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8/19/2019 Measurement of toughness in the heat affected zone of welded structural steels
1/204
Commission of the European Communit ies
t ech n ica l s tee l research
Proper t ies and serv ice per fo rmance
MEASUREMENT OF TOUGHNESS IN THE
HEAT-AFFECTED ZONE OF WELDED
STRUCTURAL STEELS
R e p o r t
EUR 9297 EN
Blow-up from microf iche original
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Commission of the European Communit ies
t e c hn i c a l s te e l re s e a rc h
Proper t ies and serv ice per fo rmance
MEASUREMENT OF TOUGHNESS IN THE
HEAT-AFFECTED ZONE OF WELDED
STRUCTURAL STEELS
M.J. GEORGE
BRITISH STEEL CORPORATION
9 , A l b e r t E m b a n k m e n t
G B - L O N D O N S E 1 7 S N
C o n t r a c t N o 7 2 1 0 - K A / 8 0 4
1 . 7 . 1 9 7 8 - 3 1 . 1 2 . 1 9 8 2 )
FINAL REPORT
Di rec to ra te -Genera l
Sc ience , Research and Deve lopment
1985 EUR 9 2 9 7 EN
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P u b l i s h e d b y t h e
C O M M I S S I O N O F T H E E U R O PE A N C O M M U N I T I E S
D i r e c t o r a t e - G e n e r a l
I n f o r m a t i o n M a r k e t a n d I n n o v a t i o n
L - 2 9 2 0 L U X E M B O U R G
L E GAL NOT ICE
Neither the Commiss ion o f the European Communi t ies nor any person act ing
on behal f o f the Commiss ion is respons ib le for the use which might be made of
the fo l low ing in fo rm a t ion
>ECSC-EEC-Euratom, Brus se ls · L uxem bourg
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MEASUREMENT OF TOUGHNESS IN THE
HEAT-AFFECTED ZONE OF WELDED
STRUCTURAL STEELS
F I N A L R E P O R T
Agreement No. 7210.KA/804
M.J. George
British Steel Corporation
Teesside Laboratories
EUR 9297 EN
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FR 62-10 822 7210.KA/804
British Steel Corporation
MEASUREM ENT OF TOUGHNESS IN THE HEAT AFFECTED ZONE
OF WELDED STRUCT URAL STEELS
ECSC Agreement No. 7210.KA/804
SUMMARY
In view of the increasing importanc e of heat affected zone (HAZ) pro pert ies in
the specification and in-service behaviour of steels for demanding structural
appl icat ions , a study has been carried out, with the aim of:-
(a) Examin ing critica lly the metho ds current ly availab le
for investigating the fracture toughness of
HAZ's,
with particular reference to the assessment of fitness
for purpose and the ability to predict the potential
service performance of HAZ's from the results of small
scale te sts, by comparison with wide plate tests
containing HAZ notches.
(b) Asses sing the prop erti es attai nable in the HAZ' s of some
structural steels currently used in applications where
high HAZ property levels are commonly specified, over
a wide range of weld energy inputs and weld type.
(c) Gaining insights, where possi ble, into the factors
affecting response to welding and the prop erti es a chie ved.
Three steels were used in the investigation; BS4360:50D and Euronorm 25-72
Fe510 DD, both of which were normalised gr ades , and RQT 500, a BSC proprietar y
quenc hed and tempered ste el, of appro ximat ely the same compo sitio n as
BS4 360 :50D . Welds were carried out at heat inputs of 2 and 5 kJ/m m, using
single V, double V and K prep arat ions , together with electroslag wel ds at
30-50 kJ/mm , dependi ng on plate thi ckn ess . The majori ty of the work was
carried out on 40 mm thick wel ds , with some compa rativ e tests at 25 and 60 mm.
The small scale tests used (Charpy V, 10 χ 10 mm COD, full thi ckness C O D ) , all
ranked the steels in the same ord er. The BS436 0:50D pla te , at 40 mm thick,
performed bes t, with RQT 500 second and Fe510DD third. The major factor
affecting HAZ properties, at least in the sample plates tested, appeared to be
the carbon equivalent value
(CEV),
which was about 0.4% in the 50D and RQT 500
plates, and 0.5% in the Fe510D D samp le. The Charpy V and COD tests showed
that,
in the coarse grained region of the HAZ , occasi onal low results could be
obtained, but, in wide plate tests at -30 and -40°C, in the presence of
9 χ 90 mm fatigued surface not che s, located in the HAZ , stresse s of the order
of plate yield lev el, and overall strai ns ranging from 1.1 to 7.5, depen ding on
the ste el, were sustained before fr actu re. Two of the plate results were
analysed, by the procedures given in PD
6493,
and it was shown tha t, as in
previous experience with weld metals, tolerable defect predictions in HAZ's
have an in-built safety fact or, in these two cases , of 2-3.
With respect to the methodology of testing, the correct placement of HAZ
notches presented the only significant problems . There was very evident
scattter in the results from all tests, although this was also a feature of
tests on some of the parent plates.
Sub-size COD tes ts, 10 mm square in cross sec tio n, giving more accurat e
indications of fracture initiation resistance, and the generation of
microstructures typical of
HAZ's,
by simulation of thermal cycles derived from
the test we ld s, were shown to have potent ial in research wo rk, although of
limited direct applicability to practical si tuatio ns.
A large body of thermal cycle data was generated from thermocouples embedded in
selected weld
HAZ's.
Good agree ment with publish ed work was obt ain ed, and
suggestions were made for modifying some of the physical constants used in
theoretical predicitions.
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FR 62-10 822 7210.KA/804
CONTENTS PAGE
1. INTRODUCTION 1
1.1 The Nature of the Heat Affected Zone 1
1.2 Importance of Heat Affected Zone Properties 3
2.
EXPERIMENTAL PROGRAMME 8
2.1 Aims and Objectives of the Work 8
2.2 Steels Used in the Test Programme 8
2.3 Weld Procedures 10
2.4 Test Methods 11
3. TEST RESULTS 31
3.1 Charpy V Impact Test Results 31
3.2 Sub-size (10 χ 10 mm Section) COD Test Results 33
3.3 Full Thickness COD Tests 33
3.4 Wide Plate Test Results 35
3.5 Test Results from Simulated HAZ's 37
4.
GENERAL DISCUSSION 75
4.1 Appraisal of Test Methods 75
4.2 Relevance of Simulative Studies 77
4.3 Effect of Steel Grade on Results Obtained 77
5. CONCLUSIONS 80
6. REFERENCES 81
TABLES
FIGURES
APPENDIX
111
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FR 62-10 822 7210.KA/804
LIST OF TABLES
2.1 Chemical Analyses of Plates Tested
2.2 Mechanical Properties of Plates Tested
2.3 Sub-Division of Weld Test Plate
3.1 Matrix of Tests Carried Out
3.2 HAZ Charpy V Test Criteria - BS4360:50D (40 mm Thick)
3.3 HAZ Charpy V Test Criteria - BS4360:50D (25 and 60 mm Thick)
3.4 HAZ Charpy V Test Criteria - Euronorm 25-72 Fe510DD (40 mm Thick)
3.5 HAZ Charpy V Test Criteria - RQT 500 (40 mm Thick)
3.6 HAZ Charpy V Test Criteria - RQT 500 (25 mm Thick)
3.7 Proportions of Weld Metal/HAZ/Plate Adjacent to Notch of Subsurface
Single and Double V Weld Charpy Tests (Plate/HAZ Boundary Taken as
Visible Aci)
3.8 0.1 mm COD Transition Temperatures (10 mm Square Transverse
40 mm Welds)
3.9 Summary of COD Test Results
3.10 Wide Plate Test Results
3.11 Wide Plate Test - Notch Locations and Dimensions
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FR 62-10 822 7210. KA/80 4
LIST OF FIGURES
1.1 Heat Affecte d Zone Thermal Cycl es - 5 kJ/mm
1.2 Weld Macro graph (5 kJ/mm , Single V) Showing Reheated Heat
Affected Zones
2.1 Microstr uctures of As-received Normalised Plates
(a) Fe51 0DD, 40 mm Thick
(b) BS4 360 :50 D, 25 mm Thick
(c) BS43 60:5 0D, 40 mm Thick
(d) BS4 360 :50 D, 60 mm Thick
2.2 Microstr uctures of As-received Quenched and Tempered Plate s,
RQT 500, 25 mm Thick
2.3 Typi cal 5 kJ/mm K Weld Proce dure
2.4 Typic al 2 kJ/mm Double V Weldin g Proce dure
2.5 Typical Electroslag Weld Procedure
2.6 Typic al 25 mm Single Bevel Weld Proce dure
2.7 Wid e Plate Test Format - Showing Locati ons of Instr ument ation
3.1 41 J Impact Transition Temperatu res - 2 kJ/mm Welds
3.2 41 J Impact Trans ition Tem pera tur es - 5 kJ/mm Welds
3.3 41 J Impact Trans ition Tem pera tur es - 2 and 5 kJ/mm K We ld s,
25 and 60 mm Thick
3.4 Shift in 41 J Impact Tran sitio n Temp erat ures - 2 kJ/mm Wel ds
3.5 Shift in 41 J Impact Tran siti on Tem pera tur es - 5 kJ/mm Wel ds
3.6 Shift in 41 J Impact Tran siti on Temp erat ure - 2 and 5 kJ/mm
K Welds, 25 and 60 mm Thick
3.7 Parent Pla te, Charpy V Impact Energy Curve Showing Scatter in
Results
3.8 HAZ Charpy V Impact Energy Curves Showing Scatter in Resul ts
3.9 Specimen Locat ions and Notch Posi tion s Charpy and 10 χ 10
COD Specimens
3.10 10 mm Square COD Result s Showing Scatter
3.11 Parent Plate Full Thick ness COD Tests Tra nsv ers e, 40 mm Thick
3.12 Comp aris on of COD Result s - 40 mm Plate s
3.13 COD Res ult s, 25 and 60 mm BS4360 :50D Plates
3.14 COD Res ult s, 25 mm RQT 500 Plates
3.15 COD Result s on Weld D4W2, 50D, Double V, 2 kJ/mm
3.16 Full Thick ness COD Results - Fe51 0DD, 5 kJ/mm Κ Weld
3.17 Full Thickn ess COD Results - BS4 360: 50D , 5 kJ/mm Κ Weld
3.18 Full Thickn ess COD Results - Fe5 10D D, Electr oslag Weld (_50 kJ/mm)
v u
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FR 62-10 822 7210.KA/804
3.19(a) Effect of Peak Temperature in Simulation 5 kJ/mm Cycle -
BS4360:50D
Effect of Tempering Cycle - BS4360:50D
Effect of Peak Temperature in Simulation 5 kJ/mm Cycle -
Fe510DD
Effect of Tempering Cycle - Fe510DD
Effect of Peak Temperature in Simulation 5 kJ/mm Cycle - RQT 500
Effect of Tempering Cycle - RQT 500
Effect of Peak Temperature - 2 kJ/mm Cycle - BS4360:50D
Effect of Peak Temperature - 2 kJ/mm Cycle - Fe510DD
Effect of Peak Temperature - 2 kJ/mm Cycle - RQT 500
Simulated HAZ Microstructures - BS4360:50D
(At
8
_
5
= 50 s,
approximating to a 5 kJ/mm heat input)
3.26 Simulated HAZ Microstructures - Fe510DD (Atg-s = 50 s, approximating
to a 5 kJ/mm heat input)
3.27 Simulated HAZ Microstructures - RQT 500 (At
8
_
5
= 50 s, approximating
to a 5 kJ/mm heat input)
3.28 Simulated HAZ Microstructures - BS4360:50D (At
8
_
5
= 20 s,
approximating to a 2 kJ/mm heat input)
3.29 Simulated HAZ Microstructures - Fe510DD (At
8
-s = 20 s, approximating
to a 2 kJ/mm heat input)
3.30 Simulated HAZ Microstructures - RQT 500
(At
8
_
5
= 20 s, approximating
to a 2 kJ/mm heat input)
4.1 Comparison of Charpy V and 10 mm Square COD Transition Temperatures
3 .
3 .
3 .
3 .
3 .
3 .
3 .
3 .
3 .
1 9 b )
2 0 a )
, 2 0 b )
2 1 a )
2 1 b )
2 2
2 3
24
, 2 5
V i l i
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FR 62-10 822 7210.KA/804
British Steel Corporation
MESURE DE LA TENACITE DANS LA ZONE DE TRANSITION
DES ACIERS DE CONSTRUCTION SOUDES
Accord C.E.C.A. No. 7210.ΚΑ/804
SOMMAIRE
Etat donné l'importance croissante des propriétés de la zone de transition dans les
cahiers des charges ainsi que pour le comportement en service des aciers utilisés en
construction et soumis à des conditions sévères, une étude a été menée dans le but de:-
(a) examiner de manière critique les méthodes dont on dispose à
l heure actuelle afin de déterminer la ténacité à la rupture
des zones de transition, en particulier lorsqu'il s agit
d'établir l'aptitude à l'emploi et de pouvoir prédire la pe r-
formance éventuelle en service des zones de transition, à
partir d'essais conduits sur une échelle limitée, par compa-
raison avec les essais pratiqués sur des plaques larges
présentant des zones de transition en entailles.
(b) établir les propriétés qu'il est possible d'obtenir dans les
zones de transition de certains aciers de construction
utilisés dans des cas où il est courant qu'on exige pour les
zones de transition des caractéristiques p oussée s, et ce pour
un large éventail d'apports d'énergie et de types de soudures.
(c) parvenir dans la mesure du possible à une meilleure compréhen-
sion des facteurs qui influent sur la réponse au soudage, ainsi
que des propriétés obtenues.
Trois aciers ont été utilisés pour cette étude, à savoir BS4360:50D et Euronorm 25-72
Fe510DD,deux nuances normal isées, et RQT 500 , un acier propre à la BSC, qui a subi trempe
et revenu et dont la composition est quasi identique à celle de BS4360:50D. Des soudures
ont été exécutées pour des apports de chaleur de 2 et 5 kJ/mm, pour des préparations de
joints chanfreinés en V, en X et en K, ainsi que des soudures sous laitier à 30-50 kJ/mm
selon l'épaisseur de la plaque. La majeure partie de l étude a porté sur des soudures
de 40 mm d'épaisseur, et certains essais comparatifs ont été pratiqués à 25 et à 60 mm.
Les essais sur une petite échelle (Charpy V, déplacement de l'ouverture de la fissure
10 xlO mm, déplacement sur épaisseur complète) ont tous donné un même ordre pour les
aciers, le meilleur étant la plaque de 40mm d'épaisseur de BS4360:50D, suivie de
RQT 500, Fe510DD arrivant en troisième lieu. En ce qui concerne les propriétés de la
zone de transition, du moins pour les échantillons soumis aux essais, il semble que le
facteur le plus important soit l'équivalent en carbone, qui était de l ordre de 0,4% pour
les plaques en 50D et RQT 500 , et de 0,5% pour l'échantillon de Fe510DD. Les essais
Charpy V et essais de déplacement de l'ouverture des fissures ont révélé que des résultats
faibles pouvaient parfois être obtenus dans la région à gros grain de la zone de tran si-
tion;
toutefois lors des essais sur plaques larges pratiqués à -30 et -40°C, en présence,
dans la zone de transition, d'entailles en surface de 9 χ 90mm soumises à la fatigue, on
a enregistré avant la rupture des sollicitations de
l ordre
de celles se produisant à
la limite élastique, et des taux de travail allant globalement de 1,1 à 7,5 selon la
nature de l'acier. Deux séries de résultats obtenus sur ces plaques ont été analysées
selon les méthodes indiquées en PD 6493, et ces analyses ont montré que comme on le savait
déjà pour les métaux d'apport, les prévisions de défauts tolerables dans les zones de
transition comportent un facteur de sécurité qui, pour ces deux cas, était de 2 - 3.
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En ce qui concerne la méthodologie des essais le seul problème appréciable a été de
trouver l'endroit approprié pour les entailles des zones de transition. On a enregist:
pour les résultats de tous les essais une très nette dispersion, qui avait d'ailleurs
déjà remarquée lors des essais sur certaines plaques de base.
On a pu voir que les essais de déplacement de l'ouverture des fissures sur de très pet:
échantillons ayant une section transversale de 10 mm de côté, qui donnent des indicate
plus précises sur la résistance à l'amorce de rupture, ainsi que la simulation des cyc
thermiques dérivés des soudures d'essai, qui engendre des microstructures caractéristii
des zones de transition, peuvent donner des résultats intéressants pour la recherche; ;
contre les possibilités d'application directe dans des cas pratiques sont limitées.
Des thermocouples pénétrant dans des zones de transition sélectionnées ont fourni un imi
tant volume d'informations sur les cycles thermiques. Les résultats ont bien concordé
avec les travaux déjà publiés et il a été possible de suggérer des modifications des
constantes physiques utilisées pour les prédictions théoriques.
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FR 62-10 822
SOMMAIRE
1, INTRODUCTION
1.1 Nature de la zone de transition
1.2 Importance des propriétés de la zone de transition
7210.KA/804
PAGE
1
1
3
8
8
8
10
11
2.
PROGRAMME EXPERIMENTAL
2.1 Buts et objectifs des travaux
2.2 Aciers utilisés pour le programme d essais
2.3 Modes de soudage
2.4 Méthodes d essai
3. RESULTATS DES ESSAIS 3J
3.1 Résultats des essais d impact Charpy V 31
3.2 Résultats des essais de déplacement de l ouverture des
fissures sur échantillons de section 10 χ 10 mm 33
3.3 Essais de déplacement de l ouverture des fissures à pleine
épaisseur 33
3.4 Résultats des essais sur plaques larges 35
3.5 Résultats des essais pratiqués sur des zones de transition
simulées 37
4. DISCUSSION GENERALE 75
4.1 Evaluation des méthodes d essai 75
4.2 Intérêt d études simulatives 77
4.3 Effet de la nuance d acier sur les résultats obtenus 77
5. CONCLUSIONS 80
6. REFERENCES 81
TABLES
CHIFFRES
ANNEXE
xi
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LISTE DES TABLEAUX
2.1 Analyses chimiques des plaques soumises aux essais
2.2 Propriétés mécaniques des plaques soumises aux essais
2.3 Sous-division des plaques soumises aux essais de soudure
3.1 Matrice des essais pratiqués
3.2 Critères essais Charpy V sur zone de transition - BS4360:50D (ép. 40mm)
3.3 Critères essais Charpy V sur zone de transition - BS4360:50D (ép. 25 et 60 mm)
3.4 Critères essais Charpy V sur zone de transition - Euronorm 25-72 Fe510DD (ép.
40 mm)
3.5 Critères essais Charpy V sur zone de transition - RQT 500 (ép. 40 mm)
3.6 Critères essais Charpy V sur zone de transition - RQT 500 (ép. 25 mm)
3 η Proportions de métal d'apport/zone de transition/plaque au voisinage de
l'entaille, essais Charpy sur soudures en V et en X, en-dessous de la sur-
face (limite plaque/zone de transition supposée être située à la transformation
visible).
3.8 Températures de transition, déplacement de l'ouverture des fissures 0,1 mm
(soudures transversales 40 mm, 10mm de côté)
3.9 Sommaires des résultats des essais de déplacement de l'ouverture des fissures
3.10 Résultats des essais sur plaque large
3.11 Essai sur plaque large - emplacement et dimensions des entailles
Xlll
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FR 62-10 822 7210 KA/80 4
LISTE DES FIGURES
1.1 Cycles thermiques, zone de transition - 5 kJ/mm
1.2 Macrographie de soudure (5 kJ/mm , en V) montrant les zones de
transition réchauffées
2.1 Microstructures des plaques brutes de normalisation
(a) Fe510DD, ép. 40 mm
(b) BS4360:50D, ép. 25 mm
(c) BS4360:50D, ép. 40 mm
(d) BS4360:50D, ép. 60 mm
2.2 Microstructures des plaques brutes de trempe et revenu,
RQT 50 0, ép. 25 mm
2.3 Mode opératoire typique 5 kJ/mm, soudure en K
2.4 Mode opératoire typiq ue, 2 kJ/mm, soudure en X
2.5 Mode opératoire typique, soudure sous laitier
2.6 Mode opératoire typiq ue, soudure un chanfrein, 25 mm
2.7 Emplacement des instruments pour les essais sur plaque large
3.1 Températures de transition, impact 41 J - soudures 2 kJ/mm
3.2 Températures de transition, impact 41 J - soudures 5 kJ/mm
3.3 Températures de transition, impact 41 J - soudures de 2 et 5 kJ/mm , en K,
ép. 25 et 60 mm
3.4 Décalage des températures de transition, impact 41 J - soudures 2 kJ/mm
3.5 Décalage des températures de transition, impact 41 J - soudures 5 kJ/mm
3.6 Décalage des températures de transition, impact 41 J - soudures 2 et 5 kJ/mm
en K, ép. 25 et 60 mm
3.7 Plaque de bas e, courbe Impact Charpy V - Energie montrant la dispersion des
résultats
3.8 Courbes Impact Charpy V - Energie pour les zones de transition, montrant
la dispersion des résultats
3.9 Emplacement des êprouvettes et des entail les, éprouvetttes Charpy et
de déplacement d'ouverture des fissures 10 χ 10
3.10 Résultats déplacement de l'ouverture des fissures, 10mm de cô té, montrant
la dispersion
3.11 Essais transversaux déplacement de l'ouverture des fissures pleine épaisseur
de la plaque de ba se, ép. 40 mm
3.12 Comparaison des résultats de déplacement de l'ouverture des fissures - plaques
de 40 mm
3.13 Résultats déplacement de l'ouverture des fissures, plaques BS4360:50D, 25 et
60 mm
3.14 Résultats déplacement de l'ouverture des fissures, plaques RQT 50 0, 25 mm
3.15 Résultats déplacement de l'ouverture des fissures sur soudure D4W2, 50D,
en X, 2 kJ/mm
3.16 Résultats déplacement de l'ouverture des fissures pleine épaisseur - Fe510DD,
5 kJ/mm. soudure en K
3.17 Résultats déplacement de l'ouverture des fissures pleine épaisseur - BS4360:50D,
5 kJ/mm, soudure en K
3.18 Résultats déplacement de l'ouverture des fissures pleine épaisseur - Fe510DD,
soudure sous laitier (- . 50 kJ/mm)
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FR 62-10 822 7210.KA/804
3.19(a) Effet de la température de pointe, simulation cycle de. 5 kJ/mm -
BS4360:50D
3.19(b) Effet du cycle de revenu - BS4360:50D
3.20(a)
Effet de la température de pointe, simulation cycle de 5 kJ/mm -
FE510DD
3.20(b) Effet du cycle de revenu - Fe5lODD
3.21(a) Effet de la température de pointa, simulation cycle de 5 kJ/mm - RQT 500
3.21(b) Effet du cycle de revenu - RQT 500
3.22 Effet de la température de pointe - cycle 2 kJ/mm - BS4360:50D
3.23 Effet de la température de pointe - cycle 2 kJ/mm - Fe510DD
3.24 Effet de la température de pointe - cycle 2 kJ/mm - RQT 500
3.25 Microstructures zones de transition simulées - BS4360:50D (kt„ = 50 s,
soit apport de chaleur d'environ 5 kJ/mm)
3.26 Microstructures zones de transition simulées - Fe510DD (i t „ , = 50 s,
soit apport de chaleur d'environ 5 kJ/mm)
3.27 Microstructures zones de transition simulées - RQT 500 (&t„ = 50 s,
soit apport de chaleur d'environ 5 kJ/mm)
3.28 Microstructures zones de transition simulées - BS4360:50D (ût„_
c
. = 20 s,
soit apport de chaleur d'environ 2 kJ/mm)
3.29 Microstructures zones de transition simulées - Fe510DD (ût„ _ = 20 s,
soit apport de chaleur d'environ 2 kJ/mm)
3.30 Microstructures zones de transition simulées - RQT 500 (At
fi
_,. = 20 s,
soit apport de chaleur d'environ 2 kJ/mm)
4.1 Comparaison des températures de transition Charpy V et déplacement de
l'ouverture des fissures 10mm de côté
X V I
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FR 62-10 822 7210.KA/804
British Steel Corporation
Messung der Festigkeit in der wärmebeeinflußten Zone der
geschweißten Konstruktionsstähle
EKSG Vertrag Nr. 7210.KA/804
Zusammenfassung
In Anbetracht auf die zunehmende Bedeutung der Eigenschaften der wärme-
beeinflußten Zone (HAZ), die in den Spezifikationen vorgeschrieben werden,
und den hohen Anforderungen, die an das Einsatzverhalten der Stähle in
Konstruktionsverwendungszwecken gestellt werden, wurde eine Untersuchung
durchgeführt, die die folgenden Ziele hatte:
a. Kritische Prüfung der zur Zeit einschlägigen Verfahren für die Unter-
suchung der Bruchfestigkeit der HAZ und zwar unter besonderer Bezugs-
nahme auf die Bewertung der Eignung für den Zweck und auf die Fähigkeit,
die potentielle Leistung der HAZ im Einsatz mit den Ergebnissen der
Prüfungen im kleinen Umfang im Vergleich zu den breiten Metallplatten-
prüfungen vorherzusagen, die HAZ Kerben enthielten.
b. Bewertung der Eigenschaften, die in den HAZ von einigender Baustähle
erreicht werden, denn für diese zur Zeit eingesetzten Stähle wird
häufig ein hohes Eigenschaftsniveau vorgeschrieben. Die Bewertung
wurde für viele verschiedene Schweißenergiezufuhren und Schweißtypen
durchge
führt.
c. Wo möglich, Gewinnung von Einblicken in die Faktoren, die die Reaktion
auf die Schweißung und die gewonnenen Eigenschaften beeinflußen.
In der Untersuchung wurden drei Stähle eingesetzt: der BS4360:50D und der
Euronorm 52-72 Fe5lODD, die beide eine normalisierte Güte hatten, und der
RQT 500, der ein vergüteter Markenstahl der British Steel Corporation ist
und ungefähr die gleiche Zusammensetzung wie der BS4360:50D hat. Die
Schweißungen wurden bei einer Wärmezufuhr von 2 und 5 kJ/mm unter Einsatz
von einfachen V, doppelten V und K Formen zusammen mit Elektroschlacken-
schweißungen von 30 - 50 kJ/mm durchgeführt, das hing von der Metallplatten-
stärke ab. Der größte Teil der Forschung wurde auf 40 mm starken Schweis-
sungen durchgeführt, aber man machte auch einige vergleichende Prüfungen auf
25 und 60 mm starken Platten.
Man konnte mit den im kleinen Umfang gemachten Prüfungen (Charpy V, ΙΟ χ 10 mm
COD,
volle Stärke COD) alle Stähle in der gleichen Anordnung einstufen. Die
BS4360:50D Metallplatte mit einer Stärke von 40 mm hatte die beste Leistung,
die RQT 500 kam an zweiter Stelle und die Fe5lODD an dritter. Es schien,
alsob der bedeutendste Faktor, der die HAZ Eigenschaften zumindest in den
geprüften Probenmetallplatten beeinflußte, der Kohlenstoffäquivalentwert
(C.EV) war, der in den 50D und den RQT 500 Platten bei ungefähr 0,4% und
in der Fe510DD Probe bei 0,5% lag. Die Charpy und COD Prüfungen zeigten,
daß in dem grob gekörnten Bereich der HAZ zuweilen niedrige Ergebnisse
gewonnen werden konnten, aber in den breiten Metallplattenprüfungen bei
-30 und -40° C, wo ermüdete 9 χ 90 mm Oberflächenkerben in der HAZ vorlagen,
wurden Beanspruchungen in der Anordnung des Plattennachgebeausmaßes und
der Gesamtverzerrungen vor dem Bruch bestätigt, die von 1,1 bis zu 7,5
reichten, was von dem Stahl abhängig war. Zwei der Metallplattenergebnisse
wurden gemäß dem im PD 6493 angegebenen Verfahren analysiert, und man konnte
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mit den aus früheren mit geschweißten Metallen gewonnenen Erfahrungen zeigen,
daß zulässige Defektvorhersagen in den HAZ einen eingebauten Sicherheits
faktor haben, der in diesen beiden Fällen bei 2 - 3 lag.
Hinsichtlich der Prüfmethodologie war nur die richtige Anordnung der HAZ
Kerben das einzige bedeutende Problem. Man gewann eine sehr deutliche
Streuung in den Ergebnissen in allen Prüfungen, aber dies war auch eine
charakteristische Eigenschaft der Prüfungen in einigen der Ausgangsmetall
platten.
Untergrößen COD Prüfungen wurden auf Proben mit einem Querschnitt von 10 mm
2
gemacht, um genauere Hinweise auf den Bruchanfangswiderstand und die für die
HAZ typischen Mikrogefüge zu gewinnen. Prüfungen wurden durch Simulierung
der thermischen Zyklen gemacht, die aus den Prüfschweißungen abgeleitet
worden waren, und man konnte damit zeigen, daß sie ein Potential in der
Forschungsarbeit haben, obwohl sie nur begrenzt direkt in praktischen
Situationen anwendbar sind.
Ein großer Teil der thermischen Zyklusdaten wurde durch die in ausgewählten,
geschweißten HAZ eingekapselten Thermoelementen erzeugt. Man gewann gute
Übereinstimmung mit den veröffentlichten Forschungsarbeiten, und Vorschläge
wurden für die Modifizierung einiger der physischen Konstanten gemacht,
die in theoretischen Vorhersagen benutzt werden.
x v m
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Aufstellung der Tabellen
2.1 Chemische Analyse der geprüften Metallplatten
2.2 Mechanische Eigenschaften der geprüften Metallplatten
2.3 Aufgliederung der geschweißten Prüfmetallplatten
3.1 Matrix der durchgeführten Prüfungen
3.2 HAZ Charpy gegen die Prüfkriterien - BS4360:50D (40 mm stark)
3.3 HAZ Charpy gegen die Prüfkriterien - BS4360:50D
(25 und 60 mm stark)
3.4 HAZ Charpy gegen die Prüfkriterien - Euronorm 25-72 Fe5lODD
(40 mm stark)
3.5 HAZ Charpy gegen die Prüfkriterien - RQT 500 (40 mm stark)
3.6 HAZ Charpy gegen die Prüfkriterien - RQT 500 (25 mm stark)
3.7 Verhältnis des Schweißmetalls:HAZ:Metallplatte neben den
unter der Oberfläche befindlichen Kerben, einfache und doppelte
V geschweißte Charpy Prüfungen (Metallplatten/HAZ-Grenze von dem
sehbaren Ac^ genommen)
3.8 0,1 mm COD Übergangstemperaturen (IO mm
2
diagnonale 40 mm
Schweißungen)
3.9 Zusammenfassung der COD Prüfergebnisse
3.10 Prüfergebnisse der breiten Metallplatten
3.11 Prüfung der breiter Metallplatten - Kerbstellen und Dimensionen
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Aufstellung der Abbildungen
1.1 Thermische Zyklen der wärmebeeinflußten Zone - 5 kJ/mm
1.2 Geschweißtes Makrodiagramm (5 kJ/mm, einfaches V ) ,
gezeigt werden die wieder erwärmten, wärmebeeinflußten
Zonen
2.1 Mikrogefüge der wie erhaltenen, normalisierten
(a) Metallplatten, Fe510DD, 40 mm stark
(b) BS4360:50D, 25 mm stark
(c) BS4360:50D, 40 mm stark
(d) BS4360-.5CD, 60 mm stark
2.2 Mikrogefüge der wie erhaltenen, vergüteten
Metallplatten, RQT 50O, 25 mm stark
2.3 Typisches 5 kJ/mm Schweißverfahren
2.4 Typisches 2 kJ/mm, doppeltes V Schweißverfahren
2.5 Typisches Elektroschlackenschweißverfahren
2.6 Typisches 25 mm einfaches Schrägschweißverfahren
2.7.
Breites Metallplattenprüfverfahren, gezeigt wird die
Anordnung der Instrumentierung
3.1 41 J Aufschlagsübergangstemperaturen - 2 kJ/mm Schweißungen
3.2 41 J Aufschlagsübergangstemperaturen - 5 kJ/mm Schweißungen
3.3 41 J Aufschlagsübergangstemperaturen - 2 und 5 kJ/mm K Schweißungen,
25 und 60 mm stark
3.4 Verschiebung in den 41 J Aufschlagsübergangstemperaturen -
2 kJ/mm Schweißungen
3.5 Verschiebung in den 41 J Aufschlagsübergangstemperaturen -
5 kJ/mm Schweißungen
3.6 Verschiebung in der 41 J Aufschlagsübergangstemperatur -
2 und 5 kJ/mm K Schweißungen, 25 und 60 mm stark
3.7 Ausgangsmetallplatte, Charpy V Aufschlagsenergiekurve,
gezeigt wird die Streuung in den Ergebnissen
3.8 HAZ Charpy V Aufschlagsenergiekurven, gezeigt wird die Streuung
in den Ergebnissen
3.9 Probeanordnungen und Kerbstellen, Charpy und 10 χ 10 COD Proben
3.10 10 mm
2
COD Ergebnisse, gezeigt wird die Streuung
3.11 Ausgangsmetallplatte, volle Stärke, diagonale COD Prüfungen, 40 mm stark
3.12 Vergleich der COD Ergebnisse - 40 mm Metallplatten
3.13 COD Ergebnisse, 25 und 60 mm, BS4360:50D Metallplatten
3.14 COD Ergebn isse, 25 mm, RQT 500 Metallplatten
3.15 COD Ergebnisse der Schweißung
D4W2,
50D, doppeltes V, 2 kJ/mm
3.16 COD Ergebnisse der vollen Stärke - Fe5lODD, 5 kJ/mm Κ Schweißung
3.17 COD Ergebnisse der vollen Stärke - BS4360:50D, 5 kJ/mm Κ Schweißung
3.18 COD Ergebnisse der vollen Stärke - Fe510DD, Elektroschlacken-
schweißung (̂ 50 kJ/mm)
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Aufstellung der Abbildungen (Forts.)
3.19 Auswirkung der Spitzentemperatur in der Simulierung, 5 kJ/mm
(a) Zyklus - BS4360:50D
3.19 Auswirkung des Vergütungszykluses - BS4360:50D
(b)
3.20 Auswirkung der Spitzentemperatur in der Simulierung, 5 kJ/mm Zyklus
(a) Fe510DD
3.20 Auswirkung des Vergütungszykluses - Fe510DD
(b)
3.21 Auswirkung der Spitzentempratur in der Simulierung, 5 kJ/mm
(a) Zyklus - RQT 500
3.21 Auswirkung des Vergütungszykluses - RQT 500
(b)
3.22 Auswirkung der Spitzentemperatur - 2 kJ/mm Zyklus - BS4360:50D
3.23 Auswirkung der Spitzentemperatur - 2 kJ/mm Zyklus - Fe510DD
3.24 Auswirkung der Spitzentemperatur - 2 kJ/mm Zyklus - RQT 500
3.25 Simulierte HAZ Mikrogefüge - BS4360:50D, (Ate~5
= 5 0 s
'
a n
eine
eine 5 kJ/mm Wärmezufuhr angeglichen)
3.26 Simulierte HAZ Mikrogefüge - Fe5l0DD (Atg~5 = 50 s, an eine
5 kJ/mm Wärmezufuhr angeglichen)
3.27 Simulierte HAZ Mikrogefüge - RQT 500 (Ate~5 = 50 s, an eine
5 kJ/mm Wärmezufuhr angeglichen)
3.28 Simulierte HAZ Mikrogefüge - BS4360:50D,
(àtg-
5
=
20 s, an
eine 2 kJ/mm Wärmezufuhr angeçlichen)
3.29 Simulierte HAZ Mikrocefürge - Fe510DD (At8~5 = 20 s, an
eine 2 kJ/mm Wärmezufuhr angeglichen)
3.30 Simulierte HAZ Mikrogefüge - RQT 500 (Ate~5 = 20 s, an eine
2 kJ/mm Wärmezufuhr angeglichen)
4.1 Vergleich zwischen den Charpy V und 10 mm
2
C0D Übergangs
temperaturen
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British Steel Corporation
MEASUREMENT OF TOUGHNESS IN THE HEAT AFFECTED ZONE
OF WELDED STRUCTUR AL STEELS
ECSC Agreement No. 7210.KA/804
FINAL TECHNICAL REPORT
1. INTRODUCTION
1.1 The Natu re of the Heat Affec ted Zone
The visible weld heat affected zone (HAZ) is by definition, that part of the
weld joint lying between the fusion boundary with the weld metal and that part
of the structure retaining, at the optical microscopy level, the original
as-delivered micro stru cture . Within this narrow band, a few millimet res wi de ,
the steel will have been subjected to one or more thermal cycles due to heating
by the individu al weld beads laid do wn. The nature of these thermal cycles at
a given location in the HAZ is a function of the position relative to the weld
bead, and the factors affecting he at flow (thickn ess, initial steel
temperature, weld energy input). The family of curves determ ined in this
programme are shown in Fig. 1.1. In a multirun weld, metal at a given point
may be subjected to a significant number of consecutive cycles with differing
peak tempe rature s and cooling ra tes . The reheated areas of HAZ's can often be
observed in macrogra phs of multirun we lds , Fig. 1.2.
Within this narrow band of material, there exists a continuum of heating
cycles,
decre asing in peak tem perat ure and overall cooling rate , from the
fusion boundary to the outer HAZ edge , giving rise to micr ost ruct ures which
change continuously over this region. A number of general zones, within the
visible HAZ, can be identified, the extent and nature of which will vary with
steel compositi on, the thermal cycle sustained and, to a variable e xtent, the
original microstructure:-
(a) Grain Coars ened HAZ
In this region, adjacent to the fusion boundary, the original microstructure
has been reaustenitised at temperatures and retention times sufficient for
marked grain growth to occ ur. The aust enit ic grain size attained will vary
according to a number of factors :-
Distance from the fusion boundary, being greatest
immediately adjacent to it.
Weld energy input, as a function of peak temperature
and relative retention time.
Original grain size; under the non-equilibrium
conditions,
finer austenite grain sizes may result
from finer original microstructures.
Steel composition, particularly with respect to the
presence of refractory carbides or nitrides which
are difficult to dissolve in the available timescale
at high temperature, thereby exercising a pinning
effect on the austenite grain bounda ries. Compositi on
may also affect the austenitising temperature itself
and, hence, the extent of coarsening.
The subsequent transformation products will be defined by the cooling rate,
over the transforma tion ran ge, and the composition and grain size of the prior
austenite, and so may differ in detail from steel to steel, depending on the
prior thermal histor y. In gene ral, howeve r, the grain coarsened region
will consist of a variable mixture of constituents
1
·
1
. These will include one
or more of the following, in order of decreasing transformation temperature:
proeutectoid ferrite at prior austenite grain boundaries or in transgranular
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Widmanstatten plate form; areas of high carbon content ranging from pearlite to
morpho logies in which carbides precipit ate as rods or spher oids, bainitic
colon ies in which the ferrite pla tes may interlock or grow side-b y-sid e in a
manner resembling classica l upper baini te, with plate widths dependent on
transform ation temper ature; lower bainite; marte nsit e.
(b) Grain Refined Regio n
As the peak temperatures fall, the situation will eventually arise where the
HAZ has been reheated just into the auste nitis ing tempe ratur e ra nge , bearing in
mind the rapid heating rate and short retention time . This will give rise to
very fine aust eni te, which coupled with the slower cooling rates at the
increased distance from the fusion boundary, transforms to a fine equiaxed
ferrite matrix with small areas of ferrite/carbide aggregate mixtures.
(c) Intercritical Region
In this portion of the heat affected zone, the Ac2 is only exceeded in the high
carbon constituents of the original microstructure, and the original ferrite is
largely untouched . Some dilution of the high carbon austenite regions may
occur by diss olut ion of the surrou nding fer rit e, and the subse quent transforme d
stru ctur e will depend on their compo sitio n and the local cooling rate. As
the peak temperature progressively decreases, the size of the reaustenitised
region s dec rea ses , and the limit of the visible HAZ is defined by a region in
which the structure of the pre-e xisti ng p earli te is merely degraded by some
extent of spheroidisation.
(d) Subcriticai Region
Out side the visibl e HAZ is a relativ ely broad zone in which the temp eratur e
peaks are low, but the heating time s are long . This region was of great
importance with C and CMn steels, since it was possible for nitrogen strain
ageing to occur, and was, indeed, the reason for the development of the
original Wells wide plate test, to investigate the effect of the consequent
loss in cleavage fracture resistance, in full thickness welds.
The two principal factors needing to be controlled have been shown to
b e
( 1 . 2 Λ . 3 ) . :
The ferrite grain size of the parent material.
The free or interstitial nitrogen content.
These factors are adequately dealt with in the more modern fine grained CMnNb
and CMnNbAl steels, and nitrogen strain ageing is no longer the potential
problem it was.
The various regions described above merge into each other and it would be
impossible in most instances to decide on a distinct boundary between them.
In practice, there is no great necessity to do so, since, so far as fracture
resistance is concerned, it is the grain coarsened region which show the
greatest degree of degradation from the original properties.
The extreme heterogeneity of even the HAZ adjacent to a single run weld, to
which must be added the variability of tempering by subsequent runs, in a
multirun situation, delineates the problem facing the research worker
investigating the properties, or even the microscopy, of real welds. The
process zone associated with the smallest mechanical test piece is bound to
encompass regions of markedly different microstructures and properties, tending
to blur any relationships sought between structure and properties and,
possibly, to introduce scatter in repeat tests taken from nominally the same
position with reference to the weld.
To some degree, the original steel is itself heterogeneous with variable
structures from surface to centre and centre to edge in plate products, and
between regions of differing thickness in rolled sections. Segregation of
various alloying elements occurs, and its effects on transformation can be
clearly seen in many HAZ macrographs. Non-metallic inclusions are always
directionally aligned, to some extent, and will ensure that, in particular,
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fracture toughness may show marked anisotropy, between longitudinal, transverse
and short transverse specimen orientations. Even when a single orientation is
taken, many types of test result show a wide normal distribution. It would be
unwise to expect a similar population of HAZ results to exhibit more convenient
characteristics.
The foregoing, therefore, presents some of the basic difficulties involved in
any attempts to characterise HAZ properties or to compare the HAZ performance
of different steels. The main aim of this programme was to assess the extent
of these problems, in real welds, when carrying out the types of fracture
toughness tests employed by the fabrication industry. This would provide
information enabling a judgement to be made on how much significance should be
attached to very limited programmes of testing, often carried out by
fabricators or even classification societies under conditions less controlled
than those of the research laboratory.
1.2 Importance of Heat Affected Zone Properties
The overall aim in a welded joint, with respect to fitness-for-purpose, must be
to obtain a joint in which the three component parts - parent steel, HAZ and
weld metal, are each capable of withstanding the demands which the application
places upon them, bearing in mind the probable size and location of defects
either present after fabrication or developing during service. The degree of
attention which the engineering industry has focussed on each of these three
types of material has varied from time to time, depending on the major current
problems.
In the early days of brittle fracture, the major cause of concern was the
fracture toughness of the parent material, leading to the wide spread use of
the Charpy impact test to classify materials, as an aid to selection of steel
for applications of varying severity. Other studies of the factors affecting
toughness, led to a long process of improvements in steel composition and
processing, has led to a situation where, it is possible to conclude that, for
the majority of structural applications, the range of steels currently
available is adequate to guarantee safety against fast fracture over those
parts of the structure unaffected by welding.
As steel properties have improved, and as welded structures have developed into
larger and more complex designs, increasingly operating under more severe
conditions and with serious commercial and safety penalties in the event of
failure,
complementary developments in welding consumables and procedures have
been necessary. The offshore oil and gas field exploitation, and the
accompanying distribution systems and processing plants, have resulted in a
marked increase in fundamental work and commercial development work on both
manual and automatic consumables and procedures, such that the properties
required, particularly fracture toughness, have been achievable in massive
complex structures. Defect tolerance approaches to design, facilitated by
improved stress calculation methods and inspection techniques, have played a
vital role.
Interest in the HAZ has varied from time to time, in technical terms, and has
in more recent years assumed strong commercial aspects.
1.2.1 Technical Importance of HAZ Properties
In the past, the importance of HAZ toughness has been closely considered with
the incidence of hydrogen induced cold cracking, on which a vast amount of
research work has, and is being carried out. It is now clearly
understoodt
1
-^ )
that three conditions must be present for H2 cracking to
occur :-
An HAZ with a susceptible hardened microstructure,
promoted by higher carbon equivalent values (CEV)
and faster cooling rates.
A weld metal hydrogen content above a critical
level for the given steel and type of joint.
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A critical level of stress across the joint,
varying depending on the severity of the two
factors,
given above, promoted by heavy
restraint in the joint, and intensified by
any unfavourable geometric features present.
Based on existing data, monograms are available
(
l
"
5
) which for the normal
range of structural grades, will allow hydrogen cracking to be avoided by weld
metal hydrogen control and/or adjustment of cooling rate by preheating to a
temperature which is defined by the CEV and combined thickness.
Investigational work continues into such areas as joints of greater thickness,
the effect of high yield stress (in, for example, Q & Τ steels), and the
behaviour of the latest types of structural steel (e.g. low carbon, very low
sulphur).
Until relatively recently, the properties of the HAZ have only been regarded in
the sense of their ability or otherwise to tolerate the presence of spasmodic
H2 cracking. The relative defect tolerance of the HAZ against other potential
failure modes has, by comparison, received much less attention, historically,
perhaps for the very good reason that it is almost impossible to discover any
failures in which the HAZ has been the prime cause, except in the presence of
H2 cracks.
The measures taken to design out H2 cracking (lowering of CEV, reduced cooling
rates, etc.) will also tend to improve the fracture toughness of the HAZ - a
dual gain in joint reliability. Therefore, the potential failure modes are
initiation from lack of fusion/penetration defects, after fabrication, or due
to environmental effects during service (fatigue, stress corrosion, corrosion
fatigue).
The toughness required to withstand pre-existing fabrication defects can be
assessed using well established defect tolerance approaches, based in this case
on the grain coarsened HAZ properties, together with a knowledge of the service
stresses and NDT discrimination level.
The situation with respect to in-service cracking is extremely complex,
particularly when corrosive environments are involved. Design procedures
against fatigue in normal atmospheres are well establishedÍ
1
-°) and now being
included in British Standards. HAZ's are of interest because the likely
initiation sites at the edges of the weld reinforcement, for instance, will
ensure that the growing crack will, firstly, have its tip located in the HAZ
for the first part of its growth, and, secondly, will, during this period, be
subjected to the maximum stress concentration factors (SCF) due to the weld
profile and any geometric effects associated with the weld location. It is
relatively easy, however, to define a worst case after the potential fatigue
initiation sites have been identified and to calculate the fracture toughness
required to ensure the survival of the structure over this interval of fatigue
crack growth.
A number of factors combine to reduce the probability of failure from fatigue
cracking:-
The region of lowest toughness, the grain coarsened
HAZ,
usually has the highest strength, and an advancing
crack will tend to turn rapidly away into softer
material, of higher toughness. This phenomenon
presents constant problems in the fatigue precracking
of HAZ test pieces, particularly where cracks adjacent
to the fusion boundary are required. The outer areas
of the HAZ and the parent plate, which come into play
as the crack grows, are of higher toughness and can provide
the necessary increased defect tolerance, once this
initial danger period is over.
In many instances, e.g. fillet welds, the SCF associated
with the fatigue crack initiation sites decays very
rapidly, and this effect coupled with the probability
of increasing crack tip toughness, can cause a progressive
decrease in crack growth rate and even lead to stable
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arrested cracks, which will be below the maximum
tolerable size for the crack tip material and, hence,
present no danger to the integrity of the structure.
In corrosive atmospheres, particularly for steels in contact with media which
charge the steel with hydrogen, the situation may be less encouraging.
Hydrogen has the general effect of reducing the resistance of steels to almost
any form of cracking, so that two factors, at least, can lead to an increased
possibility of failure:-
The crack tip fracture toughness, per se, may be
reduced, resulting in a lower tolerable defect size.
Crack growth can continue under lower stress ranges,
making the situation of sessile non-critical cracks
less likely.
The relatively high strength of some parts of the HAZ, in comparison to the
parent plate, and the presence of residual stresses from welding can sensitise
the areas adjacent to welds to certain forms of environment cracking. In some
cases,
the resistance of the parent steel to more generalised types of
cracking will be important.
The consideration of these environmental effects, which are of prime interest
at present in the oil and gas recovery and processing fields, are, however,
outside the scope of this report, but may have some influence on attitudes
towards the properties of welded joints under less severe conditions. Steel
and/or weld procedure selection may be constrained, for instance, by a maximum
HAZ hardness criterion.
Another important aspect which has reduced the effect of local embrittlement,
is the narrowness of the band of material worst affected, generally 1 mm or
less. Unless the properties are at or, near the lower shelf of the transition
behaviour, or loading is extremely rapid, the plastic zone at the crack tip
will be able to grow, under increased loading, to such an extent that tough
material on either side becomes involved in the prefracture process zone,
giving increased crack tip toughness. Ductile crack growth, if it occurs and
the mechanical constraints on crack propagation are not too severe, will tend
to favour movement into softer and tougher HAZ regions. There is a close
similarity to the situation referred to above for advancing fatigue cracks, in
that once an initial danger period is past, the situation at the crack tip can
improve markedly. This inability of most HAZ's to contain a critical event is
the most likely reason for the absence of failure case histories citing the
properties of sound HAZ's as a cause of failure, and has led to the
recommendation in the UK that it is unnecessary to carry out HAZ testing, on
the normal types of structural steels, where the weld energy lies between 1.5
kJ/mm and 4-4.5
kJ/mmt
1
-
7
)-
There is, of course, great commercial interest in
increasing productivity by using higher weld energies, but it becomes advisable
then to assess the effect of HAZ degradation, since the increased HAZ width may
allow the HAZ to assume a potentially more significant role in possible failure
modes.
Heat affected zones in electroslag welds are an extreme case, being not
only extremely wide, of the order of 5-8 mm, but having an extended region of
very coarse austenitic grain size adjacent to the fusion boundary. The
combination of low toughness and large width make the reliability of the HAZ
for structural purposes very suspect. The weld metal, similarly, with a coarse
as-cast structure, has very poor toughness, and it has been usual to normalise
electroslag welds intended for service at ambient temperatures. The economic
advantages of the process still motivate development work, directed towards
improving the as-welded properites of electroslag welds, such as narrow gap
welding to reduce heat input and improve economicsÍ
1
-
8
), improved alloyed weld
metals
I
1
-
9
),
and the use of steels more tolerant of high heat inputs(
x
-
1
°).
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Temperature, C
1500
1400.
1300-
1200-
1100
ifr
ìsai
7 Effect of varying
interpass temperature
Time, s
HEAT AFFECTED ZONE THERMAL CYCLES - 5 kJ/mm HEAT INPUT
FIG. 1.1
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F R 6 2 - 1 0 8 2 2
7 2 1 0 . K A / 8 0 4
WELD MACROGRAPH (5 kJ/mm, SINGLE V)
SHOWING REHEATED HEAT AFFECTED ZONES
FIG.
1.2
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2. EXPERIMENTAL PROGRAMME
2.1 Aims and Obj ect ives of the Work
In view of the foregoing discussion of the increasing requirements of customers
and classification authorities for HAZ testing, and the difficulties which the
inhomogeneous and narrow nature of the HAZ presents in testing, there were two
discrete but complementary major aspects to the programme:-
(a) A critical examin ation of the available methods for
investigating the fracture properties of the HAZ's
of structural stee ls, with particular reference to
their suitability for guaranteeing fitness for purpose
of welded s truc ture s, with the overall aim of assess ing
the relationships, if any, between sub-size and full
thickness te sts, and ascertaining the degree of safety
of defect tolerance predictions, using wide plate tests.
(b) Using current high quality structural steels of various
types, to gauge the practical effect of the above tests
in,
so far as possible, real situations within the
present fabrication industry.
To achieve these aims, three steels in current production were chosen:-
Fe510DD (European
25-72),
aluminium grain refined
but containing no niobium.
BS4360:Gra de 50D, an aluminium killed, niobium
grain refined steel of equivalent minimum
guaranteed tensile and impact toughness properties.
RQT 500, a BSC proprietary quenched and tempered
steel,
of similar composition to BS4360:50D,
but having higher gu arant eed t ensile and impact
energy lev els (470 N/m m
2
YS, 41 J at -40°C).
Alth ough the majori ty of the work was carried out on 40 mm thick pl at es ,
additional plates at 25 and 60 mm were included to define thickness effects
arising from thermal differences in the welds and varying constraints in full
thickness test pieces.
To preserve the relevance to current practice, tests were extracted from full
thick ness welds with various ty pes of weld prepar atio n (single and double V, K,
butt),
using prac tica l weld pro ce du re s, over a wide range of heat input (2 and
5 kJ/mm plus electroslag), to gauge weld energy and HAZ width effects.
As well as the effec ts re sulting from the metho dolog y of tes ting , it was of
interest to attempt to gain information on the underlying reasons for
differences in behaviour between weld types and heat inputs and between
different steel compo sitio ns. All welds were examined metallog raphical ly and
small scale tests were also produced by a thermal simulation technique using
specially built equip ment , programmed with thermal data derived from the test
welds.
Details of the various aspects of experimental work will be given in subsequent
sections.
2.2 Steel s Used in the Test Prog ramme
Types of steels commonly used in high demand applications, such as offshore
structures,
were chosen, over a range of composition types and yield strengths.
No attempt was made to use other than normal commercial steels; full width
plates were ordered through normal chan nels . Full ultrasonic examination was
requested to avoid wast age of test materi al due to internal de fe ct s. The
Fe510DD plate ex Creusot Loire was ultrasonically examined to NFA 04 305,
normal grade, and the BS4360:50D and RQT 500 plates, both of BSC manufacture,
to BS5996 Grade LC3.
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The chemical compositions and mechanical properties of all the steel plates
tested are given in Tables 2.1 and 2.2 , respectiv ely. Results are given from
the mill certificates and check tests carried out on the plates received.
2.2.1 Normali sed Steels
Both BS43 60:5 0D and Euron orm 25/72 : Fe510DD are steels aimed at the same
market,
high demand appli cations for welded fabrications in high yield ste el,
requiring low temperature impact energy guar ante es. Minimum property levels
are very similar in the two st ee ls . The major diff eren ce between the two
lies in the approach to grain refinement; BS4360:50D uses niobium additions to
an aluminium killed CMn steel, Fe510DD relies on the presence of A1N to
achieve grain refinement - there is no niobium additio n. The two philosophi es
have implications related to welding, with respect to the effects of the
relative CEV's required to achieve the guaranteed tensile properties and to the
effic iency of the grain refining mechanis m in the coarse grained HA Z. Both of
these have potential for affecting HAZ properties.
Compa ring the two 40 mm sample plat es in Table s 2.1 and 2.2 , it will be
that:-
(a) The chemical analyses are satisfa ctory, except that
the % C in two of the Fe510DD sa mples was margi nally
over the maximum 0.22% allowed in the product, which
together with a slightly higher Mn content and the
presence of some Cr, gave a CEV of 0.51, compared
with 0.40 in the 50D st ee l. The margin over the
minimum guaranteed yield strengths was higher in
Fe5 10D D. On the other hand , the 50D sample
achieved better impact toughness levels , at -45°C ,
than the Fe510DD at -20°C, in both testing
directions.
BS4360 :50D was used to compare thickness effe cts, and plates at 25 , 40 and 60
mm thick were teste d. Tabl es 2.1 and 2.2 show that the comp osit ions wer e
similar, the major differences lying in the carbon contents, and hence
CEV's.
All plates met the minimum tensile requi remen ts, with rather small margins in
the 40 and 60 mm plates, but a rather large margin of -40 N/mm
2
in the 25 mm
plates,
no doubt because of its rather high C conte nt. Neve rthe less , its
CEV was only 0.42%. All samples wer e, simila rly, comfortably above the
minimum guaranteed impact toughness levels, the 25 and 60 mm plates being
similar, at a much lower level than the 40 mm plate, bearing in mind the test
temperature difference.
The microstructures observed in the plates received are shown in Fig. 2.1.
They are essentially all of the same type - bands of pearlite in a ferritic
matrix, but there are differences, apparent even at the optical microscopy
level. The higher carbon conten t of the 40 mm Fe510DD plate is observed as a
higher volume fraction of pear lite . Centreline segregation is obvious in the
Fe510DD and 50D samples, causing bainitic bands to appear.
2.2.2 Quench ed and Tempe red Stee l
In order to look at the effects of chemical composition, initial microstructure
and strength level on HAZ struct ures and prop ert ies , it was decided to include
as one of the sample mater ial s, RQT 500, a BSC proprietary roller-quenched and
tempered steel . These steels are produced from, basicall y, the same feedstock
as BS4360:50D, the higher property levels being achieved by virtue of the
difference in heat treatme nt.
In Table 2.1, it will be seen that, comparing the 40 mm plates R4 and D4, the
CEV's are very similar, the lower carbon level in D4 being offset by its higher
Mn, Cu and Ni con ten ts. The 25 mm pla te, R2 , is lower in CEV, almost totally
due to lower carbon content.
Table 2.2 shows, firstly, that the plates achieve the minimum guarantee levels
comfor tably with one marg inal yield level in R4 . The longi tudina l impact
energies are comparable with those obtained in the normalised D4 plate,
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although greater anisotropy is obvious from the transverse resu lts. Second ly,
the QT treatment has raised the yield strength and UTS by -130 N/mm
2
.
The micro stru ctur es of the two RQT 500 plate s are shown in Fig. 2.2, and can be
seen to consist of equiaxed ferrite, with bainitic areas.
2.3 Weld Procedur es
The main body of the work was based on large test we ld s, aimed at :-
(a) Allowing the practic al difficulti es of the
various types of test to be assessed.
(b) Indicat ing the prope rty levels achieved by
the three steel grades used, over a range
of test types, weld c onfigurations and
energy in puts, and plate thic kness es.
So far as pos sib le, the weld proced ures laid down used normal fabric atio n sh op
methods,
to avoid creating a laboratory type study which would not be of
general applicability in the fabrication industry.
Welds were carried out on the common types of weld preparation - single V,
double V and K, plus square butt preparati ons for the electroslag we lds . For
the 25 mm plat es on ly, the K format was modified to a single bev el (90° one
side,
45° on the other), Fig. 2.6. The programme aimed to cover, also , as
wide a range of weld energy inputs as possible, from manual metal arc (MMA)
levels, through submerged arc (SA) heat in puts , up to typical elec trosl ag (ES)
levels.
Beca use of the inherent variabil ity in heat inputs in MMA we ld s, it
was decided to use two submerged arc machine settings, at 2 kJ/mm, typical of
MMA , and 5 kJ/mm, a typical input energy for single wire SA welding and
slightly above the upper limits of the range where HAZ properties of normal
structural steels are widely regarded as being of no practical concern í
1
-
7
).
The energy input to ES welds is around an order of magnitude higher, depending
on operating cond itio ns. In the 40 mm pla tes , for example, it was around 50
kJ/mm , but is diff icult to compare because of conducti ve losses to the copper
cooling shoes.
Preheat levels were applied according to the recommendations of B S S l S o t
1
-
5
) , on
the basis of combined joint th ick nes s, CEV and heat inp ut, to avoid HAZ
hydrogen induced cracking, which could, of course, have interfered seriously
with the testing pr ogr amm e. In order to avoid pote ntia l prob lems due to
fatigue cr acks , correctly located in the HA Z, breaking across into the weld
metal, as has occurred in some HAZ studies(
2
-
) ,
extremely tough SA weld metals
were prod uced using a Mo-B wire (Oerlikon Tibor 22) with a fully basic fl ux,
O P 1 2 1 T T (
2
-
2
).
Heavy strong backs were used to restrain the two halve s of the
test weld, to simulate a real structure and prevent, so far as possible,
angular distor tion, which can cause problems in COD testing. In cutting back
the original root runs prior to welding the second side of a weld , a minim um
amount of grinding was used, particularly in the Κ welds, to prevent
dist urba nce to the flat HA Z. No air-arc gouging was used becaus e of the HAZ
which it can pro du ce. This is not unduly seve re, but it was diff icul t to
assess the potential heat input, and because of its location at the weld root
might affect the heat input effects which the test programme was intended to
evaluate.
Except for the weld preparations and heat inputs, the general methods used were
identical and not all weld proc edur es will be det aile d. Exampl es are however
given in Figs. 2.3-2.6.
The large number of test specimens required necessitated the production of
2.5 m long we ld s. For con sis ten cy, these were carried out as a single weld ,
with the exception of the electroslag wel ds, where the machine size limitations
necessi tated the prep arat ion of two 1.5 m we ld s. After wel din g, the plat es
were examined ultrason ically for major defe cts, which might have caused
specimen wastage.
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2.4 Test Methods
Whenever possible, standard test methods and/or practices used in the
fabrication industry were employed, although in many instances no specific
instructions are given for the HAZ situation.
2.4.1 Charpy V-Notch Impact Tests
Charpy impact energy tests were carried out on 10 χ 10 mm standard specimens,
to BS131:Part 2. Check tests on sample plates were carried out in longitudinal
and transverse orientations, in the normal subsurface positions. In addition,
for comparison with root specimens in the two-sided welds, specimens in the
transverse orientation were extracted from the 40 and 60 mm plates. Specimens
were tested over a temperature interval to define the transition behaviour.
The specimens taken from the weld HAZ's, in subsurface and root locations
(Fig. 3.9) were marked at the fusion line (FL) and at 1 mm, 2 mm and in some
cases 5 mm into the HAZ. All specimens were transverse to the rolling
direction, to take the worst case, and the notches were oriented along the
rolling direction (TL specimen). Ten specimens were tested for each notch
location, to define the transition curve, for comparison with the parent plate
values.
In order to locate the notches, overlength specimens were etched in the finish
machined (10 χ 10 mm) size and the notch position marked by scribing. The
notches were then machined and the specimen trimmed to length. In all cases,
the FL reference was taken at the centre of the face of the specimen. In the
welds with sloping fusion boundaries, single and double V welds, the notch in
the surface specimen will therefore include about 50% weld metal in FL
specimens and progressively less at the other notch locations. Depending on
the exact shape of the fusion boundary, the root specimens and the specimens
taken from Κ and ES welds should have less weld metal involved in the notch
root.
2.4.2 Sub-size (10 χ 10 mm) Crack Opening Displacement Tests
Specimens for this test were extracted in identical fashion to the Charpy V
test specimens - subsurface and root locations, TL orientation. Specimens
were again macroetched to locate the notch positions, notching in this case
being carried out with a 0.15 mm thick rubber bonded SiC cutting wheel,
followed by fatigue extension. The provisions of BS5762:1979(*-
3
) were
followed with respect to notch geometry, testing and the calculation of crack
tip COD from the test results. Testing was carried out on a screwdriven
Instron machine (150 kN
capacity),
with a cold N2 gas atmosphere, maintained by
a feedback control system, at the test temperature, by means of a thermocouple
attached to the specimen.
2.4.3 Full Thickness COD Tests
These were carried out to the full provisions of BS5762:1979 on 2B χ Β TL
oriented specimens. The specimens were again macroetched in machined blank
condition and notch positions marked as before, for cutting with a V tipped
diamond cutter, prior to fatigue extension. Four specimens were normally used
for each notch location, with the aim of defining, if possible, the transition
range.
After testing, the broken test pieces were sectioned at right angles to the
fracture face, across the position of fracture origin, if visible, or at the
centre of the thickness, if not, polished and examined microscopically to
determine the position of the fatigue crack tip relative to the fusion
boundary.
Tests were carried out on an Avery-Denison hydraulic machine, of 50 t capacity.
2.4.4 Wide Plate Tests
Wide plate tests were carried out on a 4000 t facility, the test plate, 1 m
square,
was welded, after the longitudinal test weld has been notched, into two
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loading yokes against which the four 1000 t rams bear. Cooling was carried out
with liquid-nitrogen sprays, over the central area of the plate.
The notches in the six 5 kJ/mm K welds tested (40 mm thick, two from each
grade,
at -30 and 40°C) were surface notches with a nominal 10:1 aspect
ratio, so far as the deepest part of the notch was concerned. A 6 mm deep
pre-notch was cut into the weld so that its tip lay in the HAZ, nominally 1 mm
from the fusion boundary. Judging the position on the surface of the weld,
ground flush with the plate surface, was extremely difficult, since the only
points of reference were the ground and macroetched ends of the weld, some
0.5 m from the area of interest, and the fusion boundary of the capping bead on
the surface in the area to be notched. Any changes in the cross section of
the weld, or the width of the capping bead along the length of the weld, were
likely to lead to lateral misplacement of the notch tip. Mechanical
prenotching was carried out with a specially designed rotary saw, with a
0.15 mm SiC blade, which could be moved along the length of the notch to
produce a flat tip, with ends following the radius of the blade. This prenotch
was subsequently extended, by bending fatigue, to about 9 mm in total. The
actual values are given in Table 3.10. The progress of fatigue extension was
followed using a precalibrated ac impedance device.
The plate was instrumented using linear displacement transducers (LDT) and COD
clip gauges as shown in Fig. 2.7. A range of gauge lengths was used for the
LDT's to show, to an extent, the strain distribution in the plates. The
strain on each LDT was sampled at approximately 5 s intervals during the test
and stored, with the instantaneous load reading, in a data logger. The three
clip gauges were mounted in the centre and at the two extremities of the notch,
and their outputs were logged in the same fashion. In addition, normal COD
test XY plots against load were produced. After the test, the fracture
surfaces were photographed, and then sectioned at right angles, as in the COD
tests,
to determine the notch position relative to the fusion boundary.
2.4.5 Thermal Cycle Data Acquisition
The interest in the thermal history stemmed from a desire (a) to know the
general levels of heating rate and cooling rate over the approximate
transformation range, taking in common with many other studies as 800-500°C
(Ats-s), in order to produce representative HAZ material by thermal simulation,
and (b) to observe any systematic differences in cooling rate between the
different weld preparation types used. Details of the method used to embed
thermocouples close to the fusion face of a representative selection of the
actual test weld plates are presented in the Appendix, together with the
results obtained.
2.4.6 Simulation Studies
A simulator was built, for this programme, using resistance heating, from a
welding transformer, of 12 χ 12 mm transverse specimens, held in water cooled
jaws, which were capable of imposing cooling rates in excess of those recorded
from the test welds. Thermal cycles typical of various regions in the HAZ's
of the test welds were imposed using a Research Inc. DATA-TRAK unit controlled
by feedback from a Pt-Pt/Rh thermocouple, spot welded to the centre of the heat
treated region of the specimen.
The histograms given in the Appendix suggest that the most characteristic Ate-5
values for 2 kJ/mm, 5 kJ/mm and electroslag welds, in 40 mm plate, are 15, 48
and 245-295 s respectively. Simulated HAZ specimens were produced for a single
pass situation, i.e. no tempering effects, for peak temperatures of 950, 1150
and 1350°C, with Ate-5 values of 16 and 50 s, to cover 2 and 5 kJ/mm welds,
and, for electroslag welds, a single peak temperature, 1300°C and a Ate-5 of
300 s.
To gain some insight into the effects of tempering by subsequent runs,
specimens from each steel were given an initial thermal cycle to 1350°C and asecond to 950°C, the Ate-s value in each case being 50 s.
Charpy V impact toughness tests were carried out in each simulated condition,
together with Vickers hardness tests at 5 kg load (HV5) and optical microscopic
examination.
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TABLE 2.2 MECHANICAL PROPERTIES OF PLATES TESTED
TI
Steel Grade
Fe510DD
(Normalised)
BS4360:50D
(Normalised)
Thickness
mm
40
(DD4)
25
(D2)
40
(D4)
60
(D6)
Mill Cert.
Check 1
Check 2
Check 3
Spec.
Mill Cert.
Check 1
Check 2
Check 3
Spec.
Mill Cert.
Check 1
Check 2
Check 3
Spec.
Mill Cert.
Check 1
Check 2
Check 3
Spec.
YS
N/mm
2
(L)405
(L)384
(T)388
(L)398
(T)400
(L)404
(T)405
>345
(L)392
(L)397
(T)398
(L)397
(T)391
(L)391
(T)396
>355
(L)426
(L)365
(T)351
(L)347
(T)355
(L)353
(T)362
>345
370
(L)367
(T)357
(L)361
(T)358
(L)342
(T)342
>340
UTS
N/mm
2
585
574
572
583
588
583
590
510/610
540
542
550
546
550
549
547
490/620
525
511
499
503
505
506
504
490/620
545
526
525
516
523
519
512
490/620
Elong,
on
5.65 / S
% °
29
40
32
37
37
39
>22
29
28*
31
28
26
30
31
>20
32
43
42
41
44
43
41
>20
32
31*
32
33
39
30
32
20
Impact Energy, J
(L)
(T)
(T)
(T)
(L)
(L)
(T)
(T)
(T)
(L)
(T)
(T)
(T)
(T)
(L)
(L)
(T)
(T)
(T)
(L)
96,
72, 102 at -20°C
76,
84, 84; (L) 124, 114, 120
77,78,
82; (L) 94, 103, 11
afc
_
2()0(;
64, 81, 84; (L) 109, 126, 81
40 J average at -20°C
67, 57, 64 at -30°C
78,
100; (L) 72, 90
64, 80; (L) 103, 90
afc
_
2 Q O C
84,
76; (L) 78, 87
41 J average at -20°C, 27 J average at -30°C
57, 68, 59; (L) 94, 103, 128 at -40°C
140, 140, 150; (L) 90, 126, 136
102,
139, 128; (L) 116, 74, 121
afc
_
i50Q
134, 96, 126; (L) 130, 139, 128
41 J average at -20°C, 27 J average at -30°C
88,
116, 98 at -20°C
98, 88; (L) 96, 108
78, 70; (L) 120, 96
afc
_
2QO(:
96,
89; (L) 92, 84
41 J average at -20°C, 27 J average at -30°C
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TABLE 2.2
(Continued)
τι
55
Steel Grade
RQT 500
(Quenched
and
Tempered)
Thickness
mm
25
(R2)
40
(R4)
Mill Cert.
Check 1
Check 2
Check 3
Spec.
Mill Cert.
Check 1
Check 2
Check 3
Spec.
YS
N /mm
2
545
(L)359
(T)528
(L)506
T)
524
(LJ519
(T)520
>470
564
(L)501
(T)502
(L)485
(T)469
(L) -
(T)490
>470
UTS
N/mm
2
645
636
636
620
630
624
625
560/710
680
625
629
619
611
638
560/710
Elong,
on
5.65
fS
% °
46
42
40
42
40
42
40
>21
24
20
19
19
24
22
>21
Impact Energy, J
(L) 115, 130, 108 at -40°C
(T) 86, 86, 74; (L) 130, 126, 124
(T) 80, 76, 78; (L) 110, 105, 115 at -40°C
(L) 41 J average at -40°C
(L) 62, 66, 80 at -40°
(T) 91, 81, 85; (L) 92, 118, 82
(T) 75, 87, 94; (L) 106, 104, 86
afc
_
4 Q O C
(T) 53, 86, 7 8; (L) 178, 120, 84
L 41 J average at -40°C
Converted from non-standard gauge length to a gauge length
of 5.65 /S according to BS3894:Part 1, 1965
>
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TABLE 2.3
SUB-DIVISION OF WELD TEST PLATE
^ A Β C
E
G
A
Test Piece Allocation
mm
A -
Β -
C -
D -
E ■
F ■
G ■
Discard
- 2B χ Β Full thickness COD
Reserve
Macro/micro/analysis
Thermometry
Charpy impact toughness
10 χ 10 mm COD
80
1145
255
50
205
560
205
2500
(R1/8872)
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^«^^a^:
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x 200
Subsurface
χ 400
Subsurface
Centre
(b) BS4 360 .50 D, 25 mm thick
FIG. 2.1
Continued)
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F R 6 2 - 1 0 822 7 2 1 0 . K A / 8 0 4
Tr-· ^ ^ ^ * * * * * * ^
: ^ ^ > r ^ '
ψ0* *'Μ
^ ' Ρ * ' - V .
x 200 Subsurface
x
400 Subsurface
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2.1
(Continued)
19
8/19/2019 Measurement of toughness in the heat affected zone of welded structural steels
50/204
8/19/2019 Measurement of toughness in the heat affected zone of welded structural steels
51/204
F R 62- 1 0 822
7 2 1 0 . K A / 8 0 4
χ
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M I C R O S T R U C T U R E S OF A S - R E C E I V E D Q U EN C HE D AND T E M P E R E D P L A T E S
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T H I C K
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8/19/2019 Measurement of toughness in the heat affected zone of welded structural steels
52/204
F R 6 2 - 1 0 8 2 2
7210 .KA/804
WELD No.
D4K5
(W673)
PROJECT
ECSC
HAZ
PROGRAMME
NUMBER
7210 .KA/804
SIGNED A .
Welder
DATE
WELD PREPARATION
S e e over
PASS tOCATION AND SEQUENCE
S e e over
PARENT
PLATE
THICK
(mm)
4 0
GRADE
STOCK No
B S 4 3 6 0 : 5 0 D
WELDING PARAMETERS
W 3
POWER SUPPLY
S I D E 1
d c
SIDE 2
d c
METHOD OF PREPN.
Flame c u t
POLARITY
+ v e
+ v e
WELDING PROCESS
Submerged a r c
POSITION
Downhand
ELECTRODE
CONFIGURATION
S i n g l e
S i n g l e
TOET
1
ONSUMABLES
TYPE
STORE
No.
PASS No.
4 - 1 2
FILLER WIRE
R o o t
-
E7016-1
R p s t
-
T i h n r
? ?
DIAMETER mm)
HOT WIRE
STICK OUT mm)
3 0