MONTGOMERY WATSON A; ' rooo

MONTGOMERY WATSONRECEIVED

A1; ' roooJanuary 6, 2(XX)

Ms. Diana FingernailEPA Project CoordinatorSuperfund Branch, Waste Management DivisionI'.S. Environmental Protection Agency, Region VII901 N. 5"StreetKansas City, KS 66101

RE: Former Manufactured Gas Plant SiteClinton. IowaDocket No. VII-97-E-(X)2()

Dear Ms. Etnueman:

MW #121743 1.01 1603

S00093169SUPERFUND RECORDS

This letter is intended to serve as the December 1999 monthly progress report for theEngineering Evaluation/Cost Analysis (EE/CA) for the above-referenced site. Thisprogress report was prepared in accordance with the Ju ly 1, 1997 Adminis t ra t ive Order onConsent and is being submitted on behalf of Al l i an t Energv/Inters tate Power Company(Al l i an t Energy/IPC).

December Activities

On-site act ivi t ies in the month of December consisted of transporting the investigationderived water to the Davenport Water Pollution Control Facili ty and cleaning the on-sitewater storage tank. Sludge from the tank was drummed and is stored on site pendingdisposal. Prior to cleaning the tank, the analytical results of a sludge sample were receivedwhich verified the sludge was not a ha/ardous waste. A copy of the analyt ical report iscontained in Attachment A Transportation of the water and cleaning of the tank wereperformed by Enviromark, Inc. of Davenport. Iowa.

During December, the Quality Control reports for additional sediment samples collectedfrom the Mississippi River were received. Montgomery Watson reviewed the reports andvalidated the results. Copies of the analytical report sheets and the Quality Control reportsare contained in Attachment B.

Quality Control reports for several of the groundwater samples were also received late inthe month, with the remaining reports received on January 3, 2(XX). Copies of theanalytical reports and Quality Control reports for all of the groundwater samples wi l l bevalidated and copies submitted once data validation has been completed.

Ms. Diana Engeman Page 2 January 6, 2(KM)

Proposed January Activities

Receipt of the final Quali ty Control reports in i t i a t e s the 45 clay time al lotment forpreparing the draft site characteri/.ation and risk evaluation portions of the EE/CA Report.Throughout January, Montgomery Watson wi l l continue to evaluate the data and preparethe draft documents. Based on receipt of the Quality Control reports on January 3. the sitecharacteri/.ation and risk evaluation is due to the Environmental Protection Agency onFebruary 17, 2(KX).

Also during January, the water storage tank w i l l he removed from the site andMontgomery Watson wi l l coordinate disposal of the tank sludge.

If you have any questions, please feel free to contact Bruce Greer of A l l i an t Energy/IPC orme.

Sincerely,

Randy Kroneman. P.O.Project Manager

/rjk:vasattachmentscc: Bruce A. Greer, Al l iant Energy/IPC

Laura Clemenson, Sverdrup Environmental, Inc.Johanshir Golchin, Iowa Department of Natural Resources (2 copies)

ATTACHMENT A

MONTGOMERY WATSON

keystoneL A B O R A T O R I E S , N O .

RECEIVED

DEC 0 6 £33MW/IOWA

M E M B E R

ACIL

ANALYTICAL REPORTDecember 3. 1999 Page 1 of 4

Report To

Randy KronemanMontgomery- Watson1 1 1 5 3 Aurora Avenue

Des Momes, IA 50322

Sample Information

Work Order: 191 1 091 ~Sample No: 1 9 3 1 0 2 3

Date Collected: 1 1 29 99 ! 1 00 AMDate Received: 1 1 29 99 04:35 PM

Collector: Randy KronemanCollector Phone: 515-253-0830

Matrix: sludee

Site Information/Sample Description

Clinton - FMGP

lank Sludge

Comments

Detection DateAnalyie Analysis Result Limit Method Analyst Analyzed

Determination of TCLP volatile organic compoundsBenzene (TCLP)

Determination of volatile organic compounds.1.1.1 -Tnchloroethane1 , 1 .2.2-Tetrachloroethane1 , 1 ,2-Tnchloroe thane1.1-Dichloroethane1 , 1 -Dichloroethylene1 ,2-Dichlorobenzene1.2-Dichloroethane1 ,2-Dichloropropane1 ,3-Dichlorobenzene1 .4-Dichlorobenzene2-Butanone(MEK)2-Hexanone(MBK)4-Methyl-2-pentanone (MIBK)AcetoneBenzene

< = lessNote This repon ma\ not

< 0.25 mg L

< 0.005 mg'kg< 0.005 mg'kg< 0.005 mg'kg< 0.005 mg'kg< 0.005 mg'kg< 0.005 mg'kg< 0.005 mg'kg< 0.005 mg'kg< 0.005 mg'kg< 0.005 mg'kg< 0.025 mg'kg< 0.025 mg'kg< 0.025 mg'kg

< 0.05 mg'kg0.051 mg'kg

0.25

0.0050.0050.0050.0050.0050.0050.0050.0050.0050.0050.0250.0250.0250.050005

than; ugl, = ppb; mg'L = ppm; mg'kgbe reproduced except in f u l l , w i t h o u t written approv

EPA S260A

EPA S260AEPA 8260AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA S260AEPA 8260AEPA 8260AEPA S260A

= ppmal of the laboratory

EPP

EPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPP

12 03 99

12 02 991 2 0 2 9 91202 9912 '02 '9912029912 '02 9912 02 9912 02 9912 02 991 2 0 2 9 91 2 0 2 9 91 2 0 2 9 91 2 0 2 9 912 02 991 2 0 2 9 9

600 East 17'n Street SouthNewton. IA 50208 • 515-792-8451

3012 Ansborough AvenueWaterloo, IA 50701 • 319-235-4440

1304 AdamsKansas City KS 66103* 913-321-7856

\ keystoneL A B O R A T O R I E S , INC.

M E M B E R

ACIL

Work Order: 1911 0917Sample No: 193102?

Report Date: 12 3 99

Analyte

BromodichloromethaneBromoformBromomethaneCarbon DisulfideCarbon TetrachlondeChlorobenzeneChloroethaneChloroformChloromethanecis- 1 ,2-Dichloroeth\ lenecis-1.3-DichloropropeneDibromochloromethaneEthylbenzeneMethyl-t-butyl Ether (MTBE)Methylene ChlorideTetrachloroethylencToluenerrans- 1 .2-Dichloroethylenetrans- 1 ,3-DichloropropeneTnchloroethylene\'myl ChlorideXylenes, total

Determination of acid extractable(3 & 4)-Methylphenol2.4,5-Tnchlorophenol2,4,6-Tnchlorophenol2,4-Dichlorophenol2,4-Dimethylphenol2,4-Dmitrophenol2-Chlorophenol2-Methylphenol2-Nitrophenol4.6-Dinitro-2-methylphenol

Note This

Site Name / Sample DescriptionClinton - FMGPTank Sludge

Analysis Result

< 0.005 mg "kg< 0.005 mg kg

<0.01 mglcg< 0.005 mglcg< 0.005 mglcg< 0.005 mglcg< 0.005 mgkg< 0.005 mgkg< 0.005 mg kg< 0.005 mgkg< 0.005 mg kg< 0.005 mgkg

0.38 mgkg0.109 mgkg

< 0.025 mgkg< 0.005 mgkg

0.066 mgkg< 0.005 mglcg< 0.005 mg kg< 0.005 mgkg< 0.005 mgkg

0.866 mgkg

organic compounds.<0.33 mglcg< 1.65 mg'kg<0.33 mglcg<0.33 mglcg<0.33 mg'kg< 1.65 mglcg<0.33 mgkg<0.33 mglcg<0.33 mglcg< 1.65 mg'kg

< = less than; ug/L = ppb; mgreport ma\ not be reproduced except in fu l l .

DetectionLimit

0.0050.0050010.0050.0050.0050.0050.0050.00500050.00500050.0050.0250.02500050.0050.00500050.00500050.005

0.331.650.330.330.331 650.330.330.331 65

'L = ppm; mglcg

Method Analyst

EPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA S260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260A

EPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270B

= ppm

EPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPP

FIZFIZFIZFIZFIZFIZFIZFIZFIZFIZ

Page 2 of 4

DateAnalyzed

12 02 9912 02 9912029912 02 9912 02 9912 02 '9912 02 991 2 0 2 9 912 02 9912 02 9912 02 991 2 02 991 2 02 9912 02 9912 029912 02 991 2 0 2 9 91 2 02 991202991202991202 9912 '02 '99

12 '02 '9912029912 '02 '991 2 0 2 9 912 '02 9912 02 991 2 0 2 9 912 029912029912 02 '99

without written approval of the laboratory

600 East 17'h Street SouthNewlon. IA 50208 • 515-792-8451

3012 Ansborough AvenueWaterloo. IA 50701 • 319-235-4440

1304 AdamsKansas City, KS 66103 • 913-321-7856

LfeystoneL A B O R A T O R I E S , INC.

M E M B E R

ACILWork Order: 1911.0917

Sample No: 193102?Report Date: 12 3 99

Analyte

4-Chloro-3-methylphenol4-NitrophenolPeniachlorophenolPhenol

Determination of polynuclearAcenaphtheneAcenaphthyleneAnthraceneBenzo(a)anthraceneBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g.h.i)peryleneBenzo(k jfluorantheneChryseneDibenzo( a,h)anthraceneFluorantheneFluorenelndeno( 1 ,2,3-cd)pyreneNaphthalenePhenanthrenePyrene

Determination of metals.ArsenicBanumCadrruumChromiumCopperIronLeadMercuryNickelSeleniumSilver

Note


Analysis Result

<0.33 mg'kg<0.66 mgkg< 0.66 mgkg<0.33 mgkg

aromatic hydrocarbons.<0.05 mg'kg<0.05 mg'kg

10. mg'kg6.2 mgkg6.8 mg'kg6.6 mg'kg5.7 mg'kg2.6 mgkg7.7 mg'kg

<0.05 mg'kg13.5 mgkg12.9 mg'kg28.4 mg'kg

<0.05 mg'kg36.3 mg'kg21.8 mg'kg

5.7 mg/kg94. mg'kg

< 2. mg/kg21. mg'kg20. mgkg

13.500. mg'kg34. mg'kg

<0.5 mg'kg22. mgkg

< 2. mgkg<3. mg'kg

< = less than; ug/L = ppb; mgThis report ma> not be reproduced except in full ,

DetectionLimit

0.330.660.660.33

0.050.050.50.50.50.50.050.50.50.050.50.50.050.050.050.5

2.1.2.3.3.

3.5.0.55.2.3.

'L = ppm; mg'kgwithout written approva

Method

EPA 8270BEPA S2-OBEPA 8270BEPA 8270B

EPA 83 10EPA 83 10EPA 83 10EPA 83 10EPA 8310EPA 8310EPA 8310EPA 8310EPA 83 10EPA 83 10EPA 83 10EPA 83 10EPA 83 10EPA 83 10EPA 83 10EPA 8310

EPA 7060EPA6010AEPA6010AEPA6010AEPA6010AEPA6010AEPA ^421EPA 7471EPA6010AEPA 7740EPA6010A

= ppm1 of the laboratory

Analyst

F1ZFIZF1ZFIZ

FWMFWMFWMFWMFWMFWMFWMFWMFWMFWMFWMFWMFWMFWMFWMFWM

LARLARLARLARLARLARKJSBNSLARLARLAR

Page 3 of 4

DateAnalyzed

12 02 9912 029912 02 99120299

1 2 0 2 9 912 02 '991202 991 2 02 9912 02 9912 02 991202 991 2 0 2 9 91202 991202991202 991202991202991202 99120299120299

12/01/99120T991 2 0 1 9 91 2 0 1 9 912019912019912 01 991202 991 2 0 1 9 91201 9912'01 99

600 East 17th Street SouthNewlon. IA 50208 • 515-792-8451


1304 AdamsKansas City. KS 66103 • 913-321-7856

keystoneL A B O R A T O R I E S , INC.

M E M B E R

ACIL\VorkOrder: 1911 091'

Sample No: 193102?Report Date: 12 ? 99


Page 4 of 4

Analvte Analysis ResultDetection

Limit MethodDate

Analyst Analyzed

Zinc 110. mg"kg 3. EPA6010A LAR 1 2 0 1 9 9

Determination of general chemistry parameters.Cyanide, total 3.2 mgkg 1. EPA 9010A KJS 113099Nitrogen, Ammonia < 75. mglcg 75. EPA 350.2 MMM 113099Percent Solids 17.3% EPA BNS 113099Sulfate < 1,000. mgkg 1.000. EPA 300.0 F\VM 120299

Kevstone L&ooratones, We.

< = less than; ug/L = ppb: mg'L = ppm; mglcg = ppmNote This report ma> not be reproduced except in f u l l , without written approval of the laboratop.

600 East 17'h Street SouthNewton, IA 50208 • 515-792-8451



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ATTACHMENT B

MONTGOMERY WATSON


RECEIVEDO C T 2 9 1999

MW/IOWA

M E M B E R

ACII

ANALYTICAL REPORTOctober 28. 1999 Page 1 of 4

Report To

Randy KronemanMontgomery- Watson1 1 1 5 ? Aurora Avenue

Des Motnes. IA 50322

Sample Information

Work Order: 1909 1066Sample No: 1925496

Date Collected: 09 29 99 1 1 :?5 AMDate Received: 09 30 99 1 1 : 1 6 AM

Collector: Randy KronemanCollector Phone: 515-253-OS30

Matrix: soil


Clinton FMGP

MR09-RS-001

Comments

Detection DateAnalyte Analysis Result Limit Method Analyst Analyzed

Determination of volatile organic compounds.1 . 1 . 1 -Tnchloroethane1 , 1 ,2,2-Tetrachloroethane1 . 1 ,2-Tnchloroethane1.1-Dichloroethane1 . 1 -Dichloroethylene1 ,2-Dichlorobenzene1,2-Dichloroethane1,2-Dichloropropane1 ,3-Dichlorobenzene1 .4-Dichlorobenzene2-Butanone ( M E K )2-Hexanone(MBK)4-Methyl-2-pentanone (MIBK.)AcetoneBenzeneBromodichloromethaneBromoformBromomcthane

Note

< 0.001 mglcg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.005 mg'kg< 0.005 mg'kg< 0.005 mg'kg

<0.01 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.002 mg'kg

< = less than: ug'L = ppb: mgThii report ma> not he reproduced except in fu!!.

0.0010.0010.0010.0010.0010.0010.0010.0010.0010.0010.0050.0050.0050.010.0010.00100010.002

L = ppm: mg *kg

EPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8 2 60 A

= ppm

EPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPP

10 129910 12 '9910 12 9910 12 9910 12 9910 12'9910 12'9910 12/9910 12'9910 12 9910 12 9910 12 9910 129910 12 9910 129910 12 9910 12 9910 12 99

without written approval of the laborator\

600 East 17th Street SouthNewton, IA 50208 • 515-792-8451


1304 AdamsKansas City. KS 66103 • 913-321 -7856


M E M B E R

ACIL

Work Order: 1909.1066Sample No: 1925496


Analyte

Carbon DisulfideCarbon TetrachlondeChlorobenzencChloroethaneChloroformChloromethanecis- 1 ,2-Dichloroethylenecis-1.3-DichloropropeneDibromochloromethaneEthylbenzeneMethy l - t -bu ty l Ether ( M T B H )Methylene ChlorideTerrachloroethyleneToluenetrans-1.2-Dichloroethylenetrans- 1 .?-DichloropropeneTrichloroethyleneVinyl ChlorideXylenes. total

Determination of acid extractable(3 &4)-Methylphenol2.4.5-Tnchlorophenol2.4,6-Tnchlorophenol2.4-Dichlorophenol2.4-Dimethylphenol2,4-Dinitrophenol2-Chlorophenol2-Methylphenol2-Nitrophenol4.6-Dinitro-2-meth\ Iphenol4-Chloro-?-meth\ Iphenol4-NitrophenolPentachlorophenol

Note This

Site Name / Sample DescriptionClinton FMGPMR09-RS-001

Analysis Result

< 0.001 mg'kg< 0.001 mg'kc< 0.001 mg'kg< 0.001 mg'kc< 0.001 mg'kc< 0.001 mg'kc< 0.001 mg'kc< 0.001 mgl;g< 0.001 mg'kc< 0.001 mg'kc< 0.005 mgl;c< 0.005 mg'kc< 0.001 me Teg< 0.001 mg'kc< 0.001 mg'kc< 0.001 mg'kc< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg

organic compounds.<0.33 mg'kg< 1 .65 mg'kg<0.33 mg'kg< 0.33 mg'kg< 0.33 mg'kg< 1.65 mg'kg<0.33 mg'kg< 0.33 mg'kg< 0.33 mg'kg< 1.65 mgkg<0.33 mg'kg<0.66 mg'kc< 0.66 mglcc

< = less than; ug/L = ppb; mg L

DetectionLimit

0.0010.0010.0010.0010.0010.0010.00100010.0010.00100050.00500010.0010.0010.0010.00100010.001

0.331.650.330.330.331.650.330.330.331.650.330.660.66

= ppm; mg'kg

Method

EPA 8260AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA S260AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260A

EPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270B

= ppm

Analyst

EPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPPEPP

FIZFIZFIZFIZFIZFIZFIZFIZFIZFIZFIZFIZFIZ

Page 2 of 4

DateAnalyzed

10 129910 129910 129910 12 9910 12 9910 129910 129910 12 9910 12 9910 12 9910 129910 129910 129910 129910 12 9910 12 9910 129910 12 9910 1299

10 09 '9910099910/09 '9910 '09 99100999100999100999100999100999100999100999100999100999

report ma\ not be reproduced except in ful l , without vmtten approval of the laboratory

600 East 17'h Street SouthNewton. IA 50208 • 515-792-8451


1304 AdamsKansas City, KS 66103 • 913-321 -7856


M E M B E R

ACIL




DetectionAnalyte

Phenol

Determination of polvnuclearAcenaphtheneAcenaphthyleneAnthraceneBenzol a (anthraceneBenzol a (pyreneBenzol btfluorantheneBenzol g.h.ilperyleneBenzol k (fluorantheneChryseneDibenzol a. h (anthraceneFluorantheneFluoreneIndeno( 1 .2.3-cd)pvreneNaphthalenePhenanthrenePyrene

Determination of metals.ArsenicChromiumCopperIronLeadNickelZinc

Analysis Result

< 0.33

aromatic hydrocarbons.<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01

<24.8

< 33,080.

< 5.<510.

mg^g

mg'kgmg'kgmg'kgmg'kgmg'kgmg'kgmg'kgmg'kgmg'kgmg'kgmg'kgmg'kgmg'kgmglcgmg'kgmg'kg

mg'kgmg'kgmg'kgmg'kgmg'kgmg'kgmg'kg

Limit

0

0000000000000000

23

33553

.33

.01

.01

.0101

.01

.0101.01.01.0101.01.01.01.0101

Method

EPA

EPAEPAEPAEPAEPAEPAEPAEPAEPAEPAEPAEPAEPAEPAEPAEPA

EPAEPAEPAEPAEPAEPAEPA

8270B

8310831083108310831083108310831083108310831083108310831083108310

70606010A6010A6010A74216010A6010A

Analyst

F1Z


LKMLARLARLARKJSLARLAR

Page 3 of 4

DateAnalyzed

10

10101010101010101010101010101010

10101010101010

09

12121212121212121212121212121212

050505'05'080505

99

99999999999999999999999999999999

9999'99'99'999999

Determination of general chemistry parameters.Cyanide, totalNitrogen. AmmoniaPercent SolidsSulfate

Note

< 1.<30.

82.7< 1,000.

mg'kgmg'kg%mg'kg

130

1.000

EPAEPAEPAEPA

9010A350.2

3000

MMMMMMBNS

FWM

10101010

04'07'0407

'99999999

< = less than; ug/L = ppb; mg'L = ppm; mg'kg = ppmThis report ma> not be reproduced except in f u l l , w i t h o u t written apprmal of the laboratory

600 East 17tn street SouthNewton. IA 50208 • 515-792-8451




M E M B E R

ACILWork Order: 1909.1066

Sample No: 1925496Report Date: 102899

Site .Name / Sample DescriptionClinton FMGPMR09-RS-001

Page 4 of 4


Limit MethodDate

Analyst Analv/ed

— ^ r - - TKeystone Laborat&nes. Inc.

< = less than; ug/L = ppb; mg 'L = ppm; mg'kg = ppmNote This report ma\ not be reproduced except in fu l l , wi thout written appro\al of the laboratory

600 East 17th street SouthNewton, IA 50208 • 515-792-8451




M E M B E R

ACIL


Report To

Randy KronemanMontuomery-Watson1 1 1 5 ? Aurora Avenue

Des Momes. IA 50322

Sample Information

Work Order: 1909 1066Sample No: 192549"

Date Collected: 09 29 99 1 1 55 AMDate Received: 09 30 99 1 1 : 1 6 AM

Collector: Randy KronemanCollector Phone: 515-253-OS30

Matrix: soil


Clinton FMGP

MR10-RS-001

Comments


Determination of volatile organic compounds.1.1.1 -Tnchloroethane1 . 1 ,2.2-Tetrachloroethane1 , 1 .2-Tnchloroethane1,1-Dichloroethane1 , 1 -Dichloroethylene1 ,2-Dichloroben2ene1,2-Dichloroethane1 ,2-Dichloropropane1 ,3-Dichlorobenzene1 ,4-Dichloroben?ene2-Butanone ( M E K )2-Hexanone(MBK)4-Methyl-2-pentanone (MIBK)AcetoneBenzeneBromodichloromethaneBromoformBromo methane

Note

< 0.001 mg'kg< 0.001 mg'kg< 0.001 mglcg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mglcg< 0.001 mg'kg< 0.001 mg'kg< 0.005 mg'kg< 0.005 mg'kg< 0.005 mg'kg


< = less than; ug'L = ppb: mgL :

This report ma> not he reproduced exccpl in fu l l , with

0.0010.0010.0010.0010.0010.0010.0010.0010.0010.0010.00500050.0050.010.0010.0010.0010.002

= ppm; mg'kg

EPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 82 60 AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260A

= ppm


10 12 9910 12 9910 12 9910 12 9910 129910 12'9910 12'9910 12'9910 129910 12 9910 12 9910 12 '9910 12 9910 12 9910 12 9910 129910 129910 12 99

out written approval of the lahorator%





M E M B E R

ACIL



Analyte

Carbon DisulfideCarbon TetrachlondeChlorobenzeneChloroethaneChloroformChloromethanecis- 1 .2-Dichloroethylenecis-1.3-DichloropropeneDibromochloromethaneEthylbenzeneMethyl-t-butyl Either ( M T B E )Methylene ChlorideTetrachloroethyleneToluenetrans- 1 .2-Dichloroethylenetrans- 1 .3-DichloropropeneTnchloroethyleneVinyl ChlorideXylenes, total

Determination of acid extractable(3 & 4)-Methylphenol2,4,5-Tnchlorophcnol2,4,6-Tnchlorophenol2,4-Dichlorophenol2,4-Dimethylphenol2,4-Dimtrophenol2-Chlorophenol2-Methylphenol2-N'itrophenol4.6-Dinitro-2-meth> Iphenol4-Chloro-3-methylphenol4-N'itrophenolPentachlorophenol

Note This


Analysis Result

< 0.001 mg'kg< 0.001 mg leg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg"kg< 0.001 mglcg< 0.005 mg'kg< 0.005 mg'kg< 0.001 mg'kg< 0.001 mgkg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg

organic compounds.<0.33 mg'kg< 1.65 mg.'kg<0.33 mg'kg<0.33 mg'kg<0.33 mg'kg< 1.65 mg'kg<0.33 mg'kg<0.33 mg'kg<0.33 mg'kg< 1.65 mg'kg< 0.33 mg'kg< 0.66 mg'kg< 0.66 mg'kg

< = less than; ug'L = ppb: mgreport may nol be reproduced except in f u l l .

DetectionLimit

0.0010.0010.0010.0010.0010.0010.0010.0010.0010.0010.0050.0050.0010.0010.0010.0010.0010.0010.001

0.331.650.330.330.331.650.330.330.331.650.330660.66

'L = ppm; mg'kg

Method

EPA 8 2 60 AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260A


= ppm

Analyst



Page 2 of 4

DateAnalyzed

10 129910 129910 12 9910 129910 129910 12 9910 12 9910 129910 12 9910 12 9910 129910 12 9910 12 9910 12 9910 129910 129910 129910 12 9910 12 99

10099910/09 '9910/09 '9910099910099910099910099910 '09 '99100999100999100999100999100999

ui lhou l written approval of the laboratory

600 East 1 ?th Street SouthNewton. IA 50208 • 515-792-8451




M E M B E R

ACII



Analyte

Phenol

Determination of poh nuclearAcenaphtheneAcenaphthyleneAnthraceneBenzo< a lanthraceneBenzo(a)p\reneBenzol b (fluorantheneBenzol g.h.i iperyleneBenzo( k ifluorantheneChryseneDibeazo( a. h lanthraceneFluorantheneFluoreneIndeno( 1.2,3-cd)pvreneNaphthalenePhenanthrenePyrene



Analysis Result

<0.33 mgkg

aromatic hydrocarbons.<0.01 mgkg<0.01 mgkg<0.01 mgkg<0.01 mgkg<0.01 mg'kg<0.01 mgkg<0.01 mg'kg<0.01 mg'kg<0.01 mgkg<0.01 mgkg<0.01 mgkg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg< 0.01 mg'kg<0.01 mg'kg

< 2. mg'kg5.2 mgkg

< 3. mg'kg3,530. mg'kg

< 5. mg'kg5.2 mg'kg8.1 mg'kg

DetectionLimit

0.33

0.010.010.010010.010.010010.010.010010.010.010.010.010.010.01

2.3.3.3.5.5.

3.

Method

EPA 8270B

EPA8310EPA 83 10EPA 83 10EPA 83 10EPA 83 10EPA 83 1 0EPA 8310EPA 8310EPA 83 10EPA 83 10EPA 83 10EPA 83 10EPA 83 10EPA 83 10EPA 8310EPA 83 10

EPA 7060EPA 6010AEPA6010AEPA6010AEPA 7421EPA6010AEPA6010A

Analyst

F1Z

F\VMFWVIFWMF\VMFWMF\VMFWMFWMFWMFWMFWMFWMFWMFWMFWMFWM


Page 3 of 4

DateAnalyzed

100999

10 129910 129910 12 9910 129910 129910 129910 12 9910 129910 12 9910 12 9910 129910 129910 129910 12 9910 129910 1299

10059910059910 '05 '9910/05 '9910 08 '991005 991005 99


Sole

< 1. mg'kg<30. mgkg81.3 %

< 1.000. mg'kg

< = less than; ug^L = ppb; mgThis report ma> not be reproduced except in full.

1.30.

1.000.

EPA9010AEPA 350.2EPAEPA 300.0

MMMMMMBNSFWM

1004991007 991004991007 99

'L = ppm; mg'kg = ppmwithout written approval of the laboratory

600 East 1?th Street SouthNewlon, IA 50208 • 515-792-8451


1304 AdamsKansas City, KS 66103* 913-321-7856

keystone M E M B E R

L A B O R A T O R I E S , INC. ACIL

Work Order: 1909.1066 Site Name / Sample Description Page 4 of 4Sample No: 1925497 Clinton FMGP

Report Date: 102899 MR10-RS-001


Kevstone Laboratories, Inc

< = less than; ug/L = ppb; mg'L = ppm; mglcg = ppmNote This report may not be reproduced except in ful l , without written approval of the laboraton

600 East 17th Street South 3012 Ansborough Avenue 1304 AdamsNewton, IA 50208'515-792-8451 * Waterloo, IA 50701 • 319-235-4440 Kansas City, KS 66103* 913-321-7856


M E M B E R

ACIL


Report To

Randv KronemanMontiiomery-U'atson1 1 15? Aurora Avenue

Des Momes. 1A 50?22

Sample Information


Date Collected: 09 29 99 12: 10PMDate Received: 09 ?0 99 1 1 : 1 6 AM


Matrix: soil


Clinton FMGP

M R 1 1 - R S - 0 0 1

Comments


Determination of volatile organic compounds.1 ,1 .1 -Tnchloroethane1 , 1 ,2,2-Tetrachloroethane1 . 1 ,2-Tnchloroethane1.1-Dichloroethane1.1-Diehloroethylene1 ,2-Dichlorobenzene1 ,2-Dichloroethane1 ,2-Dichloropropane1 ,3-Dichlorobeazene1 ,4-Dichlorobenzene2-Butanone ( M E K )2-Hexanone (MBK)4-Methyl-2-pentanone ( M I B K )AcetoneBenzeneBromodichloromethaneBromoformBromo methane

Note

< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.005 mg'kg< 0.005 mg'kg< 0.005 mg'kg


< = less than; ug/L = ppb; mgThis report mas not be reproduced except in ful l .

00010.0010.0010.00100010.0010.0010.00100010.0010.00500050.0050.010.0010.0010.0010.002

L = ppm; mg'kg

EPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8260A

= ppm


10 12 9910 12 '9910 129910 12 9910 12 9910 12 '9910'12'9910 12 '9910 12'9910 12 9910 129910 129910 129910 12 9910 12'9910 12'9910 129910 12 99

without written approval of the laboraton.

600 East 17<h Street SouthNewton IA 50208 • 515-792-8451




M E M B E R

ACIl

Work Order: 19091066Sample No: 1925498

Report Date: 1028 99

Analyte

Carbon DisulfideCarbon TetrachlondeChlorobeazeneChloroethaneChloroformChloromethanecis- 1 .2-Dichloroethylenecis-l.?-DichloropropeneDibromochloromethancEthylbea/eneMethyl-t-butyl Ether (MTBE)Methylene ChlorideTetrachloroethyleneToluenetrans- 1 .2-Dichloroethylenetrans- 1 .?-DichloropropeneTnchloroethyleneVinyl ChlorideXylenes. total


Analysis Result

< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mgkg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mgkg< 0.001 mgkg< 0.005 mg'kg< 0.005 mg'kg< 0.001 mgkg< 0.001 mgkg< 0.001 mg'kg< 0.001 mgkg< 0.001 mgkg< 0.001 mg'kg< 0.001 mg'kg

DetectionLimit

0.001000100010.0010.0010.0010.0010.00100010.00100050.0050.0010.0010.0010.0010.0010.0010.001

Method

EPA 8260AEPA 8260AEPA 8260 AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA S260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA S260AEPA 8260AEPA 8260AEPA 8260A

Analyst


Page 2 of 4

DateAnalyzed

10 129910 129910 129910 129910 12 '9910 12 9910 129910 12 9910 12 9910 1 2 9910 12 9910 129910 12 9910 129910 129910 12 9910 12 9910 12'9910 1299

Determination of acid extractable organic compounds.(3 & 4)-Methylphenol2.4,5-Tnchlorophenol2,4,6-Trichlorophenol2.4-Dichlorophenol2.4-Dimethylphenol2.4-Dimtrophenol2-Chlorophenol2-Methylphenol2-Nitrophenol4,6-Dmitro-2-methylphenol4-Chloro-3-methylphenol4-NitrophenolPentachloropheno!

Note

<0.33 mg'kg< 1.65 mg'kg<0.33 mg'kg<0.33 mg'kg<0.33 mg'kg< 1.65 mg'kg<0.33 mg'kg<0.33 mg'kg<0.33 mg'kg< 1.65 mg'kg<0.33 mg'kg< 0.66 mg'kg<0.66 mg'kg

< = less than; ug/L = ppb; mgThis repon ma\ not be reproduced except in fu l l .

0.331.650.330.330.331.650.330.330.331.650.330.660.66

'L = ppm; mg'kg


= ppm


10099910099910 '09 '9910 09 '9910 09 '9910099910099910 '09 991009991009'99100999100999100999

without \ATitten approval of the laboratory




L A B O R A T O R I E S , \

M E M B E R

ACIL



Analyte

Phenol

Determination of polvnuclearAcenaphtheneAcenaphthyleneAnthraceneBenzo( a (anthraceneBenzo(a)pyreneBenzo(blfluorantheneBen/of g.h.OperyleneBenzol kif luorantheneChryseneDibenzo(a.h)anthraceneFluorantheneFluorenelndeno( 1 ,2.3-cd)pyreneNaphthalenePhenanthrenePyrene



Analysis Result

<0.33 mg'kg

aromatic hydrocarbons.<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg

< 2. mg'kg3.3 mg'kg

<3. mg'kg3,830. mg'kg

< 5. mg'kg<5. mg'kg

9. mg'kg

DetectionLimit

0.33

0.010.010.010010.010010.010010010.010.010.010.010.010.010.01

2.3.3.

3.5.5.3.

Method

EPA 8270B

EPA8310EPA 83 10EPA 83 10EPA 83 10EPA 8310EPA 8310EPA 83 10EPA 83 10EPA 8310EPA 83 10EPA 83 10EPA 83 10EPA 83 10EPA 8310EPA 83 10EPA 83 10

EPA 7060EPA6010AEPA6010AEPA 601 OAEPA 7421EPA6010AEPA6010A

Analyst

F1Z

F\VMF\VMF\VMF\VMF\VMF\VMF\VMF\VMF\VMFWMF\VMF\VMFWMFWMFWMFWM

LKMLARLARLARK.JSLARLAR

Page 3 of 4

DateAnalyzed

1 0 09 99

10 129910 129910 12 9910 12 9910 12 9910 129910 12 9910 129910 129910 12 9910 129910 12 9910 12 9910 129910 129910 12 99

1005 9910059910 '05 '9910 '05 '9910 '08 '991005 991005 99


Note

< 1. mg'kg<30. mg'kg83.5 %

< 1,000. mg'kg

< = less than; ug/L = ppb: mgThis report ma\ not he reproduced except in fu l l .

1.30.

1.000

EPA 901 OAEPA 350.2EPAEPA 300.0

KJSMMMBNS

FWM

10 05 '991007 9910049910 '07 99

'L = ppm; mg'kg = ppmwi thou t written approval of the Utwraton,

600 East 17th Street SouthNewton. IA 50208 • 515-792-8451




M E M B E R

ACIL




Page 4 of 4


Limit MethodDate

Analyst Analyzed

Kevstone Laboratories. Inc.

< = less than; ug/L = ppb; mg'L = ppm; mg1<g = ppmNote This report may not be reproduced except in fu l l , without written approval of the laboratory

600 East 17th street SouthNewton. IA 50208 • 515-792-8451




M E M B E R

ACII


Report To

Randy KronemanMontgomery -Watson1 1 15? Aurora Avenue

Des Momes. IA 50?22

Sample Information


Date Collected: 09 29 99 12 45 PMDate Received : 09 ?0 99 1 1 : 1 6 AM

Collector: Randy KronemanCollector Phone: 515-25?-08?0

Matrix: soil


Clinton FMGP

MR12-RS-001

Comments


Determination of volatile organic compounds.1.1.1 -Tnchloroethane1 . 1 .2,2-Tetrachloroethane1 . 1 ,2-Tnchlorocthane1,1-Dichloroethane1 , 1 -Dichloroethylene1 ,2-Dichlorobenzene1 .2-Dichloroethane1.2-Dichloropropane1 ,?-Dichlorobenzene1 .4-Dichlorobenzene2-Butanone ( M E K )2 -Hexanone (MBK)4-Methyl-2-pentanone ( M I B K )AcetoneBenzeneBromodichloromethaneBromoformBromomethane

Note

< 0.001 mgkg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.005 mg'kg< 0.005 mgkg< 0.005 mg'kg

<0.01 mg'kg< 0.001 mg'kg< 0.001 mgkg< 0.001 mgkg< 0.002 mgkg

< = less than; ug/L = ppb; mgThis report ma> not he reproduced except in f u l l .

0.0010.0010.0010.0010.0010.0010.0010.0010.0010.0010.0050.0050.0050.010.00100010.0010002

L = ppm; mg l<g

EPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA S260AEPA 8260A

= ppm


10 12 9910 129910 12 9910 12 9910 129910 12'9910 12 '9910 12 '9910 12'9910 12 9910 129910 129910 12 9910 12 9910 12 9910 12'9910 129910 1299

without written approval of the laboratory

600 East 17<h Street SouthNewlon. IA 50208 • 515-792-8451




M E M B E R

AC



Analyte

Carbon DisulfideCarbon TetrachlondeChlorobenzeneChloroethaneChloroformChloromethanecis- 1 .2-Dichloroethylenecis-1.3-DichloropropeneDibromochloromcthancEthylben/eneMethyi- t -buty] Ether (MTBF.)Methylene ChlorideTetrachloroethyleneToluenetrans- 1 ,2-Dichloroethylenetrans-l.?-DichloropropeneTnchloroethyleneVinyl ChlorideXylenes. total

Determination of acid extractable(3&4)-Methylphenol2,4.5-Tnchlorophcnol2,4,6-TnchlorophenoI2.4-Dichlorophenol2.4-Dimethylphenol2.4-Dmitrophenol2-Chlorophenol2-Methylphenol2-Nitrophenol4.6-Dmirro-2-methylphenol4-Chloro-3-methylphenol4-NitrophenolPentachlorophenol

Note This


Analysis Result

< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.005 mg'kg< 0.005 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mglcg< 0.001 mg'kg

organic compounds.<0.33 mg'kg< 1.65 mg'kg<0.33 mg'kg<0.33 mg'kg< 0.33 mg'kg< 1 .65 mg "kg<0.33 mg'kg<0.33 mg'kg< 0.33 mg'kg< 1.65 mg'kg<0.33 mg'kg< 0.66 mg'kg<0.66 mg'kg

< = less than; ug/L = ppb; mgreport ma> not be reproduced except in f u l l .

DetectionLimit

000100010.0010.0010.0010.0010.0010.0010.0010.00100050.0050.0010.0010.0010.0010.00100010.001

0.331.650.330.330.331.650.330.330.331.650.330.66066

'I, = ppm: mg'kgwithout vmtten appro\

Method

EPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260A

EPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 82^0BEPA 8270BEPA 8270B

= ppmal of the laboraton,

Analyst


F1ZFIZFIZFIZFIZFIZFIZFIZFIZFIZFIZFIZFIZ

Page 2 of 4

DateAnalyzed

10 12 9910 129910 12 9910 12 9910 129910 12 9910 129910 12 9910 129910 12 9910 12 9910 12 9910 129910 12 9910 129910 129910 129910 129910 1299

1 0 09 991009/9910/09/9910 '09 '9910099910099910099910 '09 991009991009991009991009 99100999



1304 AdamsKansas City. KS 66103* 913-321-7856


M E M B E R

ACIL

Work Order: 19091066Sample No: 1925499

Report Date: 102899


DetectionAnalyte

Phenol

Deternunation of polynuclearAcenaphtheneAcenaphthyleneAnthraceneBenzol a (anthraceneBenzol a )pyreneBenzol blfluorantheneBenzol g.h.i IpervlcneBenzol k IfluorantheneChryseneDibenzol a.h)anthraceneFluorantheneFluoreneIndenol 1.2,3-cd)pyreneNaphthalenePhenanthrenePyrene


Analysis Result

< 0.33

aromatic hydrocarbons.<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01<0.01

< 2 .<3.< 3

3,780.<5< 5.94

mg'kg

mg'kgmg'kgmg'kgmg'kgmg'kgmg'kgmg'kgmg'kgmg-kgmg-kgmg'kgmg'kgmg'kgmg'kgmg'kgmg'kg

mg'kgmg'kgmg'kgmg'kgmg'kgmg'kgmg'kg

Limit

0

0000000000000000

2333553

.33

.01

.01

.01

.01

.01

01

.01

.01

.01

.01

.01

.01

.01

.01

.01

.01

Method

EPA

EPAEPAEPAEPAEPAEPAEPAEPAEPAEPAEPAEPAEPAEPAEPAEPA

EPAEPAEPAEPAEPAEPAEPA

8270B

83108310831083108310831083108310S3 108310831083108310831083108310

70606010A6010A6010A74216010A6010A

Analyst

FIZ



Page 3 of 4

DateAnalyzed

10

10101010101010101010101010101010

1010

09

12121212121212121212121212121212

05'05

10 '0510 '05101010

080505

99

999999

'999999

99999999

999999

999999

9999'99'99'999999


Note

< 1.<30.80.7

< 1.000.

mg'kgmg'kg%mg'kg

< = less than; ug/L = ppb; mgThis report may not be reproduced except in f u l l .

130

1.000

EPAEPAEPAEPA

9010A3502

300.0

KJSMMMBNS

FWM

1010

0507

10 '0410 '07

'99999999

'L = ppm; mg'kg = ppmw i t h o u t written approval of the laboratory

600 East 17th Street SouthNewton. IA 50208* 515-792-8451



L A B O R A T O R I E S , INC.

M E M B E R

ACIL




Page 4 of 4


Limit MethodDate

Analyst Analyzed

Keystone LabWatones. Inc.

< = less than; ug/L = ppb; mg'L = ppm; mg^g = ppmNote This repon ma\ no! be reproduced except in ful l , without written approval of the laboraton,




keystoneL A B O R A T O R I E S . INC.

M E M B E R

ACIL


Report To

Randy KronemanMontpomer\ -\\'atson1 1 153 Aurora Avenue

Des Momev 1A 50322

Sample Information


Date Collected: 09 29 99 01:00 PMDate Received: 09 30 99 11 : 1 6 AM


Matrix: soil


Clinton FMGP

M R 1 3 - R S - 0 0 1

Comments


Determination of volatile organic compounds.1 . 1 . 1 -Tnchloroethane1 . 1 .2.2-Tetrachloroethane1 . 1 ,2-Tnchloroethane1,1-Dichloroethane1 . 1 -Dichloroethylene1 ,2-Dichlorobenzcne1,2-Dichloroethanc1 ,2-Dichloropropane1 ,3-Dichlorobenzene1 ,4-Dichlorobenzene2-Butanone(MEK)2-Uexanone (MBK.)4-Methyl-2-pentanone ( M I B K )AcetoneBenzeneBromodichloromethaneBromoformBromomethane

Note

< 0.001 mg'kg< 0.001 mg'kg< 0.001 mgkg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.005 mg'kg< 0.005 mg'kg< 0.005 mg'kg


< = less than; ug/L = ppb; mgThis report ma\ not be reproduced except in f u l l .

0.0010.00100010.0010.0010.0010.0010.0010.0010.0010.0050.0050.0050.010.001000100010.002

L = ppm; mg "kg

EPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260A

= ppm


10 129910 129910 129910 12 9910 12 9910 12'9910'12'9910 129910 129910 129910 129910 129910 129910 12 9910 129910 129910 12 9910 12 99

w i t h o u t written approval of the laboratory

600 East 17'h Street SouthNewlon, IA 50208 • 515-792-8451




M E M B E R

ACIL

%\ ork Order: 1909 1 066Sample No: 1925500


Analyte

Carbon DisulfideCarbon TetrachlondeChlorobenzeneChlorocthaneChloroformChloromethanecis- 1 ,2-Dichloroethylenecis-l.?-DichloropropeneDibromochloromethaneEihylben/eneMethyl - t -huty l Ether ( M T B E lMethylene ChlorideTetrachloroethyleneTolueneirans- 1 .2-Dichloroethylenetrans- 1 ,3-DichloropropeneTnchloroethyleneVinyl ChlorideXylenes. total

Determination of acid extractable(3 & 4)-Methylphcnol2,4,5-Tnchlorophenol2,4.6-Tnchlorophenol2,4-Dichlorophenol2.4-Dimethylphenol2.4-Dmitrophenol2-Chlorophenol2-Methylphenol2-Nitrophenol4.6-Dmitro-2-methylphenol4-Chloro-3-methylphenol4-NitrophcnolPentachlorophenol

Note This


Analysis Result

< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kc< 0.001 mg'kc< 0.001 mg"kg< 0.001 mg'kg< 0.001 mgl<g< 0.001 mg'kg< 0.005 mg'kc< 0.005 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kc< 0.001 mg'kg

organic compounds.< 0.33 mg'kg< 1.65 mg'kg<0.33 mg'kg< 0.33 mg'kg<0.33 mg'kg< 1.65 mg'kg< 0.33 mg'kg<0.33 mg'kg<0.33 mg'kg< 1.65 mg'kg<0.33 mg'kg< 0.66 mg'kg< 0.66 mg'kg

< = less than; ug/L = ppb: mgreport may not be reproduced except in f u l l .

DetectionLimit

0.0010.0010.0010.0010.0010.0010.0010.0010.0010.0010.0050.0050.0010.0010.0010.0010.0010.0010.001

0.331.650.330.330.331.650.330.330.331.650.330.660.66

L = ppm: mg'kg

Method

EPA 8260AEPA 8260AEPA S260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260A

EPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA S2~OBEPA 8270B

= ppm

Analyst



Page 2 of 4

DateAnalyzed

10 129910 129910 129910 12 9910 12 9910 12 9910 12 9910 129910 12 9910 12 9910 12 9910 12 9910 129910 12 9910 12 9910 12 9910 129910 12'9910 12 99

10 14 9910 14 '9910 149910 14'9910 149910 14 9910 14 9910 149910 149910 149910 14 9910 149910 1499

wi thou t written appunal of the laboratory

600 East 17'n Street SouthNewton. IA 50208 • 515-792-8451




M E M B E R

ACIL


Report Dale: 10 28 99

Analyte

Phenol

Determination of pol\ nuclearAcenaphtheneAcenaphthyleneAnthraceneBenzol a (anthraceneBenzol a IpyreneBenzol b ) fluorantheneBenzol g.h.i)peryleneBenzol k ) fluorantheneChrysencDibenzol a.h (anthraceneFluorantheneFluorenelndeno(1.2.3-cd)pyreneNaphthalenePhenanthrenePyrene



Analysis Result

<0.33 mg'kg

aromatic hydrocarbons.<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg

0.02 mg'kg0.03 mg'kg0.03 mg'kg

<0.01 mg'kg<0.01 mg'kg

0.02 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg

0.02 mg'kg<0.01 mg'kg

< 2. mg'kg5. mg'kg

<3 mg'kg4,880. mg/kg

< 5. mg'kg66 mg'kg

11.6 mg'kg

DetectionLimit

0.33

0010.010.010.010.010.010.010010010.010.010.010.010010.010.01

2.3.3.

3.5.5.3.

Method

EPA 8270B

EPA 8310EPA 83 10EPA 83 10EPA 83 10EPA 8310EPA 83 10EPA 8310EPA 8310EPA 8310EPA 8310EPA 83 10EPA 83 10EPA 8310EPA 83 10EPA 8310EPA 83 10

EPA 7060EPA6010AEPA6010AEPA6010AEPA 7421EPA6010AEPA6010A

Analyst

FIZ



Page 3 of 4

DateAnalyzed

10 14 99

10 129910 129910 129910 12 9910 129910 12 991 0 1 2 9910 1 2 9910 129910 129910 12'9910 12 9910 12 '9910 12 9910 12 9910 12 99

10059910 '05 9910 '05 '9910 '05 '991008991005 991005 99

Determination of general chemistry parameters.Cyanide, totalNitrogen, AmmoniaPercent SolidsSulfate

Note

< 1 . mg Vg< 30. mg'kg81.8 %

< 1.000. mg'kg

< = less than; ug/L = ppb; mgThis rcpon mas not be reproduced except in ful l .

130.

1,000.

EPA9010AEPA 350.2EPAEPA 300 0

KJSMMMBNS

FWM

10 '05 991007 991004 991007 99

'L = ppm; mg'kg = ppmwi thou t written approval of the laboratory





M E M B E R

ACIL



Site Name / Sample DescriptionClinton FMGP

MR13-RS-001

Page 4 of 4

Analyte

*y v/7 d-/'ZnAlt^s

DetectionAnalysis Result Limit Method

DateAnalyst Analyzed

Keystone Laboratories, Inc.

< = less than; ug/L - ppb; mgl, = ppm; mgTcg = ppmNote This report ma\ not be reproduced except in full, without written approval of the laboratory





M E M B E R

ACIL

ANALYTICAL REPORTOctober 28. 1999

Report To

Randv KronemanMontgomery- Watson1 1 153 Aurora Avenue

Des Momes. IA 50322

Sainple Information


Date Collected: 09 29 99 01Date Received: 09 30 99 1 1

25 PM1 6 AM

Page 1 of 4

Collector: Randy Kroneman


Clinton FMGP

MR14-RS-001

Analyte Analysis Result

^oneiiur riiunc. jis--?*-\jo.Matrix: soil

u

Comments

DetectionLimit Method Analyst

DateAnalyzed

Determination of volatile organic compounds.1,1.1 -Trichloroethane1 . 1 ,2.2-Tetrachloroethane

, 1 ,2-Tnchloroethane1,1-Dichloroethane1 , 1 -Dichloroethylene,2-Dichlorobenzene

1.2-Dichloroethane1 ,2-Dichloropropane,3-Dichlorobenzene,4-Dichlorobenzene

2-Butanone(MEK)2-Hexanone(MBK)4-Methyl-2-pentanone ( M I B K )AcetoneBenzeneBromodichloromethaneBromoformBromo methane

Note

< 0.001 mglcg< 0.001 mg/kg< 0.001 mglcg< 0.001 mglcg< 0.001 mglg< 0.001 mg/kg< 0.001 mg/kg< 0.001 mg/kg< 0.001 mg/kg< 0.001 mg'kg< 0.005 mglcg< 0.005 mg'kc< 0.005 mg'kg


< = less than; ug/L = ppb; mg'L

0 001 EPA 8260A0.001 EPA S260A0.001 EPA 8260A0.001 EPA 8260A0.001 EPA 8260A0.001 EPA 8260A0.001 EPA 8260A0.001 EPA 8260A0.001 EPA 8260A0.001 EPA 8260A0.005 EPA 8260A0.005 EPA 8260A0.005 EPA 8260A0.01 EPA 8260A0.001 EPA 8260A0.001 EPA 8260A0.001 EPA 8260A0.002 EPA 8260A

= ppm; mg'kg = ppm


10 13 9910 13 9910 139910 139910 139910 13'9910'13'9910 13 9910 13 9910 13 9910 13 9910 139910 139910 13 9910 13 9910 139910 139910 13 99

This repon ma\ not be reproduced except in ful l , w i thou t written approval of the laboratory





M E M B E R

AOL



Analyte

Carbon DisulfideCarbon TctrachlondeChlorobenzcneChloroethaneChloroformChloromethanecis- 1 .2-Dichloroethylenecis-!.3-DichloropropeneDibromochloromethaneEthylbenzeneMethyl - t -buty l Ether (MTBE)Methylene ChlorideTetrachloroethyleneToluenetrans- 1 .2-Dichloroethyleneirans- 1 .?-DichloropropeneTnchloroethyleneVinyl ChlondeXylenes. total

Determination of acid extractable(3 & 4)-Methylphcnol2.4,5-Tnchlorophenol2.4.6-Tnchlorophenol2.4-Dichlorophenol2.4-Dimethylphenol2.4-Dmitrophenol2-Chlorophenol2-Methylphenol2-N'itrophenol4.6-Dinitro-2-methylphenol4-Chloro-3-methylphenol4-NitrophenolPentachlorophenol

Note This


Analysis Result

< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.005 mg "kg< 0.005 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg< 0.001 mg'kg

organic compounds.<0.33 mg'kg< 1.65 mg'kg<0.33 mg'kg<0.33 mg'kg< 0.33 mg'kg< 1.65 mg'kg<0.33 mg'kg< 0.33 mg'kg<0.33 mg'kg< 1.65 mg'kg<0.33 mg'kg<0.66 mg'kg< 0.66 mg'kg

< = less than; ug/L = ppb; mgreport ma> not be reproduced except in fu l l .

DetectionLimit

0.0010.0010.0010.0010.0010.0010.0010.0010.0010.0010.0050.0050.0010.0010.0010.0010.0010.0010.001

0.331.650.330.330.331.650.330.330.331.650.330.660.66

'L = ppm; mg'kgwithout written appro\

Method

EPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8260AEPA 8 2 60 AEPA 8260AEPA 8260AEPA 8260AEPA 8260A

EPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA 8270BEPA S270BEPA 8270BEPA 8270BEPA 8270B

= ppmal of the laboratory

Analyst



Page 2 of 4

DateAnalyzed

10 13 991013 9910 13 9910 139910 13 9910 13 9910 13 9910 139910 13 9910 139910 13 9910 13 9910 13 9910 13 9910 13 9910 13 9910 13 9910 139910 13'99

10 13 9910 13 '9910 13 '9910 13'9910 139910 13 9910 139910 139910 139910 13 9910 139910 13 9910 13'99





M E M B E R

ACIL

NVorkOrder: 1909 1066Sample No: 1925501


Analvtc

Phenol

Determination of poh nuclearAcenaphtheneAcenaphthyleneAnthraceneBenzol a (anthraceneBenzol a IpyreneBenzol b ifluorantheneBenzol g.h.OperyleneBenzol k ifluorantheneChryseneDibenzo( a. h (anthraceneFluorantheneFluoreneIndeno( 1 ,2.3-cd)pyreneNaphthalenePhenanthrenePyrene



Analysis Result

<0.33 mglcg

aromatic hydrocarbons.<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mglcg<0.01 mg'kg<0.01 mg'kg<0.01 mglcg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg<0.01 mg'kg< 0.01 mg'kg<0.01 mg'kg<0.01 mglcg<0.01 mg'kg<0.01 mg'kg

<2. mg'kg3.9 mg'kg

<3. mg'kg3,950. mg'kg

< 5. mg'kg< 5. mg'kg9.5 mg'kg

DetectionLimit

033

0.010.010.010.010.010.010.010010010.010010.010.010.010.01001

2.3.

3.3.5.5.3.

Method

EPA 8270B

EPA8310EPA 83 10EPA 8310EPA 8310EPA 8310EPA 83 10EPA 8310EPA 8310EPA 8310EPA 83 10EPA 8310EPA 83 10EPA 83 10EPA 83 10EPA 83 10EPA 83 10

EPA 7060EPA6010AEPA6010AEPA6010AEPA 7421EPA6010AEPA6010A

Analyst

FIZ



Page 3 of 4

DateAnalyzed

10 13 99

10 12 9910 12 9910 12'9910 12 9910 129910 12 9910 12 9910 12 9910 12 9910 12 9910 129910 12 9910 129910 129910 129910 1299

10 05 9910 05 '9910'05'9910'05'9910 '08 '9910 '05 99100599


Note

< 1. mg'kg< 30. mg'kg

81. %< 1,000. mg'kg

1.30.

1 .000.

EPA9010AEPA 350 2EPAEPA 300.0

KJSMMMBNS

FWM

1005 991007 9910 '04 99100799

< = less than; ug/L = ppb; mgl, = ppm; mg'kg = ppmThis report ma\ not be reproduced except in full , wi thout written approval of the laboratory





M E M B E R

ACIL


Report Date: 102899


Page 4 of 4


Limit MethodDate

Analyst Analyzed

>

Kevstone Laboratories. Inc

< = less than; ugfL = ppb; mg^L = ppm; mg'kg = ppmNote This report may not be reproduced except in ful l , without written appro\al of the laboralop.



1304 AdamsKansas City, KS 66103 • 913-321 -7856

m co -n a> x-a

z a

>o

2 o

g I

m•

• 3

'

tn •ij CD co oo CO ro co ro *>. CO o •n 0) CO

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CO CO N)

Ai g

CO 0

ro g

00

00•&• ai o

=• r

3

(D M

ff |>

co P

w

->l

c -

-* > -3

3-

0)

CO

03

0

s s ^

co

^^

5

O 2

J53

- 3

•vl

CO CO •vl

\5 ^

-"

CO s§ a>

o CO

I

\ keystoneL A B O R A T O R I ES, INC.

RECEIVED

DEC nMW/IOWA

M E M B E R

ACIL

December 10, 1999

Randy KronemanMontgomery - Watson11153 Aurora AvenueDes Moines IA 50322

Dear Mr. Kroneman,

Please find enclosed the QC package for Work Order Number 1909.1066 I apologize forthe delay as we were trying to recover data from a damaged back up tape Feel free tocontact me if you have any questions at (319) 235-4440 or by e-mail [email protected].

Sincerely,

Tracy EildertsDirector of Quality Assurance and Safety

600 East 17'h Street SouthNewton, IA 50208 • 515-792-8451



keystoneL A B O R A T O R E S, INC

M E M B E R

ACIL

Volatiles in Water Method 8260 Quality Control ReportNovember 8,1999Report To

Randy KronemanMontgomery-Watson11153 Aurora AvenueDesMoines, IA 50322Phonc:(515)-253-0830Fax: (S15)-253-9592

Page 1 of 2Sample Information

Work Order: 1909 1066Matrix: Soil

Collector: KronemanDate Received: 09/30/1999Date Analyzed: 10/13/1999Batch Number: voc!01299a2

Keyrtoae Sample ID192549619254971925498192549919255001925501

CBetrt Sample IDMR09-RS-001MR10-RS-001MR11-RS-001MR12-RS-001MR13-RS-001MR14-RS-001

Initial Calibration: Performed on 10/01/1999 all analyses £20% RSD (acceptable)Continuing Calibration: Performed on 10/12/1999 all analytes ± 30%D acceptable range.

BFB Tune Check_______________Tune Check: All tune parameters within acceptable range

Method BUakMethod Blank: All target compounds were non-detected except:

_____Mcthylcne Chloride 106ug/L_______________

Matrix Spike/Matrix Spike Duplicate: Acceptable Ranee (70% -130% RecoveryX£20 RPD)Compound

1,1-DichloroethcneBenzeneTrichloroetheneTolueneChlorobenzene

MS •/• Recovery119114106106109

MSD % Recovery126115106110110

RPD61041

600 East 17th Street SouthNewlon. IA 50208 • 515-792-8451



\ keystoneL A B O R A T O R I ES, INC.

M E M B E R

ACILWork Order: 1909.1066Montgomery-WauonVOC Water Batch Numben voc!01299a2 Page 2 of 2S*irrBiiiiliti ':c: ••: "••.:••••

SampleMethod Blank

192549619254971925498192549919255001925501

Matrix SpikeMatrix Spike Duplicate

1 -Dichloroethane-d^111119117116118124121119124

Bromofluorobenzene111111112111110110116100101

1 ,2-Dichlorobenzene-d4991001009910010198100102

Approved by;

Director of Quality AssuranceKeystone Laboratories, Inc.




\ keystoneL A B O R A T O R I E S , I N C

M E M B E R

ACIL

PAH Water Method 8310 Quality Control Report

November 8,1999 Page 1 of 2Report To

Randy KronemanMontgomery-Watson11153 Aurora AvenueDCS Moines, IA 50322Phone:(515)-253-0830Fax: (515)-253-9592

Sample InformationWork Order: 1909.1066

Matrix: SoilCollector: Kroneman

Date Received: 09/30/1999Date Extracted: 10/06/1999Batch Number: PNA 3510-99010

KeyiteM Sample IDMethod Blank

19254%19254971925498192549919255001925501


Client Sample IDN/A

MR09-RS-001MRlO-RS-001MR11-RS-001MR12-RS-001MR13-RS-001MR14-RS-001

N/AN/A

Him Batchpna!01299alpna!01299alpna!01299alpna!01299alpna!01299alpna!01299alpna!01299alpna!01299alpna!01299al

fakiaVContinBtne CalibrationInitial Calibration: Performed on 10/12/1999 all analytes within acceptable range.Continuing Calibration: Performed on 10/12/1999 all analytes within acceptable range

Metfeod BlankMethod Blank: All target compounds were non-detected.

Matrix Spike/Matrix Spike Duplicate: Acceptable Ranee (60%-140«/. RecoveryX£30 RPD)Compound

NaphthaleneAccnaphthcnePhenanthrcnePvreneChryseneBenzo(a)p>Tene

MS % Recovery10898919894101

MSD % Recovery107110101108101110

RPD12101079

600 East 17<h street SouthNewton. IA 50208 • 515-792-8451



1 keystoneL A B O R A T O R I E S , INC.

M E M B E R

ACIL

Woric Order 1909.1066Montgomery-WatsonPNA Soil Batch Number pna!01299al Page 2 of 2Sarro£*te Recovery % Acceptable R*n» (60*A-140%)

SampleMethod Blank

192549619254971925498192549919255001925501


Decafluorobiphenyl Recovery90949398107147*85100110

•Outside of established QA/QC limhs No apparent cause for the excursion could be determined other than matrix interference effects

Aofroved by /"]

"7 x 'Eil

Director of Quality AssuranceKeystone Laboratories, Inc.

600 East 17t^ street SouthNewton, IA 50208 • 515-792-8451



\ keystoneL A B O R A T O R I E S, I N C .

M E M B E R

AC1L

Semi-Volatile Acids in Soil Method 8270 Quality Control Report

November 9,1999Report To

Ranch KronemanMontgomery- Watson11153 Aurora AvenueDCS Moines, IA 50322Phone: (515)-253-0830Fax. (515)-253-9592

Page 1 of 2Sample InformttJoa

Work Orders: 1909 1066Matrix: Soil

Collector: Randy KronemanDate Received: 09/30/1999Date Extracted: 10/06/1999Batch Number: BNA 3550-99029

Keystone Sample IDMethod Blank

1925496192549719254981925499


Client Sample IDN/A

MR09-RS-001MR10-RS-001MR11-RS-001MR12-RS-001

N/AN/A

Run Batchbna!00899a2bna!00899a2bna!00899a2bna!00899a2bna!00899a2bnal00899a2bna!00899a2

loitMd/Contnuitng CalibrationInitial Calibration: Performed on 10/08/1999 all analytes within acceptable range (£20%RSD)

Continuing Calibration: Performed on 10/08/1999 all analytes within acceptable range (±30%D)

DFTFP Tune CheckTune Check: All tune parameters within acceptable range.

Method BlankMethod Blank: All target compounds were non-detected

Matrix Spate/Matrix Spike Duplicate: Acceptable Ranee <60%-140% RecoveryX<40 RPD)Compound

Phenol2-Chlorophenol4-Chloro-3 -Methy Iphenol4-NitrophenolPentachlorophcnol

MS •/. Recovery78108868289

MSD •/• Recovery90118809581

RPD1497159

600 East I7'n Street SouthNewton. IA 50208 • 515-792-8451




M E M B E R

ACIL

Work Order 1909.1066Montgomery-WatsonBNA Soil Bitch Number BNA bni!00899i2 Page 2 of 2SatrotAie Recovery % m+ :: % % ; : : Accetx*bfe Raaee (&%-149%) • ,: : ; • : ', : - : : :

SampleMethod Blank

1925496192549719254981925499


2-Fluorophenol59*59*58*62646377

PhenolHU63636065787082

2,4,6-Tribromophenol9171727175106112

•Outside of the established QA/QC limns. No apparent cause for the excursions could be determined other than matrix interference effects

rracy EJlde isr of Quality Assurance

Keystone Laboratories, Inc.





M E M B E R

ACIL

Semi-Volatile Acids in Soil Method 8270 Quality Control Report

December 9,1999Report To

Randy KronemanMontgomery-Watson11153 Aurora AvenueDCS Momes, IA 50322Phone:(515)-253-0830Fax: (515)-253-9592


Work Orders: 1909.1066Matrix: Soil

Collector: Randy KronemanDate Received: 09/30/1999Date Extracted: 10/06/1999Batch Number: BNA 3550-99029

Keyttooe Sample IDMethod Blank

19255001925501


Client Sample IDN/A

MR13-RS-001MR14-RS-001

N/AN/A

Run Batchbnal01199a2bna!01199a2bna!01199a2bna!01199a2bna!01199a2

Initial/Continuing CalibrationInitial Calibration: Performed on 10/11/1999 all analytes within acceptable range (£20%RSD)

Continuing Calibration: Performed on 10/11/1999 all analytes within acceptable range (±30%D).

DFTPP Tone CheckTune Check: All tune parameters within acceptable range.

Method BlankMethod Blank: All target compounds were non-detected

Matrix Spike/Matrix Spike Duplicate: Acceptable Ranee <60%-140% RecoveryX£40 RPD)Compound

Phenol2-Chlorophenol4-Chloro-3 -Methy Iphenol4-NitrophenolPentachlorophenol

MS % Recovery78108868289

MSD % Recovery90118809581

RPD1497159

600 East 17'h street SouthNewton. IA 50208 • 515-792-8451



eystoneL A B O R A T O R I E S , INC.

M E M B E R

ACIL

Work Order 1909.1066Montgomery-WatsonBNA Soil Batch Number BNA bna!01299a2 Page 2 of 2Ssrrefi** Rtcovm % Acceptable JUnee <60%-140%>

SampleMethod Blank

19255001925501


2-Fluorophenol59*

227**646377

Phenols!*6384697082

2,4,6-Tribromophenol91

55*97106112

•Outside of the established QA/QC limits. No apparent cause for the excursion! could be determined other than mathx interference effects.•* The data backup tape has been damaged. At this time we are unable to recover the data and pinpoint the source of the problem.

I racyDirector of Quality AssuranceKevstonc Laboratories, Inc.

600 East 17*h Street SouthNewton. IA 50208 • 515-792-8451




M E M B E R

AC1L

Cyanide in Soil Method 9010 Quality Control Report

October 29, 1999Report To

Randy KroncmanMontgomery- Watson11153 Aurora AvenueDCS Moines, IA 50322Phone:(515)-253-0830Fax: (515)-253-9592

Keystone Sample ID19254961925497


Work Order: 1909.1066Matrix: Soil

Collector: KronemanDate Received: 09/30/1999Date Analyzed: 10/04/1999Batch Number: CN 100499a

Client Sample IDMR09-RS-001MRlO-RS-001

ParameterInitial Verification Calibration

Lab Control StandardMethod BlankMatrix Spike

Matrix Spike DuplicateMS/MSD RPD

QA/QC Result (•/•)10394

<D.L.90943.4

Acceptance Limits {•/.)90-11085- 115

No Detectable Value70 - 13070- 130

<. 15

Fracy EildDirectdwJf Quality AssuranceKeystone Laboratories, Inc.

600 East 17tn Street SouthNewton, IA 50208 • 515-792-8451




M E M B E R

ACIL

Cyanide in Soil Method 9010 Quality Control Report

October 29,1999Report To

Randy KroncmanMontgomery- Watson11153 Aurora AvenueDes Moines, IA 50322Phone:(515)-253-0830Fax: (515)-253-9592



Collector: KroncmanDate Received: 09/30/1999Date Analyzed: 10/05/1999Batch Number: CN 100599a


Client Sample IDMRll-RS-001MR12-RS-001MR13-RS-001MR14-RS-001

ParameterInitial Verification Calibration



QA/QC Result (%)94105

<D.L.9711113.4

Acceptance Limits {%)90- 11085-115

No Detectable Value70- 13070- 130

Z 15

FracyEildrff Quality Assurance

Ke>-stone Laboratories, Inc





M E M B E R

ACIL

Ammonia in Soil Method 350.2 Quality Control Report


Rand} Krone manMontgomery-Watson11153 Aurora AvenueDCS Moines, IA 50322Phone:(515)-253-0830Fax: (515)-253-9592



Collector: KronemanDate Received: 09/30/1999Date Analyzed: 10/07/1999Batch Number: Nh3 100799a


Client Sample IDMR09-RS-001MR10-RS-001MR11-RS-001MR12-RS-001MR13-RS-001MR14-RS-001

ParameterLab Control Standard

Method BlankMatrix Spike


OA/QC Result C*/o)98

<D.L98961.5

Acceptance Limits (%)90- 110


S20

AssuranceKeystone Laboratories, Inc





M E M B E R

ACIL

Arsenic in Water Method 7060 Quality Control Report


Randy KronemanMontgomery-Watson11153 Aurora AvenueDCS Moincs, IA 50322Phone:(515)-253-0830Fax: (515)-253-9592



Collector: KronemanDate Received: 09/30/1999Date Analyzed: 10/05/1999Batch Number: As 100599a


Client Sample IDMR09-RS-001MRlO-RS-001MRll-RS-001MR12-RS-001MR13-RS-001MR14-RS-001

ParameterContinuing Calibration StandardInitial Calibration Verification



OA/OC Result (V.)8511286

<D.L.97907.7

Acceptance Limits (%)85-11585- 11580- 120


S20

ived bv

<2(LLLracy 1

Direc'ter'of Quality AssuranceKeystone Laboratories, Inc





M E M B E R

ACIL

Chromium in Water Method 6010 Quality' Control Report


Randy KroncmanMontgomery-Watson11153 Aurora AvenueDes Moines, IA 50322Phone:(515)-253-0830Fax: (515)-253-9592



Collector: KroncmanDate Received: 09/30/1999Date Analyzed: 10/05/1999Batch Number: Cr 100599b






QA/QC Result (V.)007106102

<D.L.74*69*5.6

Acceptance Limits (%)85- 11585-11580 - 120

No Detectable Value75 - 12575- 125

S20•Outside of the oubluhed QA/QC No cause for the excursion could be determined

TracyEiyDirector of Quality AssuranceKeystone Laboratories, Inc.

600 East 1?th Street SouthNewton. IA 50208 • 515-792-8451


1304 AdamsKansas City KS 66103 • 913-321-7856


M E M B E R

ACIL

Copper in Water Method 6010 Quality Control Report

October 29.1999Report To

Randy Krone manMontgomery-Watson11153 Aurora AvenueDesMoines, IA 50322Phone:(515)-253-0830Fax: (515)-253-9592



Collector: KronemanDate Received: 09/30/1999Date Analyzed: 10/05/1999Batch Number: Cu 100599b

Keystone Sample ID19254%19254971925498192549919255001925501




Mathx Spike DuplicateMS/MSD RPD

QA/QC Result <%)101106103

< D L .101946.5

Acceptance Limit* (%)85- 11585-11580- 120


<;20

TracyDirector of Quality AssuranceKevstone Laboratories, Inc





M E M B E R

ACIL

Iron in Water Method 6010 Quality Control Report

October 29.1999Report To

Rand\ Krone manMontgomery- Watson11153 Aurora AvenueDcsMoines,IA50322Phone: (515)-253-0830Fax: (515)-253-9592


Work Order. 1909 1066Matrix: Soil

Collector: KronemanDate Received: 09/30/1999Date Analyzed: 10/05/1999Batch Number: Fe 100599b


Client Sample IDMR09-RS-001MR10-RS-001MRll-RS-001MR12-RS-001MR13-RS-001MR14-RS-001



Matrix Spike DuplicateSample RPD


<D.L.**

7.5

Acceptance limits (%)85- 11585- 11580- 120

No Detectable Value75- 12575-125

S20•Due to analyfl error, no Iron ipike was added to the sample. All other QC was acceptable. No additional action was taken.

Directwbf Quality AssuranceKeystone Laboratories, Inc



1304 AdamsKansas City KS 66103 • 913-321-7856


M E M B E R

ACIL

Lead in Water Method 7421 Quality Control Report


Randy KronemanMontgomery- Watson1 1 1 5 3 Aurora AvenueDCS Moincs, IA 50322Phone:(515)-253-0830Fax: (515)-253-9592



Collector: KronemanDate Received: 09/30/1999Date Analyzed: 10/08/1999Batch Number: Pb 100899b


Client Sample IDMR09-RS-001MRlO-RS-001MR11-RS-001MR12-RS-001MR13-RS-001MR14-RS-001





< D L .84840

Acceptance Limits (H)85-11585-11580- 120


S20

ived bv

Tracy EildDircctor-of Quality AssuranceKeystone Laboratories, Inc

600 East 17tn Street SouthNewton, IA 50208 • 515-792-8451



keystoneL A B O R A T O R I E S , N C.

M E M B E R

ACIL

Nickel in Water Method 6010 Quality Control Report


Ranch KronemanMontgomery- Watson11153 Aurora AvenueDCS Moincs, IA 50322Phone: (515)-253-0830Fax: (515)-253-9592



Collector: KronemanDate Received: 09/30/1999Date Analyzed 10/05/1999Batch Number: Ni 100599b



ParameterContinuing Calibration Standard

Initial Calibration VerificationLab Control Standard

Method BlankMatrix Spike


QA/QC Result (%)109107105

<D.L1061014.1

Acceptance Limits (%)85-11585-11580 - 120


520

Fracy EildDircctohof Quality AssuranceKeystone Laboratories, Inc




\L A B O R A T O R I E S , INC.

M E M B E R

ACIL

Zinc in Water Method 6010 Quality Control Report


Randy KronemanMontgomery-Watson11153 Aurora AvenueDCS Moines, IA 50322Phone:(515)-253-0830Fax: (515)-253-9592



Collector: KronemanDate Received: 09/30/1999Date Analyzed: 10/05/1999Batch Number: Zn 100599b






QA/QC Result (V,)969998

< D L96942.4

Acceptance LJmfti (9t)85-11585- 11580- 120


S20

Iracy Ell/ality Assurance

Keystone Laboratories, Lie

600 East 17<n Street SouthNewton, IA 50208 • 515-792-8451




M E M B E R

ACIL

Sulfate in Soil Method 9038 Quality Control Report

November 2,1999Report T«

Randy KroncmanMontgomery-Watson11153 Aurora AvenueDCS Moines, IA 50322Phone: (515)-253-0830Fax: (515)-253-9592

Page 1 of 1Sample Info ittt


Collector: KroncmanDate Received: 09/30/1999Date Analyzed: 10/07/1999Batch Number: SO4 100799a3


Client Sample IDMR09-RS-O01MRlO-RS-001MR11-RS-001MR12-RS-001MR13-RS-001MR14-RS-001

, - , . : PanuneterInitial Calibration

Continuing Calibration StandardMethod BlankMatrix Spike


QA/QC Remit {%)6.396

2.001 «/g/L*143**129**

10

AecdrtaaceLfaaiUfH)S20RSD90-110

No Detectable Value90-11090- 110

<; 10•Suttalr was detected in the method blank with a concentration of 1001 ugl,"CXABde of the established QA/QC limits No apparent cause for the excunion could be determined other than matrix interferenceeffects.

Director of Quality AssuranceKeystone Laboratories, Inc

600 East 17tn Street SouthNewton. IA 50208 • 515-792-8451



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