Novozymes Innovation Citrus 1212

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    Enzymes for CitrusProcessing

    NovozymesCustomer SolutionsStatus Nov 2012

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    Slide No. 2

    Main Applications in Citrus Processing

    *

    0

    / ( )

    (

    / *

    * by products

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    Slide No. 3

    Juice-Sacs

    Peel-Pellets

    Juice By-

    Pro-

    ducts

    Juice

    Fruit

    Water-Oil

    Pulp

    Peel/Core

    Separators

    Sludge

    Water

    20%

    Fresh

    Solution

    20%

    Pulp-Wash

    max

    10%

    Cloudyfier

    E

    ++

    OilCitrozym

    Cloudy

    E

    E

    The Use of Enzymes during Citrus Juice Processing

    Essential Oil Extraction

    Pulp-Wash/Core Wash

    Cloudy Peel Extract

    Viscocity reduction

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    Slide No. 4

    1st centrifuge

    Oil Extraction

    Finisher

    Oil-water Emulsion

    2nd centrifuge

    Essential Oil

    Oil-phase

    Citrozym CEO

    (or NZ 33095)

    Buffertank

    SOLIDSSLUDGE

    centrifuge

    SOLIDSSLUDGE

    Recovery of Essential Oil

    Citrozym CEO

    (or NZ 33095)

    Citrozym CEO

    (or NZ 33095)

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    Slide No. 5

    Higher yield due to easier emulsion breaking

    improved oil recovery

    10-15% more yield

    optimise the efficiency of the centrifuges

    Excellent oilquality

    Lower water consumption, and less contaminated

    waste water

    reduction of fresh water consumption

    Wast water easy to dump, due to lower BOD

    no investments (only holding tank)

    Advantages using enzyme during Recovery of Essential

    Oil (1)

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    Slide No. 6

    Essential Oil Extraction (2)

    5.7

    6.2

    6.7

    7.2

    7.7

    8.2

    8.7

    9.2

    1 2 3 4 5 6 7 8 9 10 11 av

    Citrozym CEO

    (or NZ 33095)

    3.77 kg/mt

    (8.3 lb./mt)

    control

    Oil yield lb./mt fruit

    trial days

    Industrial trials on oranges,Industrial trials on oranges,

    150,000 boxes/day, Brazil150,000 boxes/day, Brazil

    Result from an industrial trial

    in Brazil during 2

    weeks, processing 6000 tons

    of oranges/day,

    yielding +0,5 kg of oil/ton of

    fruit.

    3.27 kg/mt

    (7.2 lb./mt)

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    Slide No. 7

    Benefits from Citrozym CEO (or NZ 33095)

    on essential oil extraction (3)

    ParametersParametersParametersParameters ControlControlControlControl Citrozym CEO

    (or NZ 33095)Yield of oil

    in kg/ton of fruits

    3.27 3.77 (15% increase!)

    Efficiency of centrifuges

    (yield/capacity) in %

    50 72

    Efficiency of polishing centrifuges

    (yield/capacity) in %

    83 88

    Water consumption minus 35%

    Status of waste water Difficult to bio-degrade Easy to bio-degrade

    Enzyme cost: 100ppm Citrozym CEO (or NZ 33095)

    1200 lt water/hr (water is recicled and needs a correction with 15% additional enzyme per hr)

    1 FMC makes 3.8 tons of oranges/hr

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    Slide No. 8

    Production of PW/CW/WESOSJuice extraction

    Finisher

    pulp juice

    scroll mixers

    several

    Finisher

    Enzymation

    Centrifugation

    Pasteurization

    Concentration

    PW concentrate

    60Bx

    Citrozym Cloudy (or Pectinex SMASH XXL)5-20 ppm / 45C / ~45 min

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    Slide No. 9

    Pulp & Core Wash or WESOS

    Enzyme used for:

    In-line or off-line PW/CW

    Enzymes for extraction and/or viscosity reduction

    limiting production of Gal.Acid

    no separation and avoid clarification

    inactivation with pasteurisation

    Parameters for the Enzymation Citrozym Cloudy (or Pectinex SMASH XXL or Ultrazym AFP-L) 5 - 15 ppm for Pulp Wash

    10 - 20 ppm for Core Wash

    45C

    40 min

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    Slide No. 10

    Production of Natural Cloudy PeelProducts Cloudyfier

    Citrozym Cloudy (or Pectinex SMASH XXL20 - 30 ppm

    Citrozym Cloudy (or Pectinex SMASH XXL)

    10 - 30 ppm

    Cloudyfier 50 BX

    Natural Cloudifier

    Concentration

    Centrifugation

    Pasteurization

    Enzymation

    30 - 60 min, 45C

    Separation

    Decanter

    Enzymation

    1 hour, 45C

    stirring

    Milling

    Water addition

    water : peel = 1:1

    ev. pasteurization

    Peel of

    Orange, Lemon

    or Grapefruit

    Cloudy peel products are

    obtained from citrus

    peels. They are

    extracted by water and

    Citrozyme cloudy (or

    Pectinex SMASH XXL)

    and afterwards

    concentrated to approx

    50Bx. Natural

    cloudyfier are used asbasics for cloudy soft

    drinks industry as as

    they are extreme cloud

    stable.

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    Slide No. 11

    Viscosity reduction orange juice (Navels)Oranges

    Juice extraction

    Finisher

    Enzymation tank

    Pasteurization

    Centrifugation

    Concentration

    Cloudy 65 Bx

    OJ Concentrate

    Citrozym Cloudy (or Pectinex Ultra Clear)

    5-20 ppm

    20- 45 C, 15 - 30 min.

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    Slide No. 12

    Clarification of lemon/lime juiceLemons

    LimesJuiceExtraction

    Finisher

    Enzymationtank

    Clarificationsilica sol

    Centrifugation/

    trad. Filtration

    PasteurizationConcentration

    Clear

    LJ Concentrate

    Citrozym Ultra L

    (or Pectinex Ultra CLear)

    30 - 70 ppm

    15 - 40 C3 - 8 hours

    UF

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    Slide No. 13

    Clarification of lemon and lime juice

    fresh juice or past.& rediluted

    pH (1.8) 2.3 - 2.9

    ambient temp. (max. 45C)

    as lower the pH, as lower temp.

    has to be used

    3 - 6 hours

    trad. filtration or UF

    Citrozym Ultra L (or NZ 33095)

    Juice pectin negative and stable

    Good filterability Low arabian content

    Citrozym Ultra L (or PectinexUltra CLear)

    for production of clear lemonconcentrate

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    Slide No. 14

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    Slide No. 15

    A closer Look at the Technologies

    Whole Peeled Fruit & Fresh-Cut Fruit Segments :

    Orange & Grapefruit using Vacuum Infusion

    Pectinex

    Ultra SP-L

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    Slide No. 16

    Whats it like by enzymatic peeling

    Pectinex Ultra SP-L results in:

    - Highest possible quality

    - Reduced losses duringprocessing

    - Less manual labor costs

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    Citrus fruit processing Reduced viscosity and avoidance of problems in the

    concentration (jellification of concentrated cloudy

    material) Improved extraction of solids

    Maintained cloud stability, if necessary

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    The new NZ 33095 for citrus processing

    Due to its robustness (lowest pH, low and hightemperatures) extremly suitable for lemon

    clarification More and stronger balanced enzyme activities and

    better heat stability even at 60 C (10-60 C)

    Better than competitor non gmo derived enzymes

    Suitable for organic production Suitable for oil extraction

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    Product range Juice 2010

    Pectinex YieldMASH, Pectinex XXL, Amylase AG XXL ourpreferred choice together with Pectinex UF for highest yields and

    capacities and clear stable juices and concentrates

    Pectinex Ultra MASH, Pectinex Ultra Clear (NZ 33105), AmylaseAG 300 L and Pectinex UF for good yield and capacity and clear

    and stable juices and concentrates

    Several other enzymes, e.g. Pectine Ultra AFP (NZ 33109),

    Pectinex Ultra SP-L, Ultrazym AFP-L, Pectinex BE XXL andPectinex Ultra Colour (NZ 33103) to full fill your needs

    NOVOZYMES PRESENTATION20 02/05/2013

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    NOVOZYMES PRESENTATION20 02/05/2013

    We find the magic of nature in a handful of soil or a

    compost heap. Then we turn it into solutions fordetergents, pharmaceutical products, the energy sector andcountless other applications.

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    THANK YOU FORYOUR ATTENTION

    Novozymes is the world leader in bioinnovation.Together with our partners and with juice producersaround the world we create tomorrows industrialbiosolutions, improving our customers businessand the use of our planets resources. Read more

    at www.novozymes.com/juice

    [email protected],