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ISO/TC 213/WG 16 N 712 ISO/TC 213/WG 16 Areal and profile surface texture Email of convenor: [email protected] Convenorship: SIS (Sweden) ISO_25178-70_PTB_Germany_Circular_Chirp Document type: Other committee document Date of document: 2017-08-29 Expected action: INFO Background: Funded by the European Union’s Horizon 2020 research and innovation programme the PTB colleagues have developed a material measure to characterize optical 3D microscopes, the instrument transfer function and the topography fidelity. The European EMPIR project of the Horizon programme 14IND07- 3D Stack includes a work package on roughness and surface quality of silicon wafers. Working on this the PTB colleagues, Gaoliang Dai et al, have developed a chirp standard with concentric circular structures with its profile in radial direction being a rectangular height signal with its lateral width sequence according to a chirp frequency distribution. This presentation to introduces Gaoliang Dai's circular chirp standard as a candidate to be included into ISO 25178-70, Material measures. The presentation will be given under agenda item 19 at the IOS/TC 213/WG 16 meeting in Tokyo September 2017. Committee URL: http://isotc.iso.org/livelink/livelink/open/tc213wg16

Development of a material measure to characterize ...empir.npl.co.uk/3dstack/.../10/2018/05/3d-stack-iso...in ISO 25178-70 between Section 8.7 and 8.8 Analysis of the material measure

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Page 1: Development of a material measure to characterize ...empir.npl.co.uk/3dstack/.../10/2018/05/3d-stack-iso...in ISO 25178-70 between Section 8.7 and 8.8 Analysis of the material measure

ISO/TC 213/WG 16 N 712

ISO/TC 213/WG 16Areal and profile surface texture

Email of convenor: [email protected] Convenorship: SIS (Sweden)

ISO_25178-70_PTB_Germany_Circular_Chirp

Document type: Other committee document

Date of document: 2017-08-29

Expected action: INFO

Background: Funded by the European Union’s Horizon 2020 research andinnovation programme the PTB colleagues have developed amaterial measure to characterize optical 3D microscopes, theinstrument transfer function and the topography fidelity. TheEuropean EMPIR project of the Horizon programme 14IND07-3D Stack includes a work package on roughness and surfacequality of silicon wafers. Working on this the PTB colleagues,Gaoliang Dai et al, have developed a chirp standard withconcentric circular structures with its profile in radial directionbeing a rectangular height signal with its lateral width sequenceaccording to a chirp frequency distribution.

This presentation to introduces Gaoliang Dai's circular chirpstandard as a candidate to be included into ISO 25178-70,Material measures. The presentation will be given under agendaitem 19 at the IOS/TC 213/WG 16 meeting in Tokyo September2017.

Committee URL: http://isotc.iso.org/livelink/livelink/open/tc213wg16

Page 2: Development of a material measure to characterize ...empir.npl.co.uk/3dstack/.../10/2018/05/3d-stack-iso...in ISO 25178-70 between Section 8.7 and 8.8 Analysis of the material measure

ISO/TC 213, Sep. 5-6 Tokyo, Japan

Development of a material measure to characterize instrument transfer function and topography fidelity

Gaoliang Dai, Benedikt Seeger, Thomas Weimann,

Rainer Tutsch, Dorothee Hüser, Ludger Koenders

1

14IND07-3D

Page 3: Development of a material measure to characterize ...empir.npl.co.uk/3dstack/.../10/2018/05/3d-stack-iso...in ISO 25178-70 between Section 8.7 and 8.8 Analysis of the material measure

Circular Chirp

[email protected]

Material measure to be specifiedin ISO 25178-70 between Section 8.7 and 8.8

Analysis of the material measure consistent withISO 25178-700 Annex D

Parameter to characterize isotropy vs. anisotropy of ISO 25178-2 to be used to characterize isotropy of detection

ISO/TC 213 WG16, Sept 5th-6th, Tokyo, Japan

Page 4: Development of a material measure to characterize ...empir.npl.co.uk/3dstack/.../10/2018/05/3d-stack-iso...in ISO 25178-70 between Section 8.7 and 8.8 Analysis of the material measure

Circular Chirp

[email protected]

concentric,circular rings of- same height- varying width- varying spacing

variation of widthand spacingaccording tochirp frequencydistribution

Page 5: Development of a material measure to characterize ...empir.npl.co.uk/3dstack/.../10/2018/05/3d-stack-iso...in ISO 25178-70 between Section 8.7 and 8.8 Analysis of the material measure

Circular Chirp

[email protected]

Zoom into part to show that the Moiré structure does not belong tothe object - limitation of display.

ISO/TC 213 WG16, Sept 5th-6th, Tokyo, Japan

Page 6: Development of a material measure to characterize ...empir.npl.co.uk/3dstack/.../10/2018/05/3d-stack-iso...in ISO 25178-70 between Section 8.7 and 8.8 Analysis of the material measure

Height

Circular Chirp

radial

[email protected]

50 nm

ISO/TC 213 WG16, Sept 5th-6th, Tokyo, Japan

Page 7: Development of a material measure to characterize ...empir.npl.co.uk/3dstack/.../10/2018/05/3d-stack-iso...in ISO 25178-70 between Section 8.7 and 8.8 Analysis of the material measure

Realised Circular Chirp standard at PTB

Optical view of the manufactured standard

SEM view of the detailed part of structure

[email protected]/TC 213 WG16, Sept 5th-6th, Tokyo, Japan

Page 8: Development of a material measure to characterize ...empir.npl.co.uk/3dstack/.../10/2018/05/3d-stack-iso...in ISO 25178-70 between Section 8.7 and 8.8 Analysis of the material measure

Measurement result of a confocal microscopy

Measurement result by

commercial confocal microscope

Size: 130 µm x 130 µm

Pixels: 1024 x 1024 pixels

A cross-sectional profile of the measured image

at the marked position

[email protected]

heig

ht / n

mh

eig

ht / n

m

position / µm

position / µm

ISO/TC 213 WG16, Sept 5th-6th, Tokyo, Japan

Page 9: Development of a material measure to characterize ...empir.npl.co.uk/3dstack/.../10/2018/05/3d-stack-iso...in ISO 25178-70 between Section 8.7 and 8.8 Analysis of the material measure

Reference measurement result by Met. LR-AFM

Measurement result by

PTB’s high speed metrological large range AFM

Size: 135 µm x 135 µm

Pixels: 1080 x 1080 pixels

(the pixel distance is set to the same

as that of the optical measurement device)

A cross-sectional profile of the measured image

at the marked position

0 20 40 60 80 100 120

heig

ht / n

m

-30

-20

-10

10

20

0

position / µm

heig

ht / n

m-30

-20

-10

20

30

0

10

70 80

position / µm50 60 90

[email protected]/TC 213 WG16, Sept 5th-6th, Tokyo, Japan

Page 10: Development of a material measure to characterize ...empir.npl.co.uk/3dstack/.../10/2018/05/3d-stack-iso...in ISO 25178-70 between Section 8.7 and 8.8 Analysis of the material measure

ITF

in d

B

Circular Chirp

Polar plot of instrument transfer function

fµm-1

[email protected]/TC 213 WG16, Sept 5th-6th, Tokyo, Japan

Page 11: Development of a material measure to characterize ...empir.npl.co.uk/3dstack/.../10/2018/05/3d-stack-iso...in ISO 25178-70 between Section 8.7 and 8.8 Analysis of the material measure

Circular Chirp

Angular Power Distribution

renameto powerdistributioninstead ofspectrum

ISO 25178-2

with this integration there is no spectrum

a function of angle s

[email protected]/TC 213 WG16, Sept 5th-6th, Tokyo, Japan

Page 12: Development of a material measure to characterize ...empir.npl.co.uk/3dstack/.../10/2018/05/3d-stack-iso...in ISO 25178-70 between Section 8.7 and 8.8 Analysis of the material measure

Circular Chirp

nm

confocal

[email protected]

Polar plot of angular power distribution

ISO/TC 213 WG16, Sept 5th-6th, Tokyo, Japan

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Acknowledgments

[email protected]

The work has received funding from the EMPIR programme co-financed by the

Participating States and from the European Union’s Horizon 2020 research and

innovation programme, 14IND07-3D Stack.

ISO/TC 213 WG16, Sept 5th-6th, Tokyo, Japan