c h l o r i d e N. D .
e t t ly l ene N.D.
CLW 0 0 0 0 0 0 5 1 6 2
JTC E N V X R O N M E N T ~ C . CONSULTWTS, XNC. P R I O R I T Y POLLUTANT ANALYSIS DATA S ~ ~ E E T
VOLATILE FRACTION
JTC SAMPLE # PROJECT NO, NF-12 - - NAVY SAMPLE # Y8U DATE RECEIVED 5//3/ 8s
' i
METLIOD NO. 624 DETECTION GIMIT 10 ug/lit:
.-* - PARAMETER - =Y.C -,-
PbRAMETER RESULT RESULT ug/lit . ug7li.t
3V acrylonitrile N-D.
4~ . benzene N-D.
6V carbon tetrachloride NID,
7V chlorobenzeqe . N, D.
' LOV I, 2-dichloroethane N.D.
11V 1,1,l-trichlom- ethane N.D.
14V 1,1,2-trichloro- ethane N . D ,
1SV 1,1,2,2-tetra- chloroethane N.D.
16V chloroethane N.D.
19V 2-chloroethylvinyl ether N.D.
33V 1,3-dichloropro- pylene N.D.
38V ethylbenzene N,D. C
44V methylene chloride N.D.
4SV methyl chloride N.D.'
4 6V methyl bromide N, D,
47v bromoform 67-. 48V dichlorobmmo- 3 3
methane -a
4 9V trichlorof luoro- methane N O D ,
SOV dichlorodifluoro- methane N.D.
-. / 0
8SV tetrachloroethylene N . D .
23V chloroform 86v toluene N. D.
29V 1,l-dichloroethylene N. D. 0 7 & trichloroethylene N.D.
30V 1, 2-trans-dichloro- O8v vinyl chloride N. D .
c t h y l e n e N.D.
CLW 0 0 0 0 0 0 5 1 6 3
JTC E N V I R O N M E N T A L CONSULTWTS, I N C . P R I O R I T Y POLLUTMT ANALYSIS DATA SHEET
VOLATILE FRACTION
-
JTC SAMPLE # ! A - O 8 7 / A PROJECT NO. NF-12 . - NAVY SAMPLE # 7 x 5 DATE RECEIVED T I / - ) I g 1 METHOD NO. 624 DETECTION LIMIT 10 ug/lit
- - - - .-- -
P~RAMETER RESULT PARAMETER RESULT ug/lit . ~gi/lilt:
2V acrolein N . D . 32V 1,2-dichloropropane N.D.
4 V . benzene N . D .
6 V carbon tetrachloride N i D .
1 10V Ir 2-dichloroethane N.D.
IlV 1,l. l d d c h l o k - 9. .a ?C ethane m.
13V 1,l-dichloroethzne N O D .
14V 1,1,2-trichloro- ethane N . D .
1SV 1,1,2,2-tetra- chloroethane N.D.
1 6 V chloroethane N. D .
19V 2-chloroethylvinyl ether N.D.
Z 3 V chloroform 5; 8 m.
pylene N . D .
38V ethylbenzene N.D. L
44V methylene chloride N.D.
4SV methyl chloride N O D ,
4 6V met hvl bromide N-D-
48V dichlorobromo- / 5 methane
49V trichlorof luoro- methane N.D.
50V dichlorodifluoro- methane N . D -
8 S V tetrachloroethylene N.D.
8 6 V toluene N . D.
29V 1,l-dichloroethylene N . D . 07; trichloroethylent N.D.
30V 1, 2-trans-dichloro- 0 8 V vinyl chloride N.D. e t h y l e n e N.D.
N . D . N O T D6TECr60 N . A . =; NOT nr*r,r,rcntlr.tynNnr,uzur,
0 0 0 0 0 0 5 1 6 4
JTC E N V X R O N M E N T U CONSULTNJTS, XNC. P R I O R I T Y POLLUTANT ANALYSIS DATA SffEET
VOLATILE FRACTION
--
JTC SAMPLE # PROJECT NO. NF-12
NAVY SAMPLE # DATE RECEIVED
METCIOD NO. 624 DETECTION ~ Z M L T 10 u g / l i t
- - .=- -
PI)RAMETER RESULT PARAMETER RESULT ug/lit . ugY1i.k
2V acrolein N.D . 32V 1, 2-dichloropropane N.D.
3V acrylonitrile N.D .
4V. benzene N-D.
6V carbon tetrachloride Ni D.
10V I, 2-dichloroethane N.D.
1;V l,l,l-krichlo&- q,7 * ethane *-
1 3 V I, 1-dichloroethzme N . D .
l 4 V 1,1,2-trichxoro- ethane N . D .
1 5 V 1,1,2,2-tetra- chloroethane N . D .
1 6 V chloroethane N . D .
1 9 V 2-chloroethylvinyl e t h e r N . D .
33V 1,3-dichloropro- pylene N O D ,
38V ethylbenzene N.D. . 4 4 V r n e t h y l e n e chloride N O D ,
4SV m e k h v l chloride N-D-'
. 4 6 V methyl bromide N.D. t -
4 8 V d i c h l o r o b m m o - 3 m e t h a n e -&a.
4 9 V trichlorofluoro- m e t h a n e N . D -
50V dichlorodif luom- m e t h a n e N,D,
- 1 -
8 S V tetrachloroethylene N - D ,
2 3V c h l o r o f o r m \ I *. 8 6 v t o luene N . D.
29V 1 , l -d i ch loroe thy l ene N . D . 07b t r i c h l o r o e t h y l o n k N . D .
30V 1,2-trans-dichloro- 08v vinyl c h l o r i d e N . D . ethylene N . D .
N -1). = NOT DETECI'ED N . A . :: NOT r\[*Pr, rcnu r.r.:/nNnr,Y x i-:o
D R I O R I T Y POLLUTNJT ANALYSIS DATA S ~ ~ E E T
VOLATILE FRACTION
JTC SAMPLE # 1 a-0871 A PROJECT NO. NF-12
N A ~ SAMPLE # Y 8 L HI DATE RECEIVED 51 j 3 185 '
METHOD NO. 624 DETECTION LIMIT 10 u g / l i t
- - . -- -
PJJRAMETER RESULT PARAMETER RESULT ug/l it . ugi/li-t
2 V acrolein N.D. 32V 1,2-dichloropropane N-D,
3V acrylonitrile N.D. 3 3 V 1,3-dichloropro- pylene N.D.
4V . benzene N.D. 3 8 V ethylbenzene N,D.
6V carbon tetrachloride N.D. 4 4 V m e t h y l e n e chloride N.D.
7 V chlorobenzqe N. D. 4SV m e t h y l chloride N.D.
1 0 V 1 , Z - d i c h l o r o e t h a n e N.D. I . 4 6V m e t h y l bxomide N.D.
1 1 V 1,l. 1-trichlok- 3 ,% % ethane M . 4 7 V bromoform
1 3 V 1,l-dichloroethane N.D.
1 4 V 1,1,2-trichloro- ethane N . D .
1 S V 1,1,2,2-tetra- chloroethane N . D .
16V c h l o r o e t h a n e N.D.
19V 2-chloroethylvinyl ether N . D .
2 3V c h l o r o f o r m (g ,a&
4 8V d i c h l o r o b r o m o - m e t h a n e
4 9V trichlorof luoro- m e t h a n e N.D.
50V d i c h l o r o d i f l u o ~ - m e t h a n e N-D,
51V c h l o r o d i b r o m o m e k h ~ e ~ ?Hre.
8 5 V t e t r a c h l o r o e t h y l e n e N . D .
8 6 V to luene N. D.
30V l,2-trans-dichloro- 88v vinyl chloride N . D . e t h y l e n e N.D.
CLW 0 0 0 0 0 0 5 1 6 6
YTC E N V I R O N M E N T A L CONSULTANTS, I N C . P R I O R I T Y POLLUTANT ANALYSIS DATA SI {EET
VOLATILE FRACTION
JTC SAMPLE # PROJECT NO. NF-12
NAVY SAMPLE # DATE RECEIVED 511 3 (f
METHOD NO. 624 DETECTION ~ ~ I M I T 10 ug / l i t
-5i3- - PARAMETER
- - - - - PaRAMETER RESULT RESULT
ug/lit ugY1i.t
2V acrolein N.D. 32V 1,2-dichloropropane N.D.
3V acrylonitrile N.D. 33V 1,3-dichloropro- pylene N . D ,
4 V . benzene N-D, - -- - - - 38V ethylbenzene N . D .
6V carbon tetrachloride N ; D. . 44V methylene chloride N. D,
7V chloxobenzqe N.D. 45V methyl chloride N.D.
1 0 V 1,2-dichloroethane -
N.D. I . 4 6V methyl bromide N.D.
I ~ V ~ , ~ , ~ - t r i c ~ . o k - . - /
14V 1,1,2-trichloro- ethane N . D .
1SV 1,1,2,2-tetra- chloroethane N.D.
16V chloroethane N . D .
1 9 V 2-chloroethylvinyl ether N . D .
23V chloroform I 3 e -
48V dichlorobromo- methane
49V trichlorof luoro- methane N . D -
50V dichlorodifluor0- methane N.D.
GY S1V chlorodibromoaethane
8 SV tetrachloxoethylene N.D.
86V toluene N.D.
30V 1, Z-trans-dichloro- 88v vinyl chloride N . D .
cttlylene N.D.
0 0 0 0 0 0 5 1 6 7 YTC E N V I R O N M E N T A L , CONSULTANTS, X N C .
PRIORITY POLLUTANT ANALYSIS DATA SfiEET
VOLATILE FRRCTION
JTC SAMPLE # _ PROJECT NO. NF-12 . I -
487 W NAVY SAMPLE # DATE RECEIVED 5 1 31 85 METHOD NO. 624 DETECTION $ 1 ~ 1 ~ 10 u g / l i t
--* - - -- - PaRAMETER RESULT PARAMETER RESULT
ug/ l i t ugi/lit
2 V acxolein N O D o 32V 1 , 2 - d i c h l o r o p r o p a n e N.D.
3~ acrylonitrile N . D .
4 V . benzene N.D.
6V carbon tetrachloride N i D .
IOV lr2-dichloroethane N.D.
v 1 , x i - 8 ,8 * ethane -N-;-D.
1 3 V 1,l-dichloroethme N . D .
1 4 V l,l, 2-trichloro- ethane N.D-
1 S V 1,1,2,2-tetra- chloroethane N . D .
1 6 V chloroethane N.D.
1 9 V 2-chloroethylvinyl e t h e r N-D.
44V m e t h y l e n e chloride N . D .
4SV m e t h y l chloride N.D.'
. 4 6V methyl bromide NODo
4 8 V d i c h l o r o b r o m o - - 3 2 m e t h a n e -HTD.
49V trichlorofluoro- m e t h a n e N . D ,
SOV dichlorodif luoro- m e t h a n e N.D.
S l V c h l o r o d i b r o m o m e t h a n e
8SV tetrachloroethylene N.D.
23V c h l o r o E o r m 10 TJ73-. 8 6 V to luene N . 0 .
30V 1 , 2 - t r a n s - d i c h l o r o - c t t l y l e n e N.D.
0 7~ t r i ch loroe thy len= N.D.
8 8 V v i n y l chloride N.D.
0 0 0 0 0 0 5 1 6 8 JTC E N V I R O N M E N T A L CONSULTWTS, XNC.
!?RXORXTY POLLUTANT ~ A L Y S ~ S DATA S I ~ E E T
VOLATILE FRACTION
J T C SAMPLE # PROJECT NO, NF-12
N A W SAMPLE # ~ t g -? U \ / D _ D A T E R E C E I V E D 5 1 ) - ) / 8 s T
METHOD NO. 624 DETECTION &EMIT 10 u g / l i t
PgRAMETER RESULT ug/ l i t
2 V acrolein N.D.
3V a c r y l o n i t r i l e N, D.
4 V . benzene N.D .
6V carbon t e t r a c h l o r i d e N;D-
1, Z, l,l-kxichlo&- 9, ethane (Y.U.
14V 1 , 1 , 2 - t r i c h l o r o - ethane N . D .
15V 1 ,1 ,2 ,2 - te tra - chloroethane N.D.
1 6 V chloroethane N.D.
19V 2 - c h l o r o e t h y l v i n y l e t h e r N.D.
23V chloroform
2 9 V 1 , l - d i c h l o r o e t h y l e n e N . D.
30V 1, Z-trans-dichloro- c t h y l e n e N . D .
-- - PARAMETER
- - . ? Z - RESULT
. ug;/li't
38V e thy lbenzene NID,
4 4 V methylene c h l o r i d e N O D .
4SV methyl chloride N.D.
46V methyl bromide N.D.
4 8V dichlorobromo- methane 3 La
49V t r i c h l o r o f l u o r o - methane N . D .
50V d i c h l o r o d i f luoro- methane N - D ,
-n
8SV tetrachloroethylene N . D .
8 6 V t o l u e n e N . D .
07V t r i c h l o r o e t h y l e n b N.D.
8 8 V v i n y l c h l o r i d e N . D .
N . D . = N01' DETECI'EO N . A . rz NOT AI'PT*LCAU~.I~~/ANAI,Y %I311