54
CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465 Certificate of Test WE CERTIFY THAT THE CHEMICAL ANALYSIS AND MECHANICAL TEST RESULTS APPEARING IN THIS CERTIFICATE ARE CORRECT AND ACCURATE AS REPORTED BY THE MANUFACTURER. , S Jl BILL HUDSON PRODUCTS CORPORATION TO: ATTN: ACCTS PAYABLE 9660 GRUNWALD RD BEASLEY, TX 77417-8600 • CERTIFICATE OF COMPLIANCE: MATERIAL MEETS THE REQUIREMENTS OF YOUR PURCHASE ORDER. • THE RECORDING OF FALSE, FICTITIOUS OR FRAUDULENT STATEMENTS OR ENTRIES ON THIS DOCUMENT MAY BE PUNISHABLE AS A FELONY UNDER FEDERAL STATUTES INCLUDING FEDERAL LAW, TITLE 18, CHAPTER 47. • TEST RESULTS CONFORM WITH THE REQUIREMENTS OF EN 10204. Par 3.1.B CUSTOMER ORDER NO. 114936 TERRILL BOHNSACK, SANDMEYER STEEL COMPANY MANAGER - QUALITY ASSURANCE AND ENGINEERING DATE: 09/07/2016 GRADE:UNS S32205 HEAT#:858635 PC#:2AA DESCRIPTION PIECES SSC Type 2205 Plate PLATE NO 200469 3/8" X 90" X 133"/ SPECIFICATION: ASME SA-240 2015 ED / ASTM A240/A240M-13c . 2205 DUAL CERTIFIED (UNS S31803/S32205)'/ Additional Requirements: Material Has N0t Been Weld Repaired A923 C - OK 7 A923 Prac A- OK / Material Produced By Outokumpu Stainless, Inc.. This Material is Free From Mercury Contamination ******************************************Chemical Values****************************************** CO.022 ./ MIl 1. 14 ./ PO. 027 / SO. 001 / Si O. Ni 5.64 / Cr 22.4 / Mo 3.08 Cu 0.05 NO. 18 / Ti 0. 004 Nb 0. 01 Al 0.004 Sn 0.003 Cb + Ta 0.012 Co 0.09 Ta 0.002 Pb 0.001 PREN 35.440 Al + Ti 0.008 P+S 0.028 ******************************************Physical Values***************************:;,************ Yield (0.2%) (psi) 79,888 / / Tensile (psi) 113,920 . Elongation 37% In 2" . Reduction % 63% Hardness-RC 16 ;; Domestic True /' Date Slab Country of Great Britain ed Rolled Country of USA /" tgn . ------ Weld Repaired No \ *******************************************Testing Values******************************************* A923 C Pass /, A923 Prac A //. A370 BEND toc' I B277 II 09/07/2016 Page 3 of 3 /A4'x 90'A:/33 d

CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

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Page 1: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

Certificate of Test

WE CERTIFY THAT THE CHEMICAL ANALYSIS AND MECHANICAL TEST RESULTS APPEARING IN THIS CERTIFICATE ARE CORRECT AND ACCURATE AS REPORTED BY THE MANUFACTURER. , S

.1~C::I~)l Jl

BILL HUDSON PRODUCTS CORPORATION TO: ATTN: ACCTS PAYABLE

9660 GRUNWALD RD BEASLEY, TX 77417-8600

• CERTIFICATE OF COMPLIANCE: MATERIAL MEETS THE REQUIREMENTS OF YOUR PURCHASE ORDER. • THE RECORDING OF FALSE, FICTITIOUS OR FRAUDULENT STATEMENTS OR ENTRIES ON THIS DOCUMENT MAY BE PUNISHABLE AS A FELONY UNDER FEDERAL STATUTES INCLUDING FEDERAL LAW, TITLE 18, CHAPTER 47. • TEST RESULTS CONFORM WITH THE REQUIREMENTS OF EN 10204. Par 3.1.B

CUSTOMER ORDER NO. 114936 TERRILL BOHNSACK, SANDMEYER STEEL COMPANY MANAGER - QUALITY ASSURANCE AND ENGINEERING

DATE: 09/07/2016

GRADE:UNS S32205 HEAT#:858635 PC#:2AA

DESCRIPTIONPIECES

SSC Type 2205 Plate PLATE NO 200469

3/8" X 90" X 133"/

SPECIFICATION: ASME SA-240 2015 ED / ASTM A240/A240M-13c . 2205 DUAL CERTIFIED (UNS S31803/S32205)'/

Additional Requirements: Material Has N0t Been Weld Repaired A923 C - OK 7A923 Prac A - OK /

Material Produced By Outokumpu Stainless, Inc.. This Material is Free From Mercury Contamination

******************************************Chemical Values****************************************** CO.022 ./ MIl 1. 14 ./ PO.027 / SO.001 / Si O. 48~ Ni 5.64 / Cr 22.4 / Mo 3.08 Cu 0.05 NO.18 / Ti 0 . 004 Nb 0 . 01 Al 0.004 Sn 0.003 Cb + Ta 0.012 Co 0.09 Ta 0.002 Pb 0.001 PREN 35.440 ~ Al + Ti 0.008 P+S 0.028

******************************************Physical Values***************************:;,************ Yield (0.2%) (psi) 79,888 / / Tensile (psi) 113,920 . Elongation 37% In 2" . Reduction % 63% Hardness-RC 16 ~

::;;:**********************;::::**************Inventory********************~;;~~~~;;~~~~**;;

Domestic True /' Date J~ ~ Slab Country of Orig~n. Great Britain S· ed :;~. Rolled Country of Or~g~n USA /" tgn . ~ ----- ­Weld Repaired No \

*******************************************Testing Values******************************************* A923 C Pass /, A923 Prac A Pas~ //. A370 BEND TES~ P~ toc'

IB277 II

09/07/2016 Page 3 of 3

/A4'x 90'A:/33 ~LJ5'iJt//JLcX~7i d 858t35'~

Page 2: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

Page: 1

858635-2AA, /08/26/14

r-~--~outokumpu Outokumpu Stainless Plate, LLC I ;, ''''' ""f,~",~ ..,;,,_ ."" I r o QCerti~icate O(~naIPsis

.

OUR ORDER 0288163 - 01 HEAT .& PIECE i I

SOLD TO: SANDMEYER STEEL COMPANY SHIP TO: SANDMEYER STEEL COMPANY ONE SANDMEYER LANE ONE SANDMEYER!LANEI

PHILADELPHIA PA 19116! PHILADELPHIA PA 19116

YOUR ORDER & DATE -----------~-------------------

ITEM DESCRIPTION ------------------------------- ­! Lot No. 1640:i I /'UNS-S62205 ~ UNS-S318Q3 i

186.000 E ACT I Q : ~OO~b,

SPECIFICATIONS -----------~-------------------

fROf ~4~~i!iE~~~T~~M~LTED ELECTRIC AR ~ B ASpt5Y-~ifl ~~OF-40£)~Uk A"~'« 8-' NACE MR - 0

~g/~i'~CR~f~v~¥8~Bgg*~~is

------------------------------- ­

LIST HEAT/PCE/SIZE ON INVCE NO WELD RkpAI~S

Nb GRIPPER MARKS \ ,l I

PLATES &: TEST PCS ~SOLUTION ANNEALED @ 1950 DEGREES -·FAHRENHEIT~ MI·NIMUM.

iHii ~i5;RMiW~~~TAMINATION AT CURRE~DETECTION LIMITS HOT ROLLED, ANNEALED & PICKLED (HRAP)

----------------------------- MECHANICAL & OTHER TESTS -------------------------- ­HARDNESS HRC 16 /'YIELD STRENGTH (PSI) 79888/ I

I

TENSILE STRENGTH (PSI) 113920 ~ BEND OK

i

co~tinued

! I

ASTM A923 METHOD A OK~ I ELONGATION % IN 2" 37.4 ' REDUCTION OF AREA % 63.0

9 METHOD C CORROSION TEST M.D.

fP1~~~~~.'.rj?­~Cf,'t Outoku p'u Stainless Plate, LLC

P.O. Box 370 New Castle. Indiana 47362

Page 3: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

~ . ~outokumpu I Outokumpu Stainle~s Plate, LLC

high performance stainless stllel

(!Certificate of ~nalp5i5 anb \lI:est5 Page: 2

OUR ORDER 0288163 - 01 HEAT & PIECE 858635-2AA 08/26/14/ ;I

SOLD TO: SANDMEYER STEEL COMPANY SHIP TO: SANDMEYER STEEL COMPANY ONE SANDMEYER LANE ! ONE SANDMEYER LANE

PHILADELPHIA PA 19116 PHILADELPHIA PA 19116

- CHEMICAL COMPOSITION ---7 PRODUCT ANALYSI;V----------------~-------------------CARBON MANGANESE PHOSPHORUS

C MN P

.022/1 . 14 ,.,.

. 027 ~ SULFUR S .001 SILICON 51 .48~ CHROMIUM NICKEL COBALT

CR NI CO

22. 40 ~ 5.64/

.09 COPPER MOLY

CU MO

.05/3.08

NITROGEN COLUMBIUM

N CB

.18/

.010 TITANIUM TI .004 ALUMINUM TIN

AL SN

.004

.003 TANTALUM TA .002 PB PB .001

C .014 MN P S SI CRNI

1.11 ~ .921 /.90~ .~l ./

22.24/5.70

. j

CO .07 CU .04 MO N

3.06'/.20

CB TI AL SN

.p09

. P04

.p06

.001 TA !

WE HEREBY CERTIFY THAT THE MATERIAL HEREIN HAS BEEN MADE AND TESTED IN ACCORDANCE WITH-THE--LI-STE-D SPECIFICATION(S) AND !1'HATTHg..,·RESUL~S .. OF ALL TESTS ARE ACCEPTABLE. ;

I I

JAMES DOUSMAN/QUALITY ASSURANCE MANAGER

CERTIFICATE IN CONFORM~CE WITH EN10204-95 3 1.B/EN10204-2004 3.1 I

~~:::t~LLCP.o. Box 370 New Castle. Indiana 47362

Page 4: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

BILL HUDSON PRODUCTS CORPORATION Certificate of Test TO: ATTN: ACCTS PAYABLE WE CERTIFY THAT THE CHEMICAL ANALYSIS AND

9660 GRUNWALD RD MECHANICAL TEST RESULTS APPEARING IN THIS BEASLEY, TX 77417-8600 CERTIFICATE ARE CORRECT AND ACCURATE AS REPORTED

BY THE MANUFACTURER. • .' ') • CERTIFICATE OF COMPLIANCE: MATERIAL MEETS THE REQUIREMENTS OF YOUR PURCHASE ORDER. • THE RECORDING OF FALSE, FICTITIOUS OR FRAUDULENT STATEMENTS OR ENTRIES ON THIS DOCUMENT MAY BE PUNISHABLE AS A FELONY UNDER j·~cE~30 FEDERAL STATUTES INCLUDING FEDERAL LAW, TITLE 18, CHAPTER 47. • TEST RESULTS CONFORM WITH THE REQUIREMENTS OF EN 10204. Par 3.1.B

CUSTOMER ORDER NO. 114936 TERRILL BOHNSACK, SANDMEYER STEEL COMPANY MANAGER - QUALITY ASSURANCE AND ENGII\lEERII\lG

DATE: 09/07/2016

GRADE:UN5 532205 . HEAT#:858254 PC#:3A

DESCRIPTIONPIECES

SSC Type 2205 Plate ,/ PLATE NO 54494

1" X 31" X 90"/­

SPECIFICATION: ASME SA-240 2015 ED ./ ASTM A240/A240M-13c 1.205 DUAL CERTIFIED (UNS S31803/S32205)/

Additional Requirements: Material Has N,,9! Been Weld Repaired A923 C - OK A923 Prac A - OK ,/'

Material Produced By Outokumpu Stainless, Inc.. This Material is Free From Mercury Contamination

**********************/********************Chemical Val~s******************************************

C 0.021 Mn 1.14 / P 0.025 ~ S 0.001// Si 0.4 /"./ Ni 5.56 ./ Cr 22.56 Mo 3.03/ Cu 0.07 N 0.18/ Ti 0.004 Nb 0.009 Al 0.011 Sn 0.003 Cb + Ta 0.011 Co 0.1 Ta 0.002 Pb 0.001 PREN 35.440'/ Al + Ti 0.015 P+S 0.026

******************************************Physical Values****************************************** Yield (0.2%) (psi) 80,434 /" / Tensile (psi) 106,570 /' Elongation 38.3% In 2" Reduction % 53.8% Hardness-RC 17 / Anneal Temp (min) 1,950 ~

**********************************************InventorY*****************************************V?***t* NAFTA False CHECKED AND RELEASE Domestic True Date .' I" ? \ Slab Country of Origi~ Great Britain/ Signed, ~ j(.:-,

Rolled Country of Origin ~~

Weld Repaired No

*****************************~*************TestingValues******************************************* A923 C ./ Pass /

A923 Prac A .; Pass / (f II 8~7(G1\ ASTM A923 :a ,,/ T;;t'ed at -40C :(Ft-LbS)/129, 177, 148 (Mils' 60, 84, 82 Cr:u-'.'<.. . ASTM E562 % 45% ,7 H , A370 BEND TEST Pass /"

09/07/2016 Page 2 of 3

/-4. /~3/'/x7tJ/~~s OV;OPJ</l.a~ 85?,Z5t(·3A

Page 5: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

outokumpu Outokumpu Stainless Plate, LLC sta1n1esssteeJ.!Ihrghpe1'ormanc.e.al1oy.s

Page: 1

OUR ORDER 0287252 - 01 HEAT & PIECE 858254-3A 05/07/14

SOLD TO: SANDMEYER STEEL COMPANY SHIP TO: SANDMEYER STEEL COMPANY ONE SANDMEYER LANE ONE SANDMEYER LANE

PHILADELPHIA PA 19116 PHILADELPHIA PA 19116

-------------------------------- YOUR ORDER & DATE ------------------------------ ­62821 5/06/14 -------------------------~----- ITEM DESCRIPTION ------------------------------- ­HEAT & PIECE 858254 - 3A· Lot No. 9962 WEIGHT 8640 FINISH 1 GRADE 2205+2 / 2205 / UNS-S32205 / UNS-S31803'~ DIMENSIONS \;\ .l..:..QQ..Q. X 90.000 x ~24.000 EXACT .

-------------------------------- SPECIFICATIONS ------------------------------ ­*** MFG IN NEW CASTLE, IN, USA /' FROM SLABS IMPORTED FROM BRITAIN~

NACE MR0175-2009/ISO 15156 ASTM A240-13C ASMESA240-13ED~ ASTM A480-13 ASMESA480 13ED MELTED ELECTRIC ARC ~THOD/ REFINED A.O.D. PROCESS ASTM A 923-08 METH A,B(& C ./REQUIRES PRODUCT ANALYSIS UHA 51 CHARPY @ -40F (-40C)/ ASTM E562-08 (10% ACCURACY)' NACE MR0103-2012;;; 97!23!EC ANNEX 1 PARA 4.3 . 97/23/EC PED #228/2004/MUC MEETS EU ELECTRICAL ROHS NO WEEE RELEVANT SUBSTANCES LIST HEAT/PCE/SIZE ON INVCE NO GRIPPER MARKS NO WELD REPAIRS

PLATES & TEST PCS SOLUTION ANNEALED @ 1950 DEGREES FAHRENHEIT MINIMUM. THEN WATER OUENCHED? FREE FROM MERCURY CONTAMINATION ~T CURRENT DETECTION LIMITS HOT ROLLED, ANNEALED & PICKL~D ~(HRAP)

~ARD~~SS-~RC-------------~;-;rMECHANICAL & OTHER TESTS -------------------------- ­

YIELD STRENGTH (PSI) 80434~ TENSILE STRENGTH (PSI) 106570~ BEND OK ASTM A923 METHOD A OK / ELONGATION % IN 2" 38.3 "/ REDUCTION OF AREA % 53.8 /

CHARPY TEST AT -40F (TRANS) 177 FT-LBS. SAMPLE SIZE FULL A923 METHOD C CORROSION TEST M.D.D. = 0.00 @ 25 DEGREES C 24HRS./CHARPY TEST AT -40F (TRANS) 129, 177, 148 FT-LB~ ../FULL SAMPLE SIZ; SHEAR % = 100%, 100%, 100% /LATERAL EXPANSION = 60, 84, 82 (MILS) ~ / ASTM_.~~J21__ PQINT COUNT FERRITE @ 500X = 45% AT 10% RELATIVE ACCURACy:"

-- Continued - ­

~:~:::LCpo. Box 370 New Castle. Indiana 47362

Page 6: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

outokumpu Outokumpu Stainless Plate, LLC st..3nnle!.S steel &,. hittl performance ~kry5

Page: 2

OUR ORDER 0287252 - 01 H;;,;;E=A,;;,;;T;..."",;;o& P.._I.._E....C_E_.;;..S;;;..58;;.;2;;,,;5;;;..4;;;..-....;;3~A / 05/07 / 14

SOLD TO: SANDMEYER STEEL COMPANY SHIP TO: SANDMEYER STEEL COMPANY ONE SANDMEYER LANE ONE SANDMEYER LANE

PHILADELPHIA PA 19116 PHILADELPHIA PA 19116

- CHEMICAL COMPOSITION --~- PRODUCT ANALYSIjY ----------------------------------- ­CARBON (C ) .021 (C ) .009 MANGANESE (MN) 1.14 '/ (MN) 1.15 'l PHOSPHORUS (P ) .025 / (P ) .020/SULFUR (S ) .001 (S ) .00:" SILICON (SI) .40/' (8I) .34/CHROMIUM (CR) 22.56/ (CR) 22.75 /NICKEL (NI) 5.56/ (NI) 5.44 COBALT (CO) .10 (CO) .10 COPPER (CU) .07 (CU) .06/MOLY (MO) 3.03// (MO) 3.07/NITROGEN (N ) .1S ...... (N ) .20 COLUMBIUM (CB) .009 (CB) .010 TITANIUM (TI) .004 (TI) .006 ALUMINUM (AL) .011 (AL) .009 TIN (SN) .003 (SN) .001 TANTALUM (TA) .002 (TA) PB (PB) .001

WE HEREBY CERTIFY THAT THE MATERIAL HEREIN HAS BEEN MADE AND TESTED IN ACCORDANCE WITH THE LISTED SPECIFICATION(S) AND THAT THE RESULTS OF ALL TESTS ARE ACCEPTABLE.

JAMES DOUBMAN,QUALITY ASSURANCE MANAGER

CERTIFICATE IN CONFORMANCE WITH EN10204-95 3.1.B/EN10204-2004 3.1

~:~:::::LCPO Box 370 New Castle, Indiana 47362

Page 7: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

SANDIVIEVER STEEL COMPANY

BILL HUDSON PRODUCTS CORPORATION TO: ATTN: ACCTS PAYABLE

9660 GRUNWALD RD BEASLEY, TX 77417-8600

• CERTIFICATE OF COMPLIANCE: MATERIAL MEETS THE REQUIREMENTS OF YOUR PURCHASE ORDER. • THE RECORDING OF FALSE, FICTITIOUS OR FRAUDULENT STATEMENTS OR ENTRIES ON THIS DOCUMENT MAY BE PUNISHABLE AS A FELONY UNDER FEDERAL STATUTES INCLUDING FEDERAL LAW, TITLE 18, CHAPTER 47. • TEST RESULTS CONFORM WITH THE REQUIREMENTS OF EN 10204. Par 3.'I.B

CUSTOMER ORDER NO, 114936 TERRILL BOHNSACK, SANDMEYER STEEL COMPANY MANAGER - QUALITY ASSURANCE AND ENGINEERING

DATE: 09/07/2016

Certificate of Test

WE CERTIFY THAT THE CHEMICAL ANALYSIS AND MECHANICAL TEST RESULTS APPEARING IN THIS CERTIFICATE ARE CORRECT AND ACCURATE AS REPORTED BY THE MANUFACTURER.

GRADE:UNS S32205 I IHEAT#:858007 PC#:1A. /

PIECES

1" X 96" X 241" /

SPECIFICATION:

DESCRIPTION

SSC Type 2205 Plate /

ASME SA-240 2015 ED / ASTM A240/A240M-13c /' 2205 DUAL CERTIFIED (UNS S31803/S32205/

Additional Requirements: Material Has Not Been Weld Repaired A923 C - OK /" A923 Prac A - OK /'

PLATE NO 54303

~~"l~2/511

1

Material Produced By Outokumpu Stainless, Inc.. This Material is Free From Mercury Contamination

******************************************Chemical Valu~******************************************

CO.021 ,/ Mn 1. 120 / PO.024 / SO.00100 /' Si 0.380 /" Ni 5.560 ./ Cr 22 . 420 /' Mo 3 . 030 /' Cu 0 . 130 N 0.180 /' Ti 0.003 Nb 0.0070 Al 0.0110 Sn 0.010 Cb + Ta 0.011 Co 0.090 Ta 0.004 Pb 0.001 PREN 35.299/ Al + Ti 0.014 P+S 0.025

******************************************Physical Values****************************************** Yield (0.2%) (psi) 78,813 ./ ./ Tensile (psi) 107,540 /' Elongation 38.2% In 2" Reduction % 57.1% / Hardness-RC 20/' Anneal Temp (min) 1,950 .r

**********************************************Inventory********************************************** NAFTA False CHECKED AND RElEASED Domestic True Date ;., " Slab Country of Origin Great Britain / Signed~~~~tad~~a;.v Rolled Country of Origi~ ~,~

Weld Repaired No

*******************************************Testing Values******************************************* A923 C /" ~,/ A923 Prac A/ ~,/ /: /. ASTM A923 B / Tested at -40C (Ft-Lbs) 226, 227, 243 (Mils) 93, 93, 99 11- /(8 /7,£:;1

~;.,.=....:;;;.;;;..;;~;:;..::;..-~

ASTM E562 % 47% A370 BEND TEST Pass (1~L ~ J

09/07/2016 ," , ,,I ,Page1 of 3

112 / ~ 70 'x ,21/ .~.lIJ5f)i/;t'~ /l..tJ~ J.fr '?5?aJ?-1A

Page 8: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

outokumpu Outokumpu Stain~ess Plate, LLC high "e,fo/mane" sl"inl.,,;~ sle,,1

*****~~f!j!!H!~e of ~naI!,sis anb 'arests, '2, * RE':'CERTIFICATION * ~(/ L1\./******************** v' UlIl3 p

Page: 1 h ~"I OUR ORDER 0286487 - 16 HEAT & PIECE 858007-1A 10/05/15 II SOLD TO: SANDMEYER STEEL COMPANY SHIP TO: SANIDMEYER STEEL COMPANY

ONE SANDMEYER LANE ONE SANDMEYER LANE

PHILADELPHIA PA 19116 PHILADELPHIA PA 19116

YOUR ORDER & DATE ------------------------~~~e~62772 2/17/14--------------------------;V----- ITEM DESCRIPTION ------------------------------- ­HEAT & PIECE 858007 - 1A Lot No. 0000 WEIGHT 8960 FINISH 1 GRADE 2205+2 / 2205'/ UNS-S322QS I QNS-S31803"/ DIMENSIONS t .'1 L.Q.Q.Q X 120.000 X 2S2.000 EXACT

SPECIFICATIONS -----------------~------------:~~-~FG-I~-NEw-cAs~iE~-IN~-usA~~ FROM SLABS IMPORTED FROM BRITAIN NACE MR0175-2009/ISO 15156 ASTM A240-1SA ASME SA240-13 "7 ASTM A480-14B ASMESA480 13ED MELTED ELECTRIC ARC METHOD /REFINED A.O.D. PROCESS ASTM A 923-08 METH A,~[& C'/ REQUIRES PRODUCT ANALYSIS .~ ORA S1 CHARPY @ -40F (-40C) ASTM E562-08 (10% ACCPRACYr NACE MR0103-2012/97!23!EC ANNEX 1 PARA 4.3 97/23/EC PED #228/2004/MUCMEETS EU ELECTRICAL ROHS NO WEEE RELEVANT SUBSTANCES LIST HEAT/PCE/SIZE ON INVCE NO GRIPPER MARKS NO WELD REPAIRS

DETECTION LIMITS HOT

----------------------------- MECHANICAL & OTHER TESTS -------------------------- ­HARDNESS HRC 20 /' / YIELD STRENGTH (PSI) 78813 TENSILE STRENGTH (PSI) 107540/ BEND OK . ASTM A923 METHOD A ~.~

2 11ELONGATION % IN 38.2 /' REDUCTION OF AREA % 57.1

THE RECORDING OF FALSE, FICTITIOUS OR FRAUDULENT STATEMENTS OR RECORDS MAY BE PUNISHABLE AS A FELONY UNDER FEDERAL LAW. CHARPY TEST AT -40F (TRANS) 243 FI-LBS SAMPLE SIZE FULL ~

_A?23 METHOD C CORROSION TEST M D D. - 0 O~<@ 25 DEGREES C 24HRS.~ CHARPY TEST AT -40F (TRANS)~26, 227, 243>FT-LBS. FULL SAMPLE SIZE SHEAR % = 100%, 100%, 100% LATERAL EXPANSION = 93, 93, 99 (MILS).r ASTM E-562 POINT COUNT FERRITE @ SOOX - 47% AT lot RELATIVE ACCURACY~

-- Continued - ­

(.

~:~=:t~UC549 west Stale Road 38 New Castle, Indiana 47362

I

Page 9: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

outokumpu Outokumpu Stainless Plate, LLC hieh petfo,marice sl ..inl.....~ sleel

***J(~!!jl(f!!~e of QInalpsis anb ijCests ..1­* RE-CERTIFICATION * 111, / .

******************** Page, U(~13to2 (~,.OUR ORDER 0286487 - 16 HEAT & PIECE 858007-1A /;'0/05/15

SOLD TO: SANDMEYER STEEL COMPANY SHIP TO: SANDMEYER STEEL COMPANY ONE SANDMEYER LANE ONE SANDMEYER LANE

PHILADELPHIA PA 19116 PHILADELPHIA PA 19116

- CHEMICAL COMPOSITION ---~ PRODUCT ANALYSI;V----------------------------------- ­CARBON (C ) .021 (C ) .014 MANGANESE (MN) 1.12 "/ (MN) 1.09 ~ PHOSPHORUS (P ) .024 /' (P ) .016/SULFUR (S ) .001/ (S ) .009' SILICON (SI) .38/ (SI) .35 CHROMIUM (CR) 22.42/' (CR) 22. 26~ NICKEL (NI) 5.56/ (NI) 5.72 COBALT (CO) .09 (CO) .08 COPPER (CU) .13/ (CU) .12/MOLY (MO) 3.03 ./ (MO) 3.06/NITROGEN (N ) .18 ..... (N ) .20 COLUMBIUM (CB) .007 (CB) .008 TITANIUM (TI) .003 (TI) . 002 ALUMINUM (AL) . all (AL) . alB TIN (SN) . 010 (SN) .001 TANTALUM (TA) .004 (TA) PB (PB) .001

WE HEREBY CERTIFY THAT THE MATERIAL HEREIN HAS BEEN MADE, SUPPLIED, AND ~ . TESTED IN ACCORDANCE WITH THE LISTED SPECIFICATION(S) AND THAT THE

RESULTS OF ALL TESTS AND INSPECTIONS ARE ACCEPTABLE.,I

JAMES DOUBMAN,QUALITY ASSURANCE MANAGER

CERTIFICATE IN CONFORMANCE WITH EN10204-95 3.1.B/EN10204-2004 3.1

I t

J

I· I·

~:~=:LC549 YVest state Road 38 New Castle. Indiana 47362

Page 10: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

INSPECTION CERTIFICATE Number: 590659 Rev: 00EN 10204:2004 / 3.1 Page: 1/3

• Created on: Date: 10/09/2013

TUBACEX TTl - TUBACEX TUBOS INOXIDABLES Regislro Mercanlil de Alava, Tomo 587, Folio 189, Roja VI 2885 - NJ.F. A-O! 140227

Tres cruces, 8 11..: +34946719300

01400 L1odio (Alava) FAX: +34946125062

SPAIN E-MAIL: [email protected]

CUSTOMER DESCRIPTION

Modified on:

CLIENT SOLD TO CLIENT SHIP TO MULTALLOY INC. MULTALLOY INC. 8511 MONROE STREET 8S II MONROE STREET HOUSTON TX 77061 HOUSTON TX 77061 USA USA

CLIEl'.'T ORDER: 212739-00

SALES ORDER: 136551

MATERIAL:SEAML. STAINL. STEEL TUBES/PIPES.

HEAT-TREATED, PICKLED, PICKLED-PASSIVATED ~

GRADEl 531803,532205 1.4462, ~

STANDARD: ASME SECT.II PART.A SA790/SA790M-2010 ED. 2011 ADD.~ ASTM A790/A790M-12 CHECKED AND EN ~0215-512004 TCl

CORROSION TESTED ACC. TO ASTM A923 TEST METHOD A ~

CORROSION TESTED ACC. TO ASTM A923 TEST METHOD B/ CORROSION TESTED ACC. TO ASTM A923 TEST METHOD C ~ CORROSION TESTED ACC. TO ASTM G48 TEST METHOD A

DOW GBS-4001-51/07-APR-2011

FERRITE CONTENT IN Ace. WITH ASTM ES62-11~ NACE MROI03-2012

NACE l~017S/ISO 15156-3:2009

TOLERANCES: ASME SECT.II PART.A SA999/SA999M-2010 ED. 2011 ADD.

ASTM A999/A999M-12

EN 150 1127/03.97 D2/T2

RANDOM LENGTHS 10 I - 20 I R/L

PLAIN ENDS, /DIMENSIONS: 8" SCM 120

HOT FINISHED

Sales Hem Client Ilem Deliver), No Lot No. / Heat No / Pieces Weight Tot I.glh Un Lgth I 100 8110029635 2001I2J06 ..11221 1 451 KG 4.99 M 304&-6096 MM

Date.......~I'7A.-.r,,;:;;.-...,.y Signed,~~~~~~,

RAW MATERIAL Heftt Nr: Supplier / Method .£22L ACERALAVA (SPArN) Electric fumace+AOD

CHEMlCAL COMPOSITION (%) ·L: Ladle C:Products Hcat Seq C Mil Si P s Ni Cr Mo N

Page 11: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

I

Rev: 00

Modified on:

INSPECTION CERTIFICATE Number: 590659EN 10204:2004 / 3.1 Page: 2/3

Created on:• Date: 10109/2013

TUBACEX CHEMICAL COMPOSITION (0/0) "L: Ladle C:Producls

Ueat Seq C / Mn/ 51/ P S Ni / Cr / Mo N / L 47697 / 1 0.015 ; 1.02 0.400 0.026 / 0.0005 / 5.25 22.65 3.09 / 0.1815

IHEAT TREATMEi\'TISOLUTION ANNEALED AT 1075 °C, 25 min WATER /

TENSILE TEST Lot No. Sample T RpO.2 Rpl.O Rot A2" AS Type Spc.Type Spc.Dim

°C MPa / MPa MPa/ % % 111m

200112306 / 1 20' 535 595 745 46 / 45 L S 12.50

HARDI\"ESS TEST Lot No. Sample HRCl HRC2 200112306 1 20,0 '/21,0 /

rL\IPACf TEST A923 I1BII ./ T Wspec EC\'1 Ecv2 Ec\'3 Ec\'A\'G Type

°C J J J J/ mm -40 - 10,00 293 282 286 287 ./ L

T Pits-20x Wloss time °C MDD /loms 25 N 1,7800 / 24.0

T Plts·20x W.loss time °C g/m2 Horns 25 N 0,1800 24.0

%FeJ' Dev.Fcrr % %

51,39/ 1,64

Lot No. Sample

200112306 / I

CORROSION ACCORDING TO ASTM A923 C / Lot No, Sample

200112306/ 1

CORROSION ACCORDING TO ASTM G48A Lot No. Sample

200112306 I

l,'ERRITE ACCORDL~G TO ASTM E 562 Lot No. Sample

200112306 1

METALURGICAL TESTS ETCH STRUCTURE ACC. ASTM A923 MET.A: ~AFFECTED STRUCTURE. MATERIAL FREE

FROM INTERMETALLIC PHASES AND PRECIPITATBS. UNIFORM STRUCTURE ACROSS

FULL WALL THICKNESS ~

INTERGRANULAR CORROSION TEST ACe. TO ASTM A262 PRACT. "E": SATISFACTORY /'

NON-DESTRUCTIYE TESTS

POSITIVE MATERIAL IDENTIFICATION TEST ON EACH TUBE/PIPE BY "X-RJ\Y-FLUORESCENCE-ANALYZER": SATISFACTORY /'

~YDROSTATIC PRESSURE TESTED AT 190 bar, 2800 PSI DURING 5 SEC ON EACH ,~

Ga AENOR

TUBACEX TUBOS INOXIDABLES S.A.

AENOR

~ Gesll6nEn"r-r~ AmbleilUI

lOo.u"rosan R~,i$lJada

l,,~..(\i601c.xl ~

Page 12: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

INSPECTION CERTIFICATE EN 10204:2004 / 3.1 Number: 590659 Rev: 00

Page: 3/3

TUBACEX• Created on: Modified on: Date: 10/09/2013

TUBE/PIPE: SATISFACTORY

DIMENSlONAL CHECKING ON EACH TUBE: SATISFACTORY~

VISUAL INSPECTION ON EACH TUBE: SATISFACTORY ~

TECIL~OLOGICAL TESTS

fLATTENING TEST: SATISFACTORY /

RING TENSILB TEST: SATISFACTORY

IMARKING TX3 TUBACEX 8" SCH 120 ASME SA790 ASTM A790 EN 10216-5 TCl S31803 832205 1.4462 HFD HF SMLS HEAT/ PMI-AV LOT NO/ SPAIN

REMARKS

NO MERCURY, MERCURY COMPOUNDS OR MERCURY BEARING INSTRUMENTS AND/OR EQUTPMEl'rr HAVE BEEN USED ALONG MANUFACTURING Ai\1D INSPECTION PROCESS.

NO WEWlNG OR WELD REPAIRS WERE MADE

MATERIAL MANUFACTURER APPROVED BY TOY sOD Industrie Service GmbH (NOTIFIED BODY 036)TO ISSUE CERTiFICATES OF SPECrFIC PRODUCT CONTROL TN ACCORDING TO PRESSURE EQUIPMENT Dffi.ECTIVE 97/2J/EC ANNEX 1 rOINT 4.3.

MATERIAL CHARACTERISTICS COMPLY WITH POINT 7.5 OF ANNEX ITO PED BY HAVTNG AN ELONGATION AFTER RUPTURE AT TENSll..E TEST NO LESS THAN 14% AND A BENDING RUPTURE Er-..TERGY AT L\1.PACT TEST NO LESS THAN 27J AT 20°C.

MATERIAL]5 FREE OF RADIATION CONTAMINATION

AENOR AENOR TUBACEX TUnOS

~ G~ INOXIDABLES S.A.

EfIlV~ Rtg;s~

Gestloo ,l.mbienlal ~V<C·C"SOlQ)l

Page 13: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

MTEC Mechanical Testing Services ISO 9001-2008 8676 Taub Rd. I Houston, Texas 77064 I 281-469·2609 ISO/IEC 17025:2005

ACCREDITED

CERTIFICATE OF TEST LAB# W16012951

Certified Customer: 09-09·2016 09:26

PO NO 496254-00 J & J, INC. aTC 8" S120 3"l SMlS PIPE / 7311 GALVESTON RD. #800 MATl TYPE SA790 S32205 ./ HOUSTON, TX 77034 HEAT NO 47697 ,/

SPEC A923 METHOD B/UHA-51 (A)(2) ./Attn: PAOLO ESTRADA

TEST DATA CHARPY V NOTCH TEMP(F) FT/LBS UE MILS %D/F DIM aRlEN LaC

-40 228.7 100 100 10X10mm LONG MW 177.4 95 100 210.5 98/' 100/

AVG 205.5 ./

~)~ lJqQQ~__ IIta Hall, MTEC Representative

The recording of false, fictitious, or fraudulent statements or entries on this document may be punishable as a felony under federal statute. MTEG is accredited to ISO/lEG 17025:2005 for testing by PJLA. Accreditation No 70049.

Uncertainly information, pertinent to ISO 17025 Accredited Results, is available upon request.

Page 1 of 1

Page 14: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

II CERTIFIED MATERIAL TEST REPORT R8.2.4.4 Rev. E

Rev. Date 10/31/2012 Made in the USA /

Inspection Certificate 3.1 ace. to DIN EN 10 204 IISO 10474

Page 1 of 2

Certificate date 8/10/2015

Certificate No. MTR22234

Revision 0

Firma Our Order: USAOO0167

Schulz USA Inc. Our Item: 006 77032 Houston Your PO: 0013375

Your Item: 006

Our Ref: SXP\acavazos

Component

SXP USA ASTM A790

Material Grade: S31803/S32205 /

SML Pipe ./ S31803/S32205

175ft I 12" SCH 80S 12" SCH 80S ./ I7tN#:56238 •./

UT, SML Requirements

Raw Material: ASTM A 182/A 182M - 12a, ASTM A 276 - 10, ASTM A 479/A 479M - 10a, EN 10088-3

CHECKED, ~~~. 'tELEASED Product Form: ASTM A 790/A 790M - 09a, NORSOK M-630 MDS 041. Rev 4, NACE MR0175/.... Date 1/ . , - j(;

Description Seamless Pipe ./ Marking

Class:

Quantity:

Dimensions:

Iso 15156-3:2009/CIr.1 :2001 (E) Sign8d 4H: ~ .u ,

~

r/~End Type Plain Ends

Mfg. Method Extruded I Heat Treatment /'

solution annealed 1060 'C 1940'F Water Quenched ~

Chemical Analysis

0.015 1.560~ 0.025~

C Mn ~ P

Steel Making Process EAF/AOD I S Si MoC Mn P NHeat ~ Cr J NI Cu I PREN I....

Heat 56238 / 0.0011 0.310 22.490~

SI " Cr '" Ni

5.820. 1t'"3.200.J 0.190 ~ 0.233 I 36.090 r S MoProduct ./ N

/Product 1.510" 0.0261 <0.001 0.250 J 22.700J 5.900 ~ 3.100 ~ 0.160 ~,56238 0.014 J

Mechanlca I Properties

Tensile Test

I Test No. r Charge I specimen Test YS IS EI Ra

I lOr. Size Temp. RpO,2 % Rp1,O % Rm 40 Z

I 000860-006 I ./

56238' I L

In 'C 'F 20 I 68

MPa KSI .....-MPa KSI

1

MPa KSI

796 /115.40'

% % Std 548 I 79.5 ~ 35.0 ' 80.0

Hardness Test

IRockwell 8: < 96.4 7

Impact Test

Test No. I Charge specimen Temp Impact Energy In J LE (mm)

Or. I Size (mm) 'C 'F 1/ 1 I 2 I 3 I Average 1 I 2 I 3

000860-006 r 56238 L 110.00 x 10.00 -46 / -51 J 256 I 255 / 245 / 252 " r r

Page 15: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

CERTIFIED MATERIAL TEST REPORT

Made in the USA / Inspection Certificate 3.1 acc. to DIN EN 10204/18010474•

R8.2.4.4 Rev. E Rev. Date 10/31/2012

Page 2 of 2

Certificate date 8/10/2015

Certificate No. MTR22234

Revision 0

Mandatory Tests /'

Positive Material Identification PMI was performed on each piece of pipe and was found satisfactorYI VerwechselungsprOfung ohne beanstandung.

Visual and DImensional Insp. satisfactory /'

Metallurgical Requirements Micro-Examination Per ASTM E562 law NORSOK M-630 with a ferrite content of 45.31%. Microstructure examined at a

minimum of 400X magnification and is free from intermetallic phases and precipitates 1ohne beanstandung.

Corrosion Resistance Ferric Chloride corrosion test per ASTM G48, Method A @ 25'C for 24hrs with a weight loss of 0.2174 g/m2 and no evidence of pitting at 20X.

Additional Mech nlcal Properties Flattening Test Test performed per ASTM A790 with satisfactory results 1Faltprobe nach A790 ohne beanstandung.

Nondestructive Test Results ~

Ultrasonic Examination / 1100% tested In accordance with ASTM E213 with satisfactory result~7 UltraschallprOfung nach E213 Iohne Beanstandung

No repair by welding was performed on the material. I Kelne Reparaturschweir!ung. Material is free of low melting point material and radioactive contamination. 1Das Material ist frel von Verunrefnlgungen mit Material mit nledrigem Schmelzpunkt und Radioaktlvital.

This testimonial and certification Is recorded by computer system and Is valid without signature. Alteration or use for other products are regarded as falsification of documents and will be subject to criminal jurisdiction.

THIS IS TO CERTIFY THAT THE CONTENT OF THE REPORT IS CORRECT AND ACCURATE AND THAT ALL TEST RESULTS AND OPERATIONS PERFORMED BY SCHULZ OR ITS SUBCONTRACTORS ARE IN COMPLIANCE WITH THE MATERIAL SPECIFICATIONS LISTED IF SO STATED ELSEWHERE IN THIS CMTR AND WAS FOUND TO MEET THE REQUIREMENTS. WE HEREBY CERTIFY THAT THE MATERIAL USED FOR PRODUCT FORM CONVERSION CONFORMS TO THE APPLICABLE DIMENSIONAL REQUIREMENTS.

8/10/2015 Pat Sullivan Date Authorized Inspection Representative

Page 16: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

MTEC Mechanical Testing Services ISO 9001·2008 8676 Taub Rd. IHouston, Texas 77064 I281-469-2609 /l ISOIIEe 17025:2005

ACCREDITED.~~ ~ CERTIFICATE OF TEST LAB# W16013781rL7

1ilS :ft Certified

Customer: PO NO 502494-00 10-06-201611:31 'QTC 12" S80S C,500"W) X 3"l SMLS PIPE../'J &J, INC. »...~~:.,",~~

MATl TYPE 2205 77311 GALVESTON RD. #800 HEAT NO 56238 ./'

HOUSTON, TX 77034 SPEC A923 METHOD B/UHA-51<Al (2VA923 A A923 C Attn: PAOLO ESTRADA ORDER NO 171004-00

/ TEST DATA CHARPY V NOTCH ;;

FT/LBS UE MILS %D/F DIM ORIEN LaCTEMPC" -40 225.4 105 100 10X10mm LONG MW

239.5 105 100 246.4 110/ 100

AVG 237.1 "/

ETCH TEST (ASTM A923 METHOD A) ./ The polished specimen was electrolytfcally etched in aqueous sodium hydroxide solution at 3V dc for 5 to 60 seconds.

The specimen was then thoroughly rinsed in hot water and in alcohol, then air dried.

The etched surface was examined under a metallurgical microscope at 500X.

Results: UNAFFECTED STRUCTURE. /'

500X

CORROSION TEST (ASTM A923 METHOD C) 7 (this test continues on next page)

The recording of false. flct/tlous, or fraudulent stetements or entries on this document may be punishable as a felony under federal statute. MTEC Is accredited to ISOIIEC 17025:2005 for testing by PJL.A. Accreditation No 70049.

Uncertainly Information, pertlnent to ISO 17025 Accredlfed Resulls, Is available upon request.

Page 1 of 2

Page 17: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

MTEC Mechanical Testing Services ISO 9001-2008 8676 Taub Rd. IHouston, Texas 770641281-469-2609 . ~ ISO/IEC 17025:2005

ACCREDITED

~lv/j13qCERTIFICATE OF TEST LAB# W16013781

:/\\:J Certified Customer: PONO 502494-00 / 10·06·2016 11 :31

QTC 12" 5805 <.500"Wl X 3"L SMlS PIPE ·~bo$ ...iCjnloll.J &J, INC. . .

"~ :JIo<f.......

MATl TYPE 2205 I7311 GALVESTON RD. #800 HEAT NO 56238 ./HOUSTON, TX 77034 SPEC A923 METHOD B/UHA-51 (A) (2)/A923 A,A923 C / Attn: PAOLO ESTRADA ORDER NO 171004-00

TEST DATA (continued fronyprevlous page)

CORROSION TEST (ASTM A923 METHOD C) (cont.) / TEST PERIOD :24 hrs TEST TEMP :25C / RATE =8.480 mdd

No pitting observed @ 20X See attached report

~)~ LJcJ&~__ llta Hall, MTEC Representative

The recording of false, flctlUous, or fraudulent statements or entries on this document may be punishable as a felony under federal statute. WEe is accredited to ISOIIEe 17025:2005 for lesting by PJu.. Accreditation No 70049.

Uncertainty InformaUon, pertinent to ISO 17025 Acaedlted Results, Is available upon request.

Page 2 of2

Page 18: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

MTEC MECHANICAL

TESTING SERVICES

Test Certificate

Customer: J&J Date 10/6/2016 MTECWO#: 16013781 HT#: MATL: 2205

ASTM A923 METHOD "e" CORROSION TESTING - Weight loss rate calculation I Test Period 24hrs Test Temp. 25C

square/Rectangular prepared specimen rom

50.94 0.5094 dm 25..19 0.2519 dm 6.38 0.0638 dm

L W T

Initial weight: Final wei ht: Weight loss

3 m

I L I w 1 T AREA

1 0.50941 0.25191 0.0638 2 faces LxWx2= 0.25663572 2 ends WxTx2= 0.03214244

63.452 9 2 sides LxTx2= 0.06499944

63.449 9 total area = 0.3537776 dm2 I

rate :: 8.480 mdd

Observations @ 20X No Pitting Observed

MTEC REP.

Page 19: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

Sandvik Materials Technology

Product Area Tube

982 Griffin Pond Rd, Clarks Summit, PA US 18411, Ph: 570-585-7500

www.smt.sandvik.com www.smt.sandvik.com/nafta

Cert#: 201632303 Page 1

Plant Location: 982 Griffin Pond Road, Clarks Summit, PA 18411 Sold To: 362392 Ship To:

HUDSON PRODUCTS CORP. HUDSON PRODUCTS CORP BEASLEY TX BEASLEY TX

Customer Order No: 114772 Certification Date: 20161115 Sandvik Order No: 322872/1

Work Order/Lot: 272421 TAG: PART# 32500 ---------------------------------------------------------/7----------- ­ASTM A789-14, ASME SA-789, ASME Section II, 2015 Edition

Cold Finished BRIGHT ANNEALED Seamless Tube / Type SAF 2205!UNS 831803/S32205/ Size: 1 . 000 II X/ . 109 II MW'/

Heat: 539946 7 ANALYSIS %

C / Si Mn P / S Cr Ni Heat .013 / .48~ .86j/ .023 / . 0005 ~ 22.31~ 5.18 ~ Prod .015 .51 .85 .023 .0010 22.17 5.21

Fe Mo / Al Pb N Heat 3.15/ .013 .174/Prod 3.17 .008 .180 Mechanical Tests:

Yield Strength Tensile Elongation Reduction 0.2% 1.0% Strength in % Of Area

psi MPa psi MPa psi MPa E2 11 E10 11 E4d E5d % 90300 ~22. 8 N/A 120000 :;/827 . 6 36 / N/A N/A N/A N/A 89100 614.5 122000 841.4 38/

Hardness Test Results: 21HRC, 22HRC /

Corrosion test to ASTM A923 Method C mdd: 4'/ Flare Test er ASTM A450 A1016 and ASME SA450 SA1016.: Accept able /Microstructure examined per ASTM A923 Method A: Acceptable Tensile Test sample width (l=Full-Size 2=1/2 11 Strip): 1 Material has less than .5% of sigma and other deleterious minor phases and is free of grain CHECKED AND RE~EASED/; boundary carbides. Examined at 100x minimum magniifcationQate .-to. ... .~ Acceptable / Signed ~ ~ ~ ~ ,Country Of Origin: United States- i/100% Positive Material Identification performed/ All material subjected to a final solution annealing hea~

tr.eatment_owith material at a temperature of 1900 deg. F minimum followed by rapid quenching to below 800 deg. F in less than three (3) minutes. The material has not come in contact with Mercury or Mercury containing compounds. No welding has been performed on this material. Material has been eddy current tested in apcordance with ASTMoA450, ASTM A1016 and is acceptable. 7 Material has been manufactured/supplied in accordance with Sandvik Materials Technology Quality Manual-Standard Products Revision 17 dated Jul. 8, 2016. Quality system

d»~A:s /~/))( ,/o9/t-tt))( 30 1»05j)UPi.E.X ;;I8£:s MATCERT I/r5317(1to

Page 20: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

MATERIAL CERTIFICATE. Ij. f'

/-1"l U' /11 J.­(PACert#: 201632303 l~~lPage 2

has been approved to ISO 9001:2008 (Cert# 10004407, 14SEP18) No unauthorized alterations. The content of this inspection certificate may not be modified or revised in any way without the prior written approval of Sandvik Materials Technology. Unauthorized alterations to the inspection certifiate, including introduction of false, ficticious or fraudulent statements or entries, may be punishable by fines, imprisonment, or both. Contravention of this notice will be prosecuted to the fullest extent of the applicable law~ Melt Source: AB Sandvik MT, Sweden' Melt Method: Electric Furnace >

This is to certify that the contents of this certificate are correct and accurate as contained in Sandvik's records, and that all above test results and operations performed are in compliance with the requirements of the purchase order and the specification(s) listed above.

Electronically Generated Certificate-Valid without signature John Scherer, Quality Mgr-Tube 10 (HUDPOl14772 RO) (15) (BU7303)

MATCERT

Page 21: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

Sandvik Materials Technology MATERIAL CERTIFICATE . ')

Product Area Tube

982 Griffin Pond Rd, Clarks Summit, PA US 18411, Ph: 570-585-7500

Cert#: 201632302 ~~Iwww.smt.sandvik.com www.smt.sandvik.com/nafta Page 1 WI

Plant Location: 982 Griffin Pond Road, Clarks Summit, PA 18411 Sold To: 362392 Ship To:

HUDSON PRODUCTS CORP. HUDSON PRODUCTS CORP BEASLEY TX BEASLEY TX

Customer Order No: 114772 Certification Date: 20161115 Sandvik Order No: 322872/1

Work Order/Lot: 271061 TAG: PART# 32500

is;~-i789=i4~-is~~-si=789~-is~~-s~~~i~~-ii~-2oi5-~di~i~~~-------------

Cold Finished BRIGHT ANNEALED Seamless Tube~

Type SAF 2205/UNS S31803/S32205 7 Size: 1.000" X .109" MW'/ J!eat: 539806 ./

ANALYSIS % C s· S Cr NiMn/ P /

Heat .016/ .~5~ .74 / .023 / .0005 // 22. 31~ 5.22/'Prod .018 .48 .73 .025 .0010 22.27 5.28

Fe Mo Al Pb N Heat 3 .17 ~ .012 .176;> Prod 3.19 .0010 .180 Mechanical Tests:

Yield Strength Tensile Elongation Reduction 0.2% 1.0% Strength in % Of Area

psi .MPa psi MPa psi MPa E2" E10" E4d E5d % 88700~611.7/ N/A 125000 /~862.1 36 '/- N/A N/A N/A N/A 86700 597.9 123000/ 848.3 36

Hardness Test Results: 23HRC, 23HRC /

Corrosion tes~ to ASTM A923 Method C (mdd): 3// Flare Test per ASTM A450/A1016 and ASME SA450/SA1016: Accept ~ able MICrostructure examined per ASTM A923 Method A: AcceptableCHtCKE Tensile Test sample width (l=Full-Size 2=1/2" Strip): 2 Date Material has less than .5% of sigma Sign ......and other deleterious minor phases and is free of grain boundary carbides. Examined at 100x minimum magniifcation. Acceptable Country Of Origin: United States / r

100% Positive Material Identification performed/ All material subjected to a final solution annealing heat treatment with material at a temperature of 1900 deg. F minimum followed by rapid quenching to below 800 deg. F in less than three (3) minutes.;7 The material has not come in contact with Mercury or Mercury containing compounds. No welding has been performed on this material. Material has been eddy current tested in accordance with ASTM A450, ASTM A1016 and is acceptable. 7 Material has been manufactured/supplied in accordance with Sandvik Materials Technology Quality Manual-Standard Products Revision 17 dated Jul. 8, 2016. Quality system

ed---.,;~,....-.~.....;:I,;,,-,jl ....

6Gc; ~S /~/j)( ,/01/!4wx3o/#05 f)C/P/I)( 08C:5 MATCERf Ih5398Dfg

Page 22: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

MATERIAL CERTIFICATE

Cert#: 201632302 1~/~L~1~ Page 2 F\ l'lJ

__________________________________----1-.1' "\

has been approved to ISO 9001:2008 (Cert# 10004407, 14SEP18) No unauthorized alterations. The content of this inspection certificate may not be modified or revised in any way without the prior written approval of Sandvik Materials Technology. Unauthorized alterations to the inspection certifiate, including introduction of false, ficticious or fraudulent statements or entries, may be punishable by fines, imprisonment, or both. Contravention of this notice will be prosecuted to the fullest extent of the applicable lawsi Mel t Source: AB Sandvik MT, Sweden ,7 Melt Method: Electric Furnace This is to certify that the contents of this certificate are correct and accurate as contained in Sandvik's records, and that all above test results and operations performed are in compliance with the requirements of the purchase order and the specification(s) listed above.

Electronically Generated Certificate-Valid without signature John Scherer, Quality Mgr-Tube 10 (HUDPOl14772 RO) (15) (BU7303)

MATCERT

Page 23: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

I TO:

I ?'-:ORTH SHORE STEEL

SPECrFJc.i\T10NS

\VKSTEHN ()FTEX;-\S FOHGE L~ FLANGE CO.'. 1299 Hwy 69 r(o\lTltze, T~XLIS 77625 USA, • R77-2.:(j-2429 t

CERTfFIED Mi\TERJAL TEST REPORT

I ~.O,Ii: _ ! 2.5597JG

lJESCRWTION

~Gti:

~._

L _---.YlC~J .si Tcnsil<:(l~D _._

8.4,897 111,23& /' .--_.... ~-- ---­

/1. I, ')

tl1W.,f 0/1

Ir--1i? I

... ]]_N_[_T_li_:----, [ 2(j03!

-mw

Cr:\10

Ni i'i

I 5.8U 7J~16S0 I I _.~_~I

Sisp:\,~ nci IT COuE TYPF

186276 / P-51­ / -012,/ '" /

,. F 9" 1.66 / .0[9 ;/ .004 ,/ .55 ,/ 3.12 / 22.5V

F·(jD ~[) -f11.!t'\(,"

M/ ItH / , :&'1'OL !<

ASME SA t 82 F-5 I1F·(ilj

I t

,\SYM, SEC. I ; 1.01(, ED. I\STM, SEC. 2; 20 IGED. ASM 13,2015 clJ. /

4- I" 300 LWN R W/4~D OEVEL WI 1116" WULD !.i\r-,

LTH TOL +,'. II?:'

I 4- I" ]00 BliND

IALL 125·250 M PER n16,5 Dli\:IS

o o We cdtify Ihe IWI1.:r i;~llksail).,'d ll..:rcin !I-l':: u:Jn::111\lr,iClIll\:i1, li:scd ''!.I\d <:;':11 11\1 n~L!, nnd 11'.C~I~ t,111c(l'Il:IICC<! sJl~ciri:=.'li'JI; ;md 1~C]lIircm~m::. ~ SN l020,1:20U,t. 11. ()~iL-i1H\1 rcli.::":lIccd dC>Clll' I:II(~, lmd C:(;lil~i[i1Il;~illC IClilU~J ror Ill'lli:Jit1111111 )( lO ~;<:Jr5.

~ c..n !?<1t~.~___ Sj~£~j ,,_ .~ ~ / _'~<H Prill.t.£~Nnl!~ __..

~OLUTION ANNEALED ~:oumry of 1\'[ rg: USA ,/

;:IJ " Waynt; PCnillllCI' (1) [)-2)-~G --~----!-~1~L;;&~/th-~lJ~._...:J ••. ..••••••••

j;. / .J ~

;:IJ (1) < '\"r ill: I of lJlllpl:rill~. mlld Ilil:;.lii~lI, nIt:/:lli(llJ. (Oil :,1 errc it ill:;. I'll Lirr':tlian. fll1::':or auy <.:1(1I,:-r <11;: iCl11 1111 id: 1IiOdili;:,~ lil~ <l.:C1:1:::1'S; or dlistu: ccrti Ik!l!c . .\irJIII:lln~!il.llc

o \'I!d ;11\: CI:r1'i(j;(i\liU::~ 1I1' 11;i~ t::::l:ilit·~lc. [l)

~ \I/I'I·'F·\;';·R. R~·\·. I. L~2.·~"il?

COl;KTRY OF ORIGIN OF BILLET: SP,.\IN .",

LCV;:-.i CI IAItPy wl-,w cF IJEI A923 ~...1l.::TI10D 13 8:.. UH/\-51 (~)(2) /' f~f' LHS 7 '%SUEAR /' J.,.·IILS LAT I~X P 7

271.269,269 NH,Nn,NI1 NI3.NB,~m

PICKLED ./ A923 METHOD A: ACCEPTABLE / CCmROSrON Tf':ST fJE1 A923 METIIOD C: MDD :;,4013 /'

Ou nlil)' f>.1.:mllu....:mcnt S'<;'I~m if, [SO 9[1111 :~.,Il)~, I'I:IJ C~r\Llicd. Ilrcu Cfl:L1\1 !i·~s ;!I:",rdi "l: (l)

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§ ~As / /&:0 .tFl3/.:r~//) :2105f)ilPJ.E.)< ;:JAII/b£' !Ir&-27&

Page 24: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

~~ (J tP AccreditedO~ Labs ~",1t~~~~~~~~~~~~~~~~~~~IS!!O~9~OO~1~/1~7~02~5

L.L.P. po. Box 802404 • Houston, TX 77280-2404 • Telephone (713) 460-3655 • Fax (713) 460-3695

Report Date: 10/25/16 Report No: 760720.00

Rev.: B Cust Acct: WES704 ~O'1

To: Western Of Texas Forge & Flange 1299 Hwy 69 Kountze, TX 77625

Ordered By: Wayne PO#: 9 15 16-1WP Material: A/SA182 F51/60, 2"Sguare X 13"Long Test Piece /' HeaUID: Test Bar#6276/North Shore Steel PO#125597JG: BMT 26031 Job Info: UHA-51 (a)(2) (

I Charpy Test Results I No. Temp Location Foot-Pounds / % Shear / Mils Lat Exp /

1 -40°F LCVN / 271-269-269 NB-NB-NB NB-NB-NB

**105-100-100 Unless otherwise stated, Charpy Impact specimens are V-notch 10 x 10 mm.

Notes: Location: 1/4T (ASTM A923 method B) . ** Lateral expansion measured on unbroken specimen. /

Document ~.v~Reviewed By: Stephanie Valencia

Documentation Specialist

Our reports are for the exclusive use of our customer and our name may be used only with prior written approval. Our reports apply only to the sample tested or inspected and do not necessarily represent the quality of other apparently similar or identical materials. All test specimens and testing conforms to ASTM A-370 requirements unless otherwise stated. This test report shall not be reproduced, except in full, without the written approval of Accu-Test Labs LLP.

Page No: 1 This report contains 3 page(s)

Page 25: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

CI~tI' Accredited

/J~ab~~""~~~~~~~~~~~~~~~~~~!!'S!!O!!9!!OO!!1!!/1!!70!!2~5 L.L.P. P.O. Box 802404 • Houston, TX 77280-2404 • Telephone (713) 460-3655 • Fax (713) 460-3695

Report Date: 10/25/16 ~~o1 Report No: 760720.00

Rev.: B Cust Acct WES704

To: Western Of Texas Forge & Flange 1299 Hwy 69 Kountze, TX 77625

Ordered By: Wayne PO#: 9 15 16-1WP Material: A/SA182 F51/60 2"Sguare X 13"Long Test Piece ./ Heat/ID: Test Bar#6276/North Shore Steel PO#125597JG, BMT 26031 Job Info: UHA-51 (a)(2) / -L

ASTM A923 Method A "

This specimen was polished through alumina and electrolytically etched with a 40% by weight sodium hydroxide solution.

The test specimen was examined at :500X

The specimen was then examined thouroughly by complete traverse of the full sample and across all zones. The etched specimen was determined to have the following structure:

Unaffected Structure: The ferrite has been etched without revelation of intermetallic phase. The interphase boundaries are smooth.

Commentsl Test Notes

Document ~~ Reviewed By: Stephanie Valencia

Documentation Specialist

Our reports are for the exclusive use of our customer and our name may be used only with prior written approval. Our reports apply only to the sample tested or inspected and do not necessarily represent the quality of other apparently similar or identical materials. All test specimens and testing conforms to ASTM A-370 requirements unless otherwise stated. This test report shall not be reproduced. except in full. without the written approval of Accu-Test Labs LLP.

Page No: 2 This report contains 3 page(s)

Page 26: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

O~«I' Accredited

~ab~~""~~~~~~~~~~~~~~~~~~~'S~O~9~OO~1~/1~70~2~5 L.L.P. P.O. Box 802404 • Houston, TX 77280-2404 • Telephone (713) 460-3655 • Fax (713) 460-3695

Report Date: 10/25/16 Report No: 760720.00

Rev.: B

To: Western Of Texas Forge & Flange 1299 Hwy 69

Cust Acct: WES704

Kountze, TX 77625

Ordered By: Wayne PO#: 9 15 16-1WP Material: A1SA182 F51/60( 2"Sguare X 13"Long Test Piece / Heat/ID: Test Bar#6276/North Shore Steel PO#125597JG, BMT 26031 Job Info: UHA-51 (a)(2) ./

Corrosion Test ~er ASTM A923 Method C 7

Ferric Chloride Corrosion Test

Time(hrs.): 24 Temperature: 25°C

Length (in.):2.131

Width(in.): 1.116

Thickness(in.): 0.250

Area(cm A 2): 41.1610

Original weight(gm.): 72.9268

Weight after test(gm.): 72.9254

Weight Loss (gm.): 0.0014

Calculated weight loss in milligrams per square decimeter per day(MDD): 3.4013

Comrnentsl Test Notes

Document ~v~Reviewed By: Stephanie Valencia

Documentation Specialist

Our reports are for the exclusive use of our customer and our name may be used only with prior written approval. Our reports apply only to the sample tested or inspected and do not necessarily represent the quality of other apparently similar or identical materials. All test specimens and testing conforms to ASTM A-370 requirements unless otherwise stated. This test report shall not be reproduced, except in full, without the written approval of Accu-Test Labs LLP.

Page No: 3 This report contains 3 page(s)

Page 27: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

1

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\VESTEH.!\ ()F TEXAS FOHGE 4..~ FLANGE CO.' 1299 Ilwy 69 • K.O\lllt7.e, Texas 77625 USA. • fl77-1..:(j-2429

CERTIFiED MATERrAL TEST REPORT

TO: I1':ORTH 51·IORE STEEL

P.O.fi:I 12559710 -TAGt'.L

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ASME SA (&2 F-5 tlF·(j1) /' 4- I" 300 LWN Rf 9" /

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Page 28: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

/l

O~d' Accredited

~ab~~:;t~~~~~~~~~~~~~~~~~~~IS~O~9~00~1~/1~70~2~5 L.L.P. po. Box 802404 • Houston, TX 77280-2404 • Telephone (713) 460-3655 • Fax (713) 460-3695

Report Date: 10/25/16 Report No: 760720.00 'J

Rev.: B ,!J%01Cust Acct: WES704

II?To: Western Of Texas Forge & Flange 1299 Hwy 69 Kountze, TX 77625

Ordered By: Wayne PO#: 9 15 16-1WP Material: A/SA182 F51/60 2"Square X 13"Long Test Piece ./ Heat/ID: Test Bar#62761Jorth Shore Steel PO#125597JG, BMT 26031 Job Info: UHA-51 (a)(2) /

I Charpy Test Results 7/ I No. Temp Location/ Foot-Pounds % Shear Mils Lat Exp /'

1 -40°F LCVN, 271-269-269 / NB-NB-NB / NB-NB-NB /'

**105-100-100 Unless otherwise stated, Charpy Impact specimens are V-notch 10 x 10 mm.

Notes:

Location: 1/4T (ASTM A923 method B) / ** Lateral expansion measured on unbroken specimen.

Document ~v~Reviewed By: Stephanie Valencia

Documentation Specialist

Our reports are for the exclusive use of our customer and our name may be used only with prior written approval. Our reports apply only to the sample tested or inspected and do not necessarily represent the quality of other apparently similar or identical materials. All test specimens and testing conforms to ASTM A-370 requirements unless otherwise stated. This test report shall not be reproduced, except in full, without the written approval of Accu-Test Labs LLP.

Page No: 1 This report contains 3 page(s)

Page 29: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

(J~d' Accredited

~ab~~',I'~~~~~~~~~~~~~~~~~~~I~SO~90!!!!!!01~/~1~70~25~ L.L.P. P.O. Box 802404 • Houston, TX 77280-2404 • Telephone (713) 460-3655 • Fax (713) 460-3695

/)

Report Date: 10/25/16

Report No: 760720.00 1'~D1Rev.: B 11,1

Cust Acct: WES704 To: Western Of Texas Forge & Flange

1299 Hwy 69

Kountze, TX 77625

Ordered By: Wayne PO#: 9 15 16-1WP

Material: A/SA182 F51/60 2"Square X 13"Long Test Piece / Heat/ID: Test Bar#6276 fJorth Shore Steel PO#125597JG, BMT 26031

Job Info: UHA-51 (a)(2) /

ASTM A923 Method A -;7"

This specimen was polished through alumina and electrolytically etched with a 40% by weight sodium hydroxide solution.

The test specimen was examined at :500X

The specimen was then examined thouroughly by complete traverse of the full sample and across all zones. The etched specimen was determined to have the following structure:

Unaffected Structure: The ferrite has been etched without revelation of intermetallic phase. The interphase boundaries are smooth.

Commentsl Test Notes

Document ~v~ Reviewed By: Stephanie Valencia

Documentation Specialist

Our reports are for the exclusive use of our customer and our name may be used only with prior written approval. Our reports apply only to the sample tested or inspected and do not necessarily represent the quality of other apparently similar or identical materials. All test specimens and testing conforms to ASTM A-370 requirements unless otherwise stated. This test report shall not be reproduced, except in full, without the written approval of Accu-Test Labs LLP.

Page No: 2 This report contains 3 page(s)

Page 30: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

cf'~", Accredited

~ab~~";'~~~~~~~~~~~~~~~~~~~IS~O~9~00~1~/1~70~2~5 L.L.P. P.O. Box 802404 • Houston, TX 77280-2404 • Telephone (713) 460-3655 • Fax (713) 460-3695

r)Report Date: 10/25/16

Report No: 760720.00 Rev.: B Ktlo1

Cust Acct: WES704 II~To: Western Of Texas Forge & Flange

1299 Hwy 69 Kountze, TX 77625

Ordered By: Wayne PO#: 9 15 16-1WP

Material: NSA182 F51/60 2"Sguare X 13"Long Test Piece / i.

HeaUID: Test Bar#6276 North Shore Steel PO#125597JG, BMT 26031

Job Info: UHA-51 (a)(2) /

Corrosion Test ~er ASTM A923 Method C

Ferric Chloride Corrosion Test

Time(hrs.): 24 Temperature: 25°C

Length (in.):2.131

Width(in.): 1.116

Thickness(in.): 0.250

Area(cm"2): 41.1610

Original weight(gm.): 72.9268

Weight after test(gm.): 72.9254

Weight Loss (gm.): 0.0014

Calculated weight loss in milligrams per square decimeter per day(MDD): 3.4013 ,/

Commentsl Test Notes

Document ~v~Reviewed By: Stephanie Valencia

Documentation Specialist

Our reports are for the exclusive use of our customer and our name may be used only with prior written approval. Our reports apply only to the sample tested or inspected and do not necessarily represent the quality of other apparently similar or identical materials. All test specimens and testing conforms to ASTM A-370 requirements unless otherwise stated. This test report shall not be reproduced, except in full, without the written approval of Accu-Test Labs LLP.

Page No: 3 This report contains 3 page(s)

Page 31: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

/J

\\'ESTERN OF TE)U\.S FORGE & FLANGE CO, 1299 rrwy 69 ~ Kountze, Tcxrls 77625 USA, '" 877-21~6-21129 /1t0D1

CERTIFTED I'vfATERfAL TEST REPORT ~Sll TO: P.O.i'1: TAGH: f1i"IT~:

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Page 32: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

~~ CJ tP Accredited~~ Labs ~"~~~~~~~~~~~~~~~~~~~15~O~90~01~/~17~0~25~

L.L.p. p.o. Box 802404 • Houston, TX 77280-2404 • Telephone (713) 460-3655 • Fax (713) 460-3695

Report Date: 10/25/16 Report No: 760721.00

Rev.: B YJ1/6,0h1 /1

1 Cust Acct: WES704

To: Western Of Texas Forge & Flange 1299 Hwy 69 Kountze, TX 77625

Ordered By: Wayne PO#: 9 15 16-1WP Material: AlSA182 F51/60 2"Sguare X 13"Long Test Piece ./ Heat/ID: Test Bar#6353JNorth Shore Steel PO#125597JG, BMT 26031 Job Info: UHA-51 (a)(2) ,/

I Charpy Test Results I No. Temp Location Foot-Pounds / % Shear /' Mils Lat Exp 7

1 -40°F LCVN / 251-251-214 NB-NB-NB NB-NB-NB

**97-97-94 Unless otherwise stated, Charpy Impact specimens are V-notch 10 x 10 mm.

Notes: Location: 1/4T (ASTM A923 method B) ** Lateral expansion measured on unbroken specimen: /'

Mechanical testing performed at 1/41.

Document ~v~Reviewed By: Stephanie Valencia

Documentation Specialist

Our reports are for the exclusive use of our customer and our name may be used only with prior written approval. Our reports apply only to the sample tested or inspected and do not necessarily represent the quality of other apparently similar or identical materials. All test specimens and testing conforms to ASTM A-370 requirements unless otherwise stated. This test report shall not be reproduced, except in full, without the written approval of Accu-Test Labs LLP.

Page No: 1 This report contains 3 page(s)

Page 33: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

O~d' Accredited

~ab~~"~~~~~~~~~~~~~~~~~~~'S!!O!!9!!OO!!1!!/1~70~2~5 L.L.P. P.O. Box 802404 • Houston, TX 77280-2404 • Telephone (713) 460-3655 • Fax (713) 460-3695

~ Report Date: 10/25/16

Report No: 760721.00 IJ1~'01 Rev.: B f'1J5 1

Cust Accl: WES704 To: Western Of Texas Forge & Flange

1299 Hwy 69 Kountze, TX 77625

Ordered By: Wayne PO#: 9 15 16-1WP Material: A/SA182 F51/60 2"Sguare X 13"Long Test Piecr::: / Heat/ID: Test Bar#6353 ·1-.Jorth Shore Steel PO#125597JG, BMT 26031 Job Info: UHA-51.@20 ./

L.

This specimen was polished through alumina and electrolytically etched with a 40% by weight sodium hydroxide solution.

The test specimen was examined at :500X

The specimen was then examined thouroughly by complete traverse of the full sample and across all zones. The etched specimen was determined to have the following structure:

Unaffected Structure: The ferrite has been etched without revelation of intermetallic phase. The interphase boundaries are smooth.

Commentsl Test Notes

Document ~v~ Reviewed By: Stephanie Valencia

Documentation Specialist

Our reports are for the exclusive use of our customer and our name may be used only with prior written approval. Our reports apply only to the sample tested or inspected and do not necessarily represent the quality of other apparently similar or identical materials. All test specimens and testing conforms to ASTM A-370 requirements unless otherwise stated. This test report shall not be reproduced, except in full, without the written approval of Accu-Test Labs LLP.

Page No: 2 This report contains 3 page(s)

Page 34: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

-3 O~dt Accredited

~ab~~',I'~~~~~~~~~~~~~~~~~~~'S~O~9~OO~1~/1~70~2~5 L.L.P. P.O. Box 802404 • Houston, TX 77280-2404 • Telephone (713) 460-3655 • Fax (713) 460-3695

Report Date: 10/25/16/J/0(/(t.~ 1 Report No: 760721.00 I'" ~/' 0

Rev.: B I' Cust Acct: WES704 I

To: Western Of Texas Forge & Flange 1299 Hwy 69 Kountze, TX 77625

Ordered By: Wayne PO#: 9 15 16-1WP Material: AlSA182 F51/60 2"Sguare X 13"Long Test Piecec/ Heat/ID: Test Bar#6353/North Shore Steel PO#125597JG, BMT 26031 Job Info: UHA-51~ ./

Corrosion Test ~er ASTM A923 Method C

Ferric Chloride Corrosion Test

Time(hrs.): 24 Temperature: 25°C

Length (in.): 2.050

Width(in.): 0.842

Thickness(in.): 0.247

Area(cm"2): 31.4890

Original weight(gm.): 52.0176

Weight after test(gm.): 52.0172

Weight Loss (gm.): 0.0004

Calculated weight loss in milligrams per square decimeter per day(MDD): 1.2703 /

Commentsl Test Notes

Document ~v~Reviewed By: Stephanie Valencia

Documentation Specialist

Our reports are for the exclusive use of our customer and our name may be used only with prior written approval. Our reports apply only to the sample tested or inspected and do not necessarily represent the quality of other apparently similar or identical materials. All test specimens and testing conforms to ASTM A-370 requirements unless otherwise stated. This test report shall not be reproduced, except in full, without the written approval of Accu-Test Labs LLP.

Page No: 3 This report contains 3 page(s)

Page 35: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

TO:

I NORTH SHORE STE~L

SPECIFICATIONS

'VESTER!\" OFTEX;\S FORGE & FLA:"GE CO, '1(P~12 1)9 lh"y 69 f Kountze, TeX£1s 77625 US/\, ' R77-2'~6-?U9 tmD1

CERTIFIED MATERlf\L TEST REPORT ItJ;)

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< /"'y 1,":1 ,)r 1;::l1:v.::r IU~. 1I\/1(llli~ i1:Jl1IL, :111<:1 ~Ij~, (,"':11 III :;rl'~,t:n~. f.:I,;.rI~~llml, 111,lln, ,'II)' o£lid ;'1;1;111; "\ illch lllf>e:fICS Ille ,'.)t1\~'Il:~ ulltll' !ql o.:<:rl.ln::r<:. ,;l1JII CDIISLlhlh,: ~CD

vail! 'il": cenifiL":nilll1:; L1llhr~ .,;crldi'l~h:.o tll ro WTFi·,;~:·!·H. K.:" l. 7,~ .1·,'111:.'

SOLUTION ANNE,t\U;1) ,/ Coulltry or ~,Mg: USA 7' COUNTRY OF ORO IN or BI '-LET: rr,..\LY /'

LCVN CIIARPY (a1··lOc F PER A92.3 METHOD n & UHA·5 [ 1<1)(2)"' ­

FT 1.1>5./ ~/oSHEAR /' MIl.S Ll\T EXP 7 251,251,214 >lB,Nfl.:..;n Nn,l\8,?':J3

PICKL~D / .'\923 METIIOD 1\: .'\CCEPTAL~Lr. / COH.ROS10/,\ TEST PER ,vJ23 ~'lETHOD c: :vtDD 1.2703/

Q~i!llily Ml.lu:'l~c:m:I1' sY";(l! .l: l~ ISO IJ'~t I .~C~)S. PED ('c-rti fi'L'd, .1 ':1: ~:'IL' r.he:. Ht:o:::"n!·:Ic. U

'" l"itle:'-l Q/A Document t:~~l;dinal:~--.' -' "J

~ .--_.- . -,-_._--.-- ...._.~_.J \ l'll.tlm:~ :,r' ;1f1'~11r: h!: ..:iq; 1!1'.d!0f c: ;ml:~r;; 1,,\\ '. 1..... '. ::::0 X~ II [il

~ G~.:s Ii "/50 5(80 f,c/WN~05 f)uP/E< /lANGE J!rM353

Page 36: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

11

O~«I' Accredited

~ab~~~~~~~~~~~~~~~~~~~~~~IS~O~9~OO~1~/~17~02~5 L.L.P. P.O. Box 802404 • Houston, TX 77280-2404 • Telephone (713) 460-3655 • Fax (713) 460-3695

Report Date: 10/25/16 Report No: 760721.00

Rev.: B Cust Acct: WES704

To: Western Of Texas Forge & Flange

1299 Hwy 69 Kountze, TX 77625

Ordered By: Wayne PO#: 9 15 16-1WP

Material: A/SA182 F51/60 2"Sguare X 13"Long Test Piece /' Heat/II): Test Bar#63531N0rth Shore Steel PO#125597JG, BMT 26031

Job Info: UHA-51(a)(2) /

I Charpy Test Results No. Temp Location Foot-Pounds 7 % Shear 7 Mils Lat Exp 7

1 -40°F LCVN / 251-251-214 NB-NB-NB NB-NB-NB

**97-97-94 Unless otherwise stated, Charpy Impact specimens are V-notch 10 x 10 mm.

Notes:

Location: 1/4T (ASTM A923 method B) /

** Lateral expansion measured on unbroken specimen. /

Mechanical testing performed at 1/4T.

Document ~v~Reviewed By: Stephanie Valencia

Documentation Specialist

Our reports are for the exclusive use of our customer and our name may be used only with prior written approval. Our reports apply only to the sample tested or inspected and do not necessarily represent the quality of other apparently similar or identical materials. All test specimens and testing conforms to ASTM A-370 requirements unless otherwise stated. This test report shall not be reproduced, except in full, without the written approval of Accu-Test Labs LLP.

Page No: 1 This report contains 3 page(s)

J1IP);1 ~~.<ID Il~

J

Page 37: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

O~d' Accredited

~ab~~"~~~~~~~~~~~~~~~~~~~I~SO~90~O~1/~1~70~25~ L.L.P. P.O. Box 802404 • Houston, TX 77280-2404 • Telephone (713) 460-3655 • Fax (713) 460-3695 VJ~D1

Report Date: 10/25/16 ~611 Report No: 760721.00

Rev.: B Cust Acct: W ES704

To: Western Of Texas Forge & Flange

1299 Hwy 69 Kountze, TX 77625

Ordered By: Wayne PO#: 9 15 16-1WP

Material: AlSA182 F51/60 2"Square X 13"Long Test Piece/ Heat/ID: Test Bar#6353 /North Shore Steel PO#125597JG, BMT 26031

Job Info: UHA-51(a)(2) / £..

This specimen was polished through alumina and electrolytically etched with a 40% by weight sodium hydroxide solution.

The test specimen was examined at :500X

The specimen was then examined thouroughly by complete traverse of the full sample and across all zones. The etched specimen was determined to have the following structure:

Unaffected Structure: The ferrite has been etched without revelation of intermetallic phase. The interphase boundaries are smooth.

Comrnentsl Test Notes

Document ~v~ Reviewed By: Stephanie Valencia

Documentation Specialist

Our reports are for the exclusive use of our customer and our name may be used only with prior written approval. Our reports apply only to the sample tested or inspected and do not necessarily represent the quality of other apparently similar or identical materials. All test specimens and testing conforms to ASTM A-370 requirements unless otherwise stated. This test report shall not be reproduced, except in full, without the written approval of Accu-Test Labs LLP.

Page No: 2 This report contains 3 page(s)

Page 38: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

CJ &d' ~ " Accredited 1/1)Labs ISO 9001/17025 ~ 1J1fv701

L.L.P. P.O. Box 802404 • Houston, TX 77280-2404 • Telephone (713) 460-3655 • Fax (713) 460-3695 "15(1Report Date: 10/25/16

Report No: 760721.00 Rev.: B

Cust Acct: WES704 To: Western Of Texas Forge & Flange

1299 Hwy 69 Kountze, TX 77625

Ordered By: Wayne PO#: 9 15 16-1WP Material: A1SA182 F51/60 2"Square X 13"Long Test Piece HeaUID: Test Bar#6353iJorth Shore Steel PO#125597JG, BMT 26031 Job Info: UHA-51 (a)(2) ,/

Corrosion Test ~er ASTM A923 Method C 7

Ferric Chloride Corrosion Test

Time(hrs.): 24 Temperature: 25°C

Length (in.): 2.050

Width(in.): 0.842

Thickness(in.): 0.247

Area(cm"2): 31.4890

Original weight(gm.): 52.0176

Weight after test(gm.): 52.0172

Weight Loss (grn.): 0.0004

Calculated weight loss in milligrams per square decimeter per day(MDD): 1.270~

Commentsl Test Notes

Document ~v~Reviewed By: Stephanie Valencia

Documentation Specialist

Our reports are for the exclusive use of our customer and our name may be used only with prior written approval. Our reports apply only to the sample tested or inspected and do not necessarily represent the quality of other apparently similar or identical materials. All test specimens and testing conforms to ASTM A-370 requirements unless otherwise stated. This test report shall not be reproduced, except in full, without the written approval of Accu-Test Labs LLP.

Page No: 3 This report contains 3 page(s)

Page 39: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

/l

Page I of 1~""~'~",""'~

Sold To: NORTH SHORE SUPPLY CO. 129~.5 \-lARKET STREET tJ~/· HOUSTON TX 77015

NUCUAR PRODUCTS UllitL"u StJt~s K~'1~)D1~.l:tnuf~cl\l!ct <If l'll,in ~ J:'ld 'rl.:,~utc \' .hel l"clll'rl..'r.·:nl>

~4U-l H;]~g()lltl St· H"WilOfl. TX 77011 MlR i!: 318.811 pJ,h ,

Phonl:: 7lJ·615-3fl3J Fa.x" 713-ti95-351S PO ,~!: 1~55977-JG I

A Bonne)" FLlrgc C0l111laJ1Y

Saks Orda ;:: COO 1(j089-H'j Date: 10.'06,'201 (ifhi":' product has rwl COITI"I: in din.:d conl,lel wilh mercury or ~ny of 115 COlllp<Junus. nor with any mCH:ury-conlllining dc~'il"t.; <:rnpl(lyin~

a s.ingk boundary ofcOrll~lirHncnt. No wdJing pcrt<.lrJllcL!.

CCrliIicd IvIulcrial T~Sl R~pOrl

Wt.: l:l:rtil' th~l[ tile contents of this r~purt arL" COITl'C;[ and Heal Code: 7656,.\A./ accurate, and that illl test results ilnd operations pl:rfolim:d by \~IFI or its subcontractors are in compliance with the m<ltl.:'rial specification and n:lJuircmcnts of the rererenccd code or standard. :md that the malerial confurms to lhe dimensional n:qllircm~nts of the order. This ducllm~nt is in accordance.­witb ENI0204 3.1.

CHECKED A,N~ RE:VMmerial: A/SA 182 14a F51 Date /Io;/~ ~/~ i/

Signed ~:;;:tC (l~m Qllantiry Description >

[ 10 FLl X 3i~ 6M S\VP / SA 181F51/F60-09.t ,/ PICKLED .~ND PASSIVATION'/

Ch~rnka( Composition

LJdle C CR / MN / MO / N / N! / P / s 0.0180/ 22.45 1.290 3.160 0.1600 5.5lJO 0.019 0.001/

51 0.470 /

Product C CR /.MN / MO / N / NI P / s 0.0190/ 22,99 1.230 3.210 0.1750 5.760'/ 0.012 0.003/ S1 0.459/

Tensile PSl Yield PSI [lung ~~o / RA \u / Hardness Mill 105,000 / 72,000 / ~OAO 79.90 21 Rc

Charp\' V-Notch Properties: T~st Terno(!nuurc: -50 f ./

FT LBS: 219/219/219 / ~o Shear: 100/100/100 /' ~·tl.E: 106/110/106 / \!IlLLiCOUNTRY OF ORIGIN: COGNE (ITALY) - HEAT tr,27868 ./

ASTM E562 FERRITE: 41.8~/n 142.5% / PRE: LADLE: 35.4:2R.: PRODUCT: 36.383

j\.,lETALLOGRAPHlC EXAMINATION ACCEPTABLE: @ 500X

ASTM G48 A/AST~I A913 C: NO PITnNG AT"O X, CORROSION RATE 0.03 MOD ,/

;"'lETALLOGRAPHIC INSPECnON ACCORDING TO AST~'I A9 1 3 METHOD A: SAnSFACTOR)' /

CHARPY V-NOTCH ORIENT;\TJON: LONOlTUDI>JAL

SOLUTION ANNEALED (V 1900 DEG F MINn....1Uivl & WATER QUF.NCHED TO BELOW 500 DEG F -:: J MINUTES /'

/Ol2s J1AI.x.. -ti'GlV/ /WJs£Jt!,t)j£)( 5ae..~UT M-7t;5(;AAMarie Dehmer .

Qualily Assurance Rcpn:scnlalJ ....c

Doc#: W511 Rev#:A Rev Date:11/3/11

Page 40: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

-------

"~lo 1G? ./)

~·1;.. Bnrr~i' FO!Jc Cor;1;);':I':'

"HO~ Haygood i P.O. Box 7303 1fiIoHouston/ Texas 77248- 7303 (7l3) 695-3633 • (800) 231-0430 Fax; (713) 695-3528 y:...../v.,r ..~\rfHntl. com

Certificate of Conformance

'v'VFI Internatjonal certifies the fisted equipment to be manufactured and inspected in accordance with all applicable standards and customer purchase order requirements. Any deviations from customer purchase order have been documented, reviewed, and accepied, All equipment lfsted is deemed acceptable for its intended lise.

NORTH SHORE SUPPLY C1608946----- .- ...-_.---_._------­Customer ~AjFI Sales Order Number

1255977-JG1 _~_ ....._§epten1ber 29, 2016 ----_._~------_.

Purchase Order Number Date of Issue

Item Qty Description Materiaf Soec Heat No.

1 10 FLT X :!~ 61vl SWP / SA182F51/F60 / 7656AA /

----------------_._----_.__.-

Nqtes:

_ ...._.__._1!1/!:1!::::£~ .__ ....._..__..._~_.~ __~_". Quality Assurance RepreserJtative

Doc#: W511 Rev#:A Rev Date: 11 /3/11

Page 41: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

~ CERTIFICATE OF TEST AND INSPECTION FLOWSERVE Vagt Valve WITH MATERIAL TRACEABILITY TO

DIN-50049.3.1 B ~ Phone: (903)885-4691 AND BS EN 102043.1Sulphur Springs, Texas 75482 USA / Fax: (903)439-3386

Customer: HUDSON P"RODUCTS CORP. Qty: 10 of ST2831 ..-1/4 NPS ST2831 ·3/4 NPS A182·F316 CL 800 WB FEM THD X MALE SW GATE VALVE ,/ (316 TRIM· HFS) DWG: 46848A1 R19 • P.O. #626367 ORDER No: 1087437 Line Item: 1

. I~~ATCODE < i-----sPECiFiCATiON7 MATERIAL PRODUCECCMILL HEAT NUMBER

!01t.6 ~ BODY: PC7Z 7~182 F316/316L - 2014 T I PRADEEP ~ . FF26 _

CHEMISTRY

[- C:I' 0022 /' HEAT TREATMENT AND MN: 2.00.Y MECHANICAL PROPERTIES CHARPY VEE NOTCH

P: 0.040)/ HEAT TREATMENT: SOlution. Anneal J ITEST TEMP F (C): I1-= ~. 0.022 Y 1st CYCLE TEMP F (C): ~_ I

-- 51: 0.31 y 2nd CYCLE TEMP F.: ("C)::i-- ~===

I !

1~ CU; I ~/ YIELD KSI (MPa): 34.0 ~~ NI: ~O.OO , TENSILE KSI (MPa): 82 ~ 5~~

f-- C_R---1: ~7.00 fENLONG. GAGE In. (mm): 2.0 , 7 ~

~ FT-LBS (J): _ TEST 2 FT-LBS (J):

1----­-~

[TEST 3 FT-LBS (J):

AVERAGE FT-LBS (J):

~~ 2.00 ELONG. %: 60 i

------~-. 0.000 IRA %: 77 / i

l__ ~ 0~q HARDNESS: 156 BHN i

HEAT CODE C SPECIFICATI~~ATERIAL PRODUCER I MILL HEAT NUMBER I BONNET: WHM 7~ A182 F316 -~~~__SLATER__ 96423.~__----=J CHEMISTRY

-------cJ i 0.024 HEAT TREATMENT AND -------1 I-=- MECHANICAL PROPERTIES CHARPY VEE NOTCH

MN: 1.61I

...---- P: r 0.040 IHEAT TREATMENT: Solution Anneal ! ~MPF(C~-~~~-------1

~ ----~: 0020151 CYCLE TEMP F (e): ~=--I TEST 1 FT-LBS (J): i I

51: OAO 2nd CYCLE TEMP F (C): TEST 2 FT-LBS (J): I I ----~U: OAO YIELD KSI (MPa): . 47.8 _--329.6 TEST 3 FT-LBS (J): --I _J ~- NI: 10.00 ITENSILE KSI (MPa):-----t-------s5.6 590.2 ~VERAGE FT-LBS (J)~--==----.-J ~-- CR: 17.00YENLONG~E~m): ~I-------so.l)

E1

----MOl ~~.r.. ELONG. %: 55

v:l! 0000 ! ~% _77 ----j

~CBl: 0.000 I HARDNESS._·__ 186 _BH_N__---'

I CO::! ~.J

CHECKED AND RELEASEU. Date/~ • SignedJAr . LA

Page 1 of 2

Page 42: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

~

FLOWSERVE Vagt Valve CERTIFICATE OF TEST AND INSPECTION

WITH MATERIAL TRACEABILITY TO

~ DIN-S0049.3.1 B

Sulphur Springs, Texas 75482 USA Phone: (903)885-4691

Fax: (903)439-3386 AND as EN 102043.1

I-~AT CODE +I_- S_PE_C_I_F_IC_A_T_IO_N HEAT NUMBER__ __----F-_-_M_A_T_E_R_IA_L_P_R_O_D_U_C_E~MILL -J c,fAs~BONNE~A 7 ~PE316/316L.2014 TWMETALS --=-~ VX1805i

CHEMISTRY ,---------ClI-0~020 HEAT TREATMENT AND

1 CHARPY VEE NOTCH ----~---1. ~I MECHANICAL PROPERTIES~'

-

1.80 ~ - P~' 0.040 HEAT TR.EATMENT: I Solution Annea-,-~ TEST TEMP F (C): I __5: 0.020 1st CYCLE TEMP F (C): __----.J~ TEST 1 FT-LBS (J):

51: 0.30 2nd CYCLE TEMP F (C): ~I~~ TEST 2 FT·LBS (J): ~

CU: L..c>.41 YIELD KSI (MPa): 44.0 _ 303.4--= TEST 3 FT-LBS (J):

----N----1I: ! 10.00 ~ENSILE KSI IMPa): 88 / 606.7 - .AVERAGE FT-LBS (J): I

- __ . CR:I Pi·o~r ENLONG. GAGE In. (mm): 2cO _1 50_.0_.;

____M_~~ 2·~IELONG.%: I 55--r-- i

~~ RA %: 73 7 ~It=-__~ L~ §DNESS: _~ 166 BHN ~ i----iJ i(i1l

L CO: II QJ: I

The items listed herein were hydrostatically tested in compliance with API-598, and found to be satisfactory at the time of test.

We certify that the listed material codes are in full compliance with the listed specification and are traceable to the original mill heat

SIGNATURE: Date: Monday, November 28,2016

Quality Manaqer

Page 2 of 2

Page 43: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

Sandvik Materials Technology MATERIAL CERTIFICATE Product Area Tube .')982 Griffin Pond Rd, Clarks Summit, PA US 18411, Ph: 570-585-7500

Cert#: 201632303 '1W.,~11

'1~ www.smt.sandvik.com www.smt.sandvik.com/nafta pi' Page 1 ~

'II 1

Plant Location: 982 Griffin Pond Road, Clarks Summit, PA 18411 Sold To: 362392 Ship To:

HUDSON PRODUCTS CORP. HUDSON PRODUCTS CORP BEASLEY TX BEASLEY TX

Customer Order No: 114772 Certification Date: 20161115 Sandvik Order No: 322872/1

Work Order/Lot: 272421 TAG: PART# 32500 --------------------------------------------------------~-------------

ASTM A789-14, ASME SA-789, ASME Section II, 2015 Edition

Cold Finished BRIGHT ANNEALED Seamless Tube~

Type SAF 2205/UNS S31803/S3220~ ~ Size: 1.000 11 X .109 11 MW/ Heat: 539946 7

ANALYSIS % C Si Mn P / S / Cr / Ni /

Heat .013 / . 48 ~ .861 .023/ .0005 / 22.31 / 5.18/,Prod .015/ .51 .85/ .023 .0010 22.17 5.21

Fe Mo Al Pb N Heat 3 .15~ .013 .174:/Prod 3.17 .008 .180 Mechanical Tests:

Yield Strength Tensile Elongation Reduction 0.2% 1.0% Strength in % Of Area

psi MPa psi MPa psi MPa E2 11 E10 11 E4d E5d % 90300// 622.8 N/A 120000-j- 827.6 36/ N/A N/A N/A N/A 89100 614.5 122000 841.4 38/

Hardness Test Results: 21HRC, 22HRC /

Corrosion test to ASTM A923 Method C (mdd): 4~ Flare Test per ASTM A450!A1016 and ASME SA450/SA1016: Accept able r ;MICrostructure examined per ASTM A923 Method A: Acceptable' Tensile Test sample width (l=Full-Size 2=1/2 11 Strip): 1 Material has less than .5% of sigma and other deleterious minor phases and is free of grain boundary carbides. Examined at 100x minimum magniifcation. Acceptable Country Of Origin: United States / 100% Positive Material Identification performed~ All material subjected to a final solution annealing heat treatment with material at a temperature of 1900 deg. F minimum followed by rapid quenching to below 800 deg. F i~ less than three (3) minutes.? The material has not come in contact with Mercury or Mercury containing compounds. No welding has been performed on this material. Material has been eddy current tested in accordance with ASTM A450 ASTM A1016 and is acce table. 7 Material has been manufactured supplied' in accordance with Sandvik Materials Technology Quality Manual-Standard Products Revision 17 dated Jul. 8, 2016. Quality system

,,:?~~ ('6D X , i091lt1u.) >< Lf :v.05[)(JPI..£)( 5MbT;6r..$

1-1,..5391'I~

Page 44: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

MATERIAL CERTIFICATE

Cert#: 201632303 Page 2

has been approved to ISO 9001:2008 (Cert# 10004407, 14SEP18) No unauthorized alterations. The content of this inspection certificate may not be modified or revised in any way without the prior written approval of Sandvik Materials Technology. Unauthorized alterations to the inspection certifiate, including introduction of false, ficticious or fraudulent statements or entries, may be punishable by fines, imprisonment, or both. Contravention of this notice will be prosecuted to the fullest extent of the applicable lawyJ Melt Source: AB Sandvik MT, Swede~·

Melt Method: Electric Furnace This is to certify that the contents of this certificate are correct and accurate as contained in Sandvik's records, and that all above test results and operations performed are in compliance with the requirements of the purchase order and the specification(s) listed above.

Electronically Generated Certificate-Valid without signature John Scherer, Quality Mgr-Tube 10 (HUDP0114772 RO) (15) (BU7303)

\L\TCERT

Page 45: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

12

Sandvik Materials Technology MATERIAL CERTIFICATE

Product Area Tube

982 Griffin Pond Rd, Clarks Summit, PA US 18411, Ph: 570-585-7500 '1i;J1~ Cert#: 201632302 ~ p,iJwww.smt.sandvik.com

www.smt.sandvik.com/nafta Page 1 ~ Plant Location: 982 Griffin Pond Road, Clarks Summit, PA 18411

Sold To: 362392 Ship To: HUDSON PRODUCTS CORP. HUDSON PRODUCTS CORP BEASLEY TX BEASLEY TX

Customer Order No: 114772 Certification Date: 20161115 Sandvik Order No: 322872/1

Work Order/Lot: 271061 TAG: PART# 32500

ASTM A789-14,ASME SA-789,ASME Section II, 2015 Edition/

Cold Finished BRIGHT ANNEALED Seamless TUbe./ Type SAF 2205/UNS S31803/S32205 ~ Size: 1.000" X .109" MW/

Heat: 539806 ~ ANALYSIS %

C Si Mn P S Cr / N' Heat .016./ .45/ .74/ .023 I- .0005/ 22.31/ 5~22~ Prod .018/ .48/ .73/ .025 .0010/ 22.27 5.28

Fe Mo Al Pb N Heat 3.17~ .012 .176~ Prod 3.19 .0010 .180 Mechanical Tests:

Yield Strength Tensile Elongation Reduction 0.2% 1.0% Strength in % Of Area

psi MPa psi MPa psi MPa E2" E10" E4d E5d % 88700/ 611.7 N/A 125000 ~ 862.1 36/ N/A N/A N/A N/A86700/ 597.9 123000 848.3 36/

Hardness Test Results: 23HRC, 23HRC /

Corrosion test to ASTM A923 Method C (mdd): 3~ ~ Flare Test per ASTM A450/A1016 and ASME SA450/SA1016: Accept able MICrostructure examined per ASTM A923 Method A: Acceptable / Tensile Test sample width (I=Full-Size 2=1/2" Strip): 2 Material has less than .5% of sigma and other deleterious minor phases and is free of grain boundary carbides. Examined at 100x minimum magniifcation. Acceptable Country Of Origin: United States~ 100% Positive Material Identification performed ~ All material subjected to a final solution annealing heat treatment with material at a temperature of 1900 deg. F minimum followed b ra id uenchin to below 800 de . F in

ess than three 3 minutes .. The material has not come 1n contact with Mercury or Mercury containing compounds. No welding has been performed on this material. Material has been eddy current tested in accordance wit.h ASTM A450, ASTM A1016 and is acceptable. 7 Material has been manufactured/supplied in accordance with Sandvik Materials Technology Quality Manual-Standard Products Revision 17 dated Jul. 8, 2016. Quality system

Page 46: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

MATERIAL CERTIFICATE I?

Cert#:' 201632302 ~~1~ Page 2

I r----------------------"""----------------------- ­

has been approved to ISO 9001:2008 (Cert# 10004407, 14SEP18) No unauthorized alterations. The content of this inspection certificate may not be modified or revised in any way without the prior written approval of Sandvik Materials Technology. Unauthorized alterations to the inspection certifiate, including introduction of false, ficticious or fraudulent statements or entries, may be punishable by fines, imprisonment, or both. Contravention of this notice will be prosecuted to the fullest extent of the applicable lawsl Melt Source: AB Sandvik MT, Sweden ~ Melt Method: Electric Furnace This is to certify that the contents of this certificate are correct and accurate as contained in Sandvik's records, and that all above test results and operations performed are in compliance with the requirements of the purchase order and the specification(s) listed above.

Electronically Generated Certificate-Valid without signature John Scherer, Quality Mgr-Tube 10 (HUDPOl14772 RO) (15) (BU7303)

i\IATCERT

Page 47: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

Hudson Products 9660 Grunwald Rd.

Beasley, Tx 77417 H,UDSON Proid:ucts C,orporation

Name K763 CALIBRATION

Class Stainless

Date 09/01/2017

Time 13:34:23

Duration 8.5 s

Element TI % V% Cr % 0.00 0.09 22.97

Grades: Duplex 2205 (0.00), 552304 (0.98) Reference: Duplex 2205

Mn% 1.28

Fe % 66.81

Co % 0.00

NI % 5.79

Cu % 0.21

Nb % 0.00

Mo% 3.22

W% 0.00

Sn % 0.00

Pb % 0.00

Name K7631 ' MOCKUP TUBE HT 539946

Class Stainless

Date 09/01/2017

Time 13:49:20

Duration 8.5 s

Element TI % V% Cr % 0.00 0.07 22.37

Grades: Duplex 2205 (0.00), 552304 (0.00) Reference: Duplex 2205

Mn% 0.80

Fe % 67.58

Co % 0.00

N,% 528

Cu % 0.10

Nb % 0.00

Mo% 3.33

W% 0.07

Sn % 0.00

Pb % 0.00

Name K763 1" MOCKUP TUBE HT 539946

Class Stainless

Date 09/01/2017

Time 13:49:35

Duration 8.5 s

Element TI % V% Cr% 0.00 0.06 21.98

Grades: Duplex 2205 (0.00),552304 (0.57) Reference: Duplex 2205

Mn% 0.84

Fe % 68.18

Co % 0.00

NI % 5.68

Cu % 0.17

Nb % 0.00

Mo% 3.12

W% 0.09

Sn % 0.00

Pb % 0.00

Name K7631 ' MOCKUP TUBE HT 539946

Class Stainless

Date 09/01/2017

Time 13:49:52

Duration 8.5 s

Element TI % VOAl Cr% 0.00 0.05 22.37

Grades: Duplex 2205 (0.00), 552304 (0.06) Reference: Duplex 2205

Mn% 0.77

Fe % 67.85

Co % 0.00

N,% 5.52

Cu % 0.16

Nb % 0.00

Mo% 3.24

W% 015

Sn % 0.00

Pb % 0.00

Name K763 1" MOCKU P TU BE HT 539806

Class Stainless

Date 09/01/2017

Time 13:50:55

Duration 8.5 s

Element TI % V% Cr % 0.02 0.06 22.17

Grades: Duplex 2205 (0.00), 552304 (0.00) Reference: Duplex 2205

Mn% 0.83

Fe % 67.53

Co % 0.00

Ni % 5.43

Cu % 0.18

Nb % 0.00

Mo% 3.26

W% 0.00

Sn % 0.00

Pb % 0.00

Name K763 1" MOCKUP TUBE HT 539806

Class Stainless

Date 09/01/2017

Time 13:51:14

Duration 8.5 s

Element TI % V% Cr% 0.00 0.08 2228

Grades: Duplex 2205 (0.00), 552304 (0.12) Reference: Duplex 2205

Mn% 0.77

Fe % 67.74

Co % 0.00

NI % 5.54

Cu % 0.17

Nb % 0.00

Mo % 3.26

W% 0.15

5n % 0.00

Pb % 000

Name K763 1" MOCKUP TUBE HT 539806

Class Stainless

Date 09/01/2017

Time 13:51 :32

Duration 8.5 s

Element TI % V% Cr% 0.00 0.14 22.40

Grades: Duplex 2205 (0 DOl, 552304 (0.00) Reference: Duplex 2205

Mn% 0.62

Fe % 67.74

Co % 0.00

NI % 5.28

Cu % 0.22

Nb % 0.00

Mo% 3.29

W% 0.00

5n % 0.00

Pb % 0.00

DeVice SIN: 710199 09/01/2017 - Page 1

Page 48: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

Certified Ortlerl.O. Order Dale

1500373 nlfT'l1

1.3750 Product Shape

Cold Drawn Hex lenqlh (Inches I

132.000 T\/1 i11. 156.000 J\.lux.

5 Id ~O

To

Date· 10/5/2016 To Valbruna Stainless Inc SO# A787248 InV# 1120840 Ln# 1 PO# 12406 Part 316HX1 375 H~dt# 265300 Tag 84410010

~ .

Pl"Oduct Certification Report ~1/%Ln/'/615 Report Number: 5129920 XiS:

on A r 14 2015 Pa e 1 of 2

ClJ~tO"'l4!'r PIJrcha~1't Order

VALBRUNA STAINLESS, INC. Ship 1000 CAl'JNONBALL ROAD

POMPTON LAKES 1 NJ 07442 To

IVALBRUNA STAINLESS, INC. 1000 CANNONBALL RUN POMPTON, NJ 07442

Lifts: 0055 0061 Condition A QQ-S-76JF /\5'!M/\ ~ 32 :.11 3. Cli2Ll ~rl~_Y AS-'::fi'.A 26L-':'.5 AS:MA 276-1S / ASTMA 479-14 AS:MA L.84·14.a ASMESA 479-13· ASTMA 370-12a AHS 5648L AMS 5653H SAE-~~S QQ-S-763C CHEMICAL ANALYSIS

(;0 N(; /. Mr. / P / S Si / (;r / Ni / Mo / (;11 .018 :.48 .031 .025/ .52 16.89 10.16 2.04 .60 . :0 .os

BRINELL (Type A device used) HE\.,T

\\.5515207 PO. '# TENSILE PROPERTIES ASTM E8-13a

TS (2S1) /.Z%YS (PSI) /VoE~_(211)

94800 69300 48.8 MACRO ASTM E340-13/E381-01

MACR:J OK

GRAIN SIZE ASTM El12-13 GRAIN SIZE Etchant Magnification X

7 Oxalic 100 ASTM A262-13 PR E(A Utilized)

OX~LIC Structure Etchant Magnification X QUENCH SENS(F) S~NS(HR)

OK Step Oxalic 500 Air 1200 : .50 No mercury or low melting alloy contamination. Continuous carhide and intergranuJar corrosion test OK. No welding or \vt"!d repair done. Snlutlnn ;W!1ealt'o a1 1900r min. anJ ...... aler ~ctlon atlo ',xct'e S 4: 1 Ekctric Furnace melted; AOD refilled.

No mercury or low' melting alloy contamination. No weld repair

Results relate only to the items tested. Certification shall not be reproduced except In fUll, wJU"lOut written approval of Valbruna Stainless Inc The recording of false. fictitious. or fraudulent statements on this document may be punished as a felony under federal statutes. Including Federal law Title 18, Chapter 47 Consult material safety data sheet (MSDS) for hazard info I hereby certify that the reported figures are correct as contained in the records of the corporation

Monager Laboratory Services ;Vu~,~ ,,,"a', DHacket!@valbruna us· Dennis Hac).;t:1t

Chemical estill!,! to one or more of the listed 1\STM methods: E41:'-J4. F]()19-11. El086-14.

I.ocation of tensile fracture: inSide middle of gage length. Chemical Analysis performed at A.cciaierie Valhruna. Italy.

Page 49: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

Date 10/5/2016 To: Valbruna StaInless Inc SO# A787248 lnv#' 1120840 Ln# 1 PO# 12406 Part 316HX1 375 He~# 265300 Tag 84410010

J~eport Number:

I

Product Certjfication Report

5129920 Paqe 2 of

-----1

/ Product Snapo IPrOduCf Surt"ce

Cold Drawn Hex Cold Drawn Finish lellQlh (lnchesl 14BI121°4'Lotd1"tl # I WeiQht

132.000 Min. 156.000 !\1ax. 7 39 I i VALBRUNA STAINLESS, INC. VALBRUNA STAINLESS 1 INC. 1000 CANNONBALL ROAD Sold 1000 CANNONBALL RUN

Ship POMPTON LAKES I NJ 07442 POMPTON I NJ 07442 To To

Melted and manufactured in Ital~. / 'Matenal conforms to lIsted spec; ications and is DrARS rompl ian!. Uuality system is compliant with ISO YO() 1:2()()8. Produced in aCt.:ordanct' "vilh FN 1()I()4 , 1.

Results relate only to the items tested. Certification shall not oe reproduced except in full, wIthout written approval of Valbruna Stainless Inc The recording of false, fictitious. or fraudulent statements all this document may be punished as a felony under federal statutes. Including Federal law Title 18, Chapter 47 Consult material safety data sheet (MSOS) for hazard info. I hereby certify that the reported figures are correct as contained in the records of the corporation

\1anager I.aboratory Services ~AA"'~ era, DHackeH@valbruna uS ·[)t'nni$ Hackt.'tr

Page 50: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

09247

9/20/2016

lvialenai

Cal Dale

Batch #

80% FSH

Eeno Gel

As ForgE:-d

S,n00Hi

Uit-3:.0'1IC inSO€:C'IOn ReQ0rl

#09120535

HEX BAR STOCK

, Page

12405 Date

IRISNDTt: -------------

:•.n 9

t

P

I:Je

9r8€s'LL'§ ~ I::'equency (rltlZI / ~, ,

Couplant

Item In~pected

Heat Treatment

IRISNDT#

Primary Reference l.eve!

N/A

4 0 U T

EPOCH Xi

005 liS" SH

Procedure

UT EqUiPment

Transier Loss Cal

Cf)'S'QI Size i"IG'1es; J.~.

JOB 1+

P(l#

Lamination

Ram Machine Products l.LC

BACKVVALL

ASME SEC V SA 4351 435M 100%

IIW

IIW

Contact TOF

Ins Ndt T",Isa Okla

Cilenl

Location

Cooe

CalibratIon Block

1 est Piece

Dlstar;ceJAmp Cal

Ref Flaw Size

Scar> ioAethod

Scope 100u/" UltrasoniC InspectIon Of Hex Bar Stock

Results PO#, :2406

1'.401375" X 12' Hex Bars SS316L

/

Scanned 360 degrees

'\ )

.~

All Pieces Meet Code Requirements

Miles Hrs Consumables Technician JOHN DAGGS

I-P_e_r_s._o_n_n~e_I -'-- L- t- M_'_nl_n_lu_m_,_. -t_T_e_C_h_rl_IC_'a_n ....:- -__~_-_.'__ __-____ __'_~ (SIgn j

John Daggs SNT· TC 1A Level

r : :::::::_:::- ::: : :_~_'_a_m_ln_fu_I_1_a_

9r p

Client RepresentatIve _

I j?

Tulsa Oklahoma

I 11 f:;, v've51 41 Sf ::>treel _e_e_m_._e_n_t_W_'I_h_r_e__o_r:_c_o_n_l_e_n_15_' ..1

L Phone 918-446·3773 Fax 918-445-8777

IRISNDT2529

Page 51: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

Inspection Certificate: EXP14402121 As per: EN 10204 3.1

voestalpine Bohler Welding USA, Inc.

Test Object: SAW ./

Grade Designation: AVESTA ER2209 ,/

Marking of Product

Standard Designation: AWS/SFA A5.9: ER2209

Requirements:

voestalpine Bohler Welding USA, Inc. 10401 Greenbough Drive Stafford, TX 77477 Tele: 281-499-1212,800-527-0791 Fax: 281-499-4347

/' Dimensions: 3/32" ,

Lot No. : E50974

Delivery Qty. :

III' -'~_Wo_

/J

(£i' A

I'~

Actual Chemical Composition in % All weld metal

Lot/Heat Si Mo NC Mn P Ni Cr FN WRC 1992

E50974

S Cu

1.46 0.410.02 0.020 0.001 23.10 50.30.06 8.60 3.30 0.17

Tensile Test

Minimum: Maximum: Impact Test:

As per Test Temp.

T

°C

As per

Test Temp

T

ASTM E8 Yield Point

Reh

Mpa

ASTM E23

Absorbed Energy Minimum Values

KV

Specimen Preparation Yield Strength

Rp

0.2%MPuI.0%

Specimen Preparation

Average

AWS 84.0 Elongation

A

% Lo=4d

AWS 84.0

Lateral Expansion

Reductions Z

%

Shear Fracture

Note Note:

This product meets the requirements of the indicated filler metal specification when tested in accordance with that specification. This certificate was issued by DP-equipment and does not require siQnature. Authorized inspection representative:

°c J J MM % Russel Fuchs Loc: Stafford, TX Date: 08/08/2014

3GD /..8$ J:-£~.;LJ 9 ~ IX 00 uJ1RL

Page 52: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

voest!"Jpine Bohler Welding Belgium S.A.

voestalpine Bohler Welding Belgium S.A. Rue de I'Yser2 B·7180 Seneffe, Belgium T.+32(0) 64 520 000 F.+32(0) 64 520001

www.voeslalpine.comlwelding ~1~Yil6'lP

voestalpine Bohler Welding USA, Inc Test Report 2.2

1601 Gillingham, Suite #110 as per: EN 10204 77478 Sugar Land No. : 2016-2007050890-000010-003 USA Rev. 0 Page 1 of 1

PO no. 4250011017 of 12.05.2016

Order no. 1007027179

Delivery note/pos.lsplitt

Product

Trade name

Standard designation

Dimension

2007050890/000000/000010

Agglomerated flux .

RECORD IND 24 /'

EN ISO 14174: S A- FB 2

of 20,06.2016

300017

2S071

7FB2~03W

0072

Serial no. 7502939

Quantity 14000,0 KG

Chemical composition in % of the weld deposit"

Others

I ] I I I I G~~;::8 I Mechanical properties

RpO,2 EN RmEN A4 AS average impact test ZEN

MPA MPA % % J/20 CO I J 1-30 CO %

570 800 32 30 110 , 90 50

Chemical composition in % THERMANIT 22/09 3,0 mm

Heat No. e Si Mn P S Cr Ni Mo N Cu

102147 0,00 0,0 0,0 0,000 0,000 0,0 0,0 0,0 0,00 0,0

5 layers on inox 450N28V138cm/min

Town

Seneffe

This cer1ificate was issued bv DP-eQUipment and does not require siQnalure.

Date

30.06.2016

Authorized representative

Brion

voestalpine ONE STEP AHEAD.

0U) 185 INLJ J1 fZ if)\,

Page 53: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

lnspection Certificate: EXP 15601459 As per: EN 10204 3.1

voestalpine Bohler Welding USA, Inc.

Test Object: GTAW /'

Grade Designation: AVESTA ER2209 ,/

Marking of Product

Standard Designation: AWS/SFA AS.9: ER2209

Requirements:

Actual Chemical Composition in % All weld metal

voestalpine Bohler Welding USA, Inc. 10401 Greenbough Drive Stafford, TX 77477 Tele: 281-499-1212, 800-527-0791 Fax: 281-499-4347

/ Dimensions: 3/32 x 36 "

Lot No.: E64183

Delivery Qty. :

I~ ~~: .. ' ....

[i voesta~ BeilIer Welding 'J

A A

~L I(

Lot/Heat C Mn Si P S Cu Ni Cr Mo N FN WRC

E64183 0.01 1.46 0.43 0.020 0.001 0.04 8.60 23.10 3.30 0.14 65.2

Tensile Test

Typical

Impact Test:

As per Test Temp.

T

OF 68

As per

Test Temp

T

ASTM E8 Yield Strength

ksi

ASTM E23

Absorbed Ener:gy Minimum Values

KV

Specimen Preparation Tensile Strength

ksi 85

Specimen Preparation

Average

AWS 84.0 Elongation

A

% Lo=4d 35

AWS 84.0

Lateral Expansion

Reductions Z

%

Shear Fracture

Note Note:

This product meets the requirements of the indicated tiller metal specification when tested in accordance with that specification. This certificate was issued by DP-equipment and does not require signature. Authorized inspection representative:

OF J J MM % Russel Fuchs Loc: Stafford, TX Date: 09/16/2015

. V',! /1

f5() /.-65 £..ej,20q ~; )( 30 u.J:r.~

Page 54: CERTIFIED MATERIAL TEST REPORT SSC ORDER NO: 13465

voestalpine Bohler Welding USA Inc. voestalpine Bohler Welding USA Inc. 10401 Greenbough Drive, Stafford, Texas 77477

Tel: +1 281-499-1212 Fax: +1 281-499-4347

Website www.voestalpine.com/welding

'"

~;1 DXP Enterprise, Inc.

Houston USA

Certificate Schedule F as per: ASME/AWS A5.01 No. : 2016-2025228541-900001-004 Rev. 0 Page 1 of 1

PO no.

Order no.

Delivery note/pos.lsplitt

Product

Trade name

Standard designation

4677733

1025154526

2025228541/000010/900001

covered electrode

AVESTA 2205 BASIC ./

AWS A5.4 E2209-15

EN ISO 3581-A E 22 9 3 N L B

of

of

11.10.2016

08.12.2016

235422

81438

2SC1A06E

0251

Dimension

Serial no.

Quantity

d

~d1 SMAW 4,0 x 350 mm

2131554

20,0 KG

Chemical composition in % of the weld metal

C Si Mn P S Cr Mo Ni Cu N

0,03 0,47 1,02 0,019 0,011 22,70 2,96 9,05 0,05 0,160

Mechanical properties

Tensile test

ReL 1Rp 0,2 Z WBH RemarksRp 1,0 RmT A (Lo =4d)

PWHTMPa MPa MPa % %

~ 20~ 69020°C

Impact test

T RemarksImpact energy Shear fracture WBHAverage Lateral expansion

PWHTKV 1J mm %KV I J

Town Date Authorized representative This certificate was issued by DP-equipment and does not require signature. Russel Fuchs Stafford 12.12.2016