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OAK RIDGE NATIONAL LABORATORY U. S. DEPARTMENT OF ENERGY Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*, Russell Steel**, Scott Packer** and Stan A. David* * Oak Ridge National Laboratory, Oak Ridge, TN ** MegaStir Technologies, Provo, UT April, 2005

Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

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Page 1: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Friction Stir Welding of API Grade X65 Steel Pipes

Zhili Feng*, Russell Steel**, Scott Packer** and Stan A. David*

* Oak Ridge National Laboratory, Oak Ridge, TN** MegaStir Technologies, Provo, UT

April, 2005

Page 2: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Acknowledgement

• Research was sponsored in part by the U.S. Department of Energy, Office of Energy Efficiency and Renewable Energy, Industrial Technologies Program under contact DE-AC05-00OR22725 with UT Battelle, LLC.

• Technical and financial support of MegaStir Technologies.

Page 3: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Why FSW of Pipeline Steels

• Ultra high-strength steels• Properties• Productivities?• Hydrogen issue• Weld metal property matching the base

metal

Page 4: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Material

• API 5L Grade X-65 steel− Common in oil and gas industry for pipelines− 0.08C-1.0Mn-0.235Si-0.04Al-0.016Nb− Ceq = 0.14

• ERW Line Pipe − OD: 12.75” (324 mm)− Wall thickness: 0.25” (6.35 mm)− Base metal properties per mill specification

Yield: 67 ksiUltimate tensile: 77 ksiElongation: 33%

Page 5: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Welding• Polycrystalline cubic boron nitride

(PCBN) tool− Shoulder diameter: 1”− Pin length: 0.22”

• Girth weld − Square butt joint configuration− No special groove preparation− Surface ground before welding− Single pass full penetration from

OD• Welding parameters

− 500 - 600 rpm− 4 - 6 in/min− Welding forge force: 6500 lbf

• Special run-off tab to eliminate the exit hole on the pipe

• Argon shielding gas from the tool to protect weld from oxidation

Page 6: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Field deployable FSW system

Page 7: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Hydraulic internal support/fixture

Page 8: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Welding movie

Page 9: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Finished pipe

Page 10: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Finished pipe

Page 11: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Microstructure and Mechanical Evaluation

Scale: 1:5

12x3.14=37.7” Each section: 9” long after metallography samples

9”Weld start

1” (OD weld width)

Exit tab

0° 0°270°180°90°

3 cr

oss-

wel

d te

nsile

:4”

wid

e

3 BM tensile:4” wide

9 HAZ Charpy:4.5x3”

18 WM Charpy:9x3”

(4) Metallographic samples

Face for Metallography

9 BM Charpy:5x3”

Tool rotation: CCW

Advancing Side

Retrieving Side

Scale: 1:5

12x3.14=37.7” Each section: 9” long after metallography samples

9”Weld start

1” (OD weld width)

Exit tab

0° 0°270°180°90°

3 cr

oss-

wel

d te

nsile

:4”

wid

e

3 BM tensile:4” wide

9 HAZ Charpy:4.5x3”

18 WM Charpy:9x3”

(4) Metallographic samples

Face for Metallography

9 BM Charpy:5x3”

Tool rotation: CCW

Advancing Side

Retrieving Side

Page 12: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Mechanical Testing• Tensile

− Room temperature− 3 cross-weld tensile: (1-in wide strip) API 1104− 3 Base metal at room temperature

Orientation: AxialASTM E8, rectangular flatFull stress strain curve. Yield stress at 0.2% offset plastic strain and at 0.5% total strain

• Charpy V notch: ASTM E23, 10x5x50 (sub-sized due to wall thickness) − side V-notch through thickness− 3 repeats at each temperature.− Base metal: axial orientation @ -50, 0, 20C− HAZ: @ -50, 0, 20C− Weld: @ -50, -30, -20,-10, 0, and 20C

Weld Notch

Location

HAZ Notch

Location

~ 0.3”

Page 13: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Tensile properties• Base Metal

• Cross-weld

Page 14: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Samples failed outside the weld and HAZ during cross-weld tensile test

Page 15: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Charpy V-Notch Impact Test

Page 16: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Charpy V-Notch Impact Test• ASTM E23• 10x5x50 mm, sub-sized• All samples showed 100% shear

0

20

40

60

80

100

120

140

-60 -50 -40 -30 -20 -10 0 10 20 30

Temp, C

Ener

gy, J

Weld

HAZ

Base Metal

Page 17: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Weld Cross-Section Macro

2mm

Page 18: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

The interface is not easily distinguishable under high magnification

Page 19: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Evidence of lack of bonding on the root face

• Relative small ~ 0.15 mm• Oxide layer• Did not affect the mechanical

tensile and impact properties

0.15mm

0.07mm

Page 20: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Microstructure

Base Metal

TMAZ

Stir zone

Page 21: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Cross-weld section micro-hardness profile

0 2 4 6 8 10 12 14 16 18 20 22

0

0.8

1.6

2.4

3.2

4

4.8

Postion (mm)

Posi

tion

(mm

)

160-170 170-180 180-190 190-200 200-210 210-220

50

100

150

200

250

Hv @

200

g 1/2t

1/4t

3/4t

Page 22: Friction Stir Welding of API Grade X65 Steel Pipesfsrl.byu.edu/presentations/X65 Steel Pipes.pdf ·  · 2005-06-24Friction Stir Welding of API Grade X65 Steel Pipes Zhili Feng*,

OAK RIDGE NATIONAL LABORATORYU. S. DEPARTMENT OF ENERGY

Summary

• A portable, field deployable FSW system has been developed for successful welding of X65 pipe

• Fully consolidated weld joint can be obtained in a single pass

• Welding speed• Microstructure/microhardness• The girth show superior tensile and

impact properties