Report No D3110-13 - apps2.staffordshire.gov.uk

Report No D3110-13 GNOSALL ST LAWRENCE PRIMARY SCHOOL, GNOSALL, STAFFORD FACTUAL REPORT ON GROUND INVESTIGATION Carried out for: Education Funding Agency Engineer: Mott MacDonald Ltd November 2013

www.esg.co.uk Environmental Scientifics Group Limited

Reg office: ESG House, Bretby Business Park, Ashby Road, Burton upon Trent, DE15 0YZ Incorporated in England: 02880501

Issue No Date Details 1.0 November 2013 Draft Report 2.0 November 2013 Final Report

The title to this report is vested in the Employer named but title to copyright is retained. The Contracts (Rights of Third Parties) Act 1999 does not apply to the contract with the Employer and the provisions of the said Act are hereby excluded.

GNOSALL ST LAWRENCE PRIMARY SCHOOL, GNOSALL, STAFFORD FACTUAL REPORT ON GROUND INVESTIGATION

Unit 4, Gainsborough Trading Estate, Leamington Road, Southam, Warwickshire, CV47 1RA, UK

Tel: +44 (0) 1926 819300 Fax: +44 (0) 1926 815030 email: [email protected]

Report No: D3110-13

Date: November 2013

Employer: Education Funding Agency 33 Greycoat Street London SW1P 2QF

Engineer: Mott MacDonald Ltd 35 Newhall Street Birmingham B3 3PU

November 2013 Report No D3110-13 Issue 2.0 Page 1 of 6

C O N T E N T S

Page 1 INTRODUCTION 2 2 THE SITE AND GEOLOGY 2 2.1 The Site 2.2 Published Geology 3 FIELDWORK 3 3.1 General 3.2 Exploratory Holes 3.3 Instrumentation and Monitoring 4 LABORATORY TESTING 4 4.1 Geotechnical Testing 4.2 Geoenvironmental Testing REFERENCES 6 ENCLOSURES A EXPLORATORY HOLE RECORDS B INSTRUMENTATION AND MONITORING C GEOTECHNICAL LABORATORY TEST RESULTS D GEOENVIRONMENTAL LABORATORY TEST RESULTS E DRAWINGS


1 INTRODUCTION

In July 2013 Environmental Scientifics Group (ESG) was commissioned by Mott MacDonald Ltd,

on behalf of the Education Funding Authority, to carry out a ground investigation at Gnosall St

Lawrence Primary School, Lowfield Lane, Gnosall, Stafford. The investigation was required to

obtain preliminary geotechnical and geoenvironmental information to assist in the planning and

design of new development at the school as part of the Priority Schools Building Programme.

The scope of the investigation, which was specified by Mott MacDonald Ltd, comprised cable

percussion boreholes, windowless sampler boreholes and laboratory testing. The investigation

was carried out in accordance with the contract specification, Eurocode 7 and relevant related

standards identified below (see also References). The fieldwork was carried out between the 5th

and 7th August 2013.

This report presents the factual records of the fieldwork and laboratory testing undertaken. The

data is also presented separately in digital format following AGS (2005).

2 THE SITE AND GEOLOGY

2.1 The Site

Gnosall St Lawrence Primary School lies on the southern edge of Gnosall , see Site Location Plan

in Enclosure E, about 9km south east of Stafford. The site is at National Grid reference SJ 831

205.

The school grounds are roughly triangular in shape, bounded by Lowfield Lane on the north

eastern side. The A518 Stafford Road lies just to the north west together with an existing garage

and open land. A small wooded area lies at the south western boundary with a disused and

dismantled railway line on its southern side and open agricultural land beyond.

The existing school buildings lie at the northern end of the grounds, fronting onto Lowfield Lane,

with grassed playing fields to the south.


2.2 Published Geology

Published geological information covering the area, Geological Survey (GS) Sheet 139 'Stafford'

and the British Geological Survey (BGS) website, show superficial Glaciofluvial Sheet Deposits

underlying much of the site with Alluvium indicated along the south western side and Glacial Till to

the north east. Triassic age strata are the underlying bedrock with the Mercia Mudstone Group

shown beneath the north and east with the Bromsgrove Sandstone to the south west.

3 FIELDWORK

3.1 General

The fieldwork was carried out in general accordance with BS 5930+A2 (2010), BS EN 1997-2

(2007) and BS EN ISO 22475-1 (2006).

The exploratory hole locations were selected by Mott MacDonald Ltd and set out from local

features. The co-ordinates and reduced levels were surveyed by ESG to National Grid and

Ordnance Datum. The exploratory hole locations are shown on the Site Plan in Enclosure E.

3.2 Exploratory Holes

The exploratory holes are listed in the following table.

SUMMARY OF EXPLORATORY HOLES

TYPE QUANTITY MAXIMUM DEPTH (m) REMARKS

Cable Percussion Boring 5 6.40 BH1, BH2, BH3, BH4 and BH5

Windowless Sampler Boreholes 5 5.45 WS1, WS2, WS3, WS4 and WS5

The exploratory hole records are presented in Enclosure A and should be read in conjunction with

the Key which is included in that enclosure. The records provide descriptions of the materials

encountered in accordance with BS EN ISO 14688-1 (2002) and 14689-1 (2003), for soils and

rocks respectively, as amplified by BS 5930+A2 (2010). The records also give details of the

samples taken together with observations made during boring, windowless sampling and pitting.

Standard penetration tests (SPT) were carried out in accordance with BS EN ISO 22476-

3:2005+A1 (2011) in the boreholes and windowless sampler holes and the results are included on


the exploratory hole records. The SPT hammer energy ratio calibration certificates are also

included in Enclosure A.

On completion of the fieldwork geotechnical samples were transported to the Southam office of

ESG for temporary retention, with those required for testing being transferred to the in-house

Doncaster laboratory. Geoenvironmental samples were taken and stored in accordance with Mott

MacDonald Ltd requirements and BS EN ISO/IEC 17025 (2005) prior to and during transport to the

ESG Scientifics' Burton-on Trent laboratory.

3.3 Instrumentation and Monitoring

The instruments installed in the exploratory holes are shown on the logs and detailed in

Enclosure B. Records of groundwater and gas monitoring carried out by ESG after the fieldwork

period are presented in Enclosure B.

4 LABORATORY TESTING

4.1 Geotechnical Testing

The testing was scheduled by Mott MacDonald Ltd and was carried out in accordance with

BS 1377 (1990) unless otherwise stated. The testing is summarised below and the results are

presented in Enclosure C.

SUMMARY OF GEOTECHNICAL LABORATORY TESTING

TYPE REMARKS

Moisture Content Determination

Atterberg Limit Determination

Particle Size Distribution Analysis

Total Sulphate Content, Water Soluble Sulphate Content, Total Sulphur Content and pH Value of Soils

Testing by ESG Scientifics; test methods are BS 1377 or others recognised in BRE Special Digest 1 (2005); they are indicated on the results report sheets in Enclosure C

Organic Matter Content

Dry Density/Moisture Content Relationship (Light 2.5g compaction)

Moisture Condition Value/Moisture Content Relationship

California Bearing Ratio


REFERENCES

AGS : 2005 : Electronic transfer of geotechnical and geoenvironmental data (Edition 3.1 including addendum May 2005). Association of Geotechnical and Geoenvironmental Specialists.

Baldwin M, Gosling R C and Brownlie N : 2007 : Soil and rock descriptions - a practical guide to the implementation of BS EN ISO 14688 and 14689. Ground Engineering, July.

BRE Special Digest 1 : 2005 : Concrete in aggressive ground. Building Research Establishment.

BS 1377 : 1990 : Methods of test for soils for civil engineering purposes. British Standards Institution.

BS 5930+A2 : 2010 : Code of practice for site investigations (Amendment 2). British Standards Institution.

BS EN 1997-2 : 2007 : Eurocode 7 - Geotechnical design - Part 2 Ground investigation and testing. British Standards Institution.

BS EN ISO 14688-1 : 2002 : Geotechnical investigation and testing - Identification and classification of soil - Part 1 Identification and description. British Standards Institution.

BS EN ISO 14689-1 : 2003 : Geotechnical investigation and testing - Identification and classification of rock - Part 1 Identification and description. British Standards Institution.

BS EN ISO 22475-1 : 2006 : Geotechnical investigation and testing – Sampling methods and groundwater measurements - Part 1 Technical principles for execution. British Standards Institution.

BS EN ISO 22476-3:2005+A1 : 2011 : Geotechnical investigation and testing - Field testing - Part 3 Standard penetration test. British Standards Institution.

BS EN ISO/IEC 17025 : 2005 : General requirements for the competence of testing and calibration laboratories. British Standards Institution.

GIFA10 : 2010 : Ground Investigation Services Framework Agreement. Mott Macdonald Ltd.

GS England and Wales Sheet 139 : 1950 : Stafford. 1:633600 geological map (solid and drift). Geological Survey of England and Wales

November 2013 Report No D3110-13 Issue 2.0 Enclosure A

ENCLOSURE A

EXPLORATORY HOLE RECORDS

Key to Exploratory Hole Records Key

Hammer Energy Ratio Report Calibration certificates for JH1 and 120 38BH

Borehole Logs BH1, BH2, BH3, BH4 and BH5

Windowless Sampler Logs WS1, WS2, WS3, WS4 and WS5

Notes: See report text for full references of standards

Project

Project No. Carried out for

GNOSALL ST LAWRENCE PRIMARY SCHOOL

D3110-13 Education Funding Agency

Key Sheet 1 of 2

Key to Exploratory Hole Records

SAMPLES Undisturbed U UT TW P L CBR BLK CS AMAL

Driven tube sample Driven thin wall tube sample nominally 100 mm diameter and full recovery unless otherwise stated Pushed thin wall tube sample Pushed piston sample Liner sample (from Windowless or similar sampler), full recovery unless otherwise stated CBR mould sample Block sample Core sample (from rotary core) taken for laboratory testing Amalgamated sample

Disturbed D B

Small sample Bulk sample

Other W G ES EW

Water sample Gas sample Environmental chemistry samples (in more than one container where appropriate) Soil sample Water sample

Comments Sample reference numbers are assigned to every sample taken. A sample reference of 'NR' indicates that attempt was made to take a tube sample, however, there was no recovery. Monitoring samples taken after completion of hole construction are not shown on the exploratory hole logs.

TESTS SPT S or SPT C IV HV PP KFH, KRH, KPI

Standard Penetration Test, open shoe (S) or solid cone (C) The Standard Penetration Test is defined in BS EN ISO 22476-3 (2005). The incremental blow counts are given in the Field Records column; each increment is 75 mm unless stated otherwise and any penetration under self weight in mm (SW) is noted. Where the full 300 mm test drive is achieved the total number of blows for the test drive is presented as N = ** in the Test column. Where the test drive blows reach 50 the total blow count beyond the seating drive is given (without the N = prefix). in situ Vane shear strength, peak (p) and remoulded (r) Hand vane shear strength, peak (p) and remoulded (r) Pocket penetrometer test, converted to shear strength Permeability tests (KFH = falling head, KRH = rising head; KPI = packer inflow); results provided in Field Records column (one value per stage for packer tests)

DRILLING RECORDS The mechanical indices (TCR/SCR/RQD & If) are defined in BS 5930+A2 (2010)

TCR SCR RQD If

Total Core Recovery, % Solid Core Recovery, % Rock Quality Designation, % Fracture spacing, mm. Minimum, typical and maximum spacings are presented. The term non-intact (NI) is used where the core is fragmented.

Flush returns, estimated percentage with colour where relevant, are given in the Records column CRF AZCL NR

Core recovered (length in m) in the following run Assessed zone of core loss Not recovered

GROUNDWATER

Groundwater strike Groundwater level after standing period

Notes: See report text for full references of standards

Project

Project No. Carried out for

GNOSALL ST LAWRENCE PRIMARY SCHOOL


Key Sheet 2 of 2

Key to Exploratory Hole Records

INSTALLATION Standpipe/ piezometer SP SPIE PPIE EPIE Inclinometer or Slip Indicator ICE ICM SLIP Settlement Points or Pressure Cells ESET ETM EPCE PPCE

Details of standpipe/piezometer installations are given on the Record. Legend column shows installed instrument depths including slotted pipe section or tip depth, response zone filter material type and layers of backfill. The type of instrument installed is indicated by a code in the Legend column at the depth of the response zone: Standpipe Standpipe piezometer Pneumatic piezometer Electronic piezometer The installation of vertical profiling instruments is indicated on the Record. The base of tubing is shown in the Legend column. The type of instrument installed is indicated by a code in the Legend column at the base of the tubing: Biaxial inclinometer Inclinometer tubing for use with probe Slip indicator The installation of single point instruments is indicated on the Record. The location of the measuring device is shown in the Legend column. The type of instrument installed is indicated by a code in the Legend column: Electronic settlement cell/gauge Magnetic extensometer settlement point Electronic embedment pressure cell Electronic push in pressure cell

INSTALLATION LEGENDS

A legend describing the installation is shown in the rightmost column. Legends additional to BS5930 are used to describe the backfill materials as indicated below.

Arisings

Concrete

Grout

Bentonite

Sand

Gravel

Macadam

NOTES 1 2 3 4 5 6 7 8

Soils and rocks are described in accordance with BS EN ISO 14688-1 (2002) and 14689-1 (2003) respectively as amplified by BS 5930+A2 (2010). For fine soils, consistency determined during description is reported for those strata where undisturbed samples are available. Where the logger considers that the sample may not be representative of the condition in situ, for whatever reason, the reported consistency is given in brackets. The reliability of the sample is indicated by Probably or Possibly as appropriate. Hence (Probably firm) indicates the logger is reasonably confident of the assessment, but (Possibly firm) means less certainty. Where the samples available are too disturbed to allow a reasonable assessment of the in situ condition, no consistency is given. Evidence of the occurrence of very coarse particles (cobbles and boulders) is presented on the logs, however, because of their size in relation to the exploratory hole these records may not be fully representative of their size and frequency in the ground mass. The declination of bedding and joints is given with respect to the normal to the core axis. Thus in a vertical borehole this will be the dip. The assessment of SCR, RQD and Fracture Spacing excludes artificial fractures Strata legends are in accordance with BS 5930+A2 (2010). Water level observations of discernible entries during the advancing of the exploratory hole are given at the foot of the log and in the Legend column. The term "none observed" is used where no discrete entries are identified although this does not necessarily indicate that the hole has not been advanced below groundwater level. Under certain conditions groundwater cannot be observed, for instance, drilling with water flush or overwater, or boring at a rate much faster than water can make its way into the borehole (ref BS5930+A2:2010, Clause 47.2.7). In addition, where appropriate, water levels in the hole at the time of recovering individual samples or carrying out in situ tests and at shift changes are given in the Records column. The borehole logs present the results of Standard Penetration Tests recorded in the field without correction or interpretation. However, in certain ground conditions (eg high hydraulic head or where very coarse particles are present) some judgement may be necessary in considering whether the results are representative of in situ mass conditions.

Updated March 2012

SPT Hammer Energy Test Reportin accordance with BSEN ISO 22476-3:2005

JHl.spt

TPTest Operator:

SPT Hammer Ref: JH1

Test Date: 26/07/2012

Report Date:

File Name:

Dynamic sampling uk ltdunit 2 new zealand courtkingsway park dosekingsway ind parkderbyDE223FP

Instrumented Rod DataDiameter dr (mm):

Wall Thickness tr (mm):

Assumed Modulus Ea (GPa):

Accelerometer NO.1:

Accelerometer NO.2:

54

6.9200

6455

6457

SPT Hammer InformationHammer Mass m (kg): 63.5

Falling Height h (mm): 750

SPT String Length L (m): 15.0

Comments I LocationHammer tested at Dynamic sampling yard.

Velocity

Displacement

2 3 4 5 6 7 8 9 10Time (ms)

2 3 4 5 6 7 8 9 10Time (ms)

Force5

4

u3CD.!!2E

1

0

2 3 4 5 6 7 8 9 10 0

Time (ms)

Acceleration

0

-2

EE-4

-6

-82 3 4 5 6 7 8 9 10 0

Time (ms)o

20,000

15,000

~ 10,000

~ 5,000o

-5,000

250

200

150

~ 100

50o

-soo

CalculationsArea of Rod A (mm2): 1021

Theoretical Energy ~heor (J): 473

Measured Energy Emeas (J): 413

Energy Ratio Er (%): ~,[ _87 IT.parker

operations manager

SPTMAN ver.1.92 All rights reserved, Testconsult@2010

1:50

Time Tools usedFrom to (m)

Checked

Equipment, Methods and Remarks

Backfill/

Coordinates

ChisellingDepths (m)

Samples and Tests

Project

to

No. Post strike behaviour Depth sealed

Project No.Carried out for

Diameter Casing Depth

StrataDepth Date Time Depth,Level Legend

Start

End

(Thickness)Casing Water

Groundwater EntriesStruck

Notes: For explanation of symbols and

Instruments

(m)

abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.

Description

Depth from

Borehole

Scale

Depth Related Remarks *

Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole Log

None observed (see Key Sheet)

JHGMJRL

07/08/2013

07/08/2013

Type & No

Type & No

Pilcon 1500Service inspection pit hand excavated to 1.20mCable percussion to 5.00m

Records

Records

426.4818/11/2013 10:58:10(c) ESG www.esg.co.uk

GNOSALL St LAWRENCE PRIMARY SCHOOL

D3110-13Education Funding Agency

National Grid

Chainage

BH1Sheet 1 of 1

+104.25 mODE 383110.63N 320661.83

1.20 4.70 SPT hammer ID JH1

5.00m0.00m 150mm 4.50m

4.40 -4.70 60 mins

*

4.00-4.40 mDense to very

dense

0.100.10-0.50

0.30

0.600.60

0.80-1.20

1.101.20-1.651.20-1.65

1.902.00-2.45

2.002.00-2.45

2.60

3.00-3.453.00

3.00-3.45

3.904.00-4.454.00-4.454.00-4.50

4.70-4.984.70-4.97

D 1B 3

ES 2

D 4ES 5B 6

ES 7SPT C

B 8

ES 9SPT CD 10B 11

D 12

SPT CES 13B 14

D 15SPT SD 16B 17

SPT SD 18

N=8 (1,1/2,1,2,3)

N=11 (1,2/2,2,3,4)

N=9 (1,2/3,2,2,2)

N=50 (2,3/7,9,15,19)

50 (9,12/21,29 for 50mm)

1.20

1.50

3.00

4.00

4.50

dry

dry

dry

dry

dry

0.05

0.50

2.50

4.40

5.00

(0.45)

(2.00)

(1.90)

(0.60)

+104.20

+103.75

+101.75

+99.85

+99.25SP

MADE GROUND: macadam.

MADE GROUND: black sandy GRAVEL with lowcobble content. Gravel is angular fine tocoarse macadam, sandstone and clinker.Cobbles are sandstone and brick.

MADE GROUND: loose to medium dense brownclayey very gravelly fine to coarse SANDwith low cobble content. Gravel isrounded to angular fine to coarsequartzite, slag, sandstone and rare brick.Cobbles are brick.

Loose to medium dense, becoming dense tovery dense, light brown gravelly fine tomedium SAND with rare soft reddish brownsandy clay pockets. Gravel is angular torounded sandstone, quartzite and raremudstone.(GLACIOFLUVIAL SHEET DEPOSITS)

Extremely weak light reddish brown finegrained SANDSTONE. Recovered as sand andgravel.(BROMSGROVE SANDSTONE FORMATION)

EXPLORATORY HOLE ENDS AT 5.00 m

http://www.esg.co.uk/

sandstone.(GLACIOFLUVIAL SHEET DEPOSITS)

Stiff brown slightly sandy slightlygravelly CLAY with rare silt pockets.Gravel is angular to rounded fine tomedium quartzite and sandstone.(Possible GLACIAL TILL)

Extremely weak to very weak light greyishbrown fine grained SANDSTONE.(BROMSGROVE SANDSTONE FORMATION)


1:50


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Backfill/

Coordinates


Samples and Tests

Project

to





Start

End




Instruments

(m)


Description

Depth from

Borehole

Scale


Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole Log


JHGMJRL

07/08/2013

07/08/2013

Type & No

Type & No


Records

Records

426.4818/11/2013 10:58:16(c) ESG www.esg.co.uk



National Grid

Chainage

BH2Sheet 1 of 1

+102.14 mODE 383082.68N 320603.89


5.50m0.00m 150mm 5.00m

5.30 -5.43 60 mins

*

0.100.15

0.20-0.700.300.50

0.90-1.201.00

1.20-1.651.20

1.20-1.65

2.002.10-2.552.10-2.55

2.903.00-3.453.00-3.45

3.90

4.10-4.554.10-4.55

4.905.00-5.385.00-5.355.00-5.305.40-5.50

5.405.40-5.49

D 1ES 2B 5D 3

ES 4

B 8D 6

SPT CES 7B 9

D 10SPT CB 11

D 12SPT CB 13

D 14

SPT CB 15

D 16SPT SD 17B 18

SPT CD 19B 20

N=18 (2,3/3,4,5,6)

N=19 (2,3/5,5,4,5)

N=13 (1,2/2,3,4,4)

N=20 (8,7/5,4,5,6)

50 (4,5/8,9,33)

50 (25 for 50mm/50 for 45mm)

1.20

1.70

3.00

4.00

5.00

5.00

dry

dry

dry

dry

dry

dry

0.050.20

0.90

1.40

4.80

5.30

5.50

(0.70)

(0.50)

(3.40)

(0.50)

+102.09+101.94

+101.24

+100.74

+97.34

+96.84

+96.64SP


MADE GROUND: black sandy GRAVEL of ashand macadam.

Brown SAND and GRAVEL with low cobblecontent and rare reddish brown sandy claypockets. Sand is medium to coarse. Gravelis subangular to rounded fine to coarsesandstone and quartzite. Cobbles arequartzite.(GLACIOFLUVIAL SHEET DEPOSITS)

Brown silty gravelly fine to coarse SAND.Gravel is subangular to rounded fine tomedium sandstone and quartzite.(GLACIOFLUVIAL SHEET DEPOSITS)

Medium dense brown very sandy GRAVEL withlow cobble content and rare firm reddishbrown sandy clay pockets. Gravel issubangular to rounded fine to coarsequartzite and sandstone. Cobbles are


TOPSOIL.

Brown slightly silty gravelly fine tomedium SAND. Gravel is subangular torounded fine to coarse quartzite andsandstone.(GLACIOFLUVIAL SHEET DEPOSITS)

Firm, becoming soft to firm, reddish brownslightly sandy slightly gravelly CLAYwith rare light grey very sandy clay andblack silt pockets. Gravel is rounded tosubrounded fine to medium sandstone andquartzite.(GLACIOFLUVIAL SHEET DEPOSITS)

Loose brown slightly clayey slightlygravelly medium SAND. Gravel is subangularto rounded fine to coarse quartzite andsandstone.(GLACIOFLUVIAL SHEET DEPOSITS)

Firm brown slightly gravelly sandy CLAY.Gravel is angular to subangular finequartzite, sandstone and mudstone.(GLACIOFLUVIAL SHEET DEPOSITS)

Medium dense brown silty very sandy GRAVELwith low cobble content. Gravel isrounded fine to coarse quartzite andsandstone. Cobbles are sandstone.(GLACIOFLUVIAL SHEET DEPOSITS)

Extremely weak to very weak reddish brownsilty fine to medium grained SANDSTONE.Recovered as subangular fine to coarsegravel.(BROMSGROVE SANDSTONE FORMATION)


1:50


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Coordinates


Samples and Tests

Project

to





Start

End




Instruments

(m)


Description

Depth from

Borehole

Scale


Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole LogJHGMJRL

06/08/2013

06/08/2013

Type & No

Type & No


Records

Records

426.4818/11/2013 10:58:20(c) ESG www.esg.co.uk



National Grid

Chainage

BH3Sheet 1 of 1

+98.17 mODE 383046.90N 320562.72

0.601 Seepage -1.702 Rose to 1.40 m after 20 minutes. Slow -


6.40m0.00m 150mm 5.80m

5.80 -6.20 60 mins

*1.30-1.60 m

Becoming soft tofirm.

4.10-4.50 m Sandis fine to medium.

0.000.000.200.300.30

0.70

0.90

1.20-1.651.201.20

1.70

2.00-2.452.00

2.80

3.00-3.453.003.00

4.004.10-4.55

4.104.10

4.80

5.00-5.455.00

5.80-6.125.80

6.20-6.40

EW 19EW 20

B 3D 1

ES 2

ES 4

D 5

SPT SES 6D 7

D 8

SPT CB 9

D 10

SPT SD 11B 12

D 13SPT SD 14B 15

D 16

SPT CB 17

SPT CD 18

SPT C

N=11 (1,2/3,2,3,3)

N=9 (1,1/2,2,3,2)

N=12 (1,2/2,3,4,3)

N=16 (3,4/4,5,3,4)

N=17 (2,3/3,4,5,5)

50 (10,12/18,23,9 for 20mm)

50 (9,16 for 35mm/40,10 for 15mm)

1.20

2.00

3.00

4.00

4.50

5.80

5.80

damp

1.80

damp

damp

dry

dry

dry

0.20

0.80

1.60

2.70

4.50

5.70

6.40

(0.60)

(0.80)

(1.10)

(1.80)

(1.20)

(0.70)

+97.97

+97.37

+96.57

+95.47

+93.67

+92.47

+91.77

1

2

2

SP



Checked


Backfill/

Coordinates


Samples and Tests

Project

to





Start

End




Instruments

(m)


Description

Depth from

Borehole

Scale


Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole Log


JHGMJRL

05/08/2013

05/08/2013

Type & No

Type & No


Records

Records

426.4818/11/2013 10:58:27(c) ESG www.esg.co.uk



National Grid

Chainage

BH4Sheet 1 of 1

+99.66 mODE 383189.91N 320505.55


4.00m0.00m 150mm 3.80m

3.60 -3.90 60 mins

*

0.000.200.20

0.20-0.600.500.70

0.80-1.20

1.00

1.20-1.651.20-1.65

1.902.00-2.45

2.002.00-2.40

2.70

3.00-3.453.00

3.00-3.453.00-3.50

3.60-3.743.60

3.60-3.733.90-4.00

3.90

EW 19D 1

ES 2B 3

ES 4D 5B 6

ES 7

SPT CB 8

ES 9SPT CD 10B 11

D 12

SPT SES 13D 14B 15

SPT SD 16D 17

SPT CD 18

N=6 (1,1/1,1,2,2)

N=7 (1,1/1,1,2,3)

N=21 (2,3/3,5,6,7)

50 (19,6 for 10mm/50 for 50mm)

50 (25 for 60mm/50 for 40mm)

1.20

2.00

3.00

3.80

3.80

dry

dry

damp

damp

damp

0.15

0.60

2.20

3.50

4.00

(0.45)

(1.60)

(1.30)

(0.50)

+99.51

+99.06

+97.46

+96.16

+95.66

SP

TOPSOIL.

MADE GROUND: brown and black gravelly fineto coarse SAND. Gravel is angular torounded fine to coarse clinker, slag,quartzite and sandstone.

MADE GROUND: loose light brown slightlysilty very gravelly fine to medium SAND.Gravel is subangular to rounded fine tocoarse predominantly quartzite andsandstone with rare clinker, slag andbrick.

Medium dense brown clayey gravelly fine tomedium SAND with low cobble content.Gravel is subrounded to rounded fine tomedium sandstone and rare quartzite.Cobbles are sandstone.(GLACIOFLUVIAL SHEET DEPOSITS)

Extremely weak to very weak brown finegrained SANDSTONE.(BROMSGROVE SANDSTONE FORMATION)


1:50


Firm to stiff brown slightly gravellysandy CLAY. Gravel is subangular torounded fine to medium sandstone.(Possible GLACIAL TILL)

Dense to very dense brown gravellypredominantly fine to medium SAND withfrequent clay pockets. Gravel issubangular fine to coarse sandstone.(Possible BROMSGROVE SANDSTONEFORMATION)

Extremely weak brown fine grainedSANDSTONE. Recovered as angular tosubangular fine to coarse gravel.(BROMSGROVE SANDSTONE FORMATION)


1:50


Checked


Backfill/

Coordinates


Samples and Tests

Project

to





Start

End




Instruments

(m)


Description

Depth from

Borehole

Scale


Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Borehole Log


JHGMJRL

06/08/2013

06/08/2013

Type & No

Type & No

Pilcon 1500Service inspection pit hand excavated to 1.20mCable percusson to 6.20m

Records

Records

426.4818/11/2013 10:58:32(c) ESG www.esg.co.uk



National Grid

Chainage

BH5Sheet 1 of 1

+99.18 mODE 383248.49N 320428.97


6.20m0.00m 150mm 6.00m

5.50 -6.05 60 mins

*

0.200.20

0.20-0.600.50

0.90

1.101.20-1.651.20-1.651.20-1.70

2.00

2.20-2.652.20-2.65

3.00-3.453.00

3.00-3.45

3.70

4.00-4.454.00-4.454.00-4.50

4.80

5.00-5.455.00-5.455.00-5.50

6.00-6.226.00

D 1ES 2B 3

ES 4

D 5

ES 6SPT S

D 7B 8

D 9

SPT CB 10

SPT CD 11B 12

D 13

SPT SD 14B 15

D 16

SPT SD 17B 18

SPT CD 19

N=19 (2,4/4,5,6,4)

N=9 (1,1/1,2,2,4)

N=15 (1,2/2,4,4,5)

N=16 (2,2/3,4,4,5)

N=50 (3,4/6,10,13,21)

50 (9,16 for 55mm/39,11 for 15mm)

1.20

1.50

3.00

4.00

4.50

6.00

dry

damp

damp

dry

dry

dry

0.15

0.80

1.20

3.30

4.70

5.40

6.22

(0.65)

(0.40)

(2.10)

(1.40)

(0.70)

(0.82)

+99.03

+98.38

+97.98

+95.88

+94.48

+93.78

+92.96 SP

TOPSOIL.

MADE GROUND: brown slightly gravelly sandyCLAY with low cobble content. Gravel isangular to rounded fine to coarsesandstone and quartzite. Cobbles arelimestone.

MADE GROUND: firm brown mottled greyishbrown slightly gravelly sandy CLAY. Sandis fine. Gravel is subangular fine tomedium quartzite and rare slag. Rare blacksilt pockets.

Loose to medium dense brown slightly siltygravelly fine to medium SAND with raresandy clay pockets. Gravel is subangularto subrounded fine to coarse predominantlyquartzite with rare sandstone andmudstone.(GLACIOFLUVIAL SHEET DEPOSITS)



Checked


Backfill/

Coordinates


Samples and Tests

Project

to





Start

End




Instruments

(m)


Description

Depth from

Borehole

Scale


Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Window Sampler Hole Log


MPGMJRL

05/08/2013

05/08/2013

Type & No

Type & No

Service inspection pit hand excavated to 1.20mWindowless sampler to 3.80mRefusal at 3.80m

Records

Records

426.4818/11/2013 10:58:36(c) ESG www.esg.co.uk



National Grid

Chainage

WS1Sheet 1 of 1

+103.89 mODE 383097.88N 320646.63

1.20 3.80 SPT hammer ID 120 38BH

*

3.80 m Verydense, possible

bedrock

0.100.20-0.50

0.30

0.50-1.000.60

1.20-1.651.20-2.00

1.50

2.00-2.452.00-3.00

2.50

3.00-3.453.00-3.80

3.80-3.81

ES 1B 3

ES 2

B 5ES 4

SPT SB 7

D 6

SPT SB 9

D 8

SPT SB 10

SPT S

N=8 (2,2/2,2,2,2)

N=14 (3,4/4,3,3,4)

N=20 (4,4/5,5,5,5)

(50 for 10mm)

0.080.20

2.00

3.80

(1.80)

(1.80)

+103.81+103.69

+101.89

+100.09


MADE GROUND: black and brown sandyGRAVEL. Sand is fine to coarse. Gravel isangular fine to coarse sandstone, macadam andrare slag.

Loose brown silty very gravelly fine tocoarse SAND with rare firm sandy claypockets. Gravel is subangular to roundedfine to coarse sandstone, quartzite andrare mudstone.(GLACIOFLUVIAL SHEET DEPOSITS)

Medium dense brown slightly silty gravellyfine to medium SAND. Gravel is subangularto rounded medium to coarse quartzite andsandstone.(GLACIOFLUVIAL SHEET DEPOSITS)


1:50



Checked


Backfill/

Coordinates


Samples and Tests

Project

to





Start

End




Instruments

(m)


Description

Depth from

Borehole

Scale


Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged



MPGMJRL

05/08/2013

05/08/2013

Type & No

Type & No

Service inspection pit hand excavated to 1.20mWindowless sampler to 3.60mRefusal at 3.60m

Records

Records

426.4818/11/2013 10:58:40(c) ESG www.esg.co.uk



National Grid

Chainage

WS2Sheet 1 of 1

+104.20 mODE 383120.43N 320614.13


*

3.30-3.38 mReddish brown

mottled lightgreenish grey

slightly gravellysandy clay

band/pocket

0.100.20-0.60

0.30

0.60-1.000.70

1.20-1.651.20

1.70

2.00-2.452.00-3.00

2.50

3.00-3.45

3.30

3.503.60-4.00

ES 1B 3

ES 2

B 5ES 4

SPT SES 6

D 7

SPT SB 9

D 8

SPT S

D 10

D 11SPT S

N=8 (2,2/2,2,2,2)

N=18 (3,3/4,4,5,5)

N=12 (2,2/2,2,3,5)

50 (8,8/13,13,14,10 for 20mm)

0.080.20

3.60

(3.40)

+104.12+104.00

+100.60


MADE GROUND: dark brown and black slightlysandy GRAVEL of angular fine to coarsemacadam and sandstone.

Loose becoming medium dense brown slightlysilty very gravelly fine to coarse SANDwith occasional slightly sandy gravellyclay bands/pockets and rare black siltpockets. Gravel is subangular tosubrounded fine to coarse quartzite,sandstone and rare mudstone.(GLACIOFLUVIAL SHEET DEPOSITS)


1:50


1:50


Checked


Backfill/

Coordinates


Samples and Tests

Project

to





Start

End




Instruments

(m)


Description

Depth from

Borehole

Scale


Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Window Sampler Hole LogMPGMJRL

05/08/2013

05/08/2013

Type & No

Type & No

Service inspection pit hand excavated to 1.20mWindowless sampler to 5.00m

Records

Records

426.4818/11/2013 10:58:44(c) ESG www.esg.co.uk



National Grid

Chainage

WS3Sheet 1 of 1

+101.17 mODE 383046.73N 320587.04

3.001 Rose to 2.60 m after 20 minutes. -1.20 5.00 SPT hammer ID 120 38BH

*

0.200.20-0.70

0.300.50

0.800.901.00

1.20-1.65

1.50

1.80

2.00-2.45

2.50

3.00-3.45

3.20

3.50

4.00-4.45

4.20

4.80

5.00-5.45

ES 1B 4D 2

ES 3

ES 5D 6

ES 7

SPT S

D 8

D 9

SPT S

ES 10

SPT S

D 11

D 12

SPT S

D 13

D 14

SPT S

N=9 (1,2/2,3,2,2)

N=7 (1,1/1,1,2,3)

N=11 (2,2/2,2,3,4)

N=19 (1,1/4,5,5,5)

N=20 (5,5/5,5,5,5)

0.12

0.75

1.85

2.20

3.45

4.00

5.00

(0.63)

(1.10)

(0.35)

(1.25)

(0.55)

(1.00)

+101.05

+100.42

+99.32

+98.97

+97.72

+97.17

+96.17

1

1

Soft dark brown slightly sandy silty CLAY.Frequent rootlets. (TOPSOIL)

MADE GROUND: soft dark brown slightlysandy gravelly CLAY with medium cobblecontent. Sand is fine to coarse. Gravel isangular to rounded fine to coarsequartzite, brick, concrete, slag, slateand asbestos corrugated roof fragments.Cobbles are angular concrete and brick.

MADE GROUND: loose light brown gravellymedium to coarse SAND with low cobblecontent. Gravel is fine to coarsequartzite and rare brick, concrete andcoal. Cobble is brick.

Firm greyish brown slightly gravelly sandyCLAY. Gravel is fine to coarse subangularto rounded quartzite.(GLACIOFLUVIAL SHEET DEPOSITS)

Loose to medium dense brown slightly siltyslightly gravelly medium SAND. Gravel isangular to rounded fine to coarsequartzite and sandstone.(GLACIOFLUVIAL SHEET DEPOSITS)

Firm brown slightly sandy slightlygravelly to gravelly CLAY. Sand is fine tomedium. Gravel is subangular to roundedfine to coarse quartzite and sandstone.(GLACIOFLUVIAL SHEET DEPOSITS)

Medium dense brown slightly clayeygravelly medium SAND. Gravel is roundedfine to medium quartzite. (GLACIOFLUVIALSHEET DEPOSITS)




Checked


Backfill/

Coordinates


Samples and Tests

Project

to





Start

End




Instruments

(m)


Description

Depth from

Borehole

Scale


Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged

Window Sampler Hole LogMPGMJRL

05/08/2013

05/08/2013

Type & No

Type & No


Records

Records

426.4818/11/2013 10:58:49(c) ESG www.esg.co.uk



National Grid

Chainage

WS4Sheet 1 of 1

+101.58 mODE 383075.06N 320571.21

4.501 - -1.20 5.00 SPT hammer ID 120 38BH

*

3.40-3.48 m Firmreddish brown

slightly gravellysandy clay

0.100.20

0.400.50

0.50-1.00

1.20-1.65

1.50

2.00-2.452.00-3.00

2.50

3.00-3.453.00-4.00

3.403.50

4.00-4.45

4.50

5.00-5.45

D 1ES 2

D 3ES 4B 5

SPT S

ES 6

SPT SB 8

D 7

SPT SB 10

D 12D 9

SPT S

D 11

SPT S

N=6 (1,2/1,2,1,2)

N=10 (1,2/3,2,3,2)

N=17 (4,4/5,4,4,4)

N=6 (3,2/2,2,1,1)

N=8 (2,1/2,2,2,2)

0.30

5.00

(0.30)

(4.70)

+101.28

+96.58

1

Soft dark brown slightly gravelly sandyCLAY. Sand is predominantly fine tomedium. Gravel is subangular to roundedfine to medium quartzite. Frequentrootlets. (TOPSOIL)

Loose to medium dense brown silty verygravelly fine to coarse SAND withoccasional slightly gravelly sandy claypockets/bands. Gravel is angular torounded fine to coarse quartzite andsandstone.(GLACIOFLUVIAL SHEET DEPOSITS)


1:50



Checked


Backfill/

Coordinates


Samples and Tests

Project

to





Start

End




Instruments

(m)


Description

Depth from

Borehole

Scale


Drilled

Depth DateCasing

Time

(m)

Ground Level

Water

Logged



MPGMJRL

05/08/2013

05/08/2013

Type & No

Type & No


Records

Records

426.4818/11/2013 10:58:52(c) ESG www.esg.co.uk



National Grid

Chainage

WS5Sheet 1 of 1

+104.22 mODE 383162.73N 320576.99


*

3.50 m Refusal,possible bedrock

0.00-0.080.08-0.22

0.40

0.600.60-1.00

1.20-1.651.20

1.902.00-2.45

2.50

2.903.00-3.45

3.50-3.513.50

B 1B 2

D 3

ES 4B 5

SPT SES 6

D 7SPT S

ES 8

D 9SPT S

SPT SD 10

N=6 (1,1/2,2,1,1)

N=19 (3,4/4,5,5,5)

N=9 (3,3/3,2,2,2)

(50 for 10mm)

0.080.22

0.60

1.80

3.20

3.50

(0.38)

(1.20)

(1.40)

(0.30)

+104.14+104.00

+103.62

+102.42

+101.02

+100.72


MADE GROUND: black slightly sandy GRAVELof angular fine to medium sandstone,concrete and macadam.

MADE GROUND: brown very clayey slightlygravelly fine to medium SAND with highcobble content. Gravel is angular fine tocoarse brick fragments and roundedquartzite. Cobbles are brick and concrete.

MADE GROUND: loose brown slightly gravellyfine to medium SAND with rare firmreddish brown clay pockets. Gravel isrounded fine to coarse sandstone andquartzite with rare brick and concrete.

Medium dense light brown slightly gravellyto gravelly predominantly medium SAND.Gravel is fine to coarse quartzite andsandstone.(GLACIOFLUVIAL SHEET DEPOSITS)

Stiff reddish brown slightly sandyslightly gravelly CLAY. Gravel is roundedfine to coarse quartzite and sandstone.(Possible GLACIAL TILL)


1:50


November 2013 Report No D3110-13 Issue 2.0 Enclosure B

ENCLOSURE B

INSTRUMENTATION AND MONITORING

Installation Details B1

Groundwater Monitoring B2

Gas Monitoring

Hol

e N

o

Inst

rum

ent I

D

Inst

alla

tion

Typ

e

Dat

e of

Inst

alla

tion

Ref

eren

ce d

epth

(m

BG

L)

Pie

zom

eter

D

iam

eter

(m

m)

Top

of r

espo

nse

zone

(m

BG

L)

Bas

e of

res

pons

e zo

ne (

mB

GL)

Tub

ing

Com

plet

ion

Det

ails

Hea

dwor

ks Remarks

BH1 SP 7 Aug 2013 0.00 50 2.50 5.00 Gas tap Stop cock cover





Notes: Type: SP - Standpipe, SPIE - Standpipe Piezometer, HPIE - Hydraulic Piezometer, PPIE - Pneumatic Piezometer, EPIE - Electronic Piezometer Prepared: 04/11/2013 06:55



Project


B1

Groundwater Installation Details

Sheet 1 of 1

DateTime

(hhmmss)Comments

BH1 SP 4.7 0.00 28 Aug 2013 Dry

BH1 SP 4.7 0.00 19 Sep 2013 Dry

BH1 SP 4.7 0.00 4 Oct 2013 Dry

BH1 SP 4.7 0.00 11 Oct 2013 Dry

BH1 SP 4.7 0.00 17 Oct 2013 Dry

BH1 SP 4.7 0.00 31 Oct 2013 Dry

BH2 SP 5.4 0.00 28 Aug 2013 Dry

BH2 SP 5.4 0.00 19 Sep 2013 Dry

BH2 SP 5.4 0.00 4 Oct 2013 Dry

BH2 SP 5.4 0.00 11 Oct 2013 Dry

BH2 SP 5.4 0.00 17 Oct 2013 Dry

BH2 SP 5.4 0.00 31 Oct 2013 Dry

BH3 SP 1.7 0.00 28 Aug 2013 1.01

BH3 SP 1.7 0.00 19 Sep 2013 0.98

BH3 SP 1.7 0.00 4 Oct 2013 0.86

BH3 SP 1.7 0.00 11 Oct 2013 1.05

BH3 SP 1.7 0.00 17 Oct 2013 0.87

BH3 SP 1.7 0.00 31 Oct 2013 0.78

BH4 SP 4 0.00 28 Aug 2013 Dry

BH4 SP 4 0.00 19 Sep 2013 Dry

BH4 SP 4 0.00 4 Oct 2013 Dry

BH4 SP 4 0.00 11 Oct 2013 3.45

BH4 SP 4 0.00 17 Oct 2013 3.45

BH4 SP 4 0.00 31 Oct 2013 3.20

BH5 SP 6 0.00 28 Aug 2013 Dry

BH5 SP 6 0.00 19 Sep 2013 Dry

BH5 SP 6 0.00 4 Oct 2013 Dry

BH5 SP 6 0.00 11 Oct 2013 Dry

BH5 SP 6 0.00 17 Oct 2013 Dry

BH5 SP 6 0.00 31 Oct 2013 Dry

Reading

Hole ID

Inst

rum

ent

Typ

e

Ref

eren

ce

Dep

th(m

BG

L)

Head(m above Tip)

* calculated

Water Level (mBGL)

* calculated

Inst

rum

ent I

D

Bas

e of

In

stru

men

t(m

BG

L)

Notes: Type: SP - Standpipe, SPIE - Standpipe Piezometer, HPIE - Hydraulic Piezometer, PPIE - Pneumatic Piezometer, EPIE - Vibrating Wire Piezometer, PWEL - Pumping Well



Project


B2

Groundwater Monitoring

Sheet 1 of 1

Project No Project Sheet No

Date State of Ground 1Wind

Operator Wind Direction

Cloud CoverPrecipitation

Detection Limits

BH1Dry 0.0

5.8 0.00.0BH1 0.00 00:00:00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)

Differential Pressure

(Pa)

Time of Reading

hh:mm:ssInst

ID

Barometric Pressure(mbars)

Air temp

(oC)

2.8

0.0

Depth to Groundwater

(m BGL)

CH4(% vol)

O2(% vol)

19.9

0.0

0.20 0.0

2.8

78.5

78.5

78.5

19.9 2.8 0.0

19.9 2.9

0.0 19.8

0.0

2.9 0.00.0 77.2BH3 0.00 00:03:00

77.2

77.2

0.0

0.0

77.2

77.2

77.10.0

0.0

0.0

0.0

78.5

15.6 5.8 0.0

15.6 5.8 0.0

0.0

0.0

DryCalm

CloudyNone

78.778.5

78.5

79.2

78.8

78.8

78.8

78.8

78.8

77.8

19.9

78.8

19.6 2.6 0.0

19.9 2.8 0.0

0.0

0.0

20.6 0.5 0.00.0

20.7 0.5 0.0

20.7 0.4 0.0

0.0

0.0

20.7 0.4 0.0

20.7 0.4 0.0

0.0

0.0

20.1 0.6 0.0

20.7 0.4 0.0

0.0

0.0

0.015.6 5.8 0.0

5.8 0.0

0.0

0.0

5.8 0.0

1003 21

BH1 0.00 00:01:30

0.00 00:00:30

BH1 0.00 00:01:00 0.200.0

0.0

0.0

0.100.0

0.10 0.00.0

BH1 0.00 00:02:00 0.000.0

00:02:30BH1 0.00

BH1 0.00 00:03:00

0.20

0.0

Dry 0.00.00.00 00:00:00

BH2 0.00

BH2 0.00 00:00:30

00:01:30

BH2

1003

0.00

0.10

0.00 00:01:00 0.600.0

0.0

0.0

0.0

0.0

0.0

0.0

0.000.0

BH2 0.00 00:03:00

0.00

0.00 00:01:30

BH3

0.0

0.0

0.00 0.0

0.000.0

0.0

0.00

BH2

BH3

BH3 0.00 00:02:00 0.0

00:00:00

BH2 0.00 00:02:00

00:02:30BH2 0.00

BH3

BH3 0.00 00:01:00

BH3 0.00 00:00:30

0.00

00:02:30

0.001.01

0.0

0.0

0.000.0

0.0

0.0

0.0

0.0

0.0

0.0 15.8

0.0

0.0

0.0

15.6

5.4

15.6

15.7

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

Equipment Used LMSxi 1904 + Dip

1003

22

19

D3110-13

CH4(% LEL)

0.10 0.100.10

GNOSSALL St LAWRENCE PRIMARY SCHOOL

1.00 0.10

CO(ppm)

1.00

28/08/2013

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

Environmental Services Group Limited Gas Monitoring Record

Form IMS-SOP-SI-260-F1, 07/03





Detection Limits

BH4Dry 0.0

0.0 0.00.0BH4 0.00 00:00:00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)


(Pa)

Time of Reading

hh:mm:ssInst

ID


Air temp

(oC)

0.0


(m BGL)

CH4(% vol)

O2(% vol)

0.00 0.0

78.4

78.4

78.4

78.4

21.5 0.0 0.0

21.5 0.0 0.0

0.0

0.0

DryCalm

CloudyNone

78.978.3

78.4

78.7

78.4

78.4

78.4

78.3

78.3

78.421.2 0.3 0.00.0

21.2 0.3 0.0

21.2 0.3 0.0

0.0

0.0

21.2 0.4 0.0

21.2 0.3 0.0

0.0

0.0

20.8 0.4 0.0

21.2 0.4 0.0

0.0

0.0

0.021.5 0.0 0.0

0.0 0.0

0.0

0.0

0.0 0.0

1001 18

BH4 0.00 00:01:30

0.00 00:00:30

BH4 0.00 00:01:00 0.000.0

0.0

0.0

0.000.0

0.00 0.00.0

BH4 0.00 00:02:00 0.000.0

00:02:30BH4 0.00

BH4 0.00 00:03:00

0.00

0.0

Dry 0.00.00.00 00:00:00

BH5 0.00

BH5 0.00 00:00:30

00:01:30

BH5

1002

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.0

0.0

0.0

0.0

0.0

0.000.0

BH5 0.00 00:03:00

BH5

BH5 0.00 00:02:00

00:02:30BH5 0.00 0.0

0.0

0.0

0.0

0.0 21.0

0.0

0.0

0.0

21.5

0.0

21.5

21.6

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0


18

D3110-13

CH4(% LEL)

0.10 0.100.10


1.00 0.10

CO(ppm)

1.00

28/08/2013

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks







Detection Limits

BH1Dry 0.0

3.4 0.00.0BH1 0.00 00:00:00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)


(Pa)

Time of Reading

hh:mm:ssInst

ID


Air temp

(oC)

0.0


(m BGL)

CH4(% vol)

O2(% vol)

0.00 0.0

79.7

79.7

79.7

79.7

16.6 3.6 0.0

16.6 3.6 0.0

0.0

0.0

WetModerate

CloudyHeavy

79.779.7

79.7

78.8

78.8

78.7

78.8

78.7

78.7

78.820.7 0.4 0.00.0

20.7 0.4 0.0

20.7 0.4 0.0

0.0

0.0

20.6 0.6 0.0

20.7 0.5 0.0

0.0

0.0

20.3 0.8 0.0

20.5 0.7 0.0

0.0

0.0

0.016.6 3.6 0.0

3.5 0.0

0.0

0.0

3.5 0.0

997 13

BH1 0.00 00:01:30

0.00 00:00:30

BH1 0.00 00:01:00 0.000.0

0.0

0.0

0.000.0

0.00 0.00.0

BH1 0.00 00:02:00 0.000.0

00:02:30BH1 0.00

BH1 0.00 00:03:00

0.00

0.0

Dry 0.00.00.00 00:00:00

BH2 0.00

BH2 0.00 00:00:30

00:01:30

BH2

997

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.0

0.0

0.0

0.0

0.0

0.000.0

BH2 0.00 00:03:00

BH2

BH2 0.00 00:02:00

00:02:30BH2 0.00 0.0

0.0

0.0

0.0

0.0 16.9

0.0

0.0

0.0

16.7

3.3

16.7

16.8

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0


12

D3110-13

CH4(% LEL)

0.10 0.100.10


1.00 0.10

CO(ppm)

1.00

19/09/2013

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks







Detection Limits

BH4Dry 0.0

0.0 0.00.0BH4 0.00 00:00:00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)


(Pa)

Time of Reading

hh:mm:ssInst

ID


Air temp

(oC)

2.7

0.0


(m BGL)

CH4(% vol)

O2(% vol)

19.8

0.0

0.00 0.0

2.7

78.4

78.4

78.4

19.7 2.6 0.0

19.8 2.7

0.0 19.9

0.0

2.7 0.00.0 77.3BH3 0.00 00:03:00

77.9

77.6

0.0

0.0

77.4

77.4

77.40.0

0.0

0.0

0.0

78.4

21.5 0.0 0.0

21.5 0.0 0.0

0.0

0.0

WetModerate

CloudyHeavy

78.778.6

78.4

78.5

78.5

78.6

78.5

78.5

78.6

78.2

19.8

78.6

19.5 2.2 0.0

19.6 2.4 0.0

0.0

0.0

21.1 0.2 0.00.0

21.1 0.3 0.0

21.1 0.3 0.0

0.0

0.0

21.0 0.3 0.0

21.0 0.3 0.0

0.0

0.0

20.9 0.5 0.0

20.9 0.5 0.0

0.0

0.0

0.021.5 0.0 0.0

0.0 0.0

0.0

0.0

0.0 0.0

998 16

BH4 0.00 00:01:30

0.00 00:00:30

BH4 0.00 00:01:00 0.000.0

0.0

0.0

0.000.0

0.00 0.00.0

BH4 0.00 00:02:00 0.000.0

00:02:30BH4 0.00

BH4 0.00 00:03:00

0.00

0.0

Dry 0.00.00.00 00:00:00

BH5 0.00

BH5 0.00 00:00:30

00:01:30

BH5

998

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.0

0.0

0.0

0.0

0.0

0.000.0

BH5 0.00 00:03:00

0.00

0.00 00:01:30

BH3

0.0

0.0

0.00 0.0

0.000.0

0.0

0.00

BH5

BH3

BH3 0.00 00:02:00 0.0

00:00:00

BH5 0.00 00:02:00

00:02:30BH5 0.00

BH3

BH3 0.00 00:01:00

BH3 0.00 00:00:30

0.00

00:02:30

0.000.98

0.0

0.0

0.000.0

0.0

0.0

0.0

0.0

0.0

0.0 21.2

0.0

0.0

0.0

21.5

0.0

21.5

21.3

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0


998

15

15

D3110-13

CH4(% LEL)

0.10 0.100.10


1.00 0.10

CO(ppm)

1.00

19/09/2013

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks







Detection Limits

BH4Dry 0.0

0.0 0.00.0BH4 0.00 00:00:00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)


(Pa)

Time of Reading

hh:mm:ssInst

ID


Air temp

(oC)

3.2

0.0


(m BGL)

CH4(% vol)

O2(% vol)

19.2

0.0

0.00 0.0

3.3

78.4

78.3

78.2

19.0 3.5 0.0

19.4 3.2

0.0 19.5

0.0

3.1 0.00.0 77.4BH3 0.00 00:02:30

77.4

77.4

0.0

0.0

77.4

77.4

77.40.0

0.0

0.0

0.0

78.2

21.6 0.0 0.0

21.7 0.0 0.0

0.0

0.0

DampLight

CloudyNone

80.178.6

78.2

78.3

77.6

77.6

77.6

77.5

77.5

77.5

19.3

77.6

19.7 2.7 0.0

19.1 3.5 0.0

0.0

0.0

21.2 1.0 0.00.0

21.2 1.1 0.0

21.2 1.1 0.0

0.0

0.0

21.2 1.2 0.0

21.2 1.1 0.0

0.0

0.0

21.2 0.4 0.0

21.2 1.2 0.0

0.0

0.0

0.021.7 0.0 0.0

0.0 0.0

0.0

0.0

0.0 0.0

996

BH4 0.00 00:01:30

0.00 00:00:30

BH4 0.00 00:01:00 0.000.0

0.0

0.0

0.000.0

0.00 0.00.0

BH4 0.00 00:02:00 0.000.0

00:02:00BH4 0.00

BH4 0.00 00:02:30

0.00

0.0

Dry 0.00.00.00 00:00:00

BH5 0.00

BH5 0.00 00:00:30

00:01:30

BH5

996

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.0

0.0

0.0

0.0

0.0

0.000.0

BH5 0.00 00:02:30

0.00

0.00 00:01:30

BH3

0.0

0.0

0.00 0.0

0.000.0

0.0

0.00

BH5

BH3

BH3 0.00 00:02:00 0.0

00:00:00

BH5 0.00 00:02:00

00:02:00BH5 0.00

BH3

BH3 0.00 00:01:00

BH3 0.00 00:00:30

0.00

00:02:00

0.000.86

0.0

0.0

0.000.0

0.0

0.0

0.0

0.0

0.0

0.0 19.8

0.0

0.0

0.0

21.6

0.0

21.5

21.2

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.1

0.0

0.0

0.0

0.0

0.0

0.2


996

D3110-13

CH4(% LEL)

0.10 0.100.10


1.00 0.10

CO(ppm)

1.00

04/10/2013

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks







Detection Limits

BH2Dry 0.0

0.3 0.00.0BH2 0.00 00:00:00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)


(Pa)

Time of Reading

hh:mm:ssInst

ID


Air temp

(oC)

0.0


(m BGL)

CH4(% vol)

O2(% vol)

0.00 0.0

78.5

78.5

78.6

78.6

21.3 0.0 0.0

21.3 0.0 0.0

0.0

0.0

DryLight

CloudyNone

78.878.4

78.6

78.8

78.4

78.4

78.4

78.4

78.4

78.521.4 0.0 0.00.0

21.5 0.0 0.0

21.5 0.0 0.0

0.0

0.0

21.5 0.1 0.0

21.5 0.1 0.0

0.0

0.0

21.1 1.5 0.0

21.5 0.3 0.0

0.0

0.0

0.021.3 0.0 0.0

0.1 0.0

0.0

0.0

0.1 0.0

996

BH2 0.00 00:01:30

0.00 00:00:30

BH2 0.00 00:01:00 0.000.0

0.0

0.0

0.000.0

0.00 0.00.0

BH2 0.00 00:02:00 0.000.0

00:02:30BH2 0.00

BH2 0.00 00:03:00

0.00

0.0

Dry 0.00.00.00 00:00:00

BH1 0.00

BH1 0.00 00:00:30

00:01:30

BH1

996

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.0

0.0

0.0

0.0

0.0

0.000.0

BH1 0.00 00:03:00

BH1

BH1 0.00 00:02:00

00:02:30BH1 0.00 0.0

0.0

0.0

0.0

0.0 20.2

0.0

0.0

0.0

21.3

1.5

21.3

21.3

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0


D3110-13

CH4(% LEL)

0.10 0.100.10


1.00 0.10

CO(ppm)

1.00

04/10/2013

MQ

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks







Detection Limits

BH1Dry 0.0

0.0 0.00.0BH1 0.00 00:00:00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)


(Pa)

Time of Reading

hh:mm:ssInst

ID


Air temp

(oC)

3.8

0.0


(m BGL)

CH4(% vol)

O2(% vol)

18.0

0.0

0.00 0.0

3.8

78.5

78.5

78.4

18.0 3.8 0.0

17.9 3.8

0.0 17.9

0.0

3.9 0.00.0 78.2BH3 0.00 00:03:00 0.000.0

78.1

78.1

0.0

0.0

78.1

78.2

78.20.0

0.0

0.0

0.0

78.5

21.4 0.1 0.0

21.2 0.2 0.0

0.0

0.0

WetLight

CloudyNone

78.478.4

78.5

78.5

78.7

78.6

78.7

78.5

78.5

78.1

17.9

78.7

18.0 3.8 0.0

18.0 3.8 0.0

0.0

0.0

20.7 0.4 0.00.0

20.8 0.4 0.0

20.7 0.4 0.0

0.0

0.0

21.1 0.3 0.0

20.9 0.4 0.0

0.0

0.0

21.2 0.2 0.0

21.2 0.2 0.0

0.0

0.0

0.021.1 0.4 0.0

0.0 0.0

0.0

0.0

0.0 0.0

999 14

BH1 0.00 00:01:30

0.00 00:00:30

BH1 0.00 00:01:00 -0.200.0

0.0

0.0

0.000.0

-0.30 0.00.0

BH1 0.00 00:02:00 -0.701.0

00:02:30 -0.801.0BH1 0.00

BH1 0.00 00:03:00 -1.102.0

0.80

0.0

Dry 0.01.00.00 00:00:00

BH2 0.00

BH2 0.00 00:00:30

00:01:30

BH2

1000

0.20

0.00

0.00 00:01:00 1.503.0

0.0

0.0

0.0

0.0

0.0

0.0

0.300.0

1.0

BH2 0.00 00:03:00 0.0

0.00 0.0

0.00 00:01:30

BH3

0.0

0.0

0.00 0.0

0.000.0

0.0

0.00

BH2

BH3

BH3 0.00 00:02:00 0.0

00:00:00

BH2 0.00 00:02:00

00:02:30BH2 0.00

BH3

BH3 0.00 00:01:00

BH3 0.00 00:00:30

0.00

00:02:30 0.00

0.001.05

0.0

0.0

0.000.0

0.0

0.0

0.0

0.40

0.80

0.0

0.0

0.0 21.5

0.0

0.0

0.0

21.4

0.0

21.4

21.5

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0


1001

14

14

D3110-13

CH4(% LEL)

0.10 0.100.10


1.00 0.10

CO(ppm)

1.00

11/10/2013

SB

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks







Detection Limits

BH43.45 3.0

2.1 0.00.0BH4 0.00 00:00:00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)


(Pa)

Time of Reading

hh:mm:ssInst

ID


Air temp

(oC)

0.0


(m BGL)

CH4(% vol)

O2(% vol)

1.70 0.0

78.6

78.7

78.7

78.6

18.6 2.7 0.0

18.6 2.7 0.0

0.0

0.0

WetLight

CloudyNone

78.578.5

78.7

78.7

78.9

78.7

78.9

78.7

78.7

79.018.2 2.8 0.00.0

19.1 2.0 0.0

18.4 2.6 0.0

0.0

0.0

20.3 1.0 0.0

19.9 1.4 0.0

0.0

0.0

20.5 0.7 0.0

20.4 0.8 0.0

0.0

0.0

0.018.5 2.7 0.0

2.7 0.0

0.0

0.0

2.7 0.0

1001 14

BH4 0.00 00:01:30

0.00 00:00:30

BH4 0.00 00:01:00 1.102.0

0.0

0.0

1.603.0

0.90 0.01.0

BH4 0.00 00:02:00 0.300.0

00:02:30 1.102.0BH4 0.00

BH4 0.00 00:03:00 -0.300.0

0.00

0.0

Dry 0.00.00.00 00:00:00

BH5 0.00

BH5 0.00 00:00:30

00:01:30

BH5

1001

0.00

-0.20

0.00 00:01:00 0.000.0

0.0

0.0

0.0

0.0

0.0

0.0

0.901.0

0.0

BH5 0.00 00:03:00 0.0

BH5

BH5 0.00 00:02:00

00:02:30BH5 0.00 0.0

0.00.10

0.00

0.0

0.0

0.0 18.8

0.0

0.0

0.0

18.5

2.6

18.6

19.3

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0


14

D3110-13

CH4(% LEL)

0.10 0.100.10


1.00 0.10

CO(ppm)

1.00

11/10/2013

SB

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks







Detection Limits

17/10/2013

SB

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3110-13

CH4(% LEL)

0.10 0.100.10


1.00 0.10

CO(ppm)

1.00

9

9


987

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.4

20.7

20.7

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0 20.7

0.0

0.0

0.0

20.7

0.0

0.0

0.0

0.00

0.00

3.45

0.0

-3.0

-1.60-3.0

0.00

00:02:30 -1.60

-1.60

BH4 0.00 00:01:00

BH4 0.00 00:00:30

00:00:00

BH3 0.00 00:02:00

00:02:30BH3 0.00

BH4

BH3

BH4

BH4 0.00 00:02:00 -3.0

BH4

0.0

0.0

-1.60 0.0

-1.60-3.0

-3.0

-1.60

0.00 -3.0

0.00 00:01:30

0.0

BH3 0.00 00:03:00 0.0

0.0

0.0

0.0

0.0

0.0

0.000.0

0.00

0.00

0.00 00:01:00 0.000.0

0.0

0.00 00:00:00

BH3 0.00

BH3 0.00 00:00:30

00:01:30

BH3

989

0.0

0.87 0.00.0

00:03:00 0.000.0

-0.20

BH2 0.00

BH2 0.00

00:02:30 0.000.0

BH2 0.00 00:02:00 0.000.0

0.00 0.00.0

0.000.0

0.0

0.0

0.000.0

00:01:30

0.00 00:00:30

BH2 0.00 00:01:00

988 9

BH2 0.00 0.4 0.0

0.0

0.0

0.4 0.0

0.020.6 0.4 0.0

18.9 3.3 0.0

19.4 2.8 0.0

0.0

0.0

19.7 2.4 0.0

19.9 2.0 0.0

0.0

0.0

20.1 1.8 0.0

20.2 1.7 0.0

0.0

0.0

20.3 1.5 0.00.0

21.3 0.0 0.0

21.3 0.0 0.0

0.0

0.0

78.6

21.3

78.1

78.9

77.7

78.0

77.9

78.0

77.7

77.9

WetCalm

NoneNone

78.878.8

78.8

20.7 0.4 0.0

20.7 0.4 0.0

0.0

0.0

0.0

0.0

0.0

0.0

78.6

78.6

0.0

0.0

78.6

78.6

78.7

0.00 00:03:00 -1.60-3.0BH4 0.0 0.00.0 78.7

21.2 0.0

0.0 21.2

0.0

78.8

78.8

78.8

21.3 0.0 0.0

0.0

0.0


(m BGL)

CH4(% vol)

O2(% vol)

21.3

0.0

-0.10 0.0

0.0

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)


(Pa)

Time of Reading

hh:mm:ssInst

ID


Air temp

(oC)

BH2Dry 0.0

0.4 0.00.0BH2 0.00 00:00:00







Detection Limits

BH5Dry -3.0

0.5 0.00.0BH5 0.00 00:00:00

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)


(Pa)

Time of Reading

hh:mm:ssInst

ID


Air temp

(oC)

0.0


(m BGL)

CH4(% vol)

O2(% vol)

-1.60 0.0

78.5

78.5

78.5

78.5

20.9 0.5 0.0

20.9 0.5 0.0

0.0

0.0

Calm

SlightNone

78.478.5

78.5

78.6

78.7

78.6

78.6

78.6

78.6

78.716.6 4.6 0.00.0

16.7 4.6 0.0

16.6 4.6 0.0

0.0

0.0

16.9 4.4 0.0

16.8 4.5 0.0

0.0

0.0

17.0 4.3 0.0

16.9 4.3 0.0

0.0

0.0

0.020.9 0.5 0.0

0.5 0.0

0.0

0.0

0.5 0.0

988 9

BH5 0.00 00:01:30

0.00 00:00:30

BH5 0.00 00:01:00 -1.60-3.0

0.0

0.0

-1.60-3.0

-1.60 0.0-3.0

BH5 0.00 00:02:00 -1.60-3.0

00:02:30 -1.60-3.0BH5 0.00

BH5 0.00 00:03:00 -1.60-3.0

-0.20

0.0

Dry 0.00.00.00 00:00:00

BH1 0.00

BH1 0.00 00:00:30

00:01:30

BH1

987

-0.20

-0.20

0.00 00:01:00 -0.200.0

0.0

0.0

0.0

0.0

0.0

0.0

-0.200.0

0.0

BH1 0.00 00:03:00 0.0

BH1

BH1 0.00 00:02:00

00:02:30BH1 0.00 0.0

0.0-0.20

-0.20

0.0

0.0

0.0 21.0

0.0

0.0

0.0

20.9

0.5

20.9

20.9

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0


10

D3110-13

CH4(% LEL)

0.10 0.100.10


1.00 0.10

CO(ppm)

1.00

17/10/2013

SB

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks







Detection Limits

31/10/2013

GM

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3110-13

CH4(% LEL)

0.10 0.100.10


1.00

CO(ppm)

1.00

Equipment Used LMSxI 1904 + Dip

990

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

1.0

20.1

20.1

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0 20.3

0.0

0.0

0.0

20.0

0.0

0.0

0.0

0.00.0

0.00

0.00

0.00

0.0

0.00

BH5 0.00 00:03:00

BH5 0.00 00:02:30

00:02:00

BH5 0.00 00:00:00

00:00:30

00:01:30

BH5 0.00

BH5

BH4

BH5

0.0

0.00.00 00:03:30

0.0

BH5 0.00

BH5 0.00 00:01:00 0.0

0.0

0.0

Dry 0.00.0 0.00

0.00 00:05:00

0.00 00:04:00

BH4 0.00 00:04:30

BH4

0.0

0.0

0.00.0

0.0

0.20

00:03:00 0.501.0

0.40

00:03:30BH4 0.00

BH4 0.00

BH4 0.00

00:02:30 0.400.0

BH4 0.00 00:02:00 0.901.0

0.60 0.01.0

0.300.0

0.0

0.0

1.102.0

00:01:30

0.00 00:00:30

BH4 0.00 00:01:00

990

BH4 0.00 1.7 0.0

0.0

0.0

1.7 0.0

19.4 2.2 0.0

0.0

0.0

19.6 2.0 0.0

19.2 2.4 0.0

19.1 2.5 0.0

0.0

0.0

19.0 2.6 0.00.0

18.1 3.1 0.0

17.2 3.9 0.0

0.0

0.0

16.9 4.2 0.0

16.6 4.4 0.0

0.0

0.0

16.5 4.5 0.0

16.4 4.6 0.0

0.0

0.0

WetLight

CloudyNone

19.9 1.8 0.0

19.8 1.8 0.0

0.0

0.0

0.0

0.0

0.0

16.4 4.6 0.0

0.0


(m BGL)

CH4(% vol)

O2(% vol)

16.4

0.60 0.0

4.6

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)


(Pa)

Time of Reading

hh:mm:ssInst

ID


Air temp

(oC)

BH43.20 1.0

1.6 0.00.0BH4 0.00 00:00:00







Detection Limits

31/10/2013

GM

0.10

CO2(% vol)

H2S(ppm)

Nitrogen(%vol)

Remarks

D3110-13

CH4(% LEL)

0.10 0.100.10


1.00

CO(ppm)

1.00


988

989

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

0.0

3.3

20.2

20.1

Reading Depth

(mBGL)

0.00.0

0.0

0.0

0.0

0.0 19.2

0.0

0.0

0.0

20.3

0.0

0.0

0.0Dry

0.0

2.0

1.202.0

0.00

00:02:30 0.90

1.00

BH1 0.00 00:01:00

BH1 0.00 00:00:30

00:00:00

BH2 0.00 00:01:30

00:02:00BH2 0.00

BH1

BH1

BH1 0.00 00:02:00 2.0

BH1

0.0

0.0

1.20 0.0

1.102.0

2.0

1.40

0.00 1.0

0.00 00:01:30

BH2 0.00 00:02:30

0.0

0.0

0.0

0.0

0.0

0.000.0

0.00

Dry

0.00

0.00 00:00:30 0.000.0

0.0BH2 0.00

BH2 0.00 00:00:00

00:01:00

BH2

0.000:03:00

BH3 0.00

BH3 0.00

00:02:30

BH3 0.00 00:02:00

0.00 0.00.0

0.000.0

0.0

0.0

0.000.0

00:01:30

0.00 00:00:30

BH3 0.00 00:01:00

989

BH3 0.00 2.9 0.0

0.0

0.0

3.1 0.0

0.020.6 2.3 0.0

21.1 0.9 0.00.0

20.7 0.6 0.0

20.6 0.6 0.0

0.0

0.0

20.6 0.6 0.0

20.6 0.6 0.0

0.0

0.0

20.6 0.6 0.00.0

19.0 3.1 0.0

17.2 4.7 0.0

0.0

0.0

17.1

WetLight

CloudyNone

instrument

Water rising into

20.4 2.7 0.0

20.5 2.5 0.0

0.0

0.0

0.0

0.0

0.0

0.0

1.0

0.0

0.0

0.00 00:03:00 0.901.0BH1 4.7 0.00.0

17.1 4.7

0.80

0.0 17.1

0.0

17.2 4.7 0.0

4.7

0.0


(m BGL)

CH4(% vol)

O2(% vol)

17.2

0.0

-0.30 0.0

4.7

Borehole IDDepth of

Installation(m BGL)

FlowRate(l/hr)


(Pa)

Time of Reading

hh:mm:ssInst

ID


Air temp

(oC)

BH30.78 0.0

3.2 0.00.0BH3 0.00 00:00:00



November 2013 Report No D3110-13 Issue 2.0 Enclosure C

ENCLOSURE C

GEOTECHNICAL LABORATORY TEST RESULTS

Index Properties – Summary of Results INDX 1 and 2

Particle Size Distribution Analyses PSD 1 to 18

Soil Sample Analysis ESG Scientifics Report No EFS/135115

Chemical Tests – Summary of Results CHEM 1 Dry Density/Moisture Content Relationship (Light Compaction) COMPL 1 and 2

Moisture Condition Value/Moisture Content Relationship MCVREL 1 and 2

California Bearing Ratio CBR 1 and 2

Project No Project Name

p p d w < 425 WL WP IP p sµm

sieve

from to % % % % Mg/m3

10 2.00 DBrown slightly gravelly SAND.

3.8 40 s 19 b NP

15 3.90 DBrown slightly gravelly SAND with rare clay pockets.

6.5 52 s 17 b NP

18 4.70 4.97 DBrown slightly gravelly SAND.

7.5

16 4.90 DBrown slightly sandy slightly gravelly CLAY.

12 90 s 33 a 14 19

17 5.00 5.35 DBrown slightly sandy slightly gravelly CLAY.

8.2 81 s 29 a 13 16


17 89 s 34 a 14 20


14 89 s 34 a 15 19


18 84 s 28 a 12 16


13 89 s 28 a 12 16


11 75 s 26 a 12 14

18 5.80 DBrown slightly sandy slightly clayey GRAVEL.

5.0

14 3.00 3.45 DBrown clayey gravelly SAND.

12 72 s 28 b NP

17 3.60 3.73 DBrown gravelly SAND.

11

5 0.90 DBrown slightly sandy slightly gravelly silty CLAY.

14 77 s 26 a 15 11

7 1.20 1.65 DBrown slightly gravelly clayey SAND.

10 58 s 22 b NP


12 86 s 31 a 13 18

14 4.00 4.45 DBrown slightly sandy slightly gravelly CLAY.

11 86 s 30 a 12 18

19 6.00 DBrown slightly sandy GRAVEL.

4.9

8 2.50 DBrown slightly gravelly SAND with rare clay pockets.

8.5 33 s 23 b NP

7 1.70 DBrown gravelly SAND.

6.5 28 s 20 b NP

8 2.50 DBrown gravelly silty SAND.

4.6 18 s 19 b NP

2 0.30 DBrown slightly gravelly clayey SAND.

15 56 s 31 a 21 10

9 1.80 DBrown slightly gravelly slightly clayey SAND.

16 72 s 22 b NP


16


11 62 s 30 a 12 18


9.9

1 0.10 DBrown slightly sandy slightly gravelly CLAY with frequent rootlets and plant remains.

16 65 s 28 a 17 11

7 2.50 DOrangish brown gravelly SAND.

4.0

12 3.40 DBrown sandy slightly clayey GRAVEL.

9.0


13

3 0.40 DBrown gravelly slightly clayey SAND.

12 43 s 26 b NP


3.3

General notes: All above tests carried out to BS1377 : 1990 unless annotated otherwise. See individual test reports for further details.

Key : p bulk density, linear WL Liquid limit WP Plastic limit <425um preparation p s particle density

p d dry density a 4 point cone test NP non - plastic n from natural soil -g = gas jar

w moisture content b 1 point cone test IP s sieved specimen -p = small pyknometer

QA Ref

INDX 1

Plasticity Index

Printed:21/10/2013 16:09SLR 1Rev 91Mar 12

WS4

WS5

WS5

WS3

WS4

WS4

WS4

WS3

WS3

WS3

WS3

BH5

WS1

WS2

WS2

BH5

BH5

BH5

BH5

BH3

BH3

BH4

BH4

BH3

BH3

BH3

BH3

BH1

BH1

BH2

BH2


INDEX PROPERTIES - SUMMARY OF RESULTS

Soil Description

D3110-13

BH1

Hole No.

Mg/m3

Remarks

Sample

Depth (m)No. type

Table


p p d w < 425 WL WP IP p sµm

sieve

from to % % % % Mg/m3


INDEX PROPERTIES - SUMMARY OF RESULTS

Soil Description

D3110-13

Hole No.

Mg/m3

Remarks

Sample

Depth (m)No. type

10 3.50 DBrown sandy GRAVEL with frequent clay pockets.

5.6 36 s 27 a 13 14

General notes: All above tests carried out to BS1377 : 1990 unless annotated otherwise. See individual test reports for further details.

Key : p bulk density, linear WL Liquid limit WP Plastic limit <425um preparation p s particle density

p d dry density a 4 point cone test NP non - plastic n from natural soil -g = gas jar

w moisture content b 1 point cone test IP s sieved specimen -p = small pyknometer

QA Ref

WS5

SLR 1Rev 91Mar 12

Printed:21/10/2013 16:09INDX 2

Plasticity Index

Table

silt+clay =11

03752

11

Whole *<60mm1

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

6765

480.6001.18 60

8728

7370

81201410

7.90.063 110.150

340.425

2317

0.300

5.0

62

68

3.352.00

6.3

55

Clay

Sample Proportions

*<60mm values to aid description only

SandSilt

Cobbles / bouldersGravel

Remarks

3751

Soil description%Passing

Brown very gravelly clayey SAND.

100969237.5

Sieving Sedimentation

none

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve

Uniformity Coefficient D60 / D10

SievingSedimentation

Test Method

12590

100100

Dry mass of sample, kg

Sieve: natural material Preparation / Pretreatment

PSD 1

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13


Sample Details: Hole No

Depth (m BGL)

Samp No Type

ID

BH1

11 B

ESGD3110-13201308150000000011

QA Ref

SLR 2,9Rev 88Aug 11

2.00

SILTFine Medium Coarse

SANDFine Medium Coarse

GRAVELFine Medium CoarseCLAY COBBLES

Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

silt+clay =7

0786

7

Whole *<60mm0

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

9494

750.6001.18 92

9728

9696

96201410

8.10.063 70.150

480.425

2412

0.300

5.0

93

95

3.352.00

6.3

88

Clay

Sample Proportions


SandSilt


Remarks

786


Orangish brown gravelly SAND with rare clay pockets.

10010010037.5


none

BS 1377 : Part 2 : 1990

3

9.2 wet sieve



Test Method

12590

100100



PSD 2

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH1

14 B

ESGD3110-13201308150000000014

QA Ref

SLR 2,9Rev 88Aug 11

3.00




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

silt+clay =7

0687

7

Whole *<60mm0

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

9595

730.6001.18 93

10028

9897

99201410

7.90.063 80.150

420.425

2414

0.300

5.0

94

96

3.352.00

6.3

88

Clay

Sample Proportions


SandSilt


Remarks

687


Brown gravelly SAND with rare clay pockets.

10010010037.5


none

BS 1377 : Part 2 : 1990

4

9.2 wet sieve



Test Method

12590

100100



PSD 3

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH1

17 B

ESGD3110-13201308150000000017

QA Ref

SLR 2,9Rev 88Aug 11

4.00




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

silt+clay =3

04849

3

Whole *<60mm4

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

5754

330.6001.18 47

9128

7566

85201410

9.70.063 30.150

200.425

116

0.300

5.0

50

60

3.352.00

6.3

40

Clay

Sample Proportions


SandSilt


Remarks

4647


Brown SAND AND SAND with rare clay pockets and one cobble.

96969537.5


none

BS 1377 : Part 2 : 1990

32

9.2 wet sieve



Test Method

12590

100100



PSD 4

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH2

5 B

ESGD3110-13201308150000000021

QA Ref

SLR 2,9Rev 88Aug 11

0.20




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

silt+clay =7

0984

7

Whole *<60mm0

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

9492

740.6001.18 88

10028

9996

100201410

5.00.063 70.150

520.425

2714

0.300

5.0

91

94

3.352.00

6.3

83

Clay

Sample Proportions


SandSilt


Remarks

984


Brown gravelly silty SAND

10010010037.5


none

BS 1377 : Part 2 : 1990

4

9.2 wet sieve



Test Method

12590

100100



PSD 5

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH2

8 B

ESGD3110-13201308150000000024

QA Ref

SLR 2,9Rev 88Aug 11

0.90




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

silt+clay =9

05041

9

Whole *<60mm2

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

5653

320.6001.18 46

8528

6965

81201410

11.00.063 90.150

220.425

1614

0.300

5.0

49

59

3.352.00

6.3

39

Clay

Sample Proportions


SandSilt


Remarks

4940


Brown very sandy clayey GRAVEL.

100928837.5


none

BS 1377 : Part 2 : 1990

92

9.2 wet sieve



Test Method

12590

100100



PSD 6

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH2

13 B

ESGD3110-13201308150000000031

QA Ref

SLR 2,9Rev 88Aug 11

3.00




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

silt+clay =6

05242

6

Whole *<60mm4

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

5349

360.6001.18 43

8028

6963

74201410

14.30.063 60.150

280.425

1912

0.300

5.0

46

56

3.352.00

6.3

39

Clay

Sample Proportions


SandSilt


Remarks

5040


Brown very sandy GRAVEL with occasional clay pockets and one cobble.

97928737.5


none

BS 1377 : Part 2 : 1990

73

9.2 wet sieve



Test Method

12590

100100



PSD 7

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH3

17 B

ESGD3110-13201308150000000055

QA Ref

SLR 2,9Rev 88Aug 11

5.00




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

silt+clay =2

04454

2

Whole *<60mm0

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

6158

490.6001.18 54

9128

7670

83201410

5.80.063 20.150

350.425

178

0.300

5.0

56

63

3.352.00

6.3

52

Clay

Sample Proportions


SandSilt


Remarks

4454


Brown very gravelly SAND.

1001009437.5


none

BS 1377 : Part 2 : 1990

27

9.2 wet sieve



Test Method

12590

100100



PSD 8

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH4

6 B

ESGD3110-13201308150000000064

QA Ref

SLR 2,9Rev 88Aug 11

0.80




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

89

0137089

0.0049Whole *<60mm

00.0035

0.212

Particle Size mm

Particle Size mm

0.0374

%Passing

100756350

8888

0.0015

850.6001.18 87

10028

9591

100201410

6.1

2.65

0.063 180.150

810.425

7051

0.300

Particle density, Mg/m3

5.0

87

88

3.352.00

6.3

86

Clay

Sample Proportions


Sand

10

Silt

9 Cobbles / boulders

1211

Gravel

Remarks

1370


Brown gravelly clayey SAND

14100100100

0.02660.01890.009837.5


9.5 hydrometer

BS 1377 : Part 2 : 1990

50

9.2 wet sieve



Test Method

12590

100100

assumed


Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment

0.06300.0526

1815

1312

PSD 9

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH4

15 B

ESGD3110-13201308150000000073

QA Ref

SLR 2,9Rev 88Aug 11

3.00




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

2713

021392713

0.0046Whole *<60mm

00.0035

0.212

Particle Size mm

Particle Size mm

0.0363

%Passing

100756350

8381

0.0015

740.6001.18 77

9528

8886

94201410

7.4

2.65

0.063 420.150

670.425

6054

0.300


5.0

79

84

3.352.00

6.3

77

Clay

Sample Proportions


Sand

18

Silt


2620

Gravel

Remarks

2139


Brown slightly gravelly sandy silty CLAY.

3510010097

0.02590.01850.009737.5


9.5 hydrometer

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve



Test Method

12590

100100

assumed



0.06300.0510

4238

3330

PSD 10

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH5

3 B

ESGD3110-13201308150000000080

QA Ref

SLR 2,9Rev 88Aug 11

0.20




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

2822

07432822

0.0044Whole *<60mm

00.0032

0.212

Particle Size mm

Particle Size mm

0.0295

%Passing

100756350

9494

0.0015

860.6001.18 91

9928

9796

98201410

4.4

2.65

0.063 500.150

780.425

7062

0.300


5.0

93

95

3.352.00

6.3

89

Clay

Sample Proportions


Sand

25

Silt


3528

Gravel

Remarks

743


Brown slightly gravelly sandy CLAY.

48100100100

0.02150.01550.008437.5


9.5 hydrometer

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve



Test Method

12590

100100

assumed



0.06300.0413

5049

4442

PSD 11

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH5

15 B

ESGD3110-13201308150000000092

QA Ref

SLR 2,9Rev 88Aug 11

4.00




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

119

01070119

0.0049Whole *<60mm

00.0035

0.212

Particle Size mm

Particle Size mm

0.0367

%Passing

100756350

9292

0.0016

740.6001.18 88

10028

9695

99201410

7.2

2.65

0.063 200.150

610.425

5036

0.300


5.0

90

93

3.352.00

6.3

82

Clay

Sample Proportions


Sand

10

Silt


1412

Gravel

Remarks

1070


Brown gravelly SAND with frequent clay pockets.

18100100100

0.02600.01850.009737.5


9.5 hydrometer

BS 1377 : Part 2 : 1990

96

9.2 wet sieve



Test Method

12590

100100

assumed



0.06300.0516

2019

1816

PSD 12

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH5

18 B

ESGD3110-13201308150000000095

QA Ref

SLR 2,9Rev 88Aug 11

5.00




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

silt+clay =14

03056

14

Whole *<60mm0

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

7673

580.6001.18 68

9828

8681

95201410

6.50.063 150.150

440.425

2920

0.300

5.0

70

77

3.352.00

6.3

64

Clay

Sample Proportions


SandSilt


Remarks

3056


Brow slightly gravelly sandy CLAY.

1001009837.5


none

BS 1377 : Part 2 : 1990

Not applicable

9.2 wet sieve



Test Method

12590

100100



PSD 13

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

WS1

3 B

ESGD3110-13201308150000000099

QA Ref

SLR 2,9Rev 88Aug 11

0.20




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

silt+clay =2

01286

2

Whole *<60mm0

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

8989

780.6001.18 88

9628

9291

95201410

3.50.063 30.150

510.425

249

0.300

5.0

88

90

3.352.00

6.3

85

Clay

Sample Proportions


SandSilt


Remarks

1286


Orangish brown gravelly SAND.

1001009837.5


none

BS 1377 : Part 2 : 1990

2

9.2 wet sieve



Test Method

12590

100100



PSD 14

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

WS1

10 B

ESGD3110-13201308150000000107

QA Ref

SLR 2,9Rev 88Aug 11

3.00




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

silt+clay =4

03858

4

Whole *<60mm0

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

7066

400.6001.18 59

9728

8479

93201410

5.50.063 40.150

220.425

106

0.300

5.0

62

72

3.352.00

6.3

52

Clay

Sample Proportions


SandSilt


Remarks

3858



1001009837.5


none

BS 1377 : Part 2 : 1990

7

9.2 wet sieve



Test Method

12590

100100



PSD 15

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

WS2

9 B

ESGD3110-13201308150000000115

QA Ref

SLR 2,9Rev 88Aug 11

2.00




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

124

04438134

0.0046Whole *<60mm

90.0035

0.212

Particle Size mm

Particle Size mm

0.0352

%Passing

95756350

5855

0.0016

420.6001.18 49

8128

7166

75201410

9.1

2.65

0.063 170.150

350.425

2722

0.300


5.0

51

60

3.352.00

6.3

46

Clay

Sample Proportions


Sand

6

Silt


108

Gravel

Remarks

4035


Dark brown clayey very sandy GRAVEL with two cobbles.

15919183

0.02540.01810.009537.5


9.5 hydrometer

BS 1377 : Part 2 : 1990

562

9.2 wet sieve



Test Method

12590

100100

assumed



0.06300.0492

1716

1311

PSD 16

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

WS3

4 B

ESGD3110-13201308150000000120

QA Ref

SLR 2,9Rev 88Aug 11

0.20




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

silt+clay =6

04549

6

Whole *<60mm0

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

6058

400.6001.18 53

9628

7668

92201410

4.40.063 60.150

240.425

1510

0.300

5.0

55

62

3.352.00

6.3

48

Clay

Sample Proportions


SandSilt


Remarks

4549


Brown very gravelly SAND with rare clay pockets.

10010010037.5


none

BS 1377 : Part 2 : 1990

33

9.2 wet sieve



Test Method

12590

100100



PSD 17

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

WS4

8 B

ESGD3110-13201308150000000139

QA Ref

SLR 2,9Rev 88Aug 11

2.00




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

silt+clay =9

02269

9

Whole *<60mm0

0.212

Particle Size mm

Particle Size mm

%Passing

100756350

8381

540.6001.18 75

10028

9490

98201410

2.20.063 80.150

270.425

1712

0.300

5.0

78

84

3.352.00

6.3

68

Clay

Sample Proportions


SandSilt


Remarks

2269



10010010037.5


none

BS 1377 : Part 2 : 1990

5

9.2 wet sieve



Test Method

12590

100100


Sieve: pre dried, Preparation / Pretreatment

PSD 18

0

10

20

30

40

50

60

70

80

90

100

0.001 0.01 0.1 1 10 100 1000Particle size mm

Per

cen

t P

assi

ng


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

WS4

10 B

ESGD3110-13201308150000000141

QA Ref

SLR 2,9Rev 88Aug 11

3.00




Spec Ref

Figure

BOULDERS

� Printed:21/10/2013 16:17

ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA

Site: Gnossall St Lawrence Primary School

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 11-Sep-2013Declan Burns Operations Director

Laboratory and Analytical Business

11-Sep-2013

The 7 samples described in this report were registered for analysis by ESG on 30-Aug-2013. This report supersedes any versions previously issued by the laboratory.

TEST REPORTSOIL SAMPLE ANALYSIS

Report No. EFS/135115 (Ver. 1)

Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)

Tests marked '^' have been subcontracted to another laboratory.

ESG accepts no responsibility for any sampling not carried out by our personnel.

Page 1 of 5Where individual results are flagged see report notes for status.

EFS/135115 Ver. 1

Units : mg/kg mg/l % pH UnitsMethod Codes : ICPACIDS ICPWSS TSBRE1 WSLM50

Method Reporting Limits : 20 10 0.005UKAS Accredited : Yes Yes No No

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

SO

4-- (acid sol)

SO

4-- (H2O

sol) mg/l

Total S

ulphur.

pH (B

S1377)

1321688 BH1 B 6 0.80 07-Aug-13 886 275 0.060 7.3

1321689 BH3 B 9 2.00 06-Aug-13 98 28 0.012 7.8

1321690 BH4 B 3 0.20 05-Aug-13 608 41 0.200 6.8

1321691 BH4 B 11 2.00 05-Aug-13 256 27 0.049 7.9

1321692 BH5 B 12 3.00 06-Aug-13 168 <10 0.021 8.2

1321693 WS1 B 7 1.20 05-Aug-13 48 25 0.007 7.8

1321694 WS5 B 1 0.00 05-Aug-13 454 1110 0.159 7.7

Contact

Date Printed

Report Number EFS/135115

Table Number 1

Fax +44 (0) 1283 554422

Soil Sample Analysis

Mr J Litten

11-Sep-2013

Gnossall St Lawrence Primary School

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Southam


EFS/135115 Ver. 1

SOIL Analysis S135115

CustomerSiteReport No S135115

MethodID

BS

1377CL

CustS

erv

Dep.O

pt

ICP

AC

IDS

ICP

BR

E

ICP

WS

S

KO

NE

NS

.

TS

BR

E1

WS

LM50

ID Number Description Sampled

Chloride (A

) BS

1377

Report B

DO

Cl if pH

<5.5

DO

Mg if S

O4(W

)>3000

DO

NO

3 if pH<5.5

SO

4-- (acid sol)

Magnesium

(BR

E)

SO

4-- (H2O

sol) mg/l

Nitrite as N

:

Total S

ulphur.

pH (B

S1377)

��

CL/1321688 BH1 0.80 07/08/13CL/1321689 BH3 2.00 06/08/13CL/1321690 BH4 0.20 05/08/13CL/1321691 BH4 2.00 05/08/13CL/1321692 BH5 3.00 06/08/13CL/1321693 WS1 1.20 05/08/13CL/1321694 WS5 0.00 05/08/13

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Southam Consignment No S36992

Accredited to ISO17025

Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.

In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.

Gnossall St Lawrence Primary School Date Logged 30-Aug-2013

Report Due 11-Sep-2013


EFS/135115 Ver. 1

Matrix MethodID Analysis Basis

Method Description

Soil ICPACIDS Air Dried Determination of Total Sulphate in soil samples by Hydrochloric Acid extraction followed by ICPOES detection

Soil ICPWSS Air Dried Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection

Soil TSBRE1 Air Dried Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection

Soil WSLM50 Air Dried Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Report Number: EFS/135115

Method Descriptions


EFS/135115 Ver. 1


LOI pH CO2 <2

2:1watersol.

groundwater

acidsol.

TSMgNO3

NH4

mg/Lmg/L

watersol.

acidsol.

mm

from to % g/L g/L % % % % % %

4 0.60 DDark brown gravelly slightly clayey SAND. 0.3 c 70


0.5 c 51


0.4 c 75

5 0.70 DBrown slightly gravelly SAND. 0.6 c 74

11 3.00 DBrown gravelly slightly clayey SAND. 0.8 c 60


0.2 c 84

11 3.50 DBrown gravelly slightly silty SAND. 0.2 c 66


0.1 c 60

BS 1377 : definitive method unless stated : * Sulphate tests preparation / test methods : BRE Special Digest SD1, dependent options :

Org1. BS 1377:Part 3:1990:clause 5.3 4. TRL447 - 1 water soluble sulphate TS Total Sulphur to BR279 / EN ISO15178

LOI Mass loss on ignition at 440oC 2. BS 1377:Part 3:1990:clause 5.4 5. TRL447 - 2 acid soluble sulphate Mg Soluble Magnesium to BR279, colorimetric

CO2 Carbonate content ( rapid titration ) 3. BS 1377:Part 3:1990:clause 5.5 6. BR279 - groundwater sulphate NO3 Soluble Nitrate to BR279, colorimetric

Cl Chloride content < 2mm material passing 2mm sieve NH4 qualitative

QA Ref

WS2

WS5

Sample

Depth (m)No. type

Hole No. Soil Description

Sulphate as SO4 SD1 options

Pre

para

tion/

test

*

Org

%

Chloride, Cl

Printed:21/10/2013 16:14

BH1

Remarks

Organic matter content ( s-sulphides, c-chlorides identified )

BH2

BH3

CHEMICAL TESTS - SUMMARY OF RESULTS

CHEM 1SLR 3Rev 95Aug 11

D3110-13 GNOSSALL St LAWRENCE PRIMARY SCHOOL

BH4

BH5

WS1

Table

Soil description Derived Parameters +

Test method BS 1377:part 4:1990: clause 3.4, 2.5 kg rammer in a CBR mould Maximum dry density, Mg/m3

Preparation Original material was natural, separate specimens tested

Material > 37.5mm %

Material < 37.5mm > 20mm % Optimum moisture content, %

Particle density, Mg/m3 assumed

Remarks

1.93

12

Brown gravelly slightly clayey SAND.

2.65

1

9

COMPL 1

DRY DENSITY / MOISTURE CONTENT RELATIONSHIPBS1377 : PART 4 : 1990 : LIGHT COMPACTION, 2.5 kg rammer

Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH1

1.20

8 B

ESGD3110-13201308150000000008

QA Ref

SLD 4, 3.3/4Rev 66Aug 11

1.4

1.5

1.6

1.7

1.8

1.9

2.0

2.1

2.2

0 4 8 12 16 20 24 28 32

MOISTURE CONTENT %

DR

Y D

EN

SIT

Y M

g/m

3

----- zero, 5% and 10% air voids

Spec Ref

Figure

� Printed:21/10/2013 16:16

Soil description Derived Parameters +

Test method BS 1377:part 4:1990: clause 3.4, 2.5 kg rammer in a CBR mould Maximum dry density, Mg/m3

Preparation Original material was natural, single sample tested

Material > 37.5mm %

Material < 37.5mm > 20mm % Optimum moisture content, %

Particle density, Mg/m3 assumed

Remarks

2.00

10


2.65

0

11

COMPL 2

DRY DENSITY / MOISTURE CONTENT RELATIONSHIPBS1377 : PART 4 : 1990 : LIGHT COMPACTION, 2.5 kg rammer

Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH4

2.00

11 B

ESGD3110-13201308150000000069

QA Ref

SLD 4, 3.3/4Rev 66Aug 11

1.4

1.5

1.6

1.7

1.8

1.9

2.0

2.1

2.2

0 2 4 6 8 10 12 14 16

MOISTURE CONTENT %

DR

Y D

EN

SIT

Y M

g/m

3

----- zero, 5% and 10% air voids

Spec Ref

Figure

� Printed:21/10/2013 16:16

The above characteristics are NOT covered by UKAS accreditation to BS1377

sheet 1 of 2

Method of interpretation of MCV

-0.99

Steepest straight line

Sensitivity ( Change in MCV per 1% moisture content )

Correlation ( proximity of test points to regression line )

Characteristics of calibration line (determined using linear regression)

17.5

-0.79

1.26

Intercept

Slope

MCVREL 1

MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5

Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH5

1.20

8 B

ESGD3110-13201308150000000085

QA Ref

SLD 4, 5.5Rev 72Aug 11

MCV CALIBRATION

0

4

8

12

16

20

24

0 2 4 6 8 10 12 14 16 18 20Moisture Condition Value MCV

Moi

stur

e C

onte

nt %

valid points regression

ineffective/invalid extended regression

Spec Ref

Figure

� Printed:21/10/2013 16:16

Test No * ineffective / invalid point 1 * 2 3 4 5

%

sheet 2 of 2

Brown slightly gravelly sandy CLAY.

Remarks

%

Moisture Condition Value

Dry density after test

Moisture Content

Bulk density after test Mg/m³

Mg/m³

% #N/A

15.7

2.04

2.18 2.21

1.92 1.97

2.24

13.5 11.9 10.8

Material retained on 20mm sieve Steepest straight line

Procedure / Preparation

Initial moisture content <20mm Method of determining MCV

BS1377:Part 1 and Part 4, clause 5.5

3.7

Soil description

1.84

15.7

9.3

9.9

2.05

2.262.13

4.9 7.2 8.9

MCVREL 1


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH5

1.20

8 B

ESGD3110-13201308150000000085

QA Ref


Number of Blows

644832241612864321

1816141210864200

5

10

15

20

25

30

Moisture Condition Value , MCV,

Cha

nge

in P

enet

ratio

n -

mm

test 1 2 3 4 5

Spec Ref

Figure

� Printed:21/10/2013 16:16

The above characteristics are NOT covered by UKAS accreditation to BS1377

sheet 1 of 2

Method of interpretation of MCV

#N/A

Steepest straight line

Sensitivity ( Change in MCV per 1% moisture content )

Correlation ( proximity of test points to regression line )

Characteristics of calibration line (determined using linear regression)

#N/A

#N/A

#N/A

Intercept

Slope

MCVREL 2


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

WS2

0.60

5 B

ESGD3110-13201308150000000111

QA Ref


MCV CALIBRATION

0

2

3

5

7

8

10

0 2 4 6 8 10 12 14 16 18 20Moisture Condition Value MCV

Moi

stur

e C

onte

nt %

valid points regression

ineffective/invalid extended regression

Spec Ref

Figure

� Printed:21/10/2013 16:16

Test No * ineffective / invalid point 1 2 3 4 5

%

sheet 2 of 2

Brown gravelly SAND with occasional clay pockets.

Test Inconclusive. Material type not suitable. Remarks

%

Moisture Condition Value

Dry density after test

Moisture Content

Bulk density after test Mg/m³

Mg/m³

% #N/A

8.5

1.55

1.64 1.75

1.53 1.55

1.91

7.2 12.7 5.5

Material retained on 20mm sieve Steepest straight line

Procedure / Preparation

Initial moisture content <20mm Method of determining MCV

BS1377:Part 1 and Part 4, clause 5.5

4.3

Soil description

1.56

8.5

17.4

#N/A

1.63

1.631.69

#N/A #N/A #N/A

MCVREL 2


Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

WS2

0.60

5 B

ESGD3110-13201308150000000111

QA Ref


Number of Blows

644832241612864321

1816141210864200

5

10

15

20

25

30

Moisture Condition Value , MCV,

Cha

nge

in P

enet

ratio

n -

mm

test 1 2 3 4 5

Spec Ref

Figure

� Printed:21/10/2013 16:16

%

Notes :

Soil description

%

Mg/m³

11

2.15

12

12

Test Conditions

Sample Retained on 20 mm sieve

Sample Conditions

%

%

BASETOP

1.92Mg/m³

CBR Values %

Moisture Content - BASE

Bulk Density

Dry Density

mm

Method of Compaction

days 4Soaking PeriodPre

para

tion

11

Recompacted - Rammer compaction with specified effort ( 2.5kg )

Soaked test

2.41.5

5.0 1.9 3.40

0

1.9

Amount of Swell -0.41


Initial Moisture Content

Moisture Content - TOP

YES

Penetration mm

Accepted CBR % 3.4

kgSurcharge applied

2.5

kPa

CBR 1

0.00

0.20

0.40

0.60

0.80

1.00

1.20

1.40

1.60

1.80

2.00

0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 5.5 6 6.5 7 7.5

Penetration - mm

For

ce o

n P

lung

er -

kN

TOPBASE

California Bearing Ratio ( BS1377:1990:Part 4 , section 7 )

Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH1

1.20

8 B

ESGD3110-13201308150000000008

QA Ref

SLR 4.7Rev 89Aug 11

Spec Ref

Figure

� Printed:21/10/2013 16:15

%

Notes :

Soil description

%

Mg/m³

12

2.13

13

13

Test Conditions

Sample Retained on 20 mm sieve

Sample Conditions

%

%

BASETOP

1.90Mg/m³

CBR Values %

Moisture Content - BASE

Bulk Density

Dry Density

mm

Method of Compaction

days 4Soaking PeriodPre

para

tion

11

Recompacted - Rammer compaction with specified effort ( 2.5kg )

Soaked test

7.33.1

5.0 5.4 150

0

5.4

Amount of Swell -0.12


Initial Moisture Content

Moisture Content - TOP

YES

Penetration mm

Accepted CBR % 15

kgSurcharge applied

2.5

kPa

CBR 2

0.00

1.00

2.00

3.00

4.00

5.00

6.00

7.00

8.00

9.00

10.00

0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 5.5 6 6.5 7 7.5

Penetration - mm

For

ce o

n P

lung

er -

kN

TOPBASE

California Bearing Ratio ( BS1377:1990:Part 4 , section 7 )

Project No

Project Name

D3110-13



Depth (m BGL)

Samp No Type

ID

BH4

2.00

11 B

ESGD3110-13201308150000000069

QA Ref

SLR 4.7Rev 89Aug 11

Spec Ref

Figure

� Printed:21/10/2013 16:15

November 2013 Report No D3110-13 Issue 2.0 Enclosure D

ENCLOSURE D

GEOENVIRONMENTAL LABORATORY TEST RESULTS

ESG Scientifics Report EFS/135116M

ESG Scientifics Report EFS/135126M

ESG Scientifics Report EXR/162608




Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

END OF REPORT


EFS/135115 Ver. 1




Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS or MCERTS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.




Accreditation Codes: N (Not Accredited), U (UKAS), UM (UKAS & MCERTS)

(NVM) - denotes the sample matrix is dissimilar to matrices upon which the MCERTS validation was based,and is therefore not accredited for MCERTS.


12-Sep-2013



Report No. EFS/135116M (Ver. 1)

Table 1 Main Analysis Results (Pages 2 to 3)Table of PAH (MS-SIM) (80) Results (Pages 4 to 22)Table of GRO Results (Page 23)Table of TPH (Si) banding (std) (Page 24)GC-FID Chromatograms (Pages 25 to 62)Table of VOC (HSA) Results (Pages 63 to 80)Table of Asbestos Screening Results (Page 81)Analytical and Deviating Sample Overview (Pages 82 to 85)Table of Additional Report Notes (Page 86)Table of Method Descriptions (Page 87)Table of Report Notes (Page 88)Table of Sample Descriptions (Appendix A Page 1 of 1)


All results are reported on a dry weight basis at 105oC unless otherwise stated. (except QC samples)

Where individual results are flagged see report notes for status.EFS/135116M Ver. 1Page 1 of 88

Units : mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kgMethod Codes : GROHSA ICPBOR ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPSOIL ICPSOIL

Method Reporting Limits : 0.2 0.5 0.1 0.3 0.2 1.2 1.6 0.7 0.5 0.5 2 0.5 0.6 16 1 0.1Accreditation Code: UM U UM UM UM UM UM UM UM UM UM U UM UM UM

LAB

ID N

umber C

L/


Sam

ple Date

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Antim

ony (MS

)

Arsenic (M

S)

Cadm

ium (M

S)

Chrom

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Molybdenum

(MS

)

Nickel (M

S)

Selenium

(MS

)

Vanadium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

1321695 BH1 ES 2 0.30 07-Aug-13 Req 0.9 0.6 6.4 1.51 19.8 32.9 25.9 <0.5 1.4 68.0 1.1 69 125.5 2.39 <0.1

1321696 BH1 ES 5 0.60 07-Aug-13 Req 0.9 0.6 6.3 0.29 13.3 18.2 50.6 <0.51 0.7 15.8 <0.5 21.4 81.4 <1 <0.1

1321697 BH1 ES 9 1.90 07-Aug-13 Req <0.5 0.3 5 <0.2 12.6 11 13.2 <0.5 <0.5 11.2 <0.5 13.7 34.1 <1 <0.1

1321698 BH2 ES 2 0.15 07-Aug-13 Req <0.5 0.4 6.6 <0.20 13.6 25.2 10.7 <0.5 1.9 17.9 <0.5 30.8 27.2 1.44 <0.1

1321699 BH2 ES 4 0.50 07-Aug-13 Req <0.5 0.3 4.7 <0.2 12.7 9.8 6.4 <0.5 <0.5 12.2 <0.5 14.4 31.5 <1 <0.1

1321700 BH3 ES 2 0.30 06-Aug-13 Req <0.5 0.3 3.8 <0.2 12.7 8.8 12.4 <0.5 <0.5 10.7 <0.5 13.6 42.3 <1 <0.1

1321701 BH4 ES 2 0.20 05-Aug-13 Req <0.5 0.7 9.5 1.19 29.9 62.1 29.5 <0.5 2.5 35.6 <0.5 24.7 85.1 <1 <0.1

1321702 BH4 ES 9 1.90 05-Aug-13 Req <0.5 0.4 5 0.66 18.2 33.4 62.5 <0.5 0.7 17.4 <0.5 13.4 46.5 1.06 <0.1

1321703 BH5 ES 2 0.20 06-Aug-13 Req <0.5 0.6 6.3 <0.20 22.7 14.4 21.4 <0.5 <0.5 19.7 <0.5 32 60.4 <1 <0.1

1321704 WS1 ES 1 0.10 05-Aug-13 Req <0.5 0.2 4.9 0.34 14.7 22.9 11.7 <0.5 1.4 17.3 <0.5 41.9 76 <1 <0.1

1321705 WS1 ES 2 0.30 05-Aug-13 Req <0.5 0.3 4.2 <0.20 11.3 10.9 17.4 <0.5 <0.5 10.8 <0.5 14.5 44.1 <1 <0.1

1321706 WS2 ES 1 0.10 05-Aug-13 Req <0.5 0.2 5.2 0.47 38.8 15.2 9.1 <0.5 1.2 14.6 0.8 42.8 40.7 1.88 <0.1

1321707 WS2 ES 2 0.30 05-Aug-13 Req <0.5 0.3 5.3 <0.2 22.7 10.9 7.3 <0.5 0.6 13.0 <0.5 23.1 33.5 <1 <0.1

1321708 WS3 ES 1 0.20 05-Aug-13 Req <0.5 1.2 11.8 0.55 19 25.6 129.4 <0.52 1 17.0 0.7 26.0 164 2.34 <0.1

1321709 WS3 ES 7 1.00 05-Aug-13 Req <0.5 0.4 5.6 <0.21 13.9 11.7 20.9 <0.5 <0.5 12.6 <0.5 17 46.1 <1 <0.1

1321710 WS4 ES 2 0.20 05-Aug-13 Req <0.5 0.5 7.4 0.22 15.7 13.5 33.7 <0.5 <0.5 12.5 <0.5 19.5 64.5 <1 <0.1

1321711 WS5 ES 4 0.60 05-Aug-13 Req <0.5 0.4 4.6 0.23 12.0 10 25.5 <0.5 <0.5 8.6 <0.5 16.0 56.1 <1 <0.1

1321712 WS5 ES 6 1.20 05-Aug-13 Req <0.5 0.5 5.5 <0.20 14.5 17.0 19.5 <0.5 <0.5 17.4 <0.5 18.8 61.1 <1 <0.1

1321713 WS5 ES 8 2.50 05-Aug-13 Req <0.5 0.2 3.8 <0.20 7.9 7.4 3.6 <0.5 <0.5 8.2 <0.5 9.0 20 <1 <0.1

Contact

Date Printed

Report Number EFS/135116M

Table Number 1

Fax +44 (0) 1283 554422




Tel +44 (0) 1283 554400

Client Name ESG Southam Soil Sample Analysis

Mr J Litten

12-Sep-2013

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.

EFS/135116M Ver. 1Page 2 of 88

Units : mg/kg mg/kg pH Units mg/kg mg/kg % mg/kg µg/kg mg/kg mg/kg % % M/M mg/kgMethod Codes : ICPSOIL ICPWSS PHSOIL SFAPI SFAPI Sub002a TMSS TPHUSSI VOCHSAS CALC_CR3 KONECR TSBRE1 WSLM59 PAHMSUS

Method Reporting Limits : 36 10 0.5 0.5 0.2 10 0.5 0.1 0.005 0.02Accreditation Code: UM UM UM UM U U U N N N N

LAB

ID N

umber C

L/


Sam

ple Date

Iron

SO

4-- (H2O

sol) mg/l

pH units (A

R)

Cyanide(F

ree) (AR

)

Phenol Index.(A

R)

Âsbestos S

creen

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

VO

C H

SA

-GC

MS

Chrom

ium (III)

Chrom

ium vi:

Total S

ulphur.

Total O

rganic Carbon

PA

H (16) by G

CM

S

1321695 BH1 ES 2 0.30 07-Aug-13 211 142 8.2 <0.5 <0.5 NAIIS 6.0 Req Req <19.8 <0.1 0.362 2.61 Req









1321704 WS1 ES 1 0.10 05-Aug-13 157 72 7.8 <0.6 <0.6 NAIIS 11.0 Req Req <14.7 <0.1 0.305 >25 Req

1321705 WS1 ES 2 0.30 05-Aug-13 127 30 6.9 <0.6 <0.6 NAIIS 9.9 Req Req <11.3 <0.1 0.029 1.23 Req

1321706 WS2 ES 1 0.10 05-Aug-13 166 319 8.0 <0.5 <0.5 CH 8.2 Req Req <38.8 <0.1 0.401 11.62 Req








Contact

Date Printed


Table Number 1

Fax +44 (0) 1283 554422




Tel +44 (0) 1283 554400

Client Name ESG Southam Soil Sample Analysis

Mr J Litten

12-Sep-2013



1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: BH1 ES 2 0.30 Job Number: S13_5116MLIMS ID Number: CL1321695 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13

Quantitation File: Initial Calibration Date Analysed: 05-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 4.53 0.89 100 UAcenaphthene 83-32-9 4.66 0.41 98 UMFluorene 86-73-7 5.07 0.20 92 UMPhenanthrene 85-01-8 5.96 1.84 99 UMAnthracene 120-12-7 6.02 2.17 97 UFluoranthene 206-44-0 7.37 19.00 99 UMPyrene 129-00-0 7.67 22.40 96 UMBenzo[a]anthracene 56-55-3 9.40 13.40 96 UMChrysene 218-01-9 9.45 13.10 98 UMBenzo[b]fluoranthene 205-99-2 10.96 29.00 98 UMBenzo[k]fluoranthene 207-08-9 11.00 10.60 94 UMBenzo[a]pyrene 50-32-8 11.40 24.70 96 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 19.50 87 UMDibenzo[a,h]anthracene 53-70-3 12.85 3.88 91 UMBenzo[g,h,i]perylene 191-24-2 13.17 20.40 97 UMTotal (USEPA16) PAHs - - < 181.37 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 95 2-Fluorobiphenyl 98Acenaphthene-d10 94 Terphenyl-d14 77Phenanthrene-d10 93Chrysene-d12 98Perylene-d12 100

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.



1




Accredited?: Yes


(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 4.54 0.10 98 UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.96 0.40 98 UMAnthracene 120-12-7 6.02 0.18 94 UFluoranthene 206-44-0 7.37 2.72 99 UMPyrene 129-00-0 7.67 2.75 95 UMBenzo[a]anthracene 56-55-3 9.40 1.80 93 UMChrysene 218-01-9 9.45 1.93 98 UMBenzo[b]fluoranthene 205-99-2 10.96 3.00 98 UMBenzo[k]fluoranthene 207-08-9 11.00 1.02 94 UMBenzo[a]pyrene 50-32-8 11.40 2.32 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 1.73 89 UMDibenzo[a,h]anthracene 53-70-3 12.84 0.34 98 UMBenzo[g,h,i]perylene 191-24-2 13.17 1.76 97 UMTotal (USEPA16) PAHs - - < 20.33 - N







1




Accredited?: Yes


(min) mg/kg code

Naphthalene 91-20-3 - < 0.08 - UMAcenaphthylene 208-96-8 - < 0.08 - UAcenaphthene 83-32-9 - < 0.08 - UMFluorene 86-73-7 - < 0.08 - UMPhenanthrene 85-01-8 - < 0.08 - UMAnthracene 120-12-7 - < 0.08 - UFluoranthene 206-44-0 7.37 0.36 99 UMPyrene 129-00-0 7.67 0.39 95 UMBenzo[a]anthracene 56-55-3 9.40 0.24 91 UMChrysene 218-01-9 9.45 0.20 92 UMBenzo[b]fluoranthene 205-99-2 10.96 0.39 98 UMBenzo[k]fluoranthene 207-08-9 11.00 0.16 94 UMBenzo[a]pyrene 50-32-8 11.40 0.30 98 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 0.23 95 UMDibenzo[a,h]anthracene 53-70-3 - < 0.08 - UMBenzo[g,h,i]perylene 191-24-2 13.17 0.20 72 UMTotal (USEPA16) PAHs - - < 3.08 - N







1




Accredited?: Yes


(min) mg/kg code

Naphthalene 91-20-3 3.47 0.55 97 UMAcenaphthylene 208-96-8 4.53 0.52 86 UAcenaphthene 83-32-9 4.66 8.85 94 UMFluorene 86-73-7 5.06 9.29 93 UMPhenanthrene 85-01-8D 5.96 86.30 99 UMAnthracene 120-12-7 6.02 29.20 98 UFluoranthene 206-44-0D 7.38 142.00 97 UMPyrene 129-00-0D 7.68 109.40 94 UMBenzo[a]anthracene 56-55-3 9.41 49.70 97 UMChrysene 218-01-9 9.46 48.10 97 UMBenzo[b]fluoranthene 205-99-2 10.96 48.30 98 UMBenzo[k]fluoranthene 207-08-9 11.00 18.70 96 UMBenzo[a]pyrene 50-32-8 11.40 37.80 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 24.00 86 UMDibenzo[a,h]anthracene 53-70-3 12.85 5.32 94 UMBenzo[g,h,i]perylene 191-24-2 13.16 19.00 97 UMTotal (USEPA16) PAHs - - 636.89 - N







1




Accredited?: Yes


(min) mg/kg code

Naphthalene 91-20-3 - < 0.08 - UMAcenaphthylene 208-96-8 - < 0.08 - UAcenaphthene 83-32-9 4.66 0.61 98 UMFluorene 86-73-7 5.07 0.38 90 UMPhenanthrene 85-01-8 5.96 4.50 99 UMAnthracene 120-12-7 6.02 1.91 94 UFluoranthene 206-44-0 7.37 14.10 98 UMPyrene 129-00-0 7.67 11.40 95 UMBenzo[a]anthracene 56-55-3 9.40 5.30 96 UMChrysene 218-01-9 9.45 5.05 99 UMBenzo[b]fluoranthene 205-99-2 10.96 5.29 97 UMBenzo[k]fluoranthene 207-08-9 10.99 1.93 97 UMBenzo[a]pyrene 50-32-8 11.40 4.16 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 2.44 99 UMDibenzo[a,h]anthracene 53-70-3 12.85 0.51 92 UMBenzo[g,h,i]perylene 191-24-2 13.16 2.13 98 UMTotal (USEPA16) PAHs - - < 59.95 - N







1




Accredited?: Yes


(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 - < 0.09 - UMPyrene 129-00-0 - < 0.09 - UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 - < 0.09 - UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.46 - N







1




Accredited?: Yes


(min) mg/kg code

Naphthalene 91-20-3 3.47 0.42 97 UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.96 0.21 98 UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 - < 0.09 - UMPyrene 129-00-0 - < 0.09 - UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 - < 0.09 - UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.92 - N







1




Accredited?: Yes


(min) mg/kg code








1




Accredited?: Yes


(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 7.37 0.12 98 UMPyrene 129-00-0 7.67 0.12 98 UMBenzo[a]anthracene 56-55-3 9.40 0.10 94 UMChrysene 218-01-9 9.45 0.10 86 UMBenzo[b]fluoranthene 205-99-2 10.96 0.17 93 UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 11.40 0.13 84 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.83 0.12 98 UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 13.17 0.12 93 UMTotal (USEPA16) PAHs - - < 1.69 - N







1


Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: WS1 ES 1 0.10 Job Number: S13_5116MLIMS ID Number: CL1321704 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13


Accredited?: Yes


(min) mg/kg code

Naphthalene 91-20-3 3.47 0.25 95 UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.96 0.16 98 UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 7.37 0.17 96 UMPyrene 129-00-0 7.67 0.27 96 UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 9.45 0.09 76 UMBenzo[b]fluoranthene 205-99-2 10.96 0.25 93 UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 11.40 0.18 59 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 0.15 91 UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 13.17 0.19 82 UMTotal (USEPA16) PAHs - - < 2.33 - N







1




Accredited?: Yes


(min) mg/kg code








1




Accredited?: Yes


(min) mg/kg code

Naphthalene 91-20-3 3.47 0.41 95 UMAcenaphthylene 208-96-8 4.53 0.90 86 UAcenaphthene 83-32-9 4.66 29.20 94 UMFluorene 86-73-7 5.06 32.80 94 UMPhenanthrene 85-01-8D 5.97 181.00 97 UMAnthracene 120-12-7D 6.02 70.40 98 UFluoranthene 206-44-0D 7.38 205.00 96 UMPyrene 129-00-0D 7.68 153.00 92 UMBenzo[a]anthracene 56-55-3D 9.41 66.80 97 UMChrysene 218-01-9D 9.46 60.50 97 UMBenzo[b]fluoranthene 205-99-2D 10.97 61.70 98 UMBenzo[k]fluoranthene 207-08-9 11.00 23.50 94 UMBenzo[a]pyrene 50-32-8 11.40 46.40 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 27.50 87 UMDibenzo[a,h]anthracene 53-70-3 12.85 6.62 93 UMBenzo[g,h,i]perylene 191-24-2 13.17 24.00 97 UMTotal (USEPA16) PAHs - - 988.66 - N







1




Accredited?: Yes


(min) mg/kg code

Naphthalene 91-20-3 - < 0.08 - UMAcenaphthylene 208-96-8 - < 0.08 - UAcenaphthene 83-32-9 4.66 0.45 96 UMFluorene 86-73-7 5.06 0.46 90 UMPhenanthrene 85-01-8 5.96 3.01 99 UMAnthracene 120-12-7 6.02 1.95 98 UFluoranthene 206-44-0 7.37 5.58 98 UMPyrene 129-00-0 7.67 4.43 94 UMBenzo[a]anthracene 56-55-3 9.40 2.10 96 UMChrysene 218-01-9 9.45 2.11 95 UMBenzo[b]fluoranthene 205-99-2 10.96 2.16 98 UMBenzo[k]fluoranthene 207-08-9 11.00 0.80 93 UMBenzo[a]pyrene 50-32-8 11.40 1.70 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 1.10 88 UMDibenzo[a,h]anthracene 53-70-3 12.85 0.20 77 UMBenzo[g,h,i]perylene 191-24-2 13.17 0.97 99 UMTotal (USEPA16) PAHs - - < 27.24 - N







1




Accredited?: Yes


(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 4.54 0.13 100 UAcenaphthene 83-32-9 4.66 0.10 96 UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.96 1.26 99 UMAnthracene 120-12-7 6.02 0.44 98 UFluoranthene 206-44-0 7.37 3.32 99 UMPyrene 129-00-0 7.67 3.04 94 UMBenzo[a]anthracene 56-55-3 9.40 1.73 93 UMChrysene 218-01-9 9.45 1.80 93 UMBenzo[b]fluoranthene 205-99-2 10.96 2.79 98 UMBenzo[k]fluoranthene 207-08-9 11.00 0.92 94 UMBenzo[a]pyrene 50-32-8 11.40 2.26 99 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 1.73 84 UMDibenzo[a,h]anthracene 53-70-3 12.85 0.31 47 UMBenzo[g,h,i]perylene 191-24-2 13.17 1.62 97 UMTotal (USEPA16) PAHs - - < 21.62 - N







1




Accredited?: Yes


(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 7.37 0.10 99 UMPyrene 129-00-0 7.67 0.10 97 UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 10.96 0.10 79 UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.48 - N







1




Accredited?: Yes


(min) mg/kg code








1




Accredited?: Yes


(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.97 0.20 98 UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 7.37 0.35 99 UMPyrene 129-00-0 7.67 0.28 96 UMBenzo[a]anthracene 56-55-3 9.40 0.14 94 UMChrysene 218-01-9 9.45 0.12 98 UMBenzo[b]fluoranthene 205-99-2 10.96 0.18 95 UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 11.40 0.12 84 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.83 0.09 90 UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 13.17 0.09 72 UMTotal (USEPA16) PAHs - - < 2.20 - N







1




Accredited?: Yes


(min) mg/kg code

Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 4.54 0.10 98 UAcenaphthene 83-32-9 4.66 0.24 98 UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.96 1.25 99 UMAnthracene 120-12-7 6.02 0.76 97 UFluoranthene 206-44-0 7.37 7.87 98 UMPyrene 129-00-0 7.67 6.97 94 UMBenzo[a]anthracene 56-55-3 9.40 3.72 94 UMChrysene 218-01-9 9.45 3.72 99 UMBenzo[b]fluoranthene 205-99-2 10.96 5.04 98 UMBenzo[k]fluoranthene 207-08-9 11.00 1.86 94 UMBenzo[a]pyrene 50-32-8 11.40 4.01 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 2.70 88 UMDibenzo[a,h]anthracene 53-70-3 12.85 0.52 97 UMBenzo[g,h,i]perylene 191-24-2 13.17 2.66 92 UMTotal (USEPA16) PAHs - - < 41.60 - N







1




Accredited?: Yes


(min) mg/kg code








Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)

Customer and Site Details: ESG Southam : Gnossall St Lawrence Primary School Matrix: Soil

Job Number: s13_5116 Date Booked in: 30-Aug-13

Directory: D:\TES\DATA\Y2013\0904HSA_GC12\090413 2013-09-04 14-26-43\127B2701.D Date extracted: 04-Sep-13

Method: Headspace GCFID Date Analysed: 04-Sep-13, 23:03:42Accreditation Code: UM

* Sample data with an asterisk are not UKAS accredi ted.

Concentration, (mg/kg) - as dry weight. AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C 6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO

CL1321695 BH1 ES 2 0.30 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321696 BH1 ES 5 0.60 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321697 BH1 ES 9 1.90 <0.010 <0.010 <0.010 <0.010 <0.010 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321698 BH2 ES 2 0.15 <0.012 <0.012 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321699 BH2 ES 4 0.50 <0.010 <0.010 <0.010 <0.010 <0.010 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321700 BH3 ES 2 0.30 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321701 BH4 ES 2 0.20 <0.012 <0.012 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321702 BH4 ES 9 1.90 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321703 BH5 ES 2 0.20 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321704 WS1 ES 1 0.10 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321705 WS1 ES 2 0.30 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321706 WS2 ES 1 0.10 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321707 WS2 ES 2 0.30 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321708 WS3 ES 1 0.20 <0.012 <0.012 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321709 WS3 ES 7 1.00 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321710 WS4 ES 2 0.20 <0.012 <0.012 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321711 WS5 ES 4 0.60 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321712 WS5 ES 6 1.20 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

CL1321713 WS5 ES 8 2.50 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2

Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions



ALIPHATIC / AROMATIC FRACTION BY GC/FID

Customer and Site Details: ESG Southam : Gnossall St Lawrence Primary School Matrix: SoilJob Number: S13_5116 Separation: Silica gel Date Booked in: 30-Aug-13QC Batch Number: 130720 Eluents: Hexane, DCM Date Extracted: 05-Sep-13Directory: D:\TES\DATA\Y2013\02\0906TPH_GC3\059B6201.D Date Analysed: 06-Sep-13Method: Ultra Sonic

This sample data is not MCERTS accredited. Concentration, (mg/kg) - as dry weight.* This sample data is not ISO17025 accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40

Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aro matics Aliphatics Aromatics Aliphatics Aromatics Aliphat ics Aromatics

CL1321695 BH1 ES 2 0.30 <4 6.85 <4 <4 6.67 <4 10 49.4 111 888 174 1150

CL1321696 BH1 ES 5 0.60 <4 10.9 <4 <4 <4 <4 <4 10.5 <9.71 112 <22 151

CL1321697 BH1 ES 9 1.90 <4 4.86 <4 <4 <4 <4 <4 <4 <9.16 13.5 <21 22.5

CL1321698 BH2 ES 2 0.15 <5 <5 <5 <5 5.9 42.3 11.3 485 146 1660 199 2350

CL1321699 BH2 ES 4 0.50 <4 <4 <4 <4 <4 <4 <4 30.6 <9.17 147 <21 190

CL1321700 BH3 ES 2 0.30 <5 20.7 <5 <5 <5 <5 <5 <5 <10.01 <10.01 <23 27.7

CL1321701 BH4 ES 2 0.20 <5 <5 <5 <5 <5 <5 <5 <5 <10.14 11.3 <23 <23

CL1321702 BH4 ES 9 1.90 <4 <4 <4 <4 <4 <4 <4 <4 <9.46 <9.46 <22 <22

CL1321703 BH5 ES 2 0.20 <4 7.39 <4 <4 <4 <4 <4 <4 <9.55 14.5 <22 26

CL1321704 WS1 ES 1 0.10 <4 16.6 <4 <4 <4 <4 9.2 12 384 662 572 1000

CL1321705 WS1 ES 2 0.30 <4 14.7 <4 <4 <4 <4 <4 <4 <9.72 31.7 <22 60.9

CL1321706 WS2 ES 1 0.10 <4 8.68 <4 <4 9.9 129 26.4 1030 388 2450 584 3940

CL1321707 WS2 ES 2 0.30 <4 <4 <4 <4 <4 <4 <4 13.6 <9.29 72.9 <21 95.1

CL1321708 WS3 ES 1 0.20 <5 <5 <5 <5 <5 <5 <5 16.8 29.3 174 35.9 226

CL1321709 WS3 ES 7 1.00 <4 30.2 <4 <4 <4 <4 <4 <4 <9.82 12.7 <22 47.6

CL1321710 WS4 ES 2 0.20 <5 34.4 <5 <5 <5 <5 <5 <5 <10.12 13 <23 52

CL1321711 WS5 ES 4 0.60 <4 <4 <4 <4 <4 <4 <4 <4 <9.77 14.9 <22 <22

CL1321712 WS5 ES 6 1.20 <4 <4 <4 <4 <4 6.27 5.6 34.3 21.8 213 29.6 272

CL1321713 WS5 ES 8 2.50 <4 <4 <4 <4 <4 <4 <4 <4 <9.27 <9.27 <21 <21



Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.

Sample ID: CL1321695ALI Job Number: S13_5116MMultiplier: 14.88 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH1 ES 2 0.30Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\050F5801.D

min0 1 2 3 4 5

pA

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FID1 A, (0906TPH_GC3\050F5801.D)



Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.

Sample ID: CL1321695ARO Job Number: S13_5116MMultiplier: 11.36 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH1 ES 2 0.30Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\088B4401.D

min0 1 2 3 4 5

pA

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1400

FID2 B, (0906TPH_GC3\088B4401.D)





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FID1 A, (0906TPH_GC3\004F5901.D)




Sample ID: CL1321696ARO Job Number: S13_5116MMultiplier: 12 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH1 ES 5 0.60Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\089B4501.D

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FID2 B, (0906TPH_GC3\089B4501.D)





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FID1 A, (0906TPH_GC3\005F6001.D)





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FID2 B, (0906TPH_GC3\090B4601.D)





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FID1 A, (0906TPH_GC3\006F6101.D)




Sample ID: CL1321698ARO Job Number: S13_5116MMultiplier: 12 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH2 ES 2 0.15Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\091B4701.D

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FID2 B, (0906TPH_GC3\091B4701.D)





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FID1 A, (0906TPH_GC3\007F6201.D)





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100

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FID2 B, (0906TPH_GC3\092B4801.D)





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FID1 A, (0906TPH_GC3\008F6301.D)





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FID2 B, (0906TPH_GC3\093B4901.D)





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FID1 A, (0906TPH_GC3\009F6401.D)





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FID2 B, (0906TPH_GC3\094B5001.D)





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FID1 A, (0906TPH_GC3\010F6501.D)





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FID2 B, (0906TPH_GC3\095B5101.D)





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FID1 A, (0906TPH_GC3\011F6601.D)





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FID2 B, (0906TPH_GC3\096B5201.D)




Sample ID: CL1321704ALI Job Number: S13_5116MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS1 ES 1 0.10Acquisition Date/Time: 07-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\012F6701.D

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FID1 A, (0906TPH_GC3\012F6701.D)




Sample ID: CL1321704ARO Job Number: S13_5116MMultiplier: 11.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS1 ES 1 0.10Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\097B5301.D

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FID2 B, (0906TPH_GC3\097B5301.D)





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FID1 A, (0906TPH_GC3\013F6801.D)





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FID2 B, (0906TPH_GC3\098B5401.D)





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FID1 A, (0906TPH_GC3\014F6901.D)





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FID2 B, (0906TPH_GC3\099B5501.D)





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FID1 A, (0906TPH_GC3\015F7001.D)





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FID2 B, (0906TPH_GC3\100B5601.D)





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FID1 A, (0906TPH_GC3\016F7101.D)





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FID2 B, (0906TPH_GC3\054B5701.D)





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FID1 A, (0906TPH_GC3\017F7201.D)





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FID2 B, (0906TPH_GC3\055B5801.D)





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FID1 A, (0906TPH_GC3\018F7301.D)





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FID2 B, (0906TPH_GC3\056B5901.D)





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FID1 A, (0906TPH_GC3\019F7401.D)





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FID2 B, (0906TPH_GC3\057B6001.D)





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FID1 A, (0906TPH_GC3\020F7501.D)





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FID2 B, (0906TPH_GC3\058B6101.D)





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FID1 A, (0906TPH_GC3\021F7601.D)





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FID2 B, (0906TPH_GC3\059B6201.D)



Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH1 ES 5 0.60 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321696 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 4

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM

Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 4.58 6 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM

Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 90 Dibromofluoromethane 1161,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 90 Toluene-d8 97

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 83Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 691,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 58m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 27Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
















































Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 6.22 1 M UM





Benzene 71-43-2 4.31 4 M UM n-Butylbenzene 104-51-8 * - < 1 - N


Trichloroethene 79-01-6 4.58 26 75 UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM



Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 7.27 14 M UM


Toluene 108-88-3 5.07 8 M UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 80 Dibromofluoromethane 1221,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 76 Toluene-d8 96

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 59Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 421,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 34m and p-Xylene 108-38-3/106-42-3 5.64 6 M UM Naphthalene-d8 7.25 11Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.































































































































































Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS1 ES 1 0.10 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321704 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 12


























Toluene 108-88-3 5.07 8 M UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 66 Dibromofluoromethane 1351,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 63 Toluene-d8 89


















































Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 6.22 2 M UM










Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 7.26 31 M UM






















































































































































































































Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM









Page 1 of 1

Report No:

Report Date: 06/09/2013Project Number:

Sample Number

Sample Date

Sample Location Test DateTotal Sample Dry Weight

(g)

Weight of <2mm

Fraction (g)

Asbestos(g) in >8mm+>2mm

Asbestos(g) in <2mm

% Asbestos by weight of Total Dried Sample

CL/1321695 07/08/13 BH1 0.30 05/09/2013 Screen OnlyCL/1321696 07/08/13 BH1 0.60 05/09/2013 Screen OnlyCL/1321697 07/08/13 BH1 1.90 05/09/2013 Screen OnlyCL/1321698 07/08/13 BH2 0.15 05/09/2013 Screen OnlyCL/1321699 07/08/13 BH2 0.50 05/09/2013 Screen OnlyCL/1321700 06/08/13 BH3 0.30 05/09/2013 Screen OnlyCL/1321701 05/08/13 BH4 0.20 05/09/2013 Screen OnlyCL/1321702 05/08/13 BH4 1.90 05/09/2013 Screen OnlyCL/1321703 06/08/13 BH5 0.20 05/09/2013 Screen OnlyCL/1321704 05/08/13 WS1 0.10 05/09/2013 Screen OnlyCL/1321705 05/08/13 WS1 0.30 05/09/2013 Screen OnlyCL/1321706 05/08/13 WS2 0.10 05/09/2013 Screen & IDCL/1321707 05/08/13 WS2 0.30 05/09/2013 Screen OnlyCL/1321708 05/08/13 WS3 0.20 05/09/2013 Screen OnlyCL/1321709 05/08/13 WS3 1.00 05/09/2013 Screen OnlyCL/1321710 05/08/13 WS4 0.20 05/09/2013 Screen OnlyCL/1321711 05/08/13 WS5 0.60 05/09/2013 Screen OnlyCL/1321712 05/08/13 WS5 1.20 05/09/2013 Screen OnlyCL/1321713 05/08/13 WS5 2.50 05/09/2013 Screen Only

Name: Louise JamesAuthorised Signatory:

Position: Lab Project Manager

Sampling has been carried out by a third party

For the attention of:

Address:

ESG Environmental Chemistry

ANO-0488-06722Etwall House, Bretby Business Park, Ashby Road, Burton upon Trent

Client:

Detection limit of Method SCI-ASB-020 is 0.001%

ESG Asbestos Limited Certificate of Analysis for As bestos in Soils

ESG Southam

Asbestos Fibre Types Identified

ASBESTOS ANALYSIS RESULTS - SOIL ANALYSIS

S135116Gnossall St Lawrence Primary School

NAIISNAIIS

Site Address:

NAIISNAIIS

NAIISNAIISNAIIS

NAIISNAIIS

NAIIS

Chrysotile(Free Fibres)NAIISNAIISNAIISNAIISNAIIS

NAIISNAIIS

The sample analysis for the above results was carried out using the procedures detailed in ESG Asbestos Limited in house method (SCI-ASB-020) based on HSE document MDHS 90 - Asbestos Contaminated Land - Draft 5 - November 1997 (withdrawn). Fibre identification was carried out using ESG Asbestos Limited in house method of transmitted/polarised light microscopy and centre stop dispersion staining (SCI-ASB-007), based on HSE’s HSG 248. The analysis of fine fraction for asbestos content only includes fibres and does not discriminate non-asbestos fibres. All fibres are assumed, unless specified, to be amphiboles. All tests were carried out at ESG Asbestos Laboratory, Ashbourne House, Bretby Business Park, Ashby Road, Burton-upon-Trent, Staffordshire. DE15 0XD, UKAS Laboratory Number 1089.

NAACR = Not Analysed at Clients Request NAIIS = No A sbestos Identified in Sample (Screens Only)

NADIS = No Asbestos Detected in Sample (ID & Quant Only)Keys

NAIIS

1089




MethodID

CA

LC_C

R3

CE

N Leachate

CustS

erv

GR

OH

SA

ICP

BO

R

ICP

MS

S

ICP

SO

IL

ICP

WS

S

KO

NE

CR

MC

ertS

PA

HM

SU

S

PH

SO

IL


Chrom

ium (III)

CE

N Leac(P

)1

Report B

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Antim

ony (MS

)

Arsenic (M

S)

Cadm

ium (M

S)

Chrom

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Molybdenum

(MS

)

Nickel (M

S)

Selenium

(MS

)

Vanadium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

SO

4-- (H2O

sol) mg/l

Chrom

ium vi:

MC

ertS A

nalysis

PA

H (16) by G

CM

S

pH units (A

R)

��

CL/1321695 BH1 0.30 07/08/13CL/1321696 BH1 0.60 07/08/13CL/1321697 BH1 1.90 07/08/13CL/1321698 BH2 0.15 07/08/13CL/1321699 BH2 0.50 07/08/13CL/1321700 BH3 0.30 06/08/13CL/1321701 BH4 0.20 05/08/13CL/1321702 BH4 1.90 05/08/13CL/1321703 BH5 0.20 06/08/13CL/1321704 WS1 0.10 05/08/13CL/1321705 WS1 0.30 05/08/13CL/1321706 WS2 0.10 05/08/13CL/1321707 WS2 0.30 05/08/13CL/1321708 WS3 0.20 05/08/13CL/1321709 WS3 1.00 05/08/13















MethodID

SF

AP

I

Sub002a

TM

SS

TP

HU

SS

I

TS

BR

E1

VO

CH

SA

S

WS

LM59


Cyanide(F

ree) (AR

)

Phenol Index.(A

R)

Âsbestos S

creen

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

Total S

ulphur.

VO

C H

SA

-GC

MS

Total O

rganic Carbon

��

CL/1321695 BH1 0.30 07/08/13CL/1321696 BH1 0.60 07/08/13CL/1321697 BH1 1.90 07/08/13CL/1321698 BH2 0.15 07/08/13CL/1321699 BH2 0.50 07/08/13CL/1321700 BH3 0.30 06/08/13CL/1321701 BH4 0.20 05/08/13CL/1321702 BH4 1.90 05/08/13CL/1321703 BH5 0.20 06/08/13CL/1321704 WS1 0.10 05/08/13CL/1321705 WS1 0.30 05/08/13CL/1321706 WS2 0.10 05/08/13CL/1321707 WS2 0.30 05/08/13CL/1321708 WS3 0.20 05/08/13CL/1321709 WS3 1.00 05/08/13















MethodID

CA

LC_C

R3

CE

N Leachate

CustS

erv

GR

OH

SA

ICP

BO

R

ICP

MS

S

ICP

SO

IL

ICP

WS

S

KO

NE

CR

MC

ertS

PA

HM

SU

S

PH

SO

IL


Chrom

ium (III)

CE

N Leac(P

)1

Report B

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Antim

ony (MS

)

Arsenic (M

S)

Cadm

ium (M

S)

Chrom

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Molybdenum

(MS

)

Nickel (M

S)

Selenium

(MS

)

Vanadium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

SO

4-- (H2O

sol) mg/l

Chrom

ium vi:

MC

ertS A

nalysis

PA

H (16) by G

CM

S

pH units (A

R)

��

CL/1321710 WS4 0.20 05/08/13CL/1321711 WS5 0.60 05/08/13CL/1321712 WS5 1.20 05/08/13CL/1321713 WS5 2.50 05/08/13















MethodID

SF

AP

I

Sub002a

TM

SS

TP

HU

SS

I

TS

BR

E1

VO

CH

SA

S

WS

LM59


Cyanide(F

ree) (AR

)

Phenol Index.(A

R)

Âsbestos S

creen

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

Total S

ulphur.

VO

C H

SA

-GC

MS

Total O

rganic Carbon

��

CL/1321710 WS4 0.20 05/08/13CL/1321711 WS5 0.60 05/08/13CL/1321712 WS5 1.20 05/08/13CL/1321713 WS5 2.50 05/08/13













Report Number : EFS/135116

Method Code

Sample IDThe following information should be taken into cons ideration when using the

data contained within this report

VOCHSAS CL/1321698

Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data

VOCHSAS CL/1321701


VOCHSAS CL/1321704


VOCHSAS CL/1321706


VOCHSAS CL/1321708


Additional Report Notes




Method Description

Soil CALC_CR3 Air Dried Calculated from the difference between Total Chromium and Hexavalent Chromium

Soil GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons (GRO) by Headspace GCFID

Soil ICPBOR Air Dried Determination of Boron in soil samples by hot water extraction followed by ICPOES detection

Soil ICPMSS Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPMS

Soil ICPSOIL Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPOES detection


Soil KONECR Air Dried Determination of Chromium vi in soil samples by water extraction followed by colorimetric detection

Soil PAHMSUS As Received Determination of Polycyclic Aromatic Hydrocarbons (PAH) by hexane/acetone extraction followed by GCMS detection

Soil PHSOIL As Received Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Soil SFAPI As Received Segmented flow analysis with colorimetric detectionSoil SubCon* * Contact Laboratory for details of the methodology used by the sub-

contractor.Soil TMSS As Received Determination of the Total Moisture content at 105ºC by loss on

oven drying gravimetric analysisSoil TPHUSSI As Received Determination of hexane/acetone extractable Hydrocarbons in soil

with GCFID detection including quantitation of Aromatic and Aliphatic fractions.


Soil VOCHSAS As Received Determination of Volatile Organic Compounds (VOC) by Headspace GCMS

Soil WSLM59 Air Dried Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection


Method Descriptions


Report Notes

Generic Notes

Soil/Solid Analysis








Asbestos Analysis


Symbol Reference






Client : ESG Southam

Site : Gnossall St Lawrence Primary School

Report Number : S13_5116M

Note: major constituent in upper case

Lab ID Number Client ID

CL/1321695 BH1 ES 2 0.30CL/1321696 BH1 ES 5 0.60CL/1321697 BH1 ES 9 1.90CL/1321698 BH2 ES 2 0.15CL/1321699 BH2 ES 4 0.50CL/1321700 BH3 ES 2 0.30CL/1321701 BH4 ES 2 0.20CL/1321702 BH4 ES 9 1.90CL/1321703 BH5 ES 2 0.20CL/1321704 WS1 ES 1 0.10CL/1321705 WS1 ES 2 0.30CL/1321706 WS2 ES 1 0.10CL/1321707 WS2 ES 2 0.30CL/1321708 WS3 ES 1 0.20CL/1321709 WS3 ES 7 1.00CL/1321710 WS4 ES 2 0.20CL/1321711 WS5 ES 4 0.60CL/1321712 WS5 ES 6 1.20CL/1321713 WS5 ES 8 2.50

Sample Descriptions

Grey Stone SILT

Brown Stone SAND Brown MADE GROUND

Brown Stone SILT Brown Stone SILT

Brown Stone SAND Brown Stone SILT

Brown Stone SAND Grey Stone SILT

Grey Stone SAND

Grey Stone SILT Brown Stone SAND

Brown Stone SILT Brown Stone SAND Brown Stone SILT Brown Stone SILT

Brown Stone SAND

Description

Grey Stone SILT Brown Stone SILT

Appendix A Page 1 of 1 END OF REPORT




Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS or MCERTS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.




11-Sep-2013

The 1 sample described in this report were registered for analysis by ESG on 30-Aug-2013. This report supersedes any versions previously issued by the laboratory.


Report No. EFS/135126M (Ver. 1)


Table 1 Main Analysis Results (Pages 2 to 3)Table of PAH (MS-SIM) (80) Results (Page 4)Table of GRO Results (Page 5)Table of TPH (Si) banding (std) (Page 6)GC-FID Chromatograms (Pages 7 to 8)Table of VOC (HSA) Results (Page 9)Table of Asbestos Results (Page 10)Analytical and Deviating Sample Overview (Pages 11 to 12)Table of Method Descriptions (Page 13)Table of Report Notes (Page 14)Table of Sample Descriptions (Appendix A Page 1 of 1)


All results are reported on a dry weight basis at 105oC unless otherwise stated. (except QC samples)

Accreditation Codes: N (Not Accredited), U (UKAS), UM (UKAS & MCERTS)

(NVM) - denotes the sample matrix is dissimilar to matrices upon which the MCERTS validation was based,and is therefore not accredited for MCERTS.


Units : mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kgMethod Codes : GROHSA ICPBOR ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPSOIL ICPSOIL

Method Reporting Limits : 0.2 0.5 0.1 0.3 0.2 1.2 1.6 0.7 0.5 0.5 2 0.5 0.6 16 1 0.1Accreditation Code: UM U UM UM UM UM UM UM UM UM UM U UM UM UM

LAB

ID N

umber C

L/


Sam

ple Date

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Antim

ony (MS

)

Arsenic (M

S)

Cadm

ium (M

S)

Chrom

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Molybdenum

(MS

)

Nickel (M

S)

Selenium

(MS

)

Vanadium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

1321755 BH5 D 1.10 05-Aug-13 Req <0.5 0.4 4.9 <0.20 19.8 21 25.0 <0.5 0.5 16.1 <0.5 31.8 57.5 75.2 0.66

Contact

Date Printed


Table Number 1

Fax +44 (0) 1283 554422


Mr J Litten

11-Sep-2013




Tel +44 (0) 1283 554400




Units : mg/kg mg/kg pH Units mg/kg mg/kg % mg/kg µg/kg mg/kg mg/kg % % M/M mg/kgMethod Codes : ICPSOIL ICPWSS PHSOIL SFAPI SFAPI Sub002a TMSS TPHUSSI VOCHSAS CALC_CR3 KONECR TSBRE1 WSLM59 PAHMSUS

Method Reporting Limits : 36 10 0.5 0.5 0.2 10 0.5 0.1 0.005 0.02Accreditation Code: UM UM UM UM U U U N N N N

LAB

ID N

umber C

L/


Sam

ple Date

Iron

SO

4-- (H2O

sol) mg/l

pH units (A

R)

Cyanide(F

ree) (AR

)

Phenol Index.(A

R)

Âsbestos S

creen

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

VO

C H

SA

-GC

MS

Chrom

ium (III)

Chrom

ium vi:

Total S

ulphur.

Total O

rganic Carbon

PA

H (16) by G

CM

S

1321755 BH5 D 1.10 05-Aug-13 19400 26 7.7 <0.6 <0.6 NAIIS 13.8 Req Req <19.8 <0.1 0.019 0.74 Req

Contact

Date Printed


Table Number 1

Fax +44 (0) 1283 554422


Mr J Litten

11-Sep-2013




Tel +44 (0) 1283 554400




1


Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: BH5 D 1.10 Job Number: S13_5126MLIMS ID Number: CL1321755 Date Booked in: 30-Aug-13QC Batch Number: 130716 Date Extracted: 04-Sep-13


Accredited?: Yes


(min) mg/kg code









Customer and Site Details: ESG Southam : Gnossall St Lawrence Primary School Matrix: Soil

Job Number: S13_5126 Date Booked in: 30-Aug-13

Directory: D:\TES\DATA\Y2013\0905HSA_GC12\090513 2013-09-05 09-59-58\035F3701.D Date extracted: 05-Sep-13

Method: Headspace GCFID Date Analysed: 05-Sep-13, 21:49:27Accreditation Code: UM

* Sample data with an asterisk are not UKAS accredi ted.

Concentration, (mg/kg) - as dry weight. AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C 6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO

CL1321755 BH5 D 1.10 <0.012 <0.012 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2




Customer and Site Details: ESG Southam : Gnossall St Lawrence Primary School Matrix: SoilJob Number: S13_5126 Separation: Silica gel Date Booked in: 30-Aug-13QC Batch Number: 130716 Eluents: Hexane, DCM Date Extracted: 04-Sep-13Directory: D:\TES\DATA\Y2013\02\0905TPH_GC3\065B1901.D Date Analysed: 05-Sep-13Method: Ultra Sonic

This sample data is not MCERTS accredited. Concentration, (mg/kg) - as dry weight.* This sample data is not ISO17025 accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40


CL1321755 BH5 D 1.10 <5 <5 <5 <5 <5 <5 <5 <5 <10.16 <10.16 <23 <23




Sample ID: CL1321755ALI Job Number: S13_5126MMultiplier: 14.88 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 D 1.10Acquisition Date/Time: 05-Sep-13Datafile: D:\TES\DATA\Y2013\02\0905TPH_GC3\015F1901.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

FID1 A, (0905TPH_GC3\015F1901.D)




Sample ID: CL1321755ARO Job Number: S13_5126MMultiplier: 11.84 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 D 1.10Acquisition Date/Time: 05-Sep-13Datafile: D:\TES\DATA\Y2013\02\0905TPH_GC3\065B1901.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

450

FID2 B, (0905TPH_GC3\065B1901.D)




Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH5 D 1.10 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321755 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5126M Operator: TP Position: 2






























Page 1 of 1

Report No:

Report Date: 03/09/2013Project Number:

Sample Number

Sample Date

Sample Location Test DateTotal Sample Dry Weight

(g)

Weight of <2mm

Fraction (g)

Asbestos(g) in >8mm+>2mm

Asbestos(g) in <2mm

% Asbestos by weight of Total Dried Sample

CL/1321755 05/08/13 BH5 1.10 03/09/2013 Screen Only

Name: Louise JamesAuthorised Signatory:

Position: Lab Project Manager

The sample analysis for the above results was carried out using the procedures detailed in ESG Asbestos Limited in house method (SCI-ASB-020) based on HSE document MDHS 90 - Asbestos Contaminated Land - Draft 5 - November 1997 (withdrawn). Fibre identification was carried out using ESG Asbestos Limited in house method of transmitted/polarised light microscopy and centre stop dispersion staining (SCI-ASB-007), based on HSE’s HSG 248. The analysis of fine fraction for asbestos content only includes fibres and does not discriminate non-asbestos fibres. All fibres are assumed, unless specified, to be amphiboles. All tests were carried out at ESG Asbestos Laboratory, Ashbourne House, Bretby Business Park, Ashby Road, Burton-upon-Trent, Staffordshire. DE15 0XD, UKAS Laboratory Number 1089.

NAACR = Not Analysed at Clients Request NAIIS = No A sbestos Identified in Sample (Screens Only)

NADIS = No Asbestos Detected in Sample (ID & Quant Only)Keys

Site Address:

NAIIS

ESG Southam

Asbestos Fibre Types Identified

ASBESTOS ANALYSIS RESULTS - SOIL ANALYSIS

S135126Gnossall St Lawrence Primary School

Client:

Detection limit of Method SCI-ASB-020 is 0.001%

ESG Asbestos Limited Certificate of Analysis for As bestos in Soils Sampling has been carried out by a third party

For the attention of:

Address:

ESG Environmental Chemistry

ANO-0488-06721Etwall House, Bretby Business Park, Ashby Road, Burton upon Trent

1089




MethodID

CA

LC_C

R3

CE

N Leachate

CustS

erv

GR

OH

SA

ICP

BO

R

ICP

MS

S

ICP

SO

IL

ICP

WS

S

KO

NE

CR

MC

ertS

PA

HM

SU

S

PH

SO

IL


Chrom

ium (III)

CE

N Leac(P

)1

Report B

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Antim

ony (MS

)

Arsenic (M

S)

Cadm

ium (M

S)

Chrom

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Molybdenum

(MS

)

Nickel (M

S)

Selenium

(MS

)

Vanadium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

SO

4-- (H2O

sol) mg/l

Chrom

ium vi:

MC

ertS A

nalysis

PA

H (16) by G

CM

S

pH units (A

R)

��

CL/1321755 BH5 1.10 05/08/13 E E















MethodID

SF

AP

I

Sub002a

TM

SS

TP

HU

SS

I

TS

BR

E1

VO

CH

SA

S

WS

LM59


Cyanide(F

ree) (AR

)

Phenol Index.(A

R)

Âsbestos S

creen

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

Total S

ulphur.

VO

C H

SA

-GC

MS

Total O

rganic Carbon

��

CL/1321755 BH5 1.10 05/08/13 E E














Method Description

Soil CALC_CR3 Air Dried Calculated from the difference between Total Chromium and Hexavalent Chromium

Soil GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons (GRO) by Headspace GCFID

Soil ICPBOR Air Dried Determination of Boron in soil samples by hot water extraction followed by ICPOES detection

Soil ICPMSS Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPMS

Soil ICPSOIL Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPOES detection


Soil KONECR Air Dried Determination of Chromium vi in soil samples by water extraction followed by colorimetric detection

Soil PAHMSUS As Received Determination of Polycyclic Aromatic Hydrocarbons (PAH) by hexane/acetone extraction followed by GCMS detection

Soil PHSOIL As Received Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Soil SFAPI As Received Segmented flow analysis with colorimetric detectionSoil SubCon* * Contact Laboratory for details of the methodology used by the sub-

contractor.Soil TMSS As Received Determination of the Total Moisture content at 105ºC by loss on

oven drying gravimetric analysisSoil TPHUSSI As Received Determination of hexane/acetone extractable Hydrocarbons in soil

with GCFID detection including quantitation of Aromatic and Aliphatic fractions.


Soil VOCHSAS As Received Determination of Volatile Organic Compounds (VOC) by Headspace GCMS

Soil WSLM59 Air Dried Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection


Method Descriptions


Report Notes

Generic Notes

Soil/Solid Analysis








Asbestos Analysis


Symbol Reference






Client : ESG Southam

Site : Gnossall St Lawrence Primary School

Report Number : S13_5126M

Note: major constituent in upper case

Lab ID Number Client ID

CL/1321755 BH5 D 1.10

Sample Descriptions

Description

Brown Stone SILT

Appendix A Page 1 of 1 END OF REPORT








20-Sep-2013


TEST REPORTCEN LEACHATE 2:1

Report No. EXR/162608 (Ver. 2)

Table 1 Main Analysis Results (Pages 2 to 4)Table of Cyanide (Free) Analysis Results (Pages 5 to 25)Analytical and Deviating Sample Overview (Pages 26 to 29)Table of Method Descriptions (Page 30)Table of Report Notes (Page 31)




EXR/162608 Ver. 2

Units : pH units mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/lMethod Codes : WSLM3 Calc_CR3 KONENS ICHALW ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW ICPWATVAR

Method Reporting Limits : 0.01 1 0.1 3 1 1 0.01 0.001 0.001 0.0001 0.001 0.001 0.002 0.002 0.01UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes

LAB

ID N

umber E

X/


Sam

ple Date

pH units w

Chrom

ium (III)

Chloride as C

l w

Fluoride as F

(IC) w

Total S

ulphur as SO

4 (Dissolved) a

Calcium

as Ca (D

issolved) a

Magnesium

as Mg (D

issolved) a

Barium

as Ba (D

issolved) a

Nickel as N

i (Dissolved)

Chrom

ium as C

r (Dissolved)

Cadm

ium as C

d (Dissolved)

Copper as C

u (Dissolved)

Lead as Pb (D

issolved)

Zinc as Z

n (Dissolved)

Manganese as M

n (Dissolved)

Iron as Fe (D

issolved) a

1418768 BH1 ES 2 0.30 07-Aug-13 7.8 <0.01 4 0.4 94 40 3 0.1 0.001 0.001 <0.0001 0.007 0.001 0.034 0.148 0.05

1418769 BH1 ES 5 0.60 07-Aug-13 8.5 <0.01 12 0.8 156 84 3 0.14 0.004 0.002 <0.0001 0.012 0.001 0.035 0.101 <0.01

1418770 BH1 ES 9 1.90 07-Aug-13 7.7 <0.01 20 0.2 202 99 4 0.17 0.002 0.002 <0.0001 0.007 0.002 0.089 0.112 <0.01

1418771 BH2 ES 2 0.15 07-Aug-13 8.1 <0.01 53 0.3 44 40 2 0.19 <0.001 0.003 <0.0001 0.004 <0.001 0.096 0.019 <0.01

1418772 BH2 ES 4 0.50 07-Aug-13 8.8 <0.01 6 0.5 100 63 <1 0.11 0.002 0.008 <0.0001 0.022 0.002 0.02 0.005 0.05

1418773 BH3 ES 2 0.30 06-Aug-13 8.0 <0.01 9 0.5 17 38 7 0.22 <0.001 0.003 <0.0001 0.007 <0.001 0.134 0.004 0.02

1418774 BH4 ES 2 0.20 05-Aug-13 7.9 <0.01 4 0.4 31 45 4 0.11 0.002 0.003 <0.0001 0.01 <0.001 0.043 0.012 0.28

1418775 BH4 ES 9 1.90 05-Aug-13 8.1 <0.01 5 0.4 16 38 4 0.11 0.001 0.002 <0.0001 0.008 0.002 0.039 0.022 0.13

1418776 BH5 ES 2 0.20 06-Aug-13 8.2 <0.01 4 0.8 5 43 6 0.22 0.004 0.007 0.0001 0.013 0.004 0.087 0.125 3.44

1418777 WS1 ES 1 0.10 05-Aug-13 8.0 <0.01 4 0.3 31 55 3 0.11 <0.001 0.003 <0.0001 0.003 0.002 0.016 0.004 <0.01

1418778 WS1 ES 2 0.30 05-Aug-13 8.0 <0.01 3 0.3 9 54 3 0.13 0.002 0.003 <0.0001 0.009 0.002 0.049 0.016 0.14

1418779 WS2 ES 1 0.10 05-Aug-13 8.0 <0.01 8 0.2 128 73 9 0.14 0.003 0.002 <0.0001 0.009 0.001 0.065 0.11 0.13

1418780 WS2 ES 2 0.30 05-Aug-13 8.2 <0.01 2 2.7 15 28 2 0.18 <0.001 0.002 <0.0001 0.006 0.002 0.106 0.017 0.29

1418781 WS3 ES 1 0.20 05-Aug-13 8.2 <0.01 3 1.1 23 77 6 0.31 0.003 0.003 <0.0001 0.022 0.002 0.106 0.047 0.11

1418782 WS3 ES 7 1.00 05-Aug-13 8.2 <0.01 4 0.8 5 29 4 0.16 0.005 0.008 <0.0001 0.011 0.011 0.098 0.083 4.08

1418783 WS4 ES 2 0.20 05-Aug-13 7.9 <0.01 7 0.3 8 53 5 0.25 0.007 0.012 0.0002 0.016 0.02 0.122 0.148 5.51

1418784 WS5 ES 4 0.60 05-Aug-13 9.1 <0.01 7 0.4 15 31 4 0.5 0.008 0.009 0.0002 0.055 0.1 0.401 0.103 3.32

1418785 WS5 ES 6 1.20 05-Aug-13 8.0 <0.01 42 0.2 32 43 2 0.07 0.002 0.003 <0.0001 0.004 0.003 0.025 0.03 0.68

1418786 WS5 ES 8 2.50 05-Aug-13 8.1 <0.01 6 0.4 9 15 4 0.17 0.008 0.014 0.0003 0.013 0.008 0.071 0.247 8.25

Contact

Date Printed

Report Number EXR/162608

Table Number 1

Fax +44 (0) 1283 554422

CEN Leachate 2:1

Mr J Litten

20-Sep-2013




Tel +44 (0) 1283 554400



EXR/162608 Ver. 2

Units : mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l ug/l mg/l mg/l mg/l mg/lMethod Codes : ICPMSW ICPWATVAR ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW KONENS KONENS SFAPI SFAS Sub045 ICPWATVAR PHEHPLCVL PHEHPLCVL PHEHPLCVL

Method Reporting Limits : 0.001 0.01 0.0001 0.001 0.001 0.001 0.001 0.01 0.01 0.02 0.05 5 0.01 0.0005 0.0005 0.0005UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes No No No No No

LAB

ID N

umber E

X/


Sam

ple Date

Arsenic as A

s (Dissolved)

Boron as B

(Dissolved) a

Mercury as H

g (Dissolved)

Selenium

as Se (D

issolved)

Vanadium

as V (D

issolved)

Molybdenum

as Mo (D

issolved)

Antim

ony as Sb (D

issolved)

Am

moniacal N

itrogen as N

Chrom

ium V

I as Cr

Cyanide (T

otal) as CN

Sulphide as S

^Cyanide (F

ree) 5ug/l

Beryllium

as Be (D

issolved) a

Phenol

Cresols

Dim

ethylphenols

1418768 BH1 ES 2 0.30 07-Aug-13 0.001 0.17 <0.0001 0.002 0.005 0.005 0.002 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418769 BH1 ES 5 0.60 07-Aug-13 0.005 0.34 <0.0001 0.002 0.004 0.017 0.005 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418770 BH1 ES 9 1.90 07-Aug-13 0.002 0.23 <0.0001 0.001 0.002 0.005 0.001 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418771 BH2 ES 2 0.15 07-Aug-13 0.001 0.14 <0.0001 0.002 0.002 0.006 0.002 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418772 BH2 ES 4 0.50 07-Aug-13 0.014 0.1 <0.0001 0.003 0.022 0.006 0.003 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418773 BH3 ES 2 0.30 06-Aug-13 0.001 0.15 <0.0001 <0.001 0.002 0.003 0.001 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418774 BH4 ES 2 0.20 05-Aug-13 0.004 0.07 <0.0001 0.001 0.005 0.008 0.003 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418775 BH4 ES 9 1.90 05-Aug-13 0.007 0.07 <0.0001 <0.001 0.004 0.012 0.002 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418776 BH5 ES 2 0.20 06-Aug-13 0.003 0.1 <0.0001 <0.001 0.008 0.004 0.001 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418777 WS1 ES 1 0.10 05-Aug-13 0.001 0.05 <0.0001 0.002 0.002 0.008 0.001 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418778 WS1 ES 2 0.30 05-Aug-13 0.002 0.06 <0.0001 <0.001 0.002 0.005 0.001 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418779 WS2 ES 1 0.10 05-Aug-13 0.005 0.13 <0.0001 0.004 0.008 0.009 0.001 <0.01 <0.01 <0.02 <0.05 <5 <0.01 0.0193 0.0034 0.0075

1418780 WS2 ES 2 0.30 05-Aug-13 0.006 0.16 <0.0001 0.001 0.008 <0.001 0.001 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418781 WS3 ES 1 0.20 05-Aug-13 0.01 0.15 <0.0001 0.002 0.006 0.006 0.004 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418782 WS3 ES 7 1.00 05-Aug-13 0.011 0.13 <0.0001 0.001 0.016 0.007 0.004 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418783 WS4 ES 2 0.20 05-Aug-13 0.004 0.12 <0.0001 <0.001 0.015 0.001 0.002 0.01 <0.01 <0.02 <0.05 <5 <0.01 0.0013 0.0036 0.0088

1418784 WS5 ES 4 0.60 05-Aug-13 0.005 0.45 <0.0001 <0.001 0.013 0.002 0.004 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418785 WS5 ES 6 1.20 05-Aug-13 0.004 0.06 <0.0001 <0.001 0.004 0.002 0.002 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

1418786 WS5 ES 8 2.50 05-Aug-13 0.01 0.09 <0.0001 <0.001 0.018 0.003 0.002 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

Contact

Date Printed


Table Number 1

Fax +44 (0) 1283 554422

CEN Leachate 2:1

Mr J Litten

20-Sep-2013




Tel +44 (0) 1283 554400



EXR/162608 Ver. 2

Units : mg/lMethod Codes : PHEHPLCVL

Method Reporting Limits : 0.0005UKAS Accredited : No

LAB

ID N

umber E

X/


Sam

ple Date

Trim

ethylphenols

1418768 BH1 ES 2 0.30 07-Aug-13 <0.0005

1418769 BH1 ES 5 0.60 07-Aug-13 <0.0005

1418770 BH1 ES 9 1.90 07-Aug-13 <0.0005

1418771 BH2 ES 2 0.15 07-Aug-13 <0.0005

1418772 BH2 ES 4 0.50 07-Aug-13 <0.0005

1418773 BH3 ES 2 0.30 06-Aug-13 <0.0005

1418774 BH4 ES 2 0.20 05-Aug-13 <0.0005

1418775 BH4 ES 9 1.90 05-Aug-13 <0.0005

1418776 BH5 ES 2 0.20 06-Aug-13 <0.0005

1418777 WS1 ES 1 0.10 05-Aug-13 <0.0005

1418778 WS1 ES 2 0.30 05-Aug-13 <0.0005

1418779 WS2 ES 1 0.10 05-Aug-13 0.0052

1418780 WS2 ES 2 0.30 05-Aug-13 <0.0005

1418781 WS3 ES 1 0.20 05-Aug-13 <0.0005

1418782 WS3 ES 7 1.00 05-Aug-13 <0.0005

1418783 WS4 ES 2 0.20 05-Aug-13 <0.0005

1418784 WS5 ES 4 0.60 05-Aug-13 <0.0005

1418785 WS5 ES 6 1.20 05-Aug-13 <0.0005

1418786 WS5 ES 8 2.50 05-Aug-13 <0.0005

Contact

Date Printed


Table Number 1

Fax +44 (0) 1283 554422

CEN Leachate 2:1

Mr J Litten

20-Sep-2013




Tel +44 (0) 1283 554400



EXR/162608 Ver. 2

Report ID - 20056966 - 1

Analytical Report

0754

Final Report

Batch description: W162608Reported on:

20-Sep-2013

Louise SmithEnvironmental Scientifics Group

ESG Environmental ChemistryEtwall House - Ashby RoadBretby Business ParkBurton upon TrentStaffordshireDE15 0YZ

Dear Louise

Please find attached the results for the batch of 19 samples described below.

Samples Registered on: 12-Sep-2013

Analysis Started on: 13-Sep-2013

Analysis Completed on: 20-Sep-2013

Results for Batch Number 20056966

Your Purchase Order Number: 56037 BEC

You will be invoiced shortly by our accounts department.

If we can be of further assistance then please do not hesitate to contact us.

Yours sincerely

Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation. Details of analytical procedures and

performance data are available on request. The date of sample analysis is available on request.

The Environment Agency carries out analytical work to high standards and within the scope of its UKAS accreditation, but has no

knowledge of whether the circumstances or the validity of the procedures used to obtain the samples provided to the laboratory were

representative of the need for which the information was required.

The Environment Agency and/or its staff does not therefore accept any liability for the consequences of any acts or omissions made on

the basis of the analysis or advice or interpretation provided.

William FardonCustomer Services Team Manager

Tel: (0113) 231 [email protected]

NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 1 of 21

mailto: [email protected]

Report ID - 20056966 - 1

Analytical Report

0754

Final Report


20-Sep-2013

Environmental Scientifics Group Cyanide AnalysisClient: Project:

1

CC Environmental Scientifics GroupSample Point Name:

Folder No: 002554063 Sampled on: 7-Aug-13 @ (Time not supplied)

Comments: W1418768 BH1 0.30

Quote No: 10242 Matrix: Freshwater

Lab ID Result Units TestcodeAnalyte MRV AccredFlag

Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC

Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC

NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 2 of 21

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1








NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 3 of 21

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 5 of 21

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 6 of 21

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 7 of 21

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 8 of 21

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 9 of 21

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 10 of 21

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Comments: W1418777 WS1 0.10





NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 11 of 21

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 12 of 21

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 13 of 21

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 14 of 21

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 15 of 21

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 16 of 21

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 17 of 21

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1







Cyanide as CN SX0.00580 mg/l 182UKAS0.005DBDC

NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 18 of 21

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 19 of 21

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NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 20 of 21

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Method Description Summary for all samples in batch Number 20056966 182 SX I Cyanide - (total) - UV digested; determined colorimetrically by CF analyser

183 SX I Cyanide - (free) - determined colorimetrically by CF analyser

Laboratory Site Manager

Simon Padley

All reporting limits quoted are those achievable for clean samples of the relevant matrix. No allowance is made for instances when dilutions are

necessary owing to the nature of the sample or insufficient volume of the sample being available. In these cases higher reporting limits may be

quoted and will be above the MRV.

Solid sample results are determined on a "dried" sample fraction except for parameters where the method description identifies that "as received"

sample was used.

Key to Results Flags:

Samples received outside analysis holding times. It is possible that the results may be compromised.DB

Analysis started outside of specified holding time. It is possible that the results may be compromised.DC

Please note all samples will be retained for 10 working days for aqueous samples and 30 working days for solid samples after reporting unless

otherwise agreed with Customer Services

Key to Lab ID: LE = Leeds, NM = Nottingham, SX = Starcross, SC = Sub-Contracted outside NLS, FI = Field Data - outside NLS, NLS = Calculated

Key to Accreditation: UKAS = Methodology accredited to ISO/IEC 17025:2005, MCertS = Methodology accredited to MCertS Performance Standard

for testing of soils, none = Methodology not accredited

Any subsequent version of this report denoted with a higher version number will supersede this and any previous versions

END OF TEST REPORT

NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 21 of 21

WATER Analysis W162608

CustomerSiteReport No W162608

MethodID

Calc_C

R3

CU

ST

SE

RV

ICH

ALW

ICP

MS

W

ICP

WA

TV

AR

KO

NE

NS


Chrom

ium (III) (C

ALC

)

Report B

(CE

N1)

Fluoride as F

(IC)

Nickel as N

i MS

(Dissolved)

Chrom

ium as C

r MS

(Dissolved)

Cadm

ium as C

d MS

(Dissolved)

Copper as C

u MS

(Dissolved)

Lead as Pb M

S (D

issolved)

Zinc as Z

n MS

(Dissolved)

Manganese as M

n MS

(Dissolved)

Arsenic as A

s MS

(Dissolved)

Mercury as H

g MS

(Dissolved)

Selenium

as Se M

S (D

issolved)

Vanadium

as V M

S (D

issolved)

Molybdenum

as Mo M

S (D

issolved)

Antim

ony as Sb M

S (D

issolved)

Total S

ulphur as SO

4 (Diss) V

AR

Calcium

as Ca (D

issolved) VA

R

Magnesium

as Mg (D

issolved) VA

R

Barium

as Ba (D

issolved) VA

R

Iron as Fe (D

issolved) VA

R

Boron as B

(Dissolved) V

AR

Beryllium

as Be (D

issolved) VA

R

Chloride as C

l (Kone)

Am

moniacal N

itrogen (Kone)

��

EX/1418768 BH1 0.30 07/08/13EX/1418769 BH1 0.60 07/08/13EX/1418770 BH1 1.90 07/08/13EX/1418771 BH2 0.15 07/08/13EX/1418772 BH2 0.50 07/08/13EX/1418773 BH3 0.30 06/08/13EX/1418774 BH4 0.20 05/08/13EX/1418775 BH4 1.90 05/08/13EX/1418776 BH5 0.20 06/08/13EX/1418777 WS1 0.10 05/08/13EX/1418778 WS1 0.30 05/08/13EX/1418779 WS2 0.10 05/08/13EX/1418780 WS2 0.30 05/08/13EX/1418781 WS3 0.20 05/08/13EX/1418782 WS3 1.00 05/08/13













EXR/162608 Ver. 2



MethodID

KO

NE

NS

LeachPrep

PH

EH

PLC

VL

SF

AP

I

SF

AS

Sub045

WS

LM3


Chrom

ium V

I. as Cr (K

one)

Leachate Prep

Phenols by H

PLC

(Low Level)

Cyanide (T

otal) as CN

SF

A

Sulphide as S

SF

A

^Cyanide (F

ree) 5ug/l

pH units

��

EX/1418768 BH1 0.30 07/08/13EX/1418769 BH1 0.60 07/08/13EX/1418770 BH1 1.90 07/08/13EX/1418771 BH2 0.15 07/08/13EX/1418772 BH2 0.50 07/08/13EX/1418773 BH3 0.30 06/08/13EX/1418774 BH4 0.20 05/08/13EX/1418775 BH4 1.90 05/08/13EX/1418776 BH5 0.20 06/08/13EX/1418777 WS1 0.10 05/08/13EX/1418778 WS1 0.30 05/08/13EX/1418779 WS2 0.10 05/08/13EX/1418780 WS2 0.30 05/08/13EX/1418781 WS3 0.20 05/08/13EX/1418782 WS3 1.00 05/08/13













EXR/162608 Ver. 2



MethodID

Calc_C

R3

CU

ST

SE

RV

ICH

ALW

ICP

MS

W

ICP

WA

TV

AR

KO

NE

NS


Chrom

ium (III) (C

ALC

)

Report B

(CE

N1)

Fluoride as F

(IC)

Nickel as N

i MS

(Dissolved)

Chrom

ium as C

r MS

(Dissolved)

Cadm

ium as C

d MS

(Dissolved)

Copper as C

u MS

(Dissolved)

Lead as Pb M

S (D

issolved)

Zinc as Z

n MS

(Dissolved)

Manganese as M

n MS

(Dissolved)

Arsenic as A

s MS

(Dissolved)

Mercury as H

g MS

(Dissolved)

Selenium

as Se M

S (D

issolved)

Vanadium

as V M

S (D

issolved)

Molybdenum

as Mo M

S (D

issolved)

Antim

ony as Sb M

S (D

issolved)

Total S

ulphur as SO

4 (Diss) V

AR

Calcium

as Ca (D

issolved) VA

R

Magnesium

as Mg (D

issolved) VA

R

Barium

as Ba (D

issolved) VA

R

Iron as Fe (D

issolved) VA

R

Boron as B

(Dissolved) V

AR

Beryllium

as Be (D

issolved) VA

R

Chloride as C

l (Kone)

Am

moniacal N

itrogen (Kone)

��

EX/1418783 WS4 0.20 05/08/13EX/1418784 WS5 0.60 05/08/13EX/1418785 WS5 1.20 05/08/13EX/1418786 WS5 2.50 05/08/13













EXR/162608 Ver. 2



MethodID

KO

NE

NS

LeachPrep

PH

EH

PLC

VL

SF

AP

I

SF

AS

Sub045

WS

LM3


Chrom

ium V

I. as Cr (K

one)

Leachate Prep

Phenols by H

PLC

(Low Level)

Cyanide (T

otal) as CN

SF

A

Sulphide as S

SF

A

^Cyanide (F

ree) 5ug/l

pH units

��

EX/1418783 WS4 0.20 05/08/13EX/1418784 WS5 0.60 05/08/13EX/1418785 WS5 1.20 05/08/13EX/1418786 WS5 2.50 05/08/13













EXR/162608 Ver. 2


Method Description

Water Calc_CR3 As Received Calculation of Chromium III from Total Chromium and Chromium VI

Water ICHALW As Received Analysis of halide ions in water using ion-chromatography with conductivity detector

Water ICPMSW As Received Direct quantitative determination of Metals in water samples using ICPMS

Water ICPWATVAR As Received Direct determination of Metals and Sulphate in water samples using ICPOES

Water KONENS As Received Direct analysis using discrete colorimetric analysisWater PHEHPLCVL As Received Determination of Phenols by HPLCWater SFAPI As Received Segmented flow analysis with colorimetric detectionWater SFAS As Received Determination of Sulphide by segmented flow analysis with

colorimetric detectionWater SubCon* * Contact Laboratory for details of the methodology used by the sub-

contractor.Water WSLM3 As Received Determination of the pH of water samples by pH probe

Report Number: W/EXR/162608

Method Descriptions


EXR/162608 Ver. 2

Report Notes

Generic Notes

Soil/Solid Analysis








Asbestos Analysis


Symbol Reference





END OF REPORT


EXR/162608 Ver. 2








11-Sep-2013

The 1 sample described in this report were registered for analysis by ESG on 30-Aug-2013. This report supersedes any versions previously issued by the laboratory.

TEST REPORTCEN LEACHATE 2:1


Table 1 Main Analysis Results (Pages 2 to 4)Sub Contracted Analysis Results (Pages 5 to 7)Analytical and Deviating Sample Overview (Pages 8 to 9)Table of Method Descriptions (Page 10)Table of Report Notes (Page 11)




EXR/162639 Ver. 1

Units : pH units mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/lMethod Codes : WSLM3 Calc_CR3 KONENS ICHALW ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW ICPWATVAR

Method Reporting Limits : 0.01 1 0.1 3 1 1 0.01 0.001 0.001 0.0001 0.001 0.001 0.002 0.002 0.01UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes

LAB

ID N

umber E

X/


Sam

ple Date

pH units w

Chrom

ium (III)

Chloride as C

l w

Fluoride as F

(IC) w

Total S

ulphur as SO

4 (Dissolved) a

Calcium

as Ca (D

issolved) a

Magnesium

as Mg (D

issolved) a

Barium

as Ba (D

issolved) a

Nickel as N

i (Dissolved)

Chrom

ium as C

r (Dissolved)

Cadm

ium as C

d (Dissolved)

Copper as C

u (Dissolved)

Lead as Pb (D

issolved)

Zinc as Z

n (Dissolved)

Manganese as M

n (Dissolved)

Iron as Fe (D

issolved) a

1418932 BH5 D 1.10 05-Aug-13 8.1 <0.02 2 0.8 8 56 5 0.34 0.076 0.023 0.0002 0.07 0.016 0.507 0.03 1.78

Contact

Date Printed


Table Number 1

Fax +44 (0) 1283 554422

CEN Leachate 2:1

Mr J Litten

11-Sep-2013




Tel +44 (0) 1283 554400



EXR/162639 Ver. 1

Units : mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l ug/l mg/l mg/l mg/l mg/lMethod Codes : ICPMSW ICPWATVAR ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW KONENS KONENS SFAPI SFAS Sub045 ICPWATVAR PHEHPLCVL PHEHPLCVL PHEHPLCVL

Method Reporting Limits : 0.001 0.01 0.0001 0.001 0.001 0.001 0.001 0.01 0.01 0.02 0.05 5 0.01 0.0005 0.0005 0.0005UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes No No No No No

LAB

ID N

umber E

X/


Sam

ple Date

Arsenic as A

s (Dissolved)

Boron as B

(Dissolved) a

Mercury as H

g (Dissolved)

Selenium

as Se (D

issolved)

Vanadium

as V (D

issolved)

Molybdenum

as Mo (D

issolved)

Antim

ony as Sb (D

issolved)

Am

moniacal N

itrogen as N

Chrom

ium V

I as Cr

Cyanide (T

otal) as CN

Sulphide as S

^Cyanide (F

ree) 5ug/l

Beryllium

as Be (D

issolved) a

Phenol

Cresols

Dim

ethylphenols

1418932 BH5 D 1.10 05-Aug-13 0.002 0.16 <0.0001 <0.001 0.003 0.004 0.002 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005

Contact

Date Printed


Table Number 1

Fax +44 (0) 1283 554422

CEN Leachate 2:1

Mr J Litten

11-Sep-2013




Tel +44 (0) 1283 554400



EXR/162639 Ver. 1

Units : mg/lMethod Codes : PHEHPLCVL

Method Reporting Limits : 0.0005UKAS Accredited : No

LAB

ID N

umber E

X/


Sam

ple Date

Trim

ethylphenols

1418932 BH5 D 1.10 05-Aug-13 <0.0005

Contact

Date Printed


Table Number 1

Fax +44 (0) 1283 554422

CEN Leachate 2:1

Mr J Litten

11-Sep-2013




Tel +44 (0) 1283 554400



EXR/162639 Ver. 1

Report ID - 20056793 - 1

Analytical Report

0754

Final Report


11-Sep-2013



Dear Louise


Samples Registered on: 06-Sep-2013

Analysis Started on: 10-Sep-2013

Analysis Completed on: 10-Sep-2013





Yours sincerely










NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 1 of 3


Report ID - 20056793 - 1

Analytical Report

0754

Final Report


11-Sep-2013


1


Folder No: 002549751 Sampled on: 5-Sep-13 @ (Time not supplied)

Comments: W1418932 - BH5 1.10



Cyanide : Free as CN SX<0.005 mg/l 183UKAS0.005

NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 2 of 3

Report ID - 20056793 - 1

Analytical Report

0754

Final Report


11-Sep-2013

Method Description Summary for all samples in batch Number 20056793 183 SX I Cyanide - (free) - determined colorimetrically by CF analyser


Simon Padley





sample was used.







END OF TEST REPORT

NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 3 of 3



MethodID

Calc_C

R3

CU

ST

SE

RV

ICH

ALW

ICP

MS

W

ICP

WA

TV

AR

KO

NE

NS


Chrom

ium (III) (C

ALC

)

Report B

(CE

N1)

Fluoride as F

(IC)

Nickel as N

i MS

(Dissolved)

Chrom

ium as C

r MS

(Dissolved)

Cadm

ium as C

d MS

(Dissolved)

Copper as C

u MS

(Dissolved)

Lead as Pb M

S (D

issolved)

Zinc as Z

n MS

(Dissolved)

Manganese as M

n MS

(Dissolved)

Arsenic as A

s MS

(Dissolved)

Mercury as H

g MS

(Dissolved)

Selenium

as Se M

S (D

issolved)

Vanadium

as V M

S (D

issolved)

Molybdenum

as Mo M

S (D

issolved)

Antim

ony as Sb M

S (D

issolved)

Total S

ulphur as SO

4 (Diss) V

AR

Calcium

as Ca (D

issolved) VA

R

Magnesium

as Mg (D

issolved) VA

R

Barium

as Ba (D

issolved) VA

R

Iron as Fe (D

issolved) VA

R

Boron as B

(Dissolved) V

AR

Beryllium

as Be (D

issolved) VA

R

Chloride as C

l (Kone)

Am

moniacal N

itrogen (Kone)

��

EX/1418932 BH5 1.10 05/08/13













EXR/162639 Ver. 1



MethodID

KO

NE

NS

LeachPrep

PH

EH

PLC

VL

SF

AP

I

SF

AS

Sub045

WS

LM3


Chrom

ium V

I. as Cr (K

one)

Leachate Prep

Phenols by H

PLC

(Low Level)

Cyanide (T

otal) as CN

SF

A

Sulphide as S

SF

A

^Cyanide (F

ree) 5ug/l

pH units

��

EX/1418932 BH5 1.10 05/08/13













EXR/162639 Ver. 1


Method Description


Water ICHALW As Received Analysis of halide ions in water using ion-chromatography with conductivity detector

Water ICPMSW As Received Direct quantitative determination of Metals in water samples using ICPMS

Water ICPWATVAR As Received Direct determination of Metals and Sulphate in water samples using ICPOES

Water KONENS As Received Direct analysis using discrete colorimetric analysisWater PHEHPLCVL As Received Determination of Phenols by HPLCWater SFAPI As Received Segmented flow analysis with colorimetric detectionWater SFAS As Received Determination of Sulphide by segmented flow analysis with


contractor.Water WSLM3 As Received Determination of the pH of water samples by pH probe


Method Descriptions


EXR/162639 Ver. 1

Report Notes

Generic Notes

Soil/Solid Analysis








Asbestos Analysis


Symbol Reference





END OF REPORT


EXR/162639 Ver. 1


Site: Gnossall St. Lawrence Primary School






12-Sep-2013

The 1 sample described in this report were registered for analysis by ESG on 05-Sep-2013. This report supersedes any versions previously issued by the laboratory.

TEST REPORTWATER SAMPLE ANALYSIS


Table 1 Main Analysis Results (Pages 2 to 4)Table of PAH (MS-SIM) (10) Results (Page 5)Table of GRO Results (Page 6)Table of TPH (Si) banding (0.01) (Page 7)GC-FID Chromatograms (Pages 8 to 9)Analytical and Deviating Sample Overview (Pages 10 to 11)Table of Method Descriptions (Page 12)Table of Report Notes (Page 13)




EXR/162915 Ver. 1

Units : pH units mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l µg/l mg/l mg/lMethod Codes : WSLM3 Calc_CR3 Calc_HD KONENS ISEF ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPMSW ICPMSW ICPMSW PAHMSW ICPMSW ICPMSW

Method Reporting Limits : 0.01 7 1 0.1 3 1 1 0.01 1 0.001 0.001 0.0001 0.001 0.001UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes

LAB

ID N

umber E

X/


Sam

ple Date

pH units w

Chrom

ium (III)

Total H

ardness as CaC

O3

Chloride as C

l w

Fluoride as F

a

Total S

ulphur as SO

4 (Dissolved) a

Calcium

as Ca (D

issolved) a

Magnesium

as Mg (D

issolved) a

Barium

as Ba (D

issolved) a

Sodium

as Na (D

issolved) a

Nickel as N

i (Dissolved)

Chrom

ium as C

r (Dissolved)

Cadm

ium as C

d (Dissolved)

PA

H G

C-M

S (16) o

Copper as C

u (Dissolved)

Lead as Pb (D

issolved)

1420399 BH3 EW 19 0.00 28-Aug-13 7.2 <0.01 387 46 0.3 50 117 23 0.1 14 0.001 0.006 <0.0001 Req 0.004 <0.001

Contact

Date Printed


Table Number 1

Fax +44 (0) 1283 554422

Water Sample Analysis

Mr J Litten

12-Sep-2013

Gnossall St. Lawrence Primary School



Tel +44 (0) 1283 554400



EXR/162915 Ver. 1

Units : mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/lMethod Codes : ICPMSW ICPMSW ICPWATVAR ICPMSW ICPWATVAR ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW KONENS KONENS KONENS SFAPI SFAPI SFAS

Method Reporting Limits : 0.002 0.002 0.01 0.001 0.01 0.0001 0.001 0.001 0.001 0.001 0.01 0.2 0.01 0.02 0.02 0.05UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes

LAB

ID N

umber E

X/


Sam

ple Date

Zinc as Z

n (Dissolved)

Manganese as M

n (Dissolved)

Iron as Fe (D

issolved) a

Arsenic as A

s (Dissolved)

Boron as B

(Dissolved) a

Mercury as H

g (Dissolved)

Selenium

as Se (D

issolved)

Vanadium

as V (D

issolved)

Molybdenum

as Mo (D

issolved)

Antim

ony as Sb (D

issolved)

Am

moniacal N

itrogen as N

Nitrate as N

Chrom

ium V

I as Cr

Cyanide (F

ree) as CN

Cyanide (T

otal) as CN

Sulphide as S

1420399 BH3 EW 19 0.00 28-Aug-13 <0.002 0.052 <0.01 <0.001 <0.01 <0.0001 0.001 0.002 <0.001 <0.001 0.01 2.6 <0.01 <0.02 <0.02 <0.05

Contact

Date Printed


Table Number 1

Fax +44 (0) 1283 554422


Mr J Litten

12-Sep-2013




Tel +44 (0) 1283 554400



EXR/162915 Ver. 1

Units : mg/l mg/l mg/l µg/l µg/l µg/l µg/l µg/l µg/l mg/l mg/l mg/l mg/lMethod Codes : TPHFID-Si ICPWATVAR GROHSA VOCHSAW VOCHSAW VOCHSAW VOCHSAW VOCHSAW VOCHSAW PHEHPLCVL PHEHPLCVL PHEHPLCVL PHEHPLCVL

Method Reporting Limits : 0.01 0.01 0.1 1 1 1 2 1 1 0.0005 0.0005 0.0005 0.0005UKAS Accredited : Yes No No Yes Yes Yes Yes Yes Yes No No No No

LAB

ID N

umber E

X/


Sam

ple Date

TP

H by G

C(S

i) o

Beryllium

as Be (D

issolved) a

GR

O-H

SA

(AA

)

Benzene

Toluene

Ethyl B

enzene

Xylenes

m/p X

ylenes

o Xylene

Phenol

Cresols

Dim

ethylphenols

Trim

ethylphenols

1420399 BH3 EW 19 0.00 28-Aug-13 Req <0.01 Req <1 <1 <1 <2 <1 <1 <0.0005 <0.0005 <0.0005 <0.0005

Contact

Date Printed


Table Number 1

Fax +44 (0) 1283 554422


Mr J Litten

12-Sep-2013




Tel +44 (0) 1283 554400



EXR/162915 Ver. 1

1


Customer and Site Details: ESG Southam: Gnossall St. Lawrence Primary SchoolSample Details: BH3 EW 19 0.00 Job Number: W16_2915LIMS ID Number: EX1420399 Date Booked in: 05-Sep-13QC Batch Number: 130639 Date Extracted: 06-Sep-13

Quantitation File: Initial Calibration Date Analysed: 06-Sep-13Directory: 906MS10.PAH\ Matrix: WaterDilution: 1.0 Ext Method: Bottle

UKAS accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit(min) ug/l

Naphthalene 91-20-3 - < 0.020 -Acenaphthylene 208-96-8 - < 0.010 -Acenaphthene 83-32-9 - < 0.010 -Fluorene 86-73-7 - < 0.010 -Phenanthrene 85-01-8 - < 0.010 -Anthracene 120-12-7 - < 0.010 -Fluoranthene 206-44-0 - < 0.010 -Pyrene 129-00-0 - < 0.010 -Benzo[a]anthracene 56-55-3 - < 0.010 -Chrysene 218-01-9 - < 0.010 -Benzo[b]fluoranthene 205-99-2 - < 0.010 -Benzo[k]fluoranthene 207-08-9 - < 0.010 -Benzo[a]pyrene 50-32-8 - < 0.010 -Indeno[1,2,3-cd]pyrene 193-39-5 - < 0.010 -Dibenzo[a,h]anthracene 53-70-3 - < 0.010 -Benzo[g,h,i]perylene 191-24-2 - < 0.010 -Total (USEPA16) PAHs - - < 0.170 -





EXR/162915 Ver. 1


Customer and Site Details: ESG Southam : Gnossall St. Lawrence Primary School Matrix: Water

Job Number: W16_2915 Date Booked in: 05-Sep-13

Directory: D:\TES\DATA\Y2013\0909HSA_GC12\090913 2013-09-09 14-07-59\117B1701.D Date extracted: 09-Sep-13

Method: Headspace GCFID Date Analysed: 09-Sep-13, 19:31:56

y * Sample data with an asterisk are not UKAS accredi ted.

Concentration, (mg/l) AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C 6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO

* EX1420399 BH3 EW 19 0.00 <0.005 <0.005 <0.005 <0.005 <0.005 <0.1 <0.1 <0.1 <0.1 <0.1

Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.

Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions


EXR/162915 Ver. 1


Customer and Site Details: ESG Southam : Gnossall St. Lawrence Primary School Matrix: WaterJob Number: W16_2915 Separation: Silica gel Date Booked in: 05-Sep-13QC Batch Number: 130639 Eluents: Hexane, DCM Date Extracted: 06-Sep-13Directory: D:\TES\DATA\Y2013\090913TPH_GC16\090913 2013-09-09 08-18-23\087B4301.D Date Analysed: 09-Sep-13, 19:59:28Method: Bottle

Concentration, (mg/l)* This sample data is not UKAS accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40


EX1420399 BH3 EW 19 0.00 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 0.012


EXR/162915 Ver. 1


Sample ID: EX1420399ALI Job Number: W16_2915Multiplier: 0.019 Client: ESG SouthamDilution: 1 Site: Gnossall St. Lawrence Primary SchoolAcquisition Method: TPH_RUNF.M Client Sample Ref: BH3 EW 19 0.00Acquisition Date/Time: 09-Sep-13, 19:59:28Datafile: D:\TES\DATA\Y2013\090913TPH_GC16\090913 2013-09-09 08-18-23\031F4301.D

min0 2 4 6 8

pA

0

50

100

150

200

250

300

350

400

450

FID1 A, Front Signal (031F4301.D)


EXR/162915 Ver. 1


Sample ID: EX1420399ARO Job Number: W16_2915Multiplier: 0.0154 Client: ESG SouthamDilution: 1 Site: Gnossall St. Lawrence Primary SchoolAcquisition Method: TPH_RUNF.M Client Sample Ref: BH3 EW 19 0.00Acquisition Date/Time: 09-Sep-13, 19:59:28Datafile: D:\TES\DATA\Y2013\090913TPH_GC16\090913 2013-09-09 08-18-23\087B4301.D

min0 2 4 6 8

pA

0

100

200

300

400

FID2 B, Back Signal (087B4301.D)


EXR/162915 Ver. 1



MethodID

Calc_C

R3

Calc_H

D

CU

ST

SE

RV

GR

OH

SA

ICP

MS

W

ICP

WA

TV

AR


Chrom

ium (III) (C

ALC

)

Total H

ardness as CaC

O3 (C

ALC

)

Report A

GR

O-H

SA

GC

FID

(AA

)

Nickel as N

i MS

(Dissolved)

Chrom

ium as C

r MS

(Dissolved)

Cadm

ium as C

d MS

(Dissolved)

Copper as C

u MS

(Dissolved)

Lead as Pb M

S (D

issolved)

Zinc as Z

n MS

(Dissolved)

Manganese as M

n MS

(Dissolved)

Arsenic as A

s MS

(Dissolved)

Mercury as H

g MS

(Dissolved)

Selenium

as Se M

S (D

issolved)

Vanadium

as V M

S (D

issolved)

Molybdenum

as Mo M

S (D

issolved)

Antim

ony as Sb M

S (D

issolved)

Total S

ulphur as SO

4 (Diss) V

AR

Calcium

as Ca (D

issolved) VA

R

Magnesium

as Mg (D

issolved) VA

R

Barium

as Ba (D

issolved) VA

R

Sodium

as Na (D

issolved) VA

R

Iron as Fe (D

issolved) VA

R

Boron as B

(Dissolved) V

AR

Beryllium

as Be (D

issolved) VA

R

��

EX/1420399 BH3 0.00 28/08/13






ESG Southam Consignment No W58720




Gnossall St. Lawrence Primary School Date Logged 05-Sep-2013



EXR/162915 Ver. 1



MethodID

ISE

F

KO

NE

NS

PA

HM

SW

PH

EH

PLC

VL

SF

AP

I

SF

AS

TP

HF

ID-S

i

VO

CH

SA

W

WS

LM3


Fluoride as F

Chloride as C

l (Kone)

Am

moniacal N

itrogen (Kone)

Nitrate as N

(Kone calc)

Chrom

ium V

I. as Cr (K

one)

PA

H G

C-M

S (16)

Phenols by H

PLC

(Low Level)

Cyanide (F

ree) as CN

SF

A

Cyanide (T

otal) as CN

SF

A

Sulphide as S

SF

A

TP

H by G

C(S

i)

BT

EX

Analysis H

SA

GC

-MS

Benzene (µg/l)

Toluene (µg/l)

Ethyl B

enzene (µg/l)

Xylenes (µg/l)

m/p X

ylenes (µg/l)

o Xylene (µg/l)

pH units

��

EX/1420399 BH3 0.00 28/08/13










Gnossall St. Lawrence Primary School Date Logged 05-Sep-2013



EXR/162915 Ver. 1


Method Description


Water Calc_HD As Received Calculation based on Dissolved metals analysis by ICPOESWater GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons

(GRO) by Headspace FIDWater ICPMSW As Received Direct quantitative determination of Metals in water samples using

ICPMSWater ICPWATVAR As Received Direct determination of Metals and Sulphate in water samples using

ICPOESWater ISEF As Received Determination of Fluoride in water samples by Ion Selective

Electrode (ISE)Water KONENS As Received Direct analysis using discrete colorimetric analysisWater PAHMSW As Received Determination of PolyAromatic Hydrocarbons in water by pentane

extraction GCMS quantitationWater PHEHPLCVL As Received Determination of Phenols by HPLCWater SFAPI As Received Segmented flow analysis with colorimetric detectionWater SFAS As Received Determination of Sulphide by segmented flow analysis with

colorimetric detectionWater TPHFID-Si As Received Determination of speciated pentane extractable hydrocarbons in

water by GCFIDWater VOCHSAW As Received Determination of Volatile Organics Compounds by Headspace

GCMSWater WSLM3 As Received Determination of the pH of water samples by pH probe


Method Descriptions


EXR/162915 Ver. 1

Report Notes

Generic Notes

Soil/Solid Analysis








Asbestos Analysis


Symbol Reference





END OF REPORT


EXR/162915 Ver. 1


Site: Gnosall St Lawrence




On behalf ofESG : Date of Issue: 12-Nov-2013Declan Burns Operations Director


12-Nov-2013

The 2 samples described in this report were registered for analysis by ESG on 02-Nov-2013. This report supersedes any versions previously issued by the laboratory.

TEST REPORTWATER SAMPLE ANALYSIS


Table 1 Main Analysis Results (Pages 2 to 4)Table of PAH (MS-SIM) (10) Results (Pages 5 to 6)Table of GRO Results (Page 7)Table of TPH (Si) banding (0.01) (Page 8)GC-FID Chromatograms (Pages 9 to 12)Table of Subcontracted Analysis Results (Pages 13 to 18)Analytical and Deviating Sample Overview (Pages 19 to 20)Table of Method Descriptions (Page 21)Table of Report Notes (Page 22)




EXR/166207 Ver. 2

Units : pH units mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l µg/l mg/l mg/lMethod Codes : WSLM3 Calc_CR3 Calc_HD KONENS ISEF ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPMSW ICPMSW ICPMSW PAHMSW ICPMSW ICPMSW

Method Reporting Limits : 0.01 7 1 0.1 3 1 1 0.01 1 0.001 0.001 0.0001 0.001 0.001UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes

LAB

ID N

umber E

X/


Sam

ple Date

pH units w

Chrom

ium (III)

Total H

ardness as CaC

O3

Chloride as C

l w

Fluoride as F

a

Total S

ulphur as SO

4 (Dissolved) a

Calcium

as Ca (D

issolved) a

Magnesium

as Mg (D

issolved) a

Barium

as Ba (D

issolved) a

Sodium

as Na (D

issolved) a

Nickel as N

i (Dissolved)

Chrom

ium as C

r (Dissolved)

Cadm

ium as C

d (Dissolved)

PA

H G

C-M

S (16) o

Copper as C

u (Dissolved)

Lead as Pb (D

issolved)

1436683 BH3 W 31-Oct-13 7.2 <0.01 354 27 0.2 34 104 23 0.09 15 0.001 0.004 0.0004 Req 0.005 <0.001

1436684 BH4 W 31-Oct-13 7.4 <0.01 323 5 0.2 7 113 10 0.19 7 0.002 0.004 <0.0001 Req 0.006 <0.001

Contact

Date Printed


Table Number 1

Fax +44 (0) 1283 554422


Mr J Litten

12-Nov-2013

Gnosall St Lawrence



Tel +44 (0) 1283 554400



EXR/166207 Ver. 2

Units : mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/lMethod Codes : ICPMSW ICPMSW ICPWATVAR ICPMSW ICPWATVAR ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW KONENS KONENS KONENS SFAPI SFAS TPHFID-Si

Method Reporting Limits : 0.002 0.002 0.01 0.001 0.01 0.0001 0.001 0.001 0.001 0.001 0.01 0.2 0.01 0.02 0.05 0.01UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes

LAB

ID N

umber E

X/


Sam

ple Date

Zinc as Z

n (Dissolved)

Manganese as M

n (Dissolved)

Iron as Fe (D

issolved) a

Arsenic as A

s (Dissolved)

Boron as B

(Dissolved) a

Mercury as H

g (Dissolved)

Selenium

as Se (D

issolved)

Vanadium

as V (D

issolved)

Molybdenum

as Mo (D

issolved)

Antim

ony as Sb (D

issolved)

Am

moniacal N

itrogen as N

Nitrate as N

Chrom

ium V

I as Cr

Cyanide (T

otal) as CN

Sulphide as S

TP

H by G

C(S

i) o

1436683 BH3 W 31-Oct-13 0.005 <0.002 <0.01 <0.001 0.05 <0.0001 0.002 0.002 <0.001 <0.001 0.19 4.5 <0.01 <0.02 <0.05 Req

1436684 BH4 W 31-Oct-13 <0.002 <0.002 <0.01 0.001 0.05 <0.0001 <0.001 0.002 <0.001 <0.001 0.19 3.4 <0.01 <0.02 <0.05 Req

Contact

Date Printed


Table Number 1

Fax +44 (0) 1283 554422


Mr J Litten

12-Nov-2013

Gnosall St Lawrence



Tel +44 (0) 1283 554400



EXR/166207 Ver. 2

Units : ug/l mg/l µg/l mg/l µg/l µg/l µg/l µg/l µg/l µg/l mg/l mg/l mg/l mg/lMethod Codes : Sub045 ICPWATVAR Sub045 GROHSA BTEXHSA BTEXHSA BTEXHSA BTEXHSA BTEXHSA BTEXHSA PHEHPLCVL PHEHPLCVL PHEHPLCVL PHEHPLCVL

Method Reporting Limits : 5 0.01 0.1 5 5 5 15 10 5 0.0005 0.0005 0.0005 0.0005UKAS Accredited : No No No No Yes Yes Yes Yes Yes Yes No No No No

LAB

ID N

umber E

X/


Sam

ple Date

^Cyanide (F

ree) 5ug/l

Beryllium

as Be (D

issolved) a

^VO

C Low

Level

GR

O-H

SA

(AA

)

Ethyl B

enzene

Benzene

Toluene

Xylenes

m/p X

ylenes

o Xylene

Phenol

Cresols

Dim

ethylphenols

Trim

ethylphenols

1436683 BH3 W 31-Oct-13 <5 <0.01 Req Req <5 <5 <5 <15 <10 <5 <0.0005 <0.0005 <0.0005 <0.0005

1436684 BH4 W 31-Oct-13 <5 <0.01 Req Req <5 <5 <5 <15 <10 <5 <0.0005 <0.0005 <0.0005 <0.0005

Contact

Date Printed


Table Number 1

Fax +44 (0) 1283 554422


Mr J Litten

12-Nov-2013

Gnosall St Lawrence



Tel +44 (0) 1283 554400



EXR/166207 Ver. 2

1


Customer and Site Details: ESG Southam: Gnosall St LawrenceSample Details: BH3 W Job Number: W16_6207LIMS ID Number: EX1436683 Date Booked in: 02-Nov-13QC Batch Number: 130801 Date Extracted: 05-Nov-13

Quantitation File: Initial Calibration Date Analysed: 07-Nov-13Directory: 107MS17.PAH\ Matrix: WaterDilution: 1.0 Ext Method: Bottle



Naphthalene 91-20-3 - < 0.020 -Acenaphthylene 208-96-8 - < 0.010 -Acenaphthene 83-32-9 - < 0.010 -Fluorene 86-73-7 - < 0.010 -Phenanthrene 85-01-8 - < 0.010 -Anthracene 120-12-7 - < 0.010 -Fluoranthene 206-44-0 - < 0.010 -Pyrene 129-00-0 - < 0.010 -Benzo[a]anthracene 56-55-3 - < 0.010 -Chrysene 218-01-9 - < 0.010 -Benzo[b]fluoranthene 205-99-2 - < 0.010 -Benzo[k]fluoranthene 207-08-9 - < 0.010 -Benzo[a]pyrene 50-32-8 - < 0.010 -Indeno[1,2,3-cd]pyrene 193-39-5 - < 0.010 -Dibenzo[a,h]anthracene 53-70-3* - < 0.010 -Benzo[g,h,i]perylene 191-24-2 - < 0.010 -Total (USEPA16) PAHs - - < 0.170 -





EXR/166207 Ver. 2

1


Customer and Site Details: ESG Southam: Gnosall St LawrenceSample Details: BH4 W Job Number: W16_6207LIMS ID Number: EX1436684 Date Booked in: 02-Nov-13QC Batch Number: 130801 Date Extracted: 05-Nov-13

Quantitation File: Initial Calibration Date Analysed: 07-Nov-13Directory: 107MS17.PAH\ Matrix: WaterDilution: 1.0 Ext Method: Bottle



Naphthalene 91-20-3 - < 0.020 -Acenaphthylene 208-96-8 - < 0.010 -Acenaphthene 83-32-9 - < 0.010 -Fluorene 86-73-7 - < 0.010 -Phenanthrene 85-01-8 - < 0.010 -Anthracene 120-12-7 - < 0.010 -Fluoranthene 206-44-0 - < 0.010 -Pyrene 129-00-0 7.43 0.012 91Benzo[a]anthracene 56-55-3 - < 0.010 -Chrysene 218-01-9 - < 0.010 -Benzo[b]fluoranthene 205-99-2 - < 0.010 -Benzo[k]fluoranthene 207-08-9 - < 0.010 -Benzo[a]pyrene 50-32-8 - < 0.010 -Indeno[1,2,3-cd]pyrene 193-39-5 - < 0.010 -Dibenzo[a,h]anthracene 53-70-3* - < 0.010 -Benzo[g,h,i]perylene 191-24-2 - < 0.010 -Total (USEPA16) PAHs - - < 0.172 -





EXR/166207 Ver. 2


Customer and Site Details: ESG Southam : Gnosall St Lawrence Matrix: Water

Job Number: W16_6207 Date Booked in: 02-Nov-13

Directory: D:\TES\DATA\Y2013\1106HSA_GC12\110613 2013-11-06 16-46-52\110B1001.D Date extracted: 06-Nov-13

Method: Headspace GCFID Date Analysed: 06-Nov-13, 19:54:44

y * Sample data with an asterisk are not UKAS accredi ted.

Concentration, (mg/l) AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C 6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO

* EX1436683 BH3 W <0.005 <0.005 <0.005 <0.005 <0.005 <0.1 <0.1 <0.1 <0.1 <0.1

* EX1436684 BH4 W <0.005 <0.005 <0.005 <0.005 <0.005 <0.1 <0.1 <0.1 <0.1 <0.1

Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions


EXR/166207 Ver. 2


Customer and Site Details: ESG Southam : Gnosall St Lawrence Matrix: WaterJob Number: W16_6207 Separation: Silica gel Date Booked in: 02-Nov-13QC Batch Number: 130801 Eluents: Hexane, DCM Date Extracted: 05-Nov-13Directory: D:\TES\DATA\Y2013\110613TPH_GC16\110613 2013-11-06 11-00-05\081B3701.D Date Analysed: 06-Nov-13, 21:08:13Method: Bottle

Concentration, (mg/l)* This sample data is not UKAS accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40


EX1436683 BH3 W <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01

EX1436684 BH4 W <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01


EXR/166207 Ver. 2


Sample ID: EX1436683ALI Job Number: W16_6207Multiplier: 0.0188 Client: ESG SouthamDilution: 1 Site: Gnosall St LawrenceAcquisition Method: TPH_RUNF.M Client Sample Ref: BH3 WAcquisition Date/Time: 06-Nov-13, 20:51:41Datafile: D:\TES\DATA\Y2013\110613TPH_GC16\110613 2013-11-06 11-00-05\030F3601.D

min0 2 4 6 8

pA

0

50

100

150

200

250

300

350

400

450



EXR/166207 Ver. 2


Sample ID: EX1436683ARO Job Number: W16_6207Multiplier: 0.0144 Client: ESG SouthamDilution: 1 Site: Gnosall St LawrenceAcquisition Method: TPH_RUNF.M Client Sample Ref: BH3 WAcquisition Date/Time: 06-Nov-13, 20:51:41Datafile: D:\TES\DATA\Y2013\110613TPH_GC16\110613 2013-11-06 11-00-05\080B3601.D

min0 2 4 6 8

pA

0

100

200

300

400



EXR/166207 Ver. 2


Sample ID: EX1436684ALI Job Number: W16_6207Multiplier: 0.0188 Client: ESG SouthamDilution: 1 Site: Gnosall St LawrenceAcquisition Method: TPH_RUNF.M Client Sample Ref: BH4 WAcquisition Date/Time: 06-Nov-13, 21:08:13Datafile: D:\TES\DATA\Y2013\110613TPH_GC16\110613 2013-11-06 11-00-05\031F3701.D

min0 2 4 6 8

pA

0

50

100

150

200

250

300

350

400

450



EXR/166207 Ver. 2


Sample ID: EX1436684ARO Job Number: W16_6207Multiplier: 0.0142 Client: ESG SouthamDilution: 1 Site: Gnosall St LawrenceAcquisition Method: TPH_RUNF.M Client Sample Ref: BH4 WAcquisition Date/Time: 06-Nov-13, 21:08:13Datafile: D:\TES\DATA\Y2013\110613TPH_GC16\110613 2013-11-06 11-00-05\081B3701.D

min0 2 4 6 8

pA

0

100

200

300

400



EXR/166207 Ver. 2

Report ID - 20058864 - 1

Analytical Report

0754

Final Report


08-Nov-2013



Dear Louise


Samples Registered on: 06-Nov-2013

Analysis Started on: 07-Nov-2013

Analysis Completed on: 08-Nov-2013





Yours sincerely










NLS Starcross

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Page 1 of 6


Report ID - 20058864 - 1

Analytical Report

0754

Final Report


08-Nov-2013


1


Folder No: 002632748 Sampled on: 31-Oct-13 @ (Time not supplied)

Comments: W1436683 - BH3




1,1,1,2-Tetrachloroethane SX<0.1 ug/l 1296UKAS0.1DBDC

1,1,1-Trichloroethane SX<0.1 ug/l 1296UKAS0.1DBDC



1,1-Dichloroethane SX<0.1 ug/l 1296UKAS0.1DBDC

1,1-Dichloroethylene :- {1,1-Dichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC

1,1-Dichloropropylene :- {1,1-Dichloropropene} SX<0.1 ug/l 1296UKAS0.1DBDC

1,2,3-Trichlorobenzene SX<0.5 ug/l 1296None0.5DBDC

1,2,3-Trichloropropane SX<0.5 ug/l 1296UKAS0.5DBDC

1,2,3-Trimethylbenzene SX<0.1 ug/l 1296UKAS0.1DBDC



1,2-Dibromo-3-chloropropane SX<0.1 ug/l 1296UKAS0.1DBDC

1,2-Dibromoethane SX<0.1 ug/l 1296UKAS0.1DBDC

1,2-Dichlorobenzene SX<0.1 ug/l 1296UKAS0.1DBDC


1,2-Dichloropropane SX<0.1 ug/l 1296UKAS0.1DBDC

1,2-Dimethylbenzene :- {o-Xylene} SX<0.1 ug/l 1296UKAS0.1DBDC


1,3,5-Trimethylbenzene :- {Mesitylene} SX<0.1 ug/l 1296UKAS0.1DBDC





2-Chlorotoluene :- {1-Chloro-2-methylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC



4-Isopropyltoluene :- {4-methyl-Isopropylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC

Benzene SX<0.1 ug/l 1296UKAS0.1DBDC

Bromobenzene SX<0.1 ug/l 1296UKAS0.1DBDC

Bromochloromethane SX<0.1 ug/l 1296UKAS0.1DBDC

Bromodichloromethane SX<0.1 ug/l 1296UKAS0.1DBDC

Bromoform :- {Tribromomethane} SX<0.1 ug/l 1296UKAS0.1DBDC

Carbon Disulphide SX<0.1 ug/l 1296None0.1DBDC

Carbon tetrachloride :- {Tetrachloromethane} SX<0.1 ug/l 1296UKAS0.1DBDC

Chlorobenzene SX<0.1 ug/l 1296UKAS0.1DBDC

Chlorodibromomethane SX<0.1 ug/l 1296UKAS0.1DBDC

Chloroform :- {Trichloromethane} SX0.152 ug/l 1296UKAS0.1DBDC

Chloromethane :- {Methyl Chloride} SX<0.5 ug/l 1296None0.5DBDC

cis-1,2-Dichloroethylene :- {cis-1,2-Dichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC

cis-1,3-Dichloropropylene :- {cis-1,3-Dichloropropene} SX<0.1 ug/l 1296UKAS0.1DBDC

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Page 2 of 6

Report ID - 20058864 - 1

Analytical Report

0754

Final Report


08-Nov-2013

Dibromomethane SX<0.1 ug/l 1296UKAS0.1DBDC

Dichloromethane :- {Methylene Dichloride} SX<0.5 ug/l 1296UKAS0.5DBDC

Dimethylbenzene : Sum of isomers (1,3- 1,4-) : {m+p xylene} SX<0.2 ug/l 1296UKAS0.2DBDC

Ethyl tert-butyl ether :- {ETBE} SX<0.1 ug/l 1296UKAS0.1DBDC

Ethylbenzene SX<0.1 ug/l 1296UKAS0.1DBDC

Hexachlorobutadiene SX<0.5 ug/l 1296None0.5DBDC

Hexachloroethane SX<0.5 ug/l 1296None0.5DBDC

Isopropylbenzene SX<0.1 ug/l 1296UKAS0.1DBDC

MTBE :- {Methyl tert-butyl ether} SX<0.1 ug/l 1296UKAS0.1DBDC

Naphthalene SX<0.5 ug/l 1296None0.5DBDC

n-ButylBenzene :- {1-Phenylbutane} SX<0.1 ug/l 1296UKAS0.1DBDC

n-Propylbenzene :- {1-phenylpropane} SX<0.1 ug/l 1296UKAS0.1DBDC

sec-Butylbenzene :- {1-Methylpropylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC

Styrene :- {Vinylbenzene} SX<0.5 ug/l 1296UKAS0.5DBDC

tert-Amyl methyl ether :- {TAME} SX<0.1 ug/l 1296UKAS0.1DBDC

tert-Butylbenzene :- {(1,1-Dimethylethyl)benzene} SX<0.1 ug/l 1296UKAS0.1DBDC

Tetrachloroethylene :- {Perchloroethylene} SX<0.1 ug/l 1296UKAS0.1DBDC

Toluene :- {Methylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC

trans-1,2-Dichloroethylene :- {trans-1,2-Dichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC

trans-1,3-Dichloropropylene :- {trans-1,3-Dichloropropene} SX<0.5 ug/l 1296UKAS0.5DBDC

Trichloroethylene :- {Trichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC

Trichlorofluoromethane SX<0.1 ug/l 1296UKAS0.1DBDC

Vinyl Chloride :- {Chloroethylene} SX<0.1 ug/l 1296UKAS0.1DBDC

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Page 3 of 6

Report ID - 20058864 - 1

Analytical Report

0754

Final Report


08-Nov-2013


1


Folder No: 002632749 Sampled on: 31-Oct-13 @ (Time not supplied)

Comments: W1436684 - BH4









1,1-Dichloroethylene :- {1,1-Dichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC

1,1-Dichloropropylene :- {1,1-Dichloropropene} SX<0.1 ug/l 1296UKAS0.1DBDC


1,2,3-Trichloropropane SX<0.5 ug/l 1296UKAS0.5DBDC




1,2-Dibromo-3-chloropropane SX<0.1 ug/l 1296UKAS0.1DBDC

1,2-Dibromoethane SX<0.1 ug/l 1296UKAS0.1DBDC




1,2-Dimethylbenzene :- {o-Xylene} SX<0.1 ug/l 1296UKAS0.1DBDC


1,3,5-Trimethylbenzene :- {Mesitylene} SX<0.1 ug/l 1296UKAS0.1DBDC








4-Isopropyltoluene :- {4-methyl-Isopropylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC

Benzene SX<0.1 ug/l 1296UKAS0.1DBDC

Bromobenzene SX<0.1 ug/l 1296UKAS0.1DBDC

Bromochloromethane SX<0.1 ug/l 1296UKAS0.1DBDC

Bromodichloromethane SX<0.1 ug/l 1296UKAS0.1DBDC

Bromoform :- {Tribromomethane} SX<0.1 ug/l 1296UKAS0.1DBDC

Carbon Disulphide SX<0.1 ug/l 1296None0.1DBDC

Carbon tetrachloride :- {Tetrachloromethane} SX<0.1 ug/l 1296UKAS0.1DBDC

Chlorobenzene SX<0.1 ug/l 1296UKAS0.1DBDC

Chlorodibromomethane SX<0.1 ug/l 1296UKAS0.1DBDC

Chloroform :- {Trichloromethane} SX<0.1 ug/l 1296UKAS0.1DBDC

Chloromethane :- {Methyl Chloride} SX<0.5 ug/l 1296None0.5DBDC

cis-1,2-Dichloroethylene :- {cis-1,2-Dichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC

cis-1,3-Dichloropropylene :- {cis-1,3-Dichloropropene} SX<0.1 ug/l 1296UKAS0.1DBDC

NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 4 of 6

Report ID - 20058864 - 1

Analytical Report

0754

Final Report


08-Nov-2013

Dibromomethane SX<0.1 ug/l 1296UKAS0.1DBDC

Dichloromethane :- {Methylene Dichloride} SX<0.5 ug/l 1296UKAS0.5DBDC

Dimethylbenzene : Sum of isomers (1,3- 1,4-) : {m+p xylene} SX<0.2 ug/l 1296UKAS0.2DBDC

Ethyl tert-butyl ether :- {ETBE} SX<0.1 ug/l 1296UKAS0.1DBDC

Ethylbenzene SX<0.1 ug/l 1296UKAS0.1DBDC

Hexachlorobutadiene SX<0.5 ug/l 1296None0.5DBDC

Hexachloroethane SX<0.5 ug/l 1296None0.5DBDC

Isopropylbenzene SX<0.1 ug/l 1296UKAS0.1DBDC

MTBE :- {Methyl tert-butyl ether} SX<0.1 ug/l 1296UKAS0.1DBDC

Naphthalene SX<0.5 ug/l 1296None0.5DBDC

n-ButylBenzene :- {1-Phenylbutane} SX<0.1 ug/l 1296UKAS0.1DBDC

n-Propylbenzene :- {1-phenylpropane} SX<0.1 ug/l 1296UKAS0.1DBDC

sec-Butylbenzene :- {1-Methylpropylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC

Styrene :- {Vinylbenzene} SX<0.5 ug/l 1296UKAS0.5DBDC

tert-Amyl methyl ether :- {TAME} SX<0.1 ug/l 1296UKAS0.1DBDC

tert-Butylbenzene :- {(1,1-Dimethylethyl)benzene} SX<0.1 ug/l 1296UKAS0.1DBDC

Tetrachloroethylene :- {Perchloroethylene} SX<0.1 ug/l 1296UKAS0.1DBDC

Toluene :- {Methylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC

trans-1,2-Dichloroethylene :- {trans-1,2-Dichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC

trans-1,3-Dichloropropylene :- {trans-1,3-Dichloropropene} SX<0.5 ug/l 1296UKAS0.5DBDC

Trichloroethylene :- {Trichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC

Trichlorofluoromethane SX<0.1 ug/l 1296UKAS0.1DBDC

Vinyl Chloride :- {Chloroethylene} SX<0.1 ug/l 1296UKAS0.1DBDC

NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 5 of 6

Report ID - 20058864 - 1

Analytical Report

0754

Final Report


08-Nov-2013

Method Description Summary for all samples in batch Number 20058864 183 SX I Cyanide - (free) - determined colorimetrically by CF analyser

1296 SX O Volatiles - direct aqueous injected; determined by P and T GCMS


Simon Padley





sample was used.

Key to Results Flags:

Samples received outside analysis holding times. It is possible that the results may be compromised.DB

Analysis started outside of specified holding time. It is possible that the results may be compromised.DC

The analysis start date specified is the date of the first test, dates for other analysis are available on request.







END OF TEST REPORT

NLS Starcross

Staplake Mount

Starcross

Exeter

EX6 8FD

NLS Nottingham

Meadow Lane

Nottingham

NG2 3HN

NLS Leeds

Olympia House

Gelderd Lane

Gelderd Road

Leeds LS12 6DD

Page 6 of 6



MethodID

BT

EX

HS

A

Calc_C

R3

Calc_H

D

CU

ST

SE

RV

GR

OH

SA

ICP

MS

W

ICP

WA

TV

AR


BT

EX

-HS

A A

nalysis

Chrom

ium (III) (C

ALC

)

Total H

ardness as CaC

O3 (C

ALC

)

Report A

GR

O-H

SA

GC

FID

(AA

)

Nickel as N

i MS

(Dissolved)

Chrom

ium as C

r MS

(Dissolved)

Cadm

ium as C

d MS

(Dissolved)

Copper as C

u MS

(Dissolved)

Lead as Pb M

S (D

issolved)

Zinc as Z

n MS

(Dissolved)

Manganese as M

n MS

(Dissolved)

Arsenic as A

s MS

(Dissolved)

Mercury as H

g MS

(Dissolved)

Selenium

as Se M

S (D

issolved)

Vanadium

as V M

S (D

issolved)

Molybdenum

as Mo M

S (D

issolved)

Antim

ony as Sb M

S (D

issolved)

Total S

ulphur as SO

4 (Diss) V

AR

Calcium

as Ca (D

issolved) VA

R

Magnesium

as Mg (D

issolved) VA

R

Barium

as Ba (D

issolved) VA

R

Sodium

as Na (D

issolved) VA

R

Iron as Fe (D

issolved) VA

R

Boron as B

(Dissolved) V

AR

��

EX/1436683 BH3 31/10/13EX/1436684 BH4 31/10/13










Gnosall St Lawrence Date Logged 02-Nov-2013

Report Due 08-Nov-2013


EXR/166207 Ver. 2



MethodID

ICP

WA

TV

AR

ISE

F

KO

NE

NS

PA

HM

SW

PH

EH

PLC

VL

SF

AP

I

SF

AS

Sub045

TP

HF

ID-S

i

WS

LM3


Beryllium

as Be (D

issolved) VA

R

Fluoride as F

Chloride as C

l (Kone)

Am

moniacal N

itrogen (Kone)

Nitrate as N

(Kone calc)

Chrom

ium V

I. as Cr (K

one)

PA

H G

C-M

S (16)

Phenols by H

PLC

(Low Level)

Cyanide (T

otal) as CN

SF

A

Sulphide as S

SF

A

^Cyanide (F

ree) 5ug/l

^VO

C Low

Level

TP

H by G

C(S

i)

pH units

��

EX/1436683 BH3 31/10/13EX/1436684 BH4 31/10/13










Gnosall St Lawrence Date Logged 02-Nov-2013

Report Due 08-Nov-2013


EXR/166207 Ver. 2


Method Description

Water BTEXHSA As Received Benzene, Toluene, Ethylbenzene, & Xylenes by headspace extraction GCFID quantitation


Water Calc_HD As Received Calculation based on Dissolved metals analysis by ICPOESWater GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons

(GRO) by Headspace FIDWater ICPMSW As Received Direct quantitative determination of Metals in water samples using

ICPMSWater ICPWATVAR As Received Direct determination of Metals and Sulphate in water samples using

ICPOESWater ISEF As Received Determination of Fluoride in water samples by Ion Selective

Electrode (ISE)Water KONENS As Received Direct analysis using discrete colorimetric analysisWater PAHMSW As Received Determination of PolyAromatic Hydrocarbons in water by pentane

extraction GCMS quantitationWater PHEHPLCVL As Received Determination of Phenols by HPLCWater SFAPI As Received Segmented flow analysis with colorimetric detectionWater SFAS As Received Determination of Sulphide by segmented flow analysis with


contractor.Water TPHFID-Si As Received Determination of speciated pentane extractable hydrocarbons in

water by GCFIDWater WSLM3 As Received Determination of the pH of water samples by pH probe


Method Descriptions


EXR/166207 Ver. 2

Report Notes

Generic Notes

Soil/Solid Analysis








Asbestos Analysis


Symbol Reference





END OF REPORT


EXR/166207 Ver. 2

November 2013 Report No D3110-13 Issue 2.0 Enclosure E

ENCLOSURE E

DRAWINGS

Site Location Plan 1

Site Plan 2

Documents

Report No D3110-13 - apps2.staffordshire.gov.uk