QUARTERLY GROUND-WATER MONITORING REPORT FIFTH …

6130 Wilcox Road

Dublin, Ohio 43017

(614) 793-8777

fa* (614)793-9070

Hull & Associates, Inc.

September 8, 1995

SDMS DOCID 583248

Mr. Roger Duwart New Hampshire Superfiind Section Waste Management Division U.S. Environmental Protection Agency, Region 1 John F. Kennedy Building, HSN-CAN5 Boston, MA 02203

Re:

jrZEE&s, BREAiT^ OTHER; 1 *

Dear Mr. Duwart:

' ™££~ iJssrr

£|S=?=S3==S£

' Inb»'L3HPreSrfiMS aVefage' maximum minimum extraction rates for the wells Due to

8 gnm)- EXH ®J®xtra^n we,Is dunn* ^ quarter were as follows: EX-1 (97 gpm/+

< "gpi,/. 2 sz&i gr^.'ST"6 <54gp"'-2 »->• «•'

* • " 9 5 - — -

Toledo, OH

Moson, OH

Bedford, NH

Austin, TX

Solon, OH

o

Mr. Roger Duwart September 8, 1995 Page 2

Data presented on Table 4 were used to construct preliminary piezometric surface contour maps

for the lower, middle and upper portions of the overburden aquifer.1 A bedrock aquifer contour

map was not constructed due to insufficient data control.2

The contour maps indicate that the entire plume is being captured by the ground-water extraction system, with a possible exception being the downgradient edge of the plume at the Contoocook

. River. In general, heads during April 25, 1995 were up to two feet lower than seen approximately one year earlier (April 17, 1994). Exceptions to this trend were extraction wells EX-1, EX-4 and EX-5A, which exhibited higher water levels due to reduced flow rates. Water levels at several wells in and near the wetlands were also higher than seen approximately one year earlier due to the substantially increased volume of water discharged to the wetlands (as of November 1994).

Water samples were collected on April 9 through 12 from selected monitoring wells and extraction wells, per performance monitoring schedules and methodologies described in the Draft FEMP, Volume I (HAI Document # NHBA6D.622). Analytical results for samples collected from the monitoring wells are summarized on Table 5. Documentation for the sampling event is included in Attachment A.

Figures 1 through 18 show concentrations over time for wells sampled during the fifth quarter.3 Of the twenty wells sampled in April 1995, fifty-five percent have exhibited reductions in tetrachloroethene (PERC) concentrations, forty-five percent have shown reductions in 1,1,1-trichloroethane (1,1,1-TCA) concentrations, and forty-five percent have shown reductions'in trichloroethene (TCE) concentrations since pumping began.4 Parameter increases have been observed in twenty-five percent of the wells for PERC (twenty percent were unchanged), forty percent of the wells for 1,1,1-TCA (fifteen percent were unchanged), and twenty-five percent of the wells for TCE (thirty percent were unchanged).

1 The preliminary piezometric surface maps will be finalized and submitted with maps from subsequent quarters in the second annual monitoring report.

Specifically, water level data for GZ-4R could not be used as a control point because the well had not fully recovered following dewatering associated with sampling and installation of a packer for the casing integrity test.

Graphs were not prepared for GZ-3R and GZ-12R as they have not yielded parameters above Cleanup Levels since sampling was initiated in March 1987.

For each well, comparisons were made between VOC concentrations during the most recent sampling event prior to March 12, (pre-pumping) and VOCs detected during the April 1995 sampling event.

Mr. Roger Duwart September 8, 1995 , Page 3

Half of the monitoring wells sampled during the fifth quarter had concentrations below Cleanup Levels for all parameters. These wells included: EM-2, EMH-2U, EM-3L EM-3U GZ-3R GZ-12R, GZ-101L, GZ-105M, GZ-105U and MW-9M.

Ground-water extraction wells have been sampled thirteen times over the course of five quarters. Analytical data for these sampling events are summarized on Table 6 and plotted over time on Figures 19 (EX-1), 20 (EXH-3), 21 (EX-4), 22 (EX-5A), 23 (EX-6), 24 (EX-7), and 25 (EX-9). Documentation for sampling is included in Attachment A.

With the exception of increases of 1,1,1-TCA concentrations at EX-6 and EX-9 (and slight increases in PERC and TCE concentrations at EX-9), the extraction wells showed a continued trend contaminant reduction. VOC concentrations at EX-6 and EX-7 were below Cleanup Levels during the April 1995 sampling event. The only parameters which exceeded Cleanup Levels at EX-4 and EX-5A were PERC (at eleven jig/f) and TCE (at nine ng/f), respectively. .

No adjustments were made to the ground-water treatment plant (GWTP) during the fifth quarter of operations. The GWTP remained in operation when one or more of the extraction wells were pumping (no breakthrough events occurred).

A GWTP performance monitoring event was performed on March 14, 1995. The data from this event are included in the fourth quarter ground-water monitoring report. The GWTP performance monitoring frequency has been reduced to quarterly since this March 1995 event in accordance with the Draft FEMP Volume I. A June 1995 performance sampling event was scheduled; however, the GWTP was not operational due to a programmable logic controller failure. This failure has been repaired and the GWTP is now operational. Therefore, the quarterly GWTP performance sampling has been rescheduled for July 1995. -

Surface water discharge samples were collected on a monthly basis during the fifth quarter. Results of the sampling are presented on Table 7 and laboratory reports and chain-of-custody documents are included in Attachment B. The analytical data indicate that requirements for discharged total VOC concentrations (< 100 /tg/f) have not been exceeded.

Mr. Roger Duwart September 8, 1995 Page 4

Please contact either of the undersigned if you have questions about this letter report.

W. Lance Turley, P.G.

CAK/WLT/jm

cc: Patricia Carrier (NHBB) Chris Rawnsley (NHBB) Dave Schafer (TRC) Thomas A. Andrews (NHDES) Dave Richards (rfAI) Michael Carter (Piper & Marbury)

Enclosures

Sincerely

New Hampshire Ball Bearings, Inc. South Municipal Water Supply Well Superfund Site

Table 1

Summary of Ground-water Extraction Well Shut-downs During the Fifth Quarter of Operations

DATE OF SHUT-DOWN

3/25/95

APPROXIMATE HOURS

SHUT-DOWN

0300 - 0715

WELLS SHUT-DOWN

EXH-3, EX-4 EX-5A, EX-7

REASON FOR SHUT-DbWN

Not Known

4/3/95

5/2/95 - 5/5/95

5/17/95

0700 - 0900 All Wells

1600 - 1500 All Wells

0500 - 0730 EX-5A, EX-7

Clean EX-6's Flow Meter

GZ-4R Investigation

Communications Failure

5/18/95

5/19/95

0300 - 0700 EX-5A, EX-7

0200 - 0730 EX-5A, EX-7



6/8/95

6/12/95

0400 - 0730 EX-5A

0300 - 0730 EX-5A



HULL & ASSOCIATES, INC. DUBLIN. OHIO

SEPTEMBER 1995 NHB019D.017


Table 2

Summary of Ground-water Extraction Well Operations During the Fifth Quarter of Pumping

EXTRACTION WELL

EX-1

EXH-3

EX-4

EX-5A

EX-6

EX-7

EX-9

APPROXIMATE CUMULATIVE

HOURS OF PUMPING

2111

2107

2107

2087

2107

2095

2111

APPROXIMATE CUMULATIVE

HOURS OF SHUT-DOWN

73

77

77

97

77

89

73

PERCENT OPERATIONAL

96.7

96.4 .

96.4

95.5

96A

95^9

96.7

HULL & ASSOCIATES. INC. DUBLIN. OHIO

SEPTEMBER 1995 NHB019D.017


Table 3

Summary of Extraction Well Flow Rates Measured During the Fifth Quarter of Operation

EXTRACTION WELL

MAXIMUM FLOW RATE (gpm)

AND DATE

MINIMUM

FLOW RATE (gpm)

ANDDATE1

AVERAGE

FLOW RATE

(gpm)2

EX-1

EXH-3

EX-4

109 3/15/95

79 5/14/95

182 6/10/95

88 4/26/95

66 4/25/95

164 5/4/95

97

72

171

EX-5A 64 3/24/95

47 6/11/95

54

EX-6

EX-7 103 6/12/95

94 3/17/95

97

EX-9 33 3/16/95

29 6/12/95

31

NOTES: 1 Minimum flow rates were taken from dates that pumps were in operation for twenty-four hours.

2 Averages were taken from dates that wells performed for twenty-four hours.

3 Due to repeated malfunctions of EX-6's flow meter, flow rate maximums, minimums and averages could not be identified.

HULL St ASSOCIATES. INC. SEPTEMBER 1995 DUBLIN. OHIO NHB019D.017

New Hampshire Ball Bearings. Inc. South Municipal Water Supply Well Superfund Site

Table 4

Summary of Water Level Measurements Collected on April 25,1995

OBSERVATION LOCATION! NORTHING EASTING:

CASINO ELEV.

(NGV OATUMV

RISER ELEV.

(NOV DATUM!-

MEAS. REFER POINT {TYPE *C* « TOC, •RR ~ RISER,

•P"*RTLESS»

DEPTH TO

WATER; WATER

ELEVATION 13937.4 14444.7

13735.9 778.32 778.75 786.52

T W 769.06 EM-B1 EM-2

13191.4 13817.5

786.71 19.12 767.4 14419.6 14411.3

777.83 777.47 11.4 766.07 EMH-i-2\J EM-3L

13817.2 14779.9

777.56 777.45 10.71 766.74

EM-3U EM-106

14611.6 14614

775.45 775.68 14786.9 12888.3

11.48 775.36 803.78

775.39 11.21 764.2 764.18

13700.6 803.46 24.8 778.66 EM-107 13794.1

13793.6 13025.7 13021.9

795.91 795.92

795.56 24.33 771.23 EMH-107 EM-108

795.47 24.9 770.57 15451.6 14888.4

14519 14965.7

776.69 776.84 10.11 766.73 EM-109 GZ-1L

769.49 769.69 6.05 763.64

GZ-1U GZ-1R GZ-2L

13551.1 13547.6

13076.1 794.63 794.43 13085.5

18.36 793.32 793.37

13545.1 13092.7 792.07 17.18

N/A 13685.3 13514.2

13517.5 786.18 786.09

3.02 15.92

776.07 776.19 789.05 770.17

GZ-2U GZ-3L GZ-3U GZ-3R GZH-4I GZH-4L

13674.5 14112.9

786.7 786.51 13397.5

16.14 782.69 782.56

14106.8 13394.5 782.76 13.63

782.56 14109

14378.5 13365.2 13095.2

781.23 13.37

N/A 788.7

9.58 788.58

14398 13086.6 13089

788.94 768.59 21.78 22.08

770.37 768.93 769.19 771.65 766.8 766.51

GZH-4M 14392.1 14384.8

788.94 788.18 23.35 765.59 GZH-4U GZ-4R

13092.5 13097.4

788.58 788.39 22.29 766.1

GZ-5L GZ-5U

14365 787.39 14654.9 13966.3 14855.8 13967.5

775.48 775.38

N/A 774.9 6.37 774.82 6.26

N/A 768.53 768.56

GZH-6L GZH-6M

13944 13943.7

13209.3 789.82 789.58 24.7 764.88

GZ-6U 13216.8

13945.6 789.51 789.05

13200.9 22.14

789.89 788.06 21.09 766.91 768.8

GZ-7L GZH-7M GZ-7U

14195.7 13133.3 788.93 768.49 14186.9 13140.6

20.52 788.84 788.75

14195.5 13138.7 20.76

788.77 788.58 20.65

767.97 767.99 767.93

GZ-8L GZ-8U

14110.1 14103.9

12742.2 801.41 801.26 28.15 773.11

GZ-9L 12743.1 801.52 801.39

13553.3 14353.1 27.52

776.72 776.22 6.94 773.87 769.78

GZ-9U GZ-9R

13561 14359.6 777.52 776.39 7.32 770.2

GZ-13L GZ-13M GZ-13U GZ-13R GZ-14L GZ-14U GZ-14R GZ-15L

13550.9 14373.9 776.39 N/A 14389.7 14404.5 775.58 775.19 14383.7

8.89 14400.5 775.16 774.92

14380.2 14396.4 8.72

774.07 773.45 14387.5 14390.5

7.92 773.55 N/A

14060.1 14544.7 7.43

775.91 775.81 14056.9

R 14544

8.11 775.61 775.46

14070.7 14545.4 7.91

773.74 N/A 6.35

770.39 766.3 766.2 766.15 766.12 767.7 767.55 767.39

GZ-15U GZ-15R

13563.7 14135 778.45 777.8 13560.6 13554.4

14140.1 8.17

779.87 777.22 9.51 770.28 770.36

EX-1 EXH-3 EX-4

EX-05A

14147.6 778.61 N/A 14419.7 13087.2 786.92

6.53 N/A

14415.3 13312 31.75

781.45 N/A 14355.7 13810.5 776.31 N/A 14730 14776.5 771.73 N/A

27.6 14.8 -26.7

772.08 755.17 753.84 761.48

745® EX-6 EX-7

14121 13358 781.06 N/A 27.84 753.22 14500

13943.4 14095 775.32 N/A 14.72 761.06

EX-9 13222.8 787.79 N/A 37.14 750.65

Table Continues


Table 4 (continued)

Summary of Water Level Measurements Collected on April 25,1995

OBSERVATION I: POINT: GZ-101L

LCxJytfioi* NORTHING1 13917.8

EASTING; 12942.1

CASING ELEV

iNOVdATUiW 801.07

RISER ELEV.

(NGVDATUM» 806.79

MEAS. REFER. POINT (TYPE "C' * TOC, *R* * RISER I

•p^pmlessv

DEPTH TO

WATER WATER

ELEVATION

; LOWER <1) MODLE iM) UPPER (Ul ROCKfRl*

GZH-101M GZ-101U

13913.4 13916.9

12929.6 12937

801.08 801.01

800.95 800.77

30.22 30.12

77g*57 770.83

T N/A

R 30.08 770.69 12769

12770.4 797.45 800.4

797,07 800.04

28.69 766.38 GZ-102U GZ-103L

14308.3 14363

31.26 768.78 12888.3 12884.2

795.48 795.56

795.19 27.25 767.94 14382.1 14443.7

795.13 26.45 768.68 N/A GZ-104L GZH-104M

13305.7 13298.9

784.04 784.27

783.81 784.03

16.17 767.64 14440.9 14437

17.97 766.06 N/A 13307.8 13397.4

784.15 783.01

783.98 17.74 766.24 M.U GZ-105L GZH-105M

14290,1 14297.7

782.71 14.19 768.52 13397.5 13394.3

782.71 782.83

782.52 14.34 768.18 N/A 14301.4 14048.1

782.72 14.63 768.09 M.U MP-1 MP-6

13488.4 13403.7

776.03 775.13

N/A 6.73 769.3 14390.6 14429.3

N/A 7.3 767.83 13513.4 13579.6

775.4 775.56

N/A 5.77 769.63 MP-8 MP-9

14418.6 14680.6

N/A 4.89 770.67

MP-10 MW-1A MW-1B

14576.6 13364.8

13496.8 13663.5

779.66 N/A 777.89 N/A

9.95

13774.8 779.18 778.89

778.79 9.83 6.81

769.71 768.06 771.98

13373.4 13869.4

13774.9 14399.3

778.59 6.37 772.22 M.U 777.01 776.99

776.45 8.17 768.28 L,M MW-2B MW-3A

13896.1 14012.2

14400.5 14035.2

776.02 8.75 768.24 775.55 775.53

775.35 7.19 768.16 L.M 14005.5 14003.9

14036 14051.7

775.51 6.9 768.61 GZ-10R MW-5A

774.65 775.6

N/A 6.85 767.8 14426.6 14427.3

13996.3 774.74 8.13 766.61 L.M 14003 14001.2

774.4 774.65

774.42 7.56 766.86 GZ-12R MW-6L

14444.1 15037.5

N/A 7.38 767.27 14485.5 14483.9

773.68 773.64

773.6 8.85 764.75 L,M 15032.2 14859.4

773.56 8.84 764.72 MW-7L MW-7U

14790.2 14785.4

776.42 776.38

776 R 12.39 763.61 L.M 14861.5 14630.5

776.13 12.41 763.72 U

MW-9L MW-9M

15497 788.96 14379.6 14376.5

788.72 13670 775.24

23.82 774.07 7.21

764.9 768.03

L, M.U

13669.1 13669.3

775.44 774.15 7.83 767.61 M MW-/-9U MW-10L

14373.1 14404.7

775.56 775.01 7.62 767.94 14890.4 14888.5

771.5 771.24

770.74 5.7 765.04 14400.6 14392.1

770.55 5.51 765.04 M MW-10U P-1

14888.3 13665.3

771.03 770.36 4.54 765.82 14295.8 14341.9

774.94 773.85 5.84 768.01 P-2 13798.5 14406.6

778.26 774.51

778.17 13.27 764.9 L.M P-3 P-6 P-7 P-9

EX-8

14584.3 14797.3

773.88 15161 768.32

8.1

14300.9 768.23

13946.4 774.92 14100

14672.9

774.78 13250.1

4.4

784.52 7.88

784.33 16.05

765.78 763.83 766.9

768.28

L.M L, M, U M.U L.M

14621.7 775.72 N/A 11.14 764.58 L.M GWS-GWS-5

14420.7 14451.1

13051.8 786.88 766.65 20.45 766.2 13071

13112.5 785.84 785.32

785.64 17.9 767.74 GWS-6 GWS-7

14440 14441

784.96 18.86 766.1 U 13142.4 784.74 784.37 R 17.92 766.45 U

NOTE: 1 Designations of L. M. U and/or R apply to use of the observation point's elevation data for construction of preliminary Lower, Middle Upper and Bedrock Piezometric surface contour maps.

J GZ_4R ^covered following dewatering associated with sampling and installation of a packer for a casing integrity evaluation.

1 EX-5A'» water level meter was not operating correctly at the time water levels ware recorded. The above elevation is a value typical of elevations seen when its meter was operating property.


Table 7

Summary of Surface Water Discharge Analytical Results for the Fifth Quarter of Operations

PARAMETER »

Tetrachloroethene

1,1,1-Trichloroethane

ANALYTICAL RESULTS imglt)

3/14/95

3J

1J

4/19/95

3J

1J

5/31/95

31

ND

Trichloroethene

1,1 -Dichloroethene

Toluene

1,1 -Dichloroethane

Vinyl Chloride

Other VOCs w

Total VOCs (c)

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

Notes: (a) Parameters with Cleanup Standards are listed by name. (b) Refer to laboratory analytical report for specific compounds. (c) Discharge limitation is 100 fig/t total VOCs.

Parameter concentrations appended with a "J" are estimated values.

HULL & ASSOCIATES. INC. DUBLIN, OHIO

SEPTEMBER 1995 NHB019D.0I7

New Hampshire Ball Bearings, Inc. South Municipal Water Supply Weil Superfund Site

Table 5

Summary of Analytical Results From Ground-water Monitoring Wells (April 9 - April 12,1995 Sampling Event)

PARAMETER

TETRACHLOROETHENE

1.1,1-TRICHLOROETHANE TRICHLOROETHENE 1,1-DICHLOROETHENE 1,1-DICHLOROETHANE VINYL CHLORIDE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM CARBON TETRACHLORIDE

£M2"01$

2J

ND 2J

ND ND ND ND ND ND

EMH2U-014

ND ND

ND ND ND ND ND ND ND

ANALYTICAL RESULTS (ug/L)

EM3L-015

2J 1J

3J

ND ND ND ND ND ND

EM3U-016

ND ND ND ND ND ND ND ND ND

_EM107U-009

10

220

16

5J 5J

ND ND ND ND

EM109-016

16

2J

33 2J

2J

ND ND ND ND

GZH4I.-013 G23R.004

2500 240 ND ND ND ND ND ND ND

PARAMETER

TETRACHLOROETHENE 1,1.1-TRICHLOROETHANE TRICHLOROETHENE 1,1 -DICHLOROETHENE 1.1-DICHLOROETHANE VINYL CHLORIDE 1,2-DICHLOROETHENE (TOTAL) CHLOROFORM CARBON TETRACHLORIDE

GZ3R-004A

ND ND ND ND

ND ND ND ND ND

G24R-006

16,000

520J

ND ND

290J

ND ND ND ND


GZ4R 00GA

16,000

520 ND ND

300J

ND ND ND ND

G212R^003

ND ND ND ND ND

ND ND ND ND

GZH7M-009 5J

390

15 14

ND ND ND ND ND

GZ101L-017

ND 120

ND 2J

ND ND

ND ND ND

GZ101L-Q17A

ND 110

ND 2J

ND ND

ND ND ND

Table Continues


Table 5 (continued)

Summary of Analytical Results From Ground-water Monitoring Wells (April 9 - April 12,1995 Sampling Event)

PARAMETER

TETRACHLOROETHENE

|GZ101U-016PL

3JD

1.1,1-TRICHLOROETHANE

TRICHLOROETHENE

1,1-DICHLOROETHENE

1,1-DICHLOROETHANE

VINYL CHLORIDE

1,2-DICHLOROETHENE (TOTAL)

CHLOROFORM

CARBON TETRACHLORIDE

310D

2JD

6JD

ND

ND

ND

ND

ND

G2105L-011

36

130

21

2J

ND

ND

ND

ND

GZ10&M008

1J

ND

ND

ND

ND

ND

ND

ND

ND


G2105U-011 MW9L-006 MW9M-00B 1 P3-007

ND 190 ND 20

ND

ND

ND

ND

ND

ND

ND

ND

81

38

7J

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

250

57

14

4J

ND

ND

ND

ND

P&012

NOTES: Sample numbers designated with an "A" represent duplicates.

Sample numbers designated with a "DL" represent diluted samples.

Parameter concentrations appended with a "J" are estimated values.

"ND" indicates parameter concentrations are below Method Detection Limits.

Parameter concentrations appended with an "E" indicate an estimated value due to the concentration exceeding the GC/MS calibration range.

Parameter concentrations appended with a "D" indicate the sample was diluted prior to analysis.


Table 6

Summary of VOC Concentrations in Operating Ground-water Extraction Wells (a.)

PARAMETER

Tetrachloroethene

1,1,1-Trichtoroethane

Tnchtoroethene

1.1 -Oichtoroethene

1,1-Oichtoroelhane

EX10O1 6.900

1,900

660

190 J

Totuena

NO

NO

03/1604 EX1-0Q2 9,700

1,700

8S0

140J

NO

NO

03/25/94 £X14X»

6,700

1,900

740

210J

NO

NO

.6401/94

£Xl>004

6.900

1,600

620

160J

NO

100J

04/1204 EXWJOfi 5,600

1.400

500

110J NO

NO

EX-f 04/29/94

EX1-006

6,300

1,700

430

ND

NO

ND

05/12/94

EX14J07 6.100

1,300

460

NO

NO

ND

EX1O0M 6,100

1,200

440

ND

NO

EX1-006 6.100

1,200

430

ND

ND

06/1004

6,000

920

360

ND

ND

07/26/94

6X1Q10

5,100

720

240

ND

NO

10/12/94

EXlOll 3,800

610

210

NO

NO

NO

01/18/95

EXl-012

3,900

NO

210

NO

NO

04/12/96 EX1P13 2.800

500

160

NO

NO

PARAMETER 03/12/94 EXH3401

.M.'.M.'.'.U.WMU.U.'.y.* M.U''' 'ViVh ViYlVri lYiViVi 03/16/94

EXH3402 EXH0O63 04AH04

EXH3404

EXH-3

04/12/94 6XHU06

maam exHôofi

0S/12/B4

EXH34W7 06/27/94 06/10/94 07/26/94 10/1204 04/1205

3.900 4,100 2,000 2,100 2,000 1.1.1 -Trichtoroethane

1,300 400

1,100 640 660

Tnchtoroethene

1,1 -Dichlofoethene

1,1-Ofchtoroethane

Toluene

220

62J

460

390

670 460 450 390

560 320 130 340 310 260

450 470 420 320 310 330

240

260

200 160 160 65

43J 76J 80J 210 160 160

59J 62

50J 33J ND NO NO NO ND NO NO ND NO

NO

ND

ND

ND ND

NO NO

ND ND ND

9J

4J

NO

NO NO ND

94

39

66

ND

NO

PARAMETER,

Tetrachtoroethene

1,1.1 -Trichtoroethane

Tnchtoroethene

1,1 -Dichloroelhene

1,1-Oichtoroethane

Toluene

EX4-001

290

330

89

45

3J

NO

03/1804

EX4-D02

180

210

100

26

3J

ND

03/25/04

£X4<003

170

270

120

49

4J

ND

• • •

&40T04

EX4-004

250

270

110

42

4J

ND

EX4-004A

240

260

110

41

4J

NO

04/1204 EX44Q0

260

270

99

04/29/94

EX44JO0

270

200

81

36

5J

NO

17

NO

05/12/94

EX4-O0? 230

160 63

1 2

4J

ND

06/27/94

EX40Q6

270

140

00/1004 EX4D09

160

51

4J

110

40

3J

07/26/94

EX4-010

84

63

21

4J

ND

10/12/94

EX4-011

39

39

14

3J

2J

01/1605;

EX4-012

22

20

1J

1J

04/1206 EX4-013

11

12

4J

NO

ND

PARAMETER

Tetrachtoroethene

1.1.1-Tnchtoroethane

Tnchtoroethene

1,1 -Dichtofoethene

1.1-Oichloroelhane

Toluene

03/18/94

EXSMOi

33

100

62

19

4J

ND

QV2504

EX 6A402 40

120

74

28

4J

ND

D4/Q1/M EXSAO03

37

95

59

20

4J

NO

04/0S04

EX6A404: 1X8A-OO4 ft>T

26

73

46

14

'

04/1204

28

68

41

13

04/2604

EXSA4Q6

19

33

28

4J

NO NO ND

EX6A4Q6A

21

66

35

NO

00/1204 EXSA407

20

002704

EXSfcttft

15

47

31

3J 4J

38

24

4J 3J ND

06/1004

EX0M09

10

27

18

3J

NO

ND

07/2604

EX&A010

8

25

IS

3J

2J

ND

10/1204

Ex&um

6

19

12

2J

2J

NO

01/1606

EX6A-012

21

11

2J

1J NO

04/1206

EX6A41* 4J

17

9

NO

NO

ND

Table Continues


Table 6 (continued)

Summary of VOC Concentrations in Operating Ground-water Extraction Wells (a.)

PARAMETER 03/12/94 EX6-001

03/18/9*

6X9002 &8402A 03/26*4

EX6-O03

04/01*4

EX6-004

4/12*4

EX04KK

EX-6

94*9*4

6X6-006

95/12*4

EX6407

05/27*4

EX6-008

08/10*4

EX6-O09 EX6-9A

07/26*4

EX6-10RE

10/12*4

EX8-011

01/18*5

EX0-012

2J Tetrachtoroethene 12 14 15 13J 14J 29 12J 11J 11J

1.1.1 -Trichbroethane 790 7J 8J 10J 4J

700 730 740 630 570 460 490 Trichtoroethene 45

430 330 340 320 98 47 45 55 60 77 73

1,1-OichkMoethene 77 70 57 59

88 89 42 32

90 99 84 67 33 22 17 1,1-Dichtoroethane

15J 1SJ NO 6J ND

10J 4J 9J 10J 11J NO 8J 7J NO

Toluene NO NO NO 5J 3J

NO NO NO NO ND ND NO NO

27

NO

2J

PARAMETER 09/12*4 EX7-001

03/18*4

CX7-002

93*5*4

SX7-0P3

04*1*4

EXT-004

04/12*4

EX7-00S

EX-7 94/29*4

6X7-006 96/12*4 EX7-007

05*7*4

EX7-006

imtiw EX7-009

07/26*4

6X74)10 10/12*4

EX7-011

01/18*5

EX7-012

04/12*6:

6X7-Q13

4J Tetracnioroelhene 140 170 210 260 220 120

1.1.1-Trichbroethane 360 370 420 380 340 220 Trichtoroethene 64 110 150 150 120 76

1,1 -Oich toroetherw

80

160

60

56 24 16 120 97 72 58

41 32 20 18

20 6

12

49 52 70 58 4J

18 10 1,1 -Dbhtoroethane

4J 4J

Toluene

1J 3J NO 5J 5J

NO 6J ND 4J 3J 3J 2J 2J

NO NO NO NO

ND NO NO 3J 1J NO

ND

NO

PAfVtMETER 03/12*4

&0-O01 EX04O1A 93/18*4

EX0902RE 03/25*4 EX9-993

04*1*4

6X9*04 04/12*4

EX0-OO6

ex-S 94*9*4

6*9908 06/12*4 6X9907

05*7*4

EX9909 6X9090A

mnam: €*9-009

07/28*4

6X04)1 ORE 10/(2*4 : mn 'Sim

EX0-O12

5J Tetrachtoroethene 4J 4/ 4J 5J

1.1,1-Trichtoroethane 70 69 92 110 100

10

180

11J 24 13J 13J 11J 7J 6

590 630 Trichtoroethene 26

570 560 630 320 160 220 28 31 35 42 37 22/ 24 19J

1,1-Dichtoroethene 11 21 17 18 31 17

12 16 19J 4J NO NO 3J 1,1-Dichtoroethane

Toluene

2J

NO

NO 3J 2J 3J 3J 3J

NO 3J 19J ND NO NO

NO NO NO NO 2J NO

NO NO NO NO NO NO NO

NOTES: (a.) AO concentrations reported in ug/l.

Parameter concentrations appended with a 'J' are eatirrated values.

*NDa indicates parameter concentrations are betow Method Detection Limits.

10000 -=T PUMPING AT EX-1 OURING THE IRM

O) 3 (/> z o

§ LU o z o o a: LU H-UJ 2

*

1000 -=

100 -=

10 -=d

1 -=

0

00 -si

00 00

00 <o CO o

CO

TIME

CO N3

CO OJ CO

A CO Ol

(O o>

FIGURE 1 Hull & Associates, Inc.

Dubtn. Ohio

NEW HAMPSHIRE BALL BEARINQS, INC.

VOC Concentrations Versus Time at EM-2

PETERBOROUGH. NEW HAMPSHIRE

AUGUST 1995 NHB019

300

275

g 250 •) 3

w 225

° 200

175

150

125

100

75 -

50 -

25 -

0

Z 111 o

z o

o o r UJ h— LU

£

PUMPING AT EX-1 DURING THE IRM

CLEANUP LEVEL FOR 1,1,1-TCA

1 1 1 1 1 i i 1 1 1 M i r

00 "vl 00

00 00 CO

CO o CO

TIME c5 to CO

G> <o •U CO

tn & o>


Dubin Ohto

NEW HAMPSHIRE BALL BEARINGS. INC.

VOC Concentrations Versus Time at EMH-2U PETERBOROUGH. NEW HAMPSHIRE

AUGUST 1995 NHB019

O) D

CO z o

£ UJ O z o o a: UJ

tli

£

PUMPING AT EX-1

00 00 00

00 co

CO o CO

TIME CO ro co

co CO £ Ol CO

0)

FIGURE 3 Hull & Associates. Inc.

Dubfin, Ohio


VOC Concentrations Versus Time at EM-3L

PETERBOROUGH, NEW HAMPSHIRE

AUGUST 1995 NHB019


GO GO 00

00 CO

CO O CO

TIME

<5 ro <o

CO cB CO

On CO o>


Dubin. Ohio


VOC Concentrations Versus Time at EM-3U


AUGUST 199S NHB019


o> 3

CO z o

£ LU o z o o a: UJ h~ LU 2

00 ^1 00

00 00 CO

CD o

CD

TIME CO N5

CO Ca> J£ Oi CD

Oi


Dubfn. Ohb

NEW HAMPSHIRE BALL BEARINGS, INC.

VOC Concantrations Versus Time at EMH-107U


AUGUST 1995 NKB019


O)

CO z 0

1 h-z UJ o z o o a: LU

UJ —

2 < a.

00 -N|

00 00

00 CO

CO o

CD

TIME

CD ISO

CO 00 CD CD

O* CD 0)


Dubin, Ohio


VOC Concentrations Versus Time at EM-109


AUGUST 1995 NHB019

PUMPING AT EX-1 DURING THEIRM

o>

cn Z O

£ I-z LU O z o o a: LU h— LU 5

$

*

1000 -=

100 -=

10 —

1 -=

a> oo oo oo

co CO o

CO

TIME CO K)

£ c*> CD 4k- <D Ol

CO O)


Dubfin, Ohio


VOC Concentrations Versus Time at GZ-101L PETERBOROUGH, NEW HAMPSHIRE

AUGUST 1895 NHB019

O) 3

C/) z o

LU O z o o o: LU I— LU 5

£

1000 -=

100 -=

10

1 -=

0

PUMPING AT EX-1 OURING THEIRM


V.

CLEANUP LEVB. FORPERC AND TCE

l l l l l l l l l f f

\ I

.V-

l l l l f l l l l f f l l l l l l l l l l l

00 -vj 00 00

00 CO

CO o

CO

TIME c5 ro CO

CO CO CO

Ol CO 0)


Dubfin. Ohio


VOC Concentrations Versus Time at GZ-101U PETERBOROUGH. NEW HAMPSHIRE


o> 3

</>

o H

LU O Z o o o: LU i— LU 2

2 < Q_

1000 -d

~ 100 -=

10 —

1 -=

0

00 00 00

00 <o CO o

CO

TIME CO ISO

CO GO CO CO Ol CO O)


Dubin. Ohio

NEW HAMPSHIRE BALL SEARINGS, INC.

VOC Concentrations Versus Time at GZ-105L PETERBOROUGH, NEW HAMPSHIRE

AUGUST 1995 NHB019


100 -d

— 1000 — D) 3 CO z o

£ h-z LU o z o o K LU t— LU 2

£ < Q.

10 -=

1 -=

oo -J 00

00 00 CO

cB o CO

TIME

cB ro

CO Ct) CO CO

Ol CO o>


Dublin, Ohio


VOC Concentrations Versus Time at GZH-106M


AUGUST 1995 NHB019


o> 3 CO Z o

£ h-z LU O z o o Q: LU t— LU 2

< CL

1000 —

100 -=

10 -=

1 —

0

00 -vl 00

00 00 CO

CO o CO

TIME

CO N> CO CO 4k. 3 Ol CO

O)

FIGURE 11 „Hull & Associates, Inc.

Dublin, Ohio


VOC Concentrations Versus Time at GZ-106U PETERBOROUGH. NEW HAMPSHIRE

AUGUST 1995 NHB019


a> 3

CO z o

£ LU O z o o a: LU H-LU

< a.

100000 -=

10000 -s

1000 -=

100 -=

10 —

1 -E

00 -sj 00 00

00 (D

<s o

<5

TIME

<0 to

(O G> CO

A CO Ol

<o o>


Oublin. Ohio


VOC Concentrations Versus Time at GZH-4L


AUGUST 1995 NH8019


o> 3

o

% I-2 LU O z o o a: UJ H— LU S

£ £

10000 -=

<0 1000 -=

100 -=,

10 -=

1 -=

0

00 -«4 00 00

00 <o <o

o (O

TIME CO ro

CD oo

CD CD cn

CO O)


DubinJDhb


VOC Concentrations Versus Time at GZ-4R


AUGUST 1995 NHB019

PUMPING AT EX-1 DURING THE 1RM

2

111 o z o o CtL LU h-LU 2

£

2

1000 —

O) 3 if) Z o = 100 -d

10 —

1 -=

00 oo oo 00 <o CO

o £>

TIME

<o NO

CD G>

CO CO U1

CD 0)


Dublin. Ohto


VOC Concentrations Versus Time at GZH-7M PETERBOROUGH. NEW HAMPSHIRE

AUGUST 1995 NH8019

PUMPING AT EX-1 DURING THE IRM REMEDIAL

PUMPING

o>

CO

1000 -=

100 -d

00 00 00

00 CO

<0 o

<0

TIME £ ro

<0 CO

CO •tw CO

CJ1 (0 0)


DubMn, Ohto NEW HAMPSHIRE BALL BEARINGS, INC.

VOC Concentrations Versus Time at MW-9L


AUGUST 1995 NHB019

1000 —=r PUMPING AT EX-1 DURING THE IRM

o> 3

CO z o

LU O z o o oc Ui I-UJ 2

2 < a.

100 -a

10 —

0

1 -=a

00 -J

00 00

00 CO

CO o

co

TIME CO ro co

co CO •U

CO cn

co 0)


Dubin. Ohio


VOC Concentrations Versus Time at MW-9M


AUGUST 1995 NHB019

O) 3 <0 z o

UJ O z o o DC LU

UJ

2

300

275

250

225

200

175

150

125

100

75

50

25

0

PUMPING AT EX-1 DURING THEIRM


Minimi mm i HIT

PRE-OESIGN PUMP TESTS

LEGEND

# - PERC

-A- 1,1,1-TCA

—B TCE

CLEANUP LEVEL FOR PERC AND TCE

l l l l l l l l l l l l l l l l l l l l l l TT l l l l l l l l l l l l l l l l l

oo *>4

00 00

00 <o (O

o <o

TIME

CO N) CD CO CD CD

ttl CD O)


DubGn, Ohto


VOC Concentrations Versus Time at P-3


AUGUST 1995 NHB019

O) 3 (O z o

HI o z o o a: UJ

Ui

350

325

300

275

250

225

200

175

150

125

100

75

50

25

0


CLEANUP LEVEL FOR 1.1,1-TGA

CLEANUP LEVEL FOR PERC ANDTCE

minimi

PRE-DESIGN PUMP TESTS

minim mil ium

wl

1111J r 11111

A

1 / X

* / * »/

/ * I

REMEDIAL PUMPING

\ »AX

k m

11II11 n

OD -J CD

CD 00 CO CO

O CO

TIME CO IO CO CO CO

A co Ol CO

o>

FIGURE 18 Hull & Associates, inc.

Dublin. Ohio


VOC Concentrations Versus Time at P-6


AUGUST 1905 NHB019


Dubfin, Ohio


VOC Concentrations Versus Time at EX-1


AUGUST 1995 NKB019

ST 10000 o> 3

CO z £ 1000

Lil O z o o a: LU h LU

< Q_

100

10


Dubln, Ohio

NEW HAMPSHIRE BALI BEARINGS, INC.

VOC Concentrations Versus Time at EXH-3


AUGUST 199S NHB019

s s s s s o to to CO

£ £ 2 £ 2 Si <0 *-


Dublfl. Ohio




AUGUST 1995 NHB019

^200 O)

3

CO

Il60

LU o 100

o o LU

LU IE

s < 0.

50 -

o § % %

o £

o W o 35

g I

0 s 1 A

w

§

o § 3 A

§ -g t

a S O s «! <o cn

5 (O

w

s £ cn

s

$ £ 8


Dublin. Ohto


VOC Concentrations Versus Time at EX-6A


AUGUST 1995 NH8019


Dubfifi, Ohio




AUGUST 1995 NK8019


Dublin, Olio




AUGUST 1995 NHB019

. ^ 7 0 0 o> 3650 CO 600

O 550

F 500

S 450

400

FIGURE 26 Hull & Associates, inc.

Dublin. Ohio




AUGUST 1995 NHB019

ATTACHMENT A

Ground-Water Sampling Documentation

HULL A ASSOCIATES, INC. DUBLIN, OHIO SEPTEMBER 1995

NHB019D.017

SAMPLE DATA SUMMARY PACKAGE

LAB CODE: AOT7AT

CASE NO.: K\m/\L

SDGNO.:

CONTRACT NO.: WQSj^

INCHCAPE TESTING SERVICES AQUATEC LABORATORIES

Inchcape Testing Services Aquatec Laboratories

55 South Park Drive

Colchester, VT 05446

Tel. 802-655-1203

Fax. 802-655-1248

April 28, 1995'

Mr. Steve Dishong Hull & Associates, Inc. 360901 Pinetree Place Route 101 Bedford, NH 03110

RE: Project NHBB Superfund Site ITS-Aquatec Project No. 94246 Case No. NHBA6: SPG 50557

Dear Mr. Dishong:

Enclosed are the analytical results for the samples received intact by Inchcape Testing Services-Aquatec Laboratories on April 14, 1995. Laboratory numbers and quality control samples were assigned as follows:

Client Sample ID

Laboratory Number

Sample Matrix

Samples.Received on April 14, 1995 ETR No. 50557

GZH4L013 GZ4R006A GZ7M009 GZ7M009MS GZ7M009MSD GZ12R003 GZ101L017 GZ101L017A GZ101U016 GZ105L011 GZ105U011 MWMW9L008 MWMW9M008 MWP3007 MWP6012 TB1041095 HB

253070 253071 253072 253072MS 253072MD 253073 253074 253075 253076 253077 253078 253079 253080 253081 253082 253083 253084

Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water

The initial volatile analysis of sample GZ101U016 exhibited i* 11 l~trichloroethane above the calibration range. A subsequent dilution analysis was performed. Both sets of results have been included in this submittal.

Mr. Steve Dishong April 28, 1995 page 2

For the benefit of interested parties, documentation of sample handling and preparation is included at the end of the Sample Data Package. A colored sheet of paper entitled "Sample Preparation Package and Sample Handling" has been used to explicitly mark the location of these documents.

If there are any questions or clarifications regarding this

!802^655-1203aSe C°ntaCt yoUr Pr°3ect Director, Scot Swanborn at

Sincerely,

Karen R. Chirgwin Laboratory Operations Director

KRC/lml

Enclosure

94246B27APR95

VOLATILE ORGANICS ANALYSIS DATA SHEET SAMPLE NO

Lab Name: AQUATEC, INC. Contract: 94249

Lab Code: AQUAI Case No.: NHBA6 SAS No.: SDG No.: 50557

Matrix: (soil/water) WATER

Sample wt/vol: 5 . 0 (g/mL) ML

Level: (low/med) LOW

% Moisture: not dec.

GC Column:CAP ID: 0.53 (mm)

Soil Extract Volume: (UL)

Lab Sample ID: 253074

Lab File ID: M253074V.D

Date Received: 04/14/95

Date Analyzed: 04/19/95

Dilution Factor: 1.0

Soil Aliquot Volume: (uL)

CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L

74-87-3 — Chlorome thane 74-83- 9 Bromomethane 75-01- 4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Dichloroethene" 75-34-3 1/1- Di chloroethane" 540-59-0 1/2 - Dichloroethene" 67-66-3 Chloroform 107- 06-2 1;2 - Di chl oroet hane 78-93-3 2 -Butanone

total'

7 1 - 5 5 - 6 1 ,1, l-Trichloroethane 56-23-5 --Carbon Tetrachloride " 75-27-4 Bromodichloromethane 78-87- 5 1,2-Di chloropropane 10061-01-5 -cis-1,3-Dichloropropene 79-01-6 — Trichloroethene 124-48-1 Dibramochlorcmethane 7 9 - 0 0 - 5 1 / 1 , 2 - Trichloroe thane 71-43-2 Benzene 10061-02-6 trans-1, 3-Dichloropropene 75-25-2 Brcmoform 108-10-1 4 rMethyl - 2 - Pentanone 591-78-6 2 - Hexanone i?7:18:4 Tetrachloroe thene 79-34-5 1 , 1 , 2 , 2 - Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 100-42-5 1330-20-7

•Ethylbenzene •Styrene •Xylene total

Q

FORM I VOA 3/90

VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS

UFA SAMPLE NO.

GZ101L017 Lab Name: AQUATEC, INC. Contract: 94249

Lab Code: AQUAI Case No. : NHBA6 SAS No. : SDG No. : 50557


Sample wt/vol: 5.0 (g/mL) ML




Soil Extract Volume: (uL)

Number TICs found: 0



- Date Received: 04/14/95




CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L

CAS NUMBER

1. 2 . 3. 4. 5. • 6 . 7.

9. 10. 11.' 1 2 . ' 13.' 14.' 15." 16."

17." 18.' 19." 20 . " 21." 2 2 . " 23." 24." 25." 2 6 . " 27." 2 8 . " 29." 30."

COMPOUND NAME RT EST. CONC. Q

FORM I VOA-TIC 3/90

LA VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.


Lab Code: AQUAI Case No.: NHBA6 SAS No.:






Soil Extract Volume: <UL)

GZ101L017A


74-87-3 Chlorome thane 74-83-9 Bromomethane Z?~?Z~4 —Vinyl Chloride 75-00-3 Chloroethane 75-09-2- Methylene Chloride 67-64-1 —Acetone 75-15-0--- Carbon Disulfide 7 5 - 3 5 - 4 1 , 1 - D i c h l o r o e t h e n e 7 5 - 3 4 - 3 i , 1 - D i c h l o r o e t h a n e 5 4 0 - 5 9 - 0 1 , 2 - D i c h l o r o e t h e n e ( t o t a l ) 67-66-3 Chloroform 107-06-2 1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75 •2 7_ 4 Bromodichlorcmethane"

1*2- Dichloropropane 10061-01-5 -cis-1,3-Dichloropropene 7? T01:6 Tr ichloroethene 124-48-1 Dibrcmochlorcmethane 79-00-5 1,1,2- Trichloroe thane 71-43-2 Benzene 10061-02-6 trans-1,3-Dichloropropene 75-25-2 Brcmoform 108-10-1 4-Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene_ 108-90-7 Chi orobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 13 30-20-7 Xylene total

SDG No.: 50557







FORM I VOA 3/90

IE VOLATILE ORGANICS'ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO,

GZ101L017A Lab Name: AQUATEC, INC. Contract: 94249
















CAS NUMBER

1. 2. 3.' 4.' 5.' 6 . ' 7.' 8 . " 9/

1 0 . '

11." 12." 13." 14." 15." 16."

17." 18." 19." 2 0 . " 21." 2 2 . " 23. 24. 25. 2 6 . 27. 2 8 . 29. 30.

COMPOUND NAME RT EST. CONC.

FORM I VOA-TIC 3/90

VOLATILE ORGANICS ANALYSIS DATA SHEET UFA SAMPLE NO.

GZ101U106 Lab Name: AQUATEC, INC. Contract: 94249








CAS NO. COMPOUND

74-87-3 - Chi orome thane 74-83- 9 Bramomethane 75-01- 4 —Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0- Carbon Disulfide 75-35-4 1,1- Dichloroethene 75-34-3 1,1-Di chloroethane" 540-59-0 l,2-Dichloroethene" (total) 67-66-3 Chloroform 107-06-2 1,2 -Di chloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23 -5 Carbon Tetrachloride 75-27-4-- Brcmodichloromethane" 78-87- 5 —1,2 -Dichloropropane 10061-01-5 cis-1,3 -Di chloropropene 79-01- 6 Trichloroethene 124-48-1 Dibromochl orome thane 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene 10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromoform 108-10-1 4-Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 127-18-4- - Tet rachl oroe thene 79-34-5 1,1,2,2 - Tetrachl oroe thane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4- Ethylbenzene 100-42 - 5- - Styrene 1330-20-7 Xylene (total)






Soil Aliquot Volume:1 (uL)

CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q

FORM I VOA 3/90


fiifA SAMPLE NO.



Matrix: {soil/water) WATER













CONCENTRATION UNITS: {ug/L or ug/Kg) UG/L

CAS NUMBER

1. 2 . '

3.' 4.' 5.' 6 . '

7.' 8 . '

9.' 10." 11." 12." 13." 14." 15." 16." 17." 18."

19." 2 0 . " 21." 2 2 . 23. 24.' 25. 2 6 . 27. 2 8 . 29. 30.


FORM I VOA-TIC 3/90

1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO





Level: (1 ow/med) LOW




GZ101U016DL

SDG No.: 50557

Lab Sample ID: 253076D1

Lab File ID: M253076D3V.D






74-87-3-74-83-9-75-01-4-75-00-3-75-09-2-67-64-1-75-15-0-75-35-4-75-34-3-540-59-0 67-66-3-107-06-2 78-93-3-71-55-6-56-23-5-75-27-4-78-87-5-10061-01 79-01-6-124-48-1 79-00-5-71-43-2-10061-02 75-25-2-108-10-1 591-78-6 127-18-4 79-34-5-108-88-3 108-90-7 100-41-4 100-42-5 1330-20-

Chloromethane Bromomethane Vinyl Chloride Chloroethane

- Methylene Chloride Acetone Carbon Disulfide 1,l-Dichloroethene 1#l-Dichloroethane" 1/2-Dichloroethene (total) Chloroform 1,2-Dichloroethane 2-Butanone 1,1,l-Trichloroethane Carbon Tetrachloride Bromodichloromethane" 1,2-Dichloropropane

"5 cis-1,3-Dichloropropene - - Trichloroethene

Dibrcmochl orome thane 1,1,2-Trichloroethane Benzene trans -1,3 - Dichloropropene

—Brcmoform 4-Methyl-2-Pentanone 2-Hexanone Tetrachloroethene 1/1,2,2-Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Styrene

7 Xylene (total)

Q

FORM I VOA 3/90


UFA SAMPLE NO.

GZ101U016DL Lab Name: AQUATEC, INC. Contract: 94249









Lab Sample ID: 253076D1







CAS NUMBER

1. 2 . ' 3. 4.' 5.' 6 . '

7." 8 . '

9.' 10."

11." 12." 13." 14." 15." 16."

17." 18." 19." 2 0 . " 21." 2 2 . 23. 24. 25. 26. 27. 2 8 . 29. 30.


FORM I VOA-TIC 3/90

1A EPA SAMPLE NO. VOLATILE ORGANICS ANALYSIS DATA SHEET
















74- 87-3 Chlorome thane 74-83- 9 Br omcmethane 75-01- 4 —Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 --Carbon Disulfide 75-35-4-- i, 1-Dichloroethene 75-34-3 1,1-Dichloroethane" 540-59-0 1, 2-Dichloroethene" 67-66-3 Chloroform 107-06-2 — 1,2-Dichloroethane 78-93-3 2 - Bu tanone

total)

71-55-6 l, 1,1-Trichloroethane 56-23-5 ---Carbon Tetrachloride 75- 27-4 Bromodichloramethane 78-87-5 1,2 - Dichloropropane m n c i . m _ c ^ 10061-01-5 -cis-1,3-Dichloropropene 79-01-6 Tr ichloroethene 124-48-1 Dibramochloromethane 79-00-5 1,1,2 - Trichloroe thane 71-43-2 Benzene 10061-02-6 trans -1,3- Dichloropropene 75-25-2 Brcmoform 108 -10 -1 4 -Methyl - 2 - Pentanone 591-78-6 2 -Hexanone 12 7; - 4 Tetrachloroethene 79-34-5 1,1,2,2 - Tetrachloroethane 108-88-3 Toluene 108-90-7 - -Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 1330-20-7

Styrene •Xylene (total)

10 10 10 10 5 10 5 7 2 5 5 5 10 130 5 5 5 5 21 5 5 5 5 5

10 10 36 5 5 5 5 5 5

Q

FORM I VOA 3/90


SAMPLE NO.

GZ105L011 Lab Name: AQUATEC, INC. Contract: 94249


Matrix: (soil/water) WATER.














CAS NUMBER

1. 2. 3.' 4.' 5.' 6 . '

! . '

8 . '

9.' 10.'

11." 12.'

13." 14." 15." 16."

17." 18."

19." 20 . " 21." 2 2 . " 23. 24._ 25. 2 6 . 27. 2 8 . 29." 30.


FORM I VOA-TIC 3/90

EPA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET









CAS NO. COMPOUND








74-87-3 74-83- 9 75-01- 4 Vinyl Chloride 75-00-3 Chloroethane

• Chlorome thane Bromomethane

75-09-2 Methylene Chloride 67-64-1 —Acetone 75-15-0 — Carbon Disulfide 75-35-4 — 1 ,1-D'ichloroethene 75-34-3 1 ,1 - Dichloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1 , 2 - Dichloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bramodichloromethane" 78-87- 5 1 ,2 -Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01- 6 Trichloroethene 124-48-1 Dibromochlorcme thane 79-00-5 1 , l, 2-Trichloroethane" 71-43-2 Benzene 10061-02-6 trans -1,3 -Dichloropropene 75-25-2 "—Bromoform 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 127-18-4 - Te t rachl oroe thene 79-34-5 1,1,2,2 - Tetrachloroe thane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene (total)

FORM I VOA 3/90


SPA SAMPLE NO.

















CAS NUMBER

1. 2. 3.' 4.' 5.' 6 . '

7.' 8 . '

9.' 10.'

11." 1 2 . ' 13." 14." 15." 16." 17." 18."

19." 20. " 21."

22 . " 23." 24." 25. 2 6 . 27. 2 8 . _ 29. 30. ~

COMPOUND NAME RT EST. CONG.

FORM I VOA-TIC 3/90

LA. VOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.


Lab Code: AQUAI Case No.: NHBAS SAS No.: SDQ NO.: 50557



Level: (1ow/med) LOW




CAS NO. COMPOUND


Lab File ID: M253070DV.D






74-87-3 -Chlorome thane 74-83- 9 Bromomethane 75-01- 4 Vinyl Chloride 75-00-3 Chloroe thane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1 , 1 - Dichloroethene 75-34-3 1,1- Dichloroe thane 540-59-0 l, 2 - Dichloroethene" 67-66-3 Chloroform 107-06-2 l, 2-Dichloroethane 78-93-3 2 - Butanone

total)

7 1 - 5 5 - 6 1 , l, 1-Trichloroethane 56-23 -5 Carbon Tetrachloride 75 -27-4 Bromodichloramethane 78- 87-5 1 , 2 - Dichloropropane 10061-01-5 cis-l,3-Di chloropropene 79-01-6 Tr ichl oroe thene 124-48-1 — Dibrcmochloramethane 79-00-5 1 ,1,2-Trichloroethane 71-43-2 Benzene 10061-02-6------trans-1,3-Dichloropropene 75-25-2 Bromoform 108-10-1 - 4-Methyl - 2 - Pentanone 591-78-6 2 - Hexanone i? 7 718"4 Tetrachl oroe thene 79-34-5 1 , 1 , 2 , 2 - Tetrachl oroe thane 108-88-3 Toluene 108-90-7 Chl orobenz ene 100-41-4 --Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene (total)

170 170 170 170 84 170 84 84 84 84 84 84

170 240 84 84 84 84 84 84 84 84 84 84

170 170

2500 84 84 84 84 84 84

U U u u u u u u u u u u u

FORM I VOA 3/90

VOLATILE ORGAN!CS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS •

am jmcj

GZH4L013 Lab Name: AQUATEC, INC. Contract: 94249
















CAS NUMBER

1. 2. 3.' 4.' 5." 6 . ' 7.' 8 . " 9."

10." 11." 12." 13." 14." 15." 16." 17." 18."

19." 2 0 . 21. 2 2 . 23. 24. 25. 26." " 27. 2 8 . 29. 30.


FORM I VOA-TIC 3/90

1A VOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

GZ4R006A Lab Name: AQUATEC, INC. Contract: 94249

Lab Code: AQUAI Case No.: NHBA6 SAS No. : SDG No.: 50557







CAS NO. COMPOUND'








74-87-3 Chi orome thane 74-83- 9 Bromomethane 75-01- 4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1- Dichloroethene 75-34-3 1,1- Dichloroethane" 540-59-0 1,2-Dichloroethene (total 67-66-3- Chloroform 107-06-2 1,2- Di chloroethane 78-93-3 2 - Bu tanone 71-55-6 l, 1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75- 27-4 Bromodichloromethane" 78-87- 5 1,2 -Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01- 6 Trichloroethene 124 -48-1 Dibrcmochlorcmethane 79-00-5 1,1,2-Trichloroethane" 71-43-2 Benzene 10061-02-6 -trans-1,3-Dichloropropene 75-25-2 Brcmoform 108-10-1 4 - Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2 - Tetrachloroethane 108-88-3 —Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene (total)

FORM I VOA 3/90

IE VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

GZ4R006A Lab Name: AQUATEC, INC. Contract: 94249

Lab Code: AQUAI Case No.:. NHBA6 SAS No.: SDG No.: 50557















CAS NUMBER

1. 2 . 3. 4. 5. 6 . '

7. 8. 9.

10.' 11.' 1 2 . ' 13.' 14.' 15.' 16." 17." 18." 19. 20 . " 21."

2 2 . "

23." 24." 25." 26." 27." 2 8 . 29. 30.


FORM I VOA-TIC 3/90

VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO

GZ7M009 Lab Name: AQUATEC, INC. Contract: 94249





% Moisture: not dec. __








Soil Aliquot Volume: <uL;


74-87-3 Chlorome thane 74-83- 9 — Bromomethane 75-01- 4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 -—Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75- 35-4 1,1 - Di chl oroethene 75-34-3 1,1-Di chloroethane" 540-59-0 1/2 - Dichl oroethene" 67-66-3 Chloroform 107-06-2 1/ 2-Dichloroethane 78-93-3- 2-Butanone

total'

71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Brcmodichloramethane 78-87-5 1,2 - Dichloropropane i n n c i . m . c _ J _ - c 10061-01-5 cis-l,3-Di chloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochlorcmethane 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene 10061-02-6—_— trans-1, 3-Dichloropropene 75-25-2 Brcmoform 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachl oroethene 79-34-5 1,1,2,2 - Tetrachl oroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene .total)

25 25 25 25 12 25 12 14 12 12 12 12 25 390 25 12 12 12 15 12 12 12 12 12 25 25 5 12 12 12 12 12 12

Q

U u u u u u u J u u u u u u

FORM I VOA 3/90










SFA SAMPLE NO.

GZ7M009

SDG No.: 50557







Number TICs found: 0 CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L

CAS NUMBER

1. 2. 3. 4. 5.' 6 . 7.

9. 10.'

11.' 12.' 13.' 14.' 15.' 16." 17." 18." 19." 20. " 21." 22.* 23.* 24." 25." 26 . " 27." 2 8 . _ 29. 30.


FORM I VOA-TIC 3/90

-LA

VOLATILE ORGANICS ANALYSIS DATA SHEET


Lab Code: AQUAI Case No. : NHBA6 SAS No. :







GZ12R003

SDG No.: 50557








74-87-3 Chlorome thane 74-83- 9 Bromomethane ~~ 75-01- 4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Di chloroetheiie" 75-34-3 1,1- Dichloroe thane 540-59-0 1,2-Dichloroethene (total 67-66-3— -Chloroform 107-06-2 - -1,2- Dichloroethane 78-93-3-- 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichloromethane" 7?I?7"?T~I 1»2 - Dichloropropane 10061-01-5- cis-1, 3-Dichloropropene 7?: 01 - 6 Trichloroethene 124-48-1 Dibramochloromethane 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene 10061-02-6 trans-1, 3-Dichloropropene 75-25-2 Bromoform 108-10-1 4-Methyl-2 -Pentanone 591-78-6 2 - Hexanone 127-18-4 Tetrachloroethene 7?"34'5 1/1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethy lbenzene 100-42-5 Styrene 1330-20-7 Xylene (total

FORM I VOA 3/90


UPA SAMPLE NO.

GZ12R003 Lab Name: AQUATEC, INC. Contract: 94249













Dilution Factor: l. o



CAS NUMBER

1. 2. 3.' 4.' 5.' 6 . '

7.' 8." 9.'

10." 11." 12." 13." 14." 15." 16."

17." 18."

19." 20. " 21."

22." 23." 24. 25. 26." 27. 2 8 . 29. 30.


FORM I VOA-TIC 3/90

1A VOLATILE ORGAN!CS ANALYSIS DATA SHEET EPA SAMPLE NO.

MWMW9L008 Lab Name: AQUATEC, INC. Contract: 94249














CAS NO. COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L Q

74-87-3 Chi orome thane 74-83- 9 Br omomet hane 75-01- 4 Vinyl Chloride 75-00-3 - -Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75- 35-4 --1,1 -Dichloroethene 75-34-3 — 1,1-Dichloroethane 540-59-0- -1,2-Dichloroethene (total) 67-66-3 Chloroform 107- 06-2 1,2-Dichloroethane 78-93-3 - -2-Butanone ~ 71-55-6 1,1,1-Trichloroe thane 56-23-5 Carbon Tetrachloride 75 ~2 1~4 Brcmodichloromethane 78-87-5 1,2 - Dichloropropane 10061-01-5 cis-1, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1,2 - Trichloroethane 71-43-2 Benzene 10061-02-6 trans-1,3-Dichloropropene 75-25-2 - - - -Bromoform 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 127-18-4 Tetrachloroethene 79-34-5 1 , 1 , 2 , 2 - Tetrachloroe thane 108-88-3 Toluene 108-90-7 100-41-4 100-42-5 1330-20-7

•Chlorobenzene - Ethylbenzene_J •Styrene •Xylene , total)

16 16 16 16

8 16

8 7 8 8 8 8

16 81 16

8 8 8

38 8 8 8

16 16 190

8 8 8 8 8.

U u u u u u u J u u u u u

FORM I VOA 3/90


SAMPLE NO

MWMW9L008 Lab Name: AQUATEC, INC. Contract: 94249
















CAS NUMBER

1. 2 . 3. 4. 5. 6 . 7.

9. 10.'

11.'

12.'

13.' 14.' 15." 16.' 17." 18."

19." 20." 21.'

22." 23." 24." 25." 2 6 . " 27." 28 . " 29." 30."


FORM I VOA-TIC 3/90

VOLATILE ORGANICS ANALYSIS DATA SHEET SAMPLE NO.


Lab Code: AQUAI Case No.: NHBA6 SAS No.: SDG No. : 50557














74-87-3 Chlorome thane 74-83- 9 Bromomethane ~ 75-01- 4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Di chloroethene Z?I3^T37 i'Dichloroethane" 540-59-0 1,2 -Dichloroethene (total) 67-66-3- - Chloroform 107-06-2 — 1,2-Di chloroethane 78-93-3 2-Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5--- Carbon Tetrachloride 75-27-4 — Bromodichloramethane" 78-87- 5 -1 2-Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01- 6 Trichloroethene 124-48-1 Dibramochlorcmethane 79-00-5 1,1,2 - Tr ichloroethane 71-43-2 Benz ene 10061-02-6 trans-1,3-Dichloropropene 75-25-2 Brcmoform 10 8 -10-1 4 -Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 127-18-4 -Tetrachloroethene 79-34-5 1,1,2,2 - Tetrachloroe thane 108-88-3 Toluene 108-90-7--. Chlorobenzene 100-41-4 Ethylbenzene 100 -42-5 Styrene 1330-20-7 •Xylene (total

Q

FORM I VOA 3/90


LPA SAMPLE NO.

MWMW9M008 Lab Name: AQUATEC, INC. Contract: 94249

Lab Code: AQUAI Case No.: NHBAS SAS No.: SDG No.: 50557















CAS NUMBER

1. 2. 3.' 4.' 5." 6." 7.' 8 . '

9." 10.'

11." 12." 13." 14." 15." 16." 17." 18."

19." 2 0 . 21. 2 2 . 23. 24. 25. 26. 27. 2 8 . 29. 30.


FORM I VOA-TIC 3/90'

-LA UFA SAMPLE NO VOLATILE ORGANICS ANALYSIS DATA SHEET







GC Column:CAP ID: 0.53 {mm)








CAS NO. COMPOUND CONCENTRATION UNITS: {ug/L or ug/Kg) UG/L

74-87-3-74-83-9-75-01-4-75-00-3-75-09-2-67-64-1-75-15-0-75-35-4-75-34-3-540-59-0 67-66-3-107-06-2 78-93-3-71-55-6-56-23-5-75-27-4-78-87-5-10061-01 79-01-6-124-48-1 79-00-5-71-43-2-10061-02 75-25-2-108-10-1 591-78-6 127-18-4 79-34-5-108-88-3 108-90-7 100-41-4 100-42-5 1330-20-

— Chlorome thane - Bromomethane

Vinyl Chloride Chloroethane •Methylene Chloride •Acetone •Carbon Disulfide 1,1-Dichloroethene 1,1-Dichloroethane 1,2-Dichloroethene (total Chloroform 1» 2-Dichloroethane 2-Butanone 1/1/1-Trichloroethane Carbon Tetrachloride Bromodichloromethane_ 1,2-Dichloropropane

- 5 cis-1,3 -Dichloropropene Trichloroethene Dibromochl or omethane 1 / 1 / 2 -Trichloroethane Benzene

-6 trans -1,3-Dichloropropene Bramoform 4-Methyl-2 -Pentanone 2-Hexanone -Tetrachloroethene •1,1,2,2-Tetrachloroethane •Toluene Chlorobenzene Ethylbenzene Styrene

7 Xylene (total)

18 18 18 18 9 18 9 14 4 9 9 9 18 250 18 9 9 9 57 9 9 9 9 9 18 18 20 9 9 9 9 9 9

Q

FORM I VOA 3/90

VOLATILE ORGAN!CS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS

•tSPA SAMPLE NO.

MWP3007 Lab Name: AQUATEC, INC. Contract: 94249

Lab Code: AQUA! Case No.: NHBA6 SAS No.: SDG No.: 50557












Dilution Factor: 1 . 9



CAS NUMBER

1. 2 . ' 3. 4.' 5.' 6 . ' 7. 8 . ' 9."

10." 11.' 12."

13." 14." 15." 16."

17." 18." 19." 20 . " 21." 22 . " 23." 24. 25." 2 6 . " 27. 2 8 . 29. 30.


FORM I VOA-TIC 3/90

EPA SAMPLE NO. 1A ^ VOLATILE ORGANICS ANALYSIS DATA SHEET









CAS NO. COMPOUND






Soil Aliquot Volume: _(uL)


74-87-3 74-83- 9 75-01- 4 75-00-3-75-09-2 Methylene Chloride 67-64-1 - —Acetone

•Chloromethane •Bromomethane •Vinyl Chloride Chloroethane

75-15-0 Carbon Disulfide 75-35-4 1,1 -Dichloroethene 75-34-3— i, l-Dichloroethane" 540-59-0 1,2 -Dichloroethene" 67-66-3 -Chloroform 107-06-2 1,2 -Dichloroethane 78-93-3

total;

• 2-Butanone 71-55-6 1/1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bramodichloramethane 78-87-5 1 , 2 - Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01-6 Trichloroethene 124 -48-1 Dibromochlorcmethane 79-00-5 --1,1, 2-Trichloroethane" 71-43-2 Benzene 10061-02-6-- - — trans-1,3-Dichloropropene 75-25-2 Bromoform 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2 - Tetrachloroe thane 108-88-3 Toluene 108-90-7 - Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 1330-20-7

Styrene •Xylene ; total

10 10 10 10 5 10 5 5 3 5 5 5 10 48 5 5 5 5 29 5 5 5 5 5

10 10 11 5 5 5 5 5 5

FORM I VOA 3/90


SFA SAMPLE NO.

MWP6012 Lab Name: AQUATEC, INC. Contract: 94249


Matrix: (soil/water} WATER












Soil Aliquot Volume: (uL


CAS NUMBER

1. 2. 3. 4. 5. 6 . 7.

9. 10. 11.' 12.' 13.' 14.' 15.' 16." 17." 18."

19." 2 0 . " 21." 2 2 . "

23." 24." 25." 26." 27." 2 8 . 29. 30.


FORM I VOA-TIC 3/90

1A VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.

Lab Name: AQUATEC, INC.

Lab Code: AQUAI Case No.: NHBA6







Contract: 94249 TB1041095

CAS NO. COMPOUND

74-87-3-74-83-9-75-01-4-75-00-3-75-09-2-67-64-1-75-15-0-75-35-4-75-34-3-540-59-0 67-66-3-107-06-2 78-93-3-71-55-6-56-23-5-75-27-4-78-87-5-10061-01 79-01-6-124-48-1 79-00-5-71-43-2-10061-02 75-25-2-108-10-1 591-78-6 127-18-4 79-34-5-108-88-3 108-90-7 100-41-4 100-42-5 1330-20-

•Chloromethane • Bromomethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1/1-Dichloroethene 1,1-Dichloroethane" 1,2-Dichloroethene"

— Chloroform 1 , 2 -Dichloroethane 2-Butanone

! total

1,1,1-Trichloroethane Carbon Tetrachloride Bromodichlorcmethane' 1,2-Dichloropropane

"5 cis -1,3- Dichloropropene Trichloroethene Dibrcanochl oromet hane 1 , 1 , 2 -Trichloroethane Benzene

-6 rans-1, 3-Dichloropropene Bromoform 4'-Methyl - 2 - Pentanone 2-Hexanone Tetrachloroethene 1,1,2,2-Tetrachloroethane Toluene

--Chlorobenzene Ethylbenzene Styrene

7 Xylene (total

SAS No.: SDG No.: 50557



Date Received: 04 /14 /95

pate Analyzed: 04/19/95

Dilution Factor: 1 .0



FORM I VOA 3/90


bAMPbti NO

TB1041095 Lab Name: AQUATEC, INC. Contract: 94249







Soil Extract Volume: _JuL)









CAS NUMBER

1. 2. 3. 4.' 5.' 6. 7.' 8 . '

9.' 10.' 11." 12."

13." 14." 15." 16."

17." 18." 19." 20 . " 21." 22 . " 23." 24." 25." 2 6 . 27. 2 8 . 29. 30.


FORM I VOA-TIC 3/90










CAS NO. COMPOUND

Lab Sample ID: VBLKU4

Lab File ID: MCLB001WV.D

Date Received: / /




CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L q

74-87-3 Chlorome thane 74-83-9 Bromcmethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Di chloroethene 75-34-3 — 1 ,1-Dichloroethane 540-59-0 — 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2 - Dichloroethane 78-93-3 -2 - Butanone 71-55-6 1,1,1-Trichloroe thane 56-23-5 Carbon Tetrachloride 75 -27-4 Bromodichloromethane" 78-87- 5 1 ,2 - Dichloropropane 10061 - 01-5 cis -1, 3 - Di chloropropene 79-01-6 — Trichloroethene 124-48-1 Dibromochl or cme thane 79-00-5 1 ,1,2-Trichloroethane" 71-43-2 Benzene 10061 -02 -6 trans-l, 3-Dichloropropene 75-25-2 - -Bromoform 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 127-18-4 Te trachl or oe thene 79-34-5 1,1,2,2 - Tetrachloroe thane 108-88-3 Toluene 108-90-7 100-41-4 100-42-5 1330-20-7

•Chlorobenzene -Ethylbenzene^ • Styrene •Xylene (total)

FORM I VOA 3/90


EPA SAMPLE NO.

VBLKU4 Lab Name: AQUATEC, INC. Contract: 94249



Sample wt/vol: 5.0 <g/mL) ML








Date Received: / /



Soil Aliquot Volume: (uL}


CAS NUMBER

1. 2. 3. 4. 5. 6 . 7.

9. 10.'

11." 12.' 13.' 14.' 15.' 16.' 17.' 18." 19." 20 . " 21." 22 . " 23.* 24." 25.' 26.' 27." 2 8 . " 29." 30.


FORM I VOA-TIC 3/90

VOLATILE ORGANICS ANALYSIS DATA SHEET c-fa JNU.









CAS NO. COMPOUND


Lab File ID: MCLB001XV.D

Date Received: / /





74-87-3 Chlorome thane 74-83- 9 Br omamethane 75-01- 4 Vinyl Chloride 75-00-3— Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1- Dichloroethene 75-34-3 1,1- Dichloroethanej 540-59-0- 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2- Di chloroethane 78-93-3 2 - Bu tanone 71-55-6 i,i, 1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichl oranethane* 78-87-5 - --1,2 -Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01- 6 Trichloroethene 124-48-1 Dibromochlorctne thane 79-00-5 1,1,2 - Trichloroethane" 71-43-2 Benzene 10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromoform 108-10-1 4 - Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 127-18-4 Tet rachl oroe thene 79-34-5 1,1,2,2 - Tet rachl oroethane 108-88-3 Toluene 108-90-7 - Chlorobenzene 100-41-4 100-42-5 1330-20-7

•Ethylbenzene •Styrene •Xylene total

FORM I VOA 3/90


oni'iTLID J.NVJ











Lab File ID: MCLB001XV.D

Date Received: / /





CAS NUMBER

1. 2 . 3. 4. 5. 6 . 7.

9. 10.' 11." 12.' 13." 14." 15." 16."

17." 18.' 19." 20." 2 1 . "

22 . " 23." 24." 25. 2 6 . 27. 2 8 . 29. 30.


FORM I VOA-TIC 3/90

Ci-fM JNU j - r t .

VOLATILE ORGANICS ANALYSIS DATA SHEET





Level: {1 ow/med) LOW

% Moisture: not dec. '



Lab Sample ID: 253072MS

Lab File ID: M253072DMSV.D






74-87-3 —Chlorome thane 74-83- 9 Bromomethane 75-01- 4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 -Acetone 75-15-0 •Carbon Disulfide 75-35-4 1,1- Dichloroethene 75-34-3 -l, 1 -Di chloroethane 540-59-0 1,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2-Di chloroethane 78-93-.3 2 - Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Brcmodichloromethane 78-87-5 1,2 - Dichloropropane m n c i . m . c . c 10061-01-5 cis-1,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 71-43-2

1,1,2-Trichloroethane •Benzene

10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromoform 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 12 7 -18-4 Tetrachloroethene_ 79-34-5 1,1,2,2 - Tetrachloroe thane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene ~ 1330-20-7 •Xylene (total)

25 25 25 25 12 25 12

110 12 12 12 12 25 380 25 12 12 12 140 12 12 120 12 12 25 25 4 12 120 120 12 12 12:

Q

FORM I VOA 3/90

cjfrt. o>uvlf J_i£i JNU VOLATILE ORGANICS ANALYSIS DATA SHEET

Lab Name: AQUATEC, INC. ~ Contract: 94249








Lab Sample ID: 253072MD

Lab File ID: M253072DMDV.D





CAS NO COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L

74-87-3-- Chlorome thane 74-83- 9 Bromamethane 75-01- 4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 6/-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1- Di chl oroe thene 75-34-3 l, 1-Dichloroethane 540-59-0 l, 2 -Dichloroethene (total) 67-66-3 Chloroform

1,1,1-Trichloroethane Carbon Tetrachloride

107-06-2-- -1,2-Dichloroethane 78-93-3 2-Butanone 71-55-6 56-23-5 75- 27-4 Brcmodichloromethane 78-87- 5 1,2 - Dichloropropane 10061-01-5 cis-1, 3-Dichloropropene 79-01-6 — Trichloroethene 124-48-1 Dibromochl oromet hane 79-00-5 1,1,2 -Trichloroethane 71-43-2 Benzene 10061-02-6 trans-1,3-Dichloropropene 75-25-2 _— Bramof orm 108-10-1 4 -Methyl -2 - Pentanone 591-78-6 2-Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2 - Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene (total)

25 25 25 25 12 25 12

130 12 12 12 12 25 390 25 12 12 12 140 12 12 120 12 12 25 25 8 12 120 130 12 12 12

Q

FORM I VOA 3/90

SAMPLE DATA SUMMARY PACKAGE LAB CODE:

CASE NO.: /J SDGNO.: Sri *^6,

CONTRACT NO.:

INCHCAPE TESTING SERVICES AQUATEC LABORATORIES

Inchcape Testing Services 35 South Park Drive

Colchester, VT 05446

Tel. 802-655-1203

Fax. 802-655-1248 Aquatec Laboratories

April 28, 1995

Mr. Steve Dishong Hull & Associates, Inc. 360901 Pinetree Place Route 101 Bedford, NH 03110

RE: Project NHBB Superfund Site ITS-Aquatec Project No. 94246 Case No. NHBA6; SPG 50556

Dear Mr. Dishong:

Enclosed are the analytical results for the samples received intact by Inchcape Testing Services-Aquatec Laboratories on April 14, 1995. Laboratory numbers and quality control samples were assigned as follows:

Client Sample ID

Laboratory Number

Sample Matrix

Samples Received on April 14, 1995 ETR No. 50556

EXH3013 EX1013

253047 253048

Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water Water

EX1013MS EX1013MSD EX4013 253049

253050 253051 253052 253053 253054 253055 253056 253057 253058 253059 253060 253061 253062 253063 253064 253065 253066 253067

253048MS 253048MD

EX5A013 EX6013 EX7013 EX9013 FB1041095 FB1041195 FB1041295 H2U014 H107U009 MWEM2016 MWEM3L015 MWEM3U016 109016 H105M008 MWGZ3R004 MWGZ3R004A MWGZ4R006 HB

Mr. Steve Dishong April 28, 1995 page 2

For the benefit of interested parties, documentation of sample handling and preparation is included at the end of the Sample Data Package. A colored sheet of paper entitled "Sample Preparation Package and Sample Handling" has been used to explicitly mark the location of these documents.

If there are any questions or clarifications regarding this submittal, please contact your Project Director, Scot Swanborn (802) 655-1203.

Sincerely,

Karen R. Chirgwin Laboratory Operations Director

KRC/lml

Enclosure

942 4 6B2 7APR9 5


EPA SAMPLE NO.









SDG No.: 50556





Dilution Factor: .1.0



74-87-3-74-83-9-75-01-4-75-00-3-75-09-2-67-64-1-75-15-0-75-35-4-75-34-3-540-59-0 67-66-3-107-06-2 78-93-3-71-55-6-56-23-5-75-27-4-78-87-5-10061-01 79-01-6-124-48-1 79-00-5-71-43-2-10061-02 75-25-2-108-10-1 591-78-6 127-18-4 79-34-5-108-88-3 108-90-7 100-41-4 100-42-5 1330-20-

Chloromethane_ Bromomethane Vinyl Chloride Chloroethane

---Methylene Chloride Acetone Carbon Disulfide 1,1-Dichloroethene 1,l-Dichloroethane 1/2-Dichloroethene (total) Chloroform 1,2-Dichloroethane 2-Butanone 1/1,1-Trichloroethane Carbon Tetrachloride^ Bromodichloromethane 1,2-Di chloropropane

-5 cis -1,3 -Dichloropropene Trichloroethene •Dibromochloromethane_ •1,1,2-Trichloroethane •Benzene

-6 trans -1,3- Di chloropropene Bromoform 4-Methyl-2 -Pentanone 2-Hexanone •Tetrachloroethene 1,1,2,2-Tetrachloroethane Toluene

- - Chlorobenzene_ Ethylbenzene

— Styrene 7 Xylene (total

10 10 10 10 5 10 5 5 5 3 5 5

10 39 5 5 5 5

68 5 5 5 5 5 10 10 94 5 5 5 5 5 5

FORM I VOA 3/90



Lab Code: AQUAI Case No. : NHBA6 SAS No. :







EPA SAMPLE NO.

EXH3013

SDG No.: 50556








CAS NUMBER

1. 76-13-1 2 . 3. 4 . 5. 6 . 7. 8 . 9. 10 . 11. 12 . 13 . 14 . 15. 16 . 17. 18. 19. 2 0 . 21. 2 2 . 23. 24 . 25. 26 . 27 . 28 . 29 . 30.

COMPOUND NAME

Ethane, 1,1,2-trichloro-l,2,

RT

4.382

EST. CONC.

320 NJ

FORM I VOA-TIC 3/90

LA VOLATILE ORGANICS ANALYSIS- DATA SHEET

EPA SAMPLE NO.


Lab Code: AQUAI Case No. : NHBA6







CAS NO. COMPOUND

Contract: 94246

SAS No.: SDG

Lab Sample ID







EX1013

No.: 50556

: 253048

74-87-3 Chi orome thane 74-83-9 Bromome t hane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 -—Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1- Dichloroethene 75-34-3 1,1- Di chloroethane" 540-59-0 l, 2 - Dichloroethene" 67-66-3 Chloroform

total)

107-06-2 1,2 - Di chloroethane 78-93-3 2-Butanone 71-55-6 1,1, l-Trichloroethane_ 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichloromethane 78-87-5 1, 2-Dichloropropane 10061-01-5 -cis-1,3-Dichloropropene 79-01-6 Trichioroethene ~ 124-48-1 Dibr omochl orome thane 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene 10061-02-6 trans-1,3-Di chloropropene 75-25-2 -—Bromoform 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2-Hexanone 12 7-18-4 Tetrachloroethene 79-34-5 1,1,2,2 - Tetrachloroethane 108 - 88-3 Toluene ~ 108-90-7 Chi orobenz ene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene (total)___

170 170 170 170 84 170 84 84 84 84 84 84 170 500 84 84 84 84 160 84 84 84 84 84 170 170

2800 84 84 84 84 84 84

FORM I VOA 3/90


EPA SAMPLE NO.

EX1013 Lab Name: AQUATEC, INC. Contract: 94246
















CAS NUMBER

1. 2 . 3. 4 . 5. 6 . 7. 8 . 9. 10 . 11. 12. 13. 14. 15. 16. 17. 18. 19. 2 0 . 21. 2 2 . 23. 24 . 25. 2 6 . 27. 2 8 . 29. 30.


FORM I VOA-TIC 3/90




Matrix: (soil/water) WATER V






CAS NO. COMPOUND








74- 87-3 Chlorome thane 74-83- 9 Bromomethane 75-01- 4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 75-35-4 75-34-3

•Carbon Disulfide • 1,1-Dichloroethene •1,1-Dichloroethane"

540-59-0 1,2 -Dichloroethene" 67-66-3 - Chloroform

[total

107-06-2 1/ 2-Dichloroethane 78-93-3- 2-Butanone 71-55-6 l, l, 1-Trichloroethane 56-23-5 Carbon Tetrachloride^ 75-27-4 Bromodi chl orcme thane 78-87-5 — 1,2-Di chloropr opane 10061 -01-5 cis-1, 3-Dichloropropene 79-01-6 Trichloroethene

Dibranochlorcmethane 124-48-1 79-00-5 1,1,2 - Trichloroethane 71-43-2 Benzene 10061-02-6 trans -1,3- Dichloropropene 75-25-2 Bromof orm 108-10-1 4 - Methyl -2 - Pentanone 591-78-6 2 - Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene_ 100-41-4 Ethylbenzene 100 - 42 - 5 Styrene ~~ 1330-20-7 Xylene (total

10 10 10 10 5 10 5 5 5 5 5 5 10 12 5 5 5 5 4 5 5 5 5 5 10 10 11 5 5 5 5 5 5


FORM I VOA 3/90


EPA SAMPLE NO.

















CAS NUMBER

1. 2 . 3 . 4 . 5. 6 . 7. 8 . 9 . 10 . 11. 12 . 13 . 14. 15. 16 . 17. 18. 19 . 2 0 . 21. 2 2 . 23. 24. 25. 26 . 27. 28. 29. 30.


FORM I VOA-TIC 3/90


EPA SAMPLE NO.

EX5A013 Lab Name: AQUATEC, INC. Contract: 94246





% Moisture: not dec. ,




74-87-3 Chlorome thane 74- 83-9 Bromamethane 75-01- 4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 -—Methylene Chloride 67-64-1 Acetone 75-15-0-- Carbon Disulfide " 75-35-4 1,1- Dichloroethene_ 75-34-3 1,1- Dichloroethane 540-59-0 1,2 -Dichloroethene (total; 67-66-3 Chloroform 107-06-2 1,2 - Dichloroethane 78-93-3 2 - Bu tanone 71-55-6— 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichloromethane 78-87-5 1,2- Di chloropropane 10061-01-5 cis -1, 3-Dichloropropene 79-01-6 Trichloroethene " 124 -48-1- Dibromochloromethane 79-00-5 1,1,2-Trichloroethani 71-43-2 Benzene 10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromoform " 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2 -Hexanone 127-18-4 - Te t rachl or oe thene 79-34-5 1,1,2,2 -Tetrachloroethane 108-88-3 Toluene 108-90-7 100-41-4 100-42-5 1330-20-7

•Chlorobenzene •Ethylbenzene • Styrene •Xylene (total)

10 10 10 10 5 10 5 1 1 5 5 5

10 17 5 5 5 5 9 5 5 5 5 5 10 10 4 5 5 5 5 5 5

Q

U U U U u u u J J u u u u

u u u u u u u J u u u u u u







FORM I VOA 3/90


EPA SAMPLE NO.

EX5A013 Lab Name: AQUATEC, INC. Contract: 94246















CONCENTRATION UNITS: • (ug/L or ug/Kg) UG/L

CAS NUMBER

1 . 2 . 3 . 4 . 5 . 6 . 7 . 8 . 9 . 10 . 11 . 12 . 13 . 14 . 15 . 16 . 17 . 18 . 19 . 20 . 21 . 22 . 23 . 24 . 25 . 26 . 27 . 2 8 . 29 . 30.

COMPOUND NAME RT EST. CONC

FORM I VOA-TIC 3/90







% Moisture: not dec. __









CAS NO COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L

74-87-3 Chlorome thane 74-83-9 —Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1-- Acetone 75-15-0 Carbon Disulfide 75-35-4 1 ,1 - Dichloroethene 75-34-3 1,1- Dichloroethane 540-59-0 1,2 - Dichloroethene" 67-66-3 Chlorof om 107-06-2 1,2 -Dichloroethane 78-93-3 2-Butanone

total)

71-55-6 l, l, l-Trichloroethane 56-23-5 Carbon Tetrachloride 75- 27-4 Brcmodichloromethane 78-87-5 — 1,2-Dichloropropane 10061 -01-5 cis-1, 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 l, l, 2-Trichloroethane" 71-43-2 Benzene 10061-02-6 trans -1, 3- Dichloropropene 75-25-2 Bromof orm_ " 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 127-18-4 Te t rachl oroe thene 79-34-5 1,1,2,2 - Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100 - 41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene (total)

10 10 10 10 5 10 5 5 5 5 5 5

10 52 5 5 5 5 4 5 5 5 5 5 10 10 1 5 5 5 5 5 5

Q


u u u u J u u u u u u u J u u u u u u

FORM I VOA 3/90


Lab Name: AQUATEC, INC. Contract: 94246 '








EPA SAMPLE NO.

EX6013

SDG No.: 50556








CAS NUMBER

1 . 2 . 3 . 4 . 5 . 6 . 7 . 8 . 9 . 10 . 11 . 12 . 13 . 14 . 15 . 16 . 17 . 18 . 19 . 2 0 . 21 . 22 . 23 . 24 . 25 . 2 6 . 27 . 2 8 . 29 . 30.

COMPOUND NAME RT EST. CONC Q

FORM I VOA-TIC 3/90




Matrix: (soil/water) WATER.

Sample wt/vol:'""^' 5.0 (g/mL) ML


% Moisture: not dec. .

GC Column:CAP ID.; 0.53 (mm) , •

Soil Extract Volume: (up

CAS NO. COMPOUND








74-87-3-74-83-9-75-01-4-75-00-3-75-09-2-67-64-1-75-15-0-75-35-4-75-34-3-540-59-0 67-66-3-107-06-2 78-93-3-71-55-6-56-23-5-75-27-4-78-87-5-10061-01 79-01-6-124-48-1 79-00-5-71-43-2-10061-02 75-25-2-108-10-1 591-78-6 127-18-4 79-34-5-108-88-3 108-90-7 100-41-4 100-42-5 1330-20-

- - -Chloromethane_ Bromomethane Vinyl Chloride Chloroethane Methylene Chloride Acetone Carbon Disulfide 1,1-Dichloroethene

— 1,1- Dichloroethane" 1,2-Dichloroethene" Chloroform

: total

1,2-Dichloroethane 2-Butanone 1,1,1-Trichloroethane Carbon Tetrachloride

—Bromodichloromethane 1,2-Dichloropropane

-5 cis-l,3-Di chloropropene Trichloroethene Dibrcmochlorcmethane_ 1,1,2-Trichloroethane Benzene

-6 trans -1,3 -Di chloropropene Brcmoform. 4-Methyl-2 -Pentanone 2-Hexanone •Tetrachloroethene 1,1,2,2-Tetrachloroethane Toluene Chlorobenzene Ethylbenzene Styrene

7 Xylene (total)

10 10 10 10 5 10 5 5 5 5 5 5 10 12 5 5 5 5 4 5 5 5 5 5 10 10 4 5 5 5 5 5 5

FORM I VOA 3/90


















CAS NUMBER

1. 2. 3.' 4.' 5.' 6 . '

7.' 8 . '

9.' 10."

11." 12." 13." 14." 15." 16." 17." 18."

19." 2 0 . " 21." 2 2 . 23. 24. 25. 26. 27. 2 8 . 29. 30.


FORM I VOA-TIC 3/90

1A VOLATILE ORGAN!CS ANALYSIS DATA SHEET

EPA SAMPLE NO.


Lab Code: AQUAI Case No.: NHBA6 SAS No. : SDG No. : 50556














74- 87-3 Chloromethane ^ 74-83- 9 Bromomethane \ 75-01- 4 Vinyl Chloride ^ 75-00-3 Chloroethane 3 75-09-2 Methylene Chloride M 67-64-1 Acetone 33 75-15-0 Carbon Disulfide 1 7 7 5 - 3 5 - 4 l, 1-Dichloroethene 1 7 75-34-3 i, l-Dichloroethane 17 540-59-0 1,2-Dichloroethene (total) 1 7 67-66-3 Chloroform 1 7 107-06-2 -1, 2-Dichloroethane 1 7 78-93-3 2-Butanone 33 71-55-6 --1/1,1-Trichloroethane 530 56-23-5— Carbon Tetrachloride 17 7 5 - 2 7 - 4 Bromodichloromethane i 7

78-87- 5 1,2 -Dichloropropane 17 10061-01-5 cis-1,3-Dichloropropene 1 7 79-01- 6 Trichloroethene_ 2 2

1 2 4 - 4 8 - 1 - Dibromochloromethane 1 7 79-00-5 1,1,2-Trichloroethani 1 7 71-43-2 Benzene 17 10061-02-6 trans-1,3-Dichloropropene 1 7 I T

75-25-2 Brcmoform 17 ^ 108-10-1 4-Methyl - 2 - Pentanone 33 n 591-78-6 2 - Hexanone 33 y 127-18-4 Tetrachloroethene 16 j 79-34-5 1 , 1 , 2 , 2 - Tetrachloroethane 1 7 t t 108-88-3 Toluene 17 y 108-90-7 Chlorobenzene 17 n 100-41-4 Ethylbenzene 1 7 T T

100-42-5 Styrene 17 tt 1330-20-7 Xylene (total)

FORM I VOA 3/90

-LCj VOi^LE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS

QfH SAMPLE NO.

EX9013 Lab Name: AQUATEC, INC rv. _ Am... Contract: 94246

Lab Code: AQUA1 Case No.: NHBA6 SAS No.: SDG No.: 50556


Sample wt/vol: 5.0 (g/mIj)



GC Column:CAP iD: 0.53 (mm)

Soil Extract Volume: (ul)




Date Received: O4/14 /95


Dilution Factor: 3 .3



CAS NUMBER

1. 2 . ' 3.' 4.' 5." 6 . " 7.' 8 . " 9."

10." 11." 12." 13." 14. 15. 16. 17. 18. 19. 2 0 . 21. 22. 23. 24. 25. 2 6 . 27. 2 8 . 29. 30.


FORM I VOA-TIC 3/90


EPA SAMPLE NO.









SDG No.: 50556








74-87-3--74-83-9--75-01-4--75-00-3--75-09-2--67-64-1--75-15-0--75-35-4--75-34-3--540-59-0-67-66-3--107-06-2-78-93-3--71-55-6--56-23-5--75-27-4--78-87-5--10061-01-79-01-6'--124-48-1-79-00-5--71-43-2--10061-02-75-25-2--108-10-1-591-78-6-127-18-4-79-34-5--108-88-3-108-90-7-100-41-4-100-42-5-1330-20-7

Chloromethane_ Bromome thane

- Vinyl Chloride Chloroethane Methylene Chloride

— Acetone •Carbon Disulfide 1,l-Dichloroethene 1,1-Dichloroethane" 1,2-Dichloroethene (total) Chloroform 1 f 2-Dichloroethane 2-Butanone 1,1,1-Trichloroethane Carbon Tetrachloride Bromodichloromethane" 1,2-Dichloropropane

5 cis -1,3- Dichloropropene Trichloroethene Dibramochloromethane_ l,1,2-Trichloroethane Benzene

6 trans -1,3- Dichloropropene - = . Bromoform

4-Me thyl-2 -Pentanone 2-Hexanone Tet rachloroe thene 1,1,2,2-Tetrachloroethane Toluene Chlorobenzene_ Ethylbenzene Styrene Xylene (total

Q

FORM I VOA 3/90


EPA SAMPLE' NO.

FB1041095 Lab Name: AQUATEC, INC. Contract: 94246



Sample wt/vol: 5.0 . (g/mL) ML










Dilution Factor: l.o



GAS NUMBER

1. 2 . 3. 4. 5. ' 6 . 7.

9. 10.'

11.' 12.' 13.' 14.' 15." 16."

17." 18." 19." 20 . " 21."

2 2 . " 23." 24." 25." 2 6 . " 27. 2 8 . 29. 30.


FORM I VOA-TIC 3/90





Sample wt/vol: 5.0 (g/mL) m



GC Column:CAP iD: 0.53 (mm)


FB1041195

SDG No.: 50556






Soil Aliquot Volume: (UL)


Zf ~?Z"?— Chloromethane Z5~??~9 Bromomethane 75-01-4 Vinyl Chloride Zl~ 99"9 Chloroethane Z:2~9?~2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide Zl'l*'* 1'1" Dichloroethene"

1/ 1-Dichloroethane" -1,2-Dichloroethene~

67-66-3 - -Chloroform *97~ !?6 ~2 1 > 2 -Dichloroethane 78-93-3 2-Butanone

total

Zi"ff"f 1'1' 1_Trichloroethane n t n n A Carbon Tetrachloride " /b~z 7-4 Bromodichloromethane 1006? ni q i:2-Dichloropropane *0061-01-5 cis-l,3-Dichloropropene^ 7? T -16 Tnchloroethene l24"48"1 Dibromochloromethane Z? ~ 9? ~ l'1'2-Trichloroe thane /1-43-2 Benzene — ^°°®y°2"6 trans-1, J-Dichloropropene 75l25"2 Bromoform

"" • "ethyl - 2 - Pentanone 591-78-6 2 -Hexanone 127-18-4 •Tetrachloroethene 7Za3p~5: l»l,2f2-Tetrachloroethane iua-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 --Styrene -1330-20-7---- — •Xylene (total

10 10 10 10 5 10

10 5 5 5 5 5 5 5 5 5 5 5 10 10 5 5 5 5 5 5 5

U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u

FORM I VOA 3/90


EPA SAMPLE NO.

















CAS NUMBER

1. 2 . 3. 4. 5. 6 . 7. 8 . 9. 10 . 11. 12. 13. 14 . 15. 16 . 17. 18 . 19. 20. 21. 22. 23. 24 . 25. 26 . 27. 28. 29. 30.


FORM I VOA-TIC 3/90



Lab Code: AQUAI Case No. : NHBA6


Sample wt/vol: = n / / r, 5-0 (g/mL) ML



GC Column: CAP ID: 0 53 {mn)

Soil Extract Volume: (u£l)

Contract: 94246

SAS No.:

FB1041295'

CAS NO.

74-87-3 74-83-9 75-01-4

COMPOUND

Chlorome thane Bromomethane

SDG No.: 50556





Dilution Factor: l.o

• Soil Aliquot Volume: (uL)

CONCENTRATION UNITS • (ug/L or ug/Kg) UG/L q

' • Vinyl Chloridi" Chloroethane " —

67-64-1 Methylene ChlHHdi nL I Acetone 75.35.4 Carbon Disulfide" 75.34 _ 3 ?" ~Pichloroethene 540-59-0------- ^'o"n*C^°r0ethaneIIZlI 67-66-3 i/2-Dichloroethene (total) 107-n^.o ""-Chloroform 7a.q^ -5 1»2-Dichloroethane 71 .cil] 2"Bu tanone 56-23-5 _~"i' 1C1"Tricn-Loroethane * 75-27-4 I" ~£arbon. Tetrachloride

ne 78-87-5 Brcmodichlorometha-.^

10061-01-5 - - - 11 "rir?1^?.??rppane -

61::::::: — 79-00-5 Dibromochloromethane 71 -43°-25- -:::::: :kn4enrichloroethani==

591 - va - 6—.:: V- onf5iHESH5Hi=Lc=

Tetrachloroethene

108-88-3 - - - - - - - -Tol/^n1"Tetrachlor°ethane lotll ' l Chlorobenzeni ~~~ loo'tl'i Ethylbenzene ' 1330-20-7 StyrSne ~

Xylene (total)

10 10 10 10 5 10 5 5 5 5 5 5 10 5 5 5 5 5 5 5 5 5 5 5

10 10 5 5 5 5 5 5 5

U| ul Ui ui Ul ul Ui ul u| ui ul Ul ui ul ul U| ul Ui Uj ul ul Ul ul Ui u l ul Ui ul ul Ul ul Ui u i

FORM I VOA 3/90


iNU




Sample wt/vol: 5.0 {g/mL)



GC Coluirtn:CAP iD: 0.53 (mm)










CAS NUMBER

1. 2. 3.' 4.' 5.' 6 . ' 7.' 8 . " 9."

10."

11.' 12."

13." 14. 15." 16. 17. 18. 19. 2 0 . 21. 2 2 . 23. 24. 25. 2 6 . 27. 2 8 . 29. 30.

COMPOUND NAME RT EST. CONC

FORM I VOA-TIC 3/90


EPA SAMPLE NO.

H2U014 Lab Name: AQUATEC, INC. Contract: 94246















74-87-3 - -Chlorome thane 74-83- 9 Bromomethane 75-01-4- - Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0-- Carbon Disulfide 75-35-4 l, 1-Dichloroethene 75-34-3 l, 1-Dichloroethane 540-59-0 1,2 -Dichloroethene (total 67-66-3 Chloroform 107-06-2 1,2-Di chloroethane 78-93-3 2 - Butanone 71-55-6 1,1, l-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichloromethane" 78-87- 5 1 2-Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01- 6 Tr i chl oroe thene 124-48-1 Dibromochlorcmethane 79-00-5 1,1,2-Trichloroethane" 71-43-2 Benzene 10061-02-6 trans -1,3- Dichloropropene 75-25-2 Brcmoform 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 12 7 -18- 4 Tetrachloroethene 79-34-5 1,1,2,2 - Tetrachloroethane 108-88-3 Toluene 108-90.-7 Chl orobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 --Xylene (total)

FORM I VOA 3/90


QfA b AMPLE NO.









H2U014

SDG No.: 50556







Number TICs found: 0 CONCENTRATION UNITS : (ug/L or ug/Kg) UG/L

CAS NUMBER

1. 2 . ' 3.' 4.' 5.' 6 . ' 7.' 8 . '

9.' 10."

11." 12.' 13." 14." 15." 16." 17." 18." 19." 20 . " 21."

22 . " 23." 24. _ 25. 2 6 . " 27. 2 8 . 29. 30.


FORM I VOA-TIC 3/90










CAS NO; COMPOUND







CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L o

74- 87-3 Chlorome thane 74-83- 9 Bramomethane 75-01- 4 -Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide_ 75-35-4 1,1- Di chloroe thene 75-34-3 --1,1-Dichloroethane 540-59-0 1,2 -Dichloroethene (total) 67-66-3 Chloroform 107-06-2 —1,2- Dichloroe thane 78-93-3 2 - Butanone 71-55-6 1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichloromethane 78-87-5 1,2 - Dichloropropane 10061-01-5 - cis-1,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene 10061-02- 6 trans -1,3 - Dichloropropene 75-25-2 Bromoform " 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2 -Hexanone 127-18-4 Tetrachloroe thene 79-34-5 1,1,2,2 - Te t rachl oroe thane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 100-42-5 1330-20-7

• Ethylbenzene •Styrene Xylene total

17 17' 17 17

8 17

8 5 5 8 8 8 17

220 8 8 8 8

16 8 8 8 8 8

17 17 10

8 8 8 8 8 8

U U U u u u u J J u u u u

FORM I VOA 3/90


iiFA SAMPLE NO.

H107U009 Lab Name: AQUATEC, INC. Contract: 94246

Lab Code: AQUAI Case No.: NHBA6 SAS No.: SDG NO.: 50556















CAS NUMBER

1. 2 . 3. 4. 5. 6 . 7.

9. 10.' 11.' 12.' 13.' 14.' 15." 16." 17." 18."

19." 2 0 . ' 21."

22." 23." 24." 25." 2 6 . " 27." 2 8 . " 29." 30."


FORM I VOA-TIC 3/90


EPA SAMPLE NO.

MWEM2016 Lab Name: AQUATEC, INC. Contract: 94246









74-87-3-74-83-9-75-01-4-75-00-3-75-09-2-67-64-1-75-15-0-75-35-4-75-34-3--540-59-0-67-66-3--107-06-2-78-93-3--71-55-6- -56-23-5--75-27-4--78-87-5--10061-01-79-01-6- -124-48-1-79-00-5- -71-43-2- -10061-02-75-25-2--108-10-1-591-78-6-127-18-4-79-34-5--108-88-3-108-90-7-100-41-4-100-42-5-1330-20-7

Chioromethane Brcmomethane Vinyl Chloride Chloroethane Methylene Chloride •Acetone Carbon Disulfide 1,1-Dichloroethene 1,1-Dichloroethane" 1,2-Dichloroethene (total) Chloroform 1,2-Dichloroethane 2-Butanone 1,1, l-Trichloroethane_ Carbon Tetrachloride Bromodichloramethane" 1,2-Dichloropropane

5 cis -1,3- Dichloropropene Trichloroethene

- Dibromochl orome thane 1,1,2-Trichloroethani" Benzene

6 trans -1,3 - Dichloropropene — Bromoform

4-Methyl-2 -Pentanone 2-Hexanone Tetrachloroethene 1,1,2,2-Tetrachloroethane Toluene •Chlorobenzene_ -Ethylbenzene • Styrene •Xylene (total

Q







FORM I VOA 3/90


EPA SAMPLE NO.

MWEM2016 Lab Name: AQUATEC, INC. Contract: 94246
















CAS NUMBER

1. 2. 3. 4.' 5.' 6/ 7.' 8 . ' 9.' 10.'

11." 12." 13." 14." 15." 16."

17." 18."

19.* 2 0 . * 21." 2 2 . 23." 24." 25. 2 6 . " 27. 28. 29. 30.


FORM I VOA-TIC 3/90

-LM.

VOLATILE ORGANICS ANALYSIS DATA SHEET JiFA SAMPLE NO


Lab Code: AQUAI Case No.: NHBA6 SAS No. : SDG No. : 50556







CAS NO. COMPOUND







CONCENTRATION UNITS : (ug/L or ug/Kg) UG/L Q

74-87-3 Chlorome thane 74-83-9 — Bromomethane 75-01- 4 Vinyl Chloride^ 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 --Carbon Disulfide 75-35-4 1,1-Dichloroethene 75-34-3 1,1-Dichloroethane" 540-59-0 l, 2-Dichloroethene (total 67-66-3 Chloroform 107-06-2 1 ,2 -Dichloroethane 78-93-3 2 - Butanone 71-55-6 1/1,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4-- Bromodichloromethane" 78-87- 5 1,2 - Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01- 6 Trichloroethene ~ 124-48-1 Dibromochlorcmethane 79-00-5 1 ,1,2-Trichloroethane 71-43-2 -Benzene 10061-02-6 trans-1,3-Dichloropropene 75-25-2 Brcatiof orm 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2 - Tetrachloroe thane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 — Ethylbenzene " 100-42-5 Styrene 1330-20-7 Xylene (total)

FORM I VOA 3/90


EPA SAMPLE NO.

MWEM3L015 Lab Name: AQUATEC, INC. Contract: 94246







Soil Extract Volume: _(uL)









CAS NUMBER

1. 2. 3. 4. 5.' 6. 7. 8 . ' 9.'

10.' 11. 12.' 13." 14." 15." 16." 17." 18." 19." 2 0 . " 21." 2 2 . " 23." 24." 25." 2 6 . " 27." 28." 29." 30.


FORM I VOA-TIC 3/90

-LA VOLATILE ORGANICS ANALYSIS DATA SHEET

SPA SAMPLE NO.

MWEM3U016 Lab Name: AQUATEC, INC. Contract: 94246















74-87-3 Chloromethane m n 74-83- 9 Bromome thane 10 U 75-01- 4 Vinyl Chloride TO TT 75-00-3 Chloroethane 10 u 75-09-2 Methylene Chloride q n 67-64-1 Acetone 10 u 75-15-0 --Carbon Disulfide_ 5 u 75-35-4 l, 1-Dichloroethene 5 u 75-34-3 1,1-Dichloroethane 5 y 540-59-0 1,2-Dichloroethene (total) 5 y 67-66-3 Chloroform 5 y 107-06- 2 1,2-Dichloroethane 5 TT 78-93-3-- 2-Butanone 10 U 71-55-6— 1,1,1-Trichloroethane 5 y 56-23-5 Carbon Tetrachloride 5 TT 75-27-4 Bromodichlorcmethane 5 y 78-87-5 — l, 2-Dichloropropane 5 y 10061-01-5 cis-1,3-Dichloropropene 5 y 79-01- 6 Trichloroethene_ 5 y 124-48-1 Dibrcmochloromethane 5 y 79-00-5 1 , l, 2-Trichloroethane 5 IT 71-43-2 Benzene 5 y 10061-02-6 trans-1,3-Dichloropropene 5 y 75-25-2 Brcmoform 5 y 108-10- 1 4- Methyl - 2 - Pentanone 10 IT 591-78-6 2-Hexanone 10 u 127-18 -4 - - Tetrachloroethene 5 y 79-34-5 1,1/2,2-Tetrachloroethane 5 u 108-88-3 Toluene 5 y 108-90-7-- Chlorobenzene 5 y 100-41-4 Ethylbenzene 5 y 100-42-5 Styrene 5 y 1330-20-7 Xylene (total) 5 y

FORM I VOA 3/90


EPA SAMPLE NO.

MWEM3U016 Lab Name: AQUATEC, INC. Contract: 94246
















CAS NUMBER

1. 2. 3.' 4.' 5.' 6 . '

7.' 8 . '

9.' 10.' 11." 12." 13." 14." 15." 16."

17." 18." 19." 2 0 . " 21." 2 2 . " 23." 24." 25." 26 . " 27." 2 8 . " 29." 30."


FORM I VOA-TIC 3/90


C




Sample wt/vol: 5.0 Cg/mL) ML












74-87-3 Chlorome thane 74-83- 9 Bromamethane 75-01- 4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4— i, l-Dichloroethene 75-34-3 1,1- Dichloroethane" 540-59-0 1,2 -Dichloroethene" 67-66-3 Chloroform 107-06-2 l, 2 -Dichloroethane 78-93-3 2-Butanone

total'

71-55-6 l, l, 1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Bromodichloromethane 78-87-5 1,2-Dichloropropane i n n < r i r » i r ^ , t *• 10061-01-5 cis-1,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibromochlorcme thane 79-00-5 l, 1 ,2-Trichloroethane" 71-43-2- Benzene 10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromoform ~ 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 127-18-4 Tetrachloroethene 79-34-5 1,1,2,2 - Tetrachloroethane 108-88-3 Toluene 108-90-7 — Chlorobenzene 100-41-4 100-42-5 1330-20-7

•Ethylbenzene •Styrene ' •Xylene (total)

10 10 10 10 5 10 5 2 2 1 5 5 10

2 5 5 5 5 33 5 5 5 5 5 10 10 18 5 5 5 5 5 5

Q

U U U u u u u J J J u u u J u u u u

FORM I VOA 3/90


EPA SAMPLE NO.

109016 Lab Name: AQUATEC, INC. Contract: 94246
















CAS NUMBER

1. 2 . 3. 4. 5. 6 . 7.

9. 10. 11. 12.' 13.' 14.' 15." 16." 17." 18."

19.' 20." 21."

22 . " 23." 24." 25." 26 . " 27." 28 . " 29." 30."


FORM I VOA-TIC 3/90

LA. VOLATILE ORGANICS ANALYSIS DATA SHEET

EPA SAMPLE NO.

H105M008 Lab Name: AQUATEC, INC. Contract: 94246

Lab Code: AQUAI • Case No.: NHBA6 SAS No. : SDG No. : 50556


Sample wt/vol: 5 . 0 {g/mL) ML

Level: (low/med) LOW.


GC Column:CAP ID: 0 . 5 3 (mm)








CAS no; COMPOUND CONCENTRATION UNITS: (ug/L or ug/Kg) UG/L

74-87-3-- Chloromethane 1 n 74-83- 9 Bromomethane IQ 75-01- 4 Vinyl Chloride in 75-00-3 -Chloroethane m 75-09-2 Methylene Chloride s 67-64-1 Acetone ^ 10 75-15-0 Carbon-Disulfide q 7 5 - 3 5-4— 1 ,1-Dichloroethene 5

75-34-3- l,1-Dichloroethane 5

540-59-0- 1, 2-Dichloroethene (total) 5

67-66-3 Chloroform 5

107-06-2 1,2 - Di chloroethane S 78-93-3 2 - Butanone __ 1 0

71-55-6 -1,1,1-Trichloroethane S 56-23-5 Carbon Tetrachloride- s 7 5 - 2 7 - 4 Brcanodichloromethane 5

78-87-5-- 1,2-Dichloropropane 5

10061-01-5 cis-1,3-Dichloropropene 5

79-01-6 Tr ichloroethene_ __ 5 124-48-1 Dibromochloromethane 5 79-00-5 l,1,2-Trichloroethane 5

71-43-2 Benzene R 10061-02-6 trans-1,3-Dichloropropene 5 u 75-25-2 Brcmoform 5 u 108-10-1 4 -Methyl -2 -Pentanone 10 TT 591-78-6 2-Hexanone__ 1 0 u 127-18-4 Tetrachloroethene 1 j 79-34-5 l, 1,2,2-Tetrachloroethane 5 u 108-88-3 Toluene 5 n 108-90-7 Chlorobenzene s TT 100-41-4 Ethylbenzene x, TT

100-42-5 Styrene 5 n 1330-20-7 Xylene (total)

FORM I VOA 3/90


EPA SAMPLE NO.

H105M008 Lab Name: AQUATEC, INC. Contract: 94246
















CAS NUMBER

1. 2. 3.' 4. 5. 6. 7. 8. 9.

10.'

11.' 12.' 13.' 14.' 15.' 16.' 17.' 18.' 19." 2 0 . ' 21."

22 . " 23." 24." 25." 2 6 . " 27." 2 8 . " 29." 30."


FORM I VOA-TIC 3/90










CAS NO. COMPOUND








74-87-3-74-83-9-75-01-4-75-00-3-75-09-2-67-64-1-75-15-0-75-35-4-75-34-3-540-59-0 67-66-3-107-06-2 78-93-3-71-55-6-56-23-5-75-27-4-78-87-5-10061-01 79-01-6-124-48-1 79-00-5-71-43-2-10061-02 75-25-2-108-10-1 591-78-6 127-18-4 79-34-5-108-88-3 108-90-7 100-41-4 100-42-5 1330-20-

Chloromethane_ - - - Bromcmethane

Vinyl Chloride Chloroethane Methylene Chloride

— Acetone Carbon Disulfide 1,1-Dichloroethene 1,1-Dichloroethane 1/2-Dichloroethene (total!

--Chloroform - 1/ 2- Dichloroethane

2-Butanone 1/1,1-Trichloroethane Carbon Tetrachloride -Bramodichlorcmethane 1,2-Dichloropropane

-5 cis-1, 3-Dichloropropene Trichloroethene Dibromochloromethane 1,1/2-Trichloroe thane Benzene

-6 trans-1,3-Dichloropropene Bromoform 4-Methyl-2 -Pentanone 2-Hexanone Tetrachloroethene 1,1,2,2-Tetrachloroethane Toluene Chlorobenzene_ Ethylbenzene Styrene

7 Xylene (total

10 10 10 10 5 10 5 5 5 5 5 5 10 5 5 5 5 5 5 5 5 5 5 5 10 10 5 5 5 5 5 5 5

U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u

FORM I VOA 3/90


EPA SAMPLE NO.

MWGZ3R004 Lab Name: AQUATEC, INC. Contract: 94246

Lab Code: AQUAI Case No.: NHBA6 SAS No.: SDG No. : 50556















CAS NUMBER

1. 2. 3.' 4.' 5.' 6 . '

7.' 8 . '

9.' 10." 11." 12." 13." 14." 15." 16."

.17." 18." 19." 2 0 . " 21."

2 2 . 23. 24._ 25. 2 6 . 27. 28. 29. 30.


FORM I VOA-TIC 3/90










CAS NO. COMPOUND








74-87-3 Chlorome thane 74-83- 9 Bromomethane 75-01- 4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 75-35-4 75-34-3

•Carbon Disulfide 1/1-Dichloroethene 1,1-Dichloroethane"

540-59-0 l,2-Dichloroethene (total 67-66-3- — Chloroform 107-06-2 1,2 - Dichloroe thane 78-93-3 2-Butanone 71-55-6-- 1,1,1- Trichloroe thane 56-23-5 Carbon Tetrachloride 75- 27-4 Bromodichloromethane"

1,2-Dichloropropane 78-87-5 10061-01-5 cis-l,3-Di chloropropene 79-01-6 Trichloroethene 124-48-1 Dibrcmochloromethane 79-00-5 l, 1,2-Trichloroethane 71-43-2 Benzene 10061-02-6 trans-1,3-Dichloropropene 75-25-2 Brcmoform 108-10-1 4 -Methyl-2 - Pentanone 591-78-6 2-Hexanone 127-18-4 Te t rachl or oe thene_ 79-34-5 1,1,2,2 - Tetrachloroethane 108-88-3 Toluene 108-90-7 — Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene_ 1330-20-7 Xylene (total)

FORM I VOA 3/90.

la VOLATILE ORGANICS ANALYSIS DATA SHEET TENTATIVELY IDENTIFIED COMPOUNDS

EPA SAMPLE NO.

MWGZ3R004A Lab Name: AQUATEC, INC. Contract: 94246
















CAS NUMBER

1. 2 . 3. 4. 5. 6 . 7.

9. 10. 11. 12.'

13.' 14.' 15.' 16.'

17.' 18." 19." 20." 21."

22 . " 23." 24." 25." 26." 27." 28." 29." 30."


FORM I VOA-TIC 3/90


Lab Name: AQUATEC, INC. Contract: 9424G

Lab Code: AQUAI Case No.: NHBA6 SAS No.: * SDG No.: 50556






Soil Extract Volume: - (uL)








74- 87-3 Chlorome thane 74- 83-9 Bromomethane 75-01- 4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1/1- Dichloroethene 75-34-3 1,1-Di chloroethane 540-59-0 l,2-Dichloroethene {total) 67-66-3 Chlorof orm_ 107-06-2-- l, 2-Dichloroethane 78-93-3 2-Butanone 71-55-6 1 , 1 ,1-Trichloroethane 56-23-5 Carbon Tetrachloride 75-27-4 Brcmodichloromethane 78-87-5 1/2 - Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibrcmochl oromethane 79-00-5 l, l, 2-Trichloroethani" 71-43-2 Benzene 10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromof orm " 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 12 7-18-4 Te t rachl oroe thene__ 79-34-5 1,1, 2,2-Tetrachl oroe thane 108-88-3 Toluene 108-90-7 Chi orobenzene 100-41-4- Ethylbenzene 100-42-5 S tyrene . 1330-20-7 Xylene (total)

1200 1200 1200 1200 620 1200 620 620 290 620 620 620 1200 520 620 620 620 620 620 620 620 620 620 620 1200

' 1200 18000 620 620 620 620 620 620

Q

U U u u u u u u J. u u u u J u u u u u u u u u u u u

FORM I VOA 3/90


EPA SAMPLE NO.

MWGZ4R006 Lab Name: AQUATEC, INC. Contract: 94246








Number TICs'found: 0








CAS NUMBER

1. 2 . 3. 4. 5. 6 . 7.

9. 10. 11.' 12.' 13.' 14.' 15.' 16.'

17." 18.' 19.' 20. " 21."

22." 23." 24." 25." 2 6 . " 27." 28." 29." 30."


FORM I VOA-TIC 3/90











Lab File ID: MCLB001W.D

Date Received: / /





74-87-3 Chlorome thane 74-83- 9 Bromomethane 75-01- 4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4-- i, l-Dichloroethene Z5:3!"3: if 1-Di chloroethane 540-59-0 1 ,2-Dichloroethene (total) 67-66-3 Chloroform 107-06-2-- 1 , 2 -Di chloroethane 78-93-3 2 - Butanone 71-55-6 1/1,1-Trichloroethane 56-23-5 -Carbon Tetrachloride 75-27-4 Brcmodi chl orcmet hane

1,2-Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01-6 Trichloroethene i?4:4 8 ~1 Dibromochloromethane 79-00-5 1,1,2-Trichloroethane 71-43-2 Benzene 10061-02-6 trans-1,3-Dichloropropene 75-25-2 Bromoform 1 0 8 - 1 0 - 1 4-Methyl-2 -Pentanone 591-78-6 2 - Hexanone 127-18-4 Tet rachl or oe thene 79-34-5 1,1,2, 2-Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100-42-5 Styrene 1330-20-7 Xylene (total)

10 10 10 10 5 10 5 5 5 5 5 5 10 5 5 5 5 5 5 5 5 5 5 5 10 10 5 5 5 5 5 5 5

Q

U U u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u u

FORM I VOA 3/90


EPA SAMPLE NO.











Lab File ID: MCLB001W.D

Date Received: / /





CAS NUMBER

1. 2 . 3. 4. 5. 6 . !

7.

9. 10. 11. 12 . 13. 14. 15. 16.' 17.' 18.' 19.' 2 0 . ' 21.'

22." 23." 24." 25." 26 . ' 27." 28 . " 29." 30."


FORM I VOA-TIC 3/90

VOLATILE ORGANICS ANALYSIS DATA SHEET EFA SAiyiFLE NO.











Date Received: / /





74-87-3 Chi orome thane 74-83- 9 Bromamethane 75-01- 4 Vinyl Chloride 75-00-3 — Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone^ 75-15-0 Carbon Disulfide 75- 35-4 l, 1 -Dichloroethene 75-34-3 -1,1- Dichloroe thane" 540-59-0 1 , 2 -Dichloroethene (total) 67-66-3 Chloroform 107-06-2 1,2 -Dichloroethane 78-93-3 — -2-Butanone 71-55--6 1 , 1 ,1-Trichloroethane 56-23-5-- Carbon Tetrachloride 75- 27-4 Bromodichloramethane

2 -Dichloropropane 10061-01-5 cis-l# 3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 Dibrcmochloramethane 79-00-5 1, i, 2-Trichloroethane 71-43-2 Benzene 10061-02-6 trans -1,3- Dichloropropene 75-25-2 Bromoform 108-10-1 4 - Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 12 7 -18- 4 Tetrachloroethene 79-34-5 1,1,2,2 -Tetrachloroe thane 108-88-3 Toluene 108-90-7 Chlorobenzene 100-41-4 Ethylbenzene 100 -42-5 Styrene ~ 1330-20-7 Xylene (total

FORM I VOA 3/90


EPA SAMPLE NO.












Date Received: / /





CAS NUMBER

1. 2. 3.' 4.' 5.' 6 . ' 7.' 8 . ' 9.' 10.'

11.' 12." 13." 14." 15." 16."

17." 18." 19." 20 . " 21." 2 2 . " 23." 24." 25." 2 6 . " 27." 28 . " 29. 30.


FORM I VOA-TIC 3/90

.LA

VOLATILE ORGANICS ANALYSIS DATA SHEET EPA SAMPLE NO.

EX1013MS Lab Name: AQUATEC, INC. Contract: 94246








Lab Sample ID: 253048MS

Lab File ID: M253048MSV.D






74-87-3-74-83-9-75-01-4-75-00-3-75-09-2-67-64-1-75-15-0-75-35-4-75-34-3-540-59-0 67-66-3-107-06-2 78-93-3-71-55-6-56-23-5-75-27-4-78-87-5-10061-01 79-01-6-124-48-1 79-00-5-71-43-2-10061-02 75-25-2-108-10-1 591-78-6 127-18-4 79-34-5-108-88-3 108-90-7 100-41-4 100-42-5 1330-20-

— Chloromethane_ — Br omome t hane

Vinyl Chloride Chloroethane Methylene Chloride Acetone •Carbon Disulfide 1,l-Dichloroethene 1/l-Dichloroethane 1,2-Dichloroethene (total; Chloroform 1,2-Dichloroethane 2-Butanone 11,1/1-Trichloroethane

.-Carbon Tetrachloride —Br omod i chl or ome t hane -1/2-Dichloropropane

- 5 cis-1,3-Dichloropropene " Trichloroethene

Dibromochl oranet hane 1,1,2-Trichloroethane •Benzene

-6 trans -1, 3-Dichloropropene —Brcmoform

4-Methyl-2 -Pentanone 2 -Hexanone Tetrachloroethene 1,1,2,2-Te trachloroe thane Toluene Chlorobenzene Ethylbenzene Styrene

7 Xylene (total)

170 170 170 170 84 170 84 730 84 84 84 84 170 500 84 84 84 84

1000 84 84 840 84 84 170 170 2800 84 830 850 84 84 84

U u u

FORM I VOA 3/90


EPA SAMPLE NO.

EX1013MSD Lab Name: AQUATEC, INC. Contract: 94246




Level: {low/med) LOW




CAS NO. COMPOUND

Lab Sample ID: 253048MD

Lab File ID: M253048MDV.D






74- 87-3 Chlorome thane 74-83-9 Bromomethane 75-01-4 Vinyl Chloride 75-00-3 Chloroethane 75-09-2 Methylene Chloride 67-64-1 Acetone 75-15-0 Carbon Disulfide 75-35-4 1,1-Di chloroethene 75-34-3 l, 1-Dichloroethane 540-59-0 l, 2-Dichloroethene (total) 67-66-3— Chloroform 107-06-2 -1,2 - Di chloroethane 78-93-3 2 - Butanone 71-55-6 -1,1,1-Trichloroethane 56-23-5 Carbon Tetrachloride^ 75-27-4- - Bromodichloromethane 78-87-5 1,2 - Dichloropropane 10061-01-5 cis-1,3-Dichloropropene 79-01-6 Trichloroethene 124-48-1 - Dibromochl oromethane 79-00-5 l, l, 2-Trichloroethane" 71-43-2 Benzene 10061-02-6 trans-1,3-Dichloropropene 75-25-2 - Bromof orm " 108-10-1 4 -Methyl - 2 - Pentanone 591-78-6 2 - Hexanone 12 7 -18- 4 Tetrachloroethene 79-34-5 1,1,2,2 - Tetrachloroethane 108-88-3 Toluene 108-90-7 Chlorobenzene 100 - 41-4 Ethylbenzene 100-42-5- - Styrene 1330-20-7 •Xylene (total)

170 170 170 170 84 170 84 740 84 84 84 84 170 490 84 84 84 84

1000 84 84 840 84 84 170 170 2800 84 830 860 84 84 84

U

FORM I VOA 3/90

i ' ' . ; V '£ , : , .V

Hull & ' Associates, Inc.

6130 Wilcox Road -Dublin^ Ohio 43017 Phone: * (614) 793-8777 FAX:/ . (614) 793-9070

REPORT TO: k~±srhhr.—J f>

CHAIN |0F7 CUSTODY ^

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("UST K METUMID WIN MOOT)

w «n' V'-. ' -

V v W - YY ":v:.Vr:7,;:- r fo™qrdCresults to address at top left)

Client:

Project: 'i<: &"**> Project §: tJJ&Ac-

Samplers: K- :s <> >i~. .

/ PRESERVATIVES imfir murm wmwiB jcma. I. W» A - CM «%. <F C R - HUPP ' X'Y-T » - HMO, PKO H - GR«SPO > *g"« C.I pno-. •-•-« inr 6 " AAW pi&11 •• c. kmcnt c " 2**"*at| • HBOK "** :iS'£Sooa*,

••:\. .-i SAMPtE v'"' IDENTIFICATION

ir'K/Hw £j?( ofiX.'

RELINQUISHED BY; DATE: -TIME: -

RECEIVED BY:. v ; > ^ '^YYliYY' .';••.

DATE: ffNOTES: Y • ; .. : •-•••••! •• •:*'»-> — — - •

RELINQUISHED BY: TIME: :

DATE: ' -

TIME: RECEIVED FOR LAB BY: DATE:

TIME: />.—••«tf.

' v.v.-- •..-

. .< ...*..v

r;- " y.t

-. - \ . - 0FF/0999DIII .' ' j


„ .50 : Wilcox Road

f Dublin, Ohio 43017 Phone: - (614) 793-8777

;^'PAX: (614) 793-9070

REPORT T0:A_D_S

CHAIN OF CUSTODY RECORD • ? )

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REUNQUtSHED BY:

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DATE: /o RECEIVED -BY:

iA

t/

DATE: * >4 >if

fv f.^V

r, y- /« Method of Delivery: Airbill Number

RECEIVED FOR LAB BY:

M. Hul a Aaaectotaa, Inc.

6631 Commarea Poritwojr, Sulta E Dublin, Ohio 43017

Talaohona (614) 793-8777 Fffli (614) 793-9070

FIELD DATA SHEET GROUNDWATER MONITORING

WELL SAMPLING

CLIENT. /U/V/sS .SITE LOCATION

SITE NO. PROJECT NO..

c WELl S*// U/l

AIR TEMPERATURE WEATHER CONDITIONS

tr*n TYPE OF WELL CONSTRUCTION.

CONDITION OF WELL circle (£oog,V POOR) if poor, specify.

CAP LOCKEl^(Ygs> / NO) _ i orK N0.

DEPTH TO WATER / Z / 7 .FEET TOTAL DEPTH.

r i'i.ii

FREE PRODUCT circle (YES / NO) A)A PRODUCT THICKNESS ' A)A SAMPLE DATE

DEPTH TO PRODUCT.

— / ' O F E E T

A,'A _FEET

FEET

SAMPLE NO Mft-Mu&/h4F-rt£ - b/.<z

PURGE DATA

VOLUME PURGED

(GALLONS)/ WELL

VOLUME

N/A

NO. OF WELL VOLUMES

INITIAL

FIELD TESTING / WELL VOLUME

TEMPERATURE *C

PH

AT 25'C

CONDUCTIVITY units

AT 25*C

ONE WELL VOLUME EQUALS:

COMMENTS:

.GALLONS

DRUM INVENTORY: SOIL. PURGE WATER FREE PRODUCT

K Hul 8 Aaaoctataa, Inc.

6631 Commarca Portwcy. Sulfa E Dublin. Ohio 43017

Talaohonc (614) 793-6777 Far (614) 793-9070


WELL SAMPLING

CLIENT CL

SITE NO.

AIR TEMPERATURE.

.SITE LOCATION 1

.PROJECT. NO._

I WELL

•uU\ A Wf

TYPE OF WELL CONSTRUCTION 2!'

WEATHER CONDITIONS.

CONDITION OF WELL clrele^fGQpfl / POOR) if poor, specify

CAP LOCKEt^YFS / NO) i nru tyrt

DEPTH TO WATER /ASK f f f t TOTAL DEPTH. <&oo / M.

FEET

FEET FREE PRODUCT circle (YES / NO) A IA dfpth JO PRODUCT

PRODUCT THICKNESS. , AIA FEET .

SAMPLE DATE ^3Î_ SAMPLE NO 7/3/7 ZlZ/1 (2—C>t£

PURGE DATA

VOLUME PURGED

(GALLONS)/ WELL

VOLUME

N/A

NO. OF WELL VOLUMES

INITIAL


TEMPERATURE *C

pH

AT 25"C

CONDUCTIVITY \ir\W% _T

AT 25*C

CJ "7.4 /31,

JO 7 7 £,co 73/ is 7 ? G.o? J ^ t

ONE WELL VOLUME EQUALS:.

COMMENTS:

*S,D .GALLONS


Hul 8 Aatectetot, Inc. 6631 Cwnmarta Parkway, SuHt £

Dublin, Ohio 430rr Ttltehona (614) 793-8777

Fa (614) 793-9070


WELL SAMPLING

CLIENT A)UR1^ SITE NO.

AIR TEMPERATURE ^MTN

TYPE OF WELL CONSTRUCTION /?"

^ WELL I.D.£Hi

-SITE LOCATION If

-PROJECT NO A '/Y/TY/F

WEATHER pONDJTIONS. f lcL<f/h T

CONDITION OF WELL circle<J§0dif7 POOR) if poor, specify

CAP L0CKE1^(YES / NO) __LOCK NO

DEPTH TO WATER FEET TOTAL DEPTH.

aJA -FEET

.FEET FREE PRODUCT circle (YES / NO) /F//(NRPTM JO PRODUCT,

PRODUCT THICKNESS . .4 J A PEET

SAMPLE DATE_ -SAMPLE NO KHT7-

PURGE DATA

VOLUME PURGED

(GALLONS)/ WELL

VOLUME

N/A

NO. OF WELL VOLUMES

INITIAL


TEMPERATURE ' C

PH

AT 25*C

CONDUCTI units

AT 25'C

4 *5 ML m(

C.o 57 /¥?>•

a.o /yj>

5 .


COMMENTS-

.GALLONS


M.

Hul ft Aaaockrfaa, Inc. 6631 Commarea Psrfcvcy, Sulfa E

Dublin, Ohio 43017 Talaohona (614) 793-6777

Faa (614) 793-9070


WELL SAMPLING

CLIENT/ .SITE LOCATION.

SITE NO.

AIR TEMPERATURE -7 i ' .PROJECT Mn .C///&6/ f

.WELL I.DAtkYfL

Ac, A

TYPE OF WELL CONSTRUCTION

CONDITION OF WELL circle (fGOOb / POOR) if poor, specify

CAP LOCKED ^YES' / NO) LOCK Nn Z/77 DEPTH TO WATER FFFT TOTAL DEPTH

WEATHER CONDITIONS CJdtd)/

Sf

.DEPTH TO PRODUCT.

•FEET

FEET M .... FREE PRODUCT circle (YES / NO) /\)A

PRODUCT THICKNESS a!A SAMPLE DATE SAMPLE Uf/j9A ~~ /XK ^X

PURGE DATA

VOLUME PURGED

(GALLONS)/ WELL

VOLUME

N/A

L-l

NO. OF WELL VOLUMES

INITIAL


TEMPERATURE 'C

CA

PH

AT 25*C

CONDUCTIVITY ••"ih iff

AT 25'C

&</¥

/ZZ G-77 ivrb & 6<7 6-S7

ONE WELL VOLUME EOUALS:.

COMMENTS:

/ .GALLONS

DRUM INVENTORY: SOIL PURGE WATER FREE PRODUCT

M Hul a Aeeacfatee, Inc.

6631 Commerce Portray. Suite E Dublin. Ohio 43017

Telephone (614) 793-8777 For (614) 793-9070


WELL SAMPLING

CLIENTS

SITE NO.

AIR TEMPERATURE

-SITE LOCATION

.PROJECT ND . t Vc

,WELL \.d/,

.Sv,// Ar//

WEATHER CONDITIONS C /f'/rfy

Fian,lr^ TYPE OF WELL CONSTRUCTION

CONDITION OF WELL circglqglOb / POOR) if poor, specify

CAP LOCKEDdlES / NO) LOCK NO

DEPTH TO WATER C: / Crh , PFPT TOTAL DEPTH

FREE PRODUCT circle (YES / NO) AlA DEPTH TO PRODUCT-

PRODUCT THICKNESS- A!4 _FEET

SAMPLE DATE

jIL .FEET

.FEET

—/,ir \ FEET 4//2/9^ .SAMPLE NO.

PURGE DATA FIELD TESTING / WELL VOLUME

VOLUME PURGED

(GALLONS)/ WELL

VOLUME

N/A

NO. OF WELL VOLUMES

TEMPERATURE X

INITIAL

PH

AT 25'C

CONDUCTIVITY

AT 25*C

5; ? C>.r<F

/33 <o-3 £./~S


COMMENTS:

# / . .GALLONS


M Hul 8 AasacSetaa, Inc.

6631 Commarca Partway, Sulfa £ Dublin. Ohio 43017

Talaphona (6141 793-8777 Fa* (614) 793-9070


WELL SAMPLING

CLIENT. .SITE LOCATION.

c. y/WE>y-D

SITE NO.

AIR TEMPERATURF 5/

-project No. A kmr WEATHER CONDITIONS

-j. it TYPE OF WELL CONSTRUCTION

ZÔUl 'f

CONDITION OF WELL circle ^GOOi^V POOR) if poor, specify

CAP LOCKED rtfisZ/ NO) LOCK NO 7// 7t\ DEPTH TO WATER /-S FEET TOTAL DEPTH.

FREE PRODUCT circle (YES / NO) ////(

PRODUCT THICKNESS AJA SAMPLE DATE.

.DEPTH TO PRODUCT

.FEET

M .FEET

.FEET

SAMPLE NO. V-* X.

PURGE DATA

VOLUME PURGED

(GALLONS)/ WELL

VOLUME

N/A

NO. OF WELL VOLUMES

INITIAL


TEMPERATURE •c

PH

AT 25*C

CONDUCTIVITY units

AT 25*C


COMMENTS:

.GALLONS


M Hul 9 Assoc iota a, Ine.

6631 Commsrcs Portray, Suits E Dublin. Ohio 43017

Tslsohons (614) 793-8777 Fa* (614) 793-9070


WELL SAMPLING

CLIENT. —SITE LOCATION

SITE NO.

_ ,/WELL I.D;

AIR TEMPERATURE

-PROJECT Nn AJz-ZS /

TYPE OF WELL CONSTRUCTION Pt/( WEATHER CONDITIONS.

f-CONDITION OF WELL circle {(GOOD> / POOR) if poor, specify

CAP LOCKED NO) LOCK no

DEPTH TO WATER _FEET TOTAL DEPTH.

jK JK .FEET

.FEET FREE PRODUCT circle (YES / NO) f l j f -f nFPTH JO PRODUCT.

PRODUCT THICKNESS /(!A FEET _

SAMPLE DATE 7//T/?S~~~ c,un c Nr> X/7]7" ALTI'TAFF/?/- / '—7

PURGE DATA

VOLUME PURGED

(GALLONS)/ WELL

VOLUME

NO. OF WELL VOLUMES


TEMPERATURE •c

PH

AT 25"C

CONDUCTIVITY uni

AT 25*C

N/A INITIAL

S.C, s, 7 £. 7 2 770,0

/C-% V'O G.70 y&-o

5 .


COMMENTS:

3»b. .GALLONS


M Hul ft AsaocJetaa, inc.

6631 Commare* Partway, Sulfa E Dublin. Ohio 43017

Talaphona (614) 793-8777 Fa (614) 793-9070


WELL SAMPLING

CLIENT

SITE NO

.SITE LOCATION.

..WELL I.D.-

AIR TEMPERATURE

TYPE OF WELL CONSTRUCTION.

(gooc

-PROJECT Mn A WZf//? .WEATHER CONDITIONS ^ At out

CONDITION OF WELL circle ($000 -/ POOR) if poor, specify

CAP LOCKED <<Sr?NO)_, _LOCK Nn 'j/ Y7~,

DEPTH TO WATER KLh . FEET TOTAL DEPTH.

FREE PRODUCT circle (YES / NO) JK_ .DEPTH TO PRODUCT

PRODUCT THICKNESS . /TJA FEET SAMPLE DATE. __ SAMPLE NO

ZZAZK IK

.FEET

.FEET

PURGE DATA

VOLUME PURGED

(GALLONS)/ WELL

VOLUME

N/A

'5

NO. OF WELL VOLUMES

INITIAL


TEMPERATURE 'C

£- "7

PH

AT 25*C

£>r/7

CONDUCTIVITY unit*

AT 25'C

///, O

L // 5. 7

f (L>. 7 (o- ^ A/AC


COMMENTS;

.GALLONS


X Hul S AuoclatM, Inc.

6631 Commarc* Parkway, Sutta E Dublin, Ohio 43017

Tiltohona (614) 793-8777 Fa (6)4) 793-9070


WELL SAMPLING

CLIENT

SITE NO.

AIR TEMPERATURE. 551

WELL I.CU

.SITE LOCATION CXXtj/ /Jt-'//

-WEATHER CONDITIONS.

TYPE OF WELL CONSTRUCTION 'id'* Ît CONDITION OF WELL circle(/(GOOD> / POOR) if poor, specify.

CAP LOCKEDLÊP/ N0)__ LOCK NO

DEPTH TO WATER

.PROJECT NO. /

"Jll Oljt

FREE PRODUCT circle (YES / NO) jR

PRODUCT THICKNESS : M SAMPLE DATE SAMPLE NO

FEET TOTAL DEPTH

.DEPTH TO PRODUCT_

FEET

M XEO .FEET

.FEET

Zfo7-m£Am-a6 -

PURGE DATA

VOLUME PURGED

(GALLONS)/ WELL

VOLUME

N/A

NO. OF WELL VOLUMES

INITIAL


TEMPERATURE 'C

PH

AT 25'C

CONDUCTIVITY units.

AT 25'C

77 G. 7 G. 47 54 L- 7 5 "S3

Y.I &>/Z foi. 5


COMMENTS:

Z7 .GALLONS


M Hul 8 AiioctotBt, Inc.

6631 Cammaref Partway, &jtt« E Oublln, Ohio 43017

T»l«phen« (614) 793-8777 Fan (614) 793-9070


WELL SAMPLING

CLIENTS •S SITE NO.

AIR TEMPERATURF

WELL. I. oMIL .SITE LOCATION Z'XU-tk /\1^/( -PROJECT M.JJl

.WEATHER CONDITIONS Di

St ZIC TYPE OF WELL CONSTRUCTION __

CONDITION OF WELL circle (jSoCID* / POOR) if poor, specify.

cap locked(TyesV no)___lock no .'w76

DEPTH TO WATER /t.Si —FEET TOTAL DEPTH.

FREE PRODUCT circle {YES / NO)

PRODUCT THICKNESS A ]A SAMPLE DATE. 7/"/?±

.DEPTH TO PRODUCT

.FEET

'ilL fyc.tc .FEET

.FEET

SAMPLE NO


VOLUME PURGED (GALLONS)/ WELL

VOLUME

NO. OF WELL VOLUMES TEMPERATURE 'C

PH

AT 25'C

CONDUCTIVITY units

AT 25'C

N/A

6 . 1

// 2

INITIAL

c 1 2

(2 •

7.o/ /204 tf.3 7,oz /&2./

ONE WELL VOLUME EQUALS: _ 2 / f COMMENTS:

.GALLONS


A A Hul 8 Aaaoclataa. Ine. 6631 Cammarea Parfcvcy, Sulfa E

Dublin, Ohio 43017

J/ Taliphana (614) 793-6777 Fm (614) 793-9070

FIELD DATA SHEET -GROUNDWATER MONITORING

WELL SAMPLING

CLIENT mm ?3 ..WELL I.D. / SITE LOCATION Hi /-Jp//

SITE NO. PROJECT NO. A ¥/m/7 . —i- WEATHER CONDITIONS AIR TEMPERATURE

TYPE OF WELL CONSTRUCTION £ * ___

CONDITION OF WELL clrcle((GOOd / POOR) if poor, specify.

CAP LOCKED(fYES1 / NO) LOCK Nn 5^ 7

DEPTH TO WATER • 7. ' —2> _ .FEET TOTAL DEPTH.

FREE PRODUCT circle (YES /

PRODUCT THICKNESS

SAMPLE DATE

NO) A)A ; / NO

M .DEPTH TO PRODUCT.

.FEET

FEET

.FEET

7 7 ^— sample NO 'KFQJ-MIJPZ~(X>7-


VOLUME PURGED

(GALLONS)/ WELL

VOLUME

NO. OF WELL VOLUMES

TEMPERATURE *C

PH

AT 25*C

CONDUCTIVITY

AT 25'C

N/A INITIAL

3-2 7, 7 6 -

~i.L> 8V6

7-7 £ < / K 7

/77 6


COMMENTS:

.GALLONS


M Hul ft Aaaocletas, Inc.

6631 Commarra Porttwoy, SuHa E Dublin. Ohio 43017

Talaohona (614) 793-8777 Fa* (614) 793-9070


WELL SAMPLING

CLIENT A)TC6& SITE NO.

AIR TEMPERATURE. 537 .SITE LOCATION.

WELL

-WEATHE

PROJECT NO i (//--sv//y CONDITIONS -

y»*C.Ul_ I.U., U[ /^B/L JEP CONDITIONS - JOtlW


CONDITION OF WELL circle<<GOp[) / POOR) if poor, specify

CAP LOCKED Vi£S-> N0)__ _LOCK NO

DEPTH TO WATER .FEET TOTAL DEPTH.

FREE PRODUCT circle (YES / NO)

PRODUCT THICKNESS.

SAMPLE DATE. &

M TV. .cr>

7///7rT

DEPTH TO PRODUCT.

FEET

.FEET

.FEET

SAMPLE NO AfOY" Af/J&Y/A/A


VOLUME PURGED

(GALLONS)/ WELL

VOLUME

NO. OF WELL VOLUMES

TEMPERATURE "C

PH

AT 25*C

CONDUCTIVITY uniU^/zr">

AT 25'C

N/A

CS /Q

INITIAL

/ /< 7 /!• %

7: (-K 7. 0 7

/5A

33 //. 7 ~7,C6> U73(


COMMENTS:

.GALLONS


M Hul a Aaaeckrtaa. Inc.

6631 Cammarea Parinroy, Sulfa E Dublin, Ohio 43017

Talaphona (614) 793-6777 F« (614) 793-9070


WELL SAMPLING

CLIENT^

SITE NO.

AIR TEMPERATURE </ /

.SITE

^ ,*vELL 1,0.^

location J:U-FLT AJF /F - PROJECT NO L ( / / : v y y

(-

.WEATHER CONDITIONS

s' if Ct1 TYPE OF WELL CONSTRUCTION.

CONDITION OF WELL circl^fGOOD; / POOR) if poor, specify.

W7B

CUVUT7\

.LOCK NO. CAP LOCKED (f?ES< / NO)

DEPTH TO WATER FEET TOTAL DEPTH.

FREE PRODUCT circle (YES / NO) 1 DEPTH TO PRODUCT

PRODUCT THICKNESS M FEET

SAMPLE DATE SAMPLE NO ^7MLJ F C '&S /tK-

.FEET

.FEET

PURGE DATA

VOLUME PURGED

(GALLONS)/ WELL

VOLUME

NO. OF WELL VOLUMES


TEMPERATURE 'C

PH

AT 25'C

CONDUCTIVITY units

AT 25'C

N/A INITIAL

COMMENTS;

3CO .GALLONS TO (FT I

DRUM INVENTORY; SOIL PURGE WATER FREE PRODUCT

Hul S Aatoekxtta, Inc. 6631 Conwnarva Parinroy, Sufta E

M Dublin, Ohio 430IT Talaphcna (614) 793-8777

FOB (614) 793-9070


WELL SAMPLING

CLIENT.

SITE NO

A)t-tKK SITE LOCATION.

; "C.UL. I.U) WELL LP

AIR TEMPERATURF - //P

TCPE OF WELL CONSTRUCTION 2L * IT^fC ,

PROJECT NO. / V/Y

WEATHER CONDITIONS Cfac'cfi. •VCIJ CONDITION OF WELL circle (jjQOq>/ POOR) if poor, specify

CAP LOCKED (fYgs.// NO)____LOCK Nn ~ f 7(r>

DEPTH TO WATER f'f- 7V ~7 T F E -ET T0TAL DEPTH_

FREE PRODUCT circle (YES / NO) /L?4 DFPTH JO PRODUCT

PRODUCT THICKNESS. , .(J>T FEET

SAMPLE DATE SAMPLE Nn 307'' /c£l<~ Q~/

V A .FEET

.FEET


VOLUME PURGED

(GALLONS)/ WELL

VOLUME-

NO. OF WELL VOLUMES

TEMPERATURE "C

PH

AT 25*C

CONDUCTIVITY units^__^L_

AT 25'C

N/A

4 Y

INITIAL

U &X&>- /3 / CI 6-3 G.ov fbo.A>

FZ- 6.4 &. 07 FZF.S


COMMENTS:

TF-0 .GALLONS


A A Hul S Aatoelotat, tne. 6631 Commarca Parfcvoy, Sutta E

Dublin. Ohio 43017 M Talaphona (614) 793-8777 F« (614) 793-9070


WELL SAMPLING

CLIENT./ (V/XA SITE NO

~l—y, . 1 rnmjLL t I M I • J f <, JY 't

AIR TEMPERATURE ^ .WEATHER CONDITIONS

TYPE OF WELL CONSTRUCTION £ <4^

^ WELL I-DGffffQSM

.SITE LOCATION ~Xj{/h Lip//

PROJECT NO.X

CONDITION OF WELL circlflÔOO.)/ POOR) if poor, specify

CAP LOCKED'((Yb>/ NO) LOCK NO S¥

DEPTH TO WATER /"/ FEET TOTAL DEPTH pFFT

.FEET FREE PRODUCT circle (YES / NO) A)A nrPTH JO PRODUCT A)A PRODUCT THICKNESS. A }A FEET

SAMPLE DATE SAMPLE NO /fOT^ MU&^J/

PURGE DATA

VOLUME PURGED

(GALLONS)/ WELL

VOLUME

NO. OF WELL VOLUMES


TEMPERATURE *C

PH

AT 25*C

CONDUCTIVITY

AT 25'C

N/A INITIAL

4 b

'M 7.3

<<<;

C,2/ /ZC?. !Z 41


COMMENTS;

7f> .GALLONS


M A A Hul 9 Ai»oc(ols«, Inc.

6631 Commarca Parfcwcy, SuHa E Dublin. Ohla 43017

Tatohont (614) 793-8777 " (151 Foi (614) 793-9070


WELL SAMPLING

CLIENT. M3 'ELL I.Dh

SITE NO.

AIR TEMPERATURE_ ^ WEATHER v. TYPE OF WELL CONSTRUCTION £ /'/(

.SITE

-PROJECT NO

ER CONDITIONS.

/ y I .I <.——

LOCATION /^VU//7 AL^/F

CONDITION OF WELL circle ^jpOJ^V POOR! if poar. specify

CAP L0CKED((^s:V NO)^ LOCK NO '3/7£> DEPTH TO WATER l£jL FEET TOTAL DFPTH ^

FREE PRODUCT circle (YES / NO) d )A DFPTH TO PRODUCT A.U- FEET

PRODUCT THICKNESS- A)A FEET 0

T(UFC? sample NOM7-MA)G£/GG SAMPLE DATE.


VOLUME PURGED

(GALLONS)/ WELL

VOLUME

NO. OF WELL VOLUMES

TEMPERATURE *C

PH

AT 25'C

CONDUCTIVITY \nn\* 6t —•»

AT 25*C

N/A

!Z

6

INITIAL

IT'^ ti, rs //.S"

/77 V

7/6 /%, :s 7/ S /6$~Y


COMMENTS:

761 .GALLONS


M Hul 8 Asaoelolaa, Inc.

6631 Camrnarca Parkway, Suit* £ Dublin, Qble 43017

Taltehona (614) 793-6777 Fa* (614) 793-9070


WELL SAMPLING

CLIENT. .\77Y> <R SITE NO.

—SITE LOCATION

.PROJECT NO d.

;WELL I.D

XC/H L /-/F n

AIR TEMPERATURE. _ WEATHER CONDITIONS.

TYPE OF WELL CONSTRUCTION t' ((&•£: -MY

CONDITION OF WELL circle(jGOOp^> POOR) if poor, specify.

CAP LOCKED'^YEST; NO) LOCK NO 'S/7b

DEPTH TO WATER 7 FREE PRODUCT circle (YES / N0)/LM

PRODUCT THICKNESS.

SAMPLE DATE p N0

FEET TOTAL DEPTH

.DEPTH TO PRODUCT_

_FEET

MRON ALK

_ FEET

_FEET

77x7 mU-rtft-


VOLUME PURGED

(GALLONS)/ WELL

VOLUME

NO. OF WELL VOLUMES

TEMPERATURE *C

PH

AT 25'C

CONDUCTIVITY units

AT 25'C

N/A

3/

7 V

INITIAL

/3. <7 7>' I 2 779 &.2/

/OF. 7 917

ZD. &, 72 99.7

ONE WELL VOLUME EQUALS: 3. GALLONS

COMMENTS: A'A)(%7FL7,II- (.<> /"WS /T'(7> 77C 7'7/AJC7X//W- //VA - ZWY,


Hul 8 Asaoctotst, Inc. 6631 Corrvrsirt Partway. Sufta £

Dublin. Ohio 43017 Ttlaphona (6I4J 793-8777

Fffli (614) 793-9070


WELL SAMPLING

CLIENT. £ S SITE NO.

AIR TEMPERATURE.


CONDITION OF WELL circle

CAP LOCKED ^YES-V NO)

DEPTH TO WATFR

c/r _ WEATHER CONDITIONS C/vu//*

AUCTION ^ ' / iCi, /

WELL I.D(y il7U

SITE LOCATION - XA IT LB//

PROJECT NO A 1 '

/ POOR) if poor, specify.

-LOCK NO.


AR ^•FEEJ TOTAL DEPTH.

lY/f DEPTH TO PRODUCT

» 3

jiL .FEET

.FEET PROOUCT THICKNESS

SAMPLE DATE

.FEET

SAMPLE NO.

7 PURGE DATA FIELD TESTING / WELL VOLUME

VOLUME PURGED

(GALLONS)/ WELL

VOLUME

NO. OF WELL VOLUMES

TEMPERATURE 'C

PH

AT 25*C

CONDUCTIVITY units

AT 25'C

N/A INITIAL c-


COMMENTS-

.GALLONS


A A Hul a Aaiockrtsi. Inc. 6631 Commarca Porinray, SuHa £

Oublln. Ohio 43017 Ttlaehona (614) 793-6777

F« (614) 793-9070


WELL SAMPLING

CLIENT. A)KKY ^ // .SITE LOCATION

SITE NO.

AIR TEMPERATURE _ n,n u(, lu„

TYPE OF WELL CONSTRUCTION Y'/ ' If

PROJECT NO /I

WEATHER CONDITIONS C(cu/ft*

ELL I.D/;

IML .D /JMIWTU

CONDITION OF WELL circle / POOR) if poor, specify

CAP LOCKED NO) i nr* NO

DEPTH TO WATER. FFFT TOTAL DEPTH,


PRODUCT THICKNESS A )A SAMPLE DATF V/tOr?±

M DEPTH TO PRODUCT. M .FEET

.FEET

FEET

SAMPLE NO. //?/-- Af/y i i/Imi - ?

PURGE DATA

VOLUME PURGED

(GALLONS)/ WELL

VOLUME

N / A

O/ !,D

NO. OF WELL VOLUMES

INITIAL


TEMPERATURE *C

PH

AT 25'C

/ / / /LN

<C>' C-Y

CONDUCTjyiTY NNILC //I D> AT 25'C

YDS SI A

F'S> //.O G.CFR %'2- < 7


COMMENTS:

tY:> .GALLONS


M A A Hul a Aasockrtat, Inc.

6631 Cammarc* Poricvoy, 3utt« E Oublln. Ohio 430IT

Ttlwhoftf (614) 793-8777 Fa (614) 793-9070


WELL SAMPLING

CLIENT. '35 SITE NO.

AIR TEMPERATURE '

.SITE LOCATION

.PROJECT NO

.WEATHER CONDITIONS 77/ ' R>I !S~ / R / / / / -V Y /: /—tc_-

WELL i n (—-£(01(A

RPR7i//

MM OA

TYPE OF WELL CONSTRUCTION-.

CONDITION OF WELL circle(TG00D^/ POOR) if poor, specify,

CAP LOCKED^CfES 7 NO) LOCK NO- -^/7A

DEPTH TO WATER £>.2*/ FEET TOTAL DEPTH ,3 2 ) FEET

FREE PRODUCT circle (YES / NO) _Xi4_ DEPTH TO PRODUCT, PRODUCT THICKNESS A FEET

SAMPLE DATE 7 liO/fti

JM .FEET

SAMPLE N0 /Cy? '7 ; S£Z/J~ MA ' "?


VOLUME PURGED

(GALLONS)/ WELL

VOLUME

N/A

C&

NO. OF WELL VOLUMES

TEMPERATURE "C

PH

AT 25*C

INITIAL

L.Y 7 ;

—1

/

<£>7'7

CONDUCTiyiTY units £./

/ AT 25'C

77 7 7^ 7/ \Z.-2.


COMMENTS:

m. .GALLONS


X

Hul a Aeeoelotee, Inc. 6631 Commerce Partway, Suite E

Dublin, Ohio 43017 Telephone (6I4J 793-8777

Fat (614) 793-9070


WELL SAMPLING

CLIENT.

SITE NO.

AIR TEMPERATURE

TYPE OF WELL CONSTRUCTION.

.SITE LOCATION

-PROJECT NO..

.WEATHER CONDITIONS. P\'R CloLiiiy (J-7

CONDITION OF WELL circle((GOCyX/ POOR) if poor, specify

CAP LOCKED (?ES> NO) LOCK NO

DEPTH TO WATER ?t TOTAL DEPTH.

FREE PRODUCT circle (YES / NO) /in DFPTH JO PRODUCT_

i)T

.FEET

.FEET

PROOUCT THICKNESS

SAMPLE DATE 4LWL<?4 .FEET

SAMPLE NO. FTFD 7- ML )&G/OT I -O/ R-_>Y* >>


VOLUME PURGED

(GALLONS)/ WELL

VOLUME

N/A

NO. OF WELL VOLUMES

TEMPERATURE 'C

INITIAL

PH

AT 25"C

CONDUCTMTY unite

AT 25"C

<7 7/ %n &RT>D 36, Z

14 2,7 6, Sz 77, / y.7

ONE WELL VOLUME EQUALS* J~zL COMMENTS: L4/J^=>' / fd 7 -

.GALLONS

Q/7A -2>/<irs


ATTACHMENT B

Surface Water Discharge Sampling Documentation

HULL A ASSOCIATES. INC.

DUBLIN. OHIO SEPTEMBER 1995

NHB019D.017


A n a l y t i c a l R e p o r t

Laboratory Locations

55 South Park Drive Colchester, VT 05446

75 Green Mountain Drive South Burlington, VT 05403

150 Herman Melville Boulevard New Bedford, MA 02740

Hull & Associates, Inc. 360901 Pinetree Place Route 101 Bedford, NH 03110

Attention : Steve Dishong

Date ; ETR Number : Project No.: No. Samples: Arrived :

04/03/95 49967 94246 9

03/15/95

Page

Job:NHBA6

T e s t M e t h o d s f o r E v a l u a t f ^ S o T T d H e t ' h ^ ^ r ^ t h e EXM1" Wa%tes'" EPA-600/4/79-020,

Lab No./ *'1 results SSrlue S«!T"",,on 0f Uater Bnd

-!!I?]:e_DeSCription Metho<* No. ' Parameter

250914 250915

624 Volatile Organics

S»2Z"?WD"031495"B309:03/14/95 @1246(Water) RF07-SWD 031495A-B309:03/14/95 @1254(Water)

Result

C

C

8010

250913 250916 250917 250918 250919 250920 250921

Halogenated Volatiles

RF07 RF07 RF07 RF07 RF07 RF07 RF07

-FBI -TBI -TIE -T2E--T2I--Til--T2I-

-031495-B309;03/14/95 @1226(Water) -031495:03/14/95 @1234(Water) -014-B309:03/14/95 @1202(Water) •014-B309:03/14/95 @1242(Water) -014-B309:03/14/95 @1210(Water) -014-B309:03/14/95 @1154(Water) -014A-B309:03/14/95 @1218(Water)

c c c c c c c

250913 250916 250917 250918 250919 250920 250921

RF07-RF07-RF07-RF07-RF07-RF07-RF07-

-FB1--TBI--TIE-•T2E--T2I-•T1I-•T2I-

8020 Aromatic Volatiles

-031495-B309:03/14/95 @1226(Water) •031495:03/14/95 @1234(Water) •014-B309:03/14/95 @1202(Water) •014-B309:03/14/95 @1242(Water) '014-B309:03/14/95 @1210(Water) •014-B309:03/14/95 @1154(Water) 014A-B309:03/14/95 @1218(Water)

Comments/Notes

C = Procedure/analysis completed

< Last Page > Submitted By :

55 South Park Drive - Colchester, VT 05446 - Tel: 802-655-1203 . Fax: 802-655-1248

C c c c c c c

^ Aquatec Inc

XLG YHP,



Date: 03 April 1995 Aquatec Lab No.: 250920 ETR No.: 49967; Project No.: 94246

Sample Received On: 15 March 1995; Analyzed On: 20 March 1995 Sample Identification: Hull & Associates, water sample labeled

RF07-T1I-014-B309, 03/14/95 at 1154 hours.


55 South Park Drive Colchester. VT 05446


150 Herman Melville Boulevard

New Bedford, MA 02740

Volatile Organic Compounds in ug/1 EPA Method 8010 and 8020

benzene X0 p bromodichloromethane X0 u bromoform X0 U bromomethane XO U carbon tetrachXoride X0 U chlorobenzene X0 U chloroethane X0 U chloroform X0 U chloromethane X0 U dibromochloromethane X0 U 1. 2-dichlorobenzene X0 U 1.3-dichlorobenzene 1Q u 1. 4-dichlorobenzene X0 U dichlorodifluoromethane X0 U 1.1- dichloroethane 1Q u 1.2-dichloroethane X0 U 1.1-dichloroethene X0 U cis -1.2- dichloroethene 1Q u

trans -1.2-dichloroethene X0 U 1. 2-dichloropropane X0 U cis-1.3-dichloropropene X0 U trans -1, 3-dichloroDronene X0 U ethvlbenzene ; X0 U Freon TF 22 methylene chloride X0 U stvrene X0 U 1.1.2.2- tetrachloroethane 1Q u tetrachloroethene 540 toluene X0 U 1.1 • 1-trichloroethane 120 1.1. 2-trichloroethane XQ U trichloroethene 27 trichlorofluoromethane XO U vinvl chloride XO U m & p-xvlenes XO U o-xvlene XO U

Key to the letter used to qualify the results of the analysis:

U - The compound was analyzed for but not detected at or above the reporting limit. The number is the method specified reporting limit for the compound.

55 Soulh Park Drive • Colchester, VT 05446 • Tel: 802-655-1203 • Fax: 802-655-1248







Date: 03 April 1995 Aquatec Lab No.: 250917 ETR No.: 49967; Project No.: 94246 Sample Received On: 15 March 1995; Analyzed On: 20 March 1995 Sample Identification: Hull & Associates, water sample labeled

RF07-T1E-014-B309, 03/14/95 at 1202 hours.


benzene 0. 5 U bromodichloromethane 0.5 U bromoform . 0,5 U bromomethane 0. 5 U carbon tetrachloride 0.5 U chlorobenzene 0,5 U chloroethane 0,5 U chloroform 0.5 U chloromethane 0,5 U dibromochloromethane 0. 5 U 1.2-dichlorobenzene 0,5 U 1. 3-dichlorobenzene 0,5 U 1.4-dichlorobenzene 0,5 U dichlorodifluoromethane 0. 5 U 1.1-dichloroethane 0.5 U 1. 2-dichloroethane 0.5 U 1.1-dichloroethene 0,5 U cis-1. 2-dichloroethene 0,5 U

trans-1.2-dichloroethene 0.5 U 1.2-dichloropropane 0,5 U cis-1.3-dichloropropene 0.5 U trans -1.3- dichloropropene 0.5 U ethvlbenzene ; 0.5 U Freon TF 0.5 U methylene chloride 0,5 U stvrene 0,5 u 1.1.2. 2-tetrachloroethane 0,5 U tetrachloroethene 45 toluene | 0,5 1) 1.1.1- trichloroethane 8 . 4 1.1.2-trichloroethan e 0,5 U trichloroe thene 3 .0 trichlorofluoromethane 0. 5 U vinvl chloride 0.5 U m & p-xvlenes 0.5 U o-xvlene 0,5 U



55 South Park Drive • Colchester, VT 05446 • Tel: 802-655-1203 • Fax: 802-655-1248



Laboratory Locationi






RF07-T2I-014-B309A, 03/14/95 at 1218 hours.


benzene 0. 5 U bromodichlorome thane 0.5 U

bromoform q 5 u

bromome thane p . 5 u carbon tetrachloride 0.5 u chlorobenzene 0 . 5 U chloroethane p 5 u chloroform p.5 p chloromethane 0.5 U dibromochloromethane p. 5 u

1.2-dichlorobenzen e Q.5 u 1.3-dichlorobenzen e p.5 u 1.4-dichlorobenzene 0,5 U dichlorodifluoromethane p . 5 p

1.1- dlchloroethane p . 5 u

1.2-dichloroethan e p.5 u

1.1-dichloroethene p.5 u

cis-1. 2-dichloroethene p. 5 U

trans-1.2-dichloroethene p.5 p

1. 2-dichloropropane p,5 u cis - 1. 3-dichlorooropene 0.5 U

trans-1. 3-dichloropropene p. 5 u ethvlbenzene . 0.5 U

Freon TF P.5 U

methylene chloride 0.5 u

stvrene 0,5 p

1.1.2. 2- tetrachloroethane p. 5 u

tetrachloroethene 74

toluene ; p 5 y

1.1.1-trichloroethan e 6.4

1.1.2- trichloroethane p. 5 p

trichloroethene 2. 6 trichlorofluoromethane Q,5 p

vinvl chloride __ 0,5 u

m & p-xvlenes _ p.5 u

o-xvlene p.5 U


U - The compound was analyzed for but not detected at or above the. reporting limit. The number is the method specified reporting limit for the compound.








Date: 03 April 1995 Aquatec Lab No.: 250919

ETRNo.: 49967; Project No.: 94246


RF07-T2I-014-B309, 03/14/95 at 1210 hours.


benzene

bromodichloromethana bromoform

.0 • 5 U trans-X. 2-dichloroethena 0.5 U

bromomethane 0.5 U

1.2-dlchloropropane cis•1•3-dichloropropene

carbon tetrachloride chlorobenzene chloroethane

P•5 U trans-1.3-dichloropropene 0.5 U ethvlbenzene 0.5 U Freon TF

chloroform °t5 V methylene chloride

chloromethane 0.5 U stvrene

dibromochlorome thane 0-5 U 1.1.2.2-tetrachloroethano

1.2-dichlorobenzene 1.3-dichlorobenzene

0.5 U 0.5 U

tetrachloroethene toluene

1.4-dichlorobenzene 0-5 u 1.1.1-trichloroethane

dichlorodifluoromethane 0.5 U

1.1-dichloroethane 1.2-dichloroethane 1.1-dichloroethene

1.1.2-trichloroethane trichloroethene

0-5 U trichlorofluoromethane

0.5 U

0.5 U

cis-1.2-dichloroethene 0.5 U 0.5 U

vinvl chloride m & p-xvlenes o-xvlene



0.5 U 0.5 U 0,5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U 0.5 U

24 0.5 U

6.2 0.5 U

2.3 0.5 U 0.5 U 0.5 U 0.5 U










RF07-T2E-014-B309, 03/14/95 at 1242 hours.


benzene 0. 5 U

bromodichloromethane Q . 5 p

bromoform . p 5 p bromomethane q 5 p carbon tetrachloride 0.5 U

chlorobenzene . p 5 p

chloroethane 0.5 U

chloroform 0,5 U

chloromethane p 5 p

dibromochloromethane p t 5 p

1.2- dichlorobenzene Q 5 p

1.3-dichlorobenzen e p. 5 p

1.4- dichlorobenzene p. 5 p

dichlorodifluoromethane p 15 p

1.1-dichloroethane 0.5 U

1.2-dichloroethan e 0.5 U

1.1-dichloroethene p t5 p

cis -1. 2 -dichloroethene 0.5 U

trans -1. 2 -dichloroethene p _ 5 p

1. 2 -dichloropropano _ p 5 p cis-1.3-dichloropropene p.5 p

trans-1. 3-dichloropropene p 5 p

ethvlbenzene , P. 5 U

Freon TF ___ 0.5 U methylene chloride p 5 p

stvrene p,5 p

1.1.2. 2- tetrachloroethane p. 5 p

tetrachloroethene 3 ?

toluene - 0.5 U

1.1•1-trichloroethane Q. 8

1.1. 2-trichloroethane p, 5 p trichloroethene 0. 5 U

trichlorofluoromethane 0.5 U

vinvl chloride 0 5 p

m & o-xvlenes p a 5 p

o-xylefie 0.5 U



55 South Park Drive • Colchester, VT 05446 • Tel. 802-655-1203 • Fax: 802-655-1248



Date: 03 April 1995 Aquatec Lab No.: 250914 ETRNo.: 49967; Project No.: 94246 Sample Received On: 15 March 1995; Analyzed On: 20 March 1995 Sample Identification: Hull & Associates, water sample labeled

RF07-SWD-031495-B309, 03/14/95 at 1246 hours.

Laboratory Locations 55 South Park Drive Colchester. VT 05446




Volatile Organic Compounds in ug/1 EPA Method 624

benzene 5 U chloromethane ip p catboq. tetyflchloyj.de_ 5 U bromomethane ip p chlorobenzene 5_U bromoform ; 5 p 1...2-dichloroethane 5 U bromodichlorome thane 5 p

i J. 1 X ~ fyic^lotoethajê U dibromochloromethane 5 p 1,1-dichloroethape 5 U tetrachloroethene 3j 1«1•2 -trichloroethane 5 U toluene 5 p 1,1.2.2- tetrachloroethane 5 U trichloroethene 5 p chloroethane 10 U vinvl chloride ip p chloroform 1 5 U acetone . ip p 1,1-dichloroethene 5 U 2-butanone 1Q p 1.,2-dichloroethenes 5 U carbon disulfide 5 p 1. 2-dichloropropane 5_p 2-hexanone 10 u tyans-1, 3-dichloropropene 5_U 4-methvl-2-pentanone 10 u cis-1.3-dichloropropene 5 U stvrene 5 p ethylbepzene 5 U vinvl acetate 10 p methylene chloride 5_p total xylenes 5_U

Key to the letters used to qualify the results of the analysis:

U - The compound was analyzed for but not detected. The number is the method specified reporting limit.

J - The mass spectrum indicates the presence of the compound, but the calculated result is less than the method specified reporting limit.

LCB - Compound was found but at low concentration, comparable to that in the blank. Quantitation is not possible.

C - The result has been corrected for the presence of the compound in the blank.

Quality controls were analyzed with the sample as part of Aquatec's standard analytical procedures. The results of these are maintained on file at Aquatec.




Date; 03 April 1995 Aquatec Lab No.: 250915 ETR No.: 49967; Project No.: 94246


RF07-SWD-031495A-B309, 03/14/95 at 1254 hours.


55 South Park Drive Colchester. VT 05446

75 Green Mountain Drive South Burlington. VT 05403

150 Herman Melville Boulevard New Bedford. MA 02740

benzene carbon tetrachloride


5 U chloromethane

chlorobenzene 5 U bromomethane

1.2-dichloroethane 5 U bromoform

1.1.1"trichloroethane 1.1-dichloroethane

1J 5 U bromodichloromethane

dibromochloromethane

1.1.2-trichloroethane 5 U tetrachloroethene

1.1.2.2-tetrachloroethane 5 U toluene

chloroethane 5 U trichloroethene

chloroform 10 U vinvl chloride

1.1-dichloroethene acetone

1.2-dichloroethenes 1.2-dichloropropane

5 U 5 U 2-butanone 5 U carbon disulfide

trans -1.3-dichloropropene els -1.3-dichloropropene ethvlbenzene methylene chloride

5 U 2-hexanone 5 U 4-methvl-2-pentanone

stvrene 5 U 5 U vinvl acetate 5 U total xylenes

10 U 10 U 5 U 5 U 5 U

3J 5 U 5 U 10 U 10 U 10 U 5 U 10 U 10 U 5 U 10 U 5 U



J -

LCB -

C -

The mass spectrum indicates the presence of the compound, but the calculated result is less than the method specified reporting limit.

Compound was found but at low concentration, comparable to that in the blank. Quantitation is not possible.

The result has been corrected for the presence of the compound in the blank.


55 Soulh Park Drive • Colchester, VT 05446 • Tel: 802-655-1203 • Fax: 802-655-1248

^ Inchcape Testing Services -»• Aquatec Laboratories


Date: 03 April 1995 Aquatec Lab No.: 250913 ETRNo.: 49967; Project No.: 94246 Sample Received On: 15 March 1995; Analyzed On: 20 March 1995 Sample Identification: Hull & Associates, water sample labeled

RF07-FB1-031495-B309, 03/14/95 at 1226 hours.

Laboratory Location*





benzene 0 5 p brornodichloromethane 0,5 u

bromoform 0.5 U

bromome thane p 5 p

carbon tetrachloride Q. 5 p

chlorobenzene p. 5 p chloroethane Q t5 p chloroform p 5 p chloromethane p t 5 p

dibromochloromethane p.5 u 1.2- dichlorobenzene 0.5 U

1. 3-dichlorobenzene p. 5 u 1. 4-dichlorobenzene p. 5 p

dichlorodifluoromethane P . 5 U 1.1 -dichloroethane p.5 p

1.2-dichloroethane p.5 u 1.1-dichloroethene p.5 u

cis-1, 2-dichloroethene p. 5 u

trans -1.2- dichloroethene p t 5 p

1.2-dichloropropane p.5 U cis-1. 3 -dichloropronene p . 5 u

trans-1. 3-dichloropropene p. 5 u ethvlbenzene ; 0. 5 U

Freon TF _ 0. 5 U

methylene chloride p. 5 p

stvrene p.5 U 1.1.2 . 2- tetrachloroethane 0.5 U

tetrachloroethene _ 0.5 U

toluene • p 5 p

1.1.1- trichloroe thane 0.5 U

1.1.2-trichloroethane p.5 p trichloroe thene ; p. 5 p

trichlorofluoromethane p.5 p

vinvl chloride p.5 p m & p- xylenes p. 5 p o-xylene p.5 U

Key to the .letter used to qualify the results of the analysis:












RF07-TBI-031495-B309, 03/14/95 at 1234 hours


benzene pa 5 p

bromodichloromethane Q. 5 p

bromoform 0.5 U

bromome thane p 5 p

carbon tetrachloride p. 5 u

chlorobenzene 0 . 5 \ ] chloroethane p 5 p chloroform 0.5 U

chloromethane P. 5 U

dibromochloromethane p 5 p

1.2-dlchlorobenzen e p. 5 p

1.3- dichlorobenzene Q t 5 p

1.4-dichlorobenzen e p. 5 p dichlorodifluoromethane p. 5 p

1.1-dichloroethan e p . 5 p 1.2-dichloroethan e 0.5 p

1.1-dichloroethene p. 5 p

cis-1, 2-dichloroethene p. 5 p

trans-1.2-dichloroethene 0,5 p 1.2-dichloropropane 0, 5 U cis -1. 3-dichloropropene p. 5 p trans -1. 3 -dichloropropene p. 5 p ethvlbenzene , 0.5 U

Freon TF p.5 p methylene chloride p 5 p stvrene 0,5 U

1.1.2.2-tetrachloroethane 0,5 p tetrachloroethene p 5 p toluene 0.5 U

1.1.1-trichloroethane 0.5 U

1.1. 2- trichloroethane p . 5 p trichloroethene 0. 5 U

trichlorofluoromethane p . 5 p vinvl chloride p. 5 p m & o-xvlenes p 5 p o-xvlene Q.5 U




JJ Hull Sc Associates, Inc.

360—901 Pine Tree Place P.O. Box 10419 Bedford, New Hampshire 03110 Phone: (603) 472-8740

FAX: (603) 472-3763

REPORT TO:

CHAIN OF CUSTODY RECORD

WHfTE —LAB USE (MUST BE RETURNED WITH REPORT) YELLOW —MB USE PINK —RETAINED B1 HAI

(Please forward results to address at top left)

SAMPLE IDENTIFICATION

V£07- TL.Z- F)K/-K T, \ a%7-

>J MI::

RECEIVEl FeR^B- BY:

, TIME: - /P - RXO I.

dic<Z^crv\ fuoa^-Ô ^ Vox \y& f\ ( ^ a- <y_, IrO i^vV\cA-> 0FF/O999DIII



Laboratory Location* S3 South Park Drive Colchester, VT 03446






Date : ETR Number : Project No.: No. Samples: Arrived :

Page

05/01/95 50652 94246 4

04/20/95

Job:NHB019

Lab

Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes. EPA-600/4/79-020 Test Methods for Evaluating Solid Waste. SW-B46, or Standard Methods for the Examination of Water and Wastewater.

All results are in mg/l unless otherwise noted. No. /

Sample Description Method No. Parameter


253394 253395 253396 253397

RF07-FB1-041995-B309:04/19/95 (Water) RF07—SWD-041995-B309:04/19/95 (Water) RF07-SWD-041995A-B309:04/19/95 (Water) RF07-TB1-041995-B309:04/19/95 (Water)

Result

C

c c c

Comments/Notes


< Last Page > Submitted By : •/ ) A A Aquatec Inc

fa,** fU /2/S. 55 South Park Drive • Colchester, VT 05446 • Tel: 802-655-1203 • Fax: 802-655-1248



Date: 01 May 1995 Aquatec Lab No.: 253394 ETR No.: 50652; Project No.: 94246 Sample Received On: 20 April 1995; Analyzed On: 21 April 1995 Sample Identification: Hull & Associates, water sample labeled

RF07-FB1-041995-B309, 04/19/95 at 1043 hours.







benzene 5 U chloromethane ip p carbon tetrachloride 5 U bromomethane Tp p chlorobenzene 5_U brornoform 5_U

1 ^-dichloroethane 5 U bromodichloromethane 5 p 1111 trichloroethane 5 U dibromochloromethane 5 p jL, 1-dichloroethape 5 U tetrachloroethene 5 p 1.1.2- trichloroethane 5_jj toluene y l_i.l.2.2- tetrachloroethane 5 U trichloroethene 5 p chloroethane 10 U vinvl chloride ip p chloroform 5 U acetone ip p

^" dichloroethene 5 U 2 -butanone ip p 1,2- dichloroethenes 5 U carbon disulfide 5 p 1,2-dichloropropape 5_U 2-hexanone jp u trans-1,3-dichloropropene 5_U 4-methvl-2-oentannne jp u cis -1. 3 -dichloropropene 5_U stvrene y ethylbenzene 5 U vinvl acetate ip p methylene chloride 5 U total xylenes 5 u








Inch cape Testing Services Aquatec Laboratories


Laboratory Location! 35 South Park Drive Colchester, VT 03446



Date: 01 May 1995 Aquatec Lab No,: 253397 ETRNo.: 50652; Project No.: 94246 Sample Received On: 20 April 1995; Analyzed On: 21 April 1995 Sample Identification: Hull & Associates, water sample labeled

RF07-TBI-041995-B309, 04/19/95 at 1047 hours.

benzene carbon tetrachloride


5 U chloromethane


1.2-dichloroethane 5 U bromoform

1.1.1-trichloroethane 5 U bromodichloromethane

1.1-dichloroethane 5 U dibromochloromethane

1.1.2-trichloroethane 1.1.2.2-tetrachloroethane

5 U tetrachloroethane 5 U toluene

chloroethane 5 U trichloroethene.

chloroform 10 U vinvl chloride 5 U

1.1-dichloroethene acetone

1.2-dichloroethenes 5 U 2-butanone

1.2-dichloropropane 5 U carbon disulfide

trans -1.3-dichloropropene 5 U- 2-hexanone

cis-1.3-dichloropropene JLJI 4-methvl-2-nentanona

ethvlbenzene stvrene

methylene chloride vinvl acetate

5 U total xylenes

10 U 10 U 5 U 5 U 5 U 5 U 5 U 5 U 10 U 10 U 10 U 5 U 10 U 10 U -5JI 10 U 5 U




LCB -

C -

Compound was found but at low concentration, comparable to that in the blank. Quantitation is not possible.

The result has been corrected for the presence of the compound in the blank.








150 Herman Melvilte Boulevard New Bedford, MA 02740

Date: 01 May 1995 Aquatec Lab No.: 253396 ETR No.: 50652; Project No.: 94246

Sample Received On: 20 April 1995; Analyzed On: 20 April 1995 Sample Identification: Hull & Associates, water sample labeled

RF07-SWD-041995A-B309, 04/19/95 at 1038 hours.


benzene—. 5 U chloromethane X0 u carbon tetrachloride 5 U bromomethane X0 U chlorobenzene 5 U bromoform 5 i-...*.2-dichloroethane 5 U bromodichl'oromethane 5 u 1 • 1,1-trichloroethane 5 U dibromochloromethane 5 u 1,1-dichloroethane 5 U tetrachloroethene 3J

11•2"trichloroethane 5 U toluene 5 u 1,1,2,2- tetrachloroethane 5 U trichloroethene 5 {j chloroethane 10 U vinvl chloride X0 U sfrloroform 5 U acetone X0 U 1 • 1-dichloroethene 5 U 2-butanone xo U 1., 2- dichloroethenes 5 U carbon disulfide 5 xj 2 -^jchlofopyopane _ 5 U 2-hexanone X0 U

trans -1, 3 -dichloronropene 5_U 4-methvl-2-pentanone X0 U cis-1. 3-dichloropropene 5_u stvrene y

ethyfbenzene 5 U vinvl acetate X0 U methylene chloride 5jj total xylenes . 5 \j










Date: 01 May 1995 Aquatec Lab No.: 253395 ETR No.: 50652; Project No.: 94246 Sample Received On: 20 April 1995; Analyzed On:,20 April 1995 Sample Identification: Hull & Associates, water sample labeled

RF07-SWD-041995-B309, 04/19/95 at 1035 hours.


benzene 5 U chloromethane IP p carbon tetrachloride 5 U bromomethane ip p chlorobenzene ; 5_U bromoform 5_JJ 1.. 2 - dichloroethane 5 U bromodichloromethane 5 u 1,1,1- trrchloroethane 1J dibromochloromethane •• 5 p 1,1-dichloroethane 5 U tetrachloroethene 5 p 1 ^» 2 - trichloroethane 5 U toluene 5 u 1.1.2.2- tetrachloroethane 5 U trichloroethene 5 p chloroethane 10 U vinvl chloride XQ p chloroform 5 U acetone XQ p -!-• l~dichloroethene 5 U 2-butanone | XQ U 1. 2-dichloroethenes 5_U carbon disulfide 5 p 1, 2-dichloropropane 5 U 2-hexanone XQ U trans -1. 3-dichloropropene 5 U 4 - me thvl - 2 - pentanone XQ U cis-1. 3-dichloropropene 5_U stvrene 5 p ethylbenzene 5 U vinvl acetate XQ U methylene chloride 5 U total xylenes 5 u












J/ Hull Sc Associates, Inc.


FAX: (603) 472-37§3


white —i>e use (must ec returned wtth report) TEL LOW —l>a USE PINK —RETAINED ST HM


SAlb-Y#

7- 'NTXB-MFFLSA-W x </r?n ~rr?i YTRM- M-A/MS-TM

RELWQUISHEGBY: J

NFEE LZWU RELINQUISHED 8Y:

RELINQUISHED BY:

RELINQUISHED BY:

DATE

TIME

DATE

TIME

DATE

TIME

RECEIVED- BY: ME, RECEIVED BY:

RECEIVED BY:

RECEIVED FOR 1^8 BY:

. A 4 T

DATE

TIME

DATE

TIME

DATE X-

Deliver To:

Method of Delivery:

Airbill Number:

CBRO/- CRXMHHC>R/(

NOTES:

OFF/0999DIII





Job:NHB019

Lsooratory Location!




Date ; 06/08/95 ETR Number : 51538 Project No.: 94246 No. Samples: 4 Arrived : 06/01/95

Page

T , . A i l r e s u l t s a r e I n m g / l u n l e s s o t h e r w i s e n o t e d . Ltao NO./

Sample Description Method No. Parameter Result


258368 258369 258370 258371

RF07-FB1-053195-B309:05/31/95 (Water) RF07-SWD-053195-B309:05/31/95 (Water) RF07--SWD-053195A-B309:05/31/95 (Water) RF07-TB1-053195:05/31/95 (Water)

C C C C

Comments/Notes


< Last Page > Submitted By : „ Aquatec Inc.


Inchcape Testing Services ~ Aquatec Laboratories






Date: 08 June 1995 Aquatec Lab No.: 258369 ETRNo.: 51538; Project No.: 94246; Job: NHB019 Sample Received On: 01 June 1995; Analyzed On: 05 June 1995 1

Sample Identification: Hull & Associates, Inc., water sample labeled 1

RF07-SWD-053195-B309, 05/31/95.


benzene 5 U chloromethane lp u carbon tetrachloride 5 U bromomethane lp jj chlorobenzene 5 U bromoform 5 p 1.2-dlchloroethane 5 U bromodichloromethane 5 u 1.1.1-trichloroethane 5 U dibromochlorome thane 5 u 1.1-dichloroethane 5 U tetrachloroethene 3j

1.1.2- trichloroethane 5_U toluene ; 5 y

1.1.2.2 - tetrachloroethane 5_U trichloroethene 5 u chloroethane 10 U vinvl chloride 1Q u chloroform 5 U acetone jp u 1.1- dichloroethene 5_JJ 2-butanone jp u 1.2-dichloroethene s 5JJ carbon disulfide 5 u 1.2- dichlorooropane 5 U 2-hexanone jp u trans -1. 3 -dichloropronene 4 - me thvl - 2 - pentanone jp u cls-1.3-dichloropropene 5 U stvrene 5 u ethylfrenzene 5 U vinvl acetate jp u methylene chloride 5_U total xylenes 5 u

Sitmnpry of Surrogate Recoveries

* Rec l,2-dichloroethane-d4 94 toluene-dg 99 1 p-bromofluorobenzene 100




B - The compound was present in the method blank. The result reported here is not blank corrected.




Laboratory Location!

53 SouthPark Drive Colchester, VT 05446



Date: 08 June 1995 Aquatec Lab No.: 258370

ETR No.: 51538; Project No.: 94246; Job: NHB019 Sample Received On: 01 June 1995; Analyzed On: 06 June 1995 Sample Identification: Hull & Associates, Inc., water sample labeled

RF07-SWD-053195A-B309, 05/31/95.

benzene

carbon tetrachloride


5 U chloromethane


10 U

1.2-dichloroethane _L_U bromoform

10. U

5 U 1.1.1-1richloroe thane 1.1-dlchloroethane

bromodichloromethane dibromochloromethane

J_U

1.1.2-trichloroethane

A_U -5_U tetrachloroethene

5 U

1.1.2.2-tetrachloroethane 5 U toluene

21.

chloroethane 5 V trIchloroethene

ZM chloroform

AO vinvl chloride 5 U

5 U 10 u

1.1-dlchloroethene acetone

1.2-dichloroethenes 5 U 2-butanone

10 U

1.2-dichlorooropane 5 U carbon disulfide

10 U

trans -1.3-dichlorooronene 5 U 2-hexanone

-O

cis-1.3 -dichloronropene 5 U 4-me thvl-2-pentanone

10 U

ethvlbenzene o 5 U

10 U styrene

methylene chloride vinvl acetate

-O

5 U total xylenes 10 U _LU

Snmma^y of Surrogate Recoveries

X Rec 1,2-dichloroethane-d4 97 toluene-dg 101 i p-bromofluorobenzene 103




B - The compound was present in the method blank. The result reported,here is not blank corrected.









Date: 08 June 1995 ETRNo.: 51538; Project No.: 94246; Job: NHB019 Blank Identification: Blank CNSB002BV for Aquatec Lab No's. 258368 -

• 258371.


benzene 5 U chloromethane 1Q u carbon tetrachloride 3_U bromomethane jp u chlorobenzene 5_U bromoform 5 u 1.2- dichloroethane 5 U bromodlchloromethane ' 5 u 1.1.1- trichloroe thane 5 U dibromochloromethane 5 u 1.1-dichloroethane 5 U tetrachloroethene 5 U 1.1.2- trichloroe thane 5_U toluene 5 U 1.1.2.2- tetrachloroethane L_U trichloroethene 5 U chlorvethane ; 10 V vinvi chloride 10 u chloroform 5_U acetone 10 u 1.1- dichloroethene 5_JJ 2-butanone 10 u 1.2-dichloroethene s 5 U carbon disulfide 5 U 1.2-dlchlorooropane 5JJ 2-hexanone : 1Q u trans -1.3 -dlchloropropene 5_U 4-methvl-2-pentanone 10 U cis-1. 3 -dichloropropene 5_U stvrene 5 U ethvlbenzene 5_U vinvl acetate 10 u methylene chloride 5 U total xylenes 5 U

Snmn^ry of Surrogate Recoveries X Rec

l,2-dichloroethane-d4 101 toluene-dg 103 p-bromofluorobenzene 101







Date: 08 June 1995 Aquatec Lab No.: 258368 ETRNo.: 51538; Project No.: 94246; Job: NHB019 Sample Received On: 01 June 1995; Analyzed On: 05 June 1995 Sample Identification: Hull & Associates, Inc., water sample labeled

RF07-FBI-053195-B309, 05/31/95.


benzene 5 U chloromethane lp u carbon tetrachloride 5 U bromomethane 1Q p chlorobenzene 5_U bromoform 5 IJ 1.2 -dichloroethane 5 U bromodichloromethane 5 u 1.1.1- trichloroethane 5 U dibromochloromethane 5 u 1.1- dichloroe thane ; 5 U tetrachloroethene , 5 u 1.1. 2- tr ichloroethane 5_U toluene 5 p 1 , 1 , 2 . 2 - t e t r a c h l p i T b ^thA^ trichloroethene 5 U chloroethane 10 U vlnvl chloride lp p chloroform 5 U acetone 1Q p 1.1- dichloroethene O 2-butanone ; jp u 1.2-dlchloroethene s 5_U carbon disulfide ; 5 u 1.2- dichloropropane 5_JJ 2-hexanone lp u trans -1.3- dichloropropene 5_U 4 - me thvl - 2 -oentanone lp u cis-1.3-dichloropropene stvrene 5 p ethvlbenzene __ 5 U vinvl acetate jp p methylene thlotid? 5 U total xylenes 5 u

Laboratory Locations 55 South Park Drive Colchester. VT 05446

75 Green Mountain Drive South Burlington. VT 05403


Summary of Surrogate Recoveries X Rec

1,2-dichloroethane-d4 94 toluene-dg 1P2 p-bromofluorobenzene 101






^=8 Inchcape Testing Services Aquatec Laboratories


Date: 08 June 1995 Aquatec Lab No.: 258371 ETRNo.: 51538; Project No.: 94246; Job: NHB019 Sample Received On: 01 June 1995; Analyzed On: 06 June 1995 Sample Identification: Hull & Associates, Inc., water sample labeled

RF07-TBI-053195, 05/31/95.






benzene 5 U chloromethane 1Q u carbon tetrachloride 5 U bromomethane ip u chlorobenzene 5 U bromoform •' 5 U 1.2-dichloroethane 5 U bromodichloromethane 5 u 1.1.1- trichloroethane 5 U dibromochlorome thane 5 u 1.1-dichloroethane 5 U te trachloroe thene 5 p 1.1.2- tr ichloroethane £_JJ toluene 5 U 1, J., 2, z- mractqpFpetfaine 2_u trichloroethene 5 U chloroethane 10 U vinvl chloride jp u chloroform 5 U acetone jp u l,l,-dl,(?hloroethene 5_il 2-butanone IP u 1.2 -dichloroethenes §_JJ carbon disulfide 5 p l,^-4ichloiT9pi:opan? 5_U 2-hexanone 10 U trans -1.3- dichloropropene 5_U 4 - me thvl - 2 - oentanone 1Q u cis -1.3 -dichloropropene 5 U stvrene 5 p ethyjbensene 5_U vinvl acetate 10 U methylene chloride 5_JJ total xylenes 5 u

Summary of Surrogate Recoveries * Rec

1,2-dichloroethane-d4 94 toluene-dg 102 p-bromofluorobenzene 104






624

Laboratory Fortified Blank

Lab Name: Inchcape Testing Services - Aquatec Laboratories. Client: Hull & Associates, Inc.

Project: 94246 ETR: 51538

Client No.: LFB-CNS-B Filename: CNS001BQV

Compound Name Amount Spike

Added Percent

Recovery chloromethane

bromomethane

vinyl chloride

chloroethane

methylene chloride

acetone

carbon disulfide

1.1-dichloroethan e

1,1 -dichloroethane

1.2-dichloroethene (total),

chloroform

1.1-dichloroethan e

2-butanone

1,1,1 -trichloroethene

carbon tetrachloride

bromodichloromethane

1.2-dichforopropan e

cis-1,3-dichloropropene....

trichloroethene

benzene

dibromochloromethane

1,1,2-trichloroethane

trans-1,3-dichloropropene.

bromoform

4-methyl-2-pentanone

2-hexanone

1,1,2,2-tetrachloroethane.

tetrachloroethene

toluene

chlorobenzene

ethylbenzene

styrene

xylene (total)

13.73

9.63

9.94

10.28 9.95

18.46

9.78

8.86 9.39

18.78

9.92

10.47

11.09

8.01 8.09

6.78

8.19

6.84

8.73

9.31

6.30

8.59

5.69

7.17

8.50

8.70

9.28

9.42

9.95

10.11 9.14

9.68

27.82

10 10 10 10 10 10 10 10 10 20 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10

10 10

10 10 30

137

96

99

103

100 185

98

89

94

94

99

105

111

80 81 68 82 68 87

93

63 86 57

72

85

87

93

94

100 101

91

97

93



FAX: (603) 472-3763


WHfU LAB USE (MUST BE RETURNED WTTH REPORT) YELLOW —1*0 USE PMK —RETAM ED BY HAJ


REPORT TO:

Client:

Site: SMPSk) =>

Project: A)/F£$/9 Pmjprt §: Samplers: 1

SAMPLE IDENTIFICATION

%77- S

Y^>7'S^^-0S3I95A~-Z. "KHOI - /7?/ ^PFB7- //?./-

/ PRESERVATIVES

ANALYSES

SAMPLE MATHMC PWtSCHWHMS MfTNS A - Cool only. <4* C f - FILTERED 8 - HNO. pH<2 " " FILTERED C - HJSOJ pH<2 " "

1. WATER 2. SOI J. SLUOCE 4. OR.

OTHER: £ ~

0FF/O9990JH

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QUARTERLY GROUND-WATER MONITORING REPORT FIFTH …