Conference Agenda The Second International Process ... · Daniela Lavric1, Uroš Novak2,3, Polona Žnidaršič-Plazl2 1: Corning S.A.S. Corning European Technology Center; 2: University

Conference Agenda

The Second International Process Intensification Conference (IPIC2)

Date: Monday, 27/May/2019

8:15am Registration Location: MTC 00.03

9:00am -

9:20am

Welcome & WP Awards Location: Grote Aula

9:20am -

10:05am

Session 1 Plenary: Prof. Dr. Andrzej Stankiewicz, TU Delft, Netherlands - The missing link unearthed: materials and process intensification Location: Grote Aula Chair: Tom Van Gerven

The Missing Link Unearthed: Materials and Process Intensification Andrzej Stankiewicz1, Peng Yan2 1: TU Delft Process Technology Institute, The Netherlands; 2: School of Chemical Engineering and Technology, National Engineering Research Center of Distillation Technology, Collaborative Innovation Center of Chemical Science and Engineering (Tianjin), Tianjin University, Tianjin 300072, China

10:05am -

10:35am

Coffee break Location: MTC 00.03

Poster sessionLocation: MTC 00.03

Rapid prototyping through 3D printing as a tool for achieving intensified electrolyzer designs Stéphane Jean-Marie Christian Weusten1, Mattheus de Groot1,2, John van der Schaaf1 1: Department of Chemical Engineering and Chemistry, TU Eindhoven, P.O.Box 513 , 5600 MB Eindhoven, the Netherlands; 2: Nouryon, Christian Neefestraat 2, 1077 WW Amsterdam, the Netherlands

Cavitation Bubble Cluster Dynamics: Averaged vs. Coupled Models Dwayne Stephens, Robert Mettin University of Goettingen, Germany

Intensification of a chemical reactor for methanol synthesis through forced periodic operations - Evaluation based on Nonlinear Frequency Response Analysis Daliborka Nikolic Paunic1, Carsten Seidel2, Achim Kienle2,3, Andreas Seidel-Morgenstern2,3, Menka Petkovska4 1: Institute of Chemistry, Technology and Metallurgy, Serbia; 2: Otto-von-Guericke-University, Germany; 3: Max-Planck-Institute for Dynamics of Complex Technical Systems, Germany; 4: Faculty of Technology and Metallurgy, University of Belgrade, Serbia

Microwave radiation to intensify the hydroxymethylfurfural production from cellulose Nick Sweygers, Raf Dewil, Lise Appels KU Leuven, Belgium

Sorption-enhanced alcohol promoted liquid-phase methanol synthesis from CO2 and H2: A kinetic study

Arto Laari, Harri Nieminen, Tuomas KoiranenLUT University, Finland

Influence of surface wettability of the surface-modified stainless steel wire mesh packing on mass transfer performance in a rotating packed bed Meng-Jun Su, Yong Luo, Guang-Wen Chu, Jian-Feng Chen Research Center of the Ministry of Education for High Gravity Engineering Technology, Beijing University of Chemical Technology, Beijing 100029, PR China

Liquid-liquid mass transfer in continuous compact reactors Marwa Saïd, Nathalie Di Miceli Raimondi, Michel Cabassud, Christophe Gourdon Université de Toulouse, France

Process intensification on the vapor-liquid mass transfer process: From Microwave irradiations, Foam materials to Process integration Xin Gao, Hong Li, Xingang Li School of Chemical Engineering and Technology, National Engineering Research Center of Distillation Technology, Tianjin University, China

Characterization of cavitation bubble size distribution during sonication in a milliflow reactorJeroen Jordens, Thomas Matthys, Tom Van Gerven KU Leuven, Belgium

Development of a microalgae biocomposite-integrated Spinning Disc Bioreactor (SDBR) for bioprocess intensification of light-driven CO2 absorption Kamelia Boodhoo1, Thea Ekins-Coward1, Sharon Velasquez-Orta1, Michael Flickinger2,3 1: School of Engineering, Newcastle University, United Kingdom; 2: Chemical and Biomolecular Engineering, North Carolina State University, Raleigh, North Carolina, USA; 3: Golden LEAF Biomanufacturing Training and Education Center, BTEC, North Carolina State University, Raleigh, North Carolina, USA

A Computational Study of Microwave Heating of Reactive Multiphase Systems Himanshu Goyal, Dionisios G Vlachos University of Delaware, United States of America

Detailed Analysis of an Improved Packing Design for Distillation in Rotating Packed Beds Hina Qammar1, Konrad Gladyszewski1,2, Yutong Li1, Mirko Skiborowski1, Andrzej Górak1,2 1: TU Dortmund University, Germany; 2: Lodz University of Technology, Poland

Effect of process parameters on a novel modular continuous crystallizer Nnaemeka Ezeanowi1,2, Tuomas Koiranen1 1: School of Engineering Science, Lappeenranta University of Technology, P.O. Box 20, FIN-53851 Lappeenranta, Finland; 2: Sonotecc Oy, Laululinnuntie 18A, 00780 Helsinki, Finland

Efficient water treatment with a novel 3D printed microbubbles aerator Dmitry Vladimirovich Gradov1, Andrey Saren1, Janne Kauppi2, Kari Ullakko1, Tuomas Koiranen1 1: Lappeenranta University of Technology, Finland; 2: Outotec (Filters) Oy, Outotec dewatering technology center, Finland

Microwave-induced process intensification for Vapor-Liquid mass transfer separation process Xiaoqi Lv, Hong Li, Xin Gao Tianjin University, China, People's Republic of

Reactive Distillation: a Successful Story of Process Intensification Applied in Chemical Process Industries Jiaying Wang, Hong Li, Xin Gao Tianjin University, China, People's Republic of

Precipitation of calcium carbonate in highly alkaline solution through carbonated water Soheil Aghajanian, Harri Nieminen, Tuomas Koiranen LUT University, Finland

Oscillatory Baffled Column with Particles Present in Heat Transfer Intensification Zhongyi Yan, Huidong Zheng Fuzhou University, China, People's Republic of

Transition and scale up from batch to inline rotor-stator for microencapsulation Sven Gobert1, Roberto F.A. Teixeira2, Simon Kuhn1, Leen Braeken1, Leen C.J. Thomassen1 1: KULeuven, Belgium; 2: Devan Chemicals

Continuous Crystallization in Microfluidic Devices Naghmeh Fatemi, Zhengya Dong, Tom Van Gerven, Simon Kuhn Department of Chemical Engineering, KU Leuven, Celestijnenlaan 200F, 3001 Leuven, Belgium

Experimental heat transfer studies in heat exchanger reactor with millimetric square channels Hanbin SHI, Nathalie DI MICELI RAIMONDI, Michel CABASSUD, Christophe GOURDON

Laboratoire de Génie Chimique (LGC), France

Batch to Continuous processes: a sensitivity analysis Federico Florit1, Giuseppe Storti2, Renato Rota1 1: Politecnico di Milano, Department of Chemistry, Materials and Chemical Engineering “Giulio Natta”, piazza L. da Vinci 32, 20133, Milan, Italy; 2: ETH Zürich, Department of Chemistry and Applied Biosciences, Vladimir-Prelog-Weg 1-5/10, HCI F 125, 8093 Zürich, Switzerland

Scaling up of microstructured metallic foam application in water disinfection Jinghan Zhao, Peihua Yan, Benjamin Snow, Emily Yi Wai Chiang, Rafael M. Santos University of Guelph, Canada

The direct coupling of a continuous flow assisted reaction with a seedless continuous flow tubular crystalliser Jean Septavaux, Bart Rimez, Benoit Scheid Université Libre de Bruxelles, Belgium

Anti-fouling strategies for tubular flow crystallizersArne Vancleef1, Tom Van Gerven2, Leen Thomassen1,2, Leen Braeken1,2 1: Faculty of Engineering Technology, KU Leuven, Agoralaan building B box 8, 3590 Diepenbeek, Belgium; 2: Department of Chemical Engineering, KU Leuven, Celestijnenlaan 200F Box 2424, 3001 Leuven, Belgium

Continuous synthesys of galactooligosacharides in liquid-solid oscillatory flow reactor Danijela Slavnić, Milica Carević, Dejan Bezbradica, Nikola Nikacevic University of Belgrade, Faculty of Technology and Metallurgy, Serbia

Process intensification of sustainable quaternary ammonium salts production through temperature elevation: using thermogravimetric analysis to determine thermal stability and degradation kinetic rates Roel Kleijwegt1, Wyatt Winkenwerder2, John Van Der Schaaf1 1: Eindhoven University of Technology, Netherlands, The; 2: Nouryon

Study of the Continuous Gelation Process of Non-aqueous Carbopol Gels Simona Migliozzi, Luca Mazzei, Panagiota Angeli University College London, United Kingdom

Specialty monomers synthesis by ultrasound assisted oxidative cleavage

Ana Luisa Maria1,3, Jean-Luc Couturier1, Jean-Luc Dubois2, Giancarlo Cravotto3 1: 14 Chemin Henri Moissan, 69310 Pierre Bénite France; 2: Arkema, Colombes, 92700 FRANCE; 3: Università Degli Studi Di Torino - UNITO, Torino, 10125 ITALY

An Extractive Desulfurization Process Intensified by Water-based Deep Eutectic Solvent Chongyang Liu, Hongye Cheng, Zhiwen Qi East China University of Science and Technology, China, People's Republic of

Two-step procedure for Catellani functionalization of electron-deficient phenols Vidmantas Bieliūnas, Wim M. De Borggraeve KU Leuven, Belgium

Intensified flow separator infrastructure and expertise for the materials industry Jean Paul Gueneau de Mussy, Jeroen Jordens, Tom Van Gerven KU Leuven, Belgium

Optimisation and scale-up of a continuous synthesis in Corning® AFRTM of isoamyl acetate catalysed by lipase B catalysis in a two-liquid phase system Daniela Lavric1, Uroš Novak2,3, Polona Žnidaršič-Plazl2 1: Corning S.A.S. Corning European Technology Center; 2: University of Ljubljana; 3: National Institute of Chemistry

Application of optical fiber particle velocity and concentration in-line measurement technology Weipeng Zhang1,2,3, Chao Yang1,2, Xiangyang Li1,2, Guozheng Li1 1: Key Laboratory of Green Process and Engineering, Institute of Process Engineering, Chinese Academy of Sciences, Beijing 100190, China; 2: School of Chemical Engineering, University of Chinese Academy of Sciences, Beijing 100049, China; 3: Nanjing Jiuzhang Chemical Technology Co., Ltd., Nanjing 211800, China

Numerical simulation of micro-mixing in a solid-liquid stirred tank with E-model coupled with CFD Xiaoxia Duan1,2, Xin Feng1,2, Chao Yang1,2, Zaisha Mao1 1: Institute of Process Engineering, Chinese Academy of Science, Beijing 100190, China; 2: School of Chemical Engineering, University of Chinese Academy of Sciences,Beijing 100049, China

10:35am -

11:55am

S1 Group 1: Scale-up Location: Grote Aula Chair: Mumin Enis Leblebici 10:35am - 10:55am

Intensification and scale-up of a solvent extraction process using a modular flow distributo Eduardo Garciadiego Ortega, Dimitrios Tsaoulidis, Panagiota Angeli University College London, United Kingdom

S1 Group 2: Energy activation (Ultrasound) Location: Kleine Aula Chair: Tom Van Gerven 10:35am - 10:55am

Biorefinery process intensified by ultrasound and ozone for lipids, proteins, carbohydrates and phosphorus recovery from microalgae biomass cultivated in wastewater

10:55am - 11:15am

Numbering-up Module of Metal Microreactor for Scale-up Drug Production Gwang-Noh Ahn1, Tae-Jong Yu2, Hyune-Jea Lee1, Ki-Won Gyak1, Donghyun You2, Dong-Pyo Kim1 1: Center of Intelligent Microprocess for Pharmaceutical Synthesis, Department of Chemical Engineering, Pohang University of Science and Technology, Environ. Eng. Bldg., San 31, Hyoja-dong, Nam-gu, Pohang, South Korea; 2: Department of Mechanical Engineering, Pohang University of Science and Technology, Mechanical Eng. Bldg., San 31, Hyoja-dong, Nam-gu, Pohang, South Korea

11:15am - 11:35am

The HANU-reactor: The Development of a Scalable Continuous-flow Photoreactor Hannes P. L. Gemoets1, Wouter Debrouwer2, Koen Van Aken1 1: Creaflow, Belgium; 2: Ecosynth, Belgium

11:35am - 11:55am

Scaling-up Chemical Production by Portable Pharm micro-Plant on a Pad: Continuous-flow Synthesis of organophosphates As Key structrual Motifs of Drugs. Bandaru T.Ramanjaneyulu, Sejun Yim, Vidyacharan Shinde, Dong-Pyo Kim POSTECH, Korea, Republic of (South Korea)

R.M. Gonzalez-Balderas1, S.B. Velásquez-Orta2, M.T. Orta Ledesma1 1: Instituto de Ingeniería, Coordinación de Ingeniería Ambiental, Universidad Nacional Autónoma de México UNAM, Circuito Escolar s/n, Ciudad Universitaria, Delegación Coyoacán, México, CDMX., C.P. 04510.; 2: School of Chemical Engineering and Advanced Materials, Newcastle University, Circuito Escolar s/n, Ciudad Universitaria, Delegación Coyoacán, México, CDMX., C.P. 04510

10:55am - 11:15am

The simultaneous application of high and low frequency ultrasound for managing solids in microreactors Zhengya Dong, Aniket Pradip Udepurkar, Simon Kuhn KU Leuven, Belgium

11:15am - 11:35am

Sonochemical synthesis of mixed oxides Daria Camilla Boffito1, Zahra Khani1, Dalma Schieppati1, Federico Galli2, Claudia Letizia Bainchi2 1: Polytechnique Montreal; 2: University of Milan

11:35am - 11:55am

Impact of ultrasound on two-phase flow in a microchannel Jinu Joseph John, Simon Kuhn, Tom Van Gerven KU Leuven, Belgium

11:55am -

12:45pm

Lunch break Location: MTC 00.03






Sorption-enhanced alcohol promoted liquid-phase methanol synthesis from CO2 and H2: A kinetic study Arto Laari, Harri Nieminen, Tuomas Koiranen LUT University, Finland






A Computational Study of Microwave Heating of Reactive Multiphase Systems Himanshu Goyal, Dionisios G Vlachos

University of Delaware, United States of America









Continuous Crystallization in Microfluidic Devices

Naghmeh Fatemi, Zhengya Dong, Tom Van Gerven, Simon Kuhn Department of Chemical Engineering, KU Leuven, Celestijnenlaan 200F, 3001 Leuven, Belgium

Experimental heat transfer studies in heat exchanger reactor with millimetric square channels Hanbin SHI, Nathalie DI MICELI RAIMONDI, Michel CABASSUD, Christophe GOURDON Laboratoire de Génie Chimique (LGC), France




Anti-fouling strategies for tubular flow crystallizersArne Vancleef1, Tom Van Gerven2, Leen Thomassen1,2, Leen Braeken1,2 1: Faculty of Engineering Technology, KU Leuven, Agoralaan building B box 8, 3590 Diepenbeek, Belgium; 2: Department of Chemical Engineering, KU Leuven, Celestijnenlaan 200F Box 2424, 3001 Leuven, Belgium




Specialty monomers synthesis by ultrasound assisted oxidative cleavage Ana Luisa Maria1,3, Jean-Luc Couturier1, Jean-Luc Dubois2, Giancarlo Cravotto3 1: 14 Chemin Henri Moissan, 69310 Pierre Bénite France; 2: Arkema, Colombes, 92700 FRANCE; 3: Università Degli Studi Di Torino - UNITO, Torino, 10125 ITALY






Numerical simulation of micro-mixing in a solid-liquid stirred tank with E-model coupled with CFD Xiaoxia Duan1,2, Xin Feng1,2, Chao Yang1,2, Zaisha Mao1 1: Institute of Process Engineering, Chinese Academy of Science, Beijing 100190, China; 2: School of Chemical

Engineering, University of Chinese Academy of Sciences,Beijing 100049, China

12:45pm -

1:30pm

Session 2 Plenary: Prof. Dr. Klavs Jensen, MIT, USA - Intensification of chemical processes by integrating flow chemistry, automation, and machine learning Location: Grote Aula Chair: Simon Kuhn

Intensification of chemical processes by integrating flow chemistry, automation, and machine learning.Klavs F. Jensen MIT, United States of America

1:30pm -

3:10pm

S2.1 Group 1: Microreactors Location: Grote Aula Chair: Simon Kuhn 1:30pm - 1:50pm

Process Intensification through Microreactor Technology Igor Plazl University of Ljubljana, Slovenia

1:50pm - 2:10pm

Microreactors, a versatile tool in process intensification to produce high quality nanomaterials in continuous flow Victor Sebastian1,2, Isabel Ortiz de Solorzano1, Laura Uson1,2, Manuel Arruebo1,2 1: University of Zaragoza, Spain; 2: Networking Research Center CIBER-BBN

2:10pm - 2:30pm

Investigations of gas-liquid mass transfer around Taylor bubbles flowing in a long in-plane spiral-shaped milli-reactor Mei MEI2, Nicolas DIETRICH2, Gilles HEBRARD2, Karine LOUBIERE1 1: Laboratoire de Génie Chimique (LGC), Université de Toulouse, CNRS, INPT, UPS, Toulouse, France; 2: Laboratoire d'Ingénierie des Systèmes Biologiques et des Procédés (LISBP), Université de Toulouse, INRA, INSA, Toulouse, France

2:30pm - 2:50pm

Process Intensification of CO2 Photocatalytic Reduction Abdullahi Adamu, Fernando Russo Abegão, Kamelia Boodhoo Newcastle University, United Kingdom

S2.1 Group 2: COSMIC session Location: Kleine Aula Chair: Tuomas Koiranen 1:30pm - 1:50pm

Study of the ultrasound irradiation time and periodicity on the synthesis of zeolite FAU for its use in a continuous process Heidy Ramirez Mendoza1,2, Sylvain Lannote1, Jeroen Jordens2, Tom Van Gerven2, Serge Nicolas1, Mafalda Valdez1, Cécile Lutz1 1: Arkema GRL; 2: KU Leuven

1:50pm - 2:10pm

Innovative techniques for the synthesis of stable silver nanoclusters Roberta Manno, Victor Sebastian, Reyes Mallada, Jesus Santamaria University of Zaragoza, Spain

2:10pm - 2:30pm

Continuous synthesis of ferromagnetic iron oxide nanoparticles for magnetic hyperthermia using a droplet reactor with controlled reducing environment Luca Panariello, Gaowei Wu, Maximilian O. Besenhard, Asterios Gavriilidis UCL, United Kingdom

2:30pm - 2:50pm

Ultrasound-assisted anti-solvent crystallization in milli-flow crystallizer: Aspirin as model compound Mohammed Noorul Hussain, Jeroen Jordens, Jinu Joseph John, Leen Braeken, Tom Van Gerven Department of Chemical Engineering, KU Leuven, 3001 Leuven, Belgium

2:50pm - 3:10pm

Scale-up of an ultrasonic milli-reactor for continuous flow precipitation reactions Claire Delacour1, Cecile Lutz2, Simon Kuhn1 1: KU Leuven, Department of Chemical Engineering, Belgium; 2: Service Adsorption, ARKEMA, Groupement de recherche de Lacq, France

3:10pm -

3:40pm



Rapid prototyping through 3D printing as a tool for achieving intensified electrolyzer designs Stéphane Jean-Marie Christian Weusten1, Mattheus de Groot1,2, John van der Schaaf1

1: Department of Chemical Engineering and Chemistry, TU Eindhoven, P.O.Box 513 , 5600 MB Eindhoven, the Netherlands; 2: Nouryon, Christian Neefestraat 2, 1077 WW Amsterdam, the Netherlands















Reactive Distillation: a Successful Story of Process Intensification Applied in Chemical Process Industries Jiaying Wang, Hong Li, Xin Gao

Tianjin University, China, People's Republic of









Anti-fouling strategies for tubular flow crystallizers

Arne Vancleef1, Tom Van Gerven2, Leen Thomassen1,2, Leen Braeken1,2 1: Faculty of Engineering Technology, KU Leuven, Agoralaan building B box 8, 3590 Diepenbeek, Belgium; 2: Department of Chemical Engineering, KU Leuven, Celestijnenlaan 200F Box 2424, 3001 Leuven, Belgium








Optimisation and scale-up of a continuous synthesis in Corning® AFRTM of isoamyl acetate

catalysed by lipase B catalysis in a two-liquid phase system Daniela Lavric1, Uroš Novak2,3, Polona Žnidaršič-Plazl2 1: Corning S.A.S. Corning European Technology Center; 2: University of Ljubljana; 3: National Institute of Chemistry


Numerical simulation of micro-mixing in a solid-liquid stirred tank with E-model coupled with CFD Xiaoxia Duan1,2, Xin Feng1,2, Chao Yang1,2, Zaisha Mao1 1: Institute of Process Engineering, Chinese Academy of Science, Beijing 100190, China; 2: School of Chemical Engineering, University of Chinese Academy of Sciences,Beijing 100049, China

3:40pm -

5:20pm

S2.2 Group 1: Multifunctional reactors & hybrid separatorLocation: Grote Aula Chair: Michel Cabassud 3:40pm - 4:00pm

Reactive Extraction for Long-chain Ester Formation Intensified by Bifunctional Ionic LiquidsHao Qin, Qian Zeng, Hongye Cheng, Zhiwen Qi East China University of Science and Technology, China, People's Republic of

4:00pm - 4:20pm

Optimization-based design and evaluation of dividing wall columns Thomas Waltermann, Steffen Sibbing, Mirko SkiborowskiDepartment of Biochemical and Chemical Engineering, TU Dortmund, Germany

4:20pm - 4:40pm

Optimal feed locations of reactive distillation columns based on different boiling point rankings in quaternary systems Rahma Muthia1, Aloijsius G. J. van der Ham2, Megan Jobson1, Anton A. Kiss1,2 1: The University of Manchester, United Kingdom; 2: University of Twente, The Netherlands

4:40pm - 5:00pm

Photochemical Intensification with a Rotor-Stator Spinning Disk Reactor Parimala Shivaprasad1,2, Koen Kuijpers1, Arnab Chaudhuri1, Emma Emanuelsson2, Timothy Noël1, John van der Schaaf1 1: TU Eindhoven; 2: University of Bath, United Kingdom

S2.2 Group 2: COSMIC session Location: Kleine Aula Chair: Daria Boffito 3:40pm - 4:00pm

Green approach to copper catalyzed reduction of nitro and alkyne under hydride free condition Maria Jesus Moran Plata, Katia Martina, Giancarlo Cravotto University of Turin, Italy

4:00pm - 4:20pm

From batch to continuous flow: a life cycle assessment of gold nanoparticles production Fabio Grimaldi, Martina Pucciarelli, Asterios Gavriilidis, Paola Lettieri University College London, United Kingdom

4:20pm - 4:40pm

Sonochemistry and Bubble Dynamics in Small Channels Busra Ekim Sarac1, Julian Eisener1, Carlos Cairós2, Robert Mettin1 1: University of Goettingen, Germany; 2: University of La Laguna, Spain

4:40pm - 5:00pm

Leaching Stable Phosphine-Based Heterogeneous Catalyst for Dearomatization: Direct access to Spiroindol(en)ines from Batch to Continuous-Flow* Prabhat Ranjan1, Gerardo M. Ojeda1,2, Upendra K. Sharma1, Erik V. Van der Eycken1,3 1: Laboratory for Organic & Microwave-Assisted Chemistry (LOMAC), Department of Chemistry, University of Leuven (KU Leuven), Belgium.; 2: University of Havana, Zapata y G,

10400 Havana, Cuba; 3: People’s Friendship University of Russia (RUDN University), Moscow, Russia

5:00pm - 5:20pm

Intensification of temperature cycling-induced deracemization through microwave heating Fabio Cameli, Christos Xiouras, Georgios Stefanidis KU Leuven, Belgium

7:00pm Welcome Reception Location: Leuven City Hall

Date: Tuesday, 28/May/2019

8:00am -

9:00am

Registration Location: MTC 00.03

9:00am -

9:45am

Session 3 Plenary: Dr. Jean-Luc Dubois, ARKEMA, France - 3D printing for intensified catalytic processes. A Casestudy. Location: Grote Aula Chair: Jan Harmsen

“3D Printing for intensified catalytic processes. A case study from the PrintCr3Dit project.” Jean-Luc DUBOIS ARKEMA, France

9:45am -

10:45am

S3.1 Group 1: Industrial day (PI Succes stories)Location: Grote Aula Chair: Bora Aydin 09:45 Dermaut, W. (AGFA) - Eliminating the need for liquid bromine by means of flow technology 10:05 Camarasa, E. (SEQENS) - Isopropyl acetate reactive distillation 10:25 Schnider, C. (LONZA) - Process Intensification at Lonza: an Overview & Case Studies

S3.1 Group 2: HiGeeLocation: Kleine Aula Chair: John van der Schaaf 9:45am - 10:05am

Highly Efficient Regeneration of Triethylene Glycol Solution in Rotating Packed Bed for Natural Gas Dehydration Process Liang-Liang Zhang, Ping Liu, Guang-Wen Chu, Jian-Feng Chen Beijing University of Chemical Technology, China, People's Republic of

10:05am - 10:25am

The effect of improved liquid distribution on the gas-liquid contacting in a rotating packed bed Jasper Anton Hacking1, Michiel Marien de Beer2, John van der Schaaf1 1: Technische Universiteit Eindhoven, The Netherlands; 2: Akzo Nobel Chemicals B.V., The Netherlands

10:25am - 10:45am

Pressure Drop in Rotating Packed Beds James Hendry, Jonathan GM Lee, Pierrot Attidekou, Toluwanimi Kolawole Newcastle University, United Kingdom

10:45am -

11:15am





Intensification of a chemical reactor for methanol synthesis through forced periodic operations - Evaluation based on Nonlinear Frequency Response Analysis

Daliborka Nikolic Paunic1, Carsten Seidel2, Achim Kienle2,3, Andreas Seidel-Morgenstern2,3, Menka Petkovska4 1: Institute of Chemistry, Technology and Metallurgy, Serbia; 2: Otto-von-Guericke-University, Germany; 3: Max-Planck-Institute for Dynamics of Complex Technical Systems, Germany; 4: Faculty of Technology and Metallurgy, University of Belgrade, Serbia






Characterization of cavitation bubble size distribution during sonication in a milliflow reactor Jeroen Jordens, Thomas Matthys, Tom Van Gerven KU Leuven, Belgium

Development of a microalgae biocomposite-integrated Spinning Disc Bioreactor (SDBR) for bioprocess intensification of light-driven CO2 absorption Kamelia Boodhoo1, Thea Ekins-Coward1, Sharon Velasquez-Orta1, Michael Flickinger2,3

1: School of Engineering, Newcastle University, United Kingdom; 2: Chemical and Biomolecular Engineering, North Carolina State University, Raleigh, North Carolina, USA; 3: Golden LEAF Biomanufacturing Training and Education Center, BTEC, North Carolina State University, Raleigh, North Carolina, USA















Anti-fouling strategies for tubular flow crystallizers Arne Vancleef1, Tom Van Gerven2, Leen Thomassen1,2, Leen Braeken1,2 1: Faculty of Engineering Technology, KU Leuven, Agoralaan building B box 8, 3590 Diepenbeek, Belgium; 2: Department of Chemical Engineering, KU Leuven, Celestijnenlaan 200F Box 2424, 3001 Leuven, Belgium

Continuous synthesys of galactooligosacharides in liquid-solid oscillatory flow reactor Danijela Slavnić, Milica Carević, Dejan Bezbradica, Nikola Nikacevic

University of Belgrade, Faculty of Technology and Metallurgy, Serbia








Application of optical fiber particle velocity and concentration in-line measurement technology Weipeng Zhang1,2,3, Chao Yang1,2, Xiangyang Li1,2, Guozheng Li1

1: Key Laboratory of Green Process and Engineering, Institute of Process Engineering, Chinese Academy of Sciences, Beijing 100190, China; 2: School of Chemical Engineering, University of Chinese Academy of Sciences, Beijing 100049, China; 3: Nanjing Jiuzhang Chemical Technology Co., Ltd., Nanjing 211800, China

Numerical simulation of micro-mixing in a solid-liquid stirred tank with E-model coupled with CFDXiaoxia Duan1,2, Xin Feng1,2, Chao Yang1,2, Zaisha Mao1 1: Institute of Process Engineering, Chinese Academy of Science, Beijing 100190, China; 2: School of Chemical Engineering, University of Chinese Academy of Sciences,Beijing 100049, China

11:15am -

12:40pm

S3.2 Group 1: Industrial day (Round table discussion)Location: Grote Aula Interactive round table discussion on Changing industrial context and the use of PI for this change. Moderator: Prof. Dr. Maarten Verkerk, Maastricht University, the Netherlands End-user for pharma: Dr. Christian Schnider, LONZA, Austria End-user for specialty chemicals: Dr. Dominique Horbez, Solvay, FranceEnd-user for petrochemicals: Dr. Justin A. Federici, ExxonMobil, USA Tech provider: Dr. Christophe Cappuyns, Alfa Laval, Netherlands Engineering: Dr. Koos Overwater, Technip, Netherlands Networking: Dr. Ignasi Palou-Rivera, RAPID, USA

S3.2 Group 2: Batch to continuous Location: Kleine Aula Chair: Adam P Harvey 11:15am - 11:35am

Adventures with Mesoscale Oscillatory Baffled Reactors Adam P Harvey Newcastle University, United Kingdom

11:35am - 11:55am

Intensification of bio-based processes via oscillatory processing of substrates with high solid loading Bettina Muster-Slawitsch1, Juditj Buchmaier1, Anh N. Phan2, Rama Krishna Gudiminchi3, Bernd Nidetzky3, Christoph Brunner1 1: AEE INTEC, Industrial Processes and Energy Systems, Feldgasse 19, 8200 Gleisdorf; 2: Newcastle University, Chemical Engineering and Advanced Materials, Newcastle upon Tyne NE1 7RU, United Kingdom; 3: Austrian Center of Industrial Biotechnology, 14 Petersgasse, A- 8010 Graz, Austria

11:55am - 12:20pm

Intensified CO2 sequestration by precipitating carbonates from aqueous monoethanolamine solution with nickel nanoparticles in continuous tubular reactor Ning Zhang1, Rafael M. Santos2, Lidija Šiller1 1: School of Engineering, Newcastle University, Newcastle upon Tyne, NE1 7RU, UK; 2: School of Engineering, University of Guelph, Guelph, Ontario, N1G 2W1, Canada

12:20pm - 12:40pm

Process Intensification of Micellar Autocatalyzed Tertiary Amine Oxidation Arnab Chaudhuri1, Wyatt Winkenwerder2, John van der Schaaf1 1: Eindhoven Technical University, Netherlands, The; 2: Nouryon-Surface Chemistry

12:35pm -

1:25pm

Lunch break Location: MTC 00.03


Rapid prototyping through 3D printing as a tool for achieving intensified electrolyzer designs Stéphane Jean-Marie Christian Weusten1, Mattheus de Groot1,2, John van der Schaaf1

1: Department of Chemical Engineering and Chemistry, TU Eindhoven, P.O.Box 513 , 5600 MB Eindhoven, the Netherlands; 2: Nouryon, Christian Neefestraat 2, 1077 WW Amsterdam, the Netherlands























The direct coupling of a continuous flow assisted reaction with a seedless continuous flow tubular crystalliser

Jean Septavaux, Bart Rimez, Benoit Scheid Université Libre de Bruxelles, Belgium








Intensified flow separator infrastructure and expertise for the materials industry

Jean Paul Gueneau de Mussy, Jeroen Jordens, Tom Van Gerven KU Leuven, Belgium




1:25pm -

2:00pm

Session 4 Plenary: Dr. Jianfeng Chen, Dr. Chao Yang & Dr. Guangwen Chu, China - Process intensification development and industrial achievement in China Location: Grote Aula Chair: Dominique Horbez

Process intensification development and industrial achievement in China Chen Jian-Feng1, Yang Chao2, Chu Guang-Wen1 1: Research Center of the Ministry of Education for High Gravity Engineering and Technology, Beijing University of Chemical Technology, Beijing 100029, China; 2: Institute of Process Engineering, Chinese Academy of Sciences, Beijing 100190, China

2:00pm -

2:30pm

Global initiatives on PI Location: Grote Aula CIESC - Dr. Jian-Feng Chen, Beijing University of Chemical Technology, People's Republic of China RAPID - Dr. Ignasi Palou-Rivera, AIChE, Spain EUROPIC - Dr. Manfred Nagel, Evonik, Germany

2:30pm -

3:30pm

S4.1 Group 1: Industrial day Location: Grote Aula Chair: Jan Lerou 2:30pm - 2:50pm

Process intensification of upstream gas separations through adsorption-based, microchannel, separation technology Justin Federici1, Michelle Dose1, Phillip Schoch1, Rodrigo Blanco1, Ben Marshall2, Joey Vella2, Chien Chen3, Tracy Fowler3, Patrick McMahon3 1: ExxonMobil Research and Engineering, Clinton, NJ,; 2: ExxonMobil Research and Engineering, Houston, TX; 3: ExxonMobil Upstream Research Company, Houston, TX

2:50pm - 3:10pm

S4.1 Group 2: HiGeeLocation: Kleine Aula Chair: Andrzej Górak 2:30pm - 2:50pm

Intensified recovery of valuable metals from NdFeB magnets by mechanochemically assisted ferric sulfate leaching Steff Van Loy1, Mehmet Ali Recai Onal2, Koen Binnemans2, Tom Van Gerven1 1: KU Leuven, Department of Chemical Engineering, Celestijnenlaan 200F, B-3001 Heverlee, Belgium; 2: KU Leuven, Department of Chemistry, Celestijnenlaan 200F, B-3001 Heverlee, Belgium

2:50pm - 3:10pm

Enhanced heat transfer technology in cracking furnaces Lijun Zhang SINOPEC Beijing Research Institute of Chemical Industry

3:10pm - 3:30pm

Distributed production: Scale-up versus ExperienceGregory S. Patience, Daria Camilla Boffito Chemical Engineering, Polytechnique Montreal, Canada

Mass Transfer Modeling and Application in a Rotating Packed Bed Reactor with Mesh-pin Rotor Wei Liu, Yong Luo, Guang-Wen Chu, Jian-Feng Chen Research Center of the Ministry of Education for High Gravity Engineering and Technology, Beijing University of Chemical Technology, Beijing 100029, PR China

3:10pm - 3:30pm

Micromixing in a Rotor-Stator Spinning Disc Reactor Arturo Neissen Manzano Martinez1, Melissa Assirelli2, John van der Schaaf1 1: Eindhoven University of Technology, The Netherlands; 2: Nouryon Specialty Chemicals, The Netherlands

3:30pm -

4:00pm








Influence of surface wettability of the surface-modified stainless steel wire mesh packing on

mass transfer performance in a rotating packed bed Meng-Jun Su, Yong Luo, Guang-Wen Chu, Jian-Feng Chen Research Center of the Ministry of Education for High Gravity Engineering Technology, Beijing University of Chemical Technology, Beijing 100029, PR China







Effect of process parameters on a novel modular continuous crystallizer Nnaemeka Ezeanowi1,2, Tuomas Koiranen1

1: School of Engineering Science, Lappeenranta University of Technology, P.O. Box 20, FIN-53851 Lappeenranta, Finland; 2: Sonotecc Oy, Laululinnuntie 18A, 00780 Helsinki, Finland
















Specialty monomers synthesis by ultrasound assisted oxidative cleavage Ana Luisa Maria1,3, Jean-Luc Couturier1, Jean-Luc Dubois2, Giancarlo Cravotto3

1: 14 Chemin Henri Moissan, 69310 Pierre Bénite France; 2: Arkema, Colombes, 92700 FRANCE; 3: Università Degli Studi Di Torino - UNITO, Torino, 10125 ITALY







4:00pm -

4:40pm

Session 5 Plenary: Prof. Dr. Dionisios Vlachos, University of Delaware, USA - Modular manufacturing for emerging energy industries: Green Ammonia, Shale Gas and Biomass Upgrade Location: Kleine Aula Chair: Nikola Nikacevic

Modular Manufacturing for Emerging Energy Industries: Green Ammonia, Shale Gas and Biomass Upgrade Dion Vlachos Catalysis Center for Energy Innovation (CCEI) and Delaware Energy Institute (DEI), Harker Interdisciplinary Science and Engineering (ISE) Lab, 221 Academy St., Office 250 M, University of DelawareNewark, DE 19716, USA

4:00pm -

5:00pm

S4.2 Group A: Industrial day (Group discussion) - GROUP A: Microreactors Location: MTC 00.07 Chair: Simon Kuhn

S4.2 Group B: Industrial day(Group discussion) - GROUP B: Multifunctional Process Location: MTC 00.08 Chair: Andrzej Górak

S4.2 Group C: Industrial day (Group discussion) - GROUP C: Alternative Energy Sources Location: MTC 01.15 Chair: Andrzej Stankiewicz

S4.2 Group D: Industrialday (Group discussion) - GROUP D: 3D-Printing Location: MTC 02.11 Chair: Jean-Luc DUBOIS

4:40pm -

5:40pm

S4.2 Group 2: Batch to continuous Location: Kleine Aula Chair: Igor Plazl 4:40pm - 5:00pm

Propoxylation of Fatty Amines: How to switch from Batch to Flow? Pia Müller1, Wyatt Winkenwerder2, John van der Schaaf1 1: Eindhoven University of Technology, The Netherlands; 2: Nouryon, United States

5:00pm - 5:20pm

A Tubular Nucleation Device to Master the Spontaneous Nucleation Behavior of Small Organic Molecules Bart Rimez, Jean Septavaux, Robin Debuysschère, Benoit Scheid Université Libre de Bruxelles - TIPs, Belgium

5:20pm - 5:40pm


5:00pm -

5:40pm

S4.3: Consolidation of discussion findings industrial dayLocation: Grote Aula

7:00pm Dinner Location: Faculty Club

Date: Wednesday, 29/May/2019

8:30am -

9:15am

Registration Location: MTC 00.03

9:15am -

9:45am

PI award: Academic PI Award WinnerLocation: Grote Aula 9:15am - 9:45am

Intensification of steam methane reforming: Production of high purity H2 with reduced energy demands Andy Antzara1, Eleni Heracleous2, Angeliki Lemonidou1 1: Department of Chemical Engineering, Aristotle University of Thessaloniki, Greece; 2: School of Science & Technology, International Hellenic University, Greece

9:45am -

10:45am

S5.1 Group 1: Energy activation (Microwave-Plasma)Location: Grote Aula Chair: Georgios Stefanidis 9:45am - 10:05am

Microwave-assisted methane valorization: enhancement of oxidative and non-oxidative coupling processes by inhibiting gas-phase reactions Ignacio Julian, Jose Luis Hueso, Reyes Mallada, Jesus Santamaria Universidad de Zaragoza, Spain

10:05am - 10:25am

Ethylene production from methane in plasma-assisted processes Evangelos Delikonstantis, Marco Scapinello, Georgios D. Stefanidis KU Leuven, Belgium

10:25am - 10:45am

Removal of a tar analogue from mixture of product gas using a non-thermal plasma dielectric barrier discharge reactor Faisal saleem, Kui zhang, adam harvey Newcastle university, United Kingdom

S5.1 Group 2: Novel Process & equipment conceptsLocation: Kleine Aula Chair: Carla Perreira 9:45am - 10:05am

Integrated Carbon Capture Processes Using Carbonate Fuel Cells Jonathan Rosen1, Tim Barckholtz1, Rodrigo Blanco Gutierrez1, Keith Davis2, Frank Dobek2, Tim Geary2, Hossein Ghezel Ayagh2, Lu Han1, Abdelkader Hilmi2, Brandon O'Neill1, Carla Pereira1, Carl Willman2, Wei Yang2, Chao-Yi Yuh2 1: ExxonMobil Research and Engineering, United States of America; 2: FuelCell Energy, United States of America

10:05am - 10:25am

Spray roasting route for industrial production of NMC cathode materials Evgeny Legotin1,2, Katja Fröhlich1, Raad Hamid1, Ningxin Zhang1, Frank Bärhold3, Marcus Jahn1, Franz Winter2 1: AIT Austrian Institute of Technology GmbH, Austria; 2: TU Wien, Austria; 3: Andritz AG, Austria

10:25am - 10:45am

Onboard Fuel Separation Randall David Partridge ExxonMobil Research and Engineering Company, United States of America

10:45am -

11:15am


11:15am -

12:35pm

S5.2 Group 1: Energy activation (Light)Location: Grote Aula Chair: Ignasi Palou-Rivera 11:15am - 11:35am

About the interest of LED-driven microstructured reactors for implementing efficiently sensitized photooxygenations: chemical engineering insightsRobbie RADJAGOBALOU1, Jean-François BLANCO1, Sébastien ELGUE1, Odile DECHY-CABARET2, Michael OELGEMOLLER3, Karine LOUBIERE1 1: Laboratoire de Génie Chimique (LGC), Université de Toulouse, CNRS, INPT, UPS, Toulouse, France; 2: Laboratoire de Chimie de Coordination, CNRS, Toulouse, France; 3: James Cook University, College of Science and Engineering, Townsville, Queensland 4811, Australia

11:35am - 11:55am

S5.2 Group 2: 3D printingLocation: Kleine Aula Chair: Simon Kuhn 11:15am - 11:35am

Computer aided design of 3D printed internals for Rotating Packed Beds Kamil Kaminski1,2, Konrad Gladyszewski1,2, Mirko Skiborowski1 1: Department of Biochemical and Chemical Engineering, Laboratory of Fluid Separations, Technical University of Dortmund, Germany; 2: Faculty of Process and Environmental Engineering, Lodz University of Technology, Poland

11:35am - 11:55am

Towards green photochemistry: the principles of co-axial illumination for photochemical reactors Glen Meir1, Mumin Enis Leblebici2, Simon Kuhn1, Tom Van Gerven1 1: Department of Chemical Engineering, KU Leuven, Celestijnenlaan 200F, 3001 Leuven, Belgium; 2: KU Leuven Lab4U – Faculty of Industrial Engineering, Agoralaan Building B, B-3590 Diepenbeek, Belgium

11:55am - 12:15pm

Solution to internal mass transfer limitations in photocatalytic reactors Thomas Claes1, Mumin Enis Leblebici2, Tom Van Gerven1

1: Department of Chemical engineering, KU Leuven; 2: Faculty of Industrial Engineering, KU Leuven Lab4U

12:15pm - 12:35pm

Framing the Design of Aerosol Photoreactors Emine Kayahan, Mathias Jacobs, Senne Fransen, Simon Kuhn, Tom Van Gerven, M. Enis Leblebici KU Leuven, Belgium

Intensification of Non-Adiabatic Catalytic Processes with Packed Periodic Open Cellular Structures Matteo Ambrosetti1,2, Gianpiero Groppi1, Wilhelm Schwieger2, Enrico Tronconi1, Hannsjörg Freund2 1: Dipartimento di Energia, Politecnico di Milano, Via La Masa, 34, 20156, Milano, Italy; 2: Friedrich-Alexander-Universität Erlangen-Nürnberg (FAU), Lehrstuhl für Chemische Reaktionstechnik, Egerlandstraße 3, 91058 Erlangen, Germany

11:55am - 12:15pm

Design rules of 3D printed translucent monoliths for photo-flow processes Mathias Jacobs, Mumin Enis Leblebici KU Leuven, Belgium

12:15pm - 12:35pm

Intensified carbon capture using swirling fluidized beds: hydrodynamics investigation and sorbent screening Jonathan McDonough, Richard Law, David Reay, Vladimir Zivkovic Newcastle University, United Kingdom

12:35pm -

12:45pm

Poster Awards & Closing Session Location: Grote Aula

12:45pm Lunch break Location: MTC 00.03

Documents

Conference Agenda The Second International Process ... · Daniela Lavric1, Uroš Novak2,3, Polona Žnidaršič-Plazl2 1: Corning S.A.S. Corning European Technology Center; 2: University