Client Matrix: Water Date Received: 11/29/2007 0923

Analytical Data

Client: Hercules Inc. Job Number: 680-32249-1

Client Sample ID: HER-MWI7-112807

Lab Sample ID: 680-32249-22 Date Sampled: 11/28/2007 1505Client Matrix: Water Date Received: 11/29/2007 0923

8260B Volatile Organic Compounds by GC!MS

O Method: 8260B Analysis Batch: 680-92648 Instrument ID: GC/MS Volatiles - BPreparation: 5030B Lab File ID: b0463.dDilution: 200 Initial WeightlVolume: 5 mLDate Analyzed: 12/04/2007 1741 Final WeightNolume: 5 mLDate Prepared: 12/04/2007 1741

fl Analyte Result (ug/L) Qualifier RL1,1 2,2-Tetrachloroethane <200 200Tetrachloroethene <200 200Toluene 210 200

1,1,1-Trichloroethane

<200 2001,1,2-Trichloroethane <200 200Trichloroethene <200 200Trichlorofluoromethane <200 2001 ,2,3-Trichloropropane <200 200Vinyl acetate <400 400Vinyl chloride <200 200Xylenes, Total <400 400

Surrogate %Rec Acceptance Limits4-Bromofluorobenzene 92 75 - 120Dibromofluoromethane 103 75- 121Toluene-d8 (Surr) 91 75- 120

TestAmerica Savannah Page 52 of 151

Analytical Data

Client: Hercules Inc. Job Number 680-32249-1



8260B Volatile Organic Compounds by GCIMS

Method: 8260B Analysis Batch; 680-92858 Instwment ID: GC/MS Volatiles - BPreparation: 5030B Lab File ID: b0473.dDilution: 500 Initial WeightNolume: 5 mLDate Analyzed: 12/06/2007 1232 Run Type: DL Final WeightNolume: 5 mLDate Prepared: 12/06/2007 1232

Analyte Result (ug/L) Qualifier RLAcetone <13000 13000Acetonitrile <20000 20000Acrolein <10000 10000Acrylonitrile <10000 10000Benzene 3000 D 500Dichlorobromomethane <500 500Bromoform <500 500

U Bromomethane <500 5002-Butanone (MEK) <5000 5000Carbon disulfide <1000 1000Carbon tetrachlonde 41000 D 500

Q Chlorobenzene 890 D 500Chloroethane <500 500Chloroform 4100 D 500Chloromethane <500 5002-Chloro-i,3-butadiene <500 5003-Chloro-1-propene <500 500Chlorodibromomethane <500 5001 ,2-Dibromo-3-Chloropropane <500 500Ethylene Dibromide <500 500Dibromomethane <500 500trans-i ,4-Dichloro-2-butene <1000 1000

UDichlorodifluoromethane <500 5001,i-Dichloroethane <500 5001 2-Dichloroethane <500 5001,i-Dichloroethene <500 500cis-1 ,2-Dichloroethene <500 500trans-i 2-Dichloroethene <500 5001 ,2-Dichloropropane <500 500cis-i ,3-Dichloropropene <500 500

U trans-i 3-Dichloropropene <500 500Ethylbenzene <500 500Ethyl methacrylate <500 5002-Hexanone <5000 5000lodomethane <2500 2500lsobutyl alcohol <20000 20000Methacrylonitrile <10000 10000Methylene Chloride <2500 2500Methyl methacrylate <500 5004-Methyl-2-pentanone (MIBK) <5000 5000

O Pentachloroethane <2500 2500Propionitrile <10000 10000Styrene <500 5001,1,1 2-Tetrachloroethane <500 500


Analytical Data



Lab Sample ID: 680-32249-22 Date Sampled: 11/2812007 1505Client Matrix: Water Date Received: 11/29/2007 0923


Method: 8260B Analysis Batch: 680-92858 Instrument ID: GC/MS Volatiles - BPreparation: 5030B Lab File ID: b0473.dDilution: 500 Initial WeightNolume: 5 mLDate Analyzed: 12/06/2007 1232 Run Type: DL Final WeightNolume: 5 mLDate Prepared: 12/06/2007 1232

Analyte Result (ug/L) Qualifier RL1,1 2,2-Tetrachloroethane <500 500Tetrachloroethene <500 500Toluene <500 5001,1,1-Trichloroethane <500 5001,1,2-Trichloroethane <500 500Trichloroethene <500 500Trichlorofluoromethane <500 5001 ,2,3-Trichloropropane <500 500Vinyl acetate <1000 1000Vinyl chloride <500 500Xylenes, Total <1000 1000

Surrogate %Rec Acceptance Limits4-Bromofluorobenzene 97 75- 120Dibromofluoromethane 101 75- 121Toluene-d8 (Surr) 89 75- 120


Analytical Data

0 Client: Hercules Inc. Job Number: 680-32249-1




Method: 8260B Analysis Batch: 680-92630 Instrument ID: GC/MS Volatiles - BPreparation: 5030B Lab File ID: b0454.dDilution: 1.0 Initial Weight/Volume: 5 mLDate Analyzed: 12/04/2007 0452 Final WeightNolume: 5 mLDate Prepared: 12/04/2007 0452

Analyte Result (ug/L) Qualifier RLAcetone <25 25Acetonitrile <40 40Acrolein <20 20Acrylonitrile <20 20Benzene 1.2 1.0Dichlorobromomethane <1.0 1.0Bromoform <1.0 1.0Bromomethane <1.0 1.02-Butanone (MEK) <10 10Carbon disulfide <2.0 2.0Carbon tetrachlonde <1.0 1.0Chlorobenzene 26 1.0Chloroethane <1.0 1.0Chloroform <1.0 1.0Chloromethane <1.0 1.02-Chloro-1 3-butadiene <1.0 1.03-Chloro-1-propene <1.0 1.0Chlorodibromomethane <1.0 1.01 ,2-Dibromo-3-Chloropropane <1.0 1.0Ethylene Dibromide <1.0 1.0Dibromometharie <1.0 1.0trans-i ,4-Dichloro-2-butene <2.0 2.0Dichlorodifluoromethane <1.0 1.011-Dichloroethane <1.0 1.012-Dichloroethane <1.0 1.011-Dichloroethene 1.4 1.0] cis-12-Dichloroethene <1.0 1.0trans-i 2-Dichloroethene <1.0 1.0I ,2-Dichloropropane 1.2 1.0cis-i3-Dichloropropene <1.0 1.0trans-i 3-Dichloropropene <1.0 1.0Ethylbenzene <1.0 1.0Ethyl methacrylate <1.0 1 02-Hexanone <10 10lodomethane <5.0 5.0Isobutyl alcohol <40 40Methacrylonitrile <20 20Methylene Chloride <5.0 5.0Methyl methacrylate <1.0 1.0

J 4-Methyl-2-pentanone (MIBK) <10 10

O Pentachloroethane <5.0 5.0Propionitrile <20 207 Styrene <1.0 1.01.1,1 ,2-Tetrachloroethane <1.0 1.0


AnayticaI Data





U Method: 8260B Analysis Batch: 680-92630 Instrument ID: GC/MS Volatiles - BPreparation: 5030B Lab File ID: b0454.dDilution: 1.0 Initial WeightNolume: 5 mLDate Analyzed: 12/04/2007 0452 Final WeightNolume: 5 mLDate Prepared: 12/04/2007 0452

Analyte Result (ugIL) Qualifier AL1,1 ,2,2-Tetrachloroethane <1.0 1.0Tetrachloroethene <1.0 1.0Toluene <1.0 1.01,1,1-Trichloroethane <1.0 1.01,1 ,2-Trichloroethane <1.0 1.0Trichloroethene <1.0 1.0Tnchlorofluoromethane <1.0 1.01 ,2,3-Trichloropropane <1.0 1.0Vinyl acetate <2.0 2.0Vinyl chloride <1.0 1.0Xylenes, Total <2.0 2.0

Surrogate %Rec Acceptance Limits4-Bromofluoroberizene 91 75-120Dibromofluoromethane 99 75 - 121Toluene-d8 (Surr) 94 75 - 120


Analytical Data0 Client: Hercules Inc. Job Number: 680-32249-1


Lab Sample ID: 680-32249-24 Date Sampled: 1112812007 0830Client Matrix: Water Date Received: 11/29/2007 0923


O Method: 8260B Analysis Batch: 680-92648 Instrument ID: GC/MS Volatiles - BPreparation: 5030B Lab File ID: b0458.dDilution: 1.0 Initial WeightfVolume: 5 mLDate Analyzed: 12/04/2007 1525 Final WeightNolume: 5 mLDate Prepared: 12/04/2007 1525

flAnalyte Result (ug/L) Qualifier RLAcetone <25 25Acetonitrile <40 40Acrolein <20 20

fl Acrylonitrile <20 20Benzene 44 1.0Dichlorobromomethane <1.0 1.0Bromoform <1.0 1.0

O Bromomethane <1.0 1.02-Butanone (MEK) <10 10Carbon disulfide <2.0 2.0Carbon tetrachloride <1.0 1.0Chlorobenzene 10 1.0Chloroethane <1.0 1.0Chloroform <1.0 1.0Chloromethane <1.0 1.02-Chloro-1 ,3-butadiene <1.0 1.03-Chloro-1-propene <1.0 1.0Chlorodibromomethane <1.0 1.01,2-Dibromo-3-Chloropropane <1.0 1.0Ethylene Dibromide <1.0 1.0Dibromomethane <1.0 1.0trans-i 4-Dichloro-2-butene <2.0 2.0Dichlorodifluoromethane <1.0 1.0il-Dichloroethane <1.0 1.01 ,2-Dichloroethane <1.0 1.0i,1-Dichloroethene 1,1 1.0cis-i ,2-Dichloroethene <1.0 1.0trans-i 2-Dichloroethene <1.0 1.01,2-Dichloropropane <1.0 1.0cis-1,3-Dichloropropene <1.0 1.0trans-i ,3-Dichloropropene <1.0 1.0Ethylbenzene 2.6 1.0Ethyl methacrylate <1.0 1.02-Hexanone <10 10

fl lodomethane <5.0 5.0

J Isobutyl alcohol <40 40Methacrylonitrile <20 20Methylene Chloride <5.0 5.0Methyl methacrylate <1.0 1.04-Methyl-2-pentanone (MIBK) <10 10

O Pentachloroethane <5.0 5.0Propionitrile <20 20Styrene <1.0 1.0J 1,1,1 ,2-Tetrachloroethane <i .0 1,0


Analytical Data



Lab Sample ID: 680-32249-24 Date Sampled: 11/28/2007 0830Client Matrix: Water Date Received: 1112912007 0923


U Method: 8260B Analysis Batch: 680-92648 Instrument ID: GC/MS Volatiles - BPreparation: 503DB Lab File ID: b0458.dDilution: 1.0 Initial WeightNolume: 5 mLDate Analyzed: 12/04/2007 1525 Final Weight/Volume: 5 mLDate Prepared: 12/04/2007 1525

Analyte Result (ug/L) Qualifier RL1,1 22-Tetrachloroethane <1.0 1.0Tetrachloroethene <1.0 1.0Toluene 1.4 1.0

fl 1,1 1-Trichloroethane <1.0 1.0112-Trichloroethane <1.0 1.0Trichloroethene <1.0 1.0Trichlorofluoromethane <1.0 1.0123-Trichloropropane <1.0 1.0Vinyl acetate <2.0 2.0Vinyl chloride <1.0 1.0Xylenes, Total <2.0 2.0


TestAmericaSavannah Page 58 of 151

Analytical Data


Client Sample ID: HER-RSI-112607



Method: 8260B Analysis Batch: 680-92536 Instrument ID: GCIMS Volatlles - BPreparation: 5030B Lab File ID: b0443.dDilution: 1.0 Initial WeightNolume: 5 mLDate Analyzed: 12/03/2007 1852 Final WeightNolume: 5 mLDate Prepared: 12/03/2007 1852

Analyte Result (ug/L) Qualifier RLAcetone <25 25Acetonitrile <40 40Acrolein <20 20Acrylonitrile <20 20Benzene <1.0 1.0Dichlorobromomethane <1.0 1.0Bromoform <1.0 1.0

U Bromomethane <1.0 1.02-Butanone (MEK) <10 10Carbon disulfide <2.0 2.0Carbon tetrachloride <1.0 1.0Chlorobenzene <1.0 1.0Chloroethane <1.0 1.0Chloroform <1.0 1.0Chloromethane <1.0 1.02-Chloro-i,3-butadiene <1.0 1.03-Chloro-1-propene <1.0 1.0Chlorodibromomethane <1.0 1.01,2-Dibromo-3-Chloropropane <1.0 1.0Ethylene Dibromide <1.0 1.0Dibromomethane <1.0 1.0trans-i ,4-Dichloro-2-butene <2.0 2,0Dichlorodifluoromethane <1.0 1.0li-Dichloroethane <1.0 1.01,2-Dichloroethane <1.0 1.0i,1-Dichloroethene <1.0 1.0cis-i ,2-Dichloroethene <1.0 1.0trans-i 2-Dichloroethene <1.0 1.01,2-Dichloropropane <1.0 1.0cis-i 3-Dichloropropene <1.0 1.0

Utrans-i ,3-Dichloropropere <1.0 1.0Ethylbenzene <1.0 1.0Ethyl methacrylate <1.0 1.02-Hexanone <10 10

U lodomethane <5.0 5.0Isobutyl alcohol <40 40Methacrylonitrile <20 20Methylene Chloride <5.0 5.0

U Methyl methacrylate <1.0 1.04-Methyl-2-pentanone (MIBK) <10 10

Q Pentachloroethane <5.0 5.0Propionitrile <20 20Styrene <1.0 1.0i,1,i,2-Tetrachloroethane <1.0 1.0


AnaIytica Data

Client: Hercules Inc. Job Number 680-32249-1

Client Sample ID: HER-RSI -112607



Method: 8260B Analysis Batch: 680-92536 Instrument ID: GCIMS Volatiles - BPreparation: 5030B Lab File ID: b0443.dDilution: 1.0 Initial WeightNolume: 5 mLDate Analyzed: 12)03/2007 1852 Final WeightNolume: 5 mLDate Prepared: 12/03/2007 1852

fl Analyte Result (ug/L) Qualifier RL1,1 2,2-Tetrachloroethane <1.0 1.0Tetrachloroethene <1.0 1.0Toluene 6.1 1.0

fl 1,1,1-Trichloroethane <1.0 1.0kj 1,1,2-Trichloroethane <1.0 1.0

Trichloroetherie <1.0 1.0Trichlorofluoromethane <1.0 1.0

U i ,2,3-Tnchloropropane <1.0 1.0Vinyl acetate <2.0 2.0Vinyl chloride <1.0 1.0Xylenes, Total <2.0 2.0

Surrogate %Rec Acceptance Limits4-Bromofluorobenzene 87 75- 120Dibromofluoromethane 99 75- 121Toluene-d8 (Surr) 96 75 - 120


Analytical Data


Client Sample ID: HER-RS2-1 12707

Lab Sample ID: 680-32249-26 Date Sampled: 11/27/2007 0915Client Matrix: Water Date Received: 11129/2007 0923

8260 B Volatile Organic Compounds by GC!MS

Method: 8260B Analysis Batch: 680-92536 lnstwment ID: GC/MS Volatiles - BPreparation: 5030B Lab File ID: b0444.dDilution: 1.0 Initial WeightNolume: 5 mLDate Analyzed: 12/03/2007 1920 Final WeightNolume: 5 mLDate Prepared: 12/03/2007 1920

Analyte Result (ug/L) Qualifier RLAcetone <25 25Acetonitrile <40 40Acrolein <20 20Acrylonitrile <20 20Benzene <1.0 1.0Dichlorobromomethane <1.0 1.0Bromoform <1.0 1.0Bromomethane <1.0 1.02-Butanone (MEK) <10 10Carbon disultide <2.0 2.0Carbon tetrachloride <1.0 1.0Chlorobenzene <1.0 1.0Chloroethane <1.0 1.0Chloroform <1.0 1.0Chloromethane <1.0 1.02-Chloro-1 3-butadiene <1.0 1.03-Chloro-1-propene <1.0 1.0Chlorodibromomethane <1.0 1.01 ,2-Dibromo-3-Chloropropane <1.0 1.0Ethylene Dibromide <1.0 1.0Dibromomethane <1.0 1.0trans-i ,4-Dichloro-2-butene <2.0 2.0

ODichlorodifluoromethane <1.0 1.01,1-Dichloroethane <1.0 1.01,2-Dichloroethane <1.0 1.01,1-Dichloroethene <1.0 1.0n cis-1 2-Dichloroethene <1.0 1.0trans-i ,2-Dichloroethene <1.0 1.01 ,2-Dichloropropane <1.0 1.0cis-1 ,3-Dichloropropene <1.0 1.0trans-i ,3-Dichloropropene <1.0 1.0Ethylbenzene <1.0 1.0Ethyl methacrylate <1.0 1.02-Hexanone <10 10lodomethane <5.0 5.0Isobutyl alcohol <40 40Methacrylonitrile <20 20Methylene Chloride <5.0 5.0Methyl methacrylate <1.0 1.0


Q Pentachloroethane <5.0 5.0Propionitrile <20 20Styrene <1.0 1.01,11 2-Tetrachloroethane <1.0 1 0


Analytical Data


Client Sample ID: HER-RS2-1 12707

Lab Sample ID: 680-32249-26 Date Sampled: 11)27/2007 0915Client Matrix: Water Date Received: 11/29/2007 0923


fJ Method: 8260B Analysis Batch: 680-92536 Instrument ID: GC/MS Volatiles - BPreparation: 5030B Lab File ID: b0444.dDilution: 1.0 Initial WeightNolume: 5 mLDate Analyzed: 12/03/2007 1920 Final WeightNolume: 5 mLDate Prepared: 12)03/2007 1920

Analyte Result (ug/L) Qualifier RL1 1 2,2-Tetrachloroethane <1.0 1.0Tetrachloroethene <1.0 1.0Toluene 6.8 1.0

ri 11,1-Trichloroethane <1.0 1.01,12-Trichloroethane <1.0 1.0Trichloroethene <1.0 1.0Tnchlorofluoromethane <1.0 1.01,2,3-Trichloropropane <1.0 1.0Vinyl acetate <2.0 2.0Vinyl chloride <1.0 1.0Xylenes, Total <2.0 2.0

Surrogate %Rec Acceptance Limits4-Bromofluorobenzene 86 75 - 120Dibromofluoromethane 99 75 - 121Toluene-d8 (Surr) 95 75- 120


Analytical DataflClient: Hercules Inc. Job Number: 680-32249-1

Client Sample ID: HER-RS3-112807


826DB Volatile Organic Compounds by GC/MS

O Method: 8260B Analysis Batch: 680-92648 Instrument ID: GC/MS Volatiles - BPreparation: 5030B Lab File ID: b0466.dDilution: 1.0 Initial Weight)Volume: 5 mLDate Analyzed: 12/04/2007 1901 Final Weight)Volume: 5 mLDate Prepared: 12)04/2007 1901

fl Analyte Result (ug/L) Qualifier RLU Acetone <25 25

Acetonitrile <40 40Acrolein <20 20Acrylonitrile <20 20Benzene <1.0 1.0Dichlorobromomethane <1.0 1.0Bromoform <1.0 1.0

U Bromomethane <1.0 1.02-Butanone (MEK) <10 10Carbon disulfide <2.0 2.0Carbon tetrachlonde <1.0 1.0Chlorobenzene <1.0 1.0Chloroethane <1.0 1.0Chloroform <1.0 1.0Chloromethane <1.0 1.02-Chloro-1,3-butadiene <1.0 1.03-Chloro-1-propene <1.0 1.0Chlorodibromomethane <1.0 1.01 2-Dibromo-3-Chloropropane <1.0 1.0Ethylene Dibromide <1.0 1.0Dibromomethane <1.0 1.0trans-i ,4-Dichloro-2-butene <2.0 2.0

UDichlorodifluoromethane <1.0 1.0il-Dichloroethane <1.0 1.01 ,2-Dichloroethane <1.0 1.0il-Dichloroethene <1.0 1.0cis-1 2-Dichloroethene <1.0 1.0trans-12-Dichloroethene <1.0 1.01 2-Dichloropropane <1.0 1.0cis-1 3-Dichloropropene <1.0 1.0trans-I 3-Dichloropropene <1.0 1.0Ethylbenzene <1.0 1.0Ethyl methacrylate <1.0 1.02-Hexanone <10 10‘1 lodometharie <5.0 5.0J Isobutyl alcohol <40 40Methacrylonitrile <20 20Methylene Chloride <5.0 5.07 Methyl methacrylate <1.0 1.0J 4-Methyl-2-pentanone (MIBK) <10 10

Q Pentachloroethane <5.0 5.0Propionitrile <20 20Styrene <1.0 1.01ii2-Tetrachloroethane <1.0 1.0


O Analytical Data


Client Sample ID: HER-RS3-112807


8260B Volatile Organic Compounds by GC/MS

Method: 8260B Analysis Batch: 680-92648 Instrument ID: GC/MS Volatiles - BPreparation: 5030B Lab File ID: b0466.dDilution: 1.0 Initial WeightNolume: 5 mLDate Analyzed: 12/04/2007 1901 Final WeightNolume: 5 mLDate Prepared: 1210412007 1901

Analyte Result (ug/L) Qualifier RL1,1,2,2-Tetrachloroethane <1.0 1.0Tetrachloroethene <1.0 1.0Toluene 5.5 1.0

fl 1,1 1-Thchloroethane <1.0 1.01,1,2-Trichloroethane <1.0 1.0Trichloroethene <1.0 1.0Trichlorofluoromethane <1.0 1.0

fl 1 2,3-Trichloropropane <1.0 1.0Vinyl acetate <2.0 2.0Vinyl chloride <1.0 1.0Xylenes, Total <2.0 2.0



Analytical Data

C Client: Hercules Inc. Job Number: 680-32249-1

Client Sample ID: HER-FDI-112707




flAnalyte Result (ug/L) Qualifier RLAcetone <25 25Acetonitrile <40 40Acrolein <20 20

fl Acrylonitrile <20 20Benzene <1.0 1.0Dichlorobromomethane <1.0 1.0Bromoform <1.0 1.0Bromomethane <1.0 1.02-Butanone (MEK) <10 10Carbon disulfide <2.0 2.0Carbon tetrachloride <1.0 1.0

O Chlorobenzene <1.0 1.0Chloroethane <1.0 1.0Chloroform <1.0 1.0Chloromethane <1.0 1.02-Chloro-1 ,3-butadiene <1.0 1.03-Chloro-1-propene <1.0 1.0Chlorodibromomethane <1.0 1.0

Ui ,2-Dibromo-3-Chloroproparie <1.0 1.0Ethylene Dibromide <1.0 1.0Dibromomethane <1.0 1.0trans-i ,4-Dichloro-2-butene <2.0 2.0

flDichlorodifluoromethane <1.0 1.01,1-Dichloroethane <1.0 1.01 2-Dichloroethane <1.0 1.01,1-Dichloroethene <1.0 1.0cis-1 ,2-Dichloroethene <1.0 1.0trans-i ,2-Dichloroethene <1.0 1.01 ,2-Dichloropropane <1.0 1.0cis-1 3-Dichloropropene <1.0 1.0trans-i ,3-Dichloropropene <1.0 1.0Ethylbenzene <1.0 1,0Ethyl methacrylate <1.0 1.02-Hexanone <10 10

fl lodomethane <5.0 5.0J Isobutyl alcohol <40 40Methacrylonitrile <20 20Methylene Chloride <5.0 5.0Methyl methacrylate <1.0 1.0


Q Pentachloroethane <5.0 5.0Propionitrile <20 20Styrene <1.0 1.01,1,1 2-Tetrachloroethane <1.0 1.0


Q Analytical Data

Client: Hercules Inc Job Number: 680-32249-1

Client Sample ID: HER-FDI-112707



Method: 8260B Analysis Batch: 680-92630 Instrument ID: GC/MS Volatiles - BPreparation: 5030B Lab File ID: b0455.dDilution: 1.0 Initial WeightNolume: 5 mLDate Analyzed: 12)04/2007 0519 Final WeightNolume: 5 mLDate Prepared: 12104/2007 0519

fl Analyte . Result (ug/L) Qualifier RL

U 1,1 2,2-Tetrachloroethane <1.0 1.0Tetrachloroethene <1.0 1.0Toluene <1.0 1.0

fl 1,1,1-Trichloroethane <1.0 1.0Li 1,1 ,2-Trichloroethane <1.0 1.0

Trichloroethene <1.0 1.0

OTrichlorofluoromethane <1.0 1.01 ,2,3-Trichloropropane <1.0 1.0Vinyl acetate <2.0 2.0Vinyl chloride <1.0 1.0Xylenes, Total <2.0 2.0

Surrogate %Rec Acceptance Limits4-Bromofiuorobenzene 100 75- 120Dibromofluoromethane 101 75-121Toluene-d8 (Sun) 94 75- 120


Analytical Data


Client Sample ID: HER-FD2-112807


8260B Volatile Organic Compounds by GC/MS


fl Analyte Result (ug/L) Qualifier RLAcetone <25 25Acetonitrile <40 40Acrolein <20 20Acrylonitrile <20 20Benzene 9.4 1.0Dichlorobromomethane <1.0 1.0Bromoform <1.0 1.0Bromomethane <1.0 1.02-Butanone (MEK) <10 10Carbon disulfide <2.0 2.0Carbon tetrachloride <1.0 1.0

L Chlorobenzene <1.0 1.0Chloroethane <1.0 1.0Chloroform <1.0 1.0Chloromethane 2.1 1.02-Chloro-i,3-butadiene <1.0 1.03-Chloro-1-propene <1.0 1.0Chlorodibromomethane <1.0 1.0

II 1,2-Dibromo-3-Chloropropane <1.0 1.0Ethylene Dibromide <1.0 1.0Dibromomethane <1.0 1.0trans-i ,4-Dichloro-2-butene <2.0 2.0Dichlorodifluoromethane <1.0 1.01,1-Dichloroethane <1.0 1.01,2-Dichloroethane <1.0 1.01,1-Dichloroethene 4.1 1.0cis-i ,2-Dichloroethene <1.0 1.0trans-1,2-Dichloroethene <1.0 1.0I ,2-Dichloropropane <1.0 1.0cis-1 ,3-Dichloropropene <1.0 1.0trans-i ,3-Dichloropropene <1.0 1.0Ethylbenzene <1.0 1.0Ethyl methacrylate <1.0 1.02-Hexanone <10 10lodomethane <5.0 5.0Isobutyl alcohol <40 40Methacrylonitrile <20 20Methylene Chloride <5.0 5.0‘1 Methyl methacrylate <1.0 1.0

J 4-Methyl-2-pentanone (MIBK) <10 10Pentachloroethane <5.0 5.0Propionitrile <20 20Styrene <1.0 1.01,1,1 2-Tetrachloroethane <1.0 1.0


Analytical Data


Client Sample ID: HER-FD2-112807

Lab Sample ID: 680-32249-29 Date Sampled: 11)28/2007 0000Client Matrix: Water Date Received: 11/29/2007 0923

826DB Volatile Organic Compounds by GC/MS

Method: 826DB Analysis Batch: 680-92648 Instwment ID: GC/MS Volatiles - BPreparation: 503DB Lab File ID: b0460.dDilution: 1.0 Initial WeightNolume: 5 mLDate Analyzed: 12/04/2007 1619 Final WeightNolume: 5 mLDate Prepared: 12104/2007 1619

Analyte Result (ug/L) Qualifier RL11,2,2-Tetrachloroethane <1.0 1.0Tetrachloroethene <1.0 1.0Toluene 1.6 1.0

U 11,1-Trichloroethane <1.0 1.01,1,2-Tnchloroethane <1.0 1.0Tnchloroethene <1.0 1.0Trichlorofluoromethane <1.0 1.0

U i ,2,3-Trichloropropane <1.0 1.0Vinyl acetate <2.0 2.0Vinyl chloride <1.0 1.0Xylenes, Total <2.0 2.0



Analytical Data


Client Sample ID: HER-DAI-112807

Lab Sample ID: 680-32249-30 Date Sampled: 11)2812007 1530Client Matrix: Solid % Moisture: 18.8 Date Received: 11/29/2007 0923


L Method: 8260B Analysis Batch: 680-92984 Instrument ID: GC/MS Volatiles - LPreparation: 5030A Lab File ID: l0014,dDilution: 40 Initial Weight/Volume: 5 gDate Analyzed: 12/07/2007 1425 Final WeighiNolume: 5 mLDate Prepared: 12/07/2007 1425

flAnalyte DryWt Corrected: Y Result (ug/Kg) Qualifier RLAcetone <2500 2500Acetonitrile <9900 9900Acrolein <4900 4900Acrylonitrile <4900 4900Benzene <250 250Bromodichloromethane <250 250Bromoform <250 250Bromomethane <250 2502-Butanone <1200 1200Carbon disulfide <250 250Carbon tetrachloride <250 250Chlorobenzene <250 250Chloroprene <250 250Chloroethane <250 250Chloroform <250 250Chloromethane <250 2503-Chloro-1-propene <250 250Dibromochloromethane <250 2501 ,2-Dibromo-3-Chloropropane <490 4901 2-Dibromoethane <250 250Dibromomethane <250 250trans-i ,4-Dichloro-2-butene <490 490Dichlorodifluoromethane <250 250i,1-Dichloroethane <250 2501 2-Dichloroethane <250 250cis-1,2-Dichloroethene <250 250trans-i ,2-Dichloroethene <250 2501,i-Dichloroethene <250 2501 2-Dichloropropane <250 250cis-i 3-Dichloropropene <250 250

U trans-i 3-Dichloropropene <250 250Ethylbenzene <250 250Ethyl methacrylate <250 2502-Hexanone <1200 1200lodomethane <250 250Isobutanol <9900 9900Methacrylonitrile <4900 4900Methylene Chloride <250 250Methyl methacrylate <250 250

J 4-Methyl-2-pentanone <1200 1200

O Pentachloroethane <1200 1200Propionitrile <4900 4900Styrene <250 2501,11 ,2-Tetrachloroethane <250 250


AnalyticalData

Client:HerculesInc.JobNumber680-32249-1

ClientSampleID:HER-DAI-112807

LabSampleID:680-32249-30DateSampled:11/28/20071530ClientMatrix:Solid%Moisture:18.8DateReceived:11/29/20070923

8260BVolatileOrganicCompoundsbyGCIMS

Method:8260BAnalysisBatch:680-92984InstrumentID:GC/MSVolatiles-L

jPreparation:5030ALabFileID:10014.dDilution:40InitialWeight/Volume:5gDateAnalyzed:12/07/20071425FinalWeightNolume:5mLDatePrepared:12/07/20071425

AnalyteDryWtCorrected:YResult(ug/Kg)QualifierRL

11,2,2-Tetrachloroethane<250250

Tetrachloroethene<250250Toluene<2502501,1,1-Trichloroethane<250250

J11,2-Trichloroethane<250250Tnchloroethene<250250Trichlorofluoromethane<2502501,23-Trichloropropane<250250

3Vinylacetate<490490Vinylchloride<250250Xylenes,Total960490

Surrogate%RecAcceptanceLimits4-Bromofluorobenzene8265-124Dibromofluoromethane8765-124Toluene-d8(Surr)7265-132

TestAmericaSavannahPage70of151

AnalyticalDataClient.HerculesInc.JobNumber680-32249-1

ClientSampleID:HER-DA2-112807

LabSampleID:680-32249-31DateSampled:11/28/20071550ClientMatnx:Solid%Moisture:18.1DateReceived:11/29/20070923

8260BVolatileOrganicCompoundsbyGC/MS

Method:8260BAnalysisBatch:680-92548lnstwmentID:GC/MSVolatiles-LJPreparation:5030ALabFileID:11835.d

Dilution:1000InitialWeight/Volume:5gDateAnalyzed:11/30/20071856FinalWeightNolume:5mLDatePrepared:11/30/20071856

AnalyteDryWtCorrected:YResult(ug/Kg)QualifierRLAcetone<6100061000 Acetonitrile<240000240000Acrolein<120000120000Acrylonitrile<120000120000Benzene<61006100Bromodichloromethane<61006100Bromoform<61006100Bromomethane<610061002-Butanone<3100031000Carbondisulfide<61006100Carbontetrachloride<61006100

‘QChlorobenzene<61006100Chloroprene<61006100Chloroethane<61006100Chloroform<61006100Chloromethane<610061003-Chloro-1-propene<61006100Dibromochloromethane<610061001,2-Dibromo-3-Chloropropane<12000120001,2-Dibromoethane<61006100Dibromomethane<61006100trans-i4-Dichloro-2-butene<1200012000 Dichlorodifluoromethane<610061001,1-Dichloroethane<610061001,2-Dichloroethane<61006100cis-1,2-Dichloroethene<61006100trans-i,2-Dichloroethene<610061001,1-Dichloroethene<610061001,2-Dichloropropane<61006100cis-1,3-Dichloropropene<61006100trans-i3-Dichloropropene<61006100Ethylbenzene<61006100Ethylmethacrylate<610061002-Hexanone<3100031000lodomethane<61006100lsobutanol<240000240000Methacrylonitrile<120000120000MethyleneChloride<61006100Methylmethacrylate<610061004-Methyl-2-pentanone<3100031000Pentachloroethane<3100031000Propionitrile<120000120000Styrene<61006100

11,2-Tetrachloroethane<61006100


AnalyticalData

Client:HerculesInc.JobNumber:680-32249-1


LabSampleID:680-32249-31DateSampled:11/28/20071550ClientMatnx:Solid%Moisture:18.1DateReceived:11/29/20070923

8260BVolatileOrganicCompoundsbyGCIMS

Method:8260BAnalysisBatch:660-92548InstrumentID:GCIMSVolatiles-LJPreparation:5030ALabFileID:11835.d

Dilution:1000InitialWeight/Volume:5gDateAnalyzed:11/30/20071856FinalWeight/Volume:5mLDatePrepared:11/30/20071856

AnalyteDryWtCorrected:YResult(ug/Kg)QualifierRL1,12,2-Tetrachloroethane<61006100Tetrachloroethene<61006100Toluene<610061001,1.1-Trichloroethane<61006100

j1,1,2-Trichloroethane<61006100Trichloroethene<61006100Trichlorofluoromethane<610061001,2,3-Trichloropropane<61006100Vinylacetate<1200012000Vinylchlonde<61006100Xylenes,Total<1200012000

Surrogate%RecAcceptanceLimits4-Bromofluorobenzene0X65-124Dibromofluoromethane0X65-124Toluene-d8(Surr)0X65-132


AnalyticalData


ClientSampleID:TRIPBLANK

LabSampleID:680-32249-32TBDateSampled:11/28/20070000ClientMatrix:WaterDateReceived:11/29/20070923

82608VolatileOrganicCompoundsbyGC/MS

Method:8260BAnalysisBatch:680-92648InstrumentID:GC/MSVolatiles-BPreparation:5030BLabFileID:b0455.dDilution:1.0InitialWeight/Volume:5mLDateAnalyzed:12/04/20071403FinalWeight/Volume:5mLDatePrepared:12/04/20071403

AnalyteResult(ug/L)QualifierRLAcetone<2525Acetonhtrile<4040Acrolein<2020Acrylonitrile<2020Benzene<1.01.0Dichlorobromomethane<1.01.0Bromoform<1.01.0

(Bromomethane<1.01.02-Butanone(MEK)<1010Carbondisulfide<2.02.0Carbontetrachlonde<1.01.0Chlorobenzene<1.01.0Chloroethane<1.01.0Chloroform<1.01.0Chloromethane<1.01.02-Chloro-i,3-butadiene<1.01.03-Chloro-i-propene<1.01.0Chlorodibromomethane<1.01.012-Dibromo-3-Chloropropane<1.01.0EthyleneDibromide<1.01.0Dibromomethane<1.01.0trans-i,4-Dichloro-2-butene<2.02.0DicNorodifluoromethane<1.01.01,1-Dichloroethane<1.01.01,2-Dichloroethane<1.01.01,1-Dichloroethene<1.01.0cis-i,2-Dichloroethene<1.01.0trans-i,2-Dichloroethene<1.01.01,2-Dichloropropane<1.01.0cis-1,3-Dichloropropene<1.01.0trans-i3-Dichloropropene<1.01.0Ethylbenzene<1.01.0Ethylmethacrylate<1.01.02-Hexanone<1010lodomethane<5.05.0Isobutylalcohol<4040Methacrylonitrile<2020MethyleneChloride<5.05.0Methylmethacrylate<1.01.04-Methyl-2-pentanone(MIBK)<1010Pentachloroethane<5.05.0Propionitrile<2020Styrene<1.01.01,1,1,2-Tetrachloroethane<1.01.0


AnalyticalDataClient:HerculesInc.JobNumber:680-32249-1

ClientSampleID:TRIPBLANK

LabSampleID:680-32249-32TBDateSampled:11/28/20070000ClientMatrix:WaterDateReceived:11/29/20070923


Method:826DBAnalysisBatch:680-92648InstrumentID:GC/MSVolatiles-BJPreparation:503DBLabFileID:b0455.d

Dilution:1.0InitialWeightNolume:5mLDateAnalyzed:12/04/20071403FinalWeightNolume:5mLDatePrepared:12/04/20071403

AnalyteResult(ug/L)QualifierRL1,1,2,2-Tetrachloroethane<1.01.0 Tetrachloroethene<1.01.0Toluene<1.01.01,1,1-Tnchloroethane<1.01.0

j1,1,2-Trichloroethane<1.01.0Tnchloroethene<1.01.0Tnchlorofluoromethane<1.01.0

1,2,3-Trichloropropane

<1.01.0 Vinylacetate<2.02.0 Vinylchloride<1.01.0Xylenes,Total<2.02.0

Surrogate%RecAcceptanceLimits4-Bromofluorobenzene9275-120Dibromofluoromethane10675-121Toluene-d8(Surr)8975-120


AnaIytcaIData



LabSampleID:680-32249-30DateSampled:11128120071530ClientMatrix:Solid%Moisture:18.8DateReceived:11/29/20070923

8270CSemivolatileCompoundsbyGasChromatography/MassSpectrometry(GC/MS)

Method:8270CAnalysisBatch:680-93535InstrumentID:GC/MSSemiVolatiles-TjPreparation:3550BPrepBatch:680-92817LabFileID:t4269.d

Dilution:5.0InitialWeightNolume:15.04gDateAnalyzed:12)13120071827FinalWeight/Volume:.5mLDatePrepared:12/06/20071534InjectionVolume:1uL

RAnalyteDryWtCorrected:YResult(ug/Kg)QualifierRLAcenaphthene<20002000Thionazin<20002000Sulfotepp<20002000Pyridine<20002000

j1,1-Biphenyl<2000200012,4,5-Tetrachlorobenzene<20002000I24-Trichlorobenzerie<2000200012-Dichlorobenzene<2000200013,5-Trinitrobenzene<20002000I3-Dichlorobenzene<20002000I3-Dinitrobenzene<2000200014-Dichlorobenzene<20002000I4-Dioxane<2000200014-Naphthoquinone<20002000I-Naphthylamine<20002000234,6-Tetrachlorophenol<200020002,4,5-Trichlorophenol<200020002,4,6-Trichlorophenol<200020002,4-Dichlorophenol<200020002,4-Dimethylphenol<200020002,4-Dinitrophenol<10000100002,4-Dinitrotoluene<200020002,6-Dichlorophenol<20002000Dimethylphthalate<200020002,6-Dinitrotoluene<200020002-Acetylaminofluorene<200020002-Chlorophenol<200020002-Chloronaphthalene<200020002-Methylnaphthalene<200020002-Methylphenol<200020002-Naphthylamine<200020002-Nitroaniline<10000100002-Nitrophenol<200020002-Picoline<200020002-Toluidine<200020003&4Methylphenol<200020003,3-Dichlorobenzidine<4100410033’-Dimethylbenzidine<10000100003-Methylcholanthrene<200020003-Nitroaniline<1000010000

4’4,6-Dinitro-2-methylphenol<10000100004-Aminobiphenyl<200020004-Bromophenylphenylether<200020004-Chloro-3-methylphenol<20002000


AnalyticalDataClient:HerculesInc.JobNumber:680-32249-1



8270CSemivolatileCompoundsbyGasChromatography/MassSpectrometry(GCIMS)Method:8270CAnalysisBatch:680-93535InstrumentID:GCIMSSemiVolatiles-T

jPreparation:355DBPrepBatch:680-92817LabFileID:t4269.dDilution:5.0InitialWeightNolume:15.04gDateAnalyzed:12/13120071827FinalWeightNolume:.5mLDatePrepared:12/06/20071534InjectionVolume:1uL

AnalyteDry’.NtCorrected:YResult(ug/Kg)QualifierRL4-Chloroaniline<410041004-Chlorophenylphenylether<200020004-Nitroanhline<10000100004-Nitrophenol<1000010000

j4-Nitroquinolirie-1-oxide<20000200007,12-Dimethylbenz(a)anthracene<20002000Acenaphthylene<20002000Acetophenone<20002000alpha,alpha-Dimethylphenethylamine<410000410000Aniline<41004100Anthracene<20002000

QAramite,Total<20002000Benzo[a]anthracene<20002000Benzo[a]pyrene<20002000Benzo[b]fluoranthene<20002000Berizo[g,h,i]perylene<20002000Benzo[kjfluoranthene<20002000Benzylalcohol<20002000Bis(2-chloroethoxy)methane<20002000Bis(2chloroethyl)ether<20002000Bis(2-ethylhexyl)phthalate140002000Chrysene<20002000Diallate<20002000Dibenz(a,h)anthracene<20002000Dibenzofuran<20002000Di-n-butylphthalate<20002000Diethylphthalate<20002000p-Dimethylaminoazobenzene<20002000Dinoseb<20002000Di-n-octylphthalate<20002000Ethylmethanesulfonate<20002000Fluoranthene35002000Fluorene<20002000Hexachlorobenzene<20002000Hexachlorobutadiene<20002000Hexachlorocyclopentadiene<20002000Hexachloroethane<20002000Hexachlorophene<10000001000000Hexachloropropene<20002000lndeno[1,2,3-cd}pyrene<20002000Isophorone<20002000Isosafrole<20002000Methapyrilene<410000410000Methylmethanesulfonate<20002000


AnalyticalData



LabSampleID:680-32249-30DateSampled:11/28/20071530ClientMatrix:Solid%Moisture:18.8DateReceived:11129/20070923


Method:8270CAnalysisBatch:680-93535InstrumentID:GC/MSSemiVolatiles-TJPreparation:3550BPrepBatch:680-92817LabFileID:t4269.d

Dilution:5.0InitialWeightNolume:15.04gDateAnalyzed:12/13/20071827FinalWeightNolume:.5mLDatePrepared:12/06/20071534InjectionVolume:1uL

AnalyteDryWICorrected:YResult(ug/Kg)QualifierRLNaphthalene<20002000Nitrobenzene<20002000N-Nitrosodi-n-butylamine<20002000N-Nitrosodiethylamine<20002000

jN-Nitrosodimethylamine<20002000N-Nitrosodiphenylamine<20002000N-Nitrosodi-n-propylamine<20002000N-Nitrosomethylethylamine<20002000N-Nitrosomorpholine<20002000N-Nitrosopiperidine<20002000N-Nitrosopyrrolidine<20002000

ON-Nitro-o-toluidine<20002000Pentachlorobenzene<20002000Pentachloronitrobenzene<20002000Pentachlorophenol<1000010000Phenacetin<20002000Phenanthrene48002000Phenol<20002000p-Phenylenediamine<1000010000Pronamide<20002000Pyrene34002000Safrole,Total<20002000o,o,o-Triethylphosphorothioate75002000Disulfoton<20002000EthylParathion<20002000Methylparathion<20002000Phorate<20002000Famphur<20002000Dimethoate<20002000Butylbenzylphthalate<20002000bis(chloroisopropyl)ether<20002000

Surrogate%RecAcceptanceLimits2,4,6-Tribromophenol5236-1282-Fluorobiphenyl0D44-1102-Fluorophenol4141-110Terphenyl-d140010-112Phenol-d55043-110Nitrobenzene-d50036-110


AnalyticalData



LabSampleID:680-32249-31DateSampled:11/28120071550ClientMatrix:Solid%Moisture:18.1DateReceived:11/29/20070923

8270CSemivolatileCompoundsbyGasChromatography/MassSpectrometry(GCIMS)

Method:8270CAnalysisBatch:680-93535InstrumentID:GC/MSSemiVolatiles-TPreparation:3550BPrepBatch:680-92817LabFileID:t4270.dDilution:5.0InitialWeightNolume:15.26gDateAnalyzed:12/13/20071849FinalWeightNolume:.5mLDatePrepared:12/06/20071534InjectionVolume:1uL

AnalyteDrywtCorrected:YResult(ug/Kg)QualifierRL

JAcenaphthene<20002000Thionazin<20002000Sulfotepp<20002000Pyridine<200020001,1-Biphenyl<200020001,2,4,5-Tetrachlorobenzene<200020001,2,4-Tnchlorobenzene<200020001,2-Dichlorobenzene<200020001,3,5-Trinitrobenzene<200020001,3-Dichlorobenzene<200020001,3-Dinitrobenzene<200020001,4-Dichlorobenzene<200020001,4-Dioxane<200020001,4-Naphthoquinone<200020001-Naphthylamine<200020002,3,4,6-Tetrachlorophenol<200020002,4,5-Trichlorophenol<200020002,4,6-Trichlorophenol<2000200024-Dichlorophenol<2000200024-Dimethylphenol<200020002,4-Dinitrophenol<100001000024-Dinitrotoluene<200020002,6-Dichlorophenol<20002000Dimethylphthalate<2000200026-Dinitrotoluene<200020002-Acetylaminofluorene<200020002-Chlorophenol<200020002-Chloronaphthalene<200020002-Methylnaphthalene<200020002-Methylphenol<200020002-Naphthylamine<200020002-Nitroaniline<10000100002-Nitrophenol<200020002-Picoline<200020002-Totuidine<200020003&4Methylphenol<2000200033-Dichlorobenzidine<4000400033-Dimethylbenzidine<10000100003-Methylcholanthrene<200020003-Nitroaniline<10000100004,6-Dinitro-2-methylphenol<10000100004-Aminobiphenyl<200020004-Bromophenylphenylether<200020004-Chloro-3-methylphenol<20002000


AnalyticalData





Method:8270CAnalysisBatch:680-93535InstrumentID:GC/MSSemiVolatiles-TJPreparation:3550BPrepBatch:680-92817LabFileID:t4270.d

Dilution:5.0InitialWeight/Volume:15.26gDateAnalyzed:12/13/20071849FinalWeight/Volume:.5mLDatePrepared:12/06/20071534InjectionVolume:1uL

AnalyteDryWtCorrected:YResult(ug/Kg)QualifierRL4-Chloroaniline<400040004-Chiorophenylphenylether<200020004-Nitroaniline<10000100004-Nitrophenol<10000100004-Nitroquinoline-1-oxide<20000200007,12-Dimethylbenz(a)anthracene<20002000Acenaphthylene<20002000Acetophenone<2000

*

2000alpha,alpha-Dimethylphenethylamine<400000400000Aniline<40004000Anthracene<20002000Aramite,Total<20002000Benzo[a]anthracene<20002000Benzo[ajpyrene<20002000Benzo[b]fluoranthene<20002000Benzo[g,hj]perylene<20002000Benzo[k]fluoranthene<20002000Benzylalcohol<20002000Bis(2-chloroethoxy)methane79002000Bis(2-chloroethyl)ether<20002000Bis(2-ethylhexyl)phthalate<20002000Chrysene<20002000Diallate<20002000Dibenz(a,h)anthracene<20002000Dibenzofuran<20002000Di-n-butylphthalate<20002000Diethylphthalate<20002000p-Dimethylaminoazobenzene<20002000Dinoseb<20002000Di-n-octylphthalate<20002000Ethylmethanesulfonate<20002000Fluoranthene<20002000Fluorene<20002000Hexachlorobenzene<20002000Hexachlorobutadiene<20002000Hexachlorocyclopentadiene<20002000Hexachloroethane<20002000Hexachlorophene<10000001000000Hexachloropropene<20002000lndeno[1,23-cd]pyrene<20002000Isophorone<20002000Isosafrole<20002000Methapyrilene<400000400000Methylmethanesulfonate<20002000


AnalyticalData




827CCSemivolatileCompoundsbyGasChromatography/MassSpectrometry(GCIMS)

Method:8270CAnalysisBatch:680-93535InstrumentID:GC/MSSemiVolatiles-T

JPreparation:3550BPrepBatch:680-92817LabFileID:t4270.dDilution:5.0InitialWeightNolume:15.26gDateAnalyzed:12/13/20071849FinalWeightNolume:.5mLDatePrepared:12)06/20071534InjectionVolume:1uL

AnalyteDryWtCorrected:YResult(uglKg)QualifierRLNaphthalene<20002000Nitrobenzene<20002000N-Nitrosodi-n-butylamine<20002000

)N-Nitrosodiethylamine<20002000N-Nitrosodimethylamine<20002000N-Nitrosodiphenylamine<20002000N-Nitrosodi-n-propylamine<20002000N-Nitrosomethylethylamine<20002000N-Nitrosomorpholine<20002000N-Nitrosopiperidine<20002000N-Nitrosopyrrolidine<20002000

ON-Nitro-o-toluidine<20002000Pentachlorobenzene<20002000Pentachloronitrobenzene<20002000Pentachlorophenol<1000010000Phenacetin<20002000Phenanthrene<20002000Phenol<20002000p-Phenylenediamine<1000010000Pronamide<20002000Pyrene<20002000Safrole,Total<20002000o,o,o”-Triethylphosphorothioate290002000Disulfoton<20002000EthylParathion<20002000Methylparathion<20002000Phorate<20002000Famphur<20002000Dimethoate<20002000Butylbenzylphthalate<20002000bis(chloroisopropyl)ether<20002000

Surrogate%RecAcceptanceLimits2,4,6-Tribromophenol5536-1282-Fluorobiphenyl0044-1102-Fluorophenol5241-110Terphenyl-d140D10-112Phenol-d55843-110Nitrobenzene-d50D36-110


AnalyticalData



LabSampleID:680-32249-30DateSampled:11)28/20071530ClientMatrix:Solid%Moisture:18.8DateReceived:11)29/20070923

8081A_8082OrganochiorinePesticides&PolychlonnatedBiphenylsbyGasChromatography

RMethod:8081A_8082AnalysisBatch:680-92578InstrumentID:GCSemiVolatiles-M

JPreparation:3550BPrepBatch:680-92308LabFileID:m103013.dDilution:10InitialWeight/Volume:15.10gDateAnalyzed:12103/20071316FinalWeightNolume:5mLDatePrepared:11/30)20071149InjectionVolume:2uL

ColumnID:PRIMARY

AnalyteDryWICorrected:YResult(ug/Kg)QualifierRLAldrin<2121alpha-BHC<2121Chlordane(technical)<210210Chlorobenzilate<2102104,4-DDD<40404,4-DDE<40404,4’-DDT<4040delta-BHC2221Dieldrin<4040EndosulfanI<2121EndosulfanII<4040

OEndosulfansulfate<4040Endnn<4040Endrinaldehyde<4040Endrinketone<4040gamma-BHC(Lindane)<2121Heptachlor<2121Heptachlorepoxide<2121lsodnn<4040Kepone<21002100Methoxychlor<210210Toxaphene<21002100

Surrogate%RecAcceptanceLimitsDCBDecachlorobiphenyl0D50-129Tetrachloro-m-xylene0D26-140


AnalyticalData




8081A_8082OrganochlorinePesticides&PolychlorinatedBiphenylsbyGasChromatography

Method:8081A_8082AnalysisBatch:680-92578InstrumentID:GCSemiVolatiles-MPreparation:3550BPrepBatch:680-92308LabFileID:mI03016.dDilution:100InitialWeightNolume:15.10gDateAnalyzed:12/03/20071414FinalWeightNolume:5mLDatePrepared:11/30/20071149InjectionVolume:2uL

ColumnID:PRIMARY

AnalyteDryWtCorrected:YResult(ug/Kg)QualifierRLbeta-BHC<210210


AnalyticalData




8081A_8082OrganochlorinePesticides&PolychlorinatedBiphenylsbyGasChromatography

Method:8081A8082AnalysisBatch:680-92578InstrumentID:GCSemiVolatiles-M

JPreparation:3550BPrepBatch:680-92308LabFileID:ml03017.dDilution:10InitialWeight/Volume:15.17gDateAnalyzed:12/03)20071434FinalWeight/Volume:5mLDatePrepared:11/30/20071149InjectionVolume:2uL

ColumnID:PRIMARY

AnalyteDryWtCorrected:YResult(ugiKg)QualifierRLAldrin<2121alpha-BHC<2121Chlordane(technical)<210210Chlorobenzilate<2102104,4’-DDD<40404,4-DDE370404,4-DDT<4040delta-BHC3621Dieldrin<4040EndosulfanI<2121EndosulfanII<4040Endosulfansulfate<4040Endrin<4040Endrinaldehyde<4040Endrinketone<4040gamma-BHC(Lindane)<2121Heptachlor<2121Heptachlorepoxide<2121Isodrin<4040Kepone<21002100Methoxychlor<210210Toxaphene<21002100

Surrogate%RecAcceptanceLimitsDCBDecachlorobiphenyl0D50-129Tetrachloro-m-xylene0D26-140


AnalyticalDataClient:HerculesInc.JobNumber680-32249-1


LabSampleID:680-32249-31DateSampled:11/28/20071550ClientMatrix:Solid%Moisture:18.1DateReceived:11)29)20070923

8081A_8082OrganochlorinePesticides&PolychlorinatedBiphenylsbyGasChromatographyMethod:8081A8082AnalysisBatch:680-92578InstrumentID:CCSemiVolatiles-M

JPreparation:3550BPrepBatch:680-92308LabFileID:m103019.dDilution:100InitialWeightNolume:15.17gDateAnalyzed:12/03/20071513FinalWeightNolume:5mLDatePrepared:11)30/20071149InjectionVolume:2uL

ColumnID:PRIMARY

AnalyteDryWtCorrected:YResult(ug/Kg)QualifierRLbeta-BHC<210210


AnalyticalData



LabSampleID:680-32249-30DateSampled:11/28120071530ClientMatrix:Solid%Moisture:18.8DateReceived:11/29/20070923

8151AChlorinatedHerbicidesbyGC

]Method:8151AAnalysisBatch:680-93032InstrumentID:GCSemiVolatiles-SPreparation:8151APrepBatch:680-92620LabFileID:s108008.dDilution:1.0InitialWeightNolume:30.0gDateAnalyzed:12/08/20071031FinalWeightNolume:10mLDatePrepared:12/04/20071339InjectionVolume:1uL

ColumnID:PRIMARY

9AnalyteDryWtCorrected:YResult(uglKg)QualifierRL2,4,5-T<10102,4-D<1010Silvex(24,5-TP)<1010

Surrogate%RecAcceptanceLimits2,4-Dichlorophenylaceticacid9758-110


AnalyticalDataClient:HerculesInc.

JobNumber:680-32249-1

ClientSampleID:HER.DA2-112807


8151AChlorinatedHerbicidesbyGC

Method:8151AAnalysisBatch:680-93032InstrumentID:GCSemiVolatiles-SJPreparation:8151APrepBatch:680-92620LabFileID:s108009.d

Dilution:1.0InitialWeightNolume:30.1gDateAnalyzed:12/08/20071051FinalWeightNolume:10mLDatePrepared:12/04/20071339InjectionVolume:IuL

ColumnID:PRIMARY

AnalyteDryWtCorrected:YResult(ug/Kg)QualifierRL

j2,45-T<1010 2,4-D<1010 Silvex(2,45-TP)<1010

Surrogate%RecAcceptanceLimits2,4-Dichiorophenylaceticacid7258-110


DATAREPORTINGQUALIFIERS


LabSectionQualifierDescription

GC/MSVOA

EResultexceededcalibrationrange,secondarydilutionrequired.

XSurrogateexceedsthecontrollimits

DSurrogateormatrixspikerecoverieswerenotobtainedbecausetheextractwasdilutedforanalysis;alsocompoundsanalyzedatadilutionmaybeflaggedwithaD.

GC/MSSemiVOA

*LCSorLCSDexceedsthecontrollimits


GCSemiVOA

FMSorMSDexceedsthecontrollimits

4MS,MSD:Theanalytepresentintheoriginalsampleis4timesgreaterthanthematrixspikeconcentration;therefore,controllimitsarenotapplicable.


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]QUALITYCONTROLRESULTS

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QualityControlResults


QCAssociationSummary

Report

LabSampleIDClientSampleIDBasisClientMatrixMethodPrepBatch

GCIMSVOA

AnalysisBatch:680-92512LCS680-92512/16LabControlSpikeTWater8260BMB680-92512/18MethodBlankTWater826DB

g680-32249-2HER-CMO1-112607TWater826DB680-32249-3HER-CM02-112607TWater826DB

AnalysisBatch:680-92536LCS680-92536/5LabControlSpikeTWater8260BLCSD680-92536/6LabControlSpikeDuplicateTWater8260BMB680-92536/7MethodBlankTWater826DB680-32249-10HER-MWO5-112707TWater826DB680-32249-13HER-MWO8-1128D7TWater82608680-32249-25HER-RS1-112607TWater826DB680-32249-26HER-RS2-112707TWater826DB

AnalysisBatch:680-92548LCS680-92548/5LabControlSpikeTSolid826DB

OLCSD680-92548/6LabControlSpikeDuplicateTSolid826DBMB680-92548/7MethodBlankTSolid826DB680-32249-31HER-DA2-112807TSolid82608

AnalysisBatch:680-92567LCS680-92567/15LabControlSpikeTWater8260BMB680-92567/16MethodBlankTWater82608680-32249-1HER-CMDO-112607TWater826DB680-32249-4HER-CMD3-112607TWater826DB68D-32249-4MSMatrixSpikeTWater826DB680-32249-4MSDMatrixSpikeDuplicateTWater826DB680-32249-5HER-CMD4-112607TWater826DB680-32249-6HER-CMD5-112607TWater826DB680-32249-7HER-MWD2-112707TWater826DB68D-32249-7MSMatrixSpikeTWater826GB68D-32249-7MSDMatrixSpikeDuplicateTWater826GB680-32249-8HER-MWO3-112707TWater826DB

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ReportLabSampleIDClientSampleIDBasisClientMatrixMethodPrepBatch

GCIMSVOA

AnalysisBatch:680-92630LCS680-92630/11LabControlSpikeTWater826DB

MB680-92630/12MethodBlankTWater826DB680-32249-9HER-MWO4-112707TWater826DB680-32249-11HER-MWD6-112707TWater8260B680-32249-12HER-MWD7-1128D7TWater826DB680-32249-14HER-MWO9-112807TWater826DB680-32249-15HER-MW1O-112707TWater8260B680-32249-16HER-MW11-112707TWater826DB680-32249-17HER-MW12-112707TWater826DB680-32249-18HER-MW13-112807TWater826DB680-32249-19HER-MW14-112807TWater826DB680-32249-20HER-MW15-112807TWater8260B680-32249-21HER-MW16-1128D7TWater826DB680-32249-23HER-MW18-112707TWater826DB680-32249-28HER-FD1-112707TWater826DB

AnalysisBatch:680-92648LCS680-92648/9LabControlSpikeTWater826DBLCSD680-92648/10LabControlSpikeDuplicateTWater82606MB680-92648/11MethodBlankTWater826DB680-32249-12MSMatrixSpikeTWater826DB68D-32249-12MSDMatrixSpikeDuplicateTWater8260B680-32249-18DLHER-MW13-1128D7TWater82606680-32249-22HER-MW17-112807TWater826DB680-32249-24HER-MW19-112807TWater826DB680-32249-27HER-RS3-112807TWater826DB680-32249-29HER-FD2-112807TWater826DB680-32249-32TBTRIPBLANKTWater826DB

AnalysisBatch:680-92858LCS680-92858/8LabControlSpikeTWater826DBMB680-92858/9MethodBlankTWater826DB680-32249-22DLHER-MW17-112807TWater826DB

AnalysisBatch:680-92984LCS680-92984/3LabControlSpikeTSolid826DBMB680-92984/5MethodBlankTSolid826DB680-32249-30HER-DA1-1128071Solid826DB

epprtBasisT=Total

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GCIMSSemiVOA

PrepBatch:680-92817LCS680-92817/7-ALabControlSpikeTSolid3550BMB680-92817/6-AMethodBlankTSolid3550B

J680-32249-30HER-DA1-112807TSolid3550B680-32249-31HER-DA2-112807TSolid3550B

AnalysisBatch:680-93126LCS680-9281717-ALabControlSpikeTSolid8270C680-92817MB680-92817/6-AMethodBlankTSolid8270C680-92817

AnalysisBatch:680-93535680-32249-30HER-DA1-112807TSolid827CC680-92817680-32249-31HEl-DA2-112807TSolid827CC680-92817

ReportBasisT=Total

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GCSemiVOA

PrepBatch:680-92308LCS680-92308/10-ALabControlSpikeTSolid355DBMB680-92308/6-AMethodBlankTSolid3550B

j680-32249-30HER-DA1-112807TSolid355DB680-32249-3OMSMatrixSpikeTSolid35508680-32249-3OMSDMatrixSpikeDuplicateTSolid35508680-32249-31HER-DA2-112807TSolid3550B

AnalysisBatch:680-92578LCS680-92308/10-ALabControlSpikeTSolid8081A_8082680-92308MB680-92308/6-AMethodBlankTSolid8081A_8082680-92308680-32249-30HER-DA1-112807TSolid8081A_8082680-92308680-32249-3OMSMatrixSpikeTSolid8081A_8082680-92308680-32249-3OMSDMatrixSpikeDuplicateTSolid8081A_8082680-92308680-32249-31HER-DA2-112807TSolid8081A_8082680-92308

PrepBatch:680-92620

OLCS680-92620/4-ALabControlSpikeTSolid8151AMB680-92620/3-AMethodBlankTSolid8151A680-32249-30HER-DA1-112807TSolid8151A680-32249-31HER-DA2-112807TSolid8151A680-32249-31MSMatrixSpikeTSolid8151A680-32249-31MSDMatrixSpikeDuplicateTSolid8151A

AnalysisBatch:680-93032LCS680-92620/4-ALabControlSpikeTSolid8151A680-92620MB680-92620/3-AMethodBlankTSolid8151A680-92620680-32249-30HER-DA1-112807TSolid8151A680-92620680-32249-31HER-DA2-112807TSolid8151A680-92620680-32249-31MSMatrixSpikeTSolid8151A680-92620680-32249-3IMSDMatrixSpikeDuplicateTSolid8151A680-92620

ReportBaaIs

T=Total

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QualityControlResultsClient:HerculesInc.

SurrogateRecoveryReport

JobNumber:680-32249-1


ClientMatrix:Solid

LabSampleID

680-32249-30

680-32249-31

MB680-92548/7

MB680-92984/5

LCS680-92548/5

LCS680-92984/3

LCSD680-92548/6

ClientSampleID

HER-DA1-112807

HER-DA2-112807

BFBDBFMTOL%Rec%Rec%Rec

828772

OXOXOX

909892

738975

98102100

9410799

97102100

Surrogate

BFB=4-BromofluorobenzeneDBFMDibromofluoromethaneTOLToluene-d8(Surr)

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AcceptanceLimits65-12465-12465-132

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Documents

Client Matrix: Water Date Received: 11/29/2007 0923