Medkoo Biosciences Quality Control Data ......2013/11/08 · 20131106-1_131106130759 #77-97 RT:0.51-0.64 AV:21 NL:2.22E5 T:ITMS + c ESI sid=35.00 Full ms [100.00-1000.00] 100 200

11

.70

6

10

.39

7

9

.22

4

7

.70

8 7

.68

6 7

.49

0 7

.46

8

6

.03

0

5

.43

5

3

.35

4 2

.53

1 2

.52

6 2

.51

3 2

.50

8 2

.50

4 2

.32

2 2

.31

1 2

.29

9 2

.18

8 2

.01

6 1

.82

9 1

.81

3 1

.79

8 0

.82

5 0

.81

1

0.98 1.04 1.00 2.09

2.07

1.01 0.15

0.82

4.08

1.08

3.04 3.10

4.09

12 10 8 6 4 2 0PPM

O

NHSN

N

HNNHN

NN

Tozasertib DMSO-d6 400MHz, , F1: 400.130 F2: 1.000 SW1: 8224 OF1: 2471.0 PTS1d: 65536 EX: zg30 PW: 14.5 usec PD: 1.0 sec NA: 4 LB: 0.3

MedKoo Biosciences www.medkoo.com [email protected]

Medkoo Biosciences Quality Control Data www.medkoo.com | [email protected] Medkoo Biosciences Quality Control Data www.medkoo.com | [email protected] Medkoo Biosciences Quality Control Data www.medkoo.com | [email protected]

BioMedomics打字机文本MedKoo Cat#: 201900Name: TozasertibCAS#: 639089-54-6 Lot#: SSC31108Chemical Formula: C23H28N8OSExact Mass: 464.21068Molecular Weight: 464.59

BioMedomics打字机文本





BioMedomics打字机文本Tozasertib NMR analysis, Solvent: DMSO-d6


Sample Name: Manual Acquisition Injection Volume: 10.0

Vial Number: RB6 Channel: UV_VIS_4

Sample Type: unknown Wavelength: 252

Bandwidth: 4

Dilution Factor: 1.0000

Sample Weight: 1.0000

Control Program:

Quantif. Method: default Run Time (min): 15.06

Sample Amount: 1.0000

No. Ret.Time Peak Name Height Area Rel.Area Amount Type min mAU mAU*min % n.a.

1 2.00 n.a. 0.165 0.027 0.02 n.a. BM *2 2.14 n.a. 0.102 0.013 0.01 n.a. MB3 2.61 n.a. 0.949 0.091 0.08 n.a. BMB*4 2.72 n.a. 0.761 0.044 0.04 n.a. BMB5 3.49 n.a. 0.309 0.037 0.03 n.a. BMB*6 4.39 n.a. 0.102 0.024 0.02 n.a. BM *7 4.91 n.a. 508.807 119.881 99.78 n.a. MB*8 11.31 n.a. 0.093 0.034 0.03 n.a. BMB*

Total: 511.288 120.150 100.00 0.000

HPLC REPORT

0.0 2.0 4.0 6.0 8.0 10.0 12.0 15.1

-100

0

100

200

300

400

500

600Manual Acquisition UV_VIS_4

mAU

min

2.0

03

2.1

40

2.6

07

2.7

23

3.4

93

4.3

90

4.9

10

11

.30

7

WVL:252 nm

Med

Koo

Bio

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w.m

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msa

les@

med

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com



BioMedomics打字机文本Tozasertib HPLC analysis



20131106-1_131106130759 #77-97 RT: 0.51-0.64 AV: 21 NL: 2.22E5T: ITMS + c ESI sid=35.00 Full ms [100.00-1000.00]

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m/z

0

5

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15

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25

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100

Rela

tive A

bunda

nce

465.20

523.19945.01566.30 999.65445.08 609.41109.92 238.81 281.70 392.55180.22 913.99

20131106-1_131106130359 #67 RT: 0.53 AV: 1 NL: 2.77E5T: ITMS + c ESI sid=35.00 Full ms [100.00-1000.00]

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m/z

0

5

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45

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100

Rela

tive A

bunda

nce

465.17

941.36523.15564.27452.42253.24 999.78282.95

Med

Koo

Bio

scie

nces

ww

w.m

edko

o.co

msa

les@

med

koo.

com



BioMedomics打字机文本Tozasertib MS analysis

20131106-1_131106130759 #77-97 RT: 0.51-0.64 AV: 21 NL: 2.22E5T: ITMS + c ESI sid=35.00 Full ms [100.00-1000.00]

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tive A

bunda

nce

465.20

523.19

566.30445.98 589.62109.92 238.81 401.95281.70180.22 352.38 633.63

Med

Koo

Bio

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nces

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w.m

edko

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com




BioMedomics打字机文本Tozasertib MS analysis



Documents

Medkoo Biosciences Quality Control Data ......2013/11/08 · 20131106-1_131106130759 #77-97 RT:0.51-0.64 AV:21 NL:2.22E5 T:ITMS + c ESI sid=35.00 Full ms [100.00-1000.00] 100 200