Canadian Pacific Plaza Attn: Jeremy Coughlin 120 South 6th ... · Attn: Jeremy Coughlin 120 South 6th Street Suite 700 Minneapolis, MN 55402 RE: SHOREHAM YARD – CEDAR SERVICE PUMP

Golder Associates Inc. 1751 West County Road B, Suite 105 Roseville, Minnesota, USA 55113 T: +1 651 697-9737 +1 651 697-9735

Golder and the G logo are trademarks of Golder Associates Corporation golder.com

Project No. 0236105019 October 11, 2019

Canadian Pacific Plaza

Attn: Jeremy Coughlin

120 South 6th Street

Suite 700

Minneapolis, MN 55402

RE: SHOREHAM YARD – CEDAR SERVICE PUMP & TREAT SYSTEM MCES SPECIAL DISCHARGE PERMIT 2286 SELF-MONITORING REPORT ELECTRONIC SUBMITTAL -

AUGUST 2019 SAMPLE RESULTS INFORMATION

Dear Jeremy,

Enclosed is a copy of the Metropolitan Council Environmental Services (MCES) Self-Monitoring Report (SMR)

submitted electronically to the MCES on September 27, 2019 for the Cedar Service Pump & Treat System. The

following documents are enclosed:

Sampling Results SMR – August, 2019 Analytical Data from Pace Analytical Services – August, 2019

If you have any questions regarding these submittals, please contact the undersigned at 651-697-9737.

Sincerely,

Golder Associates Inc.

Neha Damle Ryan Birkenholz, P.E.

Engineer Associate and Senior Consultant

ND/RCB/nd

CC: Claire Mackler, Golder

rbirkenholz

RyanBirkenholz

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#=CL#

September 10, 2019

LIMS USE: FR - KAT SMITHLIMS OBJECT ID: 40193956

40193956Project:Pace Project No.:

RE:

Kat SmithGolder Associates, Inc.200 Century ParkwaySuite CMount Laurel, NJ 08054

0236105019 CP CS

Dear Kat Smith:Enclosed are the analytical results for sample(s) received by the laboratory on August 29, 2019. Theresults relate only to the samples included in this report. Results reported herein conform to the mostcurrent, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, whereapplicable, unless otherwise noted in the body of the report.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Laurie [email protected]

Project Manager(920)469-2436

Enclosures

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, LLC.

Pace Analytical Services, LLC1241 Bellevue Street - Suite 9

Green Bay, WI 54302(920)469-2436

Page 1 of 35

#=CP#

CERTIFICATIONS

Pace Project No.:Project:

401939560236105019 CP CS

Green Bay Certification IDs1241 Bellevue Street, Green Bay, WI 54302Florida/NELAP Certification #: E87948Illinois Certification #: 200050Kentucky UST Certification #: 82Louisiana Certification #: 04168Minnesota Certification #: 055-999-334New York Certification #: 12064North Dakota Certification #: R-150

Virginia VELAP ID: 460263South Carolina Certification #: 83006001Texas Certification #: T104704529-14-1Wisconsin Certification #: 405132750Wisconsin DATCP Certification #: 105-444USDA Soil Permit #: P330-16-00157Federal Fish & Wildlife Permit #: LE51774A-0




Green Bay, WI 54302(920)469-2436

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#=SS#

SAMPLE SUMMARY


401939560236105019 CP CS

Lab ID Sample ID Matrix Date Collected Date Received

40193956001 082819-0800-200 Water 08/28/19 08:00 08/29/19 09:10

40193956002 RW06-24-MS-0819-100 Water 08/28/19 10:30 08/29/19 09:10

40193956003 RW07-44-MS-0819-100 Water 08/28/19 10:45 08/29/19 09:10

40193956004 CS IN BETWEEN Water 08/28/19 11:00 08/29/19 09:10

40193956005 CS EFFLUENT Water 08/28/19 11:15 08/29/19 09:10




Green Bay, WI 54302(920)469-2436

Page 3 of 35

#=SA#

SAMPLE ANALYTE COUNT


401939560236105019 CP CS

Lab ID Sample ID MethodAnalytesReported LaboratoryAnalysts

40193956001 082819-0800-200 EPA 8260 70 PASI-GSMT

40193956002 RW06-24-MS-0819-100 EPA 8270 13 PASI-GRJN

EPA 8270 71 PASI-GRJN

EPA 8260 70 PASI-GLAP

40193956003 RW07-44-MS-0819-100 EPA 8270 13 PASI-GRJN


EPA 8260 70 PASI-GLAP

40193956004 CS IN BETWEEN EPA 8270 3 PASI-GRJN

40193956005 CS EFFLUENT EPA 8270 13 PASI-GRJN





Green Bay, WI 54302(920)469-2436

Page 4 of 35

#=AR#

ANALYTICAL RESULTS


401939560236105019 CP CS

Sample: 082819-0800-200 Lab ID: 40193956001 Collected: 08/28/19 08:00 Received: 08/29/19 09:10 Matrix: Water

Parameters Results Units DF Prepared Analyzed CAS No. QualMDLPQL

Analytical Method: EPA 82608260 MSV

Acetone <2.7 ug/L 08/30/19 14:22 67-64-120.0 2.7 1Allyl chloride <0.60 ug/L 08/30/19 14:22 107-05-15.0 0.60 1Benzene <0.25 ug/L 08/30/19 14:22 71-43-21.0 0.25 1Bromobenzene <0.24 ug/L 08/30/19 14:22 108-86-11.0 0.24 1Bromochloromethane <0.36 ug/L 08/30/19 14:22 74-97-55.0 0.36 1Bromodichloromethane <0.36 ug/L 08/30/19 14:22 75-27-41.2 0.36 1Bromoform <4.0 ug/L 08/30/19 14:22 75-25-213.2 4.0 1Bromomethane <0.97 ug/L 08/30/19 14:22 74-83-95.0 0.97 12-Butanone (MEK) <2.9 ug/L 08/30/19 14:22 78-93-320.0 2.9 1n-Butylbenzene <0.71 ug/L 08/30/19 14:22 104-51-82.4 0.71 1sec-Butylbenzene <0.85 ug/L 08/30/19 14:22 135-98-85.0 0.85 1tert-Butylbenzene <0.30 ug/L 08/30/19 14:22 98-06-61.0 0.30 1Carbon tetrachloride <0.17 ug/L 08/30/19 14:22 56-23-51.0 0.17 1Chlorobenzene <0.71 ug/L 08/30/19 14:22 108-90-72.4 0.71 1Chloroethane <1.3 ug/L 08/30/19 14:22 75-00-35.0 1.3 1Chloroform <1.3 ug/L 08/30/19 14:22 67-66-35.0 1.3 1Chloromethane <2.2 ug/L 08/30/19 14:22 74-87-37.3 2.2 12-Chlorotoluene <0.93 ug/L 08/30/19 14:22 95-49-85.0 0.93 14-Chlorotoluene <0.76 ug/L 08/30/19 14:22 106-43-42.5 0.76 11,2-Dibromo-3-chloropropane <1.8 ug/L 08/30/19 14:22 96-12-85.9 1.8 1Dibromochloromethane <2.6 ug/L 08/30/19 14:22 124-48-18.7 2.6 11,2-Dibromoethane (EDB) <0.83 ug/L 08/30/19 14:22 106-93-42.8 0.83 1Dibromomethane <0.94 ug/L 08/30/19 14:22 74-95-33.1 0.94 11,2-Dichlorobenzene <0.71 ug/L 08/30/19 14:22 95-50-12.4 0.71 11,3-Dichlorobenzene <0.63 ug/L 08/30/19 14:22 541-73-12.1 0.63 11,4-Dichlorobenzene <0.94 ug/L 08/30/19 14:22 106-46-73.1 0.94 1Dichlorodifluoromethane <0.50 ug/L 08/30/19 14:22 75-71-85.0 0.50 11,1-Dichloroethane <0.27 ug/L 08/30/19 14:22 75-34-31.0 0.27 11,2-Dichloroethane <0.28 ug/L 08/30/19 14:22 107-06-21.0 0.28 11,1-Dichloroethene <0.24 ug/L 08/30/19 14:22 75-35-41.0 0.24 1cis-1,2-Dichloroethene <0.27 ug/L 08/30/19 14:22 156-59-21.0 0.27 1trans-1,2-Dichloroethene <1.1 ug/L 08/30/19 14:22 156-60-53.6 1.1 1Dichlorofluoromethane <1.4 ug/L 08/30/19 14:22 75-43-45.0 1.4 11,2-Dichloropropane <0.28 ug/L 08/30/19 14:22 78-87-51.0 0.28 11,3-Dichloropropane <0.83 ug/L 08/30/19 14:22 142-28-92.8 0.83 12,2-Dichloropropane <2.3 ug/L 08/30/19 14:22 594-20-77.6 2.3 11,1-Dichloropropene <0.54 ug/L 08/30/19 14:22 563-58-61.8 0.54 1cis-1,3-Dichloropropene <3.6 ug/L 08/30/19 14:22 10061-01-512.1 3.6 1trans-1,3-Dichloropropene <4.4 ug/L 08/30/19 14:22 10061-02-614.6 4.4 1Diethyl ether (Ethyl ether) <1.5 ug/L 08/30/19 14:22 60-29-75.1 1.5 1Ethylbenzene <0.22 ug/L 08/30/19 14:22 100-41-41.0 0.22 1Hexachloro-1,3-butadiene <1.2 ug/L 08/30/19 14:22 87-68-35.0 1.2 1Isopropylbenzene (Cumene) <0.39 ug/L 08/30/19 14:22 98-82-85.0 0.39 1p-Isopropyltoluene <0.80 ug/L 08/30/19 14:22 99-87-62.7 0.80 1Methylene Chloride <0.58 ug/L 08/30/19 14:22 75-09-25.0 0.58 14-Methyl-2-pentanone (MIBK) <1.5 ug/L 08/30/19 14:22 108-10-15.1 1.5 1


without the written consent of Pace Analytical Services, LLC.Date: 09/10/2019 03:26 PM


Green Bay, WI 54302(920)469-2436

Page 5 of 35

#=AR#

ANALYTICAL RESULTS


401939560236105019 CP CS

Sample: 082819-0800-200 Lab ID: 40193956001 Collected: 08/28/19 08:00 Received: 08/29/19 09:10 Matrix: Water



Methyl-tert-butyl ether <1.2 ug/L 08/30/19 14:22 1634-04-44.2 1.2 1Naphthalene <1.2 ug/L 08/30/19 14:22 91-20-35.0 1.2 1n-Propylbenzene <0.81 ug/L 08/30/19 14:22 103-65-15.0 0.81 1Styrene <0.47 ug/L 08/30/19 14:22 100-42-51.6 0.47 11,1,1,2-Tetrachloroethane <0.27 ug/L 08/30/19 14:22 630-20-61.0 0.27 11,1,2,2-Tetrachloroethane <0.28 ug/L 08/30/19 14:22 79-34-51.0 0.28 1Tetrachloroethene <0.33 ug/L 08/30/19 14:22 127-18-41.1 0.33 1Toluene <0.17 ug/L 08/30/19 14:22 108-88-35.0 0.17 11,2,3-Trichlorobenzene <0.63 ug/L 08/30/19 14:22 87-61-65.0 0.63 11,2,4-Trichlorobenzene <0.95 ug/L 08/30/19 14:22 120-82-15.0 0.95 11,1,1-Trichloroethane <0.24 ug/L 08/30/19 14:22 71-55-61.0 0.24 11,1,2-Trichloroethane <0.55 ug/L 08/30/19 14:22 79-00-55.0 0.55 1Trichloroethene <0.26 ug/L 08/30/19 14:22 79-01-61.0 0.26 1Trichlorofluoromethane <0.21 ug/L 08/30/19 14:22 75-69-41.0 0.21 11,2,3-Trichloropropane <0.59 ug/L 08/30/19 14:22 96-18-45.0 0.59 11,1,2-Trichlorotrifluoroethane <0.54 ug/L 08/30/19 14:22 76-13-15.0 0.54 11,2,4-Trimethylbenzene <0.84 ug/L 08/30/19 14:22 95-63-62.8 0.84 11,3,5-Trimethylbenzene <0.87 ug/L 08/30/19 14:22 108-67-82.9 0.87 1Vinyl chloride <0.17 ug/L 08/30/19 14:22 75-01-41.0 0.17 1m&p-Xylene <0.47 ug/L 08/30/19 14:22 179601-23-12.0 0.47 1o-Xylene <0.26 ug/L 08/30/19 14:22 95-47-61.0 0.26 1Surrogates4-Bromofluorobenzene (S) 87 % 08/30/19 14:22 460-00-470-130 1Dibromofluoromethane (S) 124 % 08/30/19 14:22 1868-53-770-130 1Toluene-d8 (S) 90 % 08/30/19 14:22 2037-26-570-130 1




Green Bay, WI 54302(920)469-2436

Page 6 of 35

#=AR#

ANALYTICAL RESULTS


401939560236105019 CP CS

Sample: RW06-24-MS-0819-100 Lab ID: 40193956002 Collected: 08/28/19 10:30 Received: 08/29/19 09:10 Matrix: Water


Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Phenols

3-Chlorophenol <22.6 ug/L 09/09/19 19:19 108-43-008/30/19 07:1075.8 22.6 402,4-Dichlorophenol <21.9 ug/L 09/09/19 19:19 120-83-208/30/19 07:1072.5 21.9 403,4-Dichlorophenol <22.6 ug/L 09/09/19 19:19 95-77-208/30/19 07:1075.5 22.6 403,5-Dichlorophenol <28.3 ug/L 09/09/19 19:19 591-35-508/30/19 07:1094.0 28.3 40Pentachlorophenol 1320 ug/L 09/09/19 19:19 87-86-5 R408/30/19 07:1037.0 10.9 402,3,4,5-Tetrachlorophenol 45.1J ug/L 09/09/19 19:19 4901-51-3 R408/30/19 07:1068.7 20.8 402,3,4,6-Tetrachlorophenol 59.7J ug/L 09/09/19 19:19 58-90-208/30/19 07:10112 33.6 402,3,5-Trichlorophenol <22.3 ug/L 09/09/19 19:19 933-78-808/30/19 07:1074.0 22.3 402,3,6-Trichlorophenol <21.9 ug/L 09/09/19 19:19 933-75-508/30/19 07:1072.5 21.9 402,4,5-Trichlorophenol <17.4 ug/L 09/09/19 19:19 95-95-408/30/19 07:1057.4 17.4 402,4,6-Trichlorophenol <20.0 ug/L 09/09/19 19:19 88-06-208/30/19 07:1067.2 20.0 40SurrogatesPhenol-d6 (S) 0 % 09/09/19 19:19 13127-88-3 S408/30/19 07:1024-120 402,4,6-Tribromophenol (S) 0 % 09/09/19 19:19 118-79-6 S408/30/19 07:1043-140 40

Analytical Method: EPA 8270 Preparation Method: EPA 35108270 MSSV Semivolatile Organic

Acenaphthene <28.8 ug/L 09/06/19 19:58 83-32-909/04/19 06:07189 28.8 40Acenaphthylene <27.5 ug/L 09/06/19 19:58 208-96-809/04/19 06:07189 27.5 40Anthracene <30.6 ug/L 09/06/19 19:58 120-12-7 M609/04/19 06:07189 30.6 40Benzo(a)anthracene <32.0 ug/L 09/06/19 19:58 56-55-309/04/19 06:07189 32.0 40Benzo(a)pyrene <48.0 ug/L 09/06/19 19:58 50-32-8 M609/04/19 06:07189 48.0 40Benzo(b)fluoranthene <39.1 ug/L 09/06/19 19:58 205-99-2 M609/04/19 06:07189 39.1 40Benzo(g,h,i)perylene <52.0 ug/L 09/06/19 19:58 191-24-209/04/19 06:07189 52.0 40Benzo(k)fluoranthene <42.4 ug/L 09/06/19 19:58 207-08-9 M609/04/19 06:07189 42.4 404-Bromophenylphenyl ether <36.1 ug/L 09/06/19 19:58 101-55-309/04/19 06:07189 36.1 40Butylbenzylphthalate <49.0 ug/L 09/06/19 19:58 85-68-7 M609/04/19 06:07189 49.0 40Carbazole <34.5 ug/L 09/06/19 19:58 86-74-8 M609/04/19 06:07189 34.5 404-Chloro-3-methylphenol <25.8 ug/L 09/06/19 19:58 59-50-7 M609/04/19 06:07189 25.8 404-Chloroaniline <67.4 ug/L 09/06/19 19:58 106-47-8 M609/04/19 06:07225 67.4 40bis(2-Chloroethoxy)methane <49.3 ug/L 09/06/19 19:58 111-91-1 M609/04/19 06:07189 49.3 40bis(2-Chloroethyl) ether <44.1 ug/L 09/06/19 19:58 111-44-4 M609/04/19 06:07189 44.1 402-Chloronaphthalene <31.3 ug/L 09/06/19 19:58 91-58-7 M609/04/19 06:07189 31.3 402-Chlorophenol <31.3 ug/L 09/06/19 19:58 95-57-8 M609/04/19 06:07189 31.3 404-Chlorophenylphenyl ether <31.3 ug/L 09/06/19 19:58 7005-72-3 M609/04/19 06:07189 31.3 40Chrysene <47.9 ug/L 09/06/19 19:58 218-01-9 M609/04/19 06:07189 47.9 40Dibenz(a,h)anthracene <41.7 ug/L 09/06/19 19:58 53-70-3 M609/04/19 06:07189 41.7 40Dibenzofuran <32.0 ug/L 09/06/19 19:58 132-64-909/04/19 06:07189 32.0 401,2-Dichlorobenzene <54.5 ug/L 09/06/19 19:58 95-50-1 M609/04/19 06:07189 54.5 401,3-Dichlorobenzene <58.3 ug/L 09/06/19 19:58 541-73-1 M609/04/19 06:07194 58.3 401,4-Dichlorobenzene <54.3 ug/L 09/06/19 19:58 106-46-7 M609/04/19 06:07189 54.3 403,3'-Dichlorobenzidine <50.7 ug/L 09/06/19 19:58 91-94-1 L1,M609/04/19 06:07189 50.7 402,4-Dichlorophenol <33.8 ug/L 09/06/19 19:58 120-83-2 M609/04/19 06:07189 33.8 40Diethylphthalate <29.3 ug/L 09/06/19 19:58 84-66-2 M609/04/19 06:07189 29.3 402,4-Dimethylphenol <43.7 ug/L 09/06/19 19:58 105-67-9 M609/04/19 06:07189 43.7 40Dimethylphthalate <27.2 ug/L 09/06/19 19:58 131-11-3 M609/04/19 06:07189 27.2 40Di-n-butylphthalate <46.4 ug/L 09/06/19 19:58 84-74-2 M609/04/19 06:07189 46.4 40




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4,6-Dinitro-2-methylphenol <118 ug/L 09/06/19 19:58 534-52-1 M609/04/19 06:07392 118 402,4-Dinitrophenol <92.5 ug/L 09/06/19 19:58 51-28-5 M609/04/19 06:07308 92.5 402,4-Dinitrotoluene <40.0 ug/L 09/06/19 19:58 121-14-2 M609/04/19 06:07189 40.0 402,6-Dinitrotoluene <29.2 ug/L 09/06/19 19:58 606-20-2 M6,R409/04/19 06:07189 29.2 40Di-n-octylphthalate <180 ug/L 09/06/19 19:58 117-84-0 M609/04/19 06:07600 180 40bis(2-Ethylhexyl)phthalate <109 ug/L 09/06/19 19:58 117-81-7 M609/04/19 06:07362 109 40Fluoranthene <37.3 ug/L 09/06/19 19:58 206-44-0 M609/04/19 06:07189 37.3 40Fluorene <34.2 ug/L 09/06/19 19:58 86-73-709/04/19 06:07189 34.2 40Hexachloro-1,3-butadiene <43.3 ug/L 09/06/19 19:58 87-68-3 M609/04/19 06:07208 43.3 40Hexachlorobenzene <62.3 ug/L 09/06/19 19:58 118-74-1 M609/04/19 06:07189 62.3 40Hexachlorocyclopentadiene <38.0 ug/L 09/06/19 19:58 77-47-4 M609/04/19 06:07189 38.0 40Hexachloroethane <53.6 ug/L 09/06/19 19:58 67-72-1 M609/04/19 06:07189 53.6 40Indeno(1,2,3-cd)pyrene <45.9 ug/L 09/06/19 19:58 193-39-5 M609/04/19 06:07189 45.9 40Isophorone <29.2 ug/L 09/06/19 19:58 78-59-1 M609/04/19 06:07189 29.2 402-Methylnaphthalene <43.9 ug/L 09/06/19 19:58 91-57-609/04/19 06:07189 43.9 402-Methylphenol(o-Cresol) <35.1 ug/L 09/06/19 19:58 95-48-7 M609/04/19 06:07189 35.1 403&4-Methylphenol(m&p Cresol) <23.1 ug/L 09/06/19 19:58 M609/04/19 06:07189 23.1 40Naphthalene <46.0 ug/L 09/06/19 19:58 91-20-3 M609/04/19 06:07189 46.0 402-Nitroaniline <35.8 ug/L 09/06/19 19:58 88-74-4 M6,R409/04/19 06:07189 35.8 403-Nitroaniline <51.5 ug/L 09/06/19 19:58 99-09-2 M609/04/19 06:07189 51.5 404-Nitroaniline <113 ug/L 09/06/19 19:58 100-01-6 M609/04/19 06:07377 113 40Nitrobenzene <40.6 ug/L 09/06/19 19:58 98-95-3 M609/04/19 06:07189 40.6 402-Nitrophenol <31.2 ug/L 09/06/19 19:58 88-75-5 M609/04/19 06:07189 31.2 404-Nitrophenol <115 ug/L 09/06/19 19:58 100-02-7 M609/04/19 06:07385 115 40N-Nitroso-di-n-propylamine <42.8 ug/L 09/06/19 19:58 621-64-7 M609/04/19 06:07189 42.8 40N-Nitrosodiphenylamine <130 ug/L 09/06/19 19:58 86-30-6 M609/04/19 06:07434 130 402,2'-Oxybis(1-chloropropane) <46.5 ug/L 09/06/19 19:58 108-60-1 M609/04/19 06:07189 46.5 40Pentachlorophenol 1260 ug/L 09/06/19 19:58 87-86-5 M609/04/19 06:07574 172 40Phenanthrene <36.0 ug/L 09/06/19 19:58 85-01-809/04/19 06:07189 36.0 40Phenol <12.1 ug/L 09/06/19 19:58 108-95-2 M609/04/19 06:07189 12.1 40Pyrene <45.3 ug/L 09/06/19 19:58 129-00-0 M609/04/19 06:07189 45.3 401,2,4,5-Tetrachlorobenzene <37.7 ug/L 09/06/19 19:58 95-94-309/04/19 06:07189 37.7 401,2,4-Trichlorobenzene <59.3 ug/L 09/06/19 19:58 120-82-1 M609/04/19 06:07197 59.3 402,4,5-Trichlorophenol <24.3 ug/L 09/06/19 19:58 95-95-4 M609/04/19 06:07189 24.3 402,4,6-Trichlorophenol <30.1 ug/L 09/06/19 19:58 88-06-2 M609/04/19 06:07189 30.1 40SurrogatesNitrobenzene-d5 (S) 0 % 09/06/19 19:58 4165-60-0 S409/04/19 06:0751-108 402-Fluorobiphenyl (S) 0 % 09/06/19 19:58 321-60-8 S409/04/19 06:0747-105 40Terphenyl-d14 (S) 0 % 09/06/19 19:58 1718-51-0 S409/04/19 06:0765-147 40Phenol-d6 (S) 0 % 09/06/19 19:58 13127-88-3 S409/04/19 06:0718-120 402-Fluorophenol (S) 0 % 09/06/19 19:58 367-12-4 S409/04/19 06:0732-120 402,4,6-Tribromophenol (S) 0 % 09/06/19 19:58 118-79-6 S409/04/19 06:0757-131 40


Acetone 3.6J ug/L 09/04/19 09:32 67-64-120.0 2.7 1Allyl chloride <0.60 ug/L 09/04/19 09:32 107-05-15.0 0.60 1




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Benzene <0.25 ug/L 09/04/19 09:32 71-43-21.0 0.25 1Bromobenzene <0.24 ug/L 09/04/19 09:32 108-86-11.0 0.24 1Bromochloromethane <0.36 ug/L 09/04/19 09:32 74-97-55.0 0.36 1Bromodichloromethane <0.36 ug/L 09/04/19 09:32 75-27-41.2 0.36 1Bromoform <4.0 ug/L 09/04/19 09:32 75-25-25.0 4.0 1Bromomethane <0.97 ug/L 09/04/19 09:32 74-83-95.0 0.97 12-Butanone (MEK) <2.9 ug/L 09/04/19 09:32 78-93-320.0 2.9 1n-Butylbenzene <0.71 ug/L 09/04/19 09:32 104-51-82.4 0.71 1sec-Butylbenzene <0.85 ug/L 09/04/19 09:32 135-98-85.0 0.85 1tert-Butylbenzene <0.30 ug/L 09/04/19 09:32 98-06-61.0 0.30 1Carbon tetrachloride <0.17 ug/L 09/04/19 09:32 56-23-51.0 0.17 1Chlorobenzene <0.71 ug/L 09/04/19 09:32 108-90-72.4 0.71 1Chloroethane <1.3 ug/L 09/04/19 09:32 75-00-35.0 1.3 1Chloroform <1.3 ug/L 09/04/19 09:32 67-66-35.0 1.3 1Chloromethane <2.2 ug/L 09/04/19 09:32 74-87-37.3 2.2 12-Chlorotoluene <0.93 ug/L 09/04/19 09:32 95-49-85.0 0.93 14-Chlorotoluene <0.76 ug/L 09/04/19 09:32 106-43-42.5 0.76 11,2-Dibromo-3-chloropropane <1.8 ug/L 09/04/19 09:32 96-12-85.9 1.8 1Dibromochloromethane <2.6 ug/L 09/04/19 09:32 124-48-15.0 2.6 11,2-Dibromoethane (EDB) <0.83 ug/L 09/04/19 09:32 106-93-42.8 0.83 1Dibromomethane <0.94 ug/L 09/04/19 09:32 74-95-33.1 0.94 11,2-Dichlorobenzene <0.71 ug/L 09/04/19 09:32 95-50-12.4 0.71 11,3-Dichlorobenzene <0.63 ug/L 09/04/19 09:32 541-73-12.1 0.63 11,4-Dichlorobenzene <0.94 ug/L 09/04/19 09:32 106-46-73.1 0.94 1Dichlorodifluoromethane <0.50 ug/L 09/04/19 09:32 75-71-85.0 0.50 11,1-Dichloroethane <0.27 ug/L 09/04/19 09:32 75-34-31.0 0.27 11,2-Dichloroethane 0.38J ug/L 09/04/19 09:32 107-06-21.0 0.28 11,1-Dichloroethene <0.24 ug/L 09/04/19 09:32 75-35-41.0 0.24 1cis-1,2-Dichloroethene <0.27 ug/L 09/04/19 09:32 156-59-21.0 0.27 1trans-1,2-Dichloroethene <1.1 ug/L 09/04/19 09:32 156-60-53.6 1.1 1Dichlorofluoromethane <1.4 ug/L 09/04/19 09:32 75-43-45.0 1.4 11,2-Dichloropropane <0.28 ug/L 09/04/19 09:32 78-87-51.0 0.28 11,3-Dichloropropane <0.83 ug/L 09/04/19 09:32 142-28-92.8 0.83 12,2-Dichloropropane <2.3 ug/L 09/04/19 09:32 594-20-77.6 2.3 11,1-Dichloropropene <0.54 ug/L 09/04/19 09:32 563-58-61.8 0.54 1cis-1,3-Dichloropropene <3.6 ug/L 09/04/19 09:32 10061-01-55.0 3.6 1trans-1,3-Dichloropropene <4.4 ug/L 09/04/19 09:32 10061-02-620.0 4.4 1Diethyl ether (Ethyl ether) <1.5 ug/L 09/04/19 09:32 60-29-75.1 1.5 1Ethylbenzene <0.22 ug/L 09/04/19 09:32 100-41-41.0 0.22 1Hexachloro-1,3-butadiene <1.2 ug/L 09/04/19 09:32 87-68-35.0 1.2 1Isopropylbenzene (Cumene) <0.39 ug/L 09/04/19 09:32 98-82-85.0 0.39 1p-Isopropyltoluene <0.80 ug/L 09/04/19 09:32 99-87-62.7 0.80 1Methylene Chloride <0.58 ug/L 09/04/19 09:32 75-09-25.0 0.58 14-Methyl-2-pentanone (MIBK) <1.5 ug/L 09/04/19 09:32 108-10-120.0 1.5 1Methyl-tert-butyl ether <1.2 ug/L 09/04/19 09:32 1634-04-44.2 1.2 1Naphthalene <1.2 ug/L 09/04/19 09:32 91-20-35.0 1.2 1




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n-Propylbenzene <0.81 ug/L 09/04/19 09:32 103-65-15.0 0.81 1Styrene <0.47 ug/L 09/04/19 09:32 100-42-51.6 0.47 11,1,1,2-Tetrachloroethane <0.27 ug/L 09/04/19 09:32 630-20-61.0 0.27 11,1,2,2-Tetrachloroethane <0.28 ug/L 09/04/19 09:32 79-34-51.0 0.28 1Tetrachloroethene <0.33 ug/L 09/04/19 09:32 127-18-41.1 0.33 1Toluene <0.17 ug/L 09/04/19 09:32 108-88-35.0 0.17 11,2,3-Trichlorobenzene <0.63 ug/L 09/04/19 09:32 87-61-65.0 0.63 11,2,4-Trichlorobenzene <0.95 ug/L 09/04/19 09:32 120-82-15.0 0.95 11,1,1-Trichloroethane <0.24 ug/L 09/04/19 09:32 71-55-61.0 0.24 11,1,2-Trichloroethane <0.55 ug/L 09/04/19 09:32 79-00-55.0 0.55 1Trichloroethene <0.26 ug/L 09/04/19 09:32 79-01-61.0 0.26 1Trichlorofluoromethane <0.21 ug/L 09/04/19 09:32 75-69-41.0 0.21 11,2,3-Trichloropropane <0.59 ug/L 09/04/19 09:32 96-18-45.0 0.59 11,1,2-Trichlorotrifluoroethane <0.54 ug/L 09/04/19 09:32 76-13-15.0 0.54 11,2,4-Trimethylbenzene <0.84 ug/L 09/04/19 09:32 95-63-62.8 0.84 11,3,5-Trimethylbenzene <0.87 ug/L 09/04/19 09:32 108-67-82.9 0.87 1Vinyl chloride <0.17 ug/L 09/04/19 09:32 75-01-41.0 0.17 1m&p-Xylene <0.47 ug/L 09/04/19 09:32 179601-23-12.0 0.47 1o-Xylene 0.33J ug/L 09/04/19 09:32 95-47-61.0 0.26 1Surrogates4-Bromofluorobenzene (S) 88 % 09/04/19 09:32 460-00-470-130 1Dibromofluoromethane (S) 102 % 09/04/19 09:32 1868-53-770-130 1Toluene-d8 (S) 94 % 09/04/19 09:32 2037-26-570-130 1




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3-Chlorophenol <45.7 ug/L 09/09/19 19:44 108-43-008/30/19 07:10153 45.7 802,4-Dichlorophenol <44.2 ug/L 09/09/19 19:44 120-83-208/30/19 07:10146 44.2 803,4-Dichlorophenol <45.7 ug/L 09/09/19 19:44 95-77-208/30/19 07:10152 45.7 803,5-Dichlorophenol <57.1 ug/L 09/09/19 19:44 591-35-508/30/19 07:10190 57.1 80Pentachlorophenol 3830 ug/L 09/09/19 19:44 87-86-5 R408/30/19 07:1074.7 22.1 802,3,4,5-Tetrachlorophenol 73.8J ug/L 09/09/19 19:44 4901-51-3 R408/30/19 07:10139 41.9 802,3,4,6-Tetrachlorophenol 148J ug/L 09/09/19 19:44 58-90-208/30/19 07:10226 67.8 802,3,5-Trichlorophenol <45.0 ug/L 09/09/19 19:44 933-78-808/30/19 07:10149 45.0 802,3,6-Trichlorophenol <44.2 ug/L 09/09/19 19:44 933-75-508/30/19 07:10146 44.2 802,4,5-Trichlorophenol <35.0 ug/L 09/09/19 19:44 95-95-408/30/19 07:10116 35.0 802,4,6-Trichlorophenol <40.4 ug/L 09/09/19 19:44 88-06-208/30/19 07:10136 40.4 80SurrogatesPhenol-d6 (S) 0 % 09/09/19 19:44 13127-88-3 S408/30/19 07:1024-120 802,4,6-Tribromophenol (S) 0 % 09/09/19 19:44 118-79-6 S408/30/19 07:1043-140 80


Acenaphthene <57.6 ug/L 09/09/19 09:58 83-32-909/04/19 06:07377 57.6 80Acenaphthylene <55.1 ug/L 09/09/19 09:58 208-96-809/04/19 06:07377 55.1 80Anthracene <61.1 ug/L 09/09/19 09:58 120-12-709/04/19 06:07377 61.1 80Benzo(a)anthracene <63.9 ug/L 09/09/19 09:58 56-55-309/04/19 06:07377 63.9 80Benzo(a)pyrene <96.0 ug/L 09/09/19 09:58 50-32-809/04/19 06:07377 96.0 80Benzo(b)fluoranthene <78.1 ug/L 09/09/19 09:58 205-99-209/04/19 06:07377 78.1 80Benzo(g,h,i)perylene <104 ug/L 09/09/19 09:58 191-24-209/04/19 06:07377 104 80Benzo(k)fluoranthene <84.8 ug/L 09/09/19 09:58 207-08-909/04/19 06:07377 84.8 804-Bromophenylphenyl ether <72.1 ug/L 09/09/19 09:58 101-55-309/04/19 06:07377 72.1 80Butylbenzylphthalate <97.9 ug/L 09/09/19 09:58 85-68-709/04/19 06:07377 97.9 80Carbazole <68.9 ug/L 09/09/19 09:58 86-74-809/04/19 06:07377 68.9 804-Chloro-3-methylphenol <51.5 ug/L 09/09/19 09:58 59-50-709/04/19 06:07377 51.5 804-Chloroaniline <135 ug/L 09/09/19 09:58 106-47-809/04/19 06:07450 135 80bis(2-Chloroethoxy)methane <98.6 ug/L 09/09/19 09:58 111-91-109/04/19 06:07377 98.6 80bis(2-Chloroethyl) ether <88.1 ug/L 09/09/19 09:58 111-44-409/04/19 06:07377 88.1 802-Chloronaphthalene <62.6 ug/L 09/09/19 09:58 91-58-709/04/19 06:07377 62.6 802-Chlorophenol <62.5 ug/L 09/09/19 09:58 95-57-809/04/19 06:07377 62.5 804-Chlorophenylphenyl ether <62.5 ug/L 09/09/19 09:58 7005-72-309/04/19 06:07377 62.5 80Chrysene <95.8 ug/L 09/09/19 09:58 218-01-909/04/19 06:07377 95.8 80Dibenz(a,h)anthracene <83.4 ug/L 09/09/19 09:58 53-70-309/04/19 06:07377 83.4 80Dibenzofuran <64.0 ug/L 09/09/19 09:58 132-64-909/04/19 06:07377 64.0 801,2-Dichlorobenzene <109 ug/L 09/09/19 09:58 95-50-109/04/19 06:07377 109 801,3-Dichlorobenzene <117 ug/L 09/09/19 09:58 541-73-109/04/19 06:07389 117 801,4-Dichlorobenzene <109 ug/L 09/09/19 09:58 106-46-709/04/19 06:07377 109 803,3'-Dichlorobenzidine <101 ug/L 09/09/19 09:58 91-94-1 L109/04/19 06:07377 101 802,4-Dichlorophenol <67.7 ug/L 09/09/19 09:58 120-83-209/04/19 06:07377 67.7 80Diethylphthalate <58.5 ug/L 09/09/19 09:58 84-66-209/04/19 06:07377 58.5 802,4-Dimethylphenol <87.5 ug/L 09/09/19 09:58 105-67-909/04/19 06:07377 87.5 80Dimethylphthalate <54.4 ug/L 09/09/19 09:58 131-11-309/04/19 06:07377 54.4 80Di-n-butylphthalate <92.8 ug/L 09/09/19 09:58 84-74-209/04/19 06:07377 92.8 80




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ANALYTICAL RESULTS


401939560236105019 CP CS




4,6-Dinitro-2-methylphenol <235 ug/L 09/09/19 09:58 534-52-109/04/19 06:07785 235 802,4-Dinitrophenol <185 ug/L 09/09/19 09:58 51-28-509/04/19 06:07617 185 802,4-Dinitrotoluene <80.0 ug/L 09/09/19 09:58 121-14-209/04/19 06:07377 80.0 802,6-Dinitrotoluene <58.3 ug/L 09/09/19 09:58 606-20-2 R409/04/19 06:07377 58.3 80Di-n-octylphthalate <360 ug/L 09/09/19 09:58 117-84-009/04/19 06:071200 360 80bis(2-Ethylhexyl)phthalate <217 ug/L 09/09/19 09:58 117-81-709/04/19 06:07725 217 80Fluoranthene <74.6 ug/L 09/09/19 09:58 206-44-009/04/19 06:07377 74.6 80Fluorene <68.3 ug/L 09/09/19 09:58 86-73-709/04/19 06:07377 68.3 80Hexachloro-1,3-butadiene <86.6 ug/L 09/09/19 09:58 87-68-309/04/19 06:07416 86.6 80Hexachlorobenzene <125 ug/L 09/09/19 09:58 118-74-109/04/19 06:07377 125 80Hexachlorocyclopentadiene <76.1 ug/L 09/09/19 09:58 77-47-409/04/19 06:07377 76.1 80Hexachloroethane <107 ug/L 09/09/19 09:58 67-72-109/04/19 06:07377 107 80Indeno(1,2,3-cd)pyrene <91.8 ug/L 09/09/19 09:58 193-39-509/04/19 06:07377 91.8 80Isophorone <58.4 ug/L 09/09/19 09:58 78-59-109/04/19 06:07377 58.4 802-Methylnaphthalene <87.8 ug/L 09/09/19 09:58 91-57-609/04/19 06:07377 87.8 802-Methylphenol(o-Cresol) <70.3 ug/L 09/09/19 09:58 95-48-709/04/19 06:07377 70.3 803&4-Methylphenol(m&p Cresol) <46.2 ug/L 09/09/19 09:5809/04/19 06:07377 46.2 80Naphthalene <91.9 ug/L 09/09/19 09:58 91-20-309/04/19 06:07377 91.9 802-Nitroaniline <71.5 ug/L 09/09/19 09:58 88-74-4 R409/04/19 06:07377 71.5 803-Nitroaniline <103 ug/L 09/09/19 09:58 99-09-209/04/19 06:07377 103 804-Nitroaniline <226 ug/L 09/09/19 09:58 100-01-609/04/19 06:07754 226 80Nitrobenzene <81.1 ug/L 09/09/19 09:58 98-95-309/04/19 06:07377 81.1 802-Nitrophenol <62.3 ug/L 09/09/19 09:58 88-75-509/04/19 06:07377 62.3 804-Nitrophenol <231 ug/L 09/09/19 09:58 100-02-709/04/19 06:07770 231 80N-Nitroso-di-n-propylamine <85.6 ug/L 09/09/19 09:58 621-64-709/04/19 06:07377 85.6 80N-Nitrosodiphenylamine <260 ug/L 09/09/19 09:58 86-30-609/04/19 06:07868 260 802,2'-Oxybis(1-chloropropane) <93.1 ug/L 09/09/19 09:58 108-60-109/04/19 06:07377 93.1 80Pentachlorophenol 2380 ug/L 09/09/19 09:58 87-86-509/04/19 06:071150 344 80Phenanthrene <72.0 ug/L 09/09/19 09:58 85-01-809/04/19 06:07377 72.0 80Phenol <24.2 ug/L 09/09/19 09:58 108-95-209/04/19 06:07377 24.2 80Pyrene <90.6 ug/L 09/09/19 09:58 129-00-009/04/19 06:07377 90.6 801,2,4,5-Tetrachlorobenzene <75.4 ug/L 09/09/19 09:58 95-94-309/04/19 06:07377 75.4 801,2,4-Trichlorobenzene <119 ug/L 09/09/19 09:58 120-82-109/04/19 06:07395 119 802,4,5-Trichlorophenol <48.6 ug/L 09/09/19 09:58 95-95-409/04/19 06:07377 48.6 802,4,6-Trichlorophenol <60.2 ug/L 09/09/19 09:58 88-06-209/04/19 06:07377 60.2 80SurrogatesNitrobenzene-d5 (S) 0 % 09/09/19 09:58 4165-60-0 S409/04/19 06:0751-108 802-Fluorobiphenyl (S) 0 % 09/09/19 09:58 321-60-8 S409/04/19 06:0747-105 80Terphenyl-d14 (S) 0 % 09/09/19 09:58 1718-51-0 S409/04/19 06:0765-147 80Phenol-d6 (S) 0 % 09/09/19 09:58 13127-88-3 S409/04/19 06:0718-120 802-Fluorophenol (S) 0 % 09/09/19 09:58 367-12-4 S409/04/19 06:0732-120 802,4,6-Tribromophenol (S) 0 % 09/09/19 09:58 118-79-6 S409/04/19 06:0757-131 80


Acetone <2.7 ug/L 09/04/19 09:54 67-64-120.0 2.7 1Allyl chloride <0.60 ug/L 09/04/19 09:54 107-05-15.0 0.60 1




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ANALYTICAL RESULTS


401939560236105019 CP CS




Benzene <0.25 ug/L 09/04/19 09:54 71-43-21.0 0.25 1Bromobenzene <0.24 ug/L 09/04/19 09:54 108-86-11.0 0.24 1Bromochloromethane <0.36 ug/L 09/04/19 09:54 74-97-55.0 0.36 1Bromodichloromethane <0.36 ug/L 09/04/19 09:54 75-27-41.2 0.36 1Bromoform <4.0 ug/L 09/04/19 09:54 75-25-25.0 4.0 1Bromomethane <0.97 ug/L 09/04/19 09:54 74-83-95.0 0.97 12-Butanone (MEK) <2.9 ug/L 09/04/19 09:54 78-93-320.0 2.9 1n-Butylbenzene <0.71 ug/L 09/04/19 09:54 104-51-82.4 0.71 1sec-Butylbenzene <0.85 ug/L 09/04/19 09:54 135-98-85.0 0.85 1tert-Butylbenzene <0.30 ug/L 09/04/19 09:54 98-06-61.0 0.30 1Carbon tetrachloride <0.17 ug/L 09/04/19 09:54 56-23-51.0 0.17 1Chlorobenzene <0.71 ug/L 09/04/19 09:54 108-90-72.4 0.71 1Chloroethane <1.3 ug/L 09/04/19 09:54 75-00-35.0 1.3 1Chloroform <1.3 ug/L 09/04/19 09:54 67-66-35.0 1.3 1Chloromethane <2.2 ug/L 09/04/19 09:54 74-87-37.3 2.2 12-Chlorotoluene <0.93 ug/L 09/04/19 09:54 95-49-85.0 0.93 14-Chlorotoluene <0.76 ug/L 09/04/19 09:54 106-43-42.5 0.76 11,2-Dibromo-3-chloropropane <1.8 ug/L 09/04/19 09:54 96-12-85.9 1.8 1Dibromochloromethane <2.6 ug/L 09/04/19 09:54 124-48-15.0 2.6 11,2-Dibromoethane (EDB) <0.83 ug/L 09/04/19 09:54 106-93-42.8 0.83 1Dibromomethane <0.94 ug/L 09/04/19 09:54 74-95-33.1 0.94 11,2-Dichlorobenzene <0.71 ug/L 09/04/19 09:54 95-50-12.4 0.71 11,3-Dichlorobenzene <0.63 ug/L 09/04/19 09:54 541-73-12.1 0.63 11,4-Dichlorobenzene <0.94 ug/L 09/04/19 09:54 106-46-73.1 0.94 1Dichlorodifluoromethane <0.50 ug/L 09/04/19 09:54 75-71-85.0 0.50 11,1-Dichloroethane <0.27 ug/L 09/04/19 09:54 75-34-31.0 0.27 11,2-Dichloroethane <0.28 ug/L 09/04/19 09:54 107-06-21.0 0.28 11,1-Dichloroethene <0.24 ug/L 09/04/19 09:54 75-35-41.0 0.24 1cis-1,2-Dichloroethene <0.27 ug/L 09/04/19 09:54 156-59-21.0 0.27 1trans-1,2-Dichloroethene <1.1 ug/L 09/04/19 09:54 156-60-53.6 1.1 1Dichlorofluoromethane <1.4 ug/L 09/04/19 09:54 75-43-45.0 1.4 11,2-Dichloropropane <0.28 ug/L 09/04/19 09:54 78-87-51.0 0.28 11,3-Dichloropropane <0.83 ug/L 09/04/19 09:54 142-28-92.8 0.83 12,2-Dichloropropane <2.3 ug/L 09/04/19 09:54 594-20-77.6 2.3 11,1-Dichloropropene <0.54 ug/L 09/04/19 09:54 563-58-61.8 0.54 1cis-1,3-Dichloropropene <3.6 ug/L 09/04/19 09:54 10061-01-55.0 3.6 1trans-1,3-Dichloropropene <4.4 ug/L 09/04/19 09:54 10061-02-620.0 4.4 1Diethyl ether (Ethyl ether) <1.5 ug/L 09/04/19 09:54 60-29-75.1 1.5 1Ethylbenzene 0.33J ug/L 09/04/19 09:54 100-41-41.0 0.22 1Hexachloro-1,3-butadiene <1.2 ug/L 09/04/19 09:54 87-68-35.0 1.2 1Isopropylbenzene (Cumene) <0.39 ug/L 09/04/19 09:54 98-82-85.0 0.39 1p-Isopropyltoluene <0.80 ug/L 09/04/19 09:54 99-87-62.7 0.80 1Methylene Chloride <0.58 ug/L 09/04/19 09:54 75-09-25.0 0.58 14-Methyl-2-pentanone (MIBK) <1.5 ug/L 09/04/19 09:54 108-10-120.0 1.5 1Methyl-tert-butyl ether <1.2 ug/L 09/04/19 09:54 1634-04-44.2 1.2 1Naphthalene <1.2 ug/L 09/04/19 09:54 91-20-35.0 1.2 1




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ANALYTICAL RESULTS


401939560236105019 CP CS




n-Propylbenzene <0.81 ug/L 09/04/19 09:54 103-65-15.0 0.81 1Styrene <0.47 ug/L 09/04/19 09:54 100-42-51.6 0.47 11,1,1,2-Tetrachloroethane <0.27 ug/L 09/04/19 09:54 630-20-61.0 0.27 11,1,2,2-Tetrachloroethane <0.28 ug/L 09/04/19 09:54 79-34-51.0 0.28 1Tetrachloroethene <0.33 ug/L 09/04/19 09:54 127-18-41.1 0.33 1Toluene <0.17 ug/L 09/04/19 09:54 108-88-35.0 0.17 11,2,3-Trichlorobenzene <0.63 ug/L 09/04/19 09:54 87-61-65.0 0.63 11,2,4-Trichlorobenzene <0.95 ug/L 09/04/19 09:54 120-82-15.0 0.95 11,1,1-Trichloroethane <0.24 ug/L 09/04/19 09:54 71-55-61.0 0.24 11,1,2-Trichloroethane <0.55 ug/L 09/04/19 09:54 79-00-55.0 0.55 1Trichloroethene <0.26 ug/L 09/04/19 09:54 79-01-61.0 0.26 1Trichlorofluoromethane <0.21 ug/L 09/04/19 09:54 75-69-41.0 0.21 11,2,3-Trichloropropane <0.59 ug/L 09/04/19 09:54 96-18-45.0 0.59 11,1,2-Trichlorotrifluoroethane <0.54 ug/L 09/04/19 09:54 76-13-15.0 0.54 11,2,4-Trimethylbenzene <0.84 ug/L 09/04/19 09:54 95-63-62.8 0.84 11,3,5-Trimethylbenzene <0.87 ug/L 09/04/19 09:54 108-67-82.9 0.87 1Vinyl chloride <0.17 ug/L 09/04/19 09:54 75-01-41.0 0.17 1m&p-Xylene <0.47 ug/L 09/04/19 09:54 179601-23-12.0 0.47 1o-Xylene 1.1 ug/L 09/04/19 09:54 95-47-61.0 0.26 1Surrogates4-Bromofluorobenzene (S) 89 % 09/04/19 09:54 460-00-470-130 1Dibromofluoromethane (S) 98 % 09/04/19 09:54 1868-53-770-130 1Toluene-d8 (S) 95 % 09/04/19 09:54 2037-26-570-130 1




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ANALYTICAL RESULTS


401939560236105019 CP CS

Sample: CS IN BETWEEN Lab ID: 40193956004 Collected: 08/28/19 11:00 Received: 08/29/19 09:10 Matrix: Water



Pentachlorophenol 1.0 ug/L 09/09/19 18:55 87-86-5 R408/30/19 07:100.93 0.28 1SurrogatesPhenol-d6 (S) 26 % 09/09/19 18:55 13127-88-308/30/19 07:1024-120 12,4,6-Tribromophenol (S) 90 % 09/09/19 18:55 118-79-608/30/19 07:1043-140 1




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ANALYTICAL RESULTS


401939560236105019 CP CS

Sample: CS EFFLUENT Lab ID: 40193956005 Collected: 08/28/19 11:15 Received: 08/29/19 09:10 Matrix: Water



3-Chlorophenol <0.57 ug/L 09/09/19 18:31 108-43-008/30/19 07:101.9 0.57 12,4-Dichlorophenol <0.55 ug/L 09/09/19 18:31 120-83-208/30/19 07:101.8 0.55 13,4-Dichlorophenol <0.57 ug/L 09/09/19 18:31 95-77-208/30/19 07:101.9 0.57 13,5-Dichlorophenol <0.71 ug/L 09/09/19 18:31 591-35-508/30/19 07:102.3 0.71 1Pentachlorophenol <0.27 ug/L 09/09/19 18:31 87-86-5 R408/30/19 07:100.92 0.27 12,3,4,5-Tetrachlorophenol <0.52 ug/L 09/09/19 18:31 4901-51-3 R408/30/19 07:101.7 0.52 12,3,4,6-Tetrachlorophenol <0.84 ug/L 09/09/19 18:31 58-90-208/30/19 07:102.8 0.84 12,3,5-Trichlorophenol <0.56 ug/L 09/09/19 18:31 933-78-808/30/19 07:101.8 0.56 12,3,6-Trichlorophenol <0.55 ug/L 09/09/19 18:31 933-75-508/30/19 07:101.8 0.55 12,4,5-Trichlorophenol <0.43 ug/L 09/09/19 18:31 95-95-408/30/19 07:101.4 0.43 12,4,6-Trichlorophenol <0.50 ug/L 09/09/19 18:31 88-06-208/30/19 07:101.7 0.50 1SurrogatesPhenol-d6 (S) 25 % 09/09/19 18:31 13127-88-308/30/19 07:1024-120 12,4,6-Tribromophenol (S) 80 % 09/09/19 18:31 118-79-608/30/19 07:1043-140 1


4-Chloro-3-methylphenol <0.64 ug/L 09/09/19 10:19 59-50-709/04/19 06:074.7 0.64 12-Chlorophenol <0.78 ug/L 09/09/19 10:19 95-57-809/04/19 06:074.7 0.78 12,4-Dichlorophenol <0.85 ug/L 09/09/19 10:19 120-83-209/04/19 06:074.7 0.85 12,4-Dimethylphenol <1.1 ug/L 09/09/19 10:19 105-67-909/04/19 06:074.7 1.1 14,6-Dinitro-2-methylphenol <2.9 ug/L 09/09/19 10:19 534-52-109/04/19 06:079.8 2.9 12,4-Dinitrophenol <2.3 ug/L 09/09/19 10:19 51-28-509/04/19 06:077.7 2.3 12-Nitrophenol <0.78 ug/L 09/09/19 10:19 88-75-509/04/19 06:074.7 0.78 14-Nitrophenol <2.9 ug/L 09/09/19 10:19 100-02-709/04/19 06:079.6 2.9 1Pentachlorophenol <4.3 ug/L 09/09/19 10:19 87-86-509/04/19 06:0714.3 4.3 1Phenol <0.30 ug/L 09/09/19 10:19 108-95-209/04/19 06:074.7 0.30 12,4,5-Trichlorophenol <0.61 ug/L 09/09/19 10:19 95-95-409/04/19 06:074.7 0.61 12,4,6-Trichlorophenol <0.75 ug/L 09/09/19 10:19 88-06-209/04/19 06:074.7 0.75 1SurrogatesNitrobenzene-d5 (S) 72 % 09/09/19 10:19 4165-60-009/04/19 06:0751-108 12-Fluorobiphenyl (S) 75 % 09/09/19 10:19 321-60-809/04/19 06:0747-105 1Terphenyl-d14 (S) 87 % 09/09/19 10:19 1718-51-009/04/19 06:0765-147 1Phenol-d6 (S) 21 % 09/09/19 10:19 13127-88-309/04/19 06:0718-120 12-Fluorophenol (S) 30 % 09/09/19 10:19 367-12-4 S009/04/19 06:0732-120 12,4,6-Tribromophenol (S) 57 % 09/09/19 10:19 118-79-609/04/19 06:0757-131 1




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QUALITY CONTROL DATA


401939560236105019 CP CS

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

QC Batch:QC Batch Method:

Analysis Method:Analysis Description:

332334EPA 8260

EPA 82608260 MSV

Associated Lab Samples: 40193956001

Parameter UnitsBlankResult

ReportingLimit Qualifiers

METHOD BLANK: 1928509Associated Lab Samples: 40193956001

Matrix: Water

AnalyzedMDL

1,1,1,2-Tetrachloroethane ug/L <0.27 1.0 08/30/19 10:290.271,1,1-Trichloroethane ug/L <0.24 1.0 08/30/19 10:290.241,1,2,2-Tetrachloroethane ug/L <0.28 1.0 08/30/19 10:290.281,1,2-Trichloroethane ug/L <0.55 5.0 08/30/19 10:290.551,1,2-Trichlorotrifluoroethane ug/L <0.54 5.0 08/30/19 10:290.541,1-Dichloroethane ug/L <0.27 1.0 08/30/19 10:290.271,1-Dichloroethene ug/L <0.24 1.0 08/30/19 10:290.241,1-Dichloropropene ug/L <0.54 1.8 08/30/19 10:290.541,2,3-Trichlorobenzene ug/L <0.63 5.0 08/30/19 10:290.631,2,3-Trichloropropane ug/L <0.59 5.0 08/30/19 10:290.591,2,4-Trichlorobenzene ug/L <0.95 5.0 08/30/19 10:290.951,2,4-Trimethylbenzene ug/L <0.84 2.8 08/30/19 10:290.841,2-Dibromo-3-chloropropane ug/L <1.8 5.9 08/30/19 10:291.81,2-Dibromoethane (EDB) ug/L <0.83 2.8 08/30/19 10:290.831,2-Dichlorobenzene ug/L <0.71 2.4 08/30/19 10:290.711,2-Dichloroethane ug/L <0.28 1.0 08/30/19 10:290.281,2-Dichloropropane ug/L <0.28 1.0 08/30/19 10:290.281,3,5-Trimethylbenzene ug/L <0.87 2.9 08/30/19 10:290.871,3-Dichlorobenzene ug/L <0.63 2.1 08/30/19 10:290.631,3-Dichloropropane ug/L <0.83 2.8 08/30/19 10:290.831,4-Dichlorobenzene ug/L <0.94 3.1 08/30/19 10:290.942,2-Dichloropropane ug/L <2.3 7.6 08/30/19 10:292.32-Butanone (MEK) ug/L <2.9 20.0 08/30/19 10:292.92-Chlorotoluene ug/L <0.93 5.0 08/30/19 10:290.934-Chlorotoluene ug/L <0.76 2.5 08/30/19 10:290.764-Methyl-2-pentanone (MIBK) ug/L <1.5 5.1 08/30/19 10:291.5Acetone ug/L <2.7 20.0 08/30/19 10:292.7Allyl chloride ug/L <0.60 5.0 08/30/19 10:290.60Benzene ug/L <0.25 1.0 08/30/19 10:290.25Bromobenzene ug/L <0.24 1.0 08/30/19 10:290.24Bromochloromethane ug/L <0.36 5.0 08/30/19 10:290.36Bromodichloromethane ug/L <0.36 1.2 08/30/19 10:290.36Bromoform ug/L <4.0 13.2 08/30/19 10:294.0Bromomethane ug/L <0.97 5.0 08/30/19 10:290.97Carbon tetrachloride ug/L <0.17 1.0 08/30/19 10:290.17Chlorobenzene ug/L <0.71 2.4 08/30/19 10:290.71Chloroethane ug/L <1.3 5.0 08/30/19 10:291.3Chloroform ug/L <1.3 5.0 08/30/19 10:291.3Chloromethane ug/L <2.2 7.3 08/30/19 10:292.2cis-1,2-Dichloroethene ug/L <0.27 1.0 08/30/19 10:290.27cis-1,3-Dichloropropene ug/L <3.6 12.1 08/30/19 10:293.6




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401939560236105019 CP CS




METHOD BLANK: 1928509Associated Lab Samples: 40193956001

Matrix: Water

AnalyzedMDL

Dibromochloromethane ug/L <2.6 8.7 08/30/19 10:292.6Dibromomethane ug/L <0.94 3.1 08/30/19 10:290.94Dichlorodifluoromethane ug/L <0.50 5.0 08/30/19 10:290.50Dichlorofluoromethane ug/L <1.4 5.0 08/30/19 10:291.4Diethyl ether (Ethyl ether) ug/L <1.5 5.1 08/30/19 10:291.5Ethylbenzene ug/L <0.22 1.0 08/30/19 10:290.22Hexachloro-1,3-butadiene ug/L <1.2 5.0 08/30/19 10:291.2Isopropylbenzene (Cumene) ug/L <0.39 5.0 08/30/19 10:290.39m&p-Xylene ug/L <0.47 2.0 08/30/19 10:290.47Methyl-tert-butyl ether ug/L <1.2 4.2 08/30/19 10:291.2Methylene Chloride ug/L <0.58 5.0 08/30/19 10:290.58n-Butylbenzene ug/L <0.71 2.4 08/30/19 10:290.71n-Propylbenzene ug/L <0.81 5.0 08/30/19 10:290.81Naphthalene ug/L <1.2 5.0 08/30/19 10:291.2o-Xylene ug/L <0.26 1.0 08/30/19 10:290.26p-Isopropyltoluene ug/L <0.80 2.7 08/30/19 10:290.80sec-Butylbenzene ug/L <0.85 5.0 08/30/19 10:290.85Styrene ug/L <0.47 1.6 08/30/19 10:290.47tert-Butylbenzene ug/L <0.30 1.0 08/30/19 10:290.30Tetrachloroethene ug/L <0.33 1.1 08/30/19 10:290.33Toluene ug/L <0.17 5.0 08/30/19 10:290.17trans-1,2-Dichloroethene ug/L <1.1 3.6 08/30/19 10:291.1trans-1,3-Dichloropropene ug/L <4.4 14.6 08/30/19 10:294.4Trichloroethene ug/L <0.26 1.0 08/30/19 10:290.26Trichlorofluoromethane ug/L <0.21 1.0 08/30/19 10:290.21Vinyl chloride ug/L <0.17 1.0 08/30/19 10:290.174-Bromofluorobenzene (S) % 81 70-130 08/30/19 10:29Dibromofluoromethane (S) % 115 70-130 08/30/19 10:29Toluene-d8 (S) % 95 70-130 08/30/19 10:29

Parameter UnitsLCS

Result% RecLimits Qualifiers% RecConc.

1928510LABORATORY CONTROL SAMPLE:LCSSpike

1,1,1-Trichloroethane ug/L 51.250 102 70-1301,1,2,2-Tetrachloroethane ug/L 47.450 95 70-1301,1,2-Trichloroethane ug/L 57.550 115 70-1301,1,2-Trichlorotrifluoroethane ug/L 54.450 109 50-1501,1-Dichloroethane ug/L 47.250 94 73-1501,1-Dichloroethene ug/L 47.150 94 73-1381,2,4-Trichlorobenzene ug/L 44.750 89 70-1301,2-Dibromo-3-chloropropane ug/L 34.750 69 64-1291,2-Dibromoethane (EDB) ug/L 51.750 103 70-1301,2-Dichlorobenzene ug/L 49.750 99 70-1301,2-Dichloroethane ug/L 52.250 104 75-140




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401939560236105019 CP CS


Parameter UnitsLCS



1,2-Dichloropropane ug/L 62.750 125 73-1351,3-Dichlorobenzene ug/L 48.450 97 70-1301,4-Dichlorobenzene ug/L 53.050 106 70-130Benzene ug/L 53.550 107 70-130Bromodichloromethane ug/L 57.450 115 70-130Bromoform ug/L 47.650 95 68-129Bromomethane ug/L 38.050 76 18-159Carbon tetrachloride ug/L 53.550 107 70-130Chlorobenzene ug/L 58.550 117 70-130Chloroethane ug/L 41.050 82 53-147Chloroform ug/L 51.950 104 74-136Chloromethane ug/L 34.450 69 29-115cis-1,2-Dichloroethene ug/L 56.350 113 70-130cis-1,3-Dichloropropene ug/L 45.850 92 70-130Dibromochloromethane ug/L 53.350 107 70-130Dichlorodifluoromethane ug/L 30.850 62 10-130Ethylbenzene ug/L 56.850 114 80-124Isopropylbenzene (Cumene) ug/L 57.250 114 70-130m&p-Xylene ug/L 120100 120 70-130Methyl-tert-butyl ether ug/L 39.350 79 54-137Methylene Chloride ug/L 47.550 95 73-138o-Xylene ug/L 55.550 111 70-130Styrene ug/L 60.250 120 70-130Tetrachloroethene ug/L 60.950 122 70-130Toluene ug/L 58.450 117 80-126trans-1,2-Dichloroethene ug/L 47.050 94 73-145trans-1,3-Dichloropropene ug/L 42.050 84 70-130Trichloroethene ug/L 57.850 116 70-130Trichlorofluoromethane ug/L 54.350 109 76-147Vinyl chloride ug/L 39.550 79 51-1204-Bromofluorobenzene (S) % 102 70-130Dibromofluoromethane (S) % 101 70-130Toluene-d8 (S) % 98 70-130

Parameter UnitsMS

Result% RecLimits Qual% RecConc.

1928511MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpikeResult

40193934008

1928512

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1,1-Trichloroethane ug/L 50 105 70-130107 1 2050<0.24 52.7 53.31,1,2,2-Tetrachloroethane ug/L 50 98 70-13094 4 2050<0.28 49.2 47.21,1,2-Trichloroethane ug/L 50 116 70-137112 3 2050<0.55 57.8 56.01,1,2-Trichlorotrifluoroethane

ug/L 50 113 50-150114 1 2050<0.54 56.5 56.8

1,1-Dichloroethane ug/L 50 97 73-15397 0 2050<0.27 48.7 48.61,1-Dichloroethene ug/L 50 100 73-138101 1 2050<0.24 49.9 50.5




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401939560236105019 CP CS


Parameter UnitsMS



MSSpikeResult

40193934008

1928512

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4-Trichlorobenzene ug/L 50 96 70-13095 1 2050<0.95 48.3 47.71,2-Dibromo-3-chloropropane

ug/L 50 75 58-12970 7 2050<1.8 37.3 34.8

1,2-Dibromoethane (EDB) ug/L 50 105 70-130102 3 2050<0.83 52.4 51.01,2-Dichlorobenzene ug/L 50 100 70-130100 0 2050<0.71 50.1 50.01,2-Dichloroethane ug/L 50 107 75-140106 1 2050<0.28 53.5 52.91,2-Dichloropropane ug/L 50 125 71-138124 0 2050<0.28 62.4 62.11,3-Dichlorobenzene ug/L 50 98 70-13099 0 2050<0.63 49.2 49.31,4-Dichlorobenzene ug/L 50 106 70-130106 0 2050<0.94 53.2 53.1Benzene ug/L 50 110 70-130114 3 205010.7 65.9 67.6Bromodichloromethane ug/L 50 113 70-130112 1 2050<0.36 56.3 55.9Bromoform ug/L 50 96 68-12992 4 2050<4.0 47.9 45.9Bromomethane ug/L 50 85 15-17094 10 2050<0.97 42.4 46.8Carbon tetrachloride ug/L 50 111 70-130111 0 2050<0.17 55.4 55.6Chlorobenzene ug/L 50 118 70-130116 1 2050<0.71 58.9 58.2Chloroethane ug/L 50 90 51-14893 3 2050<1.3 44.8 46.4Chloroform ug/L 50 106 74-136107 1 2050<1.3 53.2 53.6Chloromethane ug/L 50 78 23-11580 3 2050<2.2 38.9 40.0cis-1,2-Dichloroethene ug/L 50 117 70-131118 1 2050<0.27 58.3 59.0cis-1,3-Dichloropropene ug/L 50 94 70-13093 1 2050<3.6 46.8 46.5Dibromochloromethane ug/L 50 107 70-130104 3 2050<2.6 53.7 52.2Dichlorodifluoromethane ug/L 50 75 10-13275 1 2050<0.50 37.6 37.4Ethylbenzene ug/L 50 115 80-125114 1 2050<0.22 57.5 56.9Isopropylbenzene(Cumene)

ug/L 50 117 70-130116 1 2050<0.39 58.7 58.2

m&p-Xylene ug/L 100 121 70-130119 2 20100<0.47 121 119Methyl-tert-butyl ether ug/L 50 82 51-14581 1 2050<1.2 41.0 40.5Methylene Chloride ug/L 50 98 73-14099 1 2050<0.58 49.0 49.7o-Xylene ug/L 50 112 70-130111 1 2050<0.26 56.1 55.6Styrene ug/L 50 120 70-130119 1 2050<0.47 60.0 59.4Tetrachloroethene ug/L 50 123 70-130123 1 2050<0.33 61.7 61.3Toluene ug/L 50 118 80-131117 1 2050<0.17 59.1 58.5trans-1,2-Dichloroethene ug/L 50 98 73-14899 1 2050<1.1 49.0 49.5trans-1,3-Dichloropropene ug/L 50 87 70-13086 1 2050<4.4 43.5 43.0Trichloroethene ug/L 50 115 70-130116 1 2050<0.26 57.7 58.0Trichlorofluoromethane ug/L 50 114 74-147115 0 2050<0.21 57.2 57.3Vinyl chloride ug/L 50 89 41-12989 0 2050<0.17 44.5 44.54-Bromofluorobenzene (S) % 103 70-130101Dibromofluoromethane (S) % 102 70-130102Toluene-d8 (S) % 99 70-13098




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401939560236105019 CP CS




332563EPA 8260

EPA 82608260 MSV

Associated Lab Samples: 40193956002, 40193956003



METHOD BLANK: 1930140Associated Lab Samples: 40193956002, 40193956003

Matrix: Water

AnalyzedMDL

1,1,1,2-Tetrachloroethane ug/L <0.27 1.0 09/04/19 06:540.271,1,1-Trichloroethane ug/L <0.24 1.0 09/04/19 06:540.241,1,2,2-Tetrachloroethane ug/L <0.28 1.0 09/04/19 06:540.281,1,2-Trichloroethane ug/L <0.55 5.0 09/04/19 06:540.551,1,2-Trichlorotrifluoroethane ug/L <0.54 5.0 09/04/19 06:540.541,1-Dichloroethane ug/L <0.27 1.0 09/04/19 06:540.271,1-Dichloroethene ug/L <0.24 1.0 09/04/19 06:540.241,1-Dichloropropene ug/L <0.54 1.8 09/04/19 06:540.541,2,3-Trichlorobenzene ug/L <0.63 5.0 09/04/19 06:540.631,2,3-Trichloropropane ug/L <0.59 5.0 09/04/19 06:540.591,2,4-Trichlorobenzene ug/L <0.95 5.0 09/04/19 06:540.951,2,4-Trimethylbenzene ug/L <0.84 2.8 09/04/19 06:540.841,2-Dibromo-3-chloropropane ug/L <1.8 5.9 09/04/19 06:541.81,2-Dibromoethane (EDB) ug/L <0.83 2.8 09/04/19 06:540.831,2-Dichlorobenzene ug/L <0.71 2.4 09/04/19 06:540.711,2-Dichloroethane ug/L <0.28 1.0 09/04/19 06:540.281,2-Dichloropropane ug/L <0.28 1.0 09/04/19 06:540.281,3,5-Trimethylbenzene ug/L <0.87 2.9 09/04/19 06:540.871,3-Dichlorobenzene ug/L <0.63 2.1 09/04/19 06:540.631,3-Dichloropropane ug/L <0.83 2.8 09/04/19 06:540.831,4-Dichlorobenzene ug/L <0.94 3.1 09/04/19 06:540.942,2-Dichloropropane ug/L <2.3 7.6 09/04/19 06:542.32-Butanone (MEK) ug/L <2.9 20.0 09/04/19 06:542.92-Chlorotoluene ug/L <0.93 5.0 09/04/19 06:540.934-Chlorotoluene ug/L <0.76 2.5 09/04/19 06:540.764-Methyl-2-pentanone (MIBK) ug/L <1.5 5.1 09/04/19 06:541.5Acetone ug/L <2.7 20.0 09/04/19 06:542.7Allyl chloride ug/L <0.60 5.0 09/04/19 06:540.60Benzene ug/L <0.25 1.0 09/04/19 06:540.25Bromobenzene ug/L <0.24 1.0 09/04/19 06:540.24Bromochloromethane ug/L <0.36 5.0 09/04/19 06:540.36Bromodichloromethane ug/L <0.36 1.2 09/04/19 06:540.36Bromoform ug/L <4.0 13.2 09/04/19 06:544.0Bromomethane ug/L <0.97 5.0 09/04/19 06:540.97Carbon tetrachloride ug/L <0.17 1.0 09/04/19 06:540.17Chlorobenzene ug/L <0.71 2.4 09/04/19 06:540.71Chloroethane ug/L <1.3 5.0 09/04/19 06:541.3Chloroform ug/L <1.3 5.0 09/04/19 06:541.3Chloromethane ug/L <2.2 7.3 09/04/19 06:542.2cis-1,2-Dichloroethene ug/L <0.27 1.0 09/04/19 06:540.27cis-1,3-Dichloropropene ug/L <3.6 12.1 09/04/19 06:543.6




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METHOD BLANK: 1930140Associated Lab Samples: 40193956002, 40193956003

Matrix: Water

AnalyzedMDL

Dibromochloromethane ug/L <2.6 8.7 09/04/19 06:542.6Dibromomethane ug/L <0.94 3.1 09/04/19 06:540.94Dichlorodifluoromethane ug/L <0.50 5.0 09/04/19 06:540.50Dichlorofluoromethane ug/L <1.4 5.0 09/04/19 06:541.4Diethyl ether (Ethyl ether) ug/L <1.5 5.1 09/04/19 06:541.5Ethylbenzene ug/L <0.22 1.0 09/04/19 06:540.22Hexachloro-1,3-butadiene ug/L <1.2 5.0 09/04/19 06:541.2Isopropylbenzene (Cumene) ug/L <0.39 5.0 09/04/19 06:540.39m&p-Xylene ug/L <0.47 2.0 09/04/19 06:540.47Methyl-tert-butyl ether ug/L <1.2 4.2 09/04/19 06:541.2Methylene Chloride ug/L <0.58 5.0 09/04/19 06:540.58n-Butylbenzene ug/L <0.71 2.4 09/04/19 06:540.71n-Propylbenzene ug/L <0.81 5.0 09/04/19 06:540.81Naphthalene ug/L <1.2 5.0 09/04/19 06:541.2o-Xylene ug/L <0.26 1.0 09/04/19 06:540.26p-Isopropyltoluene ug/L <0.80 2.7 09/04/19 06:540.80sec-Butylbenzene ug/L <0.85 5.0 09/04/19 06:540.85Styrene ug/L <0.47 1.6 09/04/19 06:540.47tert-Butylbenzene ug/L <0.30 1.0 09/04/19 06:540.30Tetrachloroethene ug/L <0.33 1.1 09/04/19 06:540.33Toluene ug/L <0.17 5.0 09/04/19 06:540.17trans-1,2-Dichloroethene ug/L <1.1 3.6 09/04/19 06:541.1trans-1,3-Dichloropropene ug/L <4.4 14.6 09/04/19 06:544.4Trichloroethene ug/L <0.26 1.0 09/04/19 06:540.26Trichlorofluoromethane ug/L <0.21 1.0 09/04/19 06:540.21Vinyl chloride ug/L <0.17 1.0 09/04/19 06:540.174-Bromofluorobenzene (S) % 87 70-130 09/04/19 06:54Dibromofluoromethane (S) % 93 70-130 09/04/19 06:54Toluene-d8 (S) % 96 70-130 09/04/19 06:54

Parameter UnitsLCS



1,1,1-Trichloroethane ug/L 50.750 101 70-1301,1,2,2-Tetrachloroethane ug/L 48.950 98 70-1301,1,2-Trichloroethane ug/L 53.950 108 70-1301,1,2-Trichlorotrifluoroethane ug/L 51.550 103 50-1501,1-Dichloroethane ug/L 50.950 102 73-1501,1-Dichloroethene ug/L 53.050 106 73-1381,2,4-Trichlorobenzene ug/L 49.450 99 70-1301,2-Dibromo-3-chloropropane ug/L 43.250 86 64-1291,2-Dibromoethane (EDB) ug/L 52.050 104 70-1301,2-Dichlorobenzene ug/L 51.950 104 70-1301,2-Dichloroethane ug/L 43.950 88 75-140




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401939560236105019 CP CS


Parameter UnitsLCS



1,2-Dichloropropane ug/L 52.850 106 73-1351,3-Dichlorobenzene ug/L 49.650 99 70-1301,4-Dichlorobenzene ug/L 50.150 100 70-130Benzene ug/L 49.550 99 70-130Bromodichloromethane ug/L 49.050 98 70-130Bromoform ug/L 52.150 104 68-129Bromomethane ug/L 42.950 86 18-159Carbon tetrachloride ug/L 48.650 97 70-130Chlorobenzene ug/L 52.050 104 70-130Chloroethane ug/L 44.250 88 53-147Chloroform ug/L 46.650 93 74-136Chloromethane ug/L 40.450 81 29-115cis-1,2-Dichloroethene ug/L 48.350 97 70-130cis-1,3-Dichloropropene ug/L 49.350 99 70-130Dibromochloromethane ug/L 48.050 96 70-130Dichlorodifluoromethane ug/L 27.850 56 10-130Ethylbenzene ug/L 51.450 103 80-124Isopropylbenzene (Cumene) ug/L 53.750 107 70-130m&p-Xylene ug/L 112100 112 70-130Methyl-tert-butyl ether ug/L 42.850 86 54-137Methylene Chloride ug/L 50.250 100 73-138o-Xylene ug/L 53.650 107 70-130Styrene ug/L 54.550 109 70-130Tetrachloroethene ug/L 54.450 109 70-130Toluene ug/L 52.450 105 80-126trans-1,2-Dichloroethene ug/L 54.150 108 73-145trans-1,3-Dichloropropene ug/L 50.250 100 70-130Trichloroethene ug/L 51.650 103 70-130Trichlorofluoromethane ug/L 45.050 90 76-147Vinyl chloride ug/L 41.350 83 51-1204-Bromofluorobenzene (S) % 99 70-130Dibromofluoromethane (S) % 87 70-130Toluene-d8 (S) % 99 70-130

Parameter UnitsMS



MSSpikeResult

40193956002

1930143

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1,1-Trichloroethane ug/L 50 109 70-130104 5 2050<0.24 54.4 51.81,1,2,2-Tetrachloroethane ug/L 50 109 70-130110 1 2050<0.28 54.6 55.11,1,2-Trichloroethane ug/L 50 108 70-137109 1 2050<0.55 53.9 54.41,1,2-Trichlorotrifluoroethane

ug/L 50 103 50-150105 2 2050<0.54 51.3 52.4

1,1-Dichloroethane ug/L 50 106 73-153111 5 2050<0.27 53.0 55.61,1-Dichloroethene ug/L 50 111 73-138119 7 2050<0.24 55.3 59.4




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401939560236105019 CP CS


Parameter UnitsMS



MSSpikeResult

40193956002

1930143

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4-Trichlorobenzene ug/L 50 112 70-130116 4 2050<0.95 55.8 58.21,2-Dibromo-3-chloropropane

ug/L 50 97 58-12992 6 2050<1.8 48.6 46.0

1,2-Dibromoethane (EDB) ug/L 50 107 70-130108 1 2050<0.83 53.7 54.21,2-Dichlorobenzene ug/L 50 112 70-130114 2 2050<0.71 56.1 57.21,2-Dichloroethane ug/L 50 91 75-14093 2 20500.38J 46.0 47.01,2-Dichloropropane ug/L 50 113 71-138116 2 2050<0.28 56.6 58.01,3-Dichlorobenzene ug/L 50 102 70-130106 4 2050<0.63 50.8 52.81,4-Dichlorobenzene ug/L 50 107 70-130112 4 2050<0.94 53.6 55.8Benzene ug/L 50 102 70-130108 5 2050<0.25 51.1 53.9Bromodichloromethane ug/L 50 101 70-130108 6 2050<0.36 50.7 53.8Bromoform ug/L 50 114 68-129109 4 2050<4.0 56.8 54.4Bromomethane ug/L 50 87 15-17091 4 2050<0.97 43.5 45.3Carbon tetrachloride ug/L 50 106 70-130108 2 2050<0.17 53.1 53.9Chlorobenzene ug/L 50 111 70-130108 2 2050<0.71 55.4 54.2Chloroethane ug/L 50 94 51-14895 0 2050<1.3 47.2 47.3Chloroform ug/L 50 91 74-13696 5 2050<1.3 45.5 47.9Chloromethane ug/L 50 83 23-11580 4 2050<2.2 42.1 40.4cis-1,2-Dichloroethene ug/L 50 99 70-131105 6 2050<0.27 49.7 52.7cis-1,3-Dichloropropene ug/L 50 101 70-130102 1 2050<3.6 50.5 51.2Dibromochloromethane ug/L 50 103 70-130103 0 2050<2.6 51.7 51.7Dichlorodifluoromethane ug/L 50 52 10-13254 2 2050<0.50 26.2 26.8Ethylbenzene ug/L 50 108 80-125110 2 2050<0.22 53.9 55.2Isopropylbenzene(Cumene)

ug/L 50 111 70-130112 1 2050<0.39 55.5 55.9

m&p-Xylene ug/L 100 115 70-130116 1 20100<0.47 115 116Methyl-tert-butyl ether ug/L 50 95 51-14590 5 2050<1.2 47.4 45.2Methylene Chloride ug/L 50 106 73-140107 1 2050<0.58 53.0 53.7o-Xylene ug/L 50 110 70-130113 3 20500.33J 55.2 56.7Styrene ug/L 50 111 70-130116 5 2050<0.47 55.4 58.2Tetrachloroethene ug/L 50 118 70-130116 2 2050<0.33 59.0 58.0Toluene ug/L 50 110 80-131112 2 2050<0.17 54.8 56.1trans-1,2-Dichloroethene ug/L 50 118 73-148116 2 2050<1.1 59.1 58.2trans-1,3-Dichloropropene ug/L 50 102 70-130104 2 2050<4.4 51.0 51.9Trichloroethene ug/L 50 110 70-130112 1 2050<0.26 55.1 55.9Trichlorofluoromethane ug/L 50 93 74-14797 4 2050<0.21 46.7 48.5Vinyl chloride ug/L 50 87 41-12987 1 2050<0.17 43.3 43.64-Bromofluorobenzene (S) % 98 70-13099Dibromofluoromethane (S) % 94 70-13087Toluene-d8 (S) % 102 70-13099




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401939560236105019 CP CS




332330EPA 3510

EPA 82708270 MSSV Phenols

Associated Lab Samples: 40193956002, 40193956003, 40193956004, 40193956005



METHOD BLANK: 1928496Associated Lab Samples: 40193956002, 40193956003, 40193956004, 40193956005

Matrix: Water

AnalyzedMDL

2,3,4,5-Tetrachlorophenol ug/L <0.55 1.8 08/30/19 09:570.552,3,4,6-Tetrachlorophenol ug/L <0.89 3.0 08/30/19 09:570.892,3,5-Trichlorophenol ug/L <0.59 2.0 08/30/19 09:570.592,3,6-Trichlorophenol ug/L <0.58 1.9 08/30/19 09:570.582,4,5-Trichlorophenol ug/L <0.46 1.5 08/30/19 09:570.462,4,6-Trichlorophenol ug/L <0.53 1.8 08/30/19 09:570.532,4-Dichlorophenol ug/L <0.58 1.9 08/30/19 09:570.583,4-Dichlorophenol ug/L <0.60 2.0 08/30/19 09:570.603,5-Dichlorophenol ug/L <0.75 2.5 08/30/19 09:570.753-Chlorophenol ug/L <0.60 2.0 08/30/19 09:570.60Pentachlorophenol ug/L <0.29 0.98 08/30/19 09:570.292,4,6-Tribromophenol (S) % 77 43-140 08/30/19 09:57Phenol-d6 (S) % 32 24-120 08/30/19 09:57

Parameter UnitsLCS



2,3,4,5-Tetrachlorophenol ug/L 44.750 89 48-1502,3,4,6-Tetrachlorophenol ug/L 49.050 98 50-1502,3,5-Trichlorophenol ug/L 43.850 88 50-1202,3,6-Trichlorophenol ug/L 48.850 98 50-1342,4,5-Trichlorophenol ug/L 48.150 96 50-1362,4,6-Trichlorophenol ug/L 46.050 92 50-1282,4-Dichlorophenol ug/L 46.050 92 60-1153,4-Dichlorophenol ug/L 42.250 84 43-1173,5-Dichlorophenol ug/L 46.650 93 47-1173-Chlorophenol ug/L 34.650 69 47-101Pentachlorophenol ug/L 38.250 76 50-1502,4,6-Tribromophenol (S) % 89 43-140Phenol-d6 (S) % 30 24-120

Parameter UnitsMS



MSSpikeResult

40193892001

1928499

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Pentachlorophenol ug/L 48.5 95 10-20079 19 3048.1<0.28 46.1 38.12,4,6-Tribromophenol (S) % 108 43-14085




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401939560236105019 CP CS




332672EPA 3510

EPA 82708270 Water MSSV

Associated Lab Samples: 40193956002, 40193956003, 40193956005



METHOD BLANK: 1930596Associated Lab Samples: 40193956002, 40193956003, 40193956005

Matrix: Water

AnalyzedMDL

1,2,4,5-Tetrachlorobenzene ug/L <1.0 5.0 09/05/19 08:471.01,2,4-Trichlorobenzene ug/L <1.6 5.2 09/05/19 08:471.61,2-Dichlorobenzene ug/L <1.4 5.0 09/05/19 08:471.41,3-Dichlorobenzene ug/L <1.5 5.2 09/05/19 08:471.51,4-Dichlorobenzene ug/L <1.4 5.0 09/05/19 08:471.42,2'-Oxybis(1-chloropropane) ug/L <1.2 5.0 09/05/19 08:471.22,4,5-Trichlorophenol ug/L <0.64 5.0 09/05/19 08:470.642,4,6-Trichlorophenol ug/L <0.80 5.0 09/05/19 08:470.802,4-Dichlorophenol ug/L <0.90 5.0 09/05/19 08:470.902,4-Dimethylphenol ug/L <1.2 5.0 09/05/19 08:471.22,4-Dinitrophenol ug/L <2.5 8.2 09/05/19 08:472.52,4-Dinitrotoluene ug/L <1.1 5.0 09/05/19 08:471.12,6-Dinitrotoluene ug/L <0.77 5.0 09/05/19 08:470.772-Chloronaphthalene ug/L <0.83 5.0 09/05/19 08:470.832-Chlorophenol ug/L <0.83 5.0 09/05/19 08:470.832-Methylnaphthalene ug/L <1.2 5.0 09/05/19 08:471.22-Methylphenol(o-Cresol) ug/L <0.93 5.0 09/05/19 08:470.932-Nitroaniline ug/L <0.95 5.0 09/05/19 08:470.952-Nitrophenol ug/L <0.83 5.0 09/05/19 08:470.833&4-Methylphenol(m&p Cresol) ug/L <0.61 5.0 09/05/19 08:470.613,3'-Dichlorobenzidine ug/L <1.3 5.0 09/05/19 08:471.33-Nitroaniline ug/L <1.4 5.0 09/05/19 08:471.44,6-Dinitro-2-methylphenol ug/L <3.1 10.4 09/05/19 08:473.14-Bromophenylphenyl ether ug/L <0.96 5.0 09/05/19 08:470.964-Chloro-3-methylphenol ug/L <0.68 5.0 09/05/19 08:470.684-Chloroaniline ug/L <1.8 6.0 09/05/19 08:471.84-Chlorophenylphenyl ether ug/L <0.83 5.0 09/05/19 08:470.834-Nitroaniline ug/L <3.0 10 09/05/19 08:473.04-Nitrophenol ug/L <3.1 10.2 09/05/19 08:473.1Acenaphthene ug/L <0.76 5.0 09/05/19 08:470.76Acenaphthylene ug/L <0.73 5.0 09/05/19 08:470.73Anthracene ug/L <0.81 5.0 09/05/19 08:470.81Benzo(a)anthracene ug/L <0.85 5.0 09/05/19 08:470.85Benzo(a)pyrene ug/L <1.3 5.0 09/05/19 08:471.3Benzo(b)fluoranthene ug/L <1.0 5.0 09/05/19 08:471.0Benzo(g,h,i)perylene ug/L <1.4 5.0 09/05/19 08:471.4Benzo(k)fluoranthene ug/L <1.1 5.0 09/05/19 08:471.1bis(2-Chloroethoxy)methane ug/L <1.3 5.0 09/05/19 08:471.3bis(2-Chloroethyl) ether ug/L <1.2 5.0 09/05/19 08:471.2bis(2-Ethylhexyl)phthalate ug/L <2.9 9.6 09/05/19 08:472.9Butylbenzylphthalate ug/L <1.3 5.0 09/05/19 08:471.3




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401939560236105019 CP CS




METHOD BLANK: 1930596Associated Lab Samples: 40193956002, 40193956003, 40193956005

Matrix: Water

AnalyzedMDL

Carbazole ug/L <0.91 5.0 09/05/19 08:470.91Chrysene ug/L <1.3 5.0 09/05/19 08:471.3Di-n-butylphthalate ug/L <1.2 5.0 09/05/19 08:471.2Di-n-octylphthalate ug/L <4.8 15.9 09/05/19 08:474.8Dibenz(a,h)anthracene ug/L <1.1 5.0 09/05/19 08:471.1Dibenzofuran ug/L <0.85 5.0 09/05/19 08:470.85Diethylphthalate ug/L <0.78 5.0 09/05/19 08:470.78Dimethylphthalate ug/L <0.72 5.0 09/05/19 08:470.72Fluoranthene ug/L <0.99 5.0 09/05/19 08:470.99Fluorene ug/L <0.91 5.0 09/05/19 08:470.91Hexachloro-1,3-butadiene ug/L <1.1 5.5 09/05/19 08:471.1Hexachlorobenzene ug/L <1.7 5.0 09/05/19 08:471.7Hexachlorocyclopentadiene ug/L <1.0 5.0 09/05/19 08:471.0Hexachloroethane ug/L <1.4 5.0 09/05/19 08:471.4Indeno(1,2,3-cd)pyrene ug/L <1.2 5.0 09/05/19 08:471.2Isophorone ug/L <0.77 5.0 09/05/19 08:470.77N-Nitroso-di-n-propylamine ug/L <1.1 5.0 09/05/19 08:471.1N-Nitrosodiphenylamine ug/L <3.4 11.5 09/05/19 08:473.4Naphthalene ug/L <1.2 5.0 09/05/19 08:471.2Nitrobenzene ug/L <1.1 5.0 09/05/19 08:471.1Pentachlorophenol ug/L <4.6 15.2 09/05/19 08:474.6Phenanthrene ug/L <0.95 5.0 09/05/19 08:470.95Phenol ug/L <0.32 5.0 09/05/19 08:470.32Pyrene ug/L <1.2 5.0 09/05/19 08:471.22,4,6-Tribromophenol (S) % 99 57-131 09/05/19 08:472-Fluorobiphenyl (S) % 71 47-105 09/05/19 08:472-Fluorophenol (S) % 48 32-120 09/05/19 08:47Nitrobenzene-d5 (S) % 71 51-108 09/05/19 08:47Phenol-d6 (S) % 27 18-120 09/05/19 08:47Terphenyl-d14 (S) % 95 65-147 09/05/19 08:47

Parameter UnitsLCS



1,2,4-Trichlorobenzene ug/L 41.650 83 70-1301,2-Dichlorobenzene ug/L 36.550 73 58-1301,3-Dichlorobenzene ug/L 31.450 63 53-1301,4-Dichlorobenzene ug/L 32.450 65 57-1202,2'-Oxybis(1-chloropropane) ug/L 35.950 72 55-1302,4,5-Trichlorophenol ug/L 49.450 99 59-1242,4,6-Trichlorophenol ug/L 48.150 96 64-1252,4-Dichlorophenol ug/L 48.450 97 61-1132,4-Dimethylphenol ug/L 41.150 82 30-1122,4-Dinitrophenol ug/L 38.950 78 33-136




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401939560236105019 CP CS


Parameter UnitsLCS



2,4-Dinitrotoluene ug/L 54.150 108 70-1322,6-Dinitrotoluene ug/L 52.150 104 70-1262-Chloronaphthalene ug/L 46.150 92 70-1302-Chlorophenol ug/L 41.450 83 55-1302-Methylnaphthalene ug/L 47.750 95 70-1302-Methylphenol(o-Cresol) ug/L 40.550 81 45-1072-Nitroaniline ug/L 51.450 103 57-1402-Nitrophenol ug/L 51.650 103 67-1173&4-Methylphenol(m&p Cresol) ug/L 35.450 71 39-1303,3'-Dichlorobenzidine ug/L 47.9 L150 96 38-913-Nitroaniline ug/L 46.650 93 60-1254,6-Dinitro-2-methylphenol ug/L 41.450 83 54-1394-Bromophenylphenyl ether ug/L 47.650 95 70-1304-Chloro-3-methylphenol ug/L 48.950 98 54-1184-Chloroaniline ug/L 39.350 79 60-1304-Chlorophenylphenyl ether ug/L 49.250 98 70-1304-Nitroaniline ug/L 49.250 98 53-1294-Nitrophenol ug/L 12.750 25 10-130Acenaphthene ug/L 47.450 95 69-119Acenaphthylene ug/L 51.150 102 70-130Anthracene ug/L 50.250 100 73-134Benzo(a)anthracene ug/L 50.550 101 70-130Benzo(a)pyrene ug/L 43.750 87 74-117Benzo(b)fluoranthene ug/L 43.150 86 70-125Benzo(g,h,i)perylene ug/L 45.350 91 67-130Benzo(k)fluoranthene ug/L 47.250 94 70-130bis(2-Chloroethoxy)methane ug/L 46.850 94 70-130bis(2-Chloroethyl) ether ug/L 39.450 79 63-116bis(2-Ethylhexyl)phthalate ug/L 55.350 111 70-130Butylbenzylphthalate ug/L 57.850 116 73-133Carbazole ug/L 47.350 95 70-130Chrysene ug/L 51.350 103 70-130Di-n-butylphthalate ug/L 47.250 94 71-131Di-n-octylphthalate ug/L 52.650 105 65-118Dibenz(a,h)anthracene ug/L 45.950 92 36-111Dibenzofuran ug/L 48.950 98 70-130Diethylphthalate ug/L 51.250 102 70-130Dimethylphthalate ug/L 49.950 100 70-130Fluoranthene ug/L 51.250 102 86-130Fluorene ug/L 51.050 102 70-130Hexachloro-1,3-butadiene ug/L 38.950 78 63-107Hexachlorobenzene ug/L 49.450 99 70-124Hexachlorocyclopentadiene ug/L 20.650 41 25-73Hexachloroethane ug/L 28.950 58 50-130Indeno(1,2,3-cd)pyrene ug/L 44.250 88 64-130Isophorone ug/L 46.350 93 65-130N-Nitroso-di-n-propylamine ug/L 45.850 92 67-130




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401939560236105019 CP CS


Parameter UnitsLCS



N-Nitrosodiphenylamine ug/L 45.350 91 80-121Naphthalene ug/L 46.550 93 70-130Nitrobenzene ug/L 45.850 92 70-130Pentachlorophenol ug/L 37.750 75 61-113Phenanthrene ug/L 49.550 99 70-130Phenol ug/L 17.650 35 25-120Pyrene ug/L 55.350 111 70-1302,4,6-Tribromophenol (S) % 100 57-1312-Fluorobiphenyl (S) % 78 47-1052-Fluorophenol (S) % 50 32-120Nitrobenzene-d5 (S) % 91 51-108Phenol-d6 (S) % 31 18-120Terphenyl-d14 (S) % 96 65-147

Parameter UnitsMS



MSSpikeResult

40193956002

1930599

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4-Trichlorobenzene ug/L M647.2 0 63-1300 2547.2<59.3 <59.3 <59.31,2-Dichlorobenzene ug/L M647.2 80 56-1300 2247.2<54.5 <54.5 <54.51,3-Dichlorobenzene ug/L M647.2 0 50-13066 3147.2<58.3 <58.3 <58.31,4-Dichlorobenzene ug/L M647.2 0 55-12068 2447.2<54.3 <54.3 <54.32,2'-Oxybis(1-chloropropane)

ug/L M647.2 0 48-1300 2247.2<46.5 <46.5 <46.5

2,4,5-Trichlorophenol ug/L M647.2 0 26-1240 3447.2<24.3 <24.3 <24.32,4,6-Trichlorophenol ug/L M647.2 0 29-1250 2647.2<30.1 <30.1 <30.12,4-Dichlorophenol ug/L M647.2 0 21-1140 2247.2<33.8 <33.8 <33.82,4-Dimethylphenol ug/L M647.2 0 10-1220 5047.2<43.7 <43.7 <43.72,4-Dinitrophenol ug/L M647.2 0 12-1600 2747.2<92.5 <92.5 <92.52,4-Dinitrotoluene ug/L M647.2 0 32-1430 2247.2<40.0 <40.0 <40.02,6-Dinitrotoluene ug/L M647.2 0 66-1260 2047.2<29.2 <29.2 <29.22-Chloronaphthalene ug/L M647.2 67 61-13046 2147.2<31.3 31.7J <31.32-Chlorophenol ug/L M647.2 0 37-1300 2147.2<31.3 <31.3 <31.32-Methylnaphthalene ug/L 47.2 82 68-13084 2047.2<43.9 <43.9 <43.92-Methylphenol(o-Cresol) ug/L M647.2 0 25-1070 4347.2<35.1 <35.1 <35.12-Nitroaniline ug/L M647.2 0 12-1470 2047.2<35.8 <35.8 <35.82-Nitrophenol ug/L M647.2 0 39-1180 2047.2<31.2 <31.2 <31.23&4-Methylphenol(m&pCresol)

ug/L M647.2 0 21-1300 3847.2<23.1 <23.1 <23.1

3,3'-Dichlorobenzidine ug/L M647.2 0 10-910 3847.2<50.7 <50.7 <50.73-Nitroaniline ug/L M647.2 0 13-1260 3047.2<51.5 <51.5 <51.54,6-Dinitro-2-methylphenol ug/L M647.2 0 24-1580 2347.2<118 <118 <1184-Bromophenylphenyl ether ug/L 47.2 90 48-13484 2147.2<36.1 42.3J 39.6J4-Chloro-3-methylphenol ug/L M647.2 0 37-1180 2447.2<25.8 <25.8 <25.84-Chloroaniline ug/L M647.2 0 20-1300 3747.2<67.4 <67.4 <67.44-Chlorophenylphenyl ether ug/L M647.2 90 70-1300 2047.2<31.3 42.3J <31.3




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401939560236105019 CP CS


Parameter UnitsMS



MSSpikeResult

40193956002

1930599

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

4-Nitroaniline ug/L M647.2 0 10-1350 3247.2<113 <113 <1134-Nitrophenol ug/L M647.2 0 10-1300 5047.2<115 <115 <115Acenaphthene ug/L 47.2 99 60-12289 2247.2<28.8 46.9J 41.9JAcenaphthylene ug/L 47.2 84 66-13084 2147.2<27.5 39.7J 39.6JAnthracene ug/L M647.2 0 73-13485 2147.2<30.6 <30.6 39.9JBenzo(a)anthracene ug/L 47.2 100 44-14692 2247.2<32.0 47.4J 43.3JBenzo(a)pyrene ug/L M647.2 118 10-2000 2147.2<48.0 55.7J <48.0Benzo(b)fluoranthene ug/L M647.2 143 53-125120 2447.2<39.1 67.3J 56.7JBenzo(g,h,i)perylene ug/L 47.2 125 10-200120 3447.2<52.0 59.0J 56.4JBenzo(k)fluoranthene ug/L M647.2 135 10-2000 2247.2<42.4 63.9J <42.4bis(2-Chloroethoxy)methane

ug/L M647.2 0 45-1320 2147.2<49.3 <49.3 <49.3

bis(2-Chloroethyl) ether ug/L M647.2 0 47-1160 2047.2<44.1 <44.1 <44.1bis(2-Ethylhexyl)phthalate ug/L M647.2 0 40-1460 3047.2<109 <109 <109Butylbenzylphthalate ug/L M647.2 0 44-1580 2147.2<49.0 <49.0 <49.0Carbazole ug/L M647.2 0 70-1300 2047.2<34.5 <34.5 <34.5Chrysene ug/L M647.2 121 67-1300 2247.2<47.9 57.2J <47.9Di-n-butylphthalate ug/L M647.2 0 71-1360 2047.2<46.4 <46.4 <46.4Di-n-octylphthalate ug/L M647.2 0 15-1750 2647.2<180 <180 <180Dibenz(a,h)anthracene ug/L M647.2 113 10-1600 4047.2<41.7 53.5J <41.7Dibenzofuran ug/L 47.2 88 65-13080 2047.2<32.0 41.4J 37.5JDiethylphthalate ug/L M647.2 0 70-1300 2047.2<29.3 <29.3 <29.3Dimethylphthalate ug/L M647.2 0 70-1300 2347.2<27.2 <27.2 <27.2Fluoranthene ug/L M647.2 88 60-1320 2047.2<37.3 41.5J <37.3Fluorene ug/L 47.2 98 61-13096 2147.2<34.2 46.1J 45.2JHexachloro-1,3-butadiene ug/L M647.2 0 63-1090 2047.2<43.3 <43.3 <43.3Hexachlorobenzene ug/L M647.2 0 57-1240 2047.2<62.3 <62.3 <62.3Hexachlorocyclopentadiene ug/L M647.2 0 10-730 4647.2<38.0 <38.0 <38.0Hexachloroethane ug/L M647.2 0 50-1300 3347.2<53.6 <53.6 <53.6Indeno(1,2,3-cd)pyrene ug/L M647.2 152 10-2000 3547.2<45.9 71.6J <45.9Isophorone ug/L M647.2 0 65-1300 2047.2<29.2 <29.2 <29.2N-Nitroso-di-n-propylamine ug/L M647.2 0 67-1300 2047.2<42.8 <42.8 <42.8N-Nitrosodiphenylamine ug/L M647.2 75 71-12167 3647.2<130 <130 <130Naphthalene ug/L M647.2 89 63-1300 2247.2<46.0 <46.0 <46.0Nitrobenzene ug/L M647.2 0 23-1470 2147.2<40.6 <40.6 <40.6Pentachlorophenol ug/L M647.2 -82 10-200-175 4 2447.21260 1220 1180Phenanthrene ug/L 47.2 89 70-13092 2247.2<36.0 42.0J 43.5JPhenol ug/L M647.2 0 20-1200 2547.2<12.1 <12.1 <12.1Pyrene ug/L M647.2 99 68-1300 2347.2<45.3 46.5J <45.32,4,6-Tribromophenol (S) % S40 57-13102-Fluorobiphenyl (S) % 60 47-105762-Fluorophenol (S) % S40 32-1200Nitrobenzene-d5 (S) % S40 51-1080Phenol-d6 (S) % S40 18-1200Terphenyl-d14 (S) % S40 65-1470




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#=QL#

QUALIFIERS


401939560236105019 CP CS

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.ND - Not Detected at or above adjusted reporting limit.TNTC - Too Numerous To CountJ - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.MDL - Adjusted Method Detection Limit.PQL - Practical Quantitation Limit.RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision andbias for a specific analyte in a specific matrix.S - Surrogate1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.LCS(D) - Laboratory Control Sample (Duplicate)MS(D) - Matrix Spike (Duplicate)DUP - Sample DuplicateRPD - Relative Percent DifferenceNC - Not Calculable.SG - Silica Gel - Clean-UpU - Indicates the compound was analyzed for, but not detected.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.TNI - The NELAC Institute.

LABORATORIES

Pace Analytical Services - Green BayPASI-G

ANALYTE QUALIFIERS

Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results may be biased high.L1Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6The reporting limit verification did not meet the performance criteria specified by the Minnesota Department of HealthR4Surrogate recovery outside laboratory control limits.S0Surrogate recovery not evaluated against control limits due to sample dilution.S4




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#=CR#

QUALITY CONTROL DATA CROSS REFERENCE TABLE


401939560236105019 CP CS

Lab ID Sample ID QC Batch Method QC Batch Analytical MethodAnalyticalBatch

40193956002 332330 332375RW06-24-MS-0819-100 EPA 3510 EPA 827040193956003 332330 332375RW07-44-MS-0819-100 EPA 3510 EPA 827040193956004 332330 332375CS IN BETWEEN EPA 3510 EPA 827040193956005 332330 332375CS EFFLUENT EPA 3510 EPA 8270

40193956002 332672 332780RW06-24-MS-0819-100 EPA 3510 EPA 827040193956003 332672 332780RW07-44-MS-0819-100 EPA 3510 EPA 827040193956005 332672 332780CS EFFLUENT EPA 3510 EPA 8270

40193956001 332334082819-0800-200 EPA 8260

40193956002 332563RW06-24-MS-0819-100 EPA 826040193956003 332563RW07-44-MS-0819-100 EPA 8260




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