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Renewable energies | Eco-friendly production | Innovative transport | Eco-efficient processes | Sustainable resources

IEA-GHG 2nd Post-Combustion Capture Conference

17th -20th September 2013, Bergen, Norway©20

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Demonstration of the DMXDemonstration of the DMXDemonstration of the DMXDemonstration of the DMX™™™™ processprocessprocessprocessdescription of the description of the description of the description of the OctaviusOctaviusOctaviusOctavius SP3 projectSP3 projectSP3 projectSP3 project

LudovicLudovicLudovicLudovic RaynalRaynalRaynalRaynal1111, Cristiana La Marca, Cristiana La Marca, Cristiana La Marca, Cristiana La Marca2222, Jan Mertens, Jan Mertens, Jan Mertens, Jan Mertens3333, , , , Laurent NormandLaurent NormandLaurent NormandLaurent Normand4444 and Paul Broutinand Paul Broutinand Paul Broutinand Paul Broutin1111

+ other colleagues !+ other colleagues !+ other colleagues !+ other colleagues !1111IFPEN, IFPEN, IFPEN, IFPEN, 2222ENEL,ENEL,ENEL,ENEL, 3333LABORELEC,LABORELEC,LABORELEC,LABORELEC, 4444PROSERNATPROSERNATPROSERNATPROSERNAT

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OutlookOutlookOutlookOutlook

� OctaviusOctaviusOctaviusOctavius projectprojectprojectproject

� DMXDMXDMXDMX™™™™ processprocessprocessprocess

� SP3 : Demonstration of the DMXSP3 : Demonstration of the DMXSP3 : Demonstration of the DMXSP3 : Demonstration of the DMX™™™™ processprocessprocessprocess

� Conclusions & future workConclusions & future workConclusions & future workConclusions & future work

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OCTAVIUS in Brief

� Optimisation of CO2 Capture Technology Allowing Verification and Implementation at Utility Scale

FP7 Project (Call DG Energy 2011)

� Start-up: 01/03/2012� Duration : 60 Months� Coordinator IFPEN

(Paul BROUTIN)� Total Budget: 13.56 M€� EU Funding: 7.96 M€

Kick-off Meeting on 13-14 March 2012 in Solaize

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17 Partners + 1 Sponsor

Sub-Project SP3 Sponsor: TOTAL (F)

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OCTAVIUS OrganisationOCTAVIUS OrganisationOCTAVIUS OrganisationOCTAVIUS Organisation

� 2 main technical Sub-Projects� SP2 dedicated to demonstration of operability and flexibility

aspects of first generation processes to be used for first full scale demo plant (ROAD and Porto Tolle Projects)

� SP3 dedicated to the demonstration of the DMXTM process

� 2 independent Subprojects

� a R&D Sub-Project� SP1 will support SP2 & SP3 and will also include cross-

cutting issues such as benchmarking activities

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OutlookOutlookOutlookOutlook

� OctaviusOctaviusOctaviusOctavius projectprojectprojectproject

� DMXDMXDMXDMX™™™™ processprocessprocessprocess

� SP3 : Demonstration of the DMXSP3 : Demonstration of the DMXSP3 : Demonstration of the DMXSP3 : Demonstration of the DMX™™™™ processprocessprocessprocess

� Conclusions & future workConclusions & future workConclusions & future workConclusions & future work

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PostPostPostPost----combustioncombustioncombustioncombustion capturecapturecapturecapture@ IFP Energies nouvelles@ IFP Energies nouvelles@ IFP Energies nouvelles@ IFP Energies nouvelles

� Development of new PCC processesDevelopment of new PCC processesDevelopment of new PCC processesDevelopment of new PCC processes� G1 : G1 : G1 : G1 : industrialindustrialindustrialindustrial pilot tests => pilot tests => pilot tests => pilot tests => commercializationcommercializationcommercializationcommercialization� HiCaptHiCaptHiCaptHiCapt++++™™™™ : 40 : 40 : 40 : 40 wtwtwtwt.% MEA + additives.% MEA + additives.% MEA + additives.% MEA + additives

� G2 : R&D G2 : R&D G2 : R&D G2 : R&D developmentsdevelopmentsdevelopmentsdevelopments => => => => industrialindustrialindustrialindustrial pilot testspilot testspilot testspilot tests� DMXDMXDMXDMX™™™™

� G3 : G3 : G3 : G3 : laboratorylaboratorylaboratorylaboratory studiesstudiesstudiesstudies –––– proof of conceptproof of conceptproof of conceptproof of concept� new new new new chemistrychemistrychemistrychemistry solventssolventssolventssolvents, , , , sorbentssorbentssorbentssorbents, hydrates..., hydrates..., hydrates..., hydrates...

� Development of new technologiesDevelopment of new technologiesDevelopment of new technologiesDevelopment of new technologies

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HiCapt+ process� Degradation testsDegradation testsDegradation testsDegradation tests

� very good performances of the oxidative inhibitorvery good performances of the oxidative inhibitorvery good performances of the oxidative inhibitorvery good performances of the oxidative inhibitor� Corrosion tests Corrosion tests Corrosion tests Corrosion tests

� Identification of materials with no corrosion in presence of theIdentification of materials with no corrosion in presence of theIdentification of materials with no corrosion in presence of theIdentification of materials with no corrosion in presence of theoxidative inhibitor (e.g. Duplex steel)oxidative inhibitor (e.g. Duplex steel)oxidative inhibitor (e.g. Duplex steel)oxidative inhibitor (e.g. Duplex steel)

� Price difference is very small (higher cost but less material siPrice difference is very small (higher cost but less material siPrice difference is very small (higher cost but less material siPrice difference is very small (higher cost but less material since nce nce nce better mechanical properties) + availability of material is indubetter mechanical properties) + availability of material is indubetter mechanical properties) + availability of material is indubetter mechanical properties) + availability of material is industrialstrialstrialstrial

0

5000

10000

15000

20000

25000

30000

none U2 V1 V2 Y1

Inhibitors (0,25%-wt)

Ani

on C

ance

ntra

tion

(pp

m)

0

50

100

150

200

250

300

350

400

U2 V1 V2 Y1

formiate

acetate

oxalate

nitrate

nitrite

MEA 40% at 80 C under air + CO2 during 12 days

0

5000

10000

15000

20000

25000

30000

none U2 V1 V2 Y1

Inhibitors (0,25%-wt)

Ani

on C

ance

ntra

tion

(pp

m)

0

50

100

150

200

250

300

350

400

U2 V1 V2 Y1

formiate

acetate

oxalate

nitrate

nitrite

MEA 40% at 80 C under air + CO2 during 12 days

MEA 30% at 80 C under air + CO2 during 7 days

0

1

2

3

4

5

6

7

8

0 20 40 60 80 100 120 140 160 180

Time (h)

NH

3 m

M/h

None

U1

U2

V1

V2

V3

W1

W2

W3

Y1

Y2

0.00

0.02

0.04

0.06

0.08

0.10

0.12

0.14

0 50 100 150

MEA 30% at 80 C under air + CO2 during 7 days

0

1

2

3

4

5

6

7

8

0 20 40 60 80 100 120 140 160 180

Time (h)

NH

3 m

M/h

None

U1

U2

V1

V2

V3

W1

W2

W3

Y1

Y2

0.00

0.02

0.04

0.06

0.08

0.10

0.12

0.14

0 50 100 150

MEA 40 wt % after 1000 h mini-pilot test (with and

without inhibitor)

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Pilot plant presentationMain Characteristics

CCS unit CCS unit CCS unit CCS unit –––– Main equipmentsMain equipmentsMain equipmentsMain equipments

� AbsorberAbsorberAbsorberAbsorber� ФФФФi = 1.5 m / HLT = 45 m� 3 stages solvent inlet

� StripperStripperStripperStripper� ФФФФi = 1.3 m / HLT = 31 m� Reboiler : Kettle type ~ 1 to 3 MWth

� Solvent / Solvent cross heat exchangerSolvent / Solvent cross heat exchangerSolvent / Solvent cross heat exchangerSolvent / Solvent cross heat exchanger� Plates type Plates type Plates type Plates type

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HiCapt+ main conclusionsLong run industrial pilot test main results (Long run industrial pilot test main results (Long run industrial pilot test main results (Long run industrial pilot test main results (EnelEnelEnelEnel –––– BrindisiBrindisiBrindisiBrindisi))))

� Test duration : Test duration : Test duration : Test duration : 380 h380 h380 h380 h� COCOCOCO2222 prod. :prod. :prod. :prod. : 2 327 kg/h2 327 kg/h2 327 kg/h2 327 kg/h� Efficiency :Efficiency :Efficiency :Efficiency : 89,7 %89,7 %89,7 %89,7 %� Loadings :Loadings :Loadings :Loadings : ααααL = 0,23 ���� ααααR = 0,48� Energy :Energy :Energy :Energy : ~ 3,02 GJ/t~ 3,02 GJ/t~ 3,02 GJ/t~ 3,02 GJ/tCO2 CO2 CO2 CO2 � in good agreement with process simulationsin good agreement with process simulationsin good agreement with process simulationsin good agreement with process simulations

Long run miniLong run miniLong run miniLong run mini----pilot test main results (IFPEN)pilot test main results (IFPEN)pilot test main results (IFPEN)pilot test main results (IFPEN)� use of additivesuse of additivesuse of additivesuse of additives� no or little degradationno or little degradationno or little degradationno or little degradation� much lower emissionsmuch lower emissionsmuch lower emissionsmuch lower emissions� no corrosion with Duplex (even in hot regions)no corrosion with Duplex (even in hot regions)no corrosion with Duplex (even in hot regions)no corrosion with Duplex (even in hot regions)

ready for commercialization

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DMX™

AB

SOR

BE

R

STR

IPPE

R

Decanter

Flue Gas

Gas Treated

CO2 lean amine

Rich amine

Lean amine

CO2 richamine

LP CO2

Reboiler

Leanamine

HP CO2

CO2

CO2 lean phase

CO2 rich phase

DMXDMXDMXDMX----1111™™™™ : a : a : a : a lowlowlowlow stripping, stripping, stripping, stripping, lowlowlowlow heatheatheatheat of of of of reactionreactionreactionreaction, , , , highhighhighhigh capacitycapacitycapacitycapacity demixingdemixingdemixingdemixing solventsolventsolventsolvent

+ + + + lowerlowerlowerlower degradationdegradationdegradationdegradation (and (and (and (and furtherfurtherfurtherfurther lowerlowerlowerloweremissionsemissionsemissionsemissions => => => => interestinterestinterestinterest in HP stripper) // in HP stripper) // in HP stripper) // in HP stripper) // no corrosionno corrosionno corrosionno corrosion

2.5 – 2.1 GJ/ton CO 2(-38% min in Qreb)-20-30 % in CO 2 total cost

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Scientific & Technical information� VLE data + VLE data + VLE data + VLE data + adaptedadaptedadaptedadapted thermodynamicthermodynamicthermodynamicthermodynamic modelmodelmodelmodel� DegradationDegradationDegradationDegradation / Corrosion/ Corrosion/ Corrosion/ Corrosion� OperationalOperationalOperationalOperational issuesissuesissuesissues� KineticsKineticsKineticsKinetics & Mass & Mass & Mass & Mass transfertransfertransfertransfer performancesperformancesperformancesperformances� MiniMiniMiniMini----pilot testspilot testspilot testspilot tests� ProcessProcessProcessProcess simulations / simulations / simulations / simulations / costcostcostcost evaluationsevaluationsevaluationsevaluations

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1

20

11

C102

E106

E101E

10

E104

22

V101A

C101

T101

Amine makeup

V2

17

18

13

12

V103E102

212

222

E105V102

24

K201ACOMP

14

25

3

E101A

6

5

14

P101

162

P104

K101

C100

E301

P301

P302

4

5b

6b

V101C

P102

P102

P101

E102

Water makeup

To Water makeup

P303

P304

4.6 bar

7.97.7

V1

7

V3

DMX-1 Process – Full Scale Unit PFD

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Steam Cycle Simulation: IFPEN model� Temperature and pressure levels availableTemperature and pressure levels availableTemperature and pressure levels availableTemperature and pressure levels available

T=602°°°°CP=278 bar

T=410°°°°CP=90 bar

T=600°°°°CP=56.8 bar

T=462°°°°CP=24.3 bar

T=377°°°°CP=13.4 bar

T=355°°°°CP=61.4 bar

T=285°°°°CP=6.5 bar

T=189°°°°CP=2.7 bar

T=105°°°°CP=1.09 bar

T=67°°°°CP=0.27 bar

T=27°°°°CP=0.035 bar

Thermodynamic model: ASME 1967 steam table correlationsHeat Exchanger pinch: 5 °C, pressure drop neglected

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OutlookOutlookOutlookOutlook

� OctaviusOctaviusOctaviusOctavius projectprojectprojectproject

� DMXDMXDMXDMX™™™™ processprocessprocessprocess

� SP3 : Demonstration of the DMXSP3 : Demonstration of the DMXSP3 : Demonstration of the DMXSP3 : Demonstration of the DMX™™™™ processprocessprocessprocess

� Conclusions & future workConclusions & future workConclusions & future workConclusions & future work

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- Process testing

- Analytical methodologies

development

- Performance testing

- Validation of design

- Emissions measurement and

waste characterization

- Development and testing

modeling tools

• Criteria for technology scale-up

• Full scale application Capex and

Opex evaluation (cost of CO2

avoided)

• Basic engineering

Flue gases : 10.000 Nm 3/hCO2 : 2500 kg/h

Full scale -feasibility study

PilotLab

MethodologyFrom lab to Pilot demonstration

Process modeling - Process Design

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SP3 Structure & ObjectivesSP3 Structure & ObjectivesSP3 Structure & ObjectivesSP3 Structure & Objectives

WP 3.1

Definition of the Brindisipilot plant revamping

WP 3.2

Retrofit of the Brindisi pilot

plant

WP 3.3

Demonstration of the DMX

process

WP 3.4

DMX Evaluation for PC case

WP 3.5

DMX evaluation for NGCC case

SP 3: Demonstration of the DMX TM process

� The main objective of SP3 is to demonstrate the DMX TM process on pilot scale and study its application to coal power station and NGCC units with industrial pilot test on the Enel’s coal fired power plant of Brindisi.

SP3 Objectives

Go / NoGo decision11th Dec. 2013

Technical Criteria:�energy consumption�solvent degradation and emission�main component design criteria�HSE�Capex and Opex of full scale application

Financial Criteria: cost of retrofit

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SP3 Work Packages Description SP3 Work Packages Description SP3 Work Packages Description SP3 Work Packages Description –––– WP3.1WP3.1WP3.1WP3.1

Participants: IFPEN, Enel, Laborelec/GDF SUEZ, ProsernatParticipants: IFPEN, Enel, Laborelec/GDF SUEZ, Prosernat

WP 3.1: Definition of the Brindisi pilot plant revam ping

Objectives

• Define modifications to be carried out on Enel Brindisi CO2 capture pilot plant to test DMX• Design and Estimate the cost of the pilot revamping

Task

• 3.1.1 Experimentation of DMX on Enel minipilot at Brindisi lab facilities and at IFPEN research centre• 3.1.2 Experimentation at IFPEN on decantation rate on a representative cold mock-up• 3.1.3 Preliminary process study– full scale case • 3.1.4 FEED for Enel CO2 capture pilot plant revamping• 3.1.5 Cost estimation of revamping

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IFPEN mini-pilot

�Mechanical/validation tests : T1 2013

�operation with SOx/NOx

�Long run tests on MEA (reference case) : 1000 hrs

� Long run tests on DMX : in progress

�operation on a 24/7 basis

IFPEN Lab test

Lab & Minipilot activities Lab & Minipilot activities Lab & Minipilot activities Lab & Minipilot activities –––– IFPEN IFPEN IFPEN IFPEN

Target :

�Demixing test to decanter design

�Capture efficiency (lean and reach loadings)

�Solvent degradation

�Emission

�Corrosion

� VLE data + adapted thermodynamic model

� Degradation / Corrosion and other

operational issues

� Kinetics & Mass transfer performances

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Minipilot activities Minipilot activities Minipilot activities Minipilot activities ---- Enel miniEnel miniEnel miniEnel mini----pilotpilotpilotpilot

Brindisi pilot:

Sensitivity test: to optimize the mini-pilot plant

operating conditions

Long run test: focused on the study of solvent’s

degradation / emissions in the optimized

conditions.

Flue gas conditionBrindisi pilot:

Emissions measurements: participation of

Laborelec via FTIR measurements (with

calibration at IFPEN)

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Full scale application and costingFull scale application and costingFull scale application and costingFull scale application and costing

� Assessment of the energy consumption :Assessment of the energy consumption :Assessment of the energy consumption :Assessment of the energy consumption :� Process scheme definition (steam turbine and capture process): Process scheme definition (steam turbine and capture process): Process scheme definition (steam turbine and capture process): Process scheme definition (steam turbine and capture process):

� Definition of the steam turbine scheme and optimization for the Definition of the steam turbine scheme and optimization for the Definition of the steam turbine scheme and optimization for the Definition of the steam turbine scheme and optimization for the two casestwo casestwo casestwo cases� Simulation and evaluation of the impact on the thermal cycle forSimulation and evaluation of the impact on the thermal cycle forSimulation and evaluation of the impact on the thermal cycle forSimulation and evaluation of the impact on the thermal cycle for each capture each capture each capture each capture

processprocessprocessprocess� CAPEX and OPEX estimation:CAPEX and OPEX estimation:CAPEX and OPEX estimation:CAPEX and OPEX estimation:

� Definition of the method Definition of the method Definition of the method Definition of the method � Cost estimation with accuracy Cost estimation with accuracy Cost estimation with accuracy Cost estimation with accuracy ±±±± 30% 30% 30% 30% ----

� Parameterization:Parameterization:Parameterization:Parameterization:� LCOELCOELCOELCOE� Cost of CO2 avoidedCost of CO2 avoidedCost of CO2 avoidedCost of CO2 avoided

Preliminary process study for application on a 660 M We power plant, comparison between two cases:

�MEA 30% (benchmarking) � DMX

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FEED study for EnelFEED study for EnelFEED study for EnelFEED study for Enel’’’’s pilot revampings pilot revampings pilot revampings pilot revamping

� PrePrePrePre----FEED in 2013 with strong interaction between FEED in 2013 with strong interaction between FEED in 2013 with strong interaction between FEED in 2013 with strong interaction between Enel / IFPEN / Prosernat teams Enel / IFPEN / Prosernat teams Enel / IFPEN / Prosernat teams Enel / IFPEN / Prosernat teams

� FEED : Enel engineering + Prosernat with support FEED : Enel engineering + Prosernat with support FEED : Enel engineering + Prosernat with support FEED : Enel engineering + Prosernat with support of IFPENof IFPENof IFPENof IFPEN

� KickKickKickKick----Off Meeting in Milan (28Off Meeting in Milan (28Off Meeting in Milan (28Off Meeting in Milan (28thththth May 2013) May 2013) May 2013) May 2013) � basis of design� Heat and Mass Bances� PFD – PID� piping classes� list of chemicals� Process Data Sheets of main/retrofitted equipments� Instrument list + controls� Plot plan� Operating manual� Cost estimation

� HAZOP meeting (30HAZOP meeting (30HAZOP meeting (30HAZOP meeting (30thththth Sept. 2Sept. 2Sept. 2Sept. 2ndndndnd Oct. 2013)Oct. 2013)Oct. 2013)Oct. 2013)

� Final documents for NovemberFinal documents for NovemberFinal documents for NovemberFinal documents for November

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OutlookOutlookOutlookOutlook

� OctaviusOctaviusOctaviusOctavius projectprojectprojectproject

� DMXDMXDMXDMX™™™™ processprocessprocessprocess

� SP3 : Demonstration of the DMXSP3 : Demonstration of the DMXSP3 : Demonstration of the DMXSP3 : Demonstration of the DMX™™™™ processprocessprocessprocess

� Conclusions & future workConclusions & future workConclusions & future workConclusions & future work

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Conclusions & perspectives� ConclusionsConclusionsConclusionsConclusions

� HiCaptHiCaptHiCaptHiCapt+ : a G1 demonstrated process (MEA 40wt.% + + : a G1 demonstrated process (MEA 40wt.% + + : a G1 demonstrated process (MEA 40wt.% + + : a G1 demonstrated process (MEA 40wt.% + proprietary oxidation inhibitor + material recommendation)proprietary oxidation inhibitor + material recommendation)proprietary oxidation inhibitor + material recommendation)proprietary oxidation inhibitor + material recommendation)

� DMXDMXDMXDMX----1111™™™™ : a promising G2 process under development for : a promising G2 process under development for : a promising G2 process under development for : a promising G2 process under development for reducing energy penaltyreducing energy penaltyreducing energy penaltyreducing energy penalty

� long duration minilong duration minilong duration minilong duration mini----pilot tests + FEED study for pilot tests + FEED study for pilot tests + FEED study for pilot tests + FEED study for EnelEnelEnelEnel’’’’ssss pilot pilot pilot pilot retrofit under progress retrofit under progress retrofit under progress retrofit under progress

� Future stepsFuture stepsFuture stepsFuture steps� OctaviusOctaviusOctaviusOctavius EU project EU project EU project EU project ---- Go/Go/Go/Go/NoGoNoGoNoGoNoGo milestone Dec. 2013 milestone Dec. 2013 milestone Dec. 2013 milestone Dec. 2013

(technical (technical (technical (technical –––– financial criteria)financial criteria)financial criteria)financial criteria)� tests of DMXtests of DMXtests of DMXtests of DMX----1 on 1 on 1 on 1 on Enel'sEnel'sEnel'sEnel's BrindisiBrindisiBrindisiBrindisi industrial pilot for further industrial pilot for further industrial pilot for further industrial pilot for further

evaluation on full scale cases evaluation on full scale cases evaluation on full scale cases evaluation on full scale cases –––– tests in 2015tests in 2015tests in 2015tests in 2015----2016201620162016� process ready for commercialization T1 2017process ready for commercialization T1 2017process ready for commercialization T1 2017process ready for commercialization T1 2017

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ThankThankThankThank youyouyouyou !!!!Ludovic.Raynal@ifpen.frLudovic.Raynal@ifpen.frLudovic.Raynal@ifpen.frLudovic.Raynal@ifpen.fr