Appendix I: Leachability - Laboratory Test Certificates ... · Site # 23736 Date Reported:Sep 21, 2017 Eurofins | mgt 2-5 Kingston Town Close, Oakleigh, Victoria, Australia, 3166

Appendix I: Leachability - Laboratory Test Certificates and CoC

Documentation

Certificate of Analysis

Coffey Environments Pty Ltd VIC

Level 1, 436 Johnston Street

Abbotsford

VIC 3067

Attention: Sarah Richards

Report 562180-S

Project name DOD TINDAL

Project ID 754-MELEN199420

Received Date Sep 07, 2017

Client Sample ID 0990_SS168_170821

0990_SS169_170821

0990_SS170_170821

0990_SS171_170821

Sample Matrix Soil Soil Soil Soil

Eurofins | mgt Sample No. M17-Se07424 M17-Se07425 M17-Se07426 M17-Se07427

Date Sampled Aug 31, 2017 Aug 31, 2017 Aug 31, 2017 Aug 31, 2017

Test/Reference LOR Unit

Conductivity (1:5 aqueous extract at 25°C) 10 uS/cm 97 - 13 -

pH (1:5 Aqueous extract) 0.1 pH Units 8.8 7.5 7.6 8.0

Total Organic Carbon 0.1 % 1.8 < 0.1 < 0.1 0.1

% Moisture 1 % 47 24 16 12

Cation Exchange Capacity

Cation Exchange Capacity 0.05 meq/100g 66 - 1.5 -


0990_SS173_170821

0990_SS174_170821

0990_SS175_170821







Total Organic Carbon 0.1 % 1.3 3.1 1.6 0.4

% Moisture 1 % 26 26 2.4 35


Cation Exchange Capacity 0.05 meq/100g 7.4 - 52 -


0990_SS177_170821

0990_SS178_170821

0990_SS179_170821








% Moisture 1 % 27 29 23 17


Cation Exchange Capacity 0.05 meq/100g 6.4 - 2.1 -

Date Reported: Sep 21, 2017

Eurofins | mgt 2-5 Kingston Town Close, Oakleigh, Victoria, Australia, 3166

ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 11

Report Number: 562180-S

NATA AccreditedAccreditation Number 1261Site Number 1254

Accredited for compliance with ISO/IEC 17025 – TestingThe results of the tests, calibrations and/ormeasurements included in this document are traceableto Australian/national standards.


0990_SS181_170821

0990_SS182_170821

0990_SS183_170821








% Moisture 1 % 22 23 7.7 26


Cation Exchange Capacity 0.05 meq/100g 2.4 - 40 -


0990_SS185_170821

0990_SS186_170821

0990_SS187_170821








% Moisture 1 % 15 19 19 17


Cation Exchange Capacity 0.05 meq/100g 16 - 27 -


0990_SS189_170821

0990_SS190_170821

0990_SS191_170821







Total Organic Carbon 0.1 % 1.2 0.7 < 0.1 0.4

% Moisture 1 % 23 1.4 15 < 1


Cation Exchange Capacity 0.05 meq/100g 31 - 16 -


Sample Matrix Soil

Eurofins | mgt Sample No. M17-Se07448

Date Sampled Aug 31, 2017


pH (1:5 Aqueous extract) 0.1 pH Units 5.6

Total Organic Carbon 0.1 % 0.1

% Moisture 1 % 5.3



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 11


Sample HistoryWhere samples are submitted/analysed over several days, the last date of extraction and analysis is reported.A recent review of our LIMS has resulted in the correction or clarification of some method identifications. Due to this, some of the method reference information on reports has changed. However,no substantive change has been made to our laboratory methods, and as such there is no change in the validity of current or previous results (regarding both quality and NATA accreditation).

If the date and time of sampling are not provided, the Laboratory will not be responsible for compromised results should testing be performed outside the recommended holding time.

Description Testing Site Extracted Holding Time

Conductivity (1:5 aqueous extract at 25°C) Melbourne Sep 09, 2017 7 Day

- Method: LTM-INO-4030

Cation Exchange Capacity Melbourne Sep 12, 2017 180 Days

- Method: LTM-MET-3060 - Cation Exchange Capacity (CEC) & Exchangeable Sodium Percentage (ESP)

pH (1:5 Aqueous extract) Melbourne Sep 11, 2017 7 Day

- Method: LTM-GEN-7090 pH in soil by ISE

Total Organic Carbon Melbourne Sep 12, 2017 28 Day

- Method: APHA 5310B Total Organic Carbon

% Moisture Melbourne Sep 07, 2017 14 Day

- Method: LTM-GEN-7080 Moisture



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 11


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Sep 7, 2017 12:00 AMAddress: Level 1, 436 Johnston Street Report #: 562180 Due: Sep 14, 2017

Abbotsford Phone: 03 8413 6900 Priority: 5 DayVIC 3067 Fax: Contact Name: Sarah Richards

Project Name: DOD TINDALProject ID: 754-MELEN199420

Eurofins | mgt Analytical Services Manager : Mary Makarios

Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Cation E

xchange Capacity

Per- and P

olyfluorinated Alkyl S

ubstances(P

FA

Ss)

Melbourne Laboratory - NATA Site # 1254 & 14271 X X X X

Sydney Laboratory - NATA Site # 18217

Brisbane Laboratory - NATA Site # 20794 X X

Perth Laboratory - NATA Site # 23736

External Laboratory

No Sample ID Sample Date SamplingTime

Matrix LAB ID

1 0990_SS168_170821

Aug 31, 2017 Soil M17-Se07424 X X X X

2 0990_SS169_170821

Aug 31, 2017 Soil M17-Se07425 X X X

3 0990_SS170_170821

Aug 31, 2017 Soil M17-Se07426 X X X X

4 0990_SS171_170821

Aug 31, 2017 Soil M17-Se07427 X X X

5 0990_SS172_170821

Aug 31, 2017 Soil M17-Se07428 X X X X

6 0990_SS173_ Aug 31, 2017 Soil M17-Se07429 X X X

ABN– 50 005 085 521e.mail : [email protected] : www.eurofins.com.au

MelbourneMelbourneMelbourneMelbourne2-5 Kingston Town CloseOakleigh VIC 3166Phone : +61 3 8564 5000NATA # 1261Site # 1254 & 14271

SydneySydneySydneySydneyUnit F3, Building F16 Mars RoadLane Cove West NSW 2066Phone : +61 2 9900 8400NATA # 1261 Site # 18217

BrisbaneBrisbaneBrisbaneBrisbane1/21 Smallwood PlaceMurarrie QLD 4172Phone : +61 7 3902 4600NATA # 1261 Site # 20794

PerthPerthPerthPerth2/91 Leach HighwayKewdale WA 6105Phone : +61 8 9251 9600NATA # 1261Site # 23736

Date Reported:Sep 21, 2017


ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 11


Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Sep 7, 2017 12:00 AMAddress: Level 1, 436 Johnston Street Report #: 562180 Due: Sep 14, 2017




Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Cation E

xchange Capacity

Per- and P


ubstances(P

FA

Ss)





170821

7 0990_SS174_170821

Aug 31, 2017 Soil M17-Se07430 X X X X

8 0990_SS175_170821

Aug 31, 2017 Soil M17-Se07431 X X X

9 0990_SS176_170821

Aug 31, 2017 Soil M17-Se07432 X X X X

10 0990_SS177_170821

Aug 31, 2017 Soil M17-Se07433 X X X

11 0990_SS178_170821

Aug 31, 2017 Soil M17-Se07434 X X X X

12 0990_SS179_170821

Aug 31, 2017 Soil M17-Se07435 X X X

13 0990_SS180_ Aug 31, 2017 Soil M17-Se07436 X X X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 11






Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Cation E

xchange Capacity

Per- and P


ubstances(P

FA

Ss)





170821

14 0990_SS181_170821

Aug 31, 2017 Soil M17-Se07437 X X X

15 0990_SS182_170821

Aug 31, 2017 Soil M17-Se07438 X X X X

16 0990_SS183_170821

Aug 31, 2017 Soil M17-Se07439 X X X

17 0990_SS184_170821

Aug 31, 2017 Soil M17-Se07440 X X X X

18 0990_SS185_170821

Aug 31, 2017 Soil M17-Se07441 X X X

19 0990_SS186_170821

Aug 31, 2017 Soil M17-Se07442 X X X X









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 11






Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Cation E

xchange Capacity

Per- and P


ubstances(P

FA

Ss)





170821

21 0990_SS188_170821

Aug 31, 2017 Soil M17-Se07444 X X X X

22 0990_SS189_170821

Aug 31, 2017 Soil M17-Se07445 X X X

23 0990_SS190_170821

Aug 31, 2017 Soil M17-Se07446 X X X X

24 0990_SS191_170821

Aug 31, 2017 Soil M17-Se07447 X X X

25 0990_SS192_170821

Aug 31, 2017 Soil M17-Se07448 X X X

26 0990_SS175_170821

Aug 31, 2017 AUS Leachate M17-Se07449 X X

27 0990_SS176_ Aug 31, 2017 AUS Leachate M17-Se07450 X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 11






Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Cation E

xchange Capacity

Per- and P


ubstances(P

FA

Ss)





170821

28 0990_SS186_170821


29 0990_SS188_170821


Test Counts 25 25 4 25 12 4








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 11


Internal Quality Control Review and Glossary

General

Holding Times

Units

Terms

QC - Acceptance Criteria

QC Data General Comments

1. Laboratory QC results for Method Blanks, Duplicates, Matrix Spikes, and Laboratory Control Samples are included in this QC report where applicable. Additional QC data may be available on

request.

2. All soil results are reported on a dry basis, unless otherwise stated.

3. All biota results are reported on a wet weight basis on the edible portion, unless otherwise stated.

4. Actual LORs are matrix dependant. Quoted LORs may be raised where sample extracts are diluted due to interferences.

5. Results are uncorrected for matrix spikes or surrogate recoveries except for PFAS compounds.

6. SVOC analysis on waters are performed on homogenised, unfiltered samples, unless noted otherwise.

7. Samples were analysed on an 'as received' basis.

8. This report replaces any interim results previously issued.

Please refer to 'Sample Preservation and Container Guide' for holding times (QS3001).

For samples received on the last day of holding time, notification of testing requirements should have been received at least 6 hours prior to sample receipt deadlines as stated on the Sample

Receipt Advice.

If the Laboratory did not receive the information in the required timeframe, and regardless of any other integrity issues, suitably qualified results may still be reported.

Holding times apply from the date of sampling, therefore compliance to these may be outside the laboratory's control.

**NOTE: pH duplicates are reported as a range NOT as RPD

mg/kg: milligrams per kilogram mg/L: milligrams per litre

ug/L: micrograms per litre ppm: Parts per million

ppb: Parts per billion %: Percentage

org/100mL: Organisms per 100 millilitres NTU: Nephelometric Turbidity Units

MPN/100mL: Most Probable Number of organisms per 100 millilitres

Dry Where a moisture has been determined on a solid sample the result is expressed on a dry basis.

LOR Limit of Reporting.

SPIKE Addition of the analyte to the sample and reported as percentage recovery.

RPD Relative Percent Difference between two Duplicate pieces of analysis.

LCS Laboratory Control Sample - reported as percent recovery.

CRM Certified Reference Material - reported as percent recovery.

Method Blank In the case of solid samples these are performed on laboratory certified clean sands and in the case of water samples these are performed on de-ionised water.

Surr - Surrogate The addition of a like compound to the analyte target and reported as percentage recovery.

Duplicate A second piece of analysis from the same sample and reported in the same units as the result to show comparison.

USEPA United States Environmental Protection Agency

APHA American Public Health Association

TCLP Toxicity Characteristic Leaching Procedure

COC Chain of Custody

SRA Sample Receipt Advice

QSM Quality Systems Manual ver 5.1 US Department of Defense

CP Client Parent - QC was performed on samples pertaining to this report

NCP Non-Client Parent - QC performed on samples not pertaining to this report, QC is representative of the sequence or batch that client samples were analysed within.

TEQ Toxic Equivalency Quotient

RPD Duplicates: Global RPD Duplicates Acceptance Criteria is 30% however the following acceptance guidelines are equally applicable:

Results <10 times the LOR : No Limit

Results between 10-20 times the LOR : RPD must lie between 0-50%

Results >20 times the LOR : RPD must lie between 0-30%

Surrogate Recoveries: Recoveries must lie between 50-150%-Phenols & PFASs

PFAS field samples that contain surrogate recoveries in excess of the QC limit designated in QSM 5.1 where no positive PFAS results have been reported have been reviewed and no data was

affected.

1. Where a result is reported as a less than (<), higher than the nominated LOR, this is due to either matrix interference, extract dilution required due to interferences or contaminant levels within

the sample, high moisture content or insufficient sample provided.

2. Duplicate data shown within this report that states the word "BATCH" is a Batch Duplicate from outside of your sample batch, but within the laboratory sample batch at a 1:10 ratio. The Parent

and Duplicate data shown is not data from your samples.

3. Organochlorine Pesticide analysis - where reporting LCS data, Toxaphene & Chlordane are not added to the LCS.

4. Organochlorine Pesticide analysis - where reporting Spike data, Toxaphene is not added to the Spike.

5. Total Recoverable Hydrocarbons - where reporting Spike & LCS data, a single spike of commercial Hydrocarbon products in the range of C12-C30 is added and it's Total Recovery is reported

in the C10-C14 cell of the Report.

6. pH and Free Chlorine analysed in the laboratory - Analysis on this test must begin within 30 minutes of sampling.Therefore laboratory analysis is unlikely to be completed within holding time.

Analysis will begin as soon as possible after sample receipt.

7. Recovery Data (Spikes & Surrogates) - where chromatographic interference does not allow the determination of Recovery the term "INT" appears against that analyte.

8. Polychlorinated Biphenyls are spiked only using Aroclor 1260 in Matrix Spikes and LCS.

9. For Matrix Spikes and LCS results a dash " -" in the report means that the specific analyte was not added to the QC sample.

10. Duplicate RPDs are calculated from raw analytical data thus it is possible to have two sets of data.



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 11


Quality Control Results

Test Units Result 1 AcceptanceLimits

PassLimits

QualifyingCode

Method Blank

Conductivity (1:5 aqueous extract at 25°C) uS/cm < 10 10 Pass

Total Organic Carbon % < 0.1 0.1 Pass

Method Blank


Cation Exchange Capacity meq/100g < 0.05 0.05 Pass

LCS - % Recovery

Total Organic Carbon % 89 70-130 Pass

Test Lab Sample ID QASource Units Result 1 Acceptance

LimitsPass

LimitsQualifying

Code

Duplicate

Result 1 Result 2 RPD

Total Organic Carbon M17-Se07424 CP % 1.8 1.6 11 30% Pass

% Moisture M17-Se10377 NCP % 9.3 9.3 <1 30% Pass

Duplicate

Cation Exchange Capacity Result 1 Result 2 RPD

Cation Exchange Capacity M17-Se08631 NCP meq/100g 10 10 4.0 30% Pass

Duplicate


Conductivity (1:5 aqueous extractat 25°C) M17-Se07426 CP uS/cm 13 11 20 30% Pass

pH (1:5 Aqueous extract) M17-Se07426 CP pH Units 7.6 7.6 pass 30% Pass

Duplicate


Conductivity (1:5 aqueous extractat 25°C) M17-Se07428 CP uS/cm 25 25 <1 30% Pass


Duplicate


Total Organic Carbon M17-Se07432 CP % 0.5 0.7 30 30% Pass

Duplicate


Conductivity (1:5 aqueous extractat 25°C) M17-Se07434 CP uS/cm 24 27 13 30% Pass


Duplicate


Total Organic Carbon M17-Se07440 CP % 1.1 0.7 46 30% Fail Q15

Duplicate


Conductivity (1:5 aqueous extractat 25°C) M17-Se07444 CP uS/cm 77 71 8.0 30% Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 11


Comments

Sample IntegrityCustody Seals Intact (if used) N/A

Attempt to Chill was evident Yes

Sample correctly preserved Yes

Appropriate sample containers have been used Yes

Sample containers for volatile analysis received with minimal headspace Yes

Samples received within HoldingTime Yes

Some samples have been subcontracted No

Qualifier Codes/Comments

Code DescriptionQ15 The RPD reported passes Eurofins | mgt's QC - Acceptance Criteria as defined in the Internal Quality Control Review and Glossary page of this report.

Authorised By

Mary Makarios Analytical Services Manager

Alex Petridis Senior Analyst-Metal (VIC)

Huong Le Senior Analyst-Inorganic (VIC)

Glenn Jackson

National Operations Manager

- Indicates Not Requested

* Indicates NATA accreditation does not cover the performance of this service

Measurement uncertainty of test data is available on request or please click here.Eurofins | mgt shall not be liable for loss, cost, damages or expenses incurred by the client, or any other person or company, resulting from the use of any information or interpretation given in this report. In no case shall Eurofins | mgt be liable for consequential damages including, but notlimited to, lost profits, damages for failure to meet deadlines and lost production arising from this report. This document shall not be reproduced except in full and relates only to the items tested. Unless indicated otherwise, the tests were performed on the samples as received.



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 11


http://www.eurofins.com.au/media/311687/reporting-measurement-uncertainty-of-chemical-and-microbiology-test-results.pdf




Abbotsford

VIC 3067

Attention: Ian Newby

Report 568586-L



Received Date Oct 19, 2017


0990_SS129_170712

0990_SS162_170731

0990_SS101_0.0_170706

Sample Matrix AUS Leachate AUS Leachate AUS Leachate AUS Leachate

Eurofins | mgt Sample No. B17-Oc23370 B17-Oc23372 B17-Oc23374 B17-Oc23376

Date Sampled Jul 29, 2017 Jul 12, 2017 Jul 31, 2017 Jul 06, 2017


Perfluoroalkyl carboxylic acids (PFCAs)

Perfluorobutanoic acid (PFBA)N11 0.05 ug/L < 0.05 0.28 < 0.05 < 0.05

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L < 0.01 0.25 < 0.01 < 0.01

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N090.02 N090.73 < 0.01 < 0.01

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L < 0.01 N090.14 < 0.01 < 0.01

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N090.02 N090.54 < 0.01 < 0.01

Perfluorononanoic acid (PFNA)N11 0.01 ug/L < 0.01 0.16 < 0.01 < 0.01

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L < 0.01 0.24 < 0.01 < 0.01

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.01 0.13 < 0.01 < 0.01

Perfluorododecanoic acid (PFDoA)N11 0.01 ug/L < 0.01 N090.03 < 0.01 < 0.01

Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluorotetradecanoic acid (PFTeDA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

13C4-PFBA (surr.) 1 % 137 122 139 123

13C5-PFPeA (surr.) 1 % 107 87 101 105

13C5-PFHxA (surr.) 1 % 76 64 74 83

13C4-PFHpA (surr.) 1 % 100 90 101 105

13C8-PFOA (surr.) 1 % 135 120 142 143

13C5-PFNA (surr.) 1 % 119 101 122 121

13C6-PFDA (surr.) 1 % 87 68 104 106

13C2-PFUnDA (surr.) 1 % 58 48 79 69

13C2-PFDoDA (surr.) 1 % 47 37 76 77

13C2-PFTeDA (surr.) 1 % 24 10 37 24

Perfluoroalkane sulfonamides (PFASAs)

Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L < 0.05 0.59 < 0.05 < 0.05

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

13C8-FOSA (surr.) 1 % 57 36 73 69

D3-N-MeFOSA (surr.) 1 % 28 32 43 31

Date Reported: Oct 30, 2017

Eurofins | mgt 1/21 Smallwood Place, Murarrie, QLD, Australia, 4172

ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 1 of 16

Report Number: 568586-L




0990_SS129_170712

0990_SS162_170731

0990_SS101_0.0_170706






D5-N-EtFOSA (surr.) 1 % 19 27 38 25

D7-N-MeFOSE (surr.) 1 % 29 32 48 35

D9-N-EtFOSE (surr.) 1 % 25 26 38 27

D5-N-EtFOSAA (surr.) 1 % 46 38 67 62

D3-N-MeFOSAA (surr.) 1 % 50 43 76 71

Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs)

Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L N090.02 N090.32 < 0.01 < 0.01

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.04 N090.34 < 0.01 < 0.01

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N090.24 N092.2 N090.02 N090.01

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N090.02 N090.59 < 0.01 < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.63 16 < 0.01 < 0.01

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.01 0.01 < 0.01 < 0.01

13C3-PFBS (surr.) 1 % 88 78 83 86

18O2-PFHxS (surr.) 1 % 136 103 138 135

13C8-PFOS (surr.) 1 % 84 78 93 75

n:2 Fluorotelomer sulfonic acids

1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L < 0.01 0.41 < 0.01 < 0.01

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

13C2-4:2 FTS (surr.) 1 % 84 81 79 109

13C2-6:2 FTS (surr.) 1 % 118 112 120 136

13C2-8:2 FTS (surr.) 1 % 67 63 86 94

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 0.87 18.2 0.02 0.01

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 0.65 16.54 < 0.01 < 0.01

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L 0.89 18.74 0.02 0.01

Sum of WA DER PFAS (n=10) 0.05 ug/L 0.93 20.87 < 0.05 < 0.05

Sum of PFASs (n=28) 0.1 ug/L 0.99 22.96 < 0.1 < 0.1

AUS Leaching Procedure

Leachate FluidC01 comment 4.0 4.0 4.0 4.0

pH (initial) 0.1 pH Units 8.9 8.7 8.3 8.4

pH (Leachate fluid) 0.1 pH Units 7.0 7.0 7.0 7.0

pH (off) 0.1 pH Units 8.0 7.7 7.7 7.9



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 2 of 16



0990_SS134_170713

0990_SS135_170713

0990_SS202_170929



Date Sampled Jul 12, 2017 Jul 13, 2017 Jul 13, 2017 Sep 29, 2017



Perfluorobutanoic acid (PFBA)N11 0.05 ug/L 0.42 < 0.05 < 0.05 0.07

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L N090.37 < 0.01 0.02 N090.04

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N090.57 < 0.01 N090.03 N090.14

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L < 0.2 < 0.01 0.02 N090.02

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N090.52 N090.02 N090.06 N090.04

Perfluorononanoic acid (PFNA)N11 0.01 ug/L N090.22 < 0.01 0.01 < 0.01

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L N090.43 < 0.01 < 0.01 < 0.01

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.2 < 0.01 < 0.01 < 0.01

Perfluorododecanoic acid (PFDoA)N11 0.01 ug/L < 0.2 < 0.01 < 0.01 < 0.01



13C4-PFBA (surr.) 1 % 156 120 127 112

13C5-PFPeA (surr.) 1 % 165 93 94 102

13C5-PFHxA (surr.) 1 % 134 65 67 78

13C4-PFHpA (surr.) 1 % 143 92 92 108

13C8-PFOA (surr.) 1 % 155 131 135 152

13C5-PFNA (surr.) 1 % 146 130 127 130

13C6-PFDA (surr.) 1 % 138 112 113 96

13C2-PFUnDA (surr.) 1 % 105 80 82 58

13C2-PFDoDA (surr.) 1 % 78 84 81 62

13C2-PFTeDA (surr.) 1 % 16 30 28 28


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L < 0.2 < 0.05 < 0.05 < 0.05







13C8-FOSA (surr.) 1 % 101 70 65 66

D3-N-MeFOSA (surr.) 1 % 46 60 49 38

D5-N-EtFOSA (surr.) 1 % 36 54 41 34

D7-N-MeFOSE (surr.) 1 % 52 63 59 40

D9-N-EtFOSE (surr.) 1 % 32 48 46 31

D5-N-EtFOSAA (surr.) 1 % 108 63 62 58

D3-N-MeFOSAA (surr.) 1 % 112 67 69 63


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L 0.32 < 0.01 < 0.01 N090.12

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L 0.22 < 0.01 < 0.01 N090.16


Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L 0.30 < 0.01 < 0.01 < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L 9.8 < 0.01 N090.07 N090.02

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.2 < 0.01 < 0.01 < 0.01

13C3-PFBS (surr.) 1 % 135 78 81 83

18O2-PFHxS (surr.) 1 % 164 136 137 137

13C8-PFOS (surr.) 1 % 140 108 104 88



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 3 of 16



0990_SS134_170713

0990_SS135_170713

0990_SS202_170929








1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L 1.3 < 0.01 < 0.01 < 0.01


13C2-4:2 FTS (surr.) 1 % 113 70 77 144

13C2-6:2 FTS (surr.) 1 % 118 107 115 144

13C2-8:2 FTS (surr.) 1 % 113 95 85 91

PFASs Summations


Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 10.32 0.02 0.13 0.06


Sum of WA DER PFAS (n=10) 0.05 ug/L 15.4 < 0.05 0.26 0.92

Sum of PFASs (n=28) 0.1 ug/L 16.57 < 0.1 0.27 1.08





pH (off) 0.1 pH Units 7.8 8.1 7.9 7.3


0990_SS154_170729

0990_SS122_170712

0990_SS133_170713



Date Sampled Aug 22, 2017 Jul 29, 2017 Jul 12, 2017 Jul 13, 2017



Perfluorobutanoic acid (PFBA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 < 0.05

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L N090.06 < 0.01 0.03 N090.03

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N090.12 N090.03 0.07 N090.05

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N090.02 < 0.01 N090.01 0.02


Perfluorononanoic acid (PFNA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 0.02

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01





13C4-PFBA (surr.) 1 % 92 129 121 127

13C5-PFPeA (surr.) 1 % 104 100 96 100

13C5-PFHxA (surr.) 1 % 125 68 107 71

13C4-PFHpA (surr.) 1 % 113 96 97 95

13C8-PFOA (surr.) 1 % 112 131 146 138

13C5-PFNA (surr.) 1 % 103 121 131 123

13C6-PFDA (surr.) 1 % 80 103 117 103

13C2-PFUnDA (surr.) 1 % 69 75 86 77

13C2-PFDoDA (surr.) 1 % 62 72 83 76

13C2-PFTeDA (surr.) 1 % 15 33 33 30



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 4 of 16



0990_SS154_170729

0990_SS122_170712

0990_SS133_170713













13C8-FOSA (surr.) 1 % 59 70 55 65

D3-N-MeFOSA (surr.) 1 % 18 36 22 41

D5-N-EtFOSA (surr.) 1 % 14 30 19 35

D7-N-MeFOSE (surr.) 1 % 24 45 29 56

D9-N-EtFOSE (surr.) 1 % 17 37 22 44

D5-N-EtFOSAA (surr.) 1 % 61 62 68 58

D3-N-MeFOSAA (surr.) 1 % 62 67 79 63


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L 0.01 < 0.01 0.03 0.02

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L < 0.01 N090.02 N090.05 N090.02


Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.01 < 0.01 N090.10 < 0.01


13C3-PFBS (surr.) 1 % 120 81 81 83

18O2-PFHxS (surr.) 1 % 112 137 138 135

13C8-PFOS (surr.) 1 % 83 97 103 101




1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01


13C2-4:2 FTS (surr.) 1 % 114 74 INT 87

13C2-6:2 FTS (surr.) 1 % 113 106 134 125

13C2-8:2 FTS (surr.) 1 % 88 87 103 91

PFASs Summations




Sum of WA DER PFAS (n=10) 0.05 ug/L 0.26 0.08 0.41 0.22

Sum of PFASs (n=28) 0.1 ug/L 0.26 0.1 0.46 0.26





pH (off) 0.1 pH Units 8.3 8.4 8.3 8.5



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 5 of 16



Sample Matrix AUS Leachate

Eurofins | mgt Sample No. B17-Oc23394

Date Sampled Jul 29, 2017



Perfluorobutanoic acid (PFBA)N11 0.05 ug/L < 0.05

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L N090.07

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N090.13

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N090.05

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N090.11

Perfluorononanoic acid (PFNA)N11 0.01 ug/L 0.03

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L N090.02

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.01

Perfluorododecanoic acid (PFDoA)N11 0.01 ug/L < 0.01

Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L < 0.01

Perfluorotetradecanoic acid (PFTeDA)N11 0.01 ug/L < 0.01

13C4-PFBA (surr.) 1 % 133

13C5-PFPeA (surr.) 1 % 103

13C5-PFHxA (surr.) 1 % 70

13C4-PFHpA (surr.) 1 % 97

13C8-PFOA (surr.) 1 % 135

13C5-PFNA (surr.) 1 % 128

13C6-PFDA (surr.) 1 % 120

13C2-PFUnDA (surr.) 1 % 84

13C2-PFDoDA (surr.) 1 % 81

13C2-PFTeDA (surr.) 1 % 28


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L < 0.05

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA)N11 0.05 ug/L < 0.05

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA)N11 0.05 ug/L < 0.05

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE)N11 0.05 ug/L < 0.05

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE)N11 0.05 ug/L < 0.05

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA)N11 0.05 ug/L < 0.05

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA)N11 0.05 ug/L < 0.05

13C8-FOSA (surr.) 1 % 81

D3-N-MeFOSA (surr.) 1 % 48

D5-N-EtFOSA (surr.) 1 % 44

D7-N-MeFOSE (surr.) 1 % 50

D9-N-EtFOSE (surr.) 1 % 40

D5-N-EtFOSAA (surr.) 1 % 74

D3-N-MeFOSAA (surr.) 1 % 86


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L N090.03

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.05

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N090.21

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.03

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.01

13C3-PFBS (surr.) 1 % 81

18O2-PFHxS (surr.) 1 % 134

13C8-PFOS (surr.) 1 % 114



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 6 of 16



Sample Matrix AUS Leachate





1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS)N11 0.01 ug/L < 0.01

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 0.05 ug/L < 0.05

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L 0.02

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 0.01 ug/L < 0.01

13C2-4:2 FTS (surr.) 1 % 76

13C2-6:2 FTS (surr.) 1 % 123

13C2-8:2 FTS (surr.) 1 % 106

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 0.24

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 0.14

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L 0.35

Sum of WA DER PFAS (n=10) 0.05 ug/L 0.65

Sum of PFASs (n=28) 0.1 ug/L 0.75


Leachate FluidC01 comment 4.0

pH (initial) 0.1 pH Units 8.9

pH (Leachate fluid) 0.1 pH Units 7.0

pH (off) 0.1 pH Units 8.7



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 7 of 16





Per- and Polyfluorinated Alkyl Substances (PFASs)

Perfluoroalkyl carboxylic acids (PFCAs) Brisbane Oct 23, 2017 14 Day

- Method: LTM-ORG-2100 Per- and Polyfluorinated Alkyl Substances by LC-MS/MS

Perfluoroalkane sulfonamides (PFASAs) Brisbane Oct 23, 2017 14 Day


Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Brisbane Oct 23, 2017 14 Day


n:2 Fluorotelomer sulfonic acids Brisbane Oct 23, 2017 14 Day


AUS Leaching Procedure Brisbane Oct 23, 2017 7 Days

- Method: LTM-GEN-7010 Leaching Procedure for Soils & Solid Wastes



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 8 of 16


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Oct 19, 2017 12:00 AMAddress: Level 1, 436 Johnston Street Report #: 568586 Due: Oct 26, 2017

Abbotsford Phone: 03 8413 6900 Priority: 5 DayVIC 3067 Fax: Contact Name: Ian Newby



Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)

Melbourne Laboratory - NATA Site # 1254 & 14271 X X X




External Laboratory


Matrix LAB ID

1 0990_SS151_170729

Jul 29, 2017 Soil B17-Oc23369 X X X

2 0990_SS151_170729

Jul 29, 2017 AUS Leachate B17-Oc23370 X X

3 0990_SS129_170712

Jul 12, 2017 Soil B17-Oc23371 X X X

4 0990_SS129_170712


5 0990_SS162_170731

Jul 31, 2017 Soil B17-Oc23373 X X X

6 0990_SS162_ Jul 31, 2017 AUS Leachate B17-Oc23374 X X






Date Reported:Oct 30, 2017


ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 9 of 16


Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Oct 19, 2017 12:00 AMAddress: Level 1, 436 Johnston Street Report #: 568586 Due: Oct 26, 2017




Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





170731

7 0990_SS101_0.0_170706

Jul 06, 2017 Soil B17-Oc23375 X X X

8 0990_SS101_0.0_170706


9 0990_SS126_170712

Jul 12, 2017 Soil B17-Oc23377 X X X

10 0990_SS126_170712


11 0990_SS134_170713

Jul 13, 2017 Soil B17-Oc23379 X X X

12 0990_SS134_170713


13 0990_SS135_ Jul 13, 2017 Soil B17-Oc23381 X X X








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 10 of 16






Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





170713

14 0990_SS135_170713


15 0990_SS202_170929

Sep 29, 2017 Soil B17-Oc23383 X X X

16 0990_SS202_170929

Sep 29, 2017 AUS Leachate B17-Oc23384 X X

17 0990_SS192_170822

Aug 22, 2017 Soil B17-Oc23385 X X X

18 0990_SS192_170822

Aug 22, 2017 AUS Leachate B17-Oc23386 X X

19 0990_SS154_170729

Jul 29, 2017 Soil B17-Oc23387 X X X









ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 11 of 16






Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





170729

21 0990_SS122_170712

Jul 12, 2017 Soil B17-Oc23389 X X X

22 0990_SS122_170712


23 0990_SS133_170713

Jul 13, 2017 Soil B17-Oc23391 X X X

24 0990_SS133_170713


25 0990_SS158_170729

Jul 29, 2017 Soil B17-Oc23393 X X X

26 0990_SS158_170729


Test Counts 13 13 13 13 13








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 12 of 16



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 13 of 16




PassLimits

QualifyingCode

Method Blank


Perfluorobutanoic acid (PFBA) ug/L < 0.05 0.05 Pass

Perfluoropentanoic acid (PFPeA) ug/L < 0.01 0.01 Pass

Perfluorohexanoic acid (PFHxA) ug/L < 0.01 0.01 Pass

Perfluoroheptanoic acid (PFHpA) ug/L < 0.01 0.01 Pass

Perfluorooctanoic acid (PFOA) ug/L < 0.01 0.01 Pass

Perfluorononanoic acid (PFNA) ug/L < 0.01 0.01 Pass

Perfluorodecanoic acid (PFDA) ug/L < 0.01 0.01 Pass

Perfluoroundecanoic acid (PFUnA) ug/L < 0.01 0.01 Pass

Perfluorododecanoic acid (PFDoA) ug/L < 0.01 0.01 Pass

Perfluorotridecanoic acid (PFTrDA) ug/L < 0.01 0.01 Pass

Perfluorotetradecanoic acid (PFTeDA) ug/L < 0.01 0.01 Pass

Method Blank


Perfluorooctane sulfonamide (FOSA) ug/L < 0.05 0.05 Pass

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) ug/L < 0.05 0.05 Pass

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) ug/L < 0.05 0.05 Pass

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol (N-MeFOSE) ug/L < 0.05 0.05 Pass

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) ug/L < 0.05 0.05 Pass

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) ug/L < 0.05 0.05 Pass

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) ug/L < 0.05 0.05 Pass

Method Blank


Perfluorobutanesulfonic acid (PFBS) ug/L < 0.01 0.01 Pass

Perfluoropentanesulfonic acid (PFPeS) ug/L < 0.01 0.01 Pass

Perfluorohexanesulfonic acid (PFHxS) ug/L < 0.01 0.01 Pass

Perfluoroheptanesulfonic acid (PFHpS) ug/L < 0.01 0.01 Pass

Perfluorooctanesulfonic acid (PFOS) ug/L < 0.01 0.01 Pass

Perfluorodecanesulfonic acid (PFDS) ug/L < 0.01 0.01 Pass

Method Blank


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) ug/L < 0.01 0.01 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) ug/L < 0.05 0.05 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) ug/L < 0.01 0.01 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2 FTS) ug/L < 0.01 0.01 Pass


LimitsPass

LimitsQualifying

Code

Duplicate

Perfluoroalkyl carboxylic acids (PFCAs) Result 1 Result 2 RPD

Perfluorobutanoic acid (PFBA) B17-Oc23380 CP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) B17-Oc23380 CP ug/L 0.02 0.02 5.0 30% Pass

Perfluorononanoic acid (PFNA) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 14 of 16


Duplicate

Perfluoroalkane sulfonamides (PFASAs) Result 1 Result 2 RPD

Perfluorooctane sulfonamide(FOSA) B17-Oc23380 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Oc23380 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Oc23380 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Oc23380 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Oc23380 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Oc23380 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Oc23380 CP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate

Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Result 1 Result 2 RPD

Perfluorobutanesulfonic acid(PFBS) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Oc23380 CP ug/L 0.02 0.02 6.0 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate

n:2 Fluorotelomer sulfonic acids Result 1 Result 2 RPD

1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Oc23380 CP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Oc23380 CP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 15 of 16


Comments



Sample correctly preserved No






Code DescriptionC01 Leachate Fluid Key: 1 - pH 5.0; 2 - pH 2.9; 3 - pH 9.2; 4 - Reagent (DI) water; 5 - Client sample, 6 - other

N09 Quantification of linear and branched isomers has been conducted as a single total response using the relative response factor for the corresponding linear/branched standard.

N11

Isotope dilution is used for calibration of each native compound for which an exact labelled analogue is available (Isotope Dilution Quantitation). The isotopically labelledanalogues allow identification and recovery correction of the concentration of the associated native PFAS compounds. Where the native PFAS compound does not have labelledanalogue then the quantification is made using the Extracted Internal Standard Analyte with the closest retention time to the analyte and no recovery correction has been made(Internal Standard Quantitation).

Authorised By


Jonathon Angell Senior Analyst-Organic (QLD)

Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 16 of 16


https://d1jj3zdoktl3jd.cloudfront.net/apac/media/489918/reporting-measurement-uncertainty-of-chemical-and-microbiology-test-results-september-2017.pdf




Abbotsford

VIC 3067


Report 568586-S





0990_SS129_170712

0990_SS162_170731

0990_SS101_0.0_170706







% Moisture 1 % 2.5 1.7 5.3 28


0990_SS134_170713

0990_SS135_170713

0990_SS202_170929







% Moisture 1 % 1.5 19 11 2.5


0990_SS154_170729

0990_SS122_170712

0990_SS133_170713







% Moisture 1 % 6.0 3.3 20 3.1



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 1 of 10





Sample Matrix Soil




pH (1:5 Aqueous extract) 0.1 pH Units 7.9

Total Organic Carbon 0.1 % 0.7

% Moisture 1 % 12



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 2 of 10





pH (1:5 Aqueous extract) Melbourne Oct 25, 2017 7 Day


Total Organic Carbon Melbourne Oct 26, 2017 28 Day


% Moisture Melbourne Oct 20, 2017 14 Day




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 3 of 10






Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_SS151_170729

Jul 29, 2017 Soil B17-Oc23369 X X X

2 0990_SS151_170729


3 0990_SS129_170712

Jul 12, 2017 Soil B17-Oc23371 X X X

4 0990_SS129_170712


5 0990_SS162_170731

Jul 31, 2017 Soil B17-Oc23373 X X X









ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 4 of 10






Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





170731

7 0990_SS101_0.0_170706

Jul 06, 2017 Soil B17-Oc23375 X X X

8 0990_SS101_0.0_170706


9 0990_SS126_170712

Jul 12, 2017 Soil B17-Oc23377 X X X

10 0990_SS126_170712


11 0990_SS134_170713

Jul 13, 2017 Soil B17-Oc23379 X X X

12 0990_SS134_170713


13 0990_SS135_ Jul 13, 2017 Soil B17-Oc23381 X X X








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 5 of 10






Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





170713

14 0990_SS135_170713


15 0990_SS202_170929

Sep 29, 2017 Soil B17-Oc23383 X X X

16 0990_SS202_170929

Sep 29, 2017 AUS Leachate B17-Oc23384 X X

17 0990_SS192_170822

Aug 22, 2017 Soil B17-Oc23385 X X X

18 0990_SS192_170822


19 0990_SS154_170729

Jul 29, 2017 Soil B17-Oc23387 X X X









ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 6 of 10






Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





170729

21 0990_SS122_170712

Jul 12, 2017 Soil B17-Oc23389 X X X

22 0990_SS122_170712


23 0990_SS133_170713

Jul 13, 2017 Soil B17-Oc23391 X X X

24 0990_SS133_170713


25 0990_SS158_170729

Jul 29, 2017 Soil B17-Oc23393 X X X

26 0990_SS158_170729


Test Counts 13 13 13 13 13








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Page 7 of 10



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















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Page 8 of 10




PassLimits

QualifyingCode

Method Blank


LCS - % Recovery



LimitsPass

LimitsQualifying

Code

Duplicate


pH (1:5 Aqueous extract) M17-Oc22933 NCP pH Units 7.1 7.0 pass 30% Pass

Duplicate


% Moisture B17-Oc23371 CP % 1.7 1.7 <1 30% Pass

Duplicate


Total Organic Carbon B17-Oc23377 CP % 1.3 1.6 19 30% Pass

Duplicate


Total Organic Carbon B17-Oc23393 CP % 0.7 0.6 7.5 30% Pass

% Moisture B17-Oc23393 CP % 12 11 10 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 9 of 10


Comments



Sample correctly preserved No





Authorised By




Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 10 of 10






Abbotsford

VIC 3067


Report 568621-L


Project ID ADDITIONAL ANALYSIS


Client Sample ID 0990_BH119_0.4_170712

0990_QCB114_170712

0990_QCBH116_170712

0990_BH148_0.0_170804



Date Sampled Jul 12, 2017 Jul 12, 2017 Jul 12, 2017 Aug 04, 2017



Perfluorobutanoic acid (PFBA)N11 0.05 ug/L 0.06 0.16 < 0.05 0.12

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L N090.03 N090.16 N090.06 N090.06

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N090.06 N090.36 N090.12 N090.13

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N090.02 N090.09 N090.03 N090.02


Perfluorononanoic acid (PFNA)N11 0.01 ug/L 0.02 N090.03 < 0.01 < 0.01

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L 0.01 N090.04 0.01 < 0.01

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.01 N090.02 < 0.01 < 0.01




13C4-PFBA (surr.) 1 % 126 119 121 122

13C5-PFPeA (surr.) 1 % 93 90 101 96

13C5-PFHxA (surr.) 1 % 68 63 72 64

13C4-PFHpA (surr.) 1 % 94 91 102 88

13C8-PFOA (surr.) 1 % 147 129 162 145

13C5-PFNA (surr.) 1 % 133 120 143 134

13C6-PFDA (surr.) 1 % 121 109 130 116

13C2-PFUnDA (surr.) 1 % 84 80 88 94

13C2-PFDoDA (surr.) 1 % 70 79 89 91

13C2-PFTeDA (surr.) 1 % 24 30 40 30


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L < 0.05 0.16 < 0.05 < 0.05







13C8-FOSA (surr.) 1 % 59 64 64 76

D3-N-MeFOSA (surr.) 1 % 39 47 27 44



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Page 1 of 25





0990_QCB114_170712

0990_QCBH116_170712

0990_BH148_0.0_170804






D5-N-EtFOSA (surr.) 1 % 32 39 25 38

D7-N-MeFOSE (surr.) 1 % 44 58 36 49

D9-N-EtFOSE (surr.) 1 % 35 47 29 40

D5-N-EtFOSAA (surr.) 1 % 64 63 78 71

D3-N-MeFOSAA (surr.) 1 % 75 66 87 91


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L N090.02 N090.07 N090.08 N090.20

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L 0.01 N090.10 N090.11 N090.12


Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01 N090.03 N090.03 < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.12 N091.9 N090.27 N090.11


13C3-PFBS (surr.) 1 % 83 78 82 78

18O2-PFHxS (surr.) 1 % 141 123 136 140

13C8-PFOS (surr.) 1 % 112 80 114 114




1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L < 0.01 < 0.01 0.01 < 0.01


13C2-4:2 FTS (surr.) 1 % 77 70 104 98

13C2-6:2 FTS (surr.) 1 % 124 101 154 135

13C2-8:2 FTS (surr.) 1 % 92 88 122 93

PFASs Summations





Sum of PFASs (n=28) 0.1 ug/L 0.41 4.02 1.28 1.04





pH (off) 0.1 pH Units 6.9 7.1 6.5 7.5



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 2 of 25



0990_BH149_0.5_170808

0990_BH150_0.0_170808

0990_BH175_0.0_170811






Perfluorobutanoic acid (PFBA)N11 0.05 ug/L 0.10 < 0.2 < 0.05 < 0.05

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L N090.10 < 0.2 N090.04 N090.05

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N090.42 < 0.2 N090.25 N090.09

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N090.04 < 0.2 N090.04 N090.02

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N090.05 N09< 0.2 N090.17 N090.07

Perfluorononanoic acid (PFNA)N11 0.01 ug/L < 0.01 N09< 0.2 < 0.01 0.03

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L < 0.01 < 0.2 N090.01 N090.15

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.01 < 0.2 N090.02 N090.07

Perfluorododecanoic acid (PFDoA)N11 0.01 ug/L < 0.01 N09< 0.2 < 0.01 < 0.01



13C4-PFBA (surr.) 1 % 132 131 135 134

13C5-PFPeA (surr.) 1 % 97 133 100 97

13C5-PFHxA (surr.) 1 % 64 106 65 67

13C4-PFHpA (surr.) 1 % 90 121 94 93

13C8-PFOA (surr.) 1 % 124 134 135 135

13C5-PFNA (surr.) 1 % 112 127 129 127

13C6-PFDA (surr.) 1 % 96 126 117 112

13C2-PFUnDA (surr.) 1 % 75 103 96 73

13C2-PFDoDA (surr.) 1 % 67 85 92 70

13C2-PFTeDA (surr.) 1 % 26 15 32 27


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L < 0.05 < 0.2 0.63 0.06







13C8-FOSA (surr.) 1 % 52 107 70 73

D3-N-MeFOSA (surr.) 1 % 26 49 43 36

D5-N-EtFOSA (surr.) 1 % 22 37 38 32

D7-N-MeFOSE (surr.) 1 % 36 53 51 47

D9-N-EtFOSE (surr.) 1 % 27 32 41 36

D5-N-EtFOSAA (surr.) 1 % 63 106 75 65

D3-N-MeFOSAA (surr.) 1 % 73 110 99 77


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L N090.43 < 0.2 N090.03 0.01

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.30 < 0.2 N090.07 N090.02


Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01 N09< 0.2 N090.02 < 0.01



13C3-PFBS (surr.) 1 % 75 110 80 80

18O2-PFHxS (surr.) 1 % 125 142 128 134

13C8-PFOS (surr.) 1 % 86 124 96 107



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 3 of 25



0990_BH149_0.5_170808

0990_BH150_0.0_170808

0990_BH175_0.0_170811








1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L < 0.01 < 0.2 < 0.01 0.01


13C2-4:2 FTS (surr.) 1 % 75 90 75 77

13C2-6:2 FTS (surr.) 1 % 110 100 113 127

13C2-8:2 FTS (surr.) 1 % 81 102 98 84

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 0.35 3.68 1 0.11




Sum of PFASs (n=28) 0.1 ug/L 1.79 3.68 2.28 0.69





pH (off) 0.1 pH Units 8.1 8.5 8.8 8.9


0990_BH164_2.0_170810

0990_BH165_0.0_170810

0990_BH165_1.0_170810






Perfluorobutanoic acid (PFBA)N11 0.05 ug/L < 0.05 < 0.05 0.16 0.54



Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N090.02 < 0.01 N090.13 N090.32


Perfluorononanoic acid (PFNA)N11 0.01 ug/L 0.03 < 0.01 N090.03 N090.02

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L 0.06 < 0.01 0.02 < 0.01

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L N090.02 < 0.01 < 0.01 < 0.01




13C4-PFBA (surr.) 1 % 130 135 128 117

13C5-PFPeA (surr.) 1 % 99 97 93 89

13C5-PFHxA (surr.) 1 % 66 69 62 53

13C4-PFHpA (surr.) 1 % 94 94 91 91

13C8-PFOA (surr.) 1 % 139 141 140 109

13C5-PFNA (surr.) 1 % 124 131 137 129

13C6-PFDA (surr.) 1 % 105 118 123 111

13C2-PFUnDA (surr.) 1 % 72 75 88 81

13C2-PFDoDA (surr.) 1 % 59 71 81 77

13C2-PFTeDA (surr.) 1 % 20 28 26 26



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Page 4 of 25



0990_BH164_2.0_170810

0990_BH165_0.0_170810

0990_BH165_1.0_170810






Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L N090.76 < 0.05 N090.21 < 0.05







13C8-FOSA (surr.) 1 % 58 66 70 58

D3-N-MeFOSA (surr.) 1 % 27 51 54 47

D5-N-EtFOSA (surr.) 1 % 21 44 41 39

D7-N-MeFOSE (surr.) 1 % 37 64 59 50

D9-N-EtFOSE (surr.) 1 % 27 49 46 40

D5-N-EtFOSAA (surr.) 1 % 46 47 53 49

D3-N-MeFOSAA (surr.) 1 % 54 54 58 62


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L < 0.01 < 0.01 N090.23 N091.3

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L < 0.01 < 0.01 0.25 N091.3

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N090.07 0.03 N090.96 N095.2

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01 < 0.01 N090.02 N090.10



13C3-PFBS (surr.) 1 % 81 84 81 66

18O2-PFHxS (surr.) 1 % 139 140 124 90

13C8-PFOS (surr.) 1 % 91 109 101 102




1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L < 0.01 < 0.01 0.02 < 0.01


13C2-4:2 FTS (surr.) 1 % 76 80 84 66

13C2-6:2 FTS (surr.) 1 % 131 111 118 96

13C2-8:2 FTS (surr.) 1 % 94 99 110 102

PFASs Summations





Sum of PFASs (n=28) 0.1 ug/L 1.67 0.4 4.48 14.46





pH (off) 0.1 pH Units 9.3 9.1 8.7 8.5



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Page 5 of 25



0990_BH167_0.0_170810

0990_BH167_1.0_170810

0990_BH167_2.0_170810






Perfluorobutanoic acid (PFBA)N11 0.05 ug/L 1.4 0.40 3.9 7.7


Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N098.2 N092.8 N0929 N0928

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N090.61 N090.97 N094.8 N092.7

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N091.7 N092.3 N0913 N095.9

Perfluorononanoic acid (PFNA)N11 0.01 ug/L N09< 0.2 N090.51 N090.26 N09< 0.2

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L < 0.2 0.13 < 0.2 < 0.2





13C4-PFBA (surr.) 1 % 116 132 129 134

13C5-PFPeA (surr.) 1 % 113 140 130 142

13C5-PFHxA (surr.) 1 % 84 106 105 111

13C4-PFHpA (surr.) 1 % 100 120 120 129

13C8-PFOA (surr.) 1 % 111 127 120 135

13C5-PFNA (surr.) 1 % 112 123 123 131

13C6-PFDA (surr.) 1 % 97 117 106 128

13C2-PFUnDA (surr.) 1 % 65 86 86 95

13C2-PFDoDA (surr.) 1 % 45 58 56 65

13C2-PFTeDA (surr.) 1 % 28 12 INT INT


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L < 0.2 N091.2 N091.1 < 0.2







13C8-FOSA (surr.) 1 % 78 104 109 110

D3-N-MeFOSA (surr.) 1 % 28 42 38 35

D5-N-EtFOSA (surr.) 1 % 25 33 26 24

D7-N-MeFOSE (surr.) 1 % 46 46 42 45

D9-N-EtFOSE (surr.) 1 % 36 29 25 25

D5-N-EtFOSAA (surr.) 1 % 71 87 85 95

D3-N-MeFOSAA (surr.) 1 % 77 94 97 105


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L 2.7 N090.83 5.7 7.6

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N093.5 N091.5 N099.3 N097.6

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N0923 N097.4 N0975 N0941

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N091.2 N09< 0.2 N096.4 N091.6

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N096.9 N092.0 N09210 N095.7


13C3-PFBS (surr.) 1 % 90 113 112 116

18O2-PFHxS (surr.) 1 % 115 134 112 129

13C8-PFOS (surr.) 1 % 101 119 145 126



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 6 of 25



0990_BH167_0.0_170810

0990_BH167_1.0_170810

0990_BH167_2.0_170810







1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 0.05 ug/L 0.22 0.44 0.75 0.25

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L < 0.2 1.8 0.37 < 0.2


13C2-4:2 FTS (surr.) 1 % 86 91 87 95

13C2-6:2 FTS (surr.) 1 % 94 98 92 100

13C2-8:2 FTS (surr.) 1 % 84 101 101 102

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 29.9 9.4 285 46.7

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 8.6 4.3 223 11.6

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L 31.6 11.7 298 52.6


Sum of PFASs (n=28) 0.1 ug/L 51.23 23.03 364.78 115.45





pH (off) 0.1 pH Units 8.4 8.5 8.4 8.6


0990_BH171_0.5_170811

0990_BH173_0.5_170811

0990_BH193_0.5_170815







Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L 0.03 N090.01 < 0.01 N090.03


Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N090.01 N090.01 < 0.01 < 0.01


Perfluorononanoic acid (PFNA)N11 0.01 ug/L N090.02 < 0.01 < 0.01 < 0.01






13C4-PFBA (surr.) 1 % 130 134 130 129

13C5-PFPeA (surr.) 1 % 92 96 90 93

13C5-PFHxA (surr.) 1 % 65 69 65 64

13C4-PFHpA (surr.) 1 % 94 100 96 94

13C8-PFOA (surr.) 1 % 143 142 142 144

13C5-PFNA (surr.) 1 % 141 129 129 140

13C6-PFDA (surr.) 1 % 118 104 108 121

13C2-PFUnDA (surr.) 1 % 82 79 70 83

13C2-PFDoDA (surr.) 1 % 79 73 62 79

13C2-PFTeDA (surr.) 1 % 29 29 20 25



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 7 of 25



0990_BH171_0.5_170811

0990_BH173_0.5_170811

0990_BH193_0.5_170815






Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L N090.05 < 0.05 < 0.05 < 0.05







13C8-FOSA (surr.) 1 % 70 61 54 75

D3-N-MeFOSA (surr.) 1 % 45 38 26 48

D5-N-EtFOSA (surr.) 1 % 39 31 19 39

D7-N-MeFOSE (surr.) 1 % 59 52 36 58

D9-N-EtFOSE (surr.) 1 % 46 40 28 44

D5-N-EtFOSAA (surr.) 1 % 54 54 44 49

D3-N-MeFOSAA (surr.) 1 % 63 68 54 59


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L 0.03 0.01 0.01 < 0.01


Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.21 < 0.01 N090.04 N090.02


13C3-PFBS (surr.) 1 % 83 85 83 81

18O2-PFHxS (surr.) 1 % 141 141 142 143

13C8-PFOS (surr.) 1 % 113 97 101 112






13C2-4:2 FTS (surr.) 1 % 73 73 71 67

13C2-6:2 FTS (surr.) 1 % 114 116 112 121

13C2-8:2 FTS (surr.) 1 % 97 97 90 99

PFASs Summations





Sum of PFASs (n=28) 0.1 ug/L 0.41 < 0.1 0.1 0.12





pH (off) 0.1 pH Units 8.8 8.4 9.1 8.9



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 8 of 25



0990_BH195_1.0_170824

Sample Matrix AUS Leachate AUS Leachate

Eurofins | mgt Sample No. B17-Oc23881 B17-Oc23883

Date Sampled Aug 24, 2017 Aug 24, 2017



Perfluorobutanoic acid (PFBA)N11 0.05 ug/L < 0.05 < 0.05

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L N090.03 N090.03

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N090.04 N090.05

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L < 0.01 N090.01

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N090.02 N090.05

Perfluorononanoic acid (PFNA)N11 0.01 ug/L < 0.01 < 0.01

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L < 0.01 < 0.01

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.01 < 0.01

Perfluorododecanoic acid (PFDoA)N11 0.01 ug/L < 0.01 < 0.01

Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L < 0.01 < 0.01

Perfluorotetradecanoic acid (PFTeDA)N11 0.01 ug/L < 0.01 < 0.01

13C4-PFBA (surr.) 1 % 126 146

13C5-PFPeA (surr.) 1 % 95 102

13C5-PFHxA (surr.) 1 % 67 73

13C4-PFHpA (surr.) 1 % 95 103

13C8-PFOA (surr.) 1 % 145 146

13C5-PFNA (surr.) 1 % 134 132

13C6-PFDA (surr.) 1 % 119 117

13C2-PFUnDA (surr.) 1 % 88 74

13C2-PFDoDA (surr.) 1 % 79 71

13C2-PFTeDA (surr.) 1 % 27 29


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L < 0.05 < 0.05

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA)N11 0.05 ug/L < 0.05 < 0.05

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA)N11 0.05 ug/L < 0.05 < 0.05

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE)N11 0.05 ug/L < 0.05 < 0.05

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE)N11 0.05 ug/L < 0.05 < 0.05

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA)N11 0.05 ug/L < 0.05 < 0.05

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA)N11 0.05 ug/L < 0.05 < 0.05

13C8-FOSA (surr.) 1 % 68 60

D3-N-MeFOSA (surr.) 1 % 43 47

D5-N-EtFOSA (surr.) 1 % 33 40

D7-N-MeFOSE (surr.) 1 % 62 54

D9-N-EtFOSE (surr.) 1 % 47 42

D5-N-EtFOSAA (surr.) 1 % 47 52

D3-N-MeFOSAA (surr.) 1 % 56 61


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L < 0.01 0.01

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L < 0.01 0.01

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L 0.01 0.10

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01 < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N090.05 N090.03

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.01 < 0.01

13C3-PFBS (surr.) 1 % 83 91

18O2-PFHxS (surr.) 1 % 142 142

13C8-PFOS (surr.) 1 % 118 98



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 9 of 25



0990_BH195_1.0_170824






1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS)N11 0.01 ug/L < 0.01 < 0.01

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 0.05 ug/L < 0.05 < 0.05

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L < 0.01 < 0.01

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 0.01 ug/L < 0.01 < 0.01

13C2-4:2 FTS (surr.) 1 % 77 82

13C2-6:2 FTS (surr.) 1 % 118 140

13C2-8:2 FTS (surr.) 1 % 105 106

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 0.06 0.13

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 0.07 0.08

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L 0.08 0.18

Sum of WA DER PFAS (n=10) 0.05 ug/L 0.15 0.28

Sum of PFASs (n=28) 0.1 ug/L 0.15 0.29


Leachate FluidC01 comment 4.0 4.0

pH (initial) 0.1 pH Units 7.8 7.8

pH (Leachate fluid) 0.1 pH Units 7.0 7.0

pH (off) 0.1 pH Units 8.7 8.6



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 10 of 25






Perfluoroalkyl carboxylic acids (PFCAs) Brisbane Oct 23, 2017 14 Day


Perfluoroalkane sulfonamides (PFASAs) Brisbane Oct 23, 2017 14 Day


Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Brisbane Oct 23, 2017 14 Day


n:2 Fluorotelomer sulfonic acids Brisbane Oct 23, 2017 14 Day


AUS Leaching Procedure Brisbane Oct 23, 2017 7 Days




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 11 of 25




Project Name: DOD TINDALProject ID: ADDITIONAL ANALYSIS


Sample Detail

% C

lay

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)

Melbourne Laboratory - NATA Site # 1254 & 14271 X X


Brisbane Laboratory - NATA Site # 20794 X X X X


External Laboratory


Matrix LAB ID

1 0990_BH119_0.4_170712

Jul 12, 2017 Soil B17-Oc23840 X X X X

2 0990_BH119_0.4_170712


3 0990_QCBH114_170712

Jul 12, 2017 Soil B17-Oc23842 X X X X

4 0990_QCB114_170712


5 0990_QCBH116_170712

Jul 12, 2017 Soil B17-Oc23844 X X X X

6 0990_QCBH1 Jul 12, 2017 AUS Leachate B17-Oc23845 X X








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 12 of 25






Sample Detail

% C

lay

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





16_170712

7 0990_BH148_0.0_170804

Aug 04, 2017 Soil B17-Oc23846 X X X X

8 0990_BH148_0.0_170804


9 0990_BH148_0.4_170804

Aug 04, 2017 Soil B17-Oc23848 X X X X

10 0990_BH148_0.4_170804


11 0990_BH149_0.5_170808

Aug 04, 2017 Soil B17-Oc23850 X X X X

12 0990_BH149_0.5_170808


13 0990_BH150_ Aug 08, 2017 Soil B17-Oc23852 X X X X








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 13 of 25






Sample Detail

% C

lay

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





0.0_170808

14 0990_BH150_0.0_170808


15 0990_BH175_0.0_170811

Aug 11, 2017 Soil B17-Oc23854 X X X X

16 0990_BH175_0.0_170811


17 0990_BH175_0.2_170811

Aug 11, 2017 Soil B17-Oc23856 X X X X

18 0990_BH175_0.2_170811


19 0990_BH164_2.0_170810

Aug 10, 2017 Soil B17-Oc23858 X X X X

20 0990_BH164_ Aug 10, 2017 AUS Leachate B17-Oc23859 X X








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 14 of 25






Sample Detail

% C

lay

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





2.0_170810

21 0990_BH165_0.0_170810

Aug 10, 2017 Soil B17-Oc23860 X X X X

22 0990_BH165_0.0_170810


23 0990_BH165_1.0_170810

Aug 10, 2017 Soil B17-Oc23862 X X X X

24 0990_BH165_1.0_170810


25 0990_BH165_2.0_170810

Aug 10, 2017 Soil B17-Oc23864 X X X X

26 0990_BH165_2.0_170810










ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 15 of 25






Sample Detail

% C

lay

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





0.0_170810

28 0990_BH167_0.0_170810


29 0990_BH167_1.0_170810

Aug 10, 2017 Soil B17-Oc23868 X X X X

30 0990_BH167_1.0_170810


31 0990_BH167_2.0_170810

Aug 10, 2017 Soil B17-Oc23870 X X X X

32 0990_BH167_2.0_170810


33 0990_BH169_1.0_170810

Aug 10, 2017 Soil B17-Oc23872 X X X X









ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 16 of 25






Sample Detail

% C

lay

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





1.0_170810

35 0990_BH171_0.5_170811

Aug 11, 2017 Soil B17-Oc23874 X X X X

36 0990_BH171_0.5_170811


37 0990_BH173_0.5_170811

Aug 11, 2017 Soil B17-Oc23876 X X X X

38 0990_BH173_0.5_170811


39 0990_BH193_0.5_170815

Aug 15, 2017 Soil B17-Oc23878 X X X X

40 0990_BH193_0.5_170815










ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 17 of 25






Sample Detail

% C

lay

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





0.5_170824

42 0990_BH194_0.5_170824


43 0990_BH195_1.0_170824

Aug 24, 2017 Soil B17-Oc23882 X X X X

44 0990_BH195_1.0_170824


Test Counts 22 22 22 22 22 22








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 18 of 25



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 19 of 25




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank







LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) B17-Oc23843 CP ug/L 0.16 0.17 1.0 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Oc23843 CP ug/L 0.16 0.16 <1 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Oc23843 CP ug/L 0.36 0.36 1.0 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Oc23843 CP ug/L 0.09 0.09 <1 30% Pass


Perfluorononanoic acid (PFNA) B17-Oc23843 CP ug/L 0.03 0.03 13 30% Pass

Perfluorodecanoic acid (PFDA) B17-Oc23843 CP ug/L 0.04 0.04 7.0 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Oc23843 CP ug/L 0.02 0.02 6.0 30% Pass






ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 20 of 25


Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Oc23843 CP ug/L 0.16 0.13 23 30% Pass







Duplicate


Perfluorobutanesulfonic acid(PFBS) B17-Oc23843 CP ug/L 0.07 0.07 4.0 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Oc23843 CP ug/L 0.10 0.10 1.0 30% Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Oc23843 CP ug/L 0.60 0.52 14 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Oc23843 CP ug/L 0.03 0.02 18 30% Pass

Perfluorooctanesulfonic acid(PFOS) B17-Oc23843 CP ug/L 1.9 1.5 22 30% Pass


Duplicate






Duplicate



Perfluoropentanoic acid (PFPeA) B17-Oc23855 CP ug/L 0.05 0.05 7.0 30% Pass


Perfluoroheptanoic acid (PFHpA) B17-Oc23855 CP ug/L 0.02 0.02 7.0 30% Pass


Perfluorononanoic acid (PFNA) B17-Oc23855 CP ug/L 0.03 0.02 5.0 30% Pass

Perfluorodecanoic acid (PFDA) B17-Oc23855 CP ug/L 0.15 0.14 11 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Oc23855 CP ug/L 0.07 0.06 13 30% Pass






ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 21 of 25


Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Oc23855 CP ug/L 0.06 0.06 1.0 30% Pass







Duplicate


Perfluorobutanesulfonic acid(PFBS) B17-Oc23855 CP ug/L 0.01 0.01 1.0 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Oc23855 CP ug/L 0.02 0.02 3.0 30% Pass



Perfluorooctanesulfonic acid(PFOS) B17-Oc23855 CP ug/L 0.04 0.03 26 30% Pass


Duplicate




1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Oc23855 CP ug/L 0.01 0.01 3.0 30% Pass


Duplicate



Perfluoropentanoic acid (PFPeA) B17-Oc23857 CP ug/L 0.03 0.03 3.0 30% Pass



Perfluorooctanoic acid (PFOA) B17-Oc23857 CP ug/L 0.05 0.05 <1 30% Pass

Perfluorononanoic acid (PFNA) B17-Oc23857 CP ug/L 0.03 0.02 6.0 30% Pass

Perfluorodecanoic acid (PFDA) B17-Oc23857 CP ug/L 0.06 0.07 2.0 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Oc23857 CP ug/L 0.02 0.02 1.0 30% Pass






ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 22 of 25


Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Oc23857 CP ug/L 0.76 0.71 7.0 30% Pass







Duplicate




Perfluorohexanesulfonic acid(PFHxS) B17-Oc23857 CP ug/L 0.07 0.08 8.0 30% Pass


Perfluorooctanesulfonic acid(PFOS) B17-Oc23857 CP ug/L 0.57 0.56 2.0 30% Pass


Duplicate






Duplicate



Perfluoropentanoic acid (PFPeA) B17-Oc23875 CP ug/L 0.01 0.02 10 30% Pass




Perfluorononanoic acid (PFNA) B17-Oc23875 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) B17-Oc23875 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Oc23875 CP ug/L < 0.01 < 0.01 <1 30% Pass






ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 23 of 25


Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Oc23875 CP ug/L < 0.05 < 0.05 <1 30% Pass







Duplicate






Perfluorooctanesulfonic acid(PFOS) B17-Oc23875 CP ug/L < 0.01 < 0.01 <1 30% Pass


Duplicate








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 24 of 25


Comments











N11


Authorised By



Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 25 of 25






Abbotsford

VIC 3067


Report 568621-S


Project ID ADDITIONAL ANALYSIS



0990_QCBH114_170712

0990_QCBH116_170712

0990_BH148_0.0_170804





% Clay 1 % 5.0 21 5.3 20



% Moisture 1 % < 1 10 19 5.1


0990_BH149_0.5_170808

0990_BH150_0.0_170808

0990_BH175_0.0_170811





% Clay 1 % 24 < 1 6.8 6.2


Total Organic Carbon 0.1 % 0.4 < 0.1 0.4 1.5

% Moisture 1 % 8.8 6.6 1.3 1.3


0990_BH164_2.0_170810

0990_BH165_0.0_170810

0990_BH165_1.0_170810





% Clay 1 % 14 11 13 14


Total Organic Carbon 0.1 % 1.8 < 0.1 0.1 < 0.1

% Moisture 1 % 2.6 12 5.1 8.4



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 1 of 13





0990_BH167_0.0_170810

0990_BH167_1.0_170810

0990_BH167_2.0_170810





% Clay 1 % 53 14 55 41


Total Organic Carbon 0.1 % 0.4 1.4 < 0.1 < 0.1

% Moisture 1 % 18 2.8 11 14


0990_BH171_0.5_170811

0990_BH173_0.5_170811

0990_BH193_0.5_170815





% Clay 1 % 14 29 < 1 9.9


Total Organic Carbon 0.1 % < 0.1 < 0.1 < 0.1 0.3

% Moisture 1 % 7.6 9.6 1.6 7.5


0990_BH195_1.0_170824

Sample Matrix Soil Soil




% Clay 1 % 21 28

pH (1:5 Aqueous extract) 0.1 pH Units 8.1 8.0

Total Organic Carbon 0.1 % 0.3 < 0.1

% Moisture 1 % 7.0 9.2



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 2 of 13





% Clay Brisbane Oct 23, 2017 6 Day

- Method: LTM-GEN-7040

pH (1:5 Aqueous extract) Melbourne Oct 23, 2017 7 Day


Total Organic Carbon Melbourne Oct 23, 2017 28 Day


% Moisture Melbourne Oct 20, 2017 14 Day




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 3 of 13






Sample Detail

% C

lay

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_BH119_0.4_170712

Jul 12, 2017 Soil B17-Oc23840 X X X X

2 0990_BH119_0.4_170712


3 0990_QCBH114_170712

Jul 12, 2017 Soil B17-Oc23842 X X X X

4 0990_QCB114_170712


5 0990_QCBH116_170712

Jul 12, 2017 Soil B17-Oc23844 X X X X

6 0990_QCBH1 Jul 12, 2017 AUS Leachate B17-Oc23845 X X








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 4 of 13






Sample Detail

% C

lay

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





16_170712

7 0990_BH148_0.0_170804

Aug 04, 2017 Soil B17-Oc23846 X X X X

8 0990_BH148_0.0_170804


9 0990_BH148_0.4_170804

Aug 04, 2017 Soil B17-Oc23848 X X X X

10 0990_BH148_0.4_170804


11 0990_BH149_0.5_170808

Aug 04, 2017 Soil B17-Oc23850 X X X X

12 0990_BH149_0.5_170808










ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 5 of 13






Sample Detail

% C

lay

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





0.0_170808

14 0990_BH150_0.0_170808


15 0990_BH175_0.0_170811

Aug 11, 2017 Soil B17-Oc23854 X X X X

16 0990_BH175_0.0_170811


17 0990_BH175_0.2_170811

Aug 11, 2017 Soil B17-Oc23856 X X X X

18 0990_BH175_0.2_170811


19 0990_BH164_2.0_170810

Aug 10, 2017 Soil B17-Oc23858 X X X X









ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 6 of 13






Sample Detail

% C

lay

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





2.0_170810

21 0990_BH165_0.0_170810

Aug 10, 2017 Soil B17-Oc23860 X X X X

22 0990_BH165_0.0_170810


23 0990_BH165_1.0_170810

Aug 10, 2017 Soil B17-Oc23862 X X X X

24 0990_BH165_1.0_170810


25 0990_BH165_2.0_170810

Aug 10, 2017 Soil B17-Oc23864 X X X X

26 0990_BH165_2.0_170810










ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 7 of 13






Sample Detail

% C

lay

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





0.0_170810

28 0990_BH167_0.0_170810


29 0990_BH167_1.0_170810

Aug 10, 2017 Soil B17-Oc23868 X X X X

30 0990_BH167_1.0_170810


31 0990_BH167_2.0_170810

Aug 10, 2017 Soil B17-Oc23870 X X X X

32 0990_BH167_2.0_170810


33 0990_BH169_1.0_170810

Aug 10, 2017 Soil B17-Oc23872 X X X X









ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 8 of 13






Sample Detail

% C

lay

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





1.0_170810

35 0990_BH171_0.5_170811

Aug 11, 2017 Soil B17-Oc23874 X X X X

36 0990_BH171_0.5_170811


37 0990_BH173_0.5_170811

Aug 11, 2017 Soil B17-Oc23876 X X X X

38 0990_BH173_0.5_170811


39 0990_BH193_0.5_170815

Aug 15, 2017 Soil B17-Oc23878 X X X X

40 0990_BH193_0.5_170815










ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 9 of 13






Sample Detail

% C

lay

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





0.5_170824

42 0990_BH194_0.5_170824


43 0990_BH195_1.0_170824

Aug 24, 2017 Soil B17-Oc23882 X X X X

44 0990_BH195_1.0_170824


Test Counts 22 22 22 22 22 22








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 10 of 13



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 11 of 13




PassLimits

QualifyingCode

Method Blank

% Clay % < 1 1 Pass


LCS - % Recovery

% Clay % 89 70-130 Pass



LimitsPass

LimitsQualifying

Code

Duplicate


Total Organic Carbon B17-Oc23876 CP % < 0.1 < 0.1 <1 30% Pass

Duplicate


pH (1:5 Aqueous extract) B17-Oc23878 CP pH Units 8.4 8.3 pass 30% Pass

Duplicate


% Clay B17-Oc23880 CP % 21 23 6.0 30% Pass

Duplicate


% Clay B17-Oc23882 CP % 28 26 5.0 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 12 of 13


Comments








Authorised By




Jonathon Angell Senior Analyst-Inorganic (QLD)

Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 13 of 13





3G Marine Pde

Abbotsford

VIC 3067


Report 557977-L

Project name ADDITIONAL ANALYSIS: DOD TINDAL

Project ID 754_MELEN199420

Received Date Aug 10, 2017

Client Sample ID0990_BH115_0.0_170712(JL20193)

0990_BH115_0.5_170712(JL20194)

0990_BH117_1.5_170713(JL20200)

0990_SS127_170712(JL20201)


Eurofins | mgt Sample No. B17-Au12519 B17-Au12520 B17-Au12521 B17-Au12522




Perfluorobutanoic acid (PFBA)N11 0.05 ug/L 95 3.6 0.22 0.30

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L N09390 N0914 N090.58 0.48

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N092800 N09100 N092.2 N091.1

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N09160 N0923 N090.33 N090.41

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N09130 N0942 N091.00 N091.4

Perfluorononanoic acid (PFNA)N11 0.01 ug/L < 0.2 < 0.2 N090.05 N091.1

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L < 0.2 < 0.2 0.02 2.2

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.2 < 0.2 < 0.01 0.21




13C4-PFBA (surr.) 1 % 42 71 141 73

13C5-PFPeA (surr.) 1 % 50 62 118 65

13C5-PFHxA (surr.) 1 % 55 68 104 82

13C4-PFHpA (surr.) 1 % 32 65 96 73

13C8-PFOA (surr.) 1 % 37 65 130 76

13C5-PFNA (surr.) 1 % 34 55 125 58

13C6-PFDA (surr.) 1 % 37 54 57 66

13C2-PFUnDA (surr.) 1 % 42 70 79 72

13C2-PFDoDA (surr.) 1 % 44 64 105 80

13C2-PFTeDA (surr.) 1 % 11 15 70 24


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L < 0.2 < 0.2 < 0.05 0.25







13C8-FOSA (surr.) 1 % 47 79 107 80

D3-N-MeFOSA (surr.) 1 % 32 47 71 51

Date Reported: Aug 21, 2017


ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 1 of 15





0990_BH115_0.5_170712(JL20194)

0990_BH117_1.5_170713(JL20200)

0990_SS127_170712(JL20201)






D5-N-EtFOSA (surr.) 1 % 18 26 42 28

D7-N-MeFOSE (surr.) 1 % 34 50 60 54

D9-N-EtFOSE (surr.) 1 % 28 42 66 49

D5-N-EtFOSAA (surr.) 1 % 40 66 77 68

D3-N-MeFOSAA (surr.) 1 % 40 68 88 74


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L N091400 N0948 0.63 < 0.2

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N09920 N0969 N090.67 < 0.2

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N09610 N09450 N093.4 N091.4

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N0939 N0953 N090.28 N091.2

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N0949 N09100 N0996 N09110

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.2 < 0.2 N090.05 N090.58

13C3-PFBS (surr.) 1 % 46 59 90 69

18O2-PFHxS (surr.) 1 % 62 98 92 88

13C8-PFOS (surr.) 1 % 48 75 73 89



1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 0.05 ug/L 1.5 0.86 < 0.05 < 0.2

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L < 0.2 < 0.2 0.07 16


13C2-4:2 FTS (surr.) 1 % 27 47 198 52

13C2-6:2 FTS (surr.) 1 % 28 44 113 50

13C2-8:2 FTS (surr.) 1 % 27 41 73 48

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 659 550 99.4 111.4

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 179 142 97 111.4

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L 789 592 100.4 112.8


Sum of PFASs (n=28) 0.1 ug/L 6594.5 903.46 105.5 136.63





pH (off) 0.1 pH Units 8.9 8.8 9.1 8.5



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 2 of 15



0990_BH123_0.2_170713(JL20209)

0990_SS130_170712(JL20216)

0990_SS131_170712(JL20217)






Perfluorobutanoic acid (PFBA)N11 0.05 ug/L < 0.05 0.08 < 0.05 0.06

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L 0.01 N090.08 N090.01 N090.09

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L 0.03 N090.13 N090.02 N090.20

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L < 0.01 N090.02 < 0.01 N090.04


Perfluorononanoic acid (PFNA)N11 0.01 ug/L N090.01 < 0.01 0.03 0.10

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 0.05

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 0.01




13C4-PFBA (surr.) 1 % 141 141 146 133

13C5-PFPeA (surr.) 1 % 122 121 127 119

13C5-PFHxA (surr.) 1 % 136 131 135 129

13C4-PFHpA (surr.) 1 % 93 108 101 97

13C8-PFOA (surr.) 1 % 137 125 126 134

13C5-PFNA (surr.) 1 % 117 106 108 110

13C6-PFDA (surr.) 1 % 91 81 85 78

13C2-PFUnDA (surr.) 1 % 81 76 73 81

13C2-PFDoDA (surr.) 1 % 83 84 71 96

13C2-PFTeDA (surr.) 1 % 58 50 54 58


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05 0.06







13C8-FOSA (surr.) 1 % 102 89 97 105

D3-N-MeFOSA (surr.) 1 % 47 51 49 52

D5-N-EtFOSA (surr.) 1 % 27 32 30 31

D7-N-MeFOSE (surr.) 1 % 49 43 36 53

D9-N-EtFOSE (surr.) 1 % 51 55 49 58

D5-N-EtFOSAA (surr.) 1 % 72 62 63 67

D3-N-MeFOSAA (surr.) 1 % 75 73 66 77


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L < 0.01 0.01 0.01 0.08

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L < 0.01 N090.01 < 0.01 N090.07


Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L < 0.01 N090.03 < 0.01 N090.09

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N091.1 N090.92 N090.64 N0914

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.01 < 0.01 < 0.01 N090.17

13C3-PFBS (surr.) 1 % 97 103 101 99

18O2-PFHxS (surr.) 1 % 153 143 143 134

13C8-PFOS (surr.) 1 % 83 81 83 106



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 3 of 15



0990_BH123_0.2_170713(JL20209)

0990_SS130_170712(JL20216)

0990_SS131_170712(JL20217)








1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L 0.01 < 0.01 < 0.01 0.07


13C2-4:2 FTS (surr.) 1 % 194 168 186 199

13C2-6:2 FTS (surr.) 1 % 116 109 105 120

13C2-8:2 FTS (surr.) 1 % 75 62 61 77

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 1.13 1 0.67 14.55




Sum of PFASs (n=28) 0.1 ug/L 1.23 1.43 0.76 15.78





pH (off) 0.1 pH Units 7.6 7.2 7.0 5.6

Client Sample ID0990_MW104_1.0_170719(JL27865)

0990_MW105_0.4_170719(JL27867)

0990_SS125_170711(JL16783)

Sample Matrix AUS Leachate AUS Leachate AUS Leachate

Eurofins | mgt Sample No. B17-Au12527 B17-Au12528 B17-Au12529

Date Sampled Jul 19, 2017 Jul 19, 2017 Jul 12, 2017



Perfluorobutanoic acid (PFBA)N11 0.05 ug/L 0.08 < 0.05 < 0.05

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L 0.05 0.04 < 0.01

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N090.12 N090.11 < 0.01

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N090.02 N090.02 < 0.01

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N090.13 N090.09 < 0.01

Perfluorononanoic acid (PFNA)N11 0.01 ug/L N090.01 < 0.01 < 0.01

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorododecanoic acid (PFDoA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L < 0.01 < 0.01 < 0.01

Perfluorotetradecanoic acid (PFTeDA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

13C4-PFBA (surr.) 1 % 144 139 145

13C5-PFPeA (surr.) 1 % 127 129 119

13C5-PFHxA (surr.) 1 % 133 108 132

13C4-PFHpA (surr.) 1 % 100 113 98

13C8-PFOA (surr.) 1 % 132 114 119

13C5-PFNA (surr.) 1 % 117 119 100

13C6-PFDA (surr.) 1 % 81 99 82



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 4 of 15



0990_MW105_0.4_170719(JL27867)

0990_SS125_170711(JL16783)






13C2-PFUnDA (surr.) 1 % 82 100 76

13C2-PFDoDA (surr.) 1 % 86 93 79

13C2-PFTeDA (surr.) 1 % 69 64 54


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

13C8-FOSA (surr.) 1 % 107 106 88

D3-N-MeFOSA (surr.) 1 % 56 66 46

D5-N-EtFOSA (surr.) 1 % 32 37 26

D7-N-MeFOSE (surr.) 1 % 40 50 47

D9-N-EtFOSE (surr.) 1 % 57 60 49

D5-N-EtFOSAA (surr.) 1 % 68 77 65

D3-N-MeFOSAA (surr.) 1 % 71 80 70


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L 0.05 < 0.01 < 0.01

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N090.05 < 0.01 < 0.01

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N090.49 N090.07 N090.04

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N090.04 0.03 < 0.01

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N0925 N093.7 N090.40

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L < 0.01 < 0.01 < 0.01

13C3-PFBS (surr.) 1 % 101 103 98

18O2-PFHxS (surr.) 1 % 135 149 139

13C8-PFOS (surr.) 1 % 86 79 86


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 0.05 ug/L < 0.05 < 0.05 < 0.05

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 0.01 ug/L < 0.01 < 0.01 < 0.01

13C2-4:2 FTS (surr.) 1 % 186 201 184

13C2-6:2 FTS (surr.) 1 % 114 144 99

13C2-8:2 FTS (surr.) 1 % 72 125 65

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 25.49 3.77 0.44

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 25.13 3.79 0.4

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L 25.62 3.86 0.44

Sum of WA DER PFAS (n=10) 0.05 ug/L 25.94 4.03 0.44

Sum of PFASs (n=28) 0.1 ug/L 26.04 4.06 0.44



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 5 of 15



0990_MW105_0.4_170719(JL27867)

0990_SS125_170711(JL16783)






Leachate FluidC01 comment 4.0 4.0 4.0

pH (initial) 0.1 pH Units 7.3 7.2 7.5

pH (Leachate fluid) 0.1 pH Units 7.0 7.0 7.0

pH (off) 0.1 pH Units 6.5 6.4 8.3



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 6 of 15






Perfluoroalkyl carboxylic acids (PFCAs) Brisbane Aug 17, 2017 14 Day


Perfluoroalkane sulfonamides (PFASAs) Brisbane Aug 17, 2017 14 Day


Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Brisbane Aug 17, 2017 14 Day


n:2 Fluorotelomer sulfonic acids Brisbane Aug 17, 2017 14 Day


AUS Leaching Procedure Brisbane Aug 17, 2017 7 Days




ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 7 of 15


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Aug 10, 2017 9:00 AMAddress: 3G Marine Pde Report #: 557977 Due: Aug 17, 2017


Project Name: ADDITIONAL ANALYSIS: DOD TINDALProject ID: 754_MELEN199420


Sample Detail

AU

S Leaching P

rocedure

Per- and P


ubstances(P

FA

Ss)

Melbourne Laboratory - NATA Site # 1254 & 14271




External Laboratory


Matrix LAB ID

1 0990_BH115_0.0_170712(JL20193)

Jul 12, 2017 AUS Leachate B17-Au12519X X

2 0990_BH115_0.5_170712(JL20194)


3 0990_BH117_1.5_170713(JL20200)


4 0990_SS127_170712(JL20201)







Date Reported:Aug 21, 2017


ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 8 of 15


Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Aug 10, 2017 9:00 AMAddress: 3G Marine Pde Report #: 557977 Due: Aug 17, 2017




Sample Detail

AU

S Leaching P

rocedure

Per- and P


ubstances(P

FA

Ss)





5 0990_BH121_0.2_170713(JL20205)


6 0990_BH123_0.2_170713(JL20209)


7 0990_SS130_170712(JL20216)


8 0990_SS131_170712(JL20217)


9 0990_MW104_1.0_170719(JL27865)









ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 9 of 15






Sample Detail

AU

S Leaching P

rocedure

Per- and P


ubstances(P

FA

Ss)





10 0990_MW105_0.4_170719(JL27867)


11 0990_SS125_170711(JL16783)


Test Counts 11 11








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 10 of 15



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 11 of 15




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank







LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) B17-Au12523 CP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Au12523 CP ug/L 0.01 0.01 8.0 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Au12523 CP ug/L 0.03 0.03 11 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Au12523 CP ug/L < 0.01 0.01 3.0 30% Pass

Perfluorooctanoic acid (PFOA) B17-Au12523 CP ug/L 0.04 0.04 11 30% Pass

Perfluorononanoic acid (PFNA) B17-Au12523 CP ug/L 0.01 0.01 14 30% Pass

Perfluorodecanoic acid (PFDA) B17-Au12523 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Au12523 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) B17-Au12523 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) B17-Au12523 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Au12523 CP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 12 of 15


Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Au12523 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Au12523 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Au12523 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Au12523 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Au12523 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Au12523 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Au12523 CP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) B17-Au12523 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Au12523 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Au12523 CP ug/L 0.03 0.03 7.0 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Au12523 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) B17-Au12523 CP ug/L 1.1 1.3 15 30% Pass

Perfluorodecanesulfonic acid(PFDS) B17-Au12523 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Au12523 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Au12523 CP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Au12523 CP ug/L 0.01 0.02 35 30% Fail Q15

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Au12523 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


Perfluorobutanoic acid (PFBA) B17-Au12529 CP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanoic acid (PFOA) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorononanoic acid (PFNA) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorodecanoic acid (PFDA) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 13 of 15


Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Au12529 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Au12529 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Au12529 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Au12529 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Au12529 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Au12529 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Au12529 CP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Au12529 CP ug/L 0.04 0.04 2.0 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) B17-Au12529 CP ug/L 0.40 0.41 2.0 30% Pass

Perfluorodecanesulfonic acid(PFDS) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Au12529 CP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Au12529 CP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 14 of 15


Comments











N11


Q15 The RPD reported passes Eurofins | mgt's QC - Acceptance Criteria as defined in the Internal Quality Control Review and Glossary page of this report.

Authorised By



Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 15 of 15





3G Marine Pde

Abbotsford

VIC 3067


Report 558047-L

Project name ADDITIONAL ANALYSIS: DOD TINDAL

Project ID 754_MELEN199420


Client Sample ID0990_SS113_170711(JL16771)

0990_SS114_170711(JL16772)

0990_SS116_170711(JL16780)






Perfluorobutanoic acid (PFBA)N11 0.05 ug/L 5.4 4.9 7.2

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L N0918 N0915 N0911

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N0981 N0948 N0918

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N09370 N0934 N0917

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N091100 N09140 N0928

Perfluorononanoic acid (PFNA)N11 0.01 ug/L 490 100 36

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L 71 4.3 7.9

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L 21 < 2 0.56

Perfluorododecanoic acid (PFDoA)N11 0.01 ug/L 5.5 < 2 0.45

Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L < 2 < 2 0.22

Perfluorotetradecanoic acid (PFTeDA)N11 0.01 ug/L < 2 < 2 0.60

13C4-PFBA (surr.) 1 % 78 85 91

13C5-PFPeA (surr.) 1 % 70 76 82

13C5-PFHxA (surr.) 1 % 88 97 107

13C4-PFHpA (surr.) 1 % 63 79 92

13C8-PFOA (surr.) 1 % 64 84 97

13C5-PFNA (surr.) 1 % 55 70 78

13C6-PFDA (surr.) 1 % 50 70 92

13C2-PFUnDA (surr.) 1 % 75 88 96

13C2-PFDoDA (surr.) 1 % 83 96 92

13C2-PFTeDA (surr.) 1 % 75 84 21


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L 16 < 2 0.46

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA)N11 0.05 ug/L < 2 < 2 < 0.2

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA)N11 0.05 ug/L < 2 < 2 < 0.2

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE)N11 0.05 ug/L < 2 < 2 < 0.2

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE)N11 0.05 ug/L < 2 < 2 < 0.2

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA)N11 0.05 ug/L < 2 < 2 < 0.2

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA)N11 0.05 ug/L < 2 < 2 < 0.2

13C8-FOSA (surr.) 1 % 86 93 119

D3-N-MeFOSA (surr.) 1 % 62 75 68



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 1 of 8




Client Sample ID0990_SS113_170711(JL16771)

0990_SS114_170711(JL16772)

0990_SS116_170711(JL16780)






D5-N-EtFOSA (surr.) 1 % 40 51 36

D7-N-MeFOSE (surr.) 1 % 69 77 66

D9-N-EtFOSE (surr.) 1 % 70 85 55

D5-N-EtFOSAA (surr.) 1 % 76 84 90

D3-N-MeFOSAA (surr.) 1 % 74 86 96


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L 2.5 < 2 4.1

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N0945 N094.5 N093.1

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N09690 N09150 N0915

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N09200 N0954 N092.6

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N093100 N091100 N0970

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L 26 N0910 < 0.2

13C3-PFBS (surr.) 1 % 74 82 90

18O2-PFHxS (surr.) 1 % 74 98 115

13C8-PFOS (surr.) 1 % 103 82 92


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS)N11 0.01 ug/L < 2 < 2 < 0.2

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 0.05 ug/L 1100 28 2.5

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L 730 110 20

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 0.01 ug/L 3.9 < 2 < 0.2

13C2-4:2 FTS (surr.) 1 % 66 63 78

13C2-6:2 FTS (surr.) 1 % 61 58 72

13C2-8:2 FTS (surr.) 1 % 51 58 70

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 3790 1250 85

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 4200 1240 98

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L 4890 1390 113

Sum of WA DER PFAS (n=10) 0.05 ug/L 7196.9 1629.9 192.8

Sum of PFASs (n=28) 0.1 ug/L 8075.3 1802.7 244.69


Leachate FluidC01 comment 4.0 4.0 4.0

pH (initial) 0.1 pH Units 8.3 7.2 6.7

pH (Leachate fluid) 0.1 pH Units 7.0 7.0 7.0

pH (off) 0.1 pH Units 6.1 6.3 7.4



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 2 of 8


















ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 3 of 8






Sample Detail

AU

S Leaching P

rocedure

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_SS113_170711(JL16771)


2 0990_SS114_170711(JL16772)


3 0990_SS116_170711(JL16780)


Test Counts 3 3








ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 4 of 8



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 5 of 8




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank







LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) B17-Au12523 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Au12523 NCP ug/L 0.01 0.01 8.0 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Au12523 NCP ug/L 0.03 0.03 11 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Au12523 NCP ug/L 0.01 0.01 3.0 30% Pass

Perfluorooctanoic acid (PFOA) B17-Au12523 NCP ug/L 0.04 0.04 11 30% Pass

Perfluorononanoic acid (PFNA) B17-Au12523 NCP ug/L 0.01 0.01 14 30% Pass

Perfluorodecanoic acid (PFDA) B17-Au12523 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Au12523 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorododecanoic acid (PFDoA) B17-Au12523 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) B17-Au12523 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Au12523 NCP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 6 of 8


Duplicate


Perfluorooctane sulfonamide(FOSA) B17-Au12523 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) B17-Au12523 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) B17-Au12523 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) B17-Au12523 NCP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) B17-Au12523 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) B17-Au12523 NCP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) B17-Au12523 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) B17-Au12523 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) B17-Au12523 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) B17-Au12523 NCP ug/L 0.03 0.03 7.0 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) B17-Au12523 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) B17-Au12523 NCP ug/L 1.1 1.3 15 30% Pass

Perfluorodecanesulfonic acid(PFDS) B17-Au12523 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) B17-Au12523 NCP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) B17-Au12523 NCP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) B17-Au12523 NCP ug/L 0.01 0.02 35 30% Fail Q15

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) B17-Au12523 NCP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 7 of 8


Comments











N11


Q15 The RPD reported passes Eurofins | mgt's QC - Acceptance Criteria as defined in the Internal Quality Control Review and Glossary page of this report.

Authorised By



Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 7 3902 4600

Page 8 of 8






Abbotsford

VIC 3067


Report 560144-L




Client Sample ID 0990_CONC01_170822

0990_CONC02_170822

0990_CONC03_170822

0990_CONC04_170822


Eurofins | mgt Sample No. M17-Au29753 M17-Au29754 M17-Au29755 M17-Au29756




Perfluorobutanoic acid (PFBA)N11 0.05 ug/L 0.42 13 2.5 0.22


Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N095.6 N0933 N0939 N090.91

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N092.2 N0911 N095.6 N090.12

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N097.4 N0917 N094.2 N090.31

Perfluorononanoic acid (PFNA)N11 0.01 ug/L 0.94 3.8 0.38 0.03

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L 0.46 1.6 0.40 0.02

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.2 0.31 < 0.2 0.01




13C4-PFBA (surr.) 1 % 131 104 117 80

13C5-PFPeA (surr.) 1 % 142 115 131 89

13C5-PFHxA (surr.) 1 % 143 109 122 79

13C4-PFHpA (surr.) 1 % 127 102 113 80

13C8-PFOA (surr.) 1 % 119 98 111 80

13C5-PFNA (surr.) 1 % 124 100 113 74

13C6-PFDA (surr.) 1 % 84 85 96 55

13C2-PFUnDA (surr.) 1 % 100 86 95 43

13C2-PFDoDA (surr.) 1 % 108 92 98 41

13C2-PFTeDA (surr.) 1 % 125 104 114 43


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L N095.4 N090.83 N091.4 N090.18







13C8-FOSA (surr.) 1 % 108 90 99 19

D3-N-MeFOSA (surr.) 1 % 109 97 105 10



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 15





0990_CONC02_170822

0990_CONC03_170822

0990_CONC04_170822






D5-N-EtFOSA (surr.) 1 % 66 59 64 INT

D7-N-MeFOSE (surr.) 1 % 129 112 132 16

D9-N-EtFOSE (surr.) 1 % 108 95 104 12

D5-N-EtFOSAA (surr.) 1 % 126 105 115 18

D3-N-MeFOSAA (surr.) 1 % 108 88 96 16


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L 0.88 24 5.1 0.21

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N091.7 N0925 N099.6 N090.15

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N0926 N09210 N0950 N091.0

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N097.0 N0916 N093.7 N090.02

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N09920 N09130 N09100 N090.63

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L 4.5 < 0.2 0.34 < 0.01

13C3-PFBS (surr.) 1 % 118 91 104 90

18O2-PFHxS (surr.) 1 % 110 73 93 80

13C8-PFOS (surr.) 1 % 81 99 107 70



1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 0.05 ug/L < 0.2 1.0 0.26 < 0.05

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L 7.8 3.0 3.4 0.05


13C2-4:2 FTS (surr.) 1 % 142 131 138 141

13C2-6:2 FTS (surr.) 1 % 126 109 114 128

13C2-8:2 FTS (surr.) 1 % 113 102 105 77

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 946 340 150 1.63

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 927.4 147 104.2 0.94

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L 953.4 357 154.2 1.94


Sum of PFASs (n=28) 0.1 ug/L 991.24 498.24 230.18 4.07



pH (initial) 0.1 pH Units 9.0 11 11 11


pH (off) 0.1 pH Units 9.3 12 12 12



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 15



0990_CONC06_170822


Eurofins | mgt Sample No. M17-Au29757 M17-Au29758




Perfluorobutanoic acid (PFBA)N11 0.05 ug/L 22 1.2

Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L N0931 N091.0

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N09220 N093.7

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L N0950 N090.72

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L N09110 N091.7

Perfluorononanoic acid (PFNA)N11 0.01 ug/L 0.21 0.07

Perfluorodecanoic acid (PFDA)N11 0.01 ug/L < 0.2 0.04

Perfluoroundecanoic acid (PFUnA)N11 0.01 ug/L < 0.2 < 0.01

Perfluorododecanoic acid (PFDoA)N11 0.01 ug/L < 0.2 < 0.01

Perfluorotridecanoic acid (PFTrDA) 0.01 ug/L < 0.2 < 0.01

Perfluorotetradecanoic acid (PFTeDA)N11 0.01 ug/L < 0.2 < 0.01

13C4-PFBA (surr.) 1 % 108 98

13C5-PFPeA (surr.) 1 % 109 110

13C5-PFHxA (surr.) 1 % 83 82

13C4-PFHpA (surr.) 1 % 92 96

13C8-PFOA (surr.) 1 % 74 71

13C5-PFNA (surr.) 1 % 99 87

13C6-PFDA (surr.) 1 % 53 46

13C2-PFUnDA (surr.) 1 % 86 53

13C2-PFDoDA (surr.) 1 % 91 54

13C2-PFTeDA (surr.) 1 % 106 55


Perfluorooctane sulfonamide (FOSA)N11 0.05 ug/L N093.6 N090.05

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA)N11 0.05 ug/L < 0.2 < 0.05

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA)N11 0.05 ug/L < 0.2 < 0.05

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE)N11 0.05 ug/L < 0.2 < 0.05

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE)N11 0.05 ug/L < 0.2 < 0.05

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA)N11 0.05 ug/L < 0.2 < 0.05

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA)N11 0.05 ug/L < 0.2 < 0.05

13C8-FOSA (surr.) 1 % 87 36

D3-N-MeFOSA (surr.) 1 % 94 41

D5-N-EtFOSA (surr.) 1 % 58 23

D7-N-MeFOSE (surr.) 1 % 106 52

D9-N-EtFOSE (surr.) 1 % 90 41

D5-N-EtFOSAA (surr.) 1 % 100 33

D3-N-MeFOSAA (surr.) 1 % 88 30


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L 76 3.1

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L N0990 N092.2

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N09520 N0914

Perfluoroheptanesulfonic acid (PFHpS) 0.01 ug/L N0974 N091.7

Perfluorooctanesulfonic acid (PFOS)N11 0.01 ug/L N091800 N0928

Perfluorodecanesulfonic acid (PFDS) 0.01 ug/L 0.37 < 0.01

13C3-PFBS (surr.) 1 % 76 71

18O2-PFHxS (surr.) 1 % 50 69

13C8-PFOS (surr.) 1 % 58 57



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 15



0990_CONC06_170822


Eurofins | mgt Sample No. M17-Au29757 M17-Au29758




1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS)N11 0.01 ug/L < 0.2 < 0.01

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 0.05 ug/L 0.24 0.64

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 0.01 ug/L 0.23 3.1

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 0.01 ug/L < 0.2 < 0.01

13C2-4:2 FTS (surr.) 1 % 131 147

13C2-6:2 FTS (surr.) 1 % 109 136

13C2-8:2 FTS (surr.) 1 % 91 87

PFASs Summations

Sum (PFHxS + PFOS) 0.01 ug/L 2320 42

Sum of US EPA PFAS (PFOS + PFOA) 0.01 ug/L 1910 29.7

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 0.01 ug/L 2430 43.7

Sum of WA DER PFAS (n=10) 0.05 ug/L 2829.47 57.16

Sum of PFASs (n=28) 0.1 ug/L 2997.65 61.22


Leachate FluidC01 comment 4.0 4.0

pH (initial) 0.1 pH Units 11 12

pH (Leachate fluid) 0.1 pH Units 7.1 7.1

pH (off) 0.1 pH Units 11 11



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 15


















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 15






Sample Detail

Alum

inium

Arsenic

Cadm

ium

Chrom

ium

Copper

Iron

Lead

Manganese

Mercury

Nickel

Zinc

Polycyclic A

romatic H

ydrocarbons

AU

S Leaching P

rocedure

Moisture S

et

Moisture S

et

Per- and P


ubstances(P

FA

Ss)

Melbourne Laboratory - NATA Site # 1254 & 14271 X X X X X X X X X X X X X X




External Laboratory


Matrix LAB ID

1 0990_SS168_170821

Aug 21, 2017 Soil M17-Au29720 X X

2 0990_SS169_170821

Aug 21, 2017 Soil M17-Au29721 X X

3 0990_SS170_170821

Aug 21, 2017 Soil M17-Au29722 X X

4 0990_SS171_170821

Aug 21, 2017 Soil M17-Au29723 X X

5 0990_SS172_170821

Aug 21, 2017 Soil M17-Au29724 X X

6 0990_SS173_ Aug 21, 2017 Soil M17-Au29725 X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 15






Sample Detail

Alum

inium

Arsenic

Cadm

ium

Chrom

ium

Copper

Iron

Lead

Manganese

Mercury

Nickel

Zinc

Polycyclic A

romatic H

ydrocarbons

AU

S Leaching P

rocedure

Moisture S

et

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





170821

7 0990_SS174_170821

Aug 21, 2017 Soil M17-Au29726 X X

8 0990_SS175_170821

Aug 21, 2017 Soil M17-Au29727 X X

9 0990_SS176_170821

Aug 21, 2017 Soil M17-Au29728 X X

10 0990_SS177_170821

Aug 21, 2017 Soil M17-Au29729 X X

11 0990_SS178_170821

Aug 21, 2017 Soil M17-Au29730 X X

12 0990_SS179_170821

Aug 21, 2017 Soil M17-Au29731 X X

13 0990_SS180_ Aug 21, 2017 Soil M17-Au29732 X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 15






Sample Detail

Alum

inium

Arsenic

Cadm

ium

Chrom

ium

Copper

Iron

Lead

Manganese

Mercury

Nickel

Zinc

Polycyclic A

romatic H

ydrocarbons

AU

S Leaching P

rocedure

Moisture S

et

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





170821

14 0990_SS181_170821

Aug 21, 2017 Soil M17-Au29733 X X

15 0990_SS182_170821

Aug 21, 2017 Soil M17-Au29734 X X

16 0990_SS183_170821

Aug 21, 2017 Soil M17-Au29735 X X

17 0990_SS184_170821

Aug 21, 2017 Soil M17-Au29736 X X

18 0990_QCSS193_170821

Aug 21, 2017 Soil M17-Au29737 X X

19 0990_QCSS193A_170821

Aug 21, 2017 Soil M17-Au29738 X X

20 0990_SS185_ Aug 22, 2017 Soil M17-Au29739 X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 15






Sample Detail

Alum

inium

Arsenic

Cadm

ium

Chrom

ium

Copper

Iron

Lead

Manganese

Mercury

Nickel

Zinc

Polycyclic A

romatic H

ydrocarbons

AU

S Leaching P

rocedure

Moisture S

et

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





170822

21 0990_SS186_170822

Aug 22, 2017 Soil M17-Au29740 X X

22 0990_SS187_170822

Aug 22, 2017 Soil M17-Au29741 X X

23 0990_SS188_170822

Aug 22, 2017 Soil M17-Au29742 X X

24 0990_SS189_170822

Aug 22, 2017 Soil M17-Au29743 X X

25 0990_SS190_170822

Aug 22, 2017 Soil M17-Au29744 X X

26 0990_SS191_170822

Aug 22, 2017 Soil M17-Au29745 X X X X X X X X X X X X X X

27 0990_CONC0 Aug 22, 2017 Soil M17-Au29746 X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 15






Sample Detail

Alum

inium

Arsenic

Cadm

ium

Chrom

ium

Copper

Iron

Lead

Manganese

Mercury

Nickel

Zinc

Polycyclic A

romatic H

ydrocarbons

AU

S Leaching P

rocedure

Moisture S

et

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





1_170822

28 0990_CONC02_170822

Aug 22, 2017 Solid M17-Au29747 X X

29 0990_CONC03_170822

Aug 22, 2017 Solid M17-Au29748 X X

30 0990_CONC04_170822

Aug 22, 2017 Solid M17-Au29749 X X

31 0990_CONC05_170822

Aug 22, 2017 Solid M17-Au29750 X X

32 0990_CONC06_170822

Aug 22, 2017 Solid M17-Au29751 X X

33 0990_SS192_170822

Aug 22, 2017 Soil M17-Au29752 X X

34 0990_CONC0 Aug 22, 2017 AUS Leachate M17-Au29753 X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 15






Sample Detail

Alum

inium

Arsenic

Cadm

ium

Chrom

ium

Copper

Iron

Lead

Manganese

Mercury

Nickel

Zinc

Polycyclic A

romatic H

ydrocarbons

AU

S Leaching P

rocedure

Moisture S

et

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





1_170822

35 0990_CONC02_170822

Aug 22, 2017 AUS Leachate M17-Au29754 X X

36 0990_CONC03_170822


37 0990_CONC04_170822


38 0990_CONC05_170822


39 0990_CONC06_170822


Test Counts 1 1 1 1 1 1 1 1 1 1 1 1 6 33 33 39








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 15



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 12 of 15




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank







LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) M17-Au29756 CP ug/L 0.22 0.22 1.0 30% Pass

Perfluoropentanoic acid (PFPeA) M17-Au29756 CP ug/L 0.21 0.21 1.0 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Au29756 CP ug/L 0.91 0.90 2.0 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Au29756 CP ug/L 0.12 0.11 1.0 30% Pass

Perfluorooctanoic acid (PFOA) M17-Au29756 CP ug/L 0.31 0.31 1.0 30% Pass

Perfluorononanoic acid (PFNA) M17-Au29756 CP ug/L 0.03 0.03 8.0 30% Pass

Perfluorodecanoic acid (PFDA) M17-Au29756 CP ug/L 0.02 0.02 5.0 30% Pass

Perfluoroundecanoic acid (PFUnA) M17-Au29756 CP ug/L 0.01 < 0.01 5.0 30% Pass

Perfluorododecanoic acid (PFDoA) M17-Au29756 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) M17-Au29756 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Au29756 CP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 13 of 15


Duplicate


Perfluorooctane sulfonamide(FOSA) M17-Au29756 CP ug/L 0.18 0.18 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Au29756 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Au29756 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Au29756 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Au29756 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Au29756 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Au29756 CP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Au29756 CP ug/L 0.21 0.21 1.0 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Au29756 CP ug/L 0.15 0.15 1.0 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Au29756 CP ug/L 1.0 1.0 1.0 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Au29756 CP ug/L 0.02 0.02 7.0 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-Au29756 CP ug/L 0.63 0.65 5.0 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-Au29756 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Au29756 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Au29756 CP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Au29756 CP ug/L 0.05 0.06 7.0 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Au29756 CP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 14 of 15


Comments











N11


Authorised By








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 15 of 15






Abbotsford

VIC 3067


Report 560144-S





0990_SS169_170821

0990_SS170_170821

0990_SS171_170821






Perfluorobutanoic acid (PFBA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluoropentanoic acid (PFPeA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluorohexanoic acid (PFHxA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluoroheptanoic acid (PFHpA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluorooctanoic acid (PFOA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluorononanoic acid (PFNA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluorodecanoic acid (PFDA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluoroundecanoic acid (PFUnA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluorododecanoic acid (PFDoA)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluorotridecanoic acid (PFTrDA) 5 ug/kg < 5 < 5 < 5 < 5

Perfluorotetradecanoic acid (PFTeDA)N11 5 ug/kg < 5 < 5 < 5 < 5

13C4-PFBA (surr.) 1 % 108 109 126 129

13C5-PFPeA (surr.) 1 % 96 111 99 112

13C5-PFHxA (surr.) 1 % 123 129 128 132

13C4-PFHpA (surr.) 1 % 127 132 130 133

13C8-PFOA (surr.) 1 % 116 122 119 118

13C5-PFNA (surr.) 1 % 119 123 126 125

13C6-PFDA (surr.) 1 % 125 131 135 130

13C2-PFUnDA (surr.) 1 % 170 181 161 180

13C2-PFDoDA (surr.) 1 % 162 170 165 163

13C2-PFTeDA (surr.) 1 % 151 164 151 165


Perfluorooctane sulfonamide (FOSA)N11 5 ug/kg < 5 < 5 < 5 < 5

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA)N11 5 ug/kg < 5 < 5 < 5 < 5

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA)N11 5 ug/kg < 5 < 5 < 5 < 5

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE)N11 5 ug/kg < 5 < 5 < 5 < 5

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE)N11 5 ug/kg < 5 < 5 < 5 < 5

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA)N11 10 ug/kg < 10 < 10 < 10 < 10

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA)N11 10 ug/kg < 10 < 10 < 10 < 10

13C8-FOSA (surr.) 1 % 107 112 119 101

D3-N-MeFOSA (surr.) 1 % 114 127 123 132



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 34





0990_SS169_170821

0990_SS170_170821

0990_SS171_170821






D5-N-EtFOSA (surr.) 1 % 66 70 70 77

D7-N-MeFOSE (surr.) 1 % 70 79 79 75

D9-N-EtFOSE (surr.) 1 % 95 106 108 95

D5-N-EtFOSAA (surr.) 1 % 136 142 144 153

D3-N-MeFOSAA (surr.) 1 % 159 163 152 166


Perfluorobutanesulfonic acid (PFBS)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluoropentanesulfonic acid (PFPeS) 5 ug/kg < 5 < 5 < 5 < 5

Perfluorohexanesulfonic acid (PFHxS)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluoroheptanesulfonic acid (PFHpS) 5 ug/kg < 5 < 5 < 5 < 5

Perfluorooctanesulfonic acid (PFOS)N11 5 ug/kg < 5 < 5 < 5 < 5

Perfluorodecanesulfonic acid (PFDS) 5 ug/kg < 5 < 5 < 5 < 5

13C3-PFBS (surr.) 1 % 113 121 120 123

18O2-PFHxS (surr.) 1 % 119 138 134 137

13C8-PFOS (surr.) 1 % 140 139 131 140


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS)N11 5 ug/kg < 5 < 5 < 5 < 5

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 10 ug/kg < 10 < 10 < 10 < 10

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 5 ug/kg < 5 < 5 < 5 < 5

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 5 ug/kg < 5 < 5 < 5 < 5

13C2-4:2 FTS (surr.) 1 % 79 89 98 112

13C2-6:2 FTS (surr.) 1 % 101 107 95 114

13C2-8:2 FTS (surr.) 1 % 109 100 107 114

PFASs Summations

Sum (PFHxS + PFOS) 5 ug/kg < 5 < 5 < 5 < 5

Sum of US EPA PFAS (PFOS + PFOA) 5 ug/kg < 5 < 5 < 5 < 5

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 5 ug/kg < 5 < 5 < 5 < 5

Sum of WA DER PFAS (n=10) 10 ug/kg < 10 < 10 < 10 < 10

Sum of PFASs (n=28) 50 ug/kg < 50 < 50 < 50 < 50

% Moisture 1 % 50 27 20 14


0990_SS173_170821

0990_SS174_170821

0990_SS175_170821















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 34



0990_SS173_170821

0990_SS174_170821

0990_SS175_170821










13C4-PFBA (surr.) 1 % 120 122 117 126

13C5-PFPeA (surr.) 1 % 103 102 102 116

13C5-PFHxA (surr.) 1 % 126 127 128 135

13C4-PFHpA (surr.) 1 % 129 130 133 140

13C8-PFOA (surr.) 1 % 115 121 124 132

13C5-PFNA (surr.) 1 % 114 117 119 134

13C6-PFDA (surr.) 1 % 132 118 129 131

13C2-PFUnDA (surr.) 1 % 165 168 169 181

13C2-PFDoDA (surr.) 1 % 141 133 159 170

13C2-PFTeDA (surr.) 1 % 124 136 156 171









13C8-FOSA (surr.) 1 % 93 98 103 112

D3-N-MeFOSA (surr.) 1 % 111 109 128 132

D5-N-EtFOSA (surr.) 1 % 64 66 76 75

D7-N-MeFOSE (surr.) 1 % 68 59 80 71

D9-N-EtFOSE (surr.) 1 % 74 83 100 97

D5-N-EtFOSAA (surr.) 1 % 119 106 147 152

D3-N-MeFOSAA (surr.) 1 % 148 141 165 168






Perfluorooctanesulfonic acid (PFOS)N11 5 ug/kg 5.5 < 5 < 5 N0910


13C3-PFBS (surr.) 1 % 118 120 122 129

18O2-PFHxS (surr.) 1 % 135 133 135 142

13C8-PFOS (surr.) 1 % 141 135 142 143



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 34



0990_SS173_170821

0990_SS174_170821

0990_SS175_170821










13C2-4:2 FTS (surr.) 1 % 97 102 105 116

13C2-6:2 FTS (surr.) 1 % 108 118 96 117

13C2-8:2 FTS (surr.) 1 % 112 106 113 113

PFASs Summations

Sum (PFHxS + PFOS) 5 ug/kg 5.5 < 5 < 5 10

Sum of US EPA PFAS (PFOS + PFOA) 5 ug/kg 5.5 < 5 < 5 10

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 5 ug/kg 5.5 < 5 < 5 10

Sum of WA DER PFAS (n=10) 10 ug/kg < 10 < 10 < 10 10


% Moisture 1 % 30 36 2.9 4.1


0990_SS177_170821

0990_SS178_170821

0990_SS179_170821

















13C4-PFBA (surr.) 1 % 125 125 121 127

13C5-PFPeA (surr.) 1 % 114 102 111 104

13C5-PFHxA (surr.) 1 % 130 130 125 132

13C4-PFHpA (surr.) 1 % 133 131 128 134

13C8-PFOA (surr.) 1 % 106 122 120 123

13C5-PFNA (surr.) 1 % 119 126 122 136

13C6-PFDA (surr.) 1 % 129 130 127 141

13C2-PFUnDA (surr.) 1 % 168 165 155 165

13C2-PFDoDA (surr.) 1 % 150 167 151 148

13C2-PFTeDA (surr.) 1 % 120 152 131 147



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 34



0990_SS177_170821

0990_SS178_170821

0990_SS179_170821













13C8-FOSA (surr.) 1 % 93 111 117 113

D3-N-MeFOSA (surr.) 1 % 111 132 125 127

D5-N-EtFOSA (surr.) 1 % 66 71 70 67

D7-N-MeFOSE (surr.) 1 % 71 71 78 61

D9-N-EtFOSE (surr.) 1 % 90 104 108 92

D5-N-EtFOSAA (surr.) 1 % 131 140 139 128

D3-N-MeFOSAA (surr.) 1 % 152 154 146 148






Perfluorooctanesulfonic acid (PFOS)N11 5 ug/kg N0912 < 5 < 5 < 5


13C3-PFBS (surr.) 1 % 124 122 119 126

18O2-PFHxS (surr.) 1 % 136 136 128 139

13C8-PFOS (surr.) 1 % 140 139 138 138






13C2-4:2 FTS (surr.) 1 % 105 106 103 102

13C2-6:2 FTS (surr.) 1 % 113 107 113 113

13C2-8:2 FTS (surr.) 1 % 104 109 102 116

PFASs Summations

Sum (PFHxS + PFOS) 5 ug/kg 12 < 5 < 5 < 5

Sum of US EPA PFAS (PFOS + PFOA) 5 ug/kg 12 < 5 < 5 < 5

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 5 ug/kg 12 < 5 < 5 < 5

Sum of WA DER PFAS (n=10) 10 ug/kg 12 < 10 < 10 < 10


% Moisture 1 % 20 27 26 14



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 34



0990_SS181_170821

0990_SS182_170821

0990_SS183_170821

















13C4-PFBA (surr.) 1 % 123 61 134 105

13C5-PFPeA (surr.) 1 % 114 50 111 90

13C5-PFHxA (surr.) 1 % 127 65 141 113

13C4-PFHpA (surr.) 1 % 129 65 141 117

13C8-PFOA (surr.) 1 % 119 61 139 110

13C5-PFNA (surr.) 1 % 122 61 135 112

13C6-PFDA (surr.) 1 % 143 63 135 121

13C2-PFUnDA (surr.) 1 % 165 75 186 147

13C2-PFDoDA (surr.) 1 % 152 73 167 125

13C2-PFTeDA (surr.) 1 % 139 69 164 116









13C8-FOSA (surr.) 1 % 105 59 115 84

D3-N-MeFOSA (surr.) 1 % 122 64 139 110

D5-N-EtFOSA (surr.) 1 % 68 37 79 64

D7-N-MeFOSE (surr.) 1 % 71 37 71 63

D9-N-EtFOSE (surr.) 1 % 90 51 99 80

D5-N-EtFOSAA (surr.) 1 % 140 65 145 85

D3-N-MeFOSAA (surr.) 1 % 155 68 169 134






Perfluorooctanesulfonic acid (PFOS)N11 5 ug/kg N097.2 < 5 < 5 N097.6


13C3-PFBS (surr.) 1 % 123 60 133 109

18O2-PFHxS (surr.) 1 % 130 67 151 122

13C8-PFOS (surr.) 1 % 133 69 150 115



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 34



0990_SS181_170821

0990_SS182_170821

0990_SS183_170821










13C2-4:2 FTS (surr.) 1 % 95 46 115 96

13C2-6:2 FTS (surr.) 1 % 99 51 123 115

13C2-8:2 FTS (surr.) 1 % 125 44 127 108

PFASs Summations

Sum (PFHxS + PFOS) 5 ug/kg 7.2 < 5 < 5 7.6

Sum of US EPA PFAS (PFOS + PFOA) 5 ug/kg 7.2 < 5 < 5 7.6

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 5 ug/kg 7.2 < 5 < 5 7.6



% Moisture 1 % 25 1.7 1.8 9.1


0990_QCSS193_170821

0990_QCSS193A_170821

0990_SS185_170822

















13C4-PFBA (surr.) 1 % 125 118 123 116

13C5-PFPeA (surr.) 1 % 107 112 104 102

13C5-PFHxA (surr.) 1 % 139 136 135 127

13C4-PFHpA (surr.) 1 % 139 138 138 129

13C8-PFOA (surr.) 1 % 131 131 130 119

13C5-PFNA (surr.) 1 % 136 129 128 123

13C6-PFDA (surr.) 1 % 140 133 140 133

13C2-PFUnDA (surr.) 1 % 164 157 175 162

13C2-PFDoDA (surr.) 1 % 164 149 168 146

13C2-PFTeDA (surr.) 1 % 153 134 164 118



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 34



0990_QCSS193_170821

0990_QCSS193A_170821

0990_SS185_170822













13C8-FOSA (surr.) 1 % 109 114 111 108

D3-N-MeFOSA (surr.) 1 % 133 125 131 117

D5-N-EtFOSA (surr.) 1 % 73 66 73 66

D7-N-MeFOSE (surr.) 1 % 73 74 64 67

D9-N-EtFOSE (surr.) 1 % 93 78 95 88

D5-N-EtFOSAA (surr.) 1 % 174 139 158 148

D3-N-MeFOSAA (surr.) 1 % 158 147 163 140






Perfluorooctanesulfonic acid (PFOS)N11 5 ug/kg < 5 < 5 < 5 5.0


13C3-PFBS (surr.) 1 % 129 129 131 120

18O2-PFHxS (surr.) 1 % 141 145 142 133

13C8-PFOS (surr.) 1 % 143 153 140 139






13C2-4:2 FTS (surr.) 1 % 110 118 130 105

13C2-6:2 FTS (surr.) 1 % 122 150 127 109

13C2-8:2 FTS (surr.) 1 % 138 132 123 102

PFASs Summations

Sum (PFHxS + PFOS) 5 ug/kg < 5 < 5 < 5 5

Sum of US EPA PFAS (PFOS + PFOA) 5 ug/kg < 5 < 5 < 5 5

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 5 ug/kg < 5 < 5 < 5 5



% Moisture 1 % < 1 1.7 < 1 31



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 34



0990_SS187_170822

0990_SS188_170822

0990_SS189_170822

















13C4-PFBA (surr.) 1 % 119 124 122 131

13C5-PFPeA (surr.) 1 % 109 108 112 112

13C5-PFHxA (surr.) 1 % 127 133 130 139

13C4-PFHpA (surr.) 1 % 130 135 132 139

13C8-PFOA (surr.) 1 % 102 125 124 134

13C5-PFNA (surr.) 1 % 119 129 123 134

13C6-PFDA (surr.) 1 % 111 136 130 143

13C2-PFUnDA (surr.) 1 % 120 174 158 173

13C2-PFDoDA (surr.) 1 % 80 160 140 178

13C2-PFTeDA (surr.) 1 % 90 158 132 167









13C8-FOSA (surr.) 1 % 54 107 108 112

D3-N-MeFOSA (surr.) 1 % 108 136 120 139

D5-N-EtFOSA (surr.) 1 % 68 74 67 75

D7-N-MeFOSE (surr.) 1 % 47 73 64 72

D9-N-EtFOSE (surr.) 1 % 76 110 86 106

D5-N-EtFOSAA (surr.) 1 % 64 152 140 162

D3-N-MeFOSAA (surr.) 1 % 144 167 143 180






Perfluorooctanesulfonic acid (PFOS)N11 5 ug/kg N0911 N097.1 N0945 < 5


13C3-PFBS (surr.) 1 % 122 127 125 131

18O2-PFHxS (surr.) 1 % 137 139 140 148

13C8-PFOS (surr.) 1 % 91 138 138 137



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 34



0990_SS187_170822

0990_SS188_170822

0990_SS189_170822










13C2-4:2 FTS (surr.) 1 % 105 124 113 109

13C2-6:2 FTS (surr.) 1 % 103 119 119 125

13C2-8:2 FTS (surr.) 1 % 102 115 109 111

PFASs Summations

Sum (PFHxS + PFOS) 5 ug/kg 11 7.1 45 < 5

Sum of US EPA PFAS (PFOS + PFOA) 5 ug/kg 11 7.1 45 < 5

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 5 ug/kg 11 7.1 45 < 5

Sum of WA DER PFAS (n=10) 10 ug/kg 11 < 10 45 < 10


% Moisture 1 % 26 14 27 1.7


0990_SS191_170822

0990_CONC01_170822

0990_CONC02_170822

Sample Matrix Soil Soil Soil Solid




Polycyclic Aromatic Hydrocarbons

Benzo(a)pyrene TEQ (lower bound) * 0.5 mg/kg - < 0.5 - -

Benzo(a)pyrene TEQ (medium bound) * 0.5 mg/kg - 0.6 - -

Benzo(a)pyrene TEQ (upper bound) * 0.5 mg/kg - 1.2 - -

Acenaphthene 0.5 mg/kg - < 0.5 - -

Acenaphthylene 0.5 mg/kg - < 0.5 - -

Anthracene 0.5 mg/kg - < 0.5 - -

Benz(a)anthracene 0.5 mg/kg - < 0.5 - -

Benzo(a)pyrene 0.5 mg/kg - < 0.5 - -

Benzo(b&j)fluorantheneN07 0.5 mg/kg - < 0.5 - -

Benzo(g.h.i)perylene 0.5 mg/kg - < 0.5 - -

Benzo(k)fluoranthene 0.5 mg/kg - < 0.5 - -

Chrysene 0.5 mg/kg - < 0.5 - -

Dibenz(a.h)anthracene 0.5 mg/kg - < 0.5 - -

Fluoranthene 0.5 mg/kg - < 0.5 - -

Fluorene 0.5 mg/kg - < 0.5 - -

Indeno(1.2.3-cd)pyrene 0.5 mg/kg - < 0.5 - -

Naphthalene 0.5 mg/kg - < 0.5 - -

Phenanthrene 0.5 mg/kg - < 0.5 - -

Pyrene 0.5 mg/kg - < 0.5 - -

Total PAH* 0.5 mg/kg - < 0.5 - -

2-Fluorobiphenyl (surr.) 1 % - 84 - -

p-Terphenyl-d14 (surr.) 1 % - 133 - -



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 34



0990_SS191_170822

0990_CONC01_170822

0990_CONC02_170822






Perfluorobutanoic acid (PFBA)N11 5 ug/kg < 5 < 5 7.6 N09540

Perfluoropentanoic acid (PFPeA)N11 5 ug/kg < 5 < 5 19 410

Perfluorohexanoic acid (PFHxA)N11 5 ug/kg < 5 < 5 N09100 N091300

Perfluoroheptanoic acid (PFHpA)N11 5 ug/kg < 5 < 5 N0929 N09320

Perfluorooctanoic acid (PFOA)N11 5 ug/kg < 5 < 5 N0994 N09720

Perfluorononanoic acid (PFNA)N11 5 ug/kg < 5 < 5 26 300

Perfluorodecanoic acid (PFDA)N11 5 ug/kg < 5 < 5 19 390

Perfluoroundecanoic acid (PFUnA)N11 5 ug/kg < 5 < 5 9.0 600

Perfluorododecanoic acid (PFDoA)N11 5 ug/kg < 5 < 5 9.3 650

Perfluorotridecanoic acid (PFTrDA) 5 ug/kg < 5 < 5 < 5 300

Perfluorotetradecanoic acid (PFTeDA)N11 5 ug/kg < 5 < 5 < 5 220

13C4-PFBA (surr.) 1 % 124 126 128 88

13C5-PFPeA (surr.) 1 % 109 110 106 76

13C5-PFHxA (surr.) 1 % 131 139 120 108

13C4-PFHpA (surr.) 1 % 135 140 85 85

13C8-PFOA (surr.) 1 % 126 134 97 82

13C5-PFNA (surr.) 1 % 126 137 102 59

13C6-PFDA (surr.) 1 % 133 147 56 52

13C2-PFUnDA (surr.) 1 % 168 170 121 93

13C2-PFDoDA (surr.) 1 % 162 180 133 106

13C2-PFTeDA (surr.) 1 % 155 148 111 75


Perfluorooctane sulfonamide (FOSA)N11 5 ug/kg < 5 < 5 N09160 N0988







13C8-FOSA (surr.) 1 % 105 125 91 85

D3-N-MeFOSA (surr.) 1 % 139 130 136 118

D5-N-EtFOSA (surr.) 1 % 72 75 72 54

D7-N-MeFOSE (surr.) 1 % 73 77 70 45

D9-N-EtFOSE (surr.) 1 % 107 95 103 89

D5-N-EtFOSAA (surr.) 1 % 151 166 128 118

D3-N-MeFOSAA (surr.) 1 % 159 167 137 105


Perfluorobutanesulfonic acid (PFBS)N11 5 ug/kg < 5 < 5 N0915 N09690

Perfluoropentanesulfonic acid (PFPeS) 5 ug/kg < 5 < 5 N0924 N09530

Perfluorohexanesulfonic acid (PFHxS)N11 5 ug/kg < 5 < 5 N09310 N097300

Perfluoroheptanesulfonic acid (PFHpS) 5 ug/kg < 5 < 5 N09150 N09820

Perfluorooctanesulfonic acid (PFOS)N11 5 ug/kg < 5 < 5 N0935000 N0927000

Perfluorodecanesulfonic acid (PFDS) 5 ug/kg < 5 < 5 N09310 N09320

13C3-PFBS (surr.) 1 % 128 132 124 81

18O2-PFHxS (surr.) 1 % 138 148 80 85

13C8-PFOS (surr.) 1 % 136 144 91 51



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 34



0990_SS191_170822

0990_CONC01_170822

0990_CONC02_170822







1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 10 ug/kg < 10 < 10 < 10 52

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 5 ug/kg < 5 < 5 190 410

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 5 ug/kg < 5 < 5 < 5 43

13C2-4:2 FTS (surr.) 1 % 114 117 111 157

13C2-6:2 FTS (surr.) 1 % 112 133 130 165

13C2-8:2 FTS (surr.) 1 % 104 144 139 INT

PFASs Summations

Sum (PFHxS + PFOS) 5 ug/kg < 5 < 5 35310 34300

Sum of US EPA PFAS (PFOS + PFOA) 5 ug/kg < 5 < 5 35094 27720

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 5 ug/kg < 5 < 5 35404 35020

Sum of WA DER PFAS (n=10) 10 ug/kg < 10 < 10 35764.6 38742

Sum of PFASs (n=28) 50 ug/kg < 50 < 50 36471.9 43003

Heavy Metals

Aluminium 10 mg/kg - 37000 - -

Arsenic 2 mg/kg - 4.5 - -

Cadmium 0.4 mg/kg - < 0.4 - -

Chromium 5 mg/kg - 52 - -

Copper 5 mg/kg - < 5 - -

Iron 20 mg/kg - 43000 - -

Lead 5 mg/kg - 12 - -

Manganese 5 mg/kg - 12 - -

Mercury 0.1 mg/kg - < 0.1 - -

Nickel 5 mg/kg - 7.2 - -

Zinc 5 mg/kg - 6.1 - -

% Moisture 1 % 21 < 1 < 1 11


0990_CONC04_170822

0990_CONC05_170822

0990_CONC06_170822

Sample Matrix Solid Solid Solid Solid





Perfluorobutanoic acid (PFBA)N11 5 ug/kg 92 N095.8 N09600 28

Perfluoropentanoic acid (PFPeA)N11 5 ug/kg 150 5.8 N09980 N0930

Perfluorohexanoic acid (PFHxA)N11 5 ug/kg N091200 N0924 N095400 N0981

Perfluoroheptanoic acid (PFHpA)N11 5 ug/kg N09240 < 5 N091800 N0915

Perfluorooctanoic acid (PFOA)N11 5 ug/kg N09420 N099.2 N094400 N0932

Perfluorononanoic acid (PFNA)N11 5 ug/kg 47 < 5 N0915 < 5

Perfluorodecanoic acid (PFDA)N11 5 ug/kg 110 < 5 < 5 < 5

Perfluoroundecanoic acid (PFUnA)N11 5 ug/kg 95 < 5 < 5 < 5

Perfluorododecanoic acid (PFDoA)N11 5 ug/kg 100 < 5 < 5 < 5

Perfluorotridecanoic acid (PFTrDA) 5 ug/kg 31 < 5 < 5 < 5

Perfluorotetradecanoic acid (PFTeDA)N11 5 ug/kg 25 < 5 < 5 < 5



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 12 of 34



0990_CONC04_170822

0990_CONC05_170822

0990_CONC06_170822






13C4-PFBA (surr.) 1 % 80 124 113 124

13C5-PFPeA (surr.) 1 % 73 108 125 111

13C5-PFHxA (surr.) 1 % 108 121 116 122

13C4-PFHpA (surr.) 1 % 72 131 100 107

13C8-PFOA (surr.) 1 % 66 130 88 127

13C5-PFNA (surr.) 1 % 68 134 78 117

13C6-PFDA (surr.) 1 % 38 145 24 110

13C2-PFUnDA (surr.) 1 % 82 154 101 157

13C2-PFDoDA (surr.) 1 % 74 150 157 182

13C2-PFTeDA (surr.) 1 % 38 138 176 178


Perfluorooctane sulfonamide (FOSA)N11 5 ug/kg N09180 < 5 150 < 5







13C8-FOSA (surr.) 1 % 64 108 98 112

D3-N-MeFOSA (surr.) 1 % 96 140 147 141

D5-N-EtFOSA (surr.) 1 % 50 70 63 65

D7-N-MeFOSE (surr.) 1 % 59 81 67 66

D9-N-EtFOSE (surr.) 1 % 82 114 106 110

D5-N-EtFOSAA (surr.) 1 % 73 125 149 136

D3-N-MeFOSAA (surr.) 1 % 73 116 128 116


Perfluorobutanesulfonic acid (PFBS)N11 5 ug/kg 160 < 5 2000 N0966

Perfluoropentanesulfonic acid (PFPeS) 5 ug/kg N09290 < 5 N092400 N0940

Perfluorohexanesulfonic acid (PFHxS)N11 5 ug/kg N093000 N0922 N0918000 N09300

Perfluoroheptanesulfonic acid (PFHpS) 5 ug/kg N09620 < 5 N093000 N0936

Perfluorooctanesulfonic acid (PFOS)N11 5 ug/kg N0943000 N0924 N09110000 1000

Perfluorodecanesulfonic acid (PFDS) 5 ug/kg N09590 < 5 N09110 < 5

13C3-PFBS (surr.) 1 % 72 122 94 122

18O2-PFHxS (surr.) 1 % 107 134 72 106

13C8-PFOS (surr.) 1 % 80 118 156 89



1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 10 ug/kg 20 < 10 < 10 < 10

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 5 ug/kg 360 < 5 15 180

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 5 ug/kg 27 < 5 < 5 < 5

13C2-4:2 FTS (surr.) 1 % 68 103 191 197

13C2-6:2 FTS (surr.) 1 % 90 129 INT INT

13C2-8:2 FTS (surr.) 1 % INT 182 82 INT



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 13 of 34



0990_CONC04_170822

0990_CONC05_170822

0990_CONC06_170822





PFASs Summations

Sum (PFHxS + PFOS) 5 ug/kg 46000 46 128000 1300

Sum of US EPA PFAS (PFOS + PFOA) 5 ug/kg 43420 33.2 114400 1032

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 5 ug/kg 46420 55.2 132400 1332

Sum of WA DER PFAS (n=10) 10 ug/kg 48642 90.8 143195 1732

Sum of PFASs (n=28) 50 ug/kg 50757 90.8 148870 1808

% Moisture 1 % 9.5 3.5 1.6 < 1


Sample Matrix Soil

Eurofins | mgt Sample No. M17-Au29752




Perfluorobutanoic acid (PFBA)N11 5 ug/kg < 5

Perfluoropentanoic acid (PFPeA)N11 5 ug/kg N099.3

Perfluorohexanoic acid (PFHxA)N11 5 ug/kg N0913

Perfluoroheptanoic acid (PFHpA)N11 5 ug/kg < 5

Perfluorooctanoic acid (PFOA)N11 5 ug/kg < 5

Perfluorononanoic acid (PFNA)N11 5 ug/kg < 5

Perfluorodecanoic acid (PFDA)N11 5 ug/kg < 5

Perfluoroundecanoic acid (PFUnA)N11 5 ug/kg < 5

Perfluorododecanoic acid (PFDoA)N11 5 ug/kg < 5

Perfluorotridecanoic acid (PFTrDA) 5 ug/kg < 5

Perfluorotetradecanoic acid (PFTeDA)N11 5 ug/kg < 5

13C4-PFBA (surr.) 1 % 75

13C5-PFPeA (surr.) 1 % 27

13C5-PFHxA (surr.) 1 % 95

13C4-PFHpA (surr.) 1 % 101

13C8-PFOA (surr.) 1 % 70

13C5-PFNA (surr.) 1 % 48

13C6-PFDA (surr.) 1 % 57

13C2-PFUnDA (surr.) 1 % 44

13C2-PFDoDA (surr.) 1 % 22

13C2-PFTeDA (surr.) 1 % 25


Perfluorooctane sulfonamide (FOSA)N11 5 ug/kg < 5

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA)N11 5 ug/kg < 5

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA)N11 5 ug/kg < 5

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol(N-MeFOSE)N11 5 ug/kg < 5

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE)N11 5 ug/kg < 5

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA)N11 10 ug/kg < 10

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA)N11 10 ug/kg < 10



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 14 of 34



Sample Matrix Soil

Eurofins | mgt Sample No. M17-Au29752




13C8-FOSA (surr.) 1 % 15

D3-N-MeFOSA (surr.) 1 % 19

D5-N-EtFOSA (surr.) 1 % INT

D7-N-MeFOSE (surr.) 1 % INT

D9-N-EtFOSE (surr.) 1 % INT

D5-N-EtFOSAA (surr.) 1 % 32

D3-N-MeFOSAA (surr.) 1 % 29


Perfluorobutanesulfonic acid (PFBS)N11 5 ug/kg < 5

Perfluoropentanesulfonic acid (PFPeS) 5 ug/kg < 5

Perfluorohexanesulfonic acid (PFHxS)N11 5 ug/kg N098.7

Perfluoroheptanesulfonic acid (PFHpS) 5 ug/kg < 5

Perfluorooctanesulfonic acid (PFOS)N11 5 ug/kg N0957

Perfluorodecanesulfonic acid (PFDS) 5 ug/kg 17

13C3-PFBS (surr.) 1 % 123

18O2-PFHxS (surr.) 1 % 104

13C8-PFOS (surr.) 1 % 64


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS)N11 5 ug/kg < 5

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS)N11 10 ug/kg < 10

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS)N11 5 ug/kg < 5

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2FTS) 5 ug/kg < 5

13C2-4:2 FTS (surr.) 1 % 172

13C2-6:2 FTS (surr.) 1 % 153

13C2-8:2 FTS (surr.) 1 % 68

PFASs Summations

Sum (PFHxS + PFOS) 5 ug/kg 65.7

Sum of US EPA PFAS (PFOS + PFOA) 5 ug/kg 57

Sum of enHealth PFAS (PFHxS + PFOS + PFOA) 5 ug/kg 65.7

Sum of WA DER PFAS (n=10) 10 ug/kg 88

Sum of PFASs (n=28) 50 ug/kg 105

% Moisture 1 % 6.0



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 15 of 34





Polycyclic Aromatic Hydrocarbons Melbourne Aug 26, 2017 14 Day

- Method: LTM-ORG-2140 PAH and Phenols in Soils by GCMS

Heavy Metals Melbourne Aug 26, 2017 180 Day

- Method: LTM-MET-3030 by ICP-OES (hydride ICP-OES for Mercury)










% Moisture Brisbane Aug 25, 2017 14 Day




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 16 of 34






Sample Detail

Alum

inium

Arsenic

Cadm

ium

Chrom

ium

Copper

Iron

Lead

Manganese

Mercury

Nickel

Zinc

Polycyclic A

romatic H

ydrocarbons

AU

S Leaching P

rocedure

Moisture S

et

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_SS168_170821

Aug 21, 2017 Soil M17-Au29720 X X

2 0990_SS169_170821

Aug 21, 2017 Soil M17-Au29721 X X

3 0990_SS170_170821

Aug 21, 2017 Soil M17-Au29722 X X

4 0990_SS171_170821

Aug 21, 2017 Soil M17-Au29723 X X

5 0990_SS172_170821

Aug 21, 2017 Soil M17-Au29724 X X

6 0990_SS173_ Aug 21, 2017 Soil M17-Au29725 X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 17 of 34






Sample Detail

Alum

inium

Arsenic

Cadm

ium

Chrom

ium

Copper

Iron

Lead

Manganese

Mercury

Nickel

Zinc

Polycyclic A

romatic H

ydrocarbons

AU

S Leaching P

rocedure

Moisture S

et

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





170821

7 0990_SS174_170821

Aug 21, 2017 Soil M17-Au29726 X X

8 0990_SS175_170821

Aug 21, 2017 Soil M17-Au29727 X X

9 0990_SS176_170821

Aug 21, 2017 Soil M17-Au29728 X X

10 0990_SS177_170821

Aug 21, 2017 Soil M17-Au29729 X X

11 0990_SS178_170821

Aug 21, 2017 Soil M17-Au29730 X X

12 0990_SS179_170821

Aug 21, 2017 Soil M17-Au29731 X X

13 0990_SS180_ Aug 21, 2017 Soil M17-Au29732 X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 18 of 34






Sample Detail

Alum

inium

Arsenic

Cadm

ium

Chrom

ium

Copper

Iron

Lead

Manganese

Mercury

Nickel

Zinc

Polycyclic A

romatic H

ydrocarbons

AU

S Leaching P

rocedure

Moisture S

et

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





170821

14 0990_SS181_170821

Aug 21, 2017 Soil M17-Au29733 X X

15 0990_SS182_170821

Aug 21, 2017 Soil M17-Au29734 X X

16 0990_SS183_170821

Aug 21, 2017 Soil M17-Au29735 X X

17 0990_SS184_170821

Aug 21, 2017 Soil M17-Au29736 X X

18 0990_QCSS193_170821

Aug 21, 2017 Soil M17-Au29737 X X

19 0990_QCSS193A_170821

Aug 21, 2017 Soil M17-Au29738 X X

20 0990_SS185_ Aug 22, 2017 Soil M17-Au29739 X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 19 of 34






Sample Detail

Alum

inium

Arsenic

Cadm

ium

Chrom

ium

Copper

Iron

Lead

Manganese

Mercury

Nickel

Zinc

Polycyclic A

romatic H

ydrocarbons

AU

S Leaching P

rocedure

Moisture S

et

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





170822

21 0990_SS186_170822

Aug 22, 2017 Soil M17-Au29740 X X

22 0990_SS187_170822

Aug 22, 2017 Soil M17-Au29741 X X

23 0990_SS188_170822

Aug 22, 2017 Soil M17-Au29742 X X

24 0990_SS189_170822

Aug 22, 2017 Soil M17-Au29743 X X

25 0990_SS190_170822

Aug 22, 2017 Soil M17-Au29744 X X

26 0990_SS191_170822

Aug 22, 2017 Soil M17-Au29745 X X X X X X X X X X X X X X

27 0990_CONC0 Aug 22, 2017 Soil M17-Au29746 X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 20 of 34






Sample Detail

Alum

inium

Arsenic

Cadm

ium

Chrom

ium

Copper

Iron

Lead

Manganese

Mercury

Nickel

Zinc

Polycyclic A

romatic H

ydrocarbons

AU

S Leaching P

rocedure

Moisture S

et

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





1_170822

28 0990_CONC02_170822

Aug 22, 2017 Solid M17-Au29747 X X

29 0990_CONC03_170822

Aug 22, 2017 Solid M17-Au29748 X X

30 0990_CONC04_170822

Aug 22, 2017 Solid M17-Au29749 X X

31 0990_CONC05_170822

Aug 22, 2017 Solid M17-Au29750 X X

32 0990_CONC06_170822

Aug 22, 2017 Solid M17-Au29751 X X

33 0990_SS192_170822

Aug 22, 2017 Soil M17-Au29752 X X

34 0990_CONC0 Aug 22, 2017 AUS Leachate M17-Au29753 X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 21 of 34






Sample Detail

Alum

inium

Arsenic

Cadm

ium

Chrom

ium

Copper

Iron

Lead

Manganese

Mercury

Nickel

Zinc

Polycyclic A

romatic H

ydrocarbons

AU

S Leaching P

rocedure

Moisture S

et

Moisture S

et

Per- and P


ubstances(P

FA

Ss)





1_170822

35 0990_CONC02_170822


36 0990_CONC03_170822


37 0990_CONC04_170822


38 0990_CONC05_170822


39 0990_CONC06_170822


Test Counts 1 1 1 1 1 1 1 1 1 1 1 1 6 33 33 39








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 22 of 34



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 23 of 34




PassLimits

QualifyingCode

Method Blank


Acenaphthene mg/kg < 0.5 0.5 Pass

Acenaphthylene mg/kg < 0.5 0.5 Pass

Anthracene mg/kg < 0.5 0.5 Pass

Benz(a)anthracene mg/kg < 0.5 0.5 Pass

Benzo(a)pyrene mg/kg < 0.5 0.5 Pass

Benzo(b&j)fluoranthene mg/kg < 0.5 0.5 Pass

Benzo(g.h.i)perylene mg/kg < 0.5 0.5 Pass

Benzo(k)fluoranthene mg/kg < 0.5 0.5 Pass

Chrysene mg/kg < 0.5 0.5 Pass

Dibenz(a.h)anthracene mg/kg < 0.5 0.5 Pass

Fluoranthene mg/kg < 0.5 0.5 Pass

Fluorene mg/kg < 0.5 0.5 Pass

Indeno(1.2.3-cd)pyrene mg/kg < 0.5 0.5 Pass

Naphthalene mg/kg < 0.5 0.5 Pass

Phenanthrene mg/kg < 0.5 0.5 Pass

Pyrene mg/kg < 0.5 0.5 Pass

Method Blank


Perfluorobutanoic acid (PFBA) ug/kg < 5 5 Pass

Perfluoropentanoic acid (PFPeA) ug/kg < 5 5 Pass

Perfluorohexanoic acid (PFHxA) ug/kg < 5 5 Pass

Perfluoroheptanoic acid (PFHpA) ug/kg < 5 5 Pass

Perfluorooctanoic acid (PFOA) ug/kg < 5 5 Pass

Perfluorononanoic acid (PFNA) ug/kg < 5 5 Pass

Perfluorodecanoic acid (PFDA) ug/kg < 5 5 Pass

Perfluoroundecanoic acid (PFUnA) ug/kg < 5 5 Pass

Perfluorododecanoic acid (PFDoA) ug/kg < 5 5 Pass

Perfluorotridecanoic acid (PFTrDA) ug/kg < 5 5 Pass

Perfluorotetradecanoic acid (PFTeDA) ug/kg < 5 5 Pass

Method Blank


Perfluorooctane sulfonamide (FOSA) ug/kg < 5 5 Pass

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) ug/kg < 5 5 Pass

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) ug/kg < 5 5 Pass

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol (N-MeFOSE) ug/kg < 5 5 Pass

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) ug/kg < 5 5 Pass

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) ug/kg < 10 10 Pass

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) ug/kg < 10 10 Pass

Method Blank


Perfluorobutanesulfonic acid (PFBS) ug/kg < 5 5 Pass

Perfluoropentanesulfonic acid (PFPeS) ug/kg < 5 5 Pass

Perfluorohexanesulfonic acid (PFHxS) ug/kg < 5 5 Pass

Perfluoroheptanesulfonic acid (PFHpS) ug/kg < 5 5 Pass

Perfluorooctanesulfonic acid (PFOS) ug/kg < 5 5 Pass

Perfluorodecanesulfonic acid (PFDS) ug/kg < 5 5 Pass

Method Blank


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) ug/kg < 5 5 Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 24 of 34



PassLimits

QualifyingCode

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) ug/kg < 10 10 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) ug/kg < 5 5 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2 FTS) ug/kg < 5 5 Pass

Method Blank

Heavy Metals

Aluminium mg/kg < 10 10 Pass

Arsenic mg/kg < 2 2 Pass

Cadmium mg/kg < 0.4 0.4 Pass

Chromium mg/kg < 5 5 Pass

Copper mg/kg < 5 5 Pass

Iron mg/kg < 20 20 Pass

Lead mg/kg < 5 5 Pass

Manganese mg/kg < 5 5 Pass

Mercury mg/kg < 0.1 0.1 Pass

Nickel mg/kg < 5 5 Pass

Zinc mg/kg < 5 5 Pass

LCS - % Recovery


Acenaphthene % 88 70-130 Pass

Acenaphthylene % 94 70-130 Pass

Anthracene % 94 70-130 Pass

Benz(a)anthracene % 101 70-130 Pass

Benzo(a)pyrene % 104 70-130 Pass

Benzo(b&j)fluoranthene % 99 70-130 Pass

Benzo(g.h.i)perylene % 96 70-130 Pass

Benzo(k)fluoranthene % 116 70-130 Pass

Chrysene % 101 70-130 Pass

Dibenz(a.h)anthracene % 106 70-130 Pass

Fluoranthene % 101 70-130 Pass

Fluorene % 88 70-130 Pass

Indeno(1.2.3-cd)pyrene % 103 70-130 Pass

Naphthalene % 88 70-130 Pass

Phenanthrene % 101 70-130 Pass

Pyrene % 97 70-130 Pass

LCS - % Recovery


Perfluorobutanoic acid (PFBA) % 96 50-150 Pass

Perfluoropentanoic acid (PFPeA) % 110 50-150 Pass

Perfluorohexanoic acid (PFHxA) % 91 50-150 Pass

Perfluoroheptanoic acid (PFHpA) % 95 50-150 Pass

Perfluorooctanoic acid (PFOA) % 91 50-150 Pass

Perfluorononanoic acid (PFNA) % 93 50-150 Pass

Perfluorodecanoic acid (PFDA) % 95 50-150 Pass

Perfluoroundecanoic acid (PFUnA) % 82 50-150 Pass

Perfluorododecanoic acid (PFDoA) % 87 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) % 93 50-150 Pass

Perfluorotetradecanoic acid (PFTeDA) % 94 50-150 Pass

LCS - % Recovery


Perfluorooctane sulfonamide (FOSA) % 90 50-150 Pass

N-methylperfluoro-1-octane sulfonamide (N-MeFOSA) % 101 50-150 Pass

N-ethylperfluoro-1-octane sulfonamide (N-EtFOSA) % 105 50-150 Pass

2-(N-methylperfluoro-1-octane sulfonamido)-ethanol (N-MeFOSE) % 113 50-150 Pass

2-(N-ethylperfluoro-1-octane sulfonamido)-ethanol (N-EtFOSE) % 133 50-150 Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 25 of 34



PassLimits

QualifyingCode

N-ethyl-perfluorooctanesulfonamidoacetic acid (N-EtFOSAA) % 104 50-150 Pass

N-methyl-perfluorooctanesulfonamidoacetic acid (N-MeFOSAA) % 108 50-150 Pass

LCS - % Recovery


Perfluorobutanesulfonic acid (PFBS) % 89 50-150 Pass

Perfluoropentanesulfonic acid (PFPeS) % 86 50-150 Pass

Perfluorohexanesulfonic acid (PFHxS) % 89 50-150 Pass

Perfluoroheptanesulfonic acid (PFHpS) % 102 50-150 Pass

Perfluorooctanesulfonic acid (PFOS) % 92 50-150 Pass

Perfluorodecanesulfonic acid (PFDS) % 64 50-150 Pass

LCS - % Recovery


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2 FTS) % 95 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2 FTS) % 88 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2 FTS) % 119 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid (10:2 FTS) % 117 50-150 Pass

LCS - % Recovery

Heavy Metals

Arsenic % 97 80-120 Pass

Cadmium % 100 80-120 Pass

Chromium % 104 80-120 Pass

Copper % 107 80-120 Pass

Lead % 111 80-120 Pass

Manganese % 103 80-120 Pass

Mercury % 119 75-125 Pass

Nickel % 106 80-120 Pass

Zinc % 101 80-120 Pass


LimitsPass

LimitsQualifying

Code

Spike - % Recovery

Perfluoroalkyl carboxylic acids (PFCAs) Result 1

Perfluorobutanoic acid (PFBA) M17-Au29721 CP % 101 50-150 Pass

Perfluoropentanoic acid (PFPeA) M17-Au29721 CP % 113 50-150 Pass

Perfluorohexanoic acid (PFHxA) M17-Au29721 CP % 100 50-150 Pass

Perfluoroheptanoic acid (PFHpA) M17-Au29721 CP % 100 50-150 Pass

Perfluorooctanoic acid (PFOA) M17-Au29721 CP % 98 50-150 Pass

Perfluorononanoic acid (PFNA) M17-Au29721 CP % 95 50-150 Pass

Perfluorodecanoic acid (PFDA) M17-Au29721 CP % 102 50-150 Pass

Perfluoroundecanoic acid (PFUnA) M17-Au29721 CP % 106 50-150 Pass

Perfluorododecanoic acid (PFDoA) M17-Au29721 CP % 91 50-150 Pass

Perfluorotridecanoic acid (PFTrDA) M17-Au29721 CP % 97 50-150 Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Au29721 CP % 111 50-150 Pass

Spike - % Recovery

Perfluoroalkane sulfonamides (PFASAs) Result 1

Perfluorooctane sulfonamide(FOSA) M17-Au29721 CP % 90 50-150 Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Au29721 CP % 102 50-150 Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Au29721 CP % 101 50-150 Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Au29721 CP % 92 50-150 Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Au29721 CP % 127 50-150 Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 26 of 34



LimitsPass

LimitsQualifying

Code

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Au29721 CP % 104 50-150 Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Au29721 CP % 118 50-150 Pass

Spike - % Recovery

Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Result 1

Perfluorobutanesulfonic acid(PFBS) M17-Au29721 CP % 96 50-150 Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Au29721 CP % 86 50-150 Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Au29721 CP % 95 50-150 Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Au29721 CP % 104 50-150 Pass

Perfluorooctanesulfonic acid(PFOS) M17-Au29721 CP % 99 50-150 Pass

Perfluorodecanesulfonic acid(PFDS) M17-Au29721 CP % 83 50-150 Pass

Spike - % Recovery

n:2 Fluorotelomer sulfonic acids Result 1

1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Au29721 CP % 95 50-150 Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Au29721 CP % 100 50-150 Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Au29721 CP % 126 50-150 Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Au29721 CP % 144 50-150 Pass

Spike - % Recovery













Spike - % Recovery









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 27 of 34



LimitsPass

LimitsQualifying

Code



Spike - % Recovery








Spike - % Recovery






Spike - % Recovery













Spike - % Recovery









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 28 of 34



LimitsPass

LimitsQualifying

Code



Spike - % Recovery








Spike - % Recovery






Spike - % Recovery

Polycyclic Aromatic Hydrocarbons Result 1

Acenaphthene M17-Au29808 NCP % 99 70-130 Pass

Acenaphthylene M17-Au29808 NCP % 107 70-130 Pass

Anthracene M17-Au29808 NCP % 111 70-130 Pass

Benz(a)anthracene M17-Au29808 NCP % 104 70-130 Pass

Benzo(a)pyrene M17-Au29808 NCP % 115 70-130 Pass

Benzo(b&j)fluoranthene M17-Au29808 NCP % 111 70-130 Pass

Benzo(g.h.i)perylene M17-Au29808 NCP % 111 70-130 Pass

Benzo(k)fluoranthene M17-Au29808 NCP % 121 70-130 Pass

Chrysene M17-Au29808 NCP % 103 70-130 Pass

Dibenz(a.h)anthracene M17-Au29808 NCP % 127 70-130 Pass

Fluoranthene M17-Au29808 NCP % 101 70-130 Pass

Fluorene M17-Au29808 NCP % 107 70-130 Pass

Indeno(1.2.3-cd)pyrene M17-Au29808 NCP % 123 70-130 Pass

Naphthalene M17-Au29808 NCP % 100 70-130 Pass

Phenanthrene M17-Au29808 NCP % 111 70-130 Pass

Pyrene M17-Au29808 NCP % 103 70-130 Pass

Spike - % Recovery

Heavy Metals Result 1

Arsenic M17-Au29147 NCP % 95 75-125 Pass

Cadmium M17-Au29147 NCP % 101 75-125 Pass

Chromium M17-Au29147 NCP % 120 75-125 Pass

Copper M17-Au29147 NCP % 107 75-125 Pass

Lead M17-Au29147 NCP % 110 75-125 Pass

Manganese M17-Au29147 NCP % 106 75-125 Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 29 of 34



LimitsPass

LimitsQualifying

Code

Mercury M17-Au29147 NCP % 102 70-130 Pass

Nickel M17-Au29147 NCP % 107 75-125 Pass

Zinc M17-Au29147 NCP % 107 75-125 Pass


LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluoropentanoic acid (PFPeA) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorohexanoic acid (PFHxA) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluoroheptanoic acid (PFHpA) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorooctanoic acid (PFOA) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorononanoic acid (PFNA) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorodecanoic acid (PFDA) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluoroundecanoic acid (PFUnA) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorododecanoic acid (PFDoA) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Duplicate


Perfluorooctane sulfonamide(FOSA) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Au29720 CP ug/kg < 10 < 10 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Au29720 CP ug/kg < 10 < 10 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 30 of 34


Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Au29720 CP ug/kg < 10 < 10 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Au29720 CP ug/kg < 5 < 5 <1 30% Pass

Duplicate


% Moisture M17-Au29728 CP % 20 20 3.0 30% Pass

Duplicate













Duplicate









Duplicate






Perfluorooctanesulfonic acid(PFOS) M17-Au29730 CP ug/kg < 5 < 5 <1 30% Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 31 of 34


Duplicate






Duplicate


% Moisture M17-Au29738 CP % < 1 < 1 <1 30% Pass

Duplicate













Duplicate









Duplicate






Perfluorooctanesulfonic acid(PFOS) M17-Au29740 CP ug/kg 11 11 2.0 30% Pass




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 32 of 34


Duplicate






Duplicate

Polycyclic Aromatic Hydrocarbons Result 1 Result 2 RPD

Acenaphthene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Acenaphthylene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Anthracene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benz(a)anthracene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(a)pyrene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(b&j)fluoranthene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(g.h.i)perylene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Benzo(k)fluoranthene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Chrysene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Dibenz(a.h)anthracene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Fluoranthene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Fluorene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Indeno(1.2.3-cd)pyrene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Naphthalene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Phenanthrene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Pyrene M17-Au29688 NCP mg/kg < 0.5 < 0.5 <1 30% Pass

Duplicate

Heavy Metals Result 1 Result 2 RPD

Aluminium M17-Au29137 NCP mg/kg 15000 16000 8.0 30% Pass

Arsenic M17-Au29147 NCP mg/kg 27 27 <1 30% Pass

Cadmium M17-Au29147 NCP mg/kg < 0.4 < 0.4 <1 30% Pass

Chromium M17-Au29147 NCP mg/kg 47 47 <1 30% Pass

Copper M17-Au29147 NCP mg/kg 6.7 6.6 <1 30% Pass

Iron M17-Au29137 NCP mg/kg 69000 67000 4.0 30% Pass

Lead M17-Au29147 NCP mg/kg 15 16 1.0 30% Pass

Manganese M17-Au29147 NCP mg/kg 8.4 8.4 <1 30% Pass

Mercury M17-Au29147 NCP mg/kg < 0.1 < 0.1 <1 30% Pass

Nickel M17-Au29147 NCP mg/kg < 5 < 5 <1 30% Pass

Zinc M17-Au29147 NCP mg/kg 15 14 4.0 30% Pass

Duplicate


% Moisture M17-Au29749 CP % 3.5 3.3 4.0 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 33 of 34


Comments









Code Description

N07Please note:- These two PAH isomers closely co-elute using the most contemporary analytical methods and both the reported concentration (and the TEQ) apply specifically tothe total of the two co-eluting PAHs


N11


Authorised By



Alex Petridis Senior Analyst-Organic (VIC)

Bryan Wilson Senior Analyst-Metal (QLD)


Jonathon Angell Senior Analyst-Inorganic (QLD)


Joseph Edouard Senior Analyst-Organic (VIC)

Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 34 of 34






Abbotsford

VIC 3067


Report 562180-L



Received Date Sep 07, 2017


0990_SS176_170821

0990_SS186_170821

0990_SS188_170821







Perfluoropentanoic acid (PFPeA)N11 0.01 ug/L N090.01 < 0.01 < 0.01 < 0.01

Perfluorohexanoic acid (PFHxA)N11 0.01 ug/L N090.02 < 0.01 < 0.01 < 0.01

Perfluoroheptanoic acid (PFHpA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluorooctanoic acid (PFOA)N11 0.01 ug/L < 0.01 < 0.01 N090.01 < 0.01

Perfluorononanoic acid (PFNA)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01






13C4-PFBA (surr.) 1 % 73 75 74 68

13C5-PFPeA (surr.) 1 % 84 88 86 79

13C5-PFHxA (surr.) 1 % 94 94 93 81

13C4-PFHpA (surr.) 1 % 93 89 90 79

13C8-PFOA (surr.) 1 % 88 87 84 72

13C5-PFNA (surr.) 1 % 76 78 76 61

13C6-PFDA (surr.) 1 % 68 70 71 48

13C2-PFUnDA (surr.) 1 % 48 48 49 36

13C2-PFDoDA (surr.) 1 % 38 36 37 31

13C2-PFTeDA (surr.) 1 % 20 18 19 15









13C8-FOSA (surr.) 1 % 58 56 60 47

D3-N-MeFOSA (surr.) 1 % 27 24 25 24



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 1 of 12





0990_SS176_170821

0990_SS186_170821

0990_SS188_170821






D5-N-EtFOSA (surr.) 1 % 17 15 15 14

D7-N-MeFOSE (surr.) 1 % 32 31 30 26

D9-N-EtFOSE (surr.) 1 % 24 23 21 18

D5-N-EtFOSAA (surr.) 1 % 62 63 67 57

D3-N-MeFOSAA (surr.) 1 % 60 63 66 52


Perfluorobutanesulfonic acid (PFBS)N11 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluoropentanesulfonic acid (PFPeS) 0.01 ug/L < 0.01 < 0.01 < 0.01 < 0.01

Perfluorohexanesulfonic acid (PFHxS)N11 0.01 ug/L N090.07 < 0.01 N090.04 0.02




13C3-PFBS (surr.) 1 % 91 91 90 86

18O2-PFHxS (surr.) 1 % 85 86 86 81

13C8-PFOS (surr.) 1 % 59 60 61 48






13C2-4:2 FTS (surr.) 1 % 84 78 82 81

13C2-6:2 FTS (surr.) 1 % 77 72 74 73

13C2-8:2 FTS (surr.) 1 % 56 55 60 47

PFASs Summations





Sum of PFASs (n=28) 0.1 ug/L 0.39 < 0.1 0.38 0.85





pH (off) 0.1 pH Units 8.0 7.3 8.6 8.0



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 2 of 12






Perfluoroalkyl carboxylic acids (PFCAs) Brisbane Sep 15, 2017 14 Day


Perfluoroalkane sulfonamides (PFASAs) Brisbane Sep 15, 2017 14 Day


Perfluoroalkane sulfonic acids & Perfluoroalkane sulfonates (PFSAs) Brisbane Sep 15, 2017 14 Day


n:2 Fluorotelomer sulfonic acids Brisbane Sep 15, 2017 14 Day


AUS Leaching Procedure Brisbane Sep 15, 2017 7 Days




ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 3 of 12


.Company Name: Coffey Environments Pty Ltd VIC Order No.: Received: Sep 7, 2017 12:00 AMAddress: Level 1, 436 Johnston Street Report #: 562180 Due: Sep 14, 2017




Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Cation E

xchange Capacity

Per- and P


ubstances(P

FA

Ss)





External Laboratory


Matrix LAB ID

1 0990_SS168_170821

Aug 31, 2017 Soil M17-Se07424 X X X X

2 0990_SS169_170821

Aug 31, 2017 Soil M17-Se07425 X X X

3 0990_SS170_170821

Aug 31, 2017 Soil M17-Se07426 X X X X

4 0990_SS171_170821

Aug 31, 2017 Soil M17-Se07427 X X X

5 0990_SS172_170821

Aug 31, 2017 Soil M17-Se07428 X X X X









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 4 of 12






Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Cation E

xchange Capacity

Per- and P


ubstances(P

FA

Ss)





170821

7 0990_SS174_170821

Aug 31, 2017 Soil M17-Se07430 X X X X

8 0990_SS175_170821

Aug 31, 2017 Soil M17-Se07431 X X X

9 0990_SS176_170821

Aug 31, 2017 Soil M17-Se07432 X X X X

10 0990_SS177_170821

Aug 31, 2017 Soil M17-Se07433 X X X

11 0990_SS178_170821

Aug 31, 2017 Soil M17-Se07434 X X X X

12 0990_SS179_170821

Aug 31, 2017 Soil M17-Se07435 X X X

13 0990_SS180_ Aug 31, 2017 Soil M17-Se07436 X X X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 5 of 12






Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Cation E

xchange Capacity

Per- and P


ubstances(P

FA

Ss)





170821

14 0990_SS181_170821

Aug 31, 2017 Soil M17-Se07437 X X X

15 0990_SS182_170821

Aug 31, 2017 Soil M17-Se07438 X X X X

16 0990_SS183_170821

Aug 31, 2017 Soil M17-Se07439 X X X

17 0990_SS184_170821

Aug 31, 2017 Soil M17-Se07440 X X X X

18 0990_SS185_170821

Aug 31, 2017 Soil M17-Se07441 X X X

19 0990_SS186_170821

Aug 31, 2017 Soil M17-Se07442 X X X X









ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 6 of 12






Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Cation E

xchange Capacity

Per- and P


ubstances(P

FA

Ss)





170821

21 0990_SS188_170821

Aug 31, 2017 Soil M17-Se07444 X X X X

22 0990_SS189_170821

Aug 31, 2017 Soil M17-Se07445 X X X

23 0990_SS190_170821

Aug 31, 2017 Soil M17-Se07446 X X X X

24 0990_SS191_170821

Aug 31, 2017 Soil M17-Se07447 X X X

25 0990_SS192_170821

Aug 31, 2017 Soil M17-Se07448 X X X

26 0990_SS175_170821


27 0990_SS176_ Aug 31, 2017 AUS Leachate M17-Se07450 X X








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 7 of 12






Sample Detail

pH (1:5 A

queous extract)

Total O

rganic Carbon

AU

S Leaching P

rocedure

Moisture S

et

Cation E

xchange Capacity

Per- and P


ubstances(P

FA

Ss)





170821

28 0990_SS186_170821


29 0990_SS188_170821


Test Counts 25 25 4 25 12 4








ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 8 of 12



General

Holding Times

Units

Terms




request.










Receipt Advice.

































affected.

















ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 9 of 12




PassLimits

QualifyingCode

Method Blank













Method Blank









Method Blank








Method Blank







LimitsPass

LimitsQualifying

Code

Duplicate


Perfluorobutanoic acid (PFBA) B17-Se21582 NCP ug/L < 0.05 < 0.05 <1 30% Pass

Perfluoropentanoic acid (PFPeA) B17-Se21582 NCP ug/L 0.01 0.01 1.0 30% Pass

Perfluorohexanoic acid (PFHxA) B17-Se21582 NCP ug/L 0.03 0.03 3.0 30% Pass

Perfluoroheptanoic acid (PFHpA) B17-Se21582 NCP ug/L 0.01 0.01 2.0 30% Pass

Perfluorooctanoic acid (PFOA) B17-Se21582 NCP ug/L 0.03 0.03 3.0 30% Pass

Perfluorononanoic acid (PFNA) B17-Se21582 NCP ug/L 0.01 0.01 2.0 30% Pass

Perfluorodecanoic acid (PFDA) B17-Se21582 NCP ug/L 0.03 0.03 1.0 30% Pass

Perfluoroundecanoic acid (PFUnA) B17-Se21582 NCP ug/L 0.01 0.01 1.0 30% Pass

Perfluorododecanoic acid (PFDoA) B17-Se21582 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotridecanoic acid (PFTrDA) B17-Se21582 NCP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorotetradecanoic acid(PFTeDA) B17-Se21582 NCP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 10 of 12


Duplicate


Perfluorooctane sulfonamide(FOSA) M17-Se07449 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methylperfluoro-1-octanesulfonamide (N-MeFOSA) M17-Se07449 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethylperfluoro-1-octanesulfonamide (N-EtFOSA) M17-Se07449 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-methylperfluoro-1-octanesulfonamido)-ethanol (N-MeFOSE) M17-Se07449 CP ug/L < 0.05 < 0.05 <1 30% Pass

2-(N-ethylperfluoro-1-octanesulfonamido)-ethanol (N-EtFOSE) M17-Se07449 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-ethyl-perfluorooctanesulfonamidoaceticacid (N-EtFOSAA) M17-Se07449 CP ug/L < 0.05 < 0.05 <1 30% Pass

N-methyl-perfluorooctanesulfonamidoaceticacid (N-MeFOSAA) M17-Se07449 CP ug/L < 0.05 < 0.05 <1 30% Pass

Duplicate


Perfluorobutanesulfonic acid(PFBS) M17-Se07449 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluoropentanesulfonic acid(PFPeS) M17-Se07449 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorohexanesulfonic acid(PFHxS) M17-Se07449 CP ug/L 0.07 0.07 6.0 30% Pass

Perfluoroheptanesulfonic acid(PFHpS) M17-Se07449 CP ug/L < 0.01 < 0.01 <1 30% Pass

Perfluorooctanesulfonic acid(PFOS) M17-Se07449 CP ug/L 0.29 0.28 4.0 30% Pass

Perfluorodecanesulfonic acid(PFDS) M17-Se07449 CP ug/L < 0.01 < 0.01 <1 30% Pass

Duplicate


1H.1H.2H.2H-perfluorohexanesulfonic acid (4:2FTS) M17-Se07449 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorooctanesulfonic acid (6:2FTS) M17-Se07449 CP ug/L < 0.05 < 0.05 <1 30% Pass

1H.1H.2H.2H-perfluorodecanesulfonic acid (8:2FTS) M17-Se07449 CP ug/L < 0.01 < 0.01 <1 30% Pass

1H.1H.2H.2H-perfluorododecanesulfonic acid(10:2 FTS) M17-Se07449 CP ug/L < 0.01 < 0.01 <1 30% Pass



ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 11 of 12


Comments











N11


Authorised By



Glenn Jackson







ABN : 50 005 085 521 Telephone: +61 3 8564 5000

Page 12 of 12



Documents

Appendix I: Leachability - Laboratory Test Certificates ... · Site # 23736 Date Reported:Sep 21, 2017 Eurofins | mgt 2-5 Kingston Town Close, Oakleigh, Victoria, Australia, 3166