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EuCARD-BOO-2011-002
European Coordination for Accelerator Research and Development
PUBLICATION
European infrastructures for R&D and testof superconducting radio-frequency
cavities and cryo-modules
Weingarten, W (CERN)
29 September 2011
The research leading to these results has received funding from the European Commissionunder the FP7 Research Infrastructures project EuCARD, grant agreement no. 227579.
This work is part of EuCARD Work Package 4: AccNet: Accelerator Science Networks.
The electronic version of this EuCARD Publication is available via the EuCARD web site<http://cern.ch/eucard> or on the CERN Document Server at the following URL :
<http://cdsweb.cern.ch/record/1386310
EuCARD-BOO-2011-002
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European Infrastructures for R&D and Test of Superconducting Radio‐Frequency Cavities and Cryo‐modules
Wolfgang Weingarten/CERN
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Contents
I. Introduction and scope ............................................................................................................2
II. SRF for accelerator application, past and present ....................................................................3
A. A brief historical review ............................................................................................................3
B. The present status ....................................................................................................................6
III. About the need for a SRF test infrastructure ...........................................................................7
A. International cooperation ‐ examples ......................................................................................9
B. Present funding schemes ........................................................................................................10
1. CERN consortia ...........................................................................................................10
2. European Union consortia (FP7 program) ................................................................10
3. National Consortia and Bilateral Funding Schemes ..................................................11
4. International schemes ...............................................................................................11
IV. Important future research topics and priorities ....................................................................12
A. Accelerating gradient...............................................................................................................12
B. RF losses ‐ Q‐value ..................................................................................................................15
C. Reproducibility of performance ..............................................................................................20
1. Quench and field emission .........................................................................................20
2. Diagnostics .................................................................................................................22
3. Measures to improve reproducibility ........................................................................22
a) Thermal conductivity ....................................................................................22
b) Thin film cavities ...........................................................................................22
D. Proposal for future R&D work ................................................................................................23
1. Niobium .....................................................................................................................24
2. Alternate materials ....................................................................................................26
V. Capacity and availability needs related to emerging European projects ................................27
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A. Logistical needs .......................................................................................................................28
B. Needs for R&D initiatives ........................................................................................................29
VI. Conclusions .............................................................................................................................30
VII. Glossary ..................................................................................................................................32
Acknowledgments ...............................................................................................................................34
ANNEX
SRF related specific equipment available in European Accelerator Laboratories ...............................35
Table 1: General purpose manufacture/workshop tools ........................................................35
Table 2: Specific manufacture/assembly facilities and inspection/testing tools ....................36
Table 3: Surface treatment/coating/final cleaning .................................................................38
Table 4: Warm test places ‐ high power coupler ....................................................................40
Table 5: Cold test places ‐ low power .....................................................................................41
Table 6: Cold test places ‐ high power ....................................................................................43
Table 7: Sample characterisation and other test/inspection equipment ...............................45
Specific SRF related equipment available elsewhere ..........................................................................48
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I. Introduction and scope
The need for a European facility to build and test superconducting RF accelerating structures and cryo‐modules (SRF test facility) was extensively discussed during the preparation of EuCARD1,2. It comprised a distributed network of equipment across Europe to be assessed and, if needed, completed by hardware. It also addressed the quest for a deeper basic understanding, a better control and optimisation of the manufacture of superconducting RF structures with the aim of a substantial improvement of the accelerating gradient, a reduction of its spread and a cost minimisation. However, consequent to EU budget restrictions, the proposal was not maintained. Instead, a more detailed analysis was requested by a sub‐task inside the EuCARD Network3 AccNet ‐ RFTech4.
The main objective of this “SRF sub‐task” consists of intensifying a collaborative effort between European accelerator labs. The aim focused on planning and later identifying for European accelerator users a multi‐purpose state‐of‐the‐art network of equipment for R&D and testing of SRF cavities and cryo‐modules. The duration of this sub‐task was agreed to be two years, after which the results were to be presented to the funding agencies. This shall be achieved by this report.
This report is inevitably biased by the author’s opinion and preconceptions although a balanced assessment was aimed at. It summarizes the discussions held with individuals and during specific workshops or conferences organized in 2009 ‐ 2011 under the auspices of RFTech5 and other EuCARD annual meetings6. It shall answer the following questions:
1. Is there a need for a SRF test infrastructure, distributed across, and managed by, European accelerator labs?
2. What research topics are important for the future of SRF technology and what priorities should be attributed to them?
1 https://eucard.web.cern.ch/EuCARD/index.html 2 http://esgard‐omia.web.cern.ch/ESGARD‐OMIA/Programme.html 3 https://eucard.web.cern.ch/EuCARD/activities/networks/WP4/ 4 http://accnet.web.cern.ch/accnet/RFTech/ 5 http://accnet.web.cern.ch/accnet/Activity_Reports/2009/RFTech_SRF_videoconference.pdf https://indico.desy.de/conferenceDisplay.py?confId=2831 http://lpsc.in2p3.fr/Indico/conferenceDisplay.py?confId=530 http://indico.cern.ch/conferenceDisplay.py?confId=118190 6 https://indico.cern.ch/internalPage.py?pageId=7&confId=115634 http://indico.cern.ch/conferenceDisplay.py?confId=118190
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3. Is the capacity and available equipment sufficient to cope with the demands of emerging European projects?
II. SRF for accelerator application, past and present
A. A brief historical review
When defining a program, “road map”, or strategy for the future, it is good advice to look into the past. A short summary of milestones in the development of RF Superconductivity (SRF) for accelerator applications shall serve as a guideline for future initiatives, to be proposed in this report.
RF studies on superconducting materials had already been performed many years before the BCS theory laid the ground for understanding superconductivity, which happened in 1957. Only one year later this theory was extended from DC to RF. Investigations on superconducting cavities were mainly conducted inside an academic environment to test the new theories.
The reputation of SRF in the accelerator community was dubious in the late 1960s. This was mainly because the accelerating gradients obtained were relatively small (several MV/m) and, even worse, the physical limitations were not identified. However, the high energy physics community needed more efficient and power saving accelerating systems compared to what was available at that time. The reason was that important discoveries were made at SLAC on the substructure of the proton, by hitting it with electron beams accelerated in a conventional way in pulsed mode driven copper structures. These discoveries, later decorated with the Nobel Prize, opened up the quest for higher energies and luminosities in order to resolve even more subtle structures inside the proton. Electron positron colliders entered the high energy physics field that were operated in continuous wave mode. It happened that at the same time, at the end of the 1960s, encouraging performances of small size sc cavities were obtained in several research labs by applying new techniques, such as electro‐polishing (EP) and UHV firing. The excellent results inspired sufficient confidence in the potential of SRF technology, because higher accelerating gradients than in conventional copper accelerating structures now became accessible, and ‐ even better ‐ in continuous wave mode. This hope made coincidence experiments possible with sufficient statistics.
At that time universities with high energy physics research interests joined in the efforts of understanding SRF. The number of research institutes participating in SRF developments increased significantly. The academic interest became so high that the “Workshop on RF Superconductivity” was founded (1980). It is still alive today and is organized now as the SRF
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Conference with biannual periodicity. New materials were studied for SRF accelerator application (Nb3Sn) in the 1970s. New powerful diagnostics methods were developed and industrialized, very often in fruitful collaborations between universities and accelerator centres. Also by trial and error, but very soon by rigorous research work, various limitations of SRF cavity performance were identified and cured, one after the other.
These early successes opened up an enthusiastic effort for continuously increasing applications for accelerator projects. In parallel, progress in computer codes both to solve either the relatively complicated theoretical expressions for RF superconductivity and to solve the electromagnetic fields inside cavities allowed careful and judicious design work. In the mid 1970s proposals were made to build very high energy electron‐positron colliders, with SRF accelerating systems as a serious option (LEP and the electron ring of HERA). It took another 20 years of R&D and industrialisation efforts before such a large electron positron collider such as LEP became a reality and still a few years more before LEP reached its maximum energy (209 GeV) by means of the upgrade with sc cavities.
The actual situation is as such: Starting from relatively small scale applications and pilot installations for nuclear physics (e‐linacs, sc microtron) and heavy ion physics, sc cavities of steadily increasing varieties are now operated successfully in many research areas. They stretch from nuclear physics and particle physics, to light sources for material sciences. The sc cavities are used in accelerators, such as electron linacs, equipped sometimes with re‐circulating arcs to increase efficiency. These accelerating systems for electrons are upgraded to FELs, e+e‐ storage rings and sometimes transformed into B‐factories and light sources. Proton‐proton storage rings equipped with a sc accelerating system explore the energy frontier such as the LHC. Proton linacs with a sc acceleration system serve for multi‐purpose applications, such as neutron sources, accelerating heavy ions and radioactive beams, etc. Superconducting cavities are also applied for steering or shaping the particle bunches (crab and 3rd harmonics cavities).
The history of SRF may be divided into two periods. During the first one, roughly between 1965 and 1985, universities played an important role in scientific innovations that happened in the R&D phase of SRF for accelerator application. During the second period, as of 1985 up until now, the pursuit of large scale accelerator technology and engineering was mostly done in research centres. The large scale series of components was mainly manufactured in close collaboration between industry and research centres.
The participation of universities was crucial in the first phase for guaranteeing a successful start. Innovations were often initiated at universities. They required limited resources and met academic standards. The role of universities faded, because the innovations gradually moved from existence proofs of excellently performing cavities, new materials, diagnostic tools or new treatments and techniques, towards prototyping as well as reliability and series
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production issues. In short, R&D for sc accelerators switched from research to technology and engineering. This shift required larger resources that could no longer be burdened to universities and required extensive engineering know‐how.
A key issue was the early implication of industry during this second phase. Industry responded positively towards niobium material improvement, pre‐series production of cryo‐modules, and rationalisation of the production chain to achieve cost effectiveness. Industry accomplished remarkably well the transfer of know‐how acquired at research centres. These achievements culminated in the successful pilot tests and continuous operation of SRF cavities in accelerators, owing to the close collaboration between research centres and companies.
The increasing use and acquisition of operational experience obtained in the accelerator centres with niobium sc cavities led to research and development to fully exploit the niobium technology with even larger accelerator projects in focus. The efforts were successful and paid off in a steady improvement of performance of niobium cavities up to close to the theoretical limits, at least in individual cavities (Fig. 1). It should be kept in mind, nonetheless, that it took about 40 years until the theoretical performance limit for niobium cavities was demonstrated.
Figure 1: Progress of field gradient with single cell cavities7.
7 A. Yamamoto, Superconducting RF cavity development for the International Linear Collider, ASC 2008.
The arrow indicates the approximate position of the theoretical ceiling in accelerating gradient
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Superconductors other than niobium were also studied during the first phase of research and development but did not cope with the requirements for low loss cavities for accelerators at a reasonable gradient. Copper cavities coated with a thin niobium layer on the inside were an exception. They could occupy a “niche”, for reasons of economy and stability against quenches, after a vigorous research programme had been successfully concluded. This “niche” concerned collider rings such as LEP, mainly for cost reasons, and involved a huge number of sc cavities. It also concerned the much smaller RF system of the LHC, mainly for reliability and beam stability issues. The reason is that collider rings have their cost optimum at moderate accelerating gradients, about 10 MV/m, because the RF system is periodically re‐used by the circulating beams and not only once as in a sc linac. This number depends of course on the individual accelerator and its design parameters such as the manufacturing costs per meter of structure, cryogenic cooling needs and RF power requirements. Niobium coated cavities are also applied, for various reasons, in heavy ion accelerators and are foreseen for upgrade, such as HIE Isolde at CERN.
B. The present status
The present status of SRF for accelerator application can be described as follows:
On the one hand, spectacular technological progress was achieved. Technical work is actively pushed, even worldwide, in a collaborative effort. Large SRF test infrastructures and synergies between laboratories were created. Many sources of financing render this effort possible. The biggest contribution evidently concerns approved projects, such as XFEL and ESS. Other sources such as the EU Framework Programs contribute significantly to the pursuit of other studies and smaller projects. Industry is well integrated in the SRF activity and deserves credit for improvement of the niobium sheets many years ago as well as for providing the lion’s share of SRF components for existing and recent projects. Consequently, large projects such as XFEL are being constructed by an international effort. The preparation for more far reaching projects such as ILC is continuously and successfully progressing as well. Other ongoing R&D activities are pursued, in particular linked to
• proton drivers (ADS, SPL study @ CERN, ESS) to construct pilot cryo‐modules,
• heavy ion accelerators (e.g. HIE ISOLDE with improved niobium coating methods) to reduce costs by simplifying the design and to avoid quench limitation,
• LHC upgrade (e.g. with crab cavities) to increase luminosity,
• Energy Recovery Linacs (ERL) to save electrical grid power at very large beam power,
as well as many others.
These studies or projects are concentrated around accelerator research centres but with less technical and theoretical impact from research work done at universities, as it was in the past. However, links to universities are not neglected, recruitment being an example.
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University alumni with a Bachelor degree as well as technical and doctoral students receive supplementary qualifications in the research centres themselves, financed by them, national funding agencies or the EU.
On the other hand, progress is often slow, due to the pressure of projects and their future users, and sometimes owing to trial and error. The theoretical understanding of the underlying physics does not always keep track with the technological progress. Problems of reproducibility of performance remain and require even stronger quality control at all stages of the manufacturing process. Decisions on any new high energy sc accelerator are on halt as long as results from the LHC experiments are lacking. Large world‐wide project proposals rely on the niobium technology. For good reasons the most reliable technology was therefore chosen. In particular, the technology of bulk niobium made large progress over the last 20 years. At present the niobium technology is the only choice for an accelerator project to be finished within specification, cost and time. Whether to choose niobium as a thin film or in bulk form depends on the specific application, e.g. the required accelerating gradient. There is hope that superconductors other than niobium offer more potential for future SRF projects. But no vigorous and financially well outfitted R&D program is in sight that goes beyond the niobium technology.
Therefore, the risk of stalemate of the SRF technology is real. To avoid the sc technology from being stalled, new R&D efforts are required to keep track and guide the technological advance, as was done in the past. Another unwelcome constraint is the increase of material cost for niobium, the only technical material in use for SRF. The cost of niobium increased considerably as it did for any other raw material. It nearly doubled within four years (520 €/kg in 2010).
In what follows, the three questions as mentioned in chapter II shall be addressed in the light of the long lead times required to go beyond the present technology based on niobium alone. This approach shall demonstrate that there is no fundamental reason to assume that the SRF technology is at its technological and theoretical limit.
III. About the need for a SRF test infrastructure
A. International cooperation - examples
The SRF community is relatively small and its members are well known among each other. If needed, mutual arrangements were and are taken individually between labs, even at a trans‐national or trans‐continental level, with focus on a specific project of common interest. The approach chosen is typical for “bottom‐up”. Examples are numerous and shall not be listed here, except for a few:
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• A Karlsruhe manufactured prototype sc cavity intended for electron positron storage rings such as PETRA and LEP was tested in the PETRA collider; the first beam test of a CERN manufactured sc cavity was arranged in collaboration with DESY and performed at PETRA as well.
• The SNS cavities were designed, manufactured and tested at JLAB.
• A 200 MHz mono‐cell copper cavity designated for a muon collider was manufactured and coated with a thin niobium film at CERN and tested in a wide vertical cryostat at Cornell, the only one available with the required size.
• The Beijing BEBC‐II storage ring was equipped with cryo‐modules from KEK.
• The ESS has taken collaboration arrangements for prototyping with many European accelerator labs having expertise in SRF.
There are many other collaborative efforts. The community is organized world‐wide, exchanges information efficiently, and practices fruitful collaborations, whenever it is needed. Periodic conferences/collaborations play a prominent role and complement each other, such as the biannual SRF conference8 and the International TESLA Technology Collaboration TTC9. Recently the international workshop on “Thin Films and new ideas on RF superconductivity” 10 joined these gatherings. TTC inherited its naming from an effort that started with a workshop in 1990 at Cornell University on TeV Electron Superconducting Linear Accelerator (TESLA) technology11. Meanwhile it covers many more technological fields in SRF than the naming indicates. Proton and heavy ion accelerators were included recently, because the technologies are similar to “TESLA technology” based accelerators. In summary, the international cooperation in SRF is extremely vigorous and fruitful.
B. Present funding schemes
The SRF community is well integrated in supra‐national integrative attempts which are also providing resources.
There are cross links to other institutes and funding schemes such as the following.
1. CERN consortia
• SPL study: CEA, CNRS, BNL, German Universities, ESS …
8 http://conferences.fnal.gov/srf2011/ 9 http://agenda.infn.it/conferenceDisplay.py?confId=3087 10 http://www.surfacetreatments.it/thinfilms/ 11 http://tesla‐new.desy.de/
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2. European Union consortia (FP7 program)
• CARE12 (JRA, precursor of EuCARD, mainly Work Package SRF)
• EuCARD1 (JRA, mainly Work Package 10, Superconducting RF technology for proton accelerators and electron linear accelerators)
• SLHC‐PP13
• ILC‐HiGrade14
• TIARA15
• CRISP (currently approved by EU and being launched)
• HL‐LHC (all under the auspices of ESGARD)
3. National Consortia and Bilateral Funding Schemes
• Special contribution of France to CERN
• Physics at the Terascale Initiative (D)16
• BMBF (D) Initiative (22 Oct 2008): TEMF Darmstadt, University Rostock, TUD, BUW …17 and more recent ones
4. International schemes
• The U.S. LHC Accelerator Research Program (LARP) consisting of four US laboratories, BNL, FNAL, LBNL, and SLAC, who collaborate with CERN on the Large Hadron Collider18
In conclusion, there exists de facto a distributed network of infrastructures for R&D and test of sc cavities and cryo‐modules, which is alive. So the need for a new network is certainly not a top priority. However the specific equipment available in the various accelerator centres is rapidly changing. Therefore a compact and rather detailed list of equipment is helpful to gain an updated overview and to asses whether the available equipment matches the projects and R&D work to come well. Therefore, in various discussions, the wish was uttered to list that equipment required for SRF, and, if needed, to propose completion of specific items. The available equipment related to SRF is therefore summarized in the Annex.
12 http://esgard.lal.in2p3.fr/Project/Activities/Current/ 13 http://info‐slhc‐pp.web.cern.ch/info‐SLHC‐PP/ 14 http://www.ilc‐higrade.eu/ 15 http://www.eu‐tiara.eu/ The main objective of TIARA (Test Infrastructure and Accelerator Research Area) is the integration of national and international accelerator R&D infrastructures into a single distributed European accelerator R&D facility. 16 http://www.terascale.de/ 17 http://www.bmbf.de/foerderungen/13099.php 18 http://www.uslarp.org/#
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IV. Important future research topics and priorities
A. Accelerating gradient
All SRF applications for accelerator projects are based on the metal niobium19. There is a good reason for that: niobium has the largest critical temperature Tc among all elements, is relatively ductile and commercially available in large quantities and different shapes.
However, niobium technology touches its predicted theoretical limits. Recent pulsed RF tests on a niobium cavity allowed raising of the accelerating gradient without being impeded by a quench (Fig. 2, top). This test confirmed a long‐standing conjecture, namely that the surface magnetic field determines the ultimate limit of the accelerating gradient. Its maximum is given by the superheating critical field Bsh, proportional to the thermodynamic critical field Bc and close to it by a factor depending on the purity of the niobium. This limitation is confirmed by recent tests on niobium samples with a specially designed device (quadrupole resonator): for niobium Bc = at 190 mT, and Bsh = 230 mT (Fig. 2, bottom). This device also allows evaluating the RF losses of sc samples.
In real accelerating cavities the maximum magnetic field obtained touches the theoretical limit as well. Depending on the shape of the cavity this ultimate maximum magnetic field Bsh corresponds to about 56 MV/m accelerating gradient in non shape‐optimized elliptical cavities. Measurements on single cell cavities result in values close to that number.
19 except some early developments of lead plated copper cavities of relatively complicated shape, envisaged for heavy ion accelerators, and recently as cathode material for SRF electron guns because of its improved quantum efficiency
13
Figure 2: Maximum surface magnetic field under RF exposure vs temperature for niobium cavity (top) and niobium sample (bottom) exceeding the thermodynamical critical field (Bc = 190 mT) by
about 20 %20, 21.
20 N. R. A. Valles and M. U. Liepe, Temperature dependence of the superheating field in niobium, http://arxiv.org/abs/1002.3182v1 21 Courtesy T. Junginger/CERN
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Figure 3: Q‐factor vs. accelerating gradient for a shape‐optimized mono‐cell niobium cavity (insert) from KEK ‐ Cornell collaboration22
Fig. 3 depicts the Q‐factor vs. accelerating gradient for a shape‐optimized mono‐cell niobium cavity which obtained 59 MV/m maximum gradient, 125 MV/m peak surface electric field and 206.5 mT peak surface magnetic field. The gradient was limited by a quench.
Two approaches may offer a solution to overcome this limitation in gradient. The first consists of choosing another material. As the superheating critical field Bsh is proportional to the thermodynamic critical field Bc, any metal with a larger Bc than niobium would be adequate, e.g. Nb3Sn of NbN (Table 1).
22 R.L. Geng , G.V. Eremeev, H. Padamsee, V.D. Shemelin, High gradient studies for ILC with single‐cell re‐entrant shape and elliptical shape cavities made of fine‐grain and large‐grain niobium, Proceedings of PAC07, Albuquerque, New Mexico, USA, p. 2337.
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Table 1: Possible materials for SRF application
Material Tc [K] Bc [T] Bc1 [T] Bc2 [T]Pb 7.2 0.08 n/a n/a Nb 9.2 0.2 0.17 0.4
Nb3Sn 18 0.54 0.05 30 NbN 16.2 0.23 0.02 15 MgB2 40 0.43 0.03 3.5 YBCO 93 1.4 0.01 100
The second approach proposed is based on one or several thin sc film ‐ insulator sandwiches on top of a bulk niobium substrate. The underlying idea consists in increasing the critical magnetic field of the uppermost layers by making them sufficiently thin and to rely on the exponential decay of the magnetic field with depth. The rational ground is the well known fact that the critical magnetic field of thin films is larger than for bulk because the shielding surface currents in the film are not yet fully developed; hence these currents cost less energy to develop than for bulk and can therefore exceed the maximum bulk surface currents. As they are proportional to the magnetic field, the bulk critical magnetic field is exceeded considerably, and by more the thinner the film is. The magnetic field inside the sandwich structure is becoming smaller and smaller going from one sandwich to the next deeper one. It must be guaranteed as a necessary condition that the remaining magnetic field at the interface to the bulk niobium substrate is below the superheating critical field there. The surface magnetic field at the uppermost surface can therefore be much larger than the superheating critical magnetic field of the bulk23.
This conjecture is certainly worth being tested. A first approach would consist in preparing a sandwiched sample for RF evaluation in a suitable host cavity (e.g. quadrupole resonator or TE011 cavity). Sample tests are convenient, or even mandatory, to fully characterize the superconducting properties on identical surfaces, both for RF and DC, before preparing real accelerating structures.
B. RF losses - Q-value
Large and costly projects such as a linear colliders with TeV beam energy require very large accelerating gradients. The simple reason is that the investment costs scale approximately with the length of the device, which, for constant beam energy, goes down inversely proportionally with the accelerating gradient. Large accelerating gradients are not for free and they are reflected in the operation costs. Increasing the accelerating gradient must be accompanied by a substantial reduction of the RF dissipation, which goes up with the square
23 A. Gurevich, Enhancement of RF breakdown of superconductors by multilayer coating, Appl. Phys. Lett. 88 (2006) 012511.
16
of the gradient. An accelerating gradient of twice the design gradient for a linear collider application such as the ILC, under preservation of the overall RF dissipation and beam energy (i.e. cutting in half its length), would require doubling the Q‐value. An accelerating gradient of, say 100 MV/m, for a linear collider application such as the ILC, under preservation of the overall RF dissipation and its total length, would require a targeted Q‐value of 8·1010. The SRF technology would allow for such a number, because, on theoretical grounds, the maximum accelerating gradient (or magnetic surface field) is correlated with the critical temperature and consequently with a small RF dissipation (large Q‐value) (Fig. 4). The reason is that the critical temperature is proportional to the energy gap, and, from the BCS theory, the RF losses decrease exponentially with the energy gap.
Fig. 4: Critical magnetic field versus critical temperature of selected elemental superconductors24
Also for relatively moderate beam energies, a large Q‐value is mandatory in order to avoid causing problems by a cavity that might have degraded and not having sufficient reserve available in cooling power.
Indeed, such large Q‐values can be achieved in bulk niobium cavities. Q‐values exceeding 1011 were obtained in individual cavities up to accelerating gradients of more than 25 MV/m (Fig. 5).
24 http://hyperphysics.phy‐astr.gsu.edu/hbase/solids/scbc.html#c2
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Figure 5: Q‐value vs. acc. gradient; Q > 2·1011 corresponds to a residual resistance < 0.5 nΩ25
For the same reasons, other materials with a critical temperature Tc larger than that of niobium would offer even more potential, because they should allow for even smaller RF losses. This explains the attractiveness of classical high‐Tc superconductors, such as NbN and Nb3Sn.
Remarkably, for thin films of these classical high Tc, and also for niobium thin films, similar or even larger Q‐values than for bulk niobium were obtained. These include thin niobium film on copper substrate cavities and thin Nb3Sn or NbTiN film on niobium substrate cavities (Figs. 6 ‐ 8). However, the large Q‐values of these thin film cavities could not be preserved up to large accelerating gradients. They show a more pronounced decrease of the Q‐value with the accelerating gradient than bulk niobium cavities (Q‐slope). But it should be kept in mind that since these early efforts (late 1980s) the efforts invested into niobium cavities exceeded by far those for thin film cavities. This fact is another illustration why the most reliable technology was preferred to that with the largest potential.
25 H. Safa, High field behaviour of superconducting cavities, 10th Workshop RF Superconductivity, Tsukuba (Japan) 2001.
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Figure 6: Q(Ea) curves of the very first 352 MHz LEP niobium thin film cavities, manufacture in the late 1980s (curves 1 and 2) (left); Q(Ea) curves for a 500 MHz single‐cell NbTiN thin film cavity; upper
curve, measurements taken at 2.6 K, lower curve, measurmeents taken at 4.2 K (right)26.
An essential by‐product is that these “classical” high Tc superconductors would also allow operation at 4.2 K instead of 2 K for sufficiently large RF frequencies; say beyond about 700 MHz (Fig. 8).
Figure 7: Q‐value vs. accelerating gradient curve of a typical high performance niobium cavity showing indicators of field dependent surface resistance (intermediate Q‐slope and Q‐drop)27.
26 C. Benvenuti, D. Bloess, E. Chiaveri, N. Hilleret, M. Minestrini and W. Weingarten, Proc. 4th Workshop RF Superconductivity 1989, KEK, Tsukuba (Japan), p. 869. 27 L. Lilje et al., Nucl. Instr. Meth. A 524 (2004) 1.
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The physical reason for the Q‐slope is presently under investigation in several laboratories. Several models were proposed to explain this observation, but a breakthrough in understanding is still pending. A most probable explanation is flux entry into the surface, preferentially at oxides or other non‐stoichiometric areas (nucleation centres) and its growth inside the superficial oxide layer under the action of the RF magnetic field.
Figure 8: Electric peak field dependence of Q‐value of a single‐cell 1.5 GHz cavity as measured before (Nb) and after Nb3Sn coating at 2 and 4.2 K. The electrical peak field of 27 MV/m corresponds to an
accelerating gradient of 12 MV/m28.
Fig. 9 presents a phase diagram for Nb3Sn, the material that was tested for accelerator application with the results as shown in Fig. 8. Only one individual phase is the correct one for SRF application. To prepare the correct one and suppress all other unwanted phases is a challenging task and might explain the results obtained so far as being inferior to bulk niobium at large accelerating gradients.
28 G. Müller, P. Kneisel, D. Mansen, H. Piel, J. Pouryamout, and R.W. Röth , Proc. of the 5th EPAC, London, p. 2085 (1996).
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Figure 9: Phase diagram of Nb and Sn showing many phases apart from the useful phase for SRF (Nb3Sn)29.
C. Reproducibility of performance
In spite of the remarkable successes in the performance of bulk niobium cavities in terms of accelerating gradient and Q‐value, as described before, issues such as the reproducibility of that performance in real accelerator cavities with many cells and in assembled cryo‐modules with many cavities remain challenging. The term “reproducibility” is understood as the variation of performance after application of an identical cavity treatment protocol. The scatter of performance proves that apart from the deterministic performance factors, such as temperature, frequency, magnetic field etc., there are others of stochastic nature, not strictly under control of the experimenter.
1. Quench and field emission
Reproducibility is at stake for several reasons. Whereas the average gradient doubled from about 15 MV/m to about 30 MV/m within the last decade, the relative scatter of the gradient remained about the same. The breakdown mechanism also remained unchanged.
29 A. Godeke, A review of the properties of Nb3Sn and their variation with A15 composition, morphology and strain state, Supercond. Sci. Technol. 19 (2006) R68–R80.
21
The niobium cavities are in nearly all cases limited by a quench or by field emission. One flawed site on the surface is sufficient to limit the gradient of the cavity.
A quench is usually provoked by excessive local heat dissipation at a normal conducting defect under the action of a large magnetic surface field. As soon as the temperature in its vicinity comes close to the critical temperature Tc (at the magnetic surface field Bc) a temperature run‐away forces the circumjacent niobium normal conducting. The consequence is a periodic or single‐event instability, depending on the RF power available, leading to large RF dissipation.
Field emission is caused by a large electric surface field. The detrimental action of the mechanism of field emission consists in drawing energy out of the electromagnetic field of the cavity and loading it as kinetic energy to the cavity wall. In addition, equally bad, field emission aggravates exponentially with the accelerating gradient.
Field emission occurs at high gradients, however far below the theoretical predictions for ideal surfaces. Hence the process of field emission is more complex than treated in theory. Diagnostics on sc cavities accompanied by computer simulations and DC sample tests with a field emission microscope identified the field emitters as “dust” particles of various compositions. Since clean working practice was adopted from the vast experience accumulated in the semiconductor industry, the failure of sc cavities rate by field emission has considerably decreased.
Both effects are a nuisance for a reliable cavity operation, but one must keep in mind that they do not pose a fundamental limit. The ultimate limit in gradient was achieved in individual cavities without a quench, and a surface electric field as large as 1 GV/m was obtained locally on small niobium samples without field emission30.
Another reason affecting the reproducibility is the size of the superconducting surface. As even one single emitter or defect may degrade the performance of the cavity, it is clear the more cells a cavity has or the lower the frequency is the higher is the probability of a limitation of the gradient by either a field emitter or a defect.
As an illustration, about four decades R&D efforts passed until obtaining the theoretical limit of the niobium SRF technology in individual cavities ‐ more time will pass before we can obtain reproducible results in real accelerating structures.
30 A. Dangwal et al., Proceedings of SRF2007, Peking Univ., Beijing, China.
22
2. Diagnostics
The location of the quench or of a field emitting site can in principle be identified by suitable diagnostics. In most cases either a rotating arm or a fixed frame of thermometers is used. The signals they provide are visualised by a two dimensional loss distribution plot (temperature map). The thermometers allow detection of the additional heat flow on the cavity outside surface that originates on the inside from the quench locations or the impinging electrons. If inspected from the inside a defect is often found as a culprit on a weld. Quench locations show up as a circular heat sources, field emission electrons leave a linear trace, from which the emission site may be identified by computer simulations. Other diagnostics such as X‐ray sensors complement the diagnostics tools. Evidently suitable diagnostics is mandatory for manufacture control and fault analysis.
3. Measures to improve reproducibility
a) Thermal conductivity
High thermal conductivity niobium helps in stabilizing the temperature around the defect thus pushing the quench field up for the same type of defect. A more favoured heat removal allows smaller temperatures in the vicinity of the defect and hence larger magnetic fields or accelerating gradients. The transition from the superconducting phase to the normal conducting phase near Tc (B) is thus impeded. But even for niobium with high thermal conductivity a limitation of the gradient by a quench cannot be safely avoided.
b) Thin film cavities
Instead of pushing the thermal conductivity of niobium even further up an alternative does exist for instance, coating a thin niobium film inside a copper cavity making use of its intrinsic large thermal conductivity. All cavities for the LHC and the vast majority of cavities for LEP were produced by this technique. Among other advantages offered by this technique, field limitations by a quench were practically absent. Other advantages are a larger Q‐value at small gradients compared to bulk niobium cavities. However the decrease of the Q‐value with the gradient is more pronounced (Fig. 10). Irrespective of its potential for the future the technique of thin niobium film coating on copper is presently fully adequate for low and intermediate gradients as required in circular and heavy ion linear accelerators, as described before.
23
Figure 10: Q vs. accelerating gradient for 1500 MHz mono‐cell copper cavities at 1.7 K sputter coated with a thin niobium film under argon31 and krypton32 atmosphere (left and right, resp.).
D. Proposal for future R&D work Niobium bulk cavities are in a favoured position of being pushed still further in performance, because the approved and emerging projects are based on that technology. Therefore R&D resources will be available to further develop their performance. However, the long lead times needed to further develop a relatively complicated and multi‐discipline technology such as SRF, top priority should be attributed to materials beyond bulk niobium. Evidently every endeavour must be made to thoroughly understand the performance limitations including the Q‐slope. It is doubtful that a deeper understanding can be achieved without active participation in the experimental work of experts in superconductivity with a solid theoretical background. It is not sufficient to delegate the analysis merely to theorists without involving them in the experimental work. A reliable assessment of new SRF surfaces is eventually only possible by submitting them to RF exposure. Therefore all attempts to develop or improve host cavities for sample tests beyond what exists should have priority. Close collaborations with surface analysis laboratories are evidently needed to correlate the RF results on sample with those on DC.
For these reasons the proposal presented here will not cover the ongoing R&D work in relation with the approved or planned projects. This work is well underway and endowed with the resources needed. It follows the conventional paths, which comprise large RRR niobium as a starting material, shaping and welding, smoothing the welds by mechanical abrasion (tumbling), chemical or electrochemical removal of surface damage layers, heat treatment, rinsing with ultraclean water, mild baking, assembling under dust‐free conditions, etc. Thanks to continuous improvement of preparation techniques, with close
31P. Bosland, A. Aspart, E. Jacques, M. Ribeaudeau, IEEE Trans. Appl. Supercond. 9 (1999) 896. 32 V. Arbet‐Engels, C. Benvenuti, S. Calatroni, P. Darriulat, M. A. Peck, A.‐M. Valente, C. A. Van’t Hof, Nucl. Instr. Meth. A 463 (2001) 1.
24
application of lessons from the wafer preparation, the niobium technology matured up until achieving the theoretical limits, as described before. The manufacture steps need, of course, further improvements in quality assurance in order to keep the performance at a constant high level. Further efforts in theoretical understanding are followed as well, as for example the Q‐slope.
What will be proposed in what follows goes beyond this conventional path. The seeds for a strategy to eliminate the performance flaws of sc cavities as of today and to push further development are rather obvious from what was described before. Promising cures are the following.
1. Niobium
• RF Losses by field emission increase exponentially with the gradient, therefore overloading the cooling capacity of the refrigerator, and may lead to a quench and reduce the reproducibility of performance. The cure is conventional and followed up routinely. The procedures for processing and assembling the cavities and cryo‐modules are continuously improved by applying ultrapure clean conditions. The semiconductor industry has developed adequate techniques that are copied if needed. An example applicable for SRF can be the total absence of human intervention during the wafer processing, the human body being the principle source of dust. This possibility should be assessed for SRF purposes.
• Welding defects often cause a quench and also affect the reproducibility. The cure consists in completely avoiding welds that feature a high probability of defects. High thermal conductivity substrates are used to stabilize prevailing defects. Studies on thin niobium films on copper as a high thermal conductivity substrate deserve continuation; a possible shaping technique to produce seamless cavities without welds consists in spinning or hydro‐forming. One may both manufacture a copper cavity and coat it inside with a niobium film (Fig. 11) or one may produce a niobium cavity from a thin tube and cold‐ spray copper on the outside for mechanical stabilisation of the cavity shape33.
33 N. Valverde and S. Atieh, Novel fabrication techniques for SRF cavities, note CERN‐EN 8 March 2011
25
Figure 11: Hydro‐formed mono‐and multi‐cell copper cavities at 2.1 and 1.5 GHz34.
• The Q‐slope at intermediate gradients35 indicates that the RF losses increase more rapidly than predicted by theory and are largely insensitive to the treatment applied. Two possible cures are promising, always under the hypothesis of the Q‐slope being created by the entry of magnetic flux at low Bc nucleation centres:
(i) coat the niobium surface with a protective superconducting layer other than niobium to cover the nucleation centres for flux entry; this layer must be sufficiently thin to exclude that it may limit the accelerating gradient;
(ii) modify the morphology of the niobium oxides by vacuum firing the cavity; it should be remembered that the first breakthroughs in the niobium SRF technology were obtained by electro‐polishing and UHV firing.
These proposals should be accompanied by making extensive use of surface analysis methods (e.g. TEM). The contacts to material science institutions must be strengthened in order to obtain their expertise knowledge. Analyzing not only the impurity depth profile, as was done by now, but also the impurity lateral profile (plan view) in high resolution would be needed;
34 C. Hauviller, Fully hydroformed RF cavities, Proc. 1989 Part. Acc. Conf. Chicago, Ill. (USA). 35 The Q‐slope at high gradient (Q‐drop) can be cured by moderate baking of the cavity (120 – 140 °C)
26
• The accelerating gradient is not sufficient for future linear colliders for particle physics. A very promising cure is already actively followed in several SRF labs and should be boosted more. It consists in coating on top of the niobium substrate a sandwiched film of one or more bi‐layers of isolator and superconductor sufficiently thin that it can prevail in a magnetic field larger than the superheating field of niobium. This layer shall sufficiently reduce the magnetic field amplitude at the isolator‐niobium substrate interface. Samples possessing such an isolator niobium sandwich shall be validated under RF inside a host cavity (e. g.TE011 cavity or quadrupole resonator36) before applying this technique to a RF cavity.
2. Alternate materials
In view of the long lead time until technical maturity is achieved several alternatives to bulk or thin film niobium should be investigated as soon as possible.
• There is a continuous quest for lower RF losses compared to niobium. Alternatively, but closely linked to that, the operation of accelerating structures at 4.5 K instead in super‐fluid helium at 2K would be possible. Candidates to get around this issue are materials with a larger Tc than niobium, such as the “classical” high Tc superconductors, NbN and Nb3Sn.
• The limitation in accelerating gradient inherent to niobium shall be extended. As a cure is offered by the conjecture confirmed meanwhile that the ultimate limitation is proportional to the superheating magnetic field, being on its part proportional to the thermodynamic critical field Bth, Therefore materials with a larger Bth than niobium are promising, such as “classical” high Tc superconductors NbN or Nb3Sn.
These alternate materials have already been proven to possess Q‐values larger than niobium, however only at low gradient; the reason is probably their relatively complicated phase diagram; a wise beginning of a R&D program would consist in preparing samples and evaluating their performance under RF exposure again in a host cavity, before applying the optimized coating procedure to a full RF cavity or accelerating structure. Substrates to be studied are niobium or copper. Coating can be done by thermal diffusion of tin into niobium in a dedicated furnace or by co‐deposition of niobium and tin. The equipment needed consists of a vacuum furnace providing a temperature of about 1100 °C and co‐deposition
36 A quadrupole resonator is operational at CERN
27
equipment. The study can then extend to “multi‐layers” of a thin film of, say, niobium, Nb3Sn or NbN37.
These technical actions should be accompanied by a continuous funding and strong links with non‐accelerator institutes including universities for guidance in theory and application of surface analysis methods other than practiced by now.
V. Capacity and availability needs related to emerging European projects
Any missing equipment or initiatives, in the European context, shall be identified by comparing the needs of technical equipment with the available one, related to both R&D and emerging or approved projects. What future R&D work will require was described in the previous chapters. What emerging or approved projects will need in the forthcoming years is summarized in Table 2.
Table 2 shows that the different projects are pushing against different technical frontiers. Inspecting it shows that there are large variations in the specifications (number of cavities, beam current, accelerating gradient, etc.). These variations obviously define the need and scope of R&D work required for the future projects.
A large number of cavities will raise the question whether the available test facilities are sufficient in capacity and technical capability or need to be upgraded. This frontier concerns logistics, quality assurance, reproducibility of performance and cost. A large beam current will touch the frontier of the maximum total beam power and the individual power to be allotted per cavity by the power coupler. A large accelerating gradient accompanied by reasonably moderate RF losses, will require crossing the fundamental and technological limits of the SRF niobium technology.
These three frontiers ask for different approaches for a solution.
The cost and RF power coupler frontiers are not fundamental, but more of political and technological nature. The total beam power, instead of dumping it and facing the implications of safety and environment, may be reused by energy recovery schemes (ERL). The RF power to be imparted per cavity can for instance be reduced by limiting the number of cells or increasing the number of power couplers. These issues are nevertheless considered as outside the scope of this report, because they are already covered and
37 A. Gurevich, Enhancement of RF breakdown field of superconductors by multilayer coating, Appl. Phys. Letts. 88, 012511 (2006).
28
treated by the R&D work related to the up‐to‐date SRF projects. As they do not affect the future of the SRF field, they will not be discussed in more detail in what follows.
Table 2: Emerging/approved SRF projects related to ESFRI38
Field of research
Project (approved or
emerging)
First operation for users
Accelerated particles
Accelerating gradient [MV/m]
Current [mA]
Frequency [MHz]
Number of sc
cavities ESS: The
European Spallation
Source
2019 protons 15 50 352/704 234
European XFEL 2015 electrons 24 5 1300 909 Materials Sciences
FEL (ALICE, BERLinPro S‐
DALINAC, FLASH, ELBE)
2006‐2015 electrons ~5 – 251) ~1001) 1300 ~101)
HIE‐ISOLDE 2016 heavy ions 62) ≤ 10‐7 1) 101 32
FAIR/UNILAC 2014 heavy ions 52) 1 217 9
SPIRAL2 2012/13 deuterons/heavy
ions 6.52) 5 88 26
SPL (neutrino physics)
2015 protons 25 n/a 704 43)
HL‐LHC4) ~2020 protons 20‐255) 580 400 16
Astronomy, Astrophysics,
Nuclear and Particle
Physics
ILC 2012 (TDR) electrons 31.5 9 1300 266)
ADS MYRRHA 2023 protons ~5‐107) 2.5 ‐ 4 352/704 155 1) order of magnitude 2) per world region as defined in Global Design Effort (GDE)
3) for SPL study 4) crab cavities for luminosity upgrade
5) equivalent acc. gradient with 1 MV/m equivalent to 4 mT 6) the maximum magnetic surface in mT corresponds to about ten times this number 7) the maximum magnetic surface in mT corresponds to about five to ten times this number
A. Logistical needs
Being guided by the ESFRI Road map39, Table 2 summarizes the SRF related projects in Europe, either emerging, approved, or under construction. Based on the total number of cavities to be acquired the XFEL project is certainly the most ambitious one. The projects with smaller number of cavities are ESS, MYRRHA, HIE‐Isolde, and preparation for the ILC and SPIRAL2, in decreasing order. It is difficult to predict possible collisions as far as testing places are concerned. But there could be a coincidence, mainly as of 2012, for cavity reception and cryo‐module qualification tests for SLHC, ESS, ILC and HIE‐Isolde.
38 http://ec.europa.eu/research/infrastructures/index_en.cfm?pg=esfri 39 http://ec.europa.eu/research/infrastructures/pdf/esfri_report_20090123.pdf
29
B. Needs for R&D initiatives
Clean assembly and ultrapure water installations are in widespread use and operational. The technology has been adopted from the semiconductor industry, and staff in the SRF laboratories are aware of the need to permanently monitor and upgrade the existing equipment. Samples prepared with the aim to reduce field emission can be investigated in the scanning field emission microscope of Wuppertal University.
Hydro‐forming seamless niobium cavities is done at DESY, spinning at Legnaro, and hydro‐forming of seamless copper cavities has been done at CERN in the past and could be revitalized.
The Q‐slope is being studied theoretically, however only marginally with an active participation of theoreticians in superconductivity. Connections between them and experimentalists should be intensified, as is the case in the US. Sample testing equipment under RF exposure is available at CERN (quadrupole resonator with variable frequency range from 400 to 1200 MHz) and at IPN Orsay (TE011 cavity at 3.9 and 5.1 GHz). A dedicated furnace allowing the firing of niobium cavities up to 1800 °C under preservation of UHV conditions is available at Darmstadt University40. General purpose furnaces of different capacities and useful volumes are available at CERN. General purpose surface analysis tools are fairly common41; more sophisticated equipment is also available in European accelerator or other labs42. The collaboration with non accelerator labs could nevertheless be intensified.
Classical high‐Tc superconductors are at present not being investigated in Europe. The US started a campaign to reproduce the results on Nb3Sn coating on bulk niobium43. The main missing equipment is a furnace that should go up in temperature to at least 1250 °C. It would allow continuation of the past studies of coating with Nb3Sn on bulk niobium by a diffusion process. The excellent results already obtained raise hope for rapid improvement.
Multi‐layers are studied at Argonne Laboratory (US) and at CEA Saclay. This activity is certainly worth being endowed with sufficient resources and extended.
Expertise and instruments would be available in specialized research centres, such as the Ernst‐Ruska Centre for Microscopy and Spectroscopy with Electrons at Jülich (Germany), to give an example
40 The furnace needs to be partially refurbished 41 E. g. SEM, Auger depth profiling, SIMS, Magnetisation, RRR and Tc measurements of superconductors, Eddy current surface scanning, ... 42 E. g. TEM, ERD, NRA, PIXE, RBS, Squid surface scanning, ... 43 Cornell University
30
VI. Conclusions
(i) The SRF community is relatively small and well known among each other and well integrated in supra‐national integrative attempts. De facto, a distributed network of infrastructures for R&D and test of sc cavities and cryo‐modules has been established in a bottom up approach in Europe and beyond. Therefore a need for a SRF test infrastructure, distributed across, and managed by, European accelerator labs, does not exist.
(ii) Important issues defining the research topics for the future of SRF technology are the accelerating gradient, the RF losses and the reproducibility of performance. As an increase of the accelerating gradient requires a simultaneous reduction of the RF losses, both topics have similar priority. The gradient limitation is in most cases caused by a surface defect or by field emission. Clean surface preparation and cavity assembling is absolutely mandatory to avoid field emission. Seamless cavities or thin niobium films on copper cavities may offer quench‐free performance. There is a gap in performance between small mono‐cell and large accelerating cavities, results on the latter being less reproducible. To assess the priority of solving the reproducibility issue depends primarily on scale of the specific project.
The niobium technology is approaching the predicted theoretical limit in accelerating gradient, the superheating critical magnetic field Bsh. To overcome this barrier, both materials with a larger Bc than niobium should be studied and the merits of thin superconductor ‐ insulator sandwiches should be continued to be explored. The most promising candidate for SRF application in the future is the classical high Tc superconductor Nb3Sn, because of its stoichiometry and therewith the appropriate phase is well known and it has the largest Bc among the sufficiently understood superconductors44. Complementary to, and equally important for, an increasing accelerating gradient is a larger Q‐value, in order to limit the cryogenic power and operating costs. This potential in principle is also in reach with Nb3Sn.
All surfaces that were used so far for SRF application suffer, though to a different degree, by an increase of the RF dissipation with the accelerating gradient more than expected (Q‐slope). As this observation is quite universal and lacks a physical explanation it should therefore be studied with priority and understood.
44 MgB2 and YBCO are not considered as such
31
Sample tests under RF and DC are important because they allow an independent assessment of, and a correlation between, RF and DC properties of sc materials. Host cavities are available in a few labs but their number should be increased.
Mutual interaction of universities and research centres laid the ground for technological and scientific innovations; their implementation was successfully driven by collaborative efforts between research centres and industry. The links between accelerator labs and non‐accelerator institutes and universities should be reinforced.
(iii) The available equipment in European accelerator labs is considerable and close to complete. It is adapted to the TESLA niobium technology and consequently satisfies the needs of XFEL. The largest concentrations of equipment are located around the laboratories such as DESY, CEA Saclay/IPN‐Orsay‐Supratech and CERN.
However, the revived interest and the upcoming projects for proton drivers (ESS, Myrrha, neutrino facories) demand a thorough re‐assessment of the available test infrastructures.
Equipment to produce thin niobium films on copper is traditionally housed at CERN, but also at INFN Legnaro. Research work is going on in the frame of the EuCARD initiative.
Any other research initiatives beyond these materials do not practically exist.
In view of the very long adolescence and in order to tap the full potential of the SRF technology, new materials and approaches should be pursued now. Encouraging results were already obtained in the past, such as for niobium film on copper and classical high Tc superconductors. If the same resources were applied for these materials as for niobium bulk material, progress is attainable.
32
VII. Glossary AccNet Accelerator Science Network
ADS Accelerator Driven Systems (neutron sources for nuclear waste transmutation or triggering subcritical fission reactors)
ALICE Accelerators and Lasers In Combined Experiments BCS surface resistance
Surface resistance that depends exponentially on the ration of energy gap and temperature
BCS theory Bardeen Cooper Schrieffer theory of superconductivity BEBC Beijing based electron positron collider
BERLinPro Berlin Energy Recovery Linac Project Beta Ratio of particle to light speed
B‐factory High luminosity electron positron storage producing abundantly B‐mesons CARE Coordinated Accelerator Research in Europe CERN Centre Européen pour la recherche nucléaire at Geneva (Switzerland)
Cooper pair Interacting electrons with opposite spin that carry the super‐current Crab cavity RF cavity for bunch rotation to make them collide head‐on
CRISP Cluster of Research Infrastructures for Synergies in Physics Critical magnetic
field Bc Magnetic field below which the metal is superconducting (at zero
temperature) Critical temperature
Tc Temperature below which the metal is superconducting (at zero magnetic
field) Cryo‐module String of sc cavities inside a dedicated cryostat equipped with all ancillary
elements required for accelerating a beam of particles EB welding Electron beam welding
ELBE Electron Linac for beams with high Brilliance and low Emittance at HZDR Dresden (Germany)
EP Electro‐Polishing ERD Elastic Recoil Detection ERL Electron Recovery Linac
ESFRI European Strategy Forum on Research Infrastructures ESGARD European Steering Group on Accelerator R&D
ESS European Spallation Source (for neutrons) EuCard European Coordinated Accelerator Research and Development
FEL Free electron laser Field emission Extraction of electrons off the surface by the action of the electric field
FP Framework program (Research Initiative of the European Union) HPR High Pressure Rinsing ILC International linear collider IOT Inductive Output Tube (RF power source)
IPN‐Supratech SRF technology platform for future accelerators shared between CEA‐Saclay and CNRS Institute de Physique Nucléaire at Université of Paris XI, Orsay
(France) ISOLDE Source of low‐energy beams of radioactive isotopes obtained from on‐line
isotope mass separator JRA Joint Research Activity
33
KEK Japanese centre for high energy physics at Tsukuba LARP US LHC Accelerator Research Program LeHC Large electron Hadron Collider LEP Large electron positron project at CERN, Geneva (Switzerland)
Linac Linear accelerator; “recirculating linacs” cf. under “recyclotron” Microtron Linear electron accelerator with D‐shaped magnets for beam recirculation
NRA Nuclear Reaction Analysis PETRA Positron electron tandem ring accelerator at DESY, Hamburg (Germany) PIXE Proton Induced X‐ray Emission
Quench Sudden breakdown of stored energy in a cavity and its local dissipation by the action of the magnetic field
RBS Rutherford Backscattering Spectroscopy Recyclotron Linear accelerator with distributed magnet system for beam recirculation
Residual surface resistance
Contribution to the surface resistance at small magnetic field in addition to the BCS surface resistance
RFTech Radio‐Frequency Technology networking activity SC Superconducting
S‐DALINAC Superconducting recyclotron housed at the Institute for Nuclear Physics at the University of Darmstadt (Germany)
SEM Scanning Electron Microscopy (with X‐ray analysis) SIMS Secondary Ion Mass Spectroscopy SLAC Stanford Linear Accelerator Centre
S‐LHC‐PP Large Hadron Collider upgrade Preparatory Phase SNS Superconducting spallation source at Oak Ridge National Laboratory, TN
(USA) SRF Superconducting RF
Superconducting energy gap
Energy that an electron gains when interacting with another electron to form a Copper pair
Supratech Technological premises located at IPN Orsay devoted to develop sc cavities relevant for high intensity proton or deuteron beams in close coordination
with CEA‐Saclay (France) TEM Transmission Electron Microscopy
TESLA TeV electron superconducting linear accelerator and the technology that goes with it
TIARA Test Infrastructure and Accelerator Research Area TJLAB Thomas Jefferson Accelerator Lab at Newport News, VA (USA) TTC TESLA Technology Collaboration UHV Ultra high vacuum
UPWR Ultrapure water rinsing at low pressure (~ 6 bar) US Ultrasound
XFEL X‐ray free electron laser at DESY, Hamburg (Germany)
34
Acknowledgments
The work is co‐funded by the European Commission within the Framework Program 7 Capacities Specific Program, Grant Agreement 227579 – EuCARD.
This report would not have been possible without the information and valuable comments received from many individuals, whom I want to thank with gratitude. Particularly important were the comments by the participants of the RFTech meetings and by D. Proch (DESY), as to the contents, and the contributions by S. Chel (CEA‐Saclay), R. Eichhorn (University Darmstadt), P. McIntosh (Cockcroft Institute), W.‐D. Möller (DESY) , G. Müller (University of Wuppertal), G. Olry (IPN Orsay),V. Palmieri (INFN Legnaro), U. Ratzinger (University Frankfurt), and J. Teichert (HZDR), as to the equipment available in their respective laboratories.
35
AN
NEX
SRF
rela
ted
sp
ecif
ic e
qu
ipm
ent a
vail
able
in E
uro
pea
n A
ccel
erat
or
Lab
orat
orie
s
Tab
le 1
: Gen
eral
pu
rpos
e m
anu
fact
ure
/wor
ksh
op t
ools
La
bora
tory
El
ectr
on b
eam
wel
ding
mac
hine
s
Shap
ing/
form
ing
tool
s U
HV
furn
ace
CE
A‐S
acla
y (F
ranc
e)
‐h
ydro‐f
orm
ing
Cu a
nd N
b ap
para
tus
(pre
sent
ly a
t BO
URG
OG
NE‐
HYD
RO)
‐hig
h te
mpe
ratu
re a
nnea
ling
UH
V fu
rnac
e (9
00 °C
) for
1‐c
ell c
aviti
es
CERN
(S
wit
zerl
and)
‐1
m3 E
B w
eldi
ng m
achi
ne 1
50 k
V 7.
5 kW
‐1
m lo
ng E
B w
eldi
ng m
achi
ne 7
0 kV
70
kW
(p <
10‐5
mba
r)
‐spi
nnin
g fa
cilit
y ‐h
ydro‐f
orm
ing
copp
er (t
o be
re‐
furb
ishe
d)
‐5.5
m h
igh
0.95
m d
iam
eter
110
0 °C
@10
‐6 T
orr
‐1
m h
igh
0.24
m d
iam
eter
140
0 °C
@10
‐7 T
orr
‐1 m
hig
h 0.
15 m
dia
met
er 2
000
°C@
10‐7
Tor
r bo
th w
ith s
epar
ate
vacu
ums
for
the
furn
ace
and
the
piec
es to
be
trea
ted
‐sev
eral
bra
zing
furn
aces
~10
00 °C
10‐5
mba
r D
ESY
(Ger
man
y)
‐EB
wel
ding
mac
hine
3.2
x1.6
x1.4
m3
p <
10‐6
mba
r ‐h
ydro‐f
orm
ing
9‐ce
ll ni
obiu
m c
aviti
es
(ste
pwis
e fr
om 3‐c
ells
) ‐1
400
°C U
HV
furn
ace
p<10
‐8 m
bar
< 14
50 °C
‐8
00 °C
UH
V fu
rnac
e p<
10‐7
mba
r <
1100
°C
INFN
Leg
naro
(I
taly
)
‐spi
nnin
g of
nio
bium
and
cop
per
seam
less
mul
ti‐ce
ll ca
vitie
s an
d tu
bes
‐vac
uum
and
atm
osph
ere
cont
rolle
d ov
ens
IPN‐O
rsay
(F
ranc
e)
‐h
ydra
ulic
pre
ss (5
00 k
N)
‐hig
h te
mpe
ratu
re a
nnea
ling
36
Tab
le 2
: Sp
ecif
ic m
anu
fact
ure
/ass
emb
ly fa
cili
ties
an
d in
spec
tion
/tes
tin
g to
ols
Labo
rato
ry
Fiel
d fla
tnes
s te
stin
g/tu
ning
Cl
ean
room
s In
spec
tion
/tes
ting
tool
s CE
A‐S
acla
y (F
ranc
e)
‐2 b
ench
es fo
r fie
ld fl
atne
ss tu
ning
of 7
04
MH
z ca
vitie
s of
var
ious
bet
as
‐ ISO
7 ~6
x5 m
2 ‐IS
O5
~8x5
m2 in
clud
ing
UPW
R ‐IS
O4
~8x1
4 m
2 incl
udin
g ca
vity
was
her,
HPW
R, U
PWR
‐ISO
7 2x
5m2
‐ISO
5 6x
5 m
2 incl
udin
g H
PWR
‐mov
able
cle
an r
oom
s (2
x2 m
2 ) ‐p
artic
le c
ount
ers,
slo
w p
umpi
ng s
tatio
ns, i
oniz
ing
air
guns
CERN
(S
wit
zerl
and)
‐ISO
4 15
x4 m
2 ‐IS
O5
3x5
m2
‐ISO
5 8x
5 m
2
‐ opt
ical
insp
ectio
n of
inne
r cav
ity
surf
ace
Cock
crof
t In
stit
ute
(UK)
‐b
ead
pull
appa
ratu
s in
side
tem
pera
ture
an
d hu
mid
ity c
ontr
olle
d en
clos
ure
‐ISO
4 6x
4 m
2 ‐IS
O5
4x8
m2 in
clud
ing
UPW
R an
d H
PWR
‐mov
eabl
e IS
O4‐
6 cl
ean
room
s (2
x2 to
4x4
m2 )
‐par
ticle
cou
nter
s, s
low
pum
ping
sta
tions
, ion
izin
g ai
r gu
ns
DES
Y (G
erm
any)
‐t
unin
g m
achi
ne in
ded
icat
ed la
b ‐s
emi a
utom
atic
tuni
ng m
achi
nes
for
XFEL
‐a
utom
atis
ed R
F m
easu
rem
ent m
achi
ne fo
r ha
lf‐ce
lls &
dum
b‐be
lls (H
AZE
MEM
A)
‐ Bld
. 28,
ISO
4 20
m2 to
51
m2 w
ith 3
oil
free
pum
p st
atio
ns; 1
sl
ow p
umpi
ng, s
low
ven
ting
equi
pmen
t; in
clud
ing
UPW
R, 2
x H
PWR
‐ ISO
5 62
m2 to
81
m2
‐ ISO
6 ‐s
tand
ard
ISO
6 &
loca
l ISO
4
‐cle
an r
oom
Bld
. 47
‐ISO
5 40
m2 w
ith 1
oil
free
pum
ping
uni
t, U
P W
R H
PWR,
dry
ic
e cl
eani
ng
‐”Ky
oto”
cam
era
‐3D
mec
hani
cal i
nspe
ctio
n ‐m
icro
stru
ctur
e ‐e
ddy
curr
ent s
cann
ing
‐ten
sile
test
‐h
ardn
ess
‐ int
erst
itial
impu
rity
ana
lysi
s (H
,N,O
, C)
‐ met
allic
impu
ritie
s an
alys
is b
y SE
M (F
e,
Ni e
tc.)
‐ sur
face
rou
ghne
ss
‐the
rmal
con
duct
ivity
IN
FN L
egna
ro
(Ita
ly)
‐bea
d pu
ll ap
para
tus
insi
de th
erm
osta
tic
cham
ber
‐are
a of
150
m2 IS
O7
and
15 m
2 of c
lean
roo
m IS
O6
‐dig
ital c
amer
a an
d sy
stem
for
insp
ectio
n in
side
mon
o‐ce
ll ca
vitie
s
IPN‐O
rsay
(F
ranc
e)
‐IS
O4
(45m
²) in
clud
ing
HPW
R (1
00 b
ar)
‐vid
eo‐s
cope
for
insp
ectio
n of
inne
r su
rfac
e ca
vity
37
Tab
le 3
: Su
rfac
e tr
eatm
ent/
coat
ing/
fin
al c
lean
ing
Labo
rato
ry
Surf
ace
trea
tmen
t
Surf
ace
coat
ing/
proc
essi
ng e
quip
men
t
Fina
l cle
anin
g
CEA‐S
acla
y (F
ranc
e)
‐hor
izon
tal E
P fo
r sm
all N
b ca
vitie
s an
d ve
rtic
al E
P fo
r al
l cav
ities
‐2
fully
aut
omat
ed B
CP s
tatio
ns a
nd 2
CP
stat
ions
for
cavi
ties
‐sev
eral
US
degr
easi
ng ta
nks
(larg
est =
250
l)
‐mag
netr
on s
putt
erin
g ap
para
tus
for N
b de
posi
tion
on s
mal
l cav
ities
‐H
PWR
100
bar,
18
MO
hmcm
(in
clea
n ro
om)
CERN
(S
wit
zerl
and)
‐C
u‐CP
LEP
‐LH
C ca
vity
siz
e
‐Cu‐
EP 1
.3‐1
.5 G
Hz
cavi
ties
‐ver
tical
Nb
EP 7
04 M
Hz
5‐ce
ll ca
vitie
s ‐U
S de
grea
sing
16x
0.6
m2
‐US
degr
easi
ng 7
x2 m
2
‐Nb
coat
ing
for 1
.3÷1
.5 G
Hz
cavi
ties
‐Nb
coat
ing
for L
HC
cavi
ties
(400
MH
z m
ono‐
cell)
‐N
b co
atin
g fo
r HIE‐IS
OLD
E ca
vitie
s (1
01 M
Hz
QW
R)
‐HPW
R 10
0 ba
r 18
MO
hmcm
‐U
PWR
6 ba
r 18
MO
hmcm
Cock
crof
t In
stit
ute
(UK)
‐H
PWR
100
bar,
18
MO
hmcm
in IS
O4
clea
n ro
om fo
r si
ngle
and
mul
ti‐ce
ll ca
vitie
s D
ESY
(Ger
man
y)
‐clo
sed‐
circ
uit N
b‐CP
in IS
O7
clea
n ro
om
‐clo
sed‐
circ
uit N
b‐EP
‐H
PR 1
00 b
ar in
ISO
4 cl
ean
room
‐H
PR 2
00 b
ar in
ISO
4 cl
ean
room
‐b
akin
g TE
SLA
cav
ities
@ 1
20 °C
in in
ert g
as
atm
osph
ere
‐bak
ing
TESL
A c
aviti
es @
120
°C in
iner
t gas
at
mos
pher
e an
d IS
O5
clea
n ro
om
‐UPW
R an
d U
S cl
eani
ng in
sta
ndar
d IS
O6
& lo
cal I
SO4
clea
n ro
oms
‐cen
trifu
gal b
arre
l pol
ishi
ng
‐H
PWR:
100
bar
, 18
MO
hmcm
in IS
O5
clea
n ro
om fo
r 9‐
cell
cavi
ty
‐150
bar
18
MO
hmcm
, 3‐c
ell c
avity
‐h
oriz
onta
l dry‐ic
e cl
eani
ng o
f 3‐c
ell
INFN
Leg
naro
(I
taly
) ‐C
P, E
P, tu
mbl
ing
& g
rind
ing,
all
for
QW
R an
d fo
r m
ono‐
cells
and
thre
e ce
lls 1
.3/1
.5 G
Hz
cavi
ties
‐thi
n fil
ms
synt
hesi
s by
mea
ns o
f RF
and
puls
ed D
C m
agne
tron
spu
tter
ing
‐ion
impl
ante
r (ne
w h
eavy
ion
acce
lera
tor
with
ene
rgie
s up
to 2
00 k
eV)
‐HPW
R: 1
00 b
ar, 1
8 M
Ohm
cm
IPN‐O
rsay
(F
ranc
e)
‐bak
ing
(120
°C) i
n IS
O4
clea
n ro
om
‐US
degr
easi
ng ta
nk
‐BCP
faci
lity
(2 s
tatio
ns)
‐H
PWR
(100
bar
) in
ISO
4 cl
ean
room
38
Tab
le 4
: War
m t
est
pla
ces
- hig
h p
ower
cou
ple
r La
bora
tory
Te
st p
lace
s
RF
Uti
litie
s CE
A‐S
acla
y (F
ranc
e)
‐SU
PRA
TECH
: pow
er c
oupl
er te
sts
for
sc c
aviti
es
‐sta
nd fo
r te
st o
f 352
MH
z co
uple
rs a
nd w
indo
ws
at h
igh
pow
er
‐704
MH
z 1.
2 M
W 5
0Hz
2ms
klys
tron
‐7
04 M
Hz
80 k
W c
w IO
T ‐1
300
MH
z 1.
5 M
W 1
0Hz
1ms
klys
tron
‐2
x 3
52 M
Hz
CW k
lyst
rons
on
loan
from
CE
RN
‐cle
an p
umpi
ng s
yste
m, w
ater
coo
ling
and
air
cool
ing
of c
oupl
ers
CERN
(S
wit
zerl
and)
‐ SPL
pow
er c
oupl
ers:
704
MH
z ~1
MW
50
Hz
(SM
18)
‐LH
C:40
0MH
z, 3
30kW
CW
‐f
or e
xter
nal r
eque
sts:
352
MH
z 1
MW
DES
Y (G
erm
any)
‐p
ower
cou
pler
test
s ‐5
MW
Kly
stro
n, 1
.3G
Hz,
pul
sed
‐1.7
MW
, 500
MH
z, C
W
TiN
coa
ting
INFN
Leg
naro
(I
taly
)
IPN‐O
rsay
(F
ranc
e)
39
Tab
le 5
: Col
d t
est
pla
ces
- low
pow
er
Labo
rato
ry
Test
pla
ces/
cryo
stat
s
RF
Cryo
‐inst
alla
tion
CE
A‐S
acla
y (F
ranc
e)
‐ver
tical
test
cry
osta
t CV1
, use
ful d
epth
/dia
met
er 1
.9 m
/0.7
m
‐ver
tical
test
cry
osta
t CV2
, use
ful d
epth
/dia
met
er 1
.2 m
/0.5
m
‐700
MH
z –
1.5
GH
z, 2
00 W
cw
‐4
.2 –
8.6
GH
z, 8
0 W
cw
‐7
00 M
Hz
800
W c
w
‐88
MH
z 20
0 W
cw
‐ tem
pera
ture
ope
ratio
n of
CV1
and
CV2
fr
om 4
.4K
to 1
.6K
‐2 p
umpi
ng u
nits
1 g
/s @
13
mba
r
CERN
(Sw
itze
rlan
d)
‐14m
bun
ker
for
hori
zont
al te
sts
4.5
K (2
K)
‐14m
bun
ker
for
hori
zont
al te
sts
4.5
K ‐v
ertic
al te
st c
ryos
tat
4.2
m d
eep/
1.1m
dia
met
er 2
K
‐ver
tical
test
cry
osta
t 2.
5 m
dee
p/1.
1m d
iam
eter
2 K
‐v
ertic
al te
st c
ryos
tat
4.2
m d
eep/
1.1m
dia
met
er 4
.2 K
‐v
ertic
al te
st c
ryos
tat
4.2
m d
eep/
1.1m
dia
met
er 4
.2 K
‐s
mal
l ver
tical
test
cry
osta
t 4.2‐1
.8 K
mon
o‐ce
ll 1.
5 G
Hz
cavi
ties
‐300
W C
W 3
40 –
355
MH
z ‐3
00 W
CW
390
– 4
10 M
Hz
‐300
W C
W 7
00 M
Hz
‐500
W C
W 2
00 W
120
0 M
Hz
‐600
W C
W 1
00 M
Hz
‐101
W C
W 1
‐2 G
Hz
‐6 k
W @
4.5
K, l
ique
fact
ion
capa
city
of 2
6 g/
s ‐h
eliu
m p
umpi
ng u
nits
of 1
8 g/
s at
3 k
Pa (3
0 m
bar)
Cock
crof
t Ins
titu
te
(UK)
‐v
ertic
al te
st c
ryos
tat
3.5
m d
eep/
0.8m
dia
met
er 4
.2 a
nd 2
K
‐2
50W
CW
1.3
GH
z ‐5
00W
CW
1.3
GH
z ‐2
0kW
CW
1.3
GH
z
‐4.2
K a
nd 2
50 m
3 /h r
oots
pum
ping
sta
tion
for
1.5
K
DES
Y (G
erm
any)
‐2
ver
tical
test
cry
osta
t, d
iam
eter
0.6
m
‐2 v
ertic
al te
st c
ryos
tat (
AM
TF, X
FEL)
, dia
met
er 1
.1m
‐2
x 10
00 W
cw
1.3
GH
z ‐2
x 10
00 W
cw
1.3
GH
z ‐2
00W
, 2K
per c
ryos
tat
‐400
W, 2
K pe
r cry
osta
t (A
MTF
, XFE
L)
INFN
Leg
naro
(I
taly
) ‐s
tand
for
6 G
Hz
cavi
ty te
st
‐ver
tical
cry
osta
t for
1.5
/1.3
GH
z m
ono‐
cell
and
mul
ti‐ce
ll ca
vitie
s ‐1
.3/1
.5 G
Hz,
500
W C
W
‐6 G
Hz
200W
CW
‐4
.2 K
and
200
00 m
3 /h r
oots
pum
ping
st
atio
n fo
r 1.8
K
IPN‐O
rsay
(Fra
nce)
‐v
ertic
al c
ryos
tat 2
.5 m
dee
p 0.
8 m
dia
met
er w
ith m
icro
phon
ics
and
acce
lero
met
er te
sts
for b
are
and
jack
eted
cav
ities
‐v
ertic
al c
ryos
tat 2
m d
eep,
0.3
5 m
dia
met
er
‐tw
o ho
rizo
ntal
cry
osta
ts: o
ne fo
r 35
2 M
Hz
and
one
704
MH
z ca
vitie
s
‐250
W @
3 to
6 G
Hz
‐3 k
W @
704
MH
z ‐2
50 W
and
600
W @
350
MH
z ‐2
x1 k
W @
88
MH
z
‐liqu
efie
r, 7
0l/h
rat
e pr
oduc
tion
4K a
nd 2
K op
erat
ing
tem
pera
ture
40
Tab
le 6
: Col
d t
est
pla
ces
- hig
h p
ower
La
bora
tory
Te
st p
lace
s/cr
yost
ats
RF
Cr
yo‐in
stal
lati
on
CEA‐S
acla
y (F
ranc
e)
‐“Cr
yhol
ab”
faci
lity,
hor
izon
tal c
ryos
tat f
or h
igh
pow
er R
F te
sts
at 1
.3
GH
z/70
4 M
Hz
at 1
/8 K
‐ 4.
5 K,
sim
ilar
as o
pera
ted
in a
ccel
erat
or (1
.5
m lo
ng, 0
.7 m
dia
.) ‐p
ower
test
sta
nd fo
r 88
MH
z SP
IRA
L2 c
aviti
es a
nd c
ryo‐
mod
ules
‐1
5 m
bun
ker f
or te
st o
f var
ious
cry
o‐m
odul
es (I
FMIF
, ESS
, …)
‐704
MH
z 1.
2 M
W 5
0Hz
2ms
klys
tron
‐7
04 M
Hz
80 k
W c
w IO
T ‐1
300
MH
z 1.
5 M
W 1
0Hz
1ms
klys
tron
‐2
x 3
52 M
Hz
cw k
lyst
rons
on
loan
from
CER
N
‐88
MH
z 10
kW
cw
sol
id s
tate
am
plifi
er o
n lo
an
from
GA
NIL
‐140
l/h
LHeI
liqu
efie
r 4 g
/s
pum
ping
spe
ed @
13
mba
r
CERN
(S
wit
zerl
and)
‐1
4m b
unke
r fo
r ho
rizo
ntal
test
s 4.
5K 2
K ‐1
4m b
unke
r fo
r ho
rizo
ntal
test
s 4.
5K
‐1M
W c
w 3
52±1
MH
z ‐1
MW
pul
sed
700
MH
z ‐3
00kW
cw
400
±1 M
Hz
‐6 k
W @
4.5
K, l
ique
fact
ion
capa
city
of 2
6 g/
s ‐h
eliu
m p
umpi
ng u
nits
of 1
8 g/
s at
3 k
Pa
DES
Y (G
erm
any)
‐“
Chec
hia”
faci
lity
for
high
and
low
pow
er o
pera
tion
at 1
.3 G
Hz
of
fully
equ
ippe
d ca
vity
sys
tem
s at
1.8‐2
K
‐CM
TB te
st s
tand
for F
LASH
/ X
FEL
mod
ules
‐A
MTF
with
3 te
st s
tand
s fo
r XFE
L m
odul
es
‐Che
chia
: 5M
W K
lyst
ron
1.3
GH
z
‐CM
TB: 1
0MW
Kly
stro
n 1.
3 G
Hz
‐AM
TF: 3
test
sta
nds
with
5M
W K
lyst
ron
1.3G
Hz
each
‐Che
chia
: <50
W, 2
K ‐C
MTB
: 200
W, 2
K ‐ A
MTF
: 200
W, 2
K ea
ch
INFN
Leg
naro
(I
taly
)
IPN‐O
rsay
(F
ranc
e)
‐tw
o ho
rizo
ntal
cry
osta
ts: o
ne fo
r 35
2 M
Hz
and
one
704
MH
z ca
vitie
s ‐8
8 M
Hz,
2 x
10
kW (S
olid‐s
tate
) cw
‐7
04 M
Hz,
80
kW (I
OT)
cw
‐3
50 M
Hz,
10
kW (2
0 kW
) (so
lid‐s
tate
) cw
‐3
50 M
Hz,
2.8
MW
(Kly
stro
n), p
ulse
d
41
Tab
le 7
: Sam
ple
ch
arac
teri
sati
on a
nd
oth
er te
st/i
nsp
ecti
on e
qu
ipm
ent
Labo
rato
ry
RF S
ampl
e ch
arac
teri
zati
on
DC
Sam
ple
char
acte
risa
tion
O
ther
equ
ipm
ent
CEA‐S
acla
y (F
ranc
e)
‐o
ptic
al m
icro
scop
e an
d ca
mer
a ‐p
reci
sion
sca
les
‐glo
ssm
eter
‐v
ideo
‐end
osco
pe
‐RRR
mea
sure
men
ts o
f sam
ples
at 1
.6 –
300
K ‐m
echa
nica
l coe
ffic
ient
s of
sam
ples
at c
old
(4K)
Sam
ple
prep
arat
ion:
‐s
ampl
e en
caps
ulat
ion
‐mec
hani
cal,
mec
hani
cal &
che
mic
al p
olis
hing
CERN
(S
wit
zerl
and)
‐q
uadr
upol
e re
sona
tor
(400
/120
0 M
Hz
sam
ple
diam
eter
7.5
cm
abo
ve 2
K)
‐sca
nnin
g el
ectr
on m
icro
scop
e co
uple
d w
ith E
DX
com
posi
tion
anal
ysis
‐X‐r
ay d
iffra
ctom
eter
fitt
ed w
ith E
uler
ian
crad
le
‐XPS
che
mic
al s
urfa
ce a
naly
sis
and
Aug
er c
ompo
sitio
n an
alys
is
‐Tc
& R
RR m
easu
rem
ents
‐X‐r
ay fl
uore
scen
ce
DES
Y (G
erm
any)
‐RRR
‐S
EM &
ED
X ‐s
ee a
lso
insp
ectio
n/te
stin
g to
ols
(Tab
le 2
)
Acc
ess
to b
eam
faci
litie
s:
‐XFE
L in
fras
truc
ture
and
TES
LA T
est F
acili
ty
‐FLA
SH w
ith 1
GeV
e‐b
eam
IN
FN L
ASA
M
ilano
(Ita
ly)
Man
ufac
ture
and
des
ign:
‐d
evel
opm
ent a
nd d
esig
n fo
r sc
cavi
ties,
cr
yom
odul
es a
nd a
cces
sori
es
Proc
essi
ng a
nd a
ssem
bly:
‐H
PWR
stat
ions
RF
test
ing:
‐v
ertic
al c
ryos
tat f
or 5
00, 7
04 a
nd 1
300
MH
z, 4
.2 –
1.
8 K
300
m3 /h
gH
e pu
mpi
ng s
tatio
n IN
FN L
egna
ro
(Ita
ly)
‐ n
ucle
ar te
chni
ques
with
ion
beam
s (R
BS, E
RD, P
IXE,
NRA
) X‐r
ay
ener
gy a
naly
sis;
‐s
cann
ing
elec
tron
mic
rosc
opy
(SEM
) ‐m
icro‐s
crat
ch‐t
este
r ‐X‐r
ay d
iffra
ctom
etry
42
IPN‐O
rsay
(F
ranc
e)
‐TE 0
11 c
avity
for
surf
ace
resi
stan
ce m
easu
rem
ents
(3
.88
& 5
.12
GH
z) s
ampl
e on
dis
c of
125
mm
di
amet
er (1
10 m
m o
f ef
fect
ive
diam
eter
)
‐RRR
(100
mm
x 3
.5 m
m) i
n cr
yost
at w
ith 0
.15
m d
iam
eter
0.9
m
deep
‐t
herm
al c
ondu
ctiv
ity o
f iso
latin
g an
d co
nduc
ting
mat
eria
ls 4
.2 ‐
300
K ‐K
apitz
a re
sist
ance
1.7
– 2
.1 K
(0.5
mm
thic
k, <
80
mm
dia
met
er)
Acc
ess
to b
eam
faci
litie
s:
‐ ALT
O, 1
0 –
50 M
eV, 1
0 µA
e‐b
eam
‐ T
AN
DEM
Van
de
Gra
af, 1
5 M
V H‐ io
ns, a
ggre
gate
io
n be
ams
LAL‐
Ors
ay
(Fra
nce)
W
arm
test
pla
ces:
‐1
300
MH
z 5
MW
‐7
904
MH
z, b
oth
in fu
ll re
flect
ion
and
unde
r m
atch
ed c
ondi
tions
‐A
r di
scha
rge
clea
ning
43
Specific SRF related equipment available elsewhere Institution/University Equipment
Cockcroft Institute Daresbury/Universitie
s of Lancaster, Liverpool and
Manchester (UK)
Processing and assembly: ‐ISO6 7x9 m2 clean room ‐3x4m2 clean room
RF testing: ‐20 kW 1.3 GHz IOT ‐300 W 1.3 GHz
‐250 kW 500 MHz Klystron ‐6 MWpk (12 kWavg) 2998 MHz klystron (6μs pulse)
Cryogenics: ‐150W @ 1.8 K‐120W @ 4.5 K
Sample characterisation: ‐XPS/SEM
‐ultrasonic force microscopy Access to beam facilities:
‐ALICE IR‐ERL 13 �A 35 MeV e‐beam ‐EMMA NS‐FFAG 10 – 20 MeV e‐beam
Darmstadt Institut für Kernphysik (Germany)
Processing and assembly: ‐ISO5 clean room
‐chemical polishing facility ‐temperature annealing of samples and small size cavities in UHV furnace: max. sample diameter: 120 mm, max. sample length: 1400 mm, max. temperature:
1800°C, min. pressure: 10‐8 mbar, sample chamber built of reactor grade niobium RF testing:
‐bath cryostat testing area Access to beam facilities:
‐S‐DALINAC e‐recyclotron 60 �A 2.5 – 130 MeV Frankfurt University Institute of Applied
Physics
Processing and assembly: ‐ISO7 clean room
RF testing: 3 m high vertical cryostat, transport dewar, helium recovery system, 150 W cryo plant at 4K, 3000 l helium storage, 330‐370 MHz amp. 2 kW cw, 325 MHz 40 kW
pulsed, 2 ms, 5 Hz (200 W cw), 50‐1000 MHz, 50 W cw, concrete test cave 5 x 4.5 x 3.5 m3, LLRF 100‐400 MHz
HZB Berlin (Germany) RF testing: ‐power coupler tests
‐solid state amplifiers, klystron and IOT 1300 MHz 200 W‐30 kW CW ‐“HoBiCaT” test facility for high and low power simultaneous test of fully equipped
cavity systems 3.5 m long 1.1 m useful diameter‐1.8‐2.2 K@ 4 g/s 80 W‐180 l/ h 4.5 K TCF50 helium refrigeration plant at BESSYII
Access to beam facilities: ‐BESSY FEL
HZDR Dresden (Germany)
RF testing: ‐power coupler tests 1300 MHz CPI klystron 10 kW CW RF power
Access to beam facilities: ‐ELBE radiation source 40 MeV 1 mA average beam current
Wuppertal FB Physik (Germany)
Sample characterisation: ‐DC field emission scanning microscope and spectrometer
‐surface roughness measurements on Nb samples (optical profilometer, atomic force microscope)
44