2016

POST-CONFERENCE WORKSHOP “INDUSTRIALIZATION OF CATALYSTS AND

PROCESS” BY PROF HIDESHI HATTORI, HOKKAIDO UNIVERISTY JAPAN

PARTICIPANT

ZEOLITE MODIFICATION ENHANCED ON BENZENE ALKYLATION PERFORMANCE

PUBLICATION ON SCIENTIFIC JOURNAL AS FIRST AUTHOR (IN PROGRESS)

INTERNATIONAL SEMNIAR ON CHEMISTRY SURABAYA, INDONESIA

PARTICIPANT

CONFERENCE ON EMERGING ENERGY AND PROCESS TECHNOLOGY

(CONCEPT 2015), CENTRE OF HYDROGEN ENERGY

PARTICIPANT

UNDERGRADUATE FINAL YEAR DESIGN PROJECT (FYDP) “PRODUCTION OF

GLYCEROL MONOSTEARATE FROM CRUDE GLYCEROL”

MASS BALANCE MANAGER, REACTOR AND PROCESS PLANT DESIGNER, AUTHOR

OFFSHORE TECHNOLOGY CONFERENCE ASIA (OTC), KLCC MALAYSIA

PARTICIPANT

2O16

2015

STATISTICA 8.0.360.0 ENGLISH

OBJECTIVE

PRODUCTION ENGINEER. INTEREST IN UNIT OPTIMIZATION FOR IMPROVING

EFFICIENCY AND MONITORING PROCESSES FOR IMPROVEMENTS. ALSO CAN BE

ASSIST TO INNOVATE THE EXISTING PROCESS, INSTALL NEW EQUIPMENT OR

MATERIAL AND DO FOR MAINTAINANCE IN IMPROVING UNIT YIELDS AND PRODUCT

QUALITY.

WILLING TO LEARN, OPTIMISTIC, MULTI-TASKING, FOCUS,

ADAPTABLE, ORGANIZER PERSON, PROBLEM SOLVER THINKER

Responsibility and Experience as Research Assistant :

1) Independently conducts analyses and interprets results, with direction on more

complicated analyses on instruments results such as GC-FID, GC-MSD, FTIR, BET,

UV-Vis and Gas Reactor.

2) Perform scientific work requiring application of standard techniques, procedures, and

criteria in carrying out a sequence of related scientific tasks.

3) Learn analytical techniques and apply learning to standardized methods.

4) Apply basic scientific knowledge to solve simple process problems.

5) Learn and follow all Standard Operating Procedures (SOPs) and Good Manufacturing

Practices (GMPs).

6) Troubleshoot, and make adjustments to laboratory equipment consisting of small

scale reactors. 8)

7) Prepare documentation in accordance with SOPs.

8) Document scientific procedures and results in lab notebooks, or other designated

forms and prepare scientific reports with guidance from an experienced team

member.

9) Optimize synthetic routes, scale up & scale down synthesis material or processes.

10) Review other team member’s data for simple tests.

11) Exercise judgment within generally defined practices and policies in selecting

methods and techniques for obtaining solutions to complex problems.

12) Performs routine scientific work without instruction and receives general instructions

on new assignments from an experienced team member.

13) Deal with vendor in buying process such as high purity nitrogen, hydrogen, air,

helium, carbon dioxide from supplier (Mega Mount).

14) Other duties as assigned.

114

Crude Glycerol

Hexane

Tristearin

Gas waste

B101 – Blower C101 – Cooler 1

E101 – Multistage Evaporator 1E102 – Multistage Evaporator 2E103 – Multistage Evaporator 3

H101 – Heat Exchanger 1 H102 – Heat Exchanger 2

H103 – Heater 3H104 – Heater 4

H107 – Heat Exchanger 7P101 – Pump 1P102 – Pump 2

8

9

11

12

10

15

13

19

24

28

31

34

35

Ash

F101 – CentrifugeH105 – Heat Exchanger 5H106 – Heat Exchanger 6H108 – Heat Exchanger 8H109 – Heat Exchanger 9

R101 – Interesterification Reactor S101 – Separator 1

D101 – Spray DryerH111 – Heat Exchanger 11

P103 – Pump 3S102 – Separator 2

Air

Methanol

GMS

Organic Waste

P101

P102

H101

E101 E102 E103

B101

F101

R101

S101 S102

D101

H103

NaOH Catalyst

Faculty of Engineering and Built Environment

Department of Chemical and Process Engineering

Group: KK1

Date:2 March 2015

Scale:Not to Scale

Stream Number

Input

Output

Project:P&ID of Glycerol Monostearate

(after heat integration)

Supervisor of Project:1. Prof. Dr. Abu Bakar Mohamad2. Prof Madya IR. Dr. Masturah Markom3. Dr. Manal Ismail4. Pn. Reehan Adne Ab. Rahim

Drawn by :Noor Shazleen Sharfadeen (A136900)Chew Li Wen(A136541)Ahmad Hafizuddin Bin Mohd Roston(A135895)Afifah Syafiqah Zolkifli(A136280)Nor Zuraini binti Che Hashim(A136485)Hosaini Faiz(A138796)

H104

C101

H105

H106

H109

P103

H108

H107

H110

H111

H102

30

17

18

38

45

22

26

10

12

34

6 7 14

16

20

25

23

2729

32

33

36

37

42 43 44

47

46

V-1

TC

TT

V-2

TC

TT

FC

FT

V-3

V-4 PC

PT

PC

PT

FC

FT

V-5

V-6

V-7

PC

PT

LC

LT

V-8V-9 T

C

TT

V-10 TC

TT

V-11

TC

TT

V-12

TC

TT

V-13

TC

TT

21

FC

FT

V-14 V-15

PC

PT

V-16TC

TT

414039

V-17

TC

TT

V-18

TC

TT

V-19

PC

PT

PC

PT

V-20

V-21 LC

LT

V-22

TC

TT

V-23

TC

TT

V-24LC

LT

V-26

TC

TT

V-25

PC

PT

V-27

LC

LT

V-28

TC

TT

5

PSV-E101 PSV-E102

PSV-E103

PSV-F101PSV-R101

PSV-S101 PSV-S102

PSV-D101

Figure 5.7 Piping and instrumentation diagram of the glycerol monostearate plant after heat

integration

Hv=2580

He=430

He=430

Hs = 2000

Manhole skirt

= 254

Ma

nh

ole

ve

sse

l

= 2

03

Di = 1720

S1

S2

S3

w =190

L = 250

Connection

Nominal size, (mm)

Minimum thickness,t

(mm)

A(mm) B(mm) OD(mm) K(mm) D(mm)

S1 (Mixture In) 80 12 49 14 27.0000 79 108

S2 (Catalysts In) 20 10 30 12 15 60 89

S3 (Mixture Out) 100 12 246 28 202 298 343

Manhole vessel 100 22 - 28 - 298 343

Manhole skirt 254 22 - 30 - 362 406

Cross Sectional of

Welding Neck Flange

Top view of Reactor

R101

Cross Sectional of Reactor

R101

Cross Sectional of ManholeCross Sectional of Skirt

Support

Faculty of Engineering and Built

Environment

Department of Chemical and

Process Engineering

Project title:

Production of glycerol

monostearate from crude glycerol

Drawing title:

Continous Stirred Tank Reactor

with membrane wall, R101

Prepared by:

KK1

Drawn by:

Afifah Syafiqah binti Zolkifli

A136280

Groupmate:

Noor Shazleen binti Sharfadeen

A136900

Afifah Syafiqah binti Zolkifli

A136280

Nor Zuraini binti Che Hashim

A136485

Chew Li Wen

A136541

Ahmad Hafizuddin bin Mohd

Roston A135895

Hosaini Faiz

A138796

Date of submission:

28 May 2015

Scale:

Not To Scale

Drawing Number:

Revision:

Checked:Prof Ir Dr Siti Rozaimah

Sheikh Abdullah

Drawing Unit:

Milimeter

Design Specifications:

Operating Temperature: 200

degree Celcius

Operating Pressure: 200 kPa

Internal Diameter: 1720 mm

Outside Diameter: 1740 mm

Vessel Height: 3440 mm

Head Height: 430 mm

Wall Thickness: 10 mm

Corrosion Allowance: 2 mm

Material: Austenitic stainless steel

Type 316

Type of Head: Elipsoidal

Type of Support: Straight Skirt

Skirt Thickness: 22 mm

Type of Layout: Vertical

OD

B

D

K

A

D

K

PR

OD

UC

ED

B

Y A

N A

UT

OD

ES

K E

DU

CA

TIO

NA

L P

RO

DU

CT

PRODUCED BY AN AUTODESK EDUCATIONAL PRODUCT

PR

OD

UC

ED

B

Y A

N A

UT

OD

ES

K E

DU

CA

TIO

NA

L P

RO

DU

CT

PRODUCED BY AN AUTODESK EDUCATIONAL PRODUCT

Original copy : Afifah Syafiqah Binti Zolkifli

Summary Of Detail Design For Reactor CSTR R101

VESSEL JACKET VESSEL

Working volume (m3

) :6 Type of jacket :Cooling jacket

Assumption vessel filled :75% Spacing between jacket and vessel wall (mm) :35

Total volume (m3

) :8 Continuous spiral channel section (m2

) :7 x 10-3

Diameter (m) :1.72 Number of spirals :44

Height (m) :3.44 Hydraulic mean diameter, de (m) :0.0596

BAFFLES Velocity through channel (m/s) :3.72 x 10-3

Baffles width per each (m) :0.20 Type of flow region for cooling water :Laminar region (Re = 332)

Number of baffles used :4 heat transfer coefficient for jacket, hj (W/m

2

o

C) :427.55

Gap (m) :0.04 VESSEL

IMPELLER Type of flow region vessel :Turbulent region (Re = 4.2 x 105 )

Type of impeller :3 propeller six pitched blade turbine

impeller heat transfer coefficient inside vessel, h

v (W/m

2

o

C) :2412.85

Rotational speed impeller (rpm) :10 Overall heat transfer coefficient (W/m2

o

C) :355.13

Re impeller :5.1 x 105

Pressure drop, △P (N/m2

) :1.44

Power impeller, P (kW) :0.2

Up

HE-1

01

E-101C-101

YARD IMPROVEMENT

LOADING

AREA WAREHOUSE

WASTE

ORGANICASH

WASTE

LABORATORY

CANTEEN

SURAU

OFFICE

BUILDING

ASSEMBLY

POINT

H-103

H-104

R2

R1

COOLING TOWER

CONTROL

BUILDING

ELECTRIC

ROOM

SWITCH HOUSE

R3

R4

R-101

H-105

H-110

D-101STACK GAS

`

SECURITY

`

SECURITY

`

SECURITY

P1

P2

UNIT OPERATION

H-101/2/3/4/5 Heat exchanger

C-101/4/5 Reflux drum

C-102/3/6/7 Cooler

S-101 3 phase separator

R-101 Reactor interesterification

S-102 Decanter 1

E-101 Evaporator

S-103 Decanter 2

T-101 Spray dryer

CODE

R1

R2

R3

R4

P1

P2

DESIGNATION

TRISTEARIN STORAGE TANK

CRUDE GLYCEROL STORAGE TANK

HEXANE STORAGE TANK

AIR STORAGE TANK

GLYCEROL MONOSTEARATE (GMS) STORAGE TANK

METHANOL BY-PRODUCT

SYMBOL DESIGNATION

RESTRICTED AREA

BUILDING

ROOF

OWNER :

DEPARTMENT OF PROCESS

AND CHEMICAL

ENGINEERING

UKM BANGI

DRAWING TITLE :

PRODUCTION OF GLYCEROL

MONOSTEARATE (GMS) FROM

CRUDE GLYCEROL

(GROUP KK1)

SCALE : NOT TO SCALE

TEAM MEMBERS :

Noor Shazleen Sharfadeen A136900

Chew Li Wen A136541

Ahmad Hafizuddin

Mohd Roston A135895

Afifah Syafiqah Zolkifli A136280

Nor Zuraini Che Hashim A136485

Hosaini Faiz A138796

SUPERVISOR :

Prof. Dr. Abu Bakar Bin Mohamad

Prof. Madya Ir. Dr. Masturah Binti

Markom

Dr. Manal Binti Ismail

Puan Reehan Adne Abdul Rahim

SUBMISSION DATE :

3 APRIL 2015

Wind power : 11 rpm

Equipment layout referred to :

Technical Research Centre VTT

Publications “Inherent Safety in

Process Plant Design An Index-Based

Approach”

BOILER

TNB

SUBSTATION

HE-1

02

E-102

E-103

F-101

S-101

S-102

HE-106

HE-109

HE-111

HE-108

HE-107