Disclosure to Promote the Right To Information

Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public.

इंटरनेट मानक

“!ान $ एक न' भारत का +नम-ण”Satyanarayan Gangaram Pitroda

“Invent a New India Using Knowledge”

“प0रा1 को छोड न' 5 तरफ”Jawaharlal Nehru

“Step Out From the Old to the New”

“जान1 का अ+धकार, जी1 का अ+धकार”Mazdoor Kisan Shakti Sangathan

“The Right to Information, The Right to Live”

“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता है”Bhartṛhari—Nītiśatakam

“Knowledge is such a treasure which cannot be stolen”

“Invent a New India Using Knowledge”

है”ह”ह

IS 12016 (1987): Cypermethrin EC [FAD 1: Pesticides andPesticides Residue Analysis]

GrZ

IS s 12016 • 1987( Realnnned 1997)

Indian StandardSPECIFICATION FORCYPERMETHRIN EC

( Second Reprint DECEMBER 20(0)

UDe 632.951 cvr

(0 Copynglu llJS7

BUR E A U 0 FIN D I A N S TAN DAR I) SMANAK BHAVAN, 9 BAI~ADUR SIIAJI ZAl~AR MARG

NEW DEUll 110002

Stptembei 1987

IS I 12016 • 1987

Indian StandardSPECIFICATION FORCYPERMETHRIN EC

Pest Control Sectional Committee, AFCDC 6

Chairmal'lbR R. L. RAJAK

Repres,.,tlng

Directorate of Plant Protection, Quarantine &.Storage (Ministry of Agriculture & RuralDevelopment ), Faridabad

Committee,

SHRI S. K. GHOSH (Allerna', I )SHRI R. S. SJiAJ(IIA ( Alt,rnat, I I )

DR S. S. GUPT~ Bayer ( India) Limited, BombayOlt R. N.JUKAR (Alt,rnat, )

DR V. N. IVElt Coromandcl Indag Products India (P) Limited,Madras

Sunl O. K. BHATN'AGAR

M",,6,rsOK P. K. AOGARWAL IDMA Laboratories, Chand'Barh

I Suur ACHJN'r CHAUDHRY ( .Alternat,). DR H. L. BAMI Pesticides Residue Analy,is Sectional

AFDC 56, BIS1l)1~ B. BANBRJEE Tea Research Association, Jorhat

DIe. G. SATYANARAYANA ( Alternate I )SURI S. C. DAB ( Alt,rnat, II )

DR S. R. BAROOAH Pesticides Formulators Association of India ( 551 ).Bombay

Agriculture Department, Government of UttarPradesh, Lucknow

I SHRI RAM NARAJN SINGH ( Alt,rnal, )~ SHRI N. S. BUtDIE Shriram Institute for Industrial Research, Delhit SHin R. K. BAJfSRJEB ( Alt,rnat, )~ SHIH D. CUATTEUJEE Agriculture Department, Government of West1 Bengal, CalcuttaI SHIH M. V. DESAI Atul Products Limited, AlUI• SKRI A. R. 01-:9Al ( Altmad/, )t SlIRI G. D. GOKHALF~ Bombay Chemicals Private Limited, BombayI SHRI P. M.JADHAV ( Altlrn"t')r 58ftl B. K. VI.T A Y A GOPAL Agromore Limited, Bangalore

SHRI S. K. RAMAN ( AII,rnat, )DR R. C. GUPTA Central Insecticides Laboratory, Directorate of Plant

Protection. Quarantine & Storage ( Ministry ofAgriculture & Rural Development ), Faridabad

DR M. O. ALIAS ( Alt,rnat, )

( Conlinu,d on !'aR'2 )

@ Co/J.1rl,Ia, 1987BUREAU OF INDIAN STANDARDS

This publicatioD is protected under the IniilliJ Cop"rl,h' Ad (XIV of 1957 ) andreproductioD in whole or in part by any means exeept with written permission of thepublisher shall be deemed to be an in(rlD.ement of copyright under the said Act.

IS : 12016 • 1917

( Conlinwtl from /Jag' I )

Department of Agriculture, Government ofKamataka, Bangalore

Agriculture Department, Government of Punjab,Chandigarh .

National Organic Chemical Industries Limited,Bombay

Central Food Technological Research Institute( CSIR ), Mysore

R,pr,sentin,National Institute of Communicable Diseases, Delhi

SHRJ M. P. SItAH ( AllerntJt, )DR KENCHAIAH

DR S. K. KAS.RYAP

SBRIJA8WANT SINOH KHOXBAB.

SHRI S. G. Krc.ISHNAN

DnJ. S. VERMA ( All,rnat, )SHRI S. K. MAJUMDAR

M.m66rsSRBI N. L. KALKA.

SHR1 G. C. J08KI ( Alternat, )DR R. L. KALRA Punjab AgricuturaJ University, Ludhiana

DR R. P. CHAWLA ( Alternate)OK KALYAN SU~TOB e.S.A. University of Agriculture & Technology,

KanpurNational Institute of Occupational Health ( ICMR ),

Ahmadabad

Rallis India Limited, Bombay

I n personal capacity [ Prof of Em;,."", (Rltd) ,ARF,New Dell.. J

National Malaria Eradication Programme, Delhi

SHRI N. MUTHU ( Alumat» )SUItt B. P. S. MANN Pesticides Associat ion of India, New Delhi

DR B. S. 8HETorv ( Alternate I )8HRI T. V. JAGADISAN ( Alternate II )

SHRI K. S. MEHT.o\ Bharat Pulverising ~1i1Js Private Limited, BombaySHRY S. CK ATT)~RJEE ( Alterllate )

Dn A. L. MOOKElC.JEJo-: Cynamid India Limited, BombayDn A. P. SHI~THE (Alttrnat')

DR S. K. MUKERJI

SHIn NAWAB SIN(;n

Cn Kar'hiNA R .'0 ( Alt,rna', )Sanr Y. A. PItADH.\N

SHJU M. L. SHA II ( Alterntlt. )Dn P. S. RA)fAN.\1'HAN Gharda Chemicals Private Limited, Thane

DR A. M. MALTE ( AII,rnat, I )SHRI D. G. UDAS ( AltnntJt, II )

na N. K. Roy Agricultural Chemicals Division, Indian Alricultu-ral Research Institute ( ICAR ), New Delhi

SUBI H. V. RUPAREL Gujarat Insecti("idt:1 Limited, AnkleshwarDRJ. K. ASTIX ( Alt,r".")

~aBI P. K. RAO Ministry of Defence ( OnI )SHRt P. N. AOA,1tWAL ( Alima"', )

SBCRETARY ( CIa It RC ) Central Insecticides Cell. Dkectorate of Plant Pro-tection, Quarantine & Storale (Ministry ofAgriculture & Rural Development ), Faridabad

Saar V. C. BRA_O••• ( All,,,,.,, I )DB SBABTI SARV. ( All"",," II )

Da K. D. SBARKA. Directorate General of Tecbnical Development,New Didhi

SRRI N. R.. NARAYANAN ( AlImuJII)Ssal V . C. SHAlI.A. Department of Agriculture. Government of

Rajasthan, JaipurDR K. N. SBRIVA8TAVA Shaw Wallace Company Limited, Calcutta

SaRI R. N. ROY'CJlOWDJIt1BY ( Aim"'''' )( CMI.",tl ... JIt'" 7 )

2

AMENDMENT NO. 1 MARCil 1992

TOIS 12016: 1987 SPECIFICATION FOR CVPERMETIIRIN

EC

( PQge 4, clause %.1.1 ) - Substitute the following for the existing clause:

'%.1.1 10 percent EC shall be manufactured front cypermethrin, technicalconcentrate conforming to Grades 1 and 2 of IS 12017 : 1987· or fromcypermetbrin, technical conforming to IS 1201S : 1987 t . 2S percent EC shall bemanur.aClU~ from cypermethrin, technical concentrate conforming to Grade 2 ofIS 12017 : 1987· or from cypermetbrin, technical conforming 10 IS 12015 :t981t .'

(FAD 1)

Printed at Pnntngr8('h. NewDeihl.Ph ~ 7~C.l8~7

AMENDMENT NO. 2 JULY 1994TO

IS 12016: 1987 SPECIFICATION FORCYPERMETHRIN EC

(Page 4, clause 2.Z..5 ) - Delete.

(Page 6, clause 4.1 ) - Substitute the following for the existing:

'Wben freshly manufactured material in bulk quantity is offered for inspection,representative samples of tbe material shall he drawn and tested as prescribed inIS 10627 : 1983 within 90 days of its manufacture, When the material is offeredfor inspection after 90 days of its manufacture, sampling shall be done asprescribed in IS 10627 : 1983. However, the criteria for conformity of tbemateriel when tested, shall be the limits of tolerances, as applicable over thedeclared nominal value and given under clause 2.3.1 of the standard.'

(FAD 1)

Printea. at Printograph. New Delhi (INDIA).

AMENDMENT NO. 3 JUNE 1997TO

IS 12016: 1987 SPECIFICATION FORCYPERMETHRIN EC

( Page 4, clause %.1.1 ( see also Amendment No.1) ] - Substitute tbefollowing forthe existing clause:

'2.1.1 Cypermethrin EC sball be manufactured from cypennetbrin tecnmcalconcentrateand/orcypennetbrin technical conforming to IS 12017 : 1987* andIS 12015: 1987t respectively.'

(Page 4, clause 1.1.3) - Substitute 'IS 1448 ( P : 20 ) : 1982§' for'IS: 1448(P: 20) -19601'.

( Page 4, footnote marked 'f') - Insert '( first ,evision )' at tbe end of tbetitle.

(Page 5, clause3.1 ) - Substitute 'IS 8190 (Part 2) : 1988t' for 'IS: 8190( Part 2 ) - 1980t'.

, ( Page S, footnote marked 't') - Substitute .( s«oNl revision )' for(first revision)'.

( Page 6, clause 5.%) - Substitute 'IS 1070 : 1992t' for 'IS: 1070 ­1977t'.

( Page 6, footnote marked 't' ) - Substitute 'Reagent erade Wiler ( thirdrevisio« )'for the existing title.

(FAD 1)

Printed at Printograph, New Delhi, Ph : 5726847

AMENDMENT NO.4 OCTOBER 2003TO

IS 12016: 1987 SPECIFICATION J4'ORCYPERMETHRIN EC

•( Page 5, clause 2.3.2, line 1 ) - Substitute '13.5 of IS 6940 . 1982 • fo)·11.3 of IS : 6940 - 1982*'.

(FAD 1)Reprography Umt,BIS.NewDeihl. India

IS I 12016 • 1917

Indian StandardSPECIFICATION FORCYPERMETHRIN EC

o. FOR E W 0 R D

0.1 This Indian Standard was adopted by the Bureau of IndianStandards on 30 June 1987t after the draft finalized by the Pest ControlSectional Committee had been approved by the Agricultural and FoodProducts Division Council and the Chemical Division Council.

0.2 Cypermethrin Ee is used as an insecticide.

0.3 Cypermethrin Ee are generally manufactured to contain 10 or 25percent ( m/m ) of cypermethrin.

0.4 In the preparation of this standard, due consideration has been givento the provisions of the I".rtttieidts Act, 1968 and the Rules framed there­under. However, this Itandard is subject to the restrictions imposedunder the Act and Rules, wherever applicable.

0.5 For the purpose of deciding whether a particular requirement of thisstandard is complied with, the final value, observed or calculated, express­ing the result of a test or analysis, shall be rounded off in accordancewith IS : 2-1960·. The number of significant places retained in therounded off value should be the same as that of the specified value inthis standard.

1. SCOPE

1.1 Thls standard prescribes the rvquirements, and the methods ofsampling and test for cypermethrin EC.

2. REQ,UlREMENTS

2.1 COD.cltaea•• - The material shall consist of cypermethrin dissolvedin suitable solvent( s ) together with emulsifying agent( s) and with Or

without Itabilizer( s ).

eRule. Cor roundinl off numerical valu. ( ,1fIis1tl ).

s

IS : 12016 • 1987

2.1.1 10 percent Ee shall be manufactured from material conformingto Grade 1 of IS : 12017-1987-. 25 percent EC shall be manufacturedfrom material conforming to Grade 2 of IS: 12017-1987* or frommaterial conforming to IS : 12015-1987t.

2.2 Pby.ical- The material shall comply with the physical requirementsspecified in 2.2.1 to 2.2.4.

2.2.1 Description -:- The material shall he homogenous and stableliquid. Sediment and/or suspended matter shall be negligible. Ondilurion with water. it shall readily form an emulsion suitable for spray,

2.2.2 Cold Test - No turbidity or separation of solid or oily matter orboth shall occur when the material is subjected to the cold test at 10°0as prescribed in 13.1 of IS : 6940-1982: or at any other lower tempera­ture as agreed to between the purchaser and the supplier. Introductionof a seeding crystal is not necessary for the test.

2.2.3 Flash Point ( Abel) - When determined by the method prescribedin IS : 1448 [ P : 20 ]-1960§, the flash point of the material shall beabove 24-5°C.

2.2.4 Emulsion Stability - Any separation includ .. t& creaming at the top'and sedimentation at the bottom of 100 ml of emulsion prepared instandard hard water with 2'0 ml of Ee for agricultural use, shall notexceed 2'0 ml when tested by the method prescribed in 13.3 of IS : 6940­1982~_

2.2.5 Heat Stability - After treating in accordance with the methodpreset ibed in 13.4 of IS : 6940-1982t, the material shall comply with therequirements specified in 2.2.1 to 2.2.4 and 2.3.1_

NO'TJ'~ -- The material ner-d not be put to heat treatmeatvif it has crossed half ofits ~}lt'lf·1ire as declared on the container.

2.3 Chemical -- The material shall comply with the chemicalrequirements specified in 2.3.1 and 2.3.2.

2.3.1 C)lpermethrin Content - When determined by the method prescribedin A-lor A·2 of IS : 12015-1987t, the observed cypermethrin

*Sp.,cification (or cyperrnethrin, technical concentrate.tSpeclfication for cypermethr!n technical.:Methods of lest for pesticides and thp.ir formulations (first "vision ).§l\ lethods of test for petroleum and its products [P: 20] Flash point by Abel

apparatus.

4

18 I 12016 • 1••7

con,tent. percent (m/m), of any of tne samples Ihall Dot differ from thedeclared nominal value by more than the percent tolerance limits indi­cated below:

Nomi".l YGlu, P,r"ra'

Upto9

Above 9 and below 50

50 and above

T"l"ane" Pm,,.,+ 101

5 I± s )- or the nominal value+ 5 I- 3J

2.3.1.1 The actual value of cypermethrin content in the formulationsshall be calculated to the second decimal place and then rounded off tothe first decimal place before applying the tolerance. given in 2.3.1.

2.3.1.2 The average cypermethrin content of all samples taken shallDot be less than the declared nominal CODtent.

2.3.2 Acidify - When tested by the method prescribed in 11.3 ofIS : 6940-1982*, acidity (as H.SOI) shall Dot be more than 0-15 percentby masl. The material shall not be alkaline when tested by litmuspaper.

. 3. PACKING AND MARKING

3.1 The material shall be packed as per requirements given in IS : 8190( Part 2 )-1980f.

3.2 MarklDI - The container shall bear legibly and indelibly thefollowing information and any other information a8 is necessary underthe Inse'ticid" Act and Rules:

a) Name of the material;

b) Name of the manufacturer or trade-mark;

c) Batch number;

d) Date of manufacture and date of expiry;

e) Net mass of contents;

f) Nominal cypermethrin content. percent ( m/m ); and

,g) A cautionary notice as worded in 1""elieitk, Act and Rules.

• Methods of test (or pesticides and their (ormulations (firs' rmsitm ).tR.equirements Cor paciiq of pesticides: Part 2 Liquid pesticides (fir,' ,.isi•• ).

5

II • 12016 • 1987

3.3 DIS CertlfieatioD Marking

The product mayalso be marked with Standard Mark.

S.3.1 The use of tbe Standard Mark is governed by the provisioDS of tbeBureau of Indian Standards Act, 1986 and the Rules Ind Regulations madethereunder. The details of conditions under which tbe licence Cor tbe use ofStandard Mark may be granted to manufacturers or producers may"be obtainedfrom theBUrelu of Indian Standards.

4. SAMPLING

4.1 Representative samples of the material Ihall be drawn as prescribedin IS : 10627-1983*.

5. TESTS

5.1 Tests shall be carried out by the appropriate methods referred toin 2.2.2 to 2.2.5" 2.3.1 and 2.3.2.

5.2 Q,aa1Ity of a...eDt. - Unless specified otherwise, pure chemicalsand distilled water ( $'. IS : 1070-1977t ), shall be employed in tests.

NOT. - 'Pure cbemicals· shan mean chemical. that do not contain impuritieswhich affect the resulta of analysi•.

-Methods Cor sampliul·oCpeticidal CormulatiODLtSpecificadOD Cor water for leDerallaboratory UH ( __~ "";,;,,, ).

6

IS : 12016 • 1987

( C."tinu,d f,om pag, 2 )

MnnIJ"s Rep"stn/,nlSHRIj. L. SIP'HIIIALAN'I CMA Laborarorres, Bombav

SHRI A. H. KARANCHI ( AI"rnal, )DR R. SOIiAN Sudarshan Chemical Industrres Limited, Pune

SHILl K. RATHI ( ,Altmutt,)DJl R. V. VEN'KATARATNAM Regional Research Laboratorv ( csm ), Ilyderabad

DR N AO A BHUltJlAN RAO ( Alt"nat, )SHill T. PURNANANDAM, Director General, BIS ( E~-offi'IO J\I,mb,,)

Director ( Agri & Food )

St"ItQ,.1

'3HRI LAJIl\J)JoR SINGn

Joint Director ( Agn & Food ), BIS

7

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