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Pg1}{\bkmkend Pg1}\par\pard\li519\sb87\sl-184\slmult0\fi0\tx4509 \up0 \expndtw-7\charscalex96 \ul0\nosupersub\cf1\f2\fs16 09.11.2013\tab \up0 \expndtw-7\charscalex96 /usr/hosting _files4/main/previews/doc397403118/preview\par\pard\ql \li3004\sb0\sl-218\slmult0 \par\pard\ql\li3004\sb0\sl-218\slmult0 \par\pard\ql\li3004\sb0\sl-218\slmult0 \par\pard\ql\li3004\sb0\sl-218\slmult0 \par\pard\ql\li3004\sb0\sl-218\slmult0 \par\pard\ql\li3004\sb0\sl-218\slmult0 \par\pard\ql\li3004\sb0\sl-218\slmult0 \par\pard\ql\li3004\sb23\sl-218\slmult0 \up0 \expndtw0\charscalex100 \ul0\nosupersub\cf2\f3\fs19 I. SUBSTAN\u354?E MEDICAMENTOASE DIN GRUPA AMINELOR \u350?I A \par\pard\ql \li4456\sb3\sl-218\slmult0 \up0 \expndtw0\charscalex100 DERIVA\u354?ILOR FUNC\u354?IONALI \par\pard\ql \li1681\ri2379\sb239\sl-246\slmult0\fi651 \up0 \expndtw-4\charscalex100 Gruparea aminic\u259? este foarte des ntlnit\u259? n structura substan\u355?elor medicamentoase sub \up0 \expndtw-4\charscalex100 form\u259? de amin\u259? primar\u259?, secundar\u259? sau ter\u355?iar\u259?. n general, pe lng\u259? gruparea aminic\u259?, n structura \line \up0 \expndtw-5\charscalex100 acestor substan\u355?e mai pot apare \u351?i alte grup\u259?ri func\u355?ionale (hidroxil, carboxil, ester etc.) avnd \up0 \expndtw-6\charscalex100 posibilitatea de a se influen\u355?a reciproc. \par\pard\qj \li1681\ri2544\sb0\sl-260\slmult0\fi651 \up0 \expndtw-4\charscalex100 n clasificarea acestor substan\u355?e medicamentoase s-a \u355?inut seama de natura aminei precum \u351?i \up0 \expndtw-4\charscalex100 de prezen\u355?a n molecul\u259? a altor grup\u259?ri func\u355?ionale. \par\pard\li1681\sb54\sl-218\slmult0\fi651\tx3234 \up0 \expndtw-6\charscalex100 n tabelele\tab \up0 \expndtw-5\charscalex100 1-3 sunt prezenta\u355?i unii dintre cei mai importan\u355?i reprezentan\u355?i ai acestei clase\par\pard\li1681\sb1\sl-209\slmult0\fi0 \up0 \expndtw-6\charscalex100 al\u259?turi de unele propriet\u259?\u355?i \u351?i constante fizico-chimice.\par\pard\qj \li1681\ri3037\sb22\sl-260\slmult0\fi651 \up0 \expndtw-7\charscalex97 Amino-acizii, sulfamidele, alcaloizii, deriva\u355?ii unor heterocicli (fenotiazine, purine, \up0 \expndtw-7\charscalex97 pirazolone), datorit\u259? comportamentului lor specific, sunt studia\u355?i n grupe separate. \par\pard\ql \li2333\sb0\sl-218\slmult0 \par\pard\ql\li2333\sb37\sl-218\slmult0 \up0 \expndtw0\charscalex103 I. Reac\u355?ii generale \par\pard\ql \li2333\sb1\sl-196\slmult0 \up0 \expndtw0\charscalex103 I.1. Reac\u355?ia de deplasare a aminei din s\u259?ruri \par\pard\ql \li2333\sb1\sl-176\slmult0 \up0 \expndtw-5\charscalex100 Din solu\u355?iile concentrate ale s\u259?rurilor, amina se poate pune n libertate prin alcalinizare cu \par\pard\ql \li1681\sb170\sl-218\slmult0 \up0 \expndtw-4\charscalex100 hidroxid de sodiu: \par\pard\li4356\sb0\sl-218\slmult0\par\pard\li4356\sb136\sl-218\slmult0\fi0\tx6550 \dn3 \expndtw0\charscalex102 R''\tab \up0 \expndtw0\charscalex102 R''\par\pard\li4386\sb1\sl-196\slmult0\fi1162 \up0 \expndtw0\charscalex101 NaOH\par\pard\li4386\sb0\sl-171\slmult0\fi0\tx5088\tx6490\tx7312\tx7973 \up0 \expndtw0\charscalex101 R NH\tab \up0 \expndtw0\charscalex101 Cl\tab \up0 \expndtw0\charscalex101 R N\tab \dn3 \expndtw0\charscalex101 NaCl\tab \dn3 \expndtw0\charscalex101 H\ul0\sub\cf4\f5\fs21 2\ul0\nosupersub\cf2\f3\fs19 O\par\pard\li4386\sb97\sl-218\slmult0\fi90\tx6670 \up2 \expndtw0\charscalex101 R'\tab \dn3 \expndtw0\charscalex101 R'\par\pard\ql \li2333\sb0\sl-218\slmult0 \par\pard\ql\li2333\sb193\sl-218\slmult0 \up0 \expndtw-4\charscalex100 - 0.2 g sare a unei amine se dizolv\u259? ntr-un ml ap\u259?, se adaug\u259? solu\u355?ie de Na OH 100g/l pn\u259? \par\pard\qj \li1681\ri2444\sb0\sl-240\slmult0 \up0 \expndtw-5\charscalex100 la pH bazic. Apare o tulbureal\u259? care n timp se transform\u259? fie n pic\u259?turi uleioase, fie ntr-un \up0 \expndtw-6\charscalex100 precipitat amorf de amin\u259? baz\u259?. \par\pard\ql \li2333\sb0\sl-218\slmult0 \par\pard\ql\li2333\sb65\sl-218\slmult0 \up0 \expndtw0\charscalex102 I.2. Reac\u355?ia de identificare a anionului \par\pard\ql \li2333\sb1\sl-196\slmult0 \up0 \expndtw-6\charscalex100 n general s\u259?rurile sunt sub form\u259? de clorhidra\u355?i, iar reac\u355?ia de identificare a anionului \par\pard\qj \li1681\ri2113\sb35\sl-280\slmult0 \up0 \expndtw-5\charscalex100 clorur\u259? se bazeaz\u259? pe precipitarea, sub form\u259? de clorur\u259? de argint, cu nitrat de argint n prezen\u355?a \up0 \expndtw-8\charscalex100 acidului nitric: \par\pard\li4136\sb139\sl-218\slmult0\fi0\tx4867\tx5448\tx6520\tx7061\tx7752 \up0 \expndtw-6\charscalex100 Cl\tab \up0 \expndtw-6\charscalex100 AgNO\tab \dn2 \expndtw-4\charscalex100 \ul0\nosupersub\cf4\f5\fs14 3\tab \dn3 \expndtw-6\charscalex100 \ul0\nosupersub\cf2\f3\fs19 AgCl\tab \dn3 \expndtw-6\charscalex100 + NO\tab \dn2 \expndtw-4\charscalex100 \ul0\nosupersub\cf4\f5\fs14 3\par\pard\ql \li2333\sb116\sl-218\slmult0 \up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf2\f3\fs19 - 2 ml solu\u355?ie apoas\u259? de clorhidrat de amin\u259? se aciduleaz\u259? cu acid nitric 100g/l \u351?i se adaug\u259? \par\pard\qj \li1681\ri2466\sb31\sl-280\slmult0 \up0 \expndtw-7\charscalex100 0.15 ml nitrat de argint 20g/l (R); se formeaz\u259? un precipitat alb, cazeos de clorur\u259? de argint, \up0 \expndtw-8\charscalex100 insolubil n ap\u259? \u351?i acid azotic, solubil n amoniac. \par\pard\ql \li2333\sb172\sl-218\slmult0 \up0 \expndtw0\charscalex100 I.3. Reac\u355?ii de eviden\u355?iere a nucleului benzenic \par\pard\ql \li2984\sb23\sl-218\slmult0 \up0 \expndtw0\charscalex104 I.3.1. Reac\u355?ia de bromurare \par\pard\li1681\sb74\sl-218\slmult0\fi651\tx2493 \up0 \expndtw-7\charscalex100 -\tab \up0 \expndtw-6\charscalex100 0.02 g substan\u355?\u259? (ex: acetanilid\u259?, fenacetin\u259?, tolazolin\u259?) se trateaz\u259? cu 2 ml ap\u259?, se\par\pard\li1681\sb23\sl-218\slmult0\fi0\tx4697 \up0 \expndtw-7\charscalex100 nc\u259?lze\u351?te; solu\u355?iei r\u259?cite i se adaug\u259?\tab \up0 \expndtw-6\charscalex100 5 pic\u259?turi ap\u259? de brom (R). Se formeaz\u259? un precipitat alb\par\pard\li1681\sb73\sl-218\slmult0\fi0 \up0 \expndtw-7\charscalex100 cristalin de derivat bromurat:\par\pard\li3154\sb34\sl-218\slmult0\fi0\tx4076\tx5588\tx6510\tx7091\tx8013\tx8824\tx9746 \up2 \expndtw-3\charscalex100 NHCOCH\tab \up0 \expndtw-2\charscalex100 \ul0\nosupersub\cf4\f5\fs14 3\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs19 NHCOCH\tab \dn2 \expndtw-2\charscalex100 \ul0\nosupersub\cf4\f5\fs14 3\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs19 NHCOCH\tab \dn2 \expndtw-2\charscalex100 \ul0\nosupersub\cf4\f5\fs14 3\tab \up0 \expndtw-3\charscalex100 \ul0\nosupersub\cf2\f3\fs19 NHCOCH\tab \dn2 \expndtw-2\charscalex100 \ul0\nosupersub\cf4\f5\fs14 3\par\pard\li4166\sb0\sl-218\slmult0\par\pard\li4166\sb106\sl-218\slmult0\fi0\tx6290\tx8123\tx9516 \up0 \expndtw-4\charscalex100 \ul0\nosupersub\cf2\f3\fs19 Br\ul0\sub\cf4\f5\fs21 2\tab \dn3 \expndtw-5\charscalex100 \ul0\nosupersub\cf2\f3\fs19 Br\tab \up0 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