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Volume 1927

The 1st International Conference and Exhibition on Powder Technology Indonesia (ICePTi) 2017

Jatinangor, Indonesia8–9 August 2017

EditorsI Made Joni and Camellia Panatarani

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Conference Proceedings

ISBN 978-0-7354-1619-200009

9 780735 416192

ISBN 978-0-7354-1619-2ISSN 0094-243X


Vol. 1927The 1

st International Conference and Exhibition on Powder Technology Indonesia (ICePTi) 2017


Melville, New York, 2018 AIP Conference Proceedings

To learn more about AIP Conference Proceedings visit http://proceedings.aip.org



The 1st International Conference and Exhibition on Powder Technology Indonesia (ICePTi) 2017Jatinangor, Indonesia8–9 August 2017

EditorsI Made JoniCamellia PanataraniUniversitas Padjadjaran, West Java, Indonesia

Sponsoring OrganizationsNanotechnology and Graphene Research Center, Universitas PadjadjaranScience and Techno Park (STP) Universitas PadjadjaranMaterial Science & Engineering Study Center, Universitas PadjadjaranJP Global TranstechAshizawa Finetech Ltd.Ohkawara Kakohki Co., Ltd.Kajiwara Inc.Kett Electric LaboratorySeishin Enterprise Co., Ltd.Tsutsui Scientific Instrument Co., Ltd.Toyo Hitec Co.,Ltd.Tokuju CorporationEriez Magnetics Japan Co., Ltd.Hakaru Plus CorporationMakino Mfg. Co., Ltd.Matsushima Measure Tech Co., Ltd.Matsubo Corporation

All papers have been peer reviewed

Volume 1927

CP_Prelim_pages_8.5x11_Blue.indd 1 11-01-2018 09:27:24

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EditorsI Made JoniCamellia PanataraniUniversitas PadjadjaranDepartment of PhysicsFaculty of Mathematics and Natural SciencesJl. Raya Bandung-Sumedang KM 21Jatinangor, West Java 45363Indonesia

Universitas PadjadjaranNanotechnology and Graphene Research CenterJl. Raya Bandung-Sumedang KM 21Jatinangor, West Java 45363Indonesia

Email: [email protected] [email protected]

ISBN 978-0-7354-1619-2ISSN 0094-243XPrinted in the United States of America


AIP Conference Proceedings, Volume 1927The 1st International Conference and Exhibition on Powder

Technology Indonesia (ICePTi) 2017

Table of Contents

Preface: The 1st International Conference and Exhibition on Powder Technology Indonesia (ICePTi 2017) 010001Committee Sponsor Advisory: The 1st International Conference and Exhibition on Powder Technology Indonesia (ICePTi 2017) 010002

INVITED PAPERSA discussion on maximum charge held by a single particle due to gas discharge limitation

Tatsushi Matsuyama 020001

Post treatment of antibiotic wastewater by adsorption on activated carbonP. Mullai and V. Rajesh 020002

Synthesis and characterization of dental compositesNina Djustiana, Nadia Greviana, Yanwar Faza, and Sunarso 020003

Brief review: Preparation techniques of biomass based activated carbon monolith electrode for supercapacitor applications

Erman Taer and Rika Taslim 020004

Nanotechnology: Development and challenges in IndonesiaI Made Joni, Vanitha Muthukannan, Wawan Hermawan, and Camellia Panatarani 020005

CONTRIBUTED SPEAKER PAPERSDetection of mercury ions using L-cysteine modified electrodes by anodic stripping voltammetric method

M. Vanitha, N. Balasubramanian, I Made Joni, and Camellia Panatarani 030001

Study and characterization of powder mackerel (Scomberomorus commerson) bone gelatin through hydrolysis of hydrochloric acid

E. Mardawati, H. Sugandi, I. L. Kayaputri, Y. Cahyana, D. W. Wira, T. Pujianto, and R. Kastaman 030002

The effect of Sinabung volcanic ash and rock phosphate nanoparticle on CEC (cation exchange capacity) base saturation exchange (K, Na, Ca, Mg) and base saturation at Andisol soils Ciater, West Java

Anni Yuniarti, Mahfud Arifin, Emma Trinurasi Sofyan, Betty Natalie, Rija Sudirja, and Dewi Dahliani 030003

Graphite tail powder and liquid biofertilizer as trace elements source for ground nutReginawanti Hindersah, M. Rochimi Setiawati, B. Natalie Fitriatin, Pujawati Suryatama, Priyanka Asmiran, Camellia Panatarani, and I Made Joni 030004

Structural properties of perovskite films on zinc oxide nanoparticles-reduced graphene oxide (ZnO-NPs/rGO) prepared by electrophoretic deposition technique

Ayi Bahtiar, Euis Siti Nurazizah, Efa Latiffah, Risdiana, and Yukio Furukawa 030005


Particle size analysis on density, surface morphology and specific capacitance of carbon electrode from rubber wood sawdust

E. Taer, B. Kurniasih, F. P. Sari, Zulkifli, R. Taslim, Sugianto, A. Purnama, Apriwandi, and Y. Susanti 030006

Bioactivity of essential oil from lemongrass (Cymbopogon citratus Stapf) as antioxidant agentNenden Indrayati Anggraeni, Ika Wiani Hidayat, Saadah Diana Rachman, and Ersanda 030007

Alkaloid and polyphenol analysis by HPLC in green and black tea powders and their potential use as additives in ruminant diets

Diky Ramdani, Abdul S. Chaudhry, and Chris J. Seal 030008

The quality of microorganism on coal bed methane processing with various livestock waste in laboratory scale

E. T. Marlina, Tb. B. A. Kurnani, Y. A. Hidayati, K. N. Rahmah, I M. Joni, and E. Harlia 030009

Influence of full cream milk powder on the characteristics of sweet potato puree instant cream soupMarleen Sunyoto, Mohamad Djali, and Intan Btari Dwiastuti 030010

Farmers behavior on using fertilizer in West JavaTomy Perdana, Eddy Renaldy, Hesty Nurul Utami, Agriani Hermita Sadeli, Mahra Arari H., Tetep Ginanjar, Ajeng Sesy N. P., Fernianda Rahayu H., and Sonny Sanjaya 030011

Consumer preference of fertilizer in West Java using multi-dimensional scaling approachHesty Nurul Utami, Agriani Hermita Sadeli, Tomy Perdana, Eddy Renaldy, Mahra Arari H., Ajeng Sesy N. P., Fernianda Rahayu H., Tetep Ginanjar, and Sonny Sanjaya 030012

Andrographolide powder treatment as antifeedant decreased digestive enzyme activity from Plutella xylostella (L.) larvae midgut

Madihah, Desak Made Malini, Hana Roviani, Nessa Vidya Rani, and Wawan Hermawan 030013

Activation of inoculum microorganism from dairy cattle fecesWidya D. Ayuningtyas, Roni Ridwan, I M. Joni, E. T. Marlina, and Ellin Harlia 030014

Biogas production from various coal types using beef cattle rumen’s liquid as a source of microorganisms consortium

Tubagus Benito Achmad Kurnani, Ellin Harlia, Yuli Astuti Hidayati, Eulis Tanti Marlina, A. N. Sugiarto, K. N. Rahmah, and I M. Joni 030015

The effect of CO2 activation temperature on the physical and electrochemical properties of activated carbon monolith from banana stem waste

E. Taer, Y. Susanti, Awitdrus, Sugianto, R. Taslim, R. N. Setiadi, S. Bahri, Agustino, P. Dewi, and B. Kurniasih 030016

The application dosage of Azolla pinnata in fresh and powder form as organic fertilizer on soil chemical properties, growth and yield of rice plant

Mieke Rochimi Setiawati, Maya Damayani, Diyan Herdiyantoro, Pujawati Suryatmana, Derisfha Anggraini, and Fiqriah Hanum Khumairah 030017


MOSFET-based high voltage short pulse generator for ultrasonic transducer excitationDarmawan Hidayat, Setianto, Nendi Suhendi Syafei, and Bambang Mukti Wibawa 030018

Formulation and physicochemical characterization of composite flour from yam (Dioscorea alata) and lima beans (Phaseolus lunatus)

Rohmah Fitri Utami, Danar Praseptiangga, Dian Rachmawanti Affandi, and Windi Atmaka 030019

Physical and chemical characterization of composite flour from canna flour (Canna edulis) and lima bean flour (Phaseolus lunatus)

Danar Praseptiangga, Anisha Ayuning Tryas, Dian Rachmawanti Affandi, Windi Atmaka, Achmad Ridwan Ariyantoro, and Slamet Minardi 030020

The production of anaerobic bacteria and biogas from dairy cattle waste in various growth mediumsY. A. Hidayati, T. B. A. Kurnani, E. T. Marlina, K. N. Rahmah, E. Harlia, and I M. Joni 030021

New insight on the formation of whey protein microbeads by a microfluidic systemRobi Andoyo, Fanny Guyomarc’h, Hervé Tabuteau, and Marie-Hélène Famelart 030022

Synthesis and characterization of CMC from water hyacinth for lithium-ion battery applicationsSahrul Hidayat, Susanty, Nowo Riveli, Bambang Joko Suroto, and Iman Rahayu 030023

Solubility and dissolution improvement of ketoprofen by emulsification ionic gelationRevika Rachmaniar, Deby Tristiyanti, Syarif Hamdani, and Afifah 030024

P retention and cation exchange as affected by nanoparticle of volcanic ash and application of phosphate solubilizing bacteria on Andisol Ciater, West Java, Indonesia

Betty Natalie Fitriatin, Mahfud Arifin, Rina Devnita, Anni Yuniarti, Rachmat Haryanto, and Mariska Amalia Setiabudi 030025

The synthesis of carbon electrode supercapacitor from durian shell based on variations in the activation time

E. Taer, P. Dewi, Sugianto, R. Syech, R. Taslim, Salomo, Y. Susanti, A. Purnama, Apriwandi, Agustino, and R. N. Setiadi 030026

Application of nanoparticle of rock phosphate and biofertilizer in increasing some soil chemical characteristics of variable charge soil

Rina Devnita, Benny Joy, Mahfud Arifin, Ridha Hudaya, and Nurul Oktaviani 030027

Evaluation of setting time and flow properties of self-synthesize alginate impressionsCalista Halim, Arief Cahyanto, Sriwidodo, and Zulia Harsatiningsih 030028

The effectiveness of Penicillium sp. mixed with silica nanoparticles in controlling Myzus persicaeHersanti, Syarif Hidayat, Agus Susanto, Regi Virgiawan, and I Made Joni 030029

Preparation and characterization of zirconia-alumina system via solution and solid phase mixing method

Yanwar Faza, Zulia Hasratiningsih, Andrie Harmaji, and I Made Joni 030030


Morphological characterization of ceramic fillers made from Indonesian natural sand as restorative dental materials

E. Karlina, S. Susra, Y. Fatmala, H. M. Hartoyo, V. Takarini, K. Usri, R. Febrida, N. Djustiana, C. Panatarani, and I M. Joni 030031

The dispersion of fine chitosan particles by beads-millingEmma Rochima, Safira Utami, Herman Hamdani, Sundoro Yoga Azhary, Danar Praseptiangga, I Made Joni, and Camellia Panatarani 030032

The variable charge of andisols as affected by nanoparticles of rock phosphate and phosphate solubilizing bacteria

M. Arifin, N. Nurlaeny, R. Devnita, B. N. Fitriatin, A. Sandrawati, and Y. Supriatna 030033

The impact of anaerobic microorganisms activities in ruminant waste and coalEllin Harlia, H. Hamdani, Winantris, Tb. B. A. Kurnani, Y. A. Hidayati, E. T. Marlina, K. N. Rahmah, H. Arief, R. Ridwan, and I M. Joni 030034

The phosphorus status of andisols as influenced by nanoparticles of volcanic ash and rock phosphate

Rina Devnita, Benny Joy, Mahfud Arifin, Ade Setiawan, Santi Rosniawaty, and Felia Shella Meidina 030035

Comparative study of CO2 and H2O activation in the synthesis of carbon electrode for supercapacitors

E. Taer, Apriwandi, Yusriwandi, W. S. Mustika, Zulkifli, R. Taslim, Sugianto, B. Kurniasih, Agustino, and P. Dewi 030036

Cell viability of mycorrhiza helper bacteria solid inoculant in different carrier materialIis Nur Asyiah, Reginawanti Hindersah, and Rita Harni 030037

Synthesis and characterization of ZnO:Ca2+ prepared by simple solution methodHeraldo Yanindra Pradana, I Made Joni, Liu Kin Men, Yayah Yuliah, Lukman Nulhakim, Vanitha Muthukanan, and Camellia Panatarani 030038

Optical transparency and mechanical properties of semi-refined iota carrageenan film reinforced with SiO2 as food packaging material

Afifah Iswara Aji, Danar Praseptiangga, Emma Rochima, I Made Joni, and Camellia Panatarani 030039

Mechanical and solubility properties of bio-nanocomposite film of semi refined kappa carrageenan/ZnO nanoparticles

Apriliana Eka Saputri, Danar Praseptiangga, Emma Rochima, Camellia Panatarani, and I Made Joni 030040

UV-screening, transparency and water barrier properties of semi refined iota carrageenan packaging film incorporated with ZnO nanoparticles

Assifa Rahma Khoirunnisa, I Made Joni, Camellia Panatarani, Emma Rochima, and Danar Praseptiangga 030041

The addition of nanochitosan suspension as filler in carrageenan-tapioca biocomposite filmEmma Rochima, Elisah Fiyanih, Eddy Afrianto, Ujang Subhan, Danar Praseptiangga, Camellia Panatarani, and I Made Joni 030042


Development and performance evaluation of air fine bubbles on water quality of thai catfish rearingUjang Subhan, Vanitha Muthukannan, Sundoro Yoga Azhary, Muhammad Fakhri Mulhadi, Emma Rochima, Camellia Panatarani, and I Made Joni 030043

Fabrication and characterization of rice husk charcoal bio briquettesS. Suryaningsih, O. Nurhilal, Y. Yuliah, and E. Salsabila 030044

Application of probiotics and different size of sodium bicarbonate powders for feedlot sheep fattening

Hery Supratman, Diky Ramdani, Sondy Kuswaryan, Dwi Cipto Budinuryanto, and I Made Joni 030045

The toxicity evaluation of prepared Lantana camara nano extract against Spodoptera litura (Lepidoptera: Noctuidae)

Hikmat Kasmara, Melanie, Dea Audia Nurfajri, Wawan Hermawan, and Camellia Panatarani 030046

Surface wettability and subcooling on nucleate pool boiling heat transferBambang Joko Suroto, Masamichi Kohno, and Yasuyuki Takata 030047


Preface: The 1st International Conference and Exhibition on Powder Technology Indonesia

(ICePTi 2017)

The 1st International Conference and Exhibition on Powder Technology Indonesia (ICePTi 2017) was held in Universitas Padjadjaran, Jatinangor Campus , Bandung, Indonesia during 8th – 9th August 2017. Jatinangor, the house for various Universities amidst the pleasant environment is an ideal venue for the conference.

ICePTi 2017, organized by Nanotechnology and Graphene Research Center (Print -G), Science & Technology Park Unpad (KST-Unpad), Material Science & Engineering (MSE) Study Center Unpad, Indonesian Powder Association and managed by JP Global Transtech. In connection with this event, The 4th Japan Powder Technology Forum was held in Indonesia. The objectives of this forum is to acquaint with the field of powder technology and technologies developed by Japanese companies.

This conference is aimed at elevating the scientific communities, explore new ideas, research progress, technological developments and light up collaboration between researchers and industries, in powder technology and its applications. Exhibition was also organized to promote the new products or technologies developed under these four categories: Manufacturing & Processing Equipment, Instrumentation, Measuring & Laboratory Equipment, Materials Engineering, Science & Technology Park Unpad.

There were 14 invited speakers, 49 abstracts and 63 scientific participants from countries like Indonesia, Japan, India and United States, contributing to the overall success of the Conference. The abstracts were considered under two categories, powder science & technology and powder applications. Among the total number of presented abstracts, 52 articles were published in AIP Conference Proceedings.

Generous support for the conference was provided by Rector, Directorate of Research and Community Service and Innovation, Universitas Padjadjaran.

On behalf of the organizing committee, we would like to register our thanks to the advisory committee, participants and all who have supported to the success of this scientific meeting. We would also like to thank all the members of the organizing committee, it is our privilege and honour to be the corresponding Editors.

Corresponding Editors

I Made Joni

Camellia Panatarani

The 1st International Conference and Exhibition on Powder Technology Indonesia (ICePTi) 2017AIP Conf. Proc. 1927, 010001-1–010001-1; https://doi.org/10.1063/1.5021187

Published by AIP Publishing. 978-0-7354-1619-2/$30.00

010001-1

Organizing Committee Chairperson: Camellia Panatarani

Program: Sundoro Yoga Azhariy, Thalita Nadya Rahma, Muhammad Fakhri Mulhadi, Adika Pambudi, Vanitha Muthukanan, Lukman Nulhakim Publication and Documentation: Ujang Subhan, Ahmad Qosam, Heraldo Yanindra Pradana, Sony Irawan, Dwindra Wilham Maulana Logistics & Transportation: Emma Rochima, Shaffira, Elisa, Ilham Dhiaputra, Ilham Zharif Mustaqim Maulana Yusuf S, Assifa Rahma Khoirunnisa, Afifah Iswara Aji, Apriliani Eka Saputri, Dodi Murtaddo, Hera Redianti, Irfan, Dana Hismawan Secretariat: Erlan Saputra, Dina Lestari, Sitti Hidayatul Hikma, Erni Yulianti

ICePTi Management Partner

https://jpfoundation.or.id/

Irfan Miswari Fenfen Fenda Florena

Ikhsan Saputro M. Abdul Al Mujahid

Angga Nugraha



010002-1

Advisory Board

1. Prof. Dr. Wuled Leggoro (Tokyo University of Agriculture Technology, Japan)

2. Prof. Dr. Heru Setiawan (Institut Teknologi Sepuluh Nopember, Indonesia)

3. Prof. Dr. Eng. I Made Joni (Universitas Padjadjaran, Indonesia)

4. Prof. Wawan Hermawan (Biology, Universitas Padjadjaran, Indonesia)

5. Tomohide Tanimoto (Tokuju Corporation, Japan)

6. Toshimitshu Makino (Makino, MFG Co. Ltd., Japan)

7. Masaki Ohkawara (Ohkawara Kakohki Co. Ltd., Japan)

8. Hideaki Tanno (Eriez Magnetics Japan Co. Ltd., Japan)

9. Dr. Muchtaridi (Pharmacy Universitas Padjadjaran, Indonesia)

10. Dr. Deo Raj Singh (Weill Cornel Medical College, Cornell University, USA)

11. Danar Praseptiangga, Ph.D (Food Science and Technology, Universitas Sebelas Maret,

Indonesia)

12. Dr. Rupiasih, M.Si. (Physics, Universitas Udayana)

13. Dr. Eng. Pramujo Widiatmoko ST, MT (Chemical Engineering, Institut Teknologi

Bandung, Indonesia

14. Rizky Abdulah, Ph.D (Pharmacy, Universitas Padjadjaran, Indonesia)

15. Dr. Abrar Ismardi (Telkom University, Indonesia)

010002-2

Organized by:

Managed by:

Supported by:

010002-3

The Dispersion of Fine Chitosan Particles by Beads-Milling

Emma Rochima1, 5, a), Safira Utami1, b), Herman Hamdani2, c), Sundoro Yoga Azhary5, d), Danar Praseptiangga3, e), I Made Joni4, 5, f) and Camellia Panatarani4, 5, g)

1Dept. of Fishery Processing Technology, Faculty of Fishery and Marine Science, Universitas Padjadjaran, 2Dept. of Management of Aquatic Resources, Faculty of Fishery and Marine Science, Universitas Padjadjaran,

Jl. Raya Bandung-Sumedang KM 21, Jatinangor, West Java 45363, Indonesia 3Dept. of Food Science and Technology, Faculty of Agriculture, Sebelas Maret University,

Jl. Ir. Sutami No. 36A 57126 Jebres, Surakarta, Central Java, Indonesia. 4Dept. of Physics, Faculty of Mathematics and Natural Sciences, Universitas Padjadjaran,

5Nanotechnology and Graphene Research Center, Universitas Padjadjaran, Jl. Raya Bandung-Sumedang KM 21, Jatinangor, West Java 45363, Indonesia

g)Corresponding author: [email protected]

a)[email protected], b)[email protected], c)[email protected], d)[email protected], e)[email protected], f)[email protected]

Abstract. This research aimed to produce fine chitosan particles from a crab shell waste by beads-milling method by two different concentration of PEG as dispersing agent (150 and 300 wt. %). The characterization was performed to obtain the size and size distribution, the characteristics of functional groups and the degree of deacetylation. The results showed that the chitosan fine particles was obtained with a milling time 120 minutes with the best concentration of PEG 400 150 wt. %. The average particle size of the as-prepared suspension is 584 nm after addition of acetic acid solution (1%, v/v). Beads milling process did not change the glucosamine and N-acetylglucosamine content on chitosan structure which is indicated by degree of deacetylation higher than 70%. It was concluded that beads milling process can be applied to prepare chitosan fineparticles by proper adjustment in the milling time, pH and dosage of dispersing agent.

INTRODUCTION

Chitosan is a natural polysaccharide and is considered as the largest biomaterial after cellulose in terms of utilization and distribution [1]. It is produced from chitin the structural element found in the exoskeleton of crustaceans such as shrimps, lobsters and crabs. Chitosan can be used in many areas of modern industry, such as pharmaceuticals, biochemicals, cosmetics, food industries and textile industry [2]. In the field of food technology, chitosan was developed by changing the particles size to become fine particles i.e. micro/nano as reinforcement for the biocomposite films. Using fine chitosan particles as filler in biocomposite film would enhance the properties of film such as mechanical and barrier properties [3]. Additionally, chitosan compared to other bio-based food packaging materials has the advantage of antibacterial activity [4]. Fine particles of chitosan are prepared using number of different strategies. These include cross linking, ionotropic gelation, microemulsion, emulsification solvent diffusion and polyelectrolyte complexation [5]. All these techniques adopt a “bottom-up” approach where particles are generated from individual macromolecules through self-assembly [6]. Extensive work had been carried out by adopting bottom-up strategies to prepare fine chitosan particles, however research carried out using top down technologies are almost insignificant [7]. Beads-milling is one of the equipment of top-down process for size reduction of bulk particles into fine particles. Furthermore, bead milling is capable of producing fine chitosan particles in suspension, since it allows using smaller beads around 0.015 to 0.5 mm and applied with a dispersing agent [8]. Therefore, the objective of this study is to obtain the well-dispersed chitosan suspension by beads milling



030032-1

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