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1 Adminsitrative Record Page 25684

Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

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Page 1: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

1Adminsitrative Record Page 25684

Page 2: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

2Adminsitrative Record Page 25685

Page 3: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

3Adminsitrative Record Page 25686

Page 4: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

4Adminsitrative Record Page 25687

Page 5: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

64443 M L Johnson ESJWQC r1.doc

EPA method 619

Triazine Herbicides

Revised report: April 9, 2012

The report was revised to remove all detections for Sample ID: 545BSAAE-GR.

Analyst and reviewer error caused the incorrect reporting of several analytes that were

outside retention time windows and did not meet confirmation criteria.

Sample Preparation:

The water samples were extracted according to EPA method 619. All holding

times were met.

Sample Analysis Information:

The samples were analyzed for Triazine Herbicides according to EPA method 619

using a Hewlett Packard GC equipped with an NPD.

Quality Control/Assurance

Spike Recovery

A laboratory control spike (LCS) was used for quality assurance. All spike

recoveries met acceptance criteria.

Sample 545XCCART-GR,MS was designated by the client for MS/MSD

analysis. All MS/MSD acceptance criteria were met.

Method blanks

No target compound was detected at or above the reporting level.

Surrogates

Surrogate recoveries are summarized on the form 2 & 8. All surrogate

recoveries were within control limits.

Calibration

The initial and continuing calibrations were performed according to the

method. All calibration acceptance criteria were met.

Summary:

No problem was encountered. The data generated are acceptable.

Adminsitrative Record Page 25688

Page 6: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

64443 M L Johnson ESJWQC r1.doc

EPA method 8141A

Organophosphorous Compounds

Revised report: April 9, 2012

The report was revised to remove all detections for Sample ID: 545BSAAE-GR.

Analyst and reviewer error caused the incorrect reporting of several analytes that were

outside retention time windows and did not meet confirmation criteria.

Sample Preparation:

The water samples were extracted according to EPA method 3510C. All holding

times were met.

Sample Analysis Information:

The samples were analyzed for Organophosphorous Pesticides according to EPA

method 8141A using a Hewlett Packard GC equipped with an NPD.

Quality Control/Assurance

Spike Recovery

A Laboratory control spike (LCS) was used for quality assurance.

Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%.

All other spike recoveries met acceptance criteria.

Sample 545XCCART-GR,MS was designated by the client for MS/MSD

analysis. All MS/MSD acceptance criteria were met.

Method blanks

No target compound was detected at or above the reporting level.

Surrogates

Surrogate recoveries are summarized on the form 2 & 8. All surrogate

recoveries were within control limits.

Calibration

The initial and continuing calibrations were performed according to the

method. All calibration acceptance criteria were met.

Summary:

No other problem was encountered.

Adminsitrative Record Page 25689

Page 7: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

7Adminsitrative Record Page 25690

Page 8: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

8Adminsitrative Record Page 25691

Page 9: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

9Adminsitrative Record Page 25692

Page 10: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

10Adminsitrative Record Page 25693

Page 11: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

11Adminsitrative Record Page 25694

Page 12: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

12Adminsitrative Record Page 25695

Page 13: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

13Adminsitrative Record Page 25696

Page 14: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

14Adminsitrative Record Page 25697

Page 15: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

15Adminsitrative Record Page 25698

Page 16: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

16Adminsitrative Record Page 25699

Page 17: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

17Adminsitrative Record Page 25700

Page 18: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

18Adminsitrative Record Page 25701

Page 19: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

19Adminsitrative Record Page 25702

Page 20: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

20Adminsitrative Record Page 25703

Page 21: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

21Adminsitrative Record Page 25704

Page 22: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

22Adminsitrative Record Page 25705

Page 23: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

23Adminsitrative Record Page 25706

Page 24: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

24Adminsitrative Record Page 25707

Page 25: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

25Adminsitrative Record Page 25708

Page 26: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

26Adminsitrative Record Page 25709

Page 27: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

27Adminsitrative Record Page 25710

Page 28: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

28Adminsitrative Record Page 25711

Page 29: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

29Adminsitrative Record Page 25712

Page 30: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

30Adminsitrative Record Page 25713

Page 31: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

31Adminsitrative Record Page 25714

Page 32: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

32Adminsitrative Record Page 25715

Page 33: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

33Adminsitrative Record Page 25716

Page 34: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

34Adminsitrative Record Page 25717

Page 35: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

35Adminsitrative Record Page 25718

Page 36: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

36Adminsitrative Record Page 25719

Page 37: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

37Adminsitrative Record Page 25720

Page 38: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

38Adminsitrative Record Page 25721

Page 39: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

39Adminsitrative Record Page 25722

Page 40: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

40Adminsitrative Record Page 25723

Page 41: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

41Adminsitrative Record Page 25724

Page 42: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

42Adminsitrative Record Page 25725

Page 43: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

43Adminsitrative Record Page 25726

Page 44: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

44Adminsitrative Record Page 25727

Page 45: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

45Adminsitrative Record Page 25728

Page 46: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

46Adminsitrative Record Page 25729

Page 47: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

47Adminsitrative Record Page 25730

Page 48: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

48Adminsitrative Record Page 25731

Page 49: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

49Adminsitrative Record Page 25732

Page 50: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

50Adminsitrative Record Page 25733

Page 51: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

51Adminsitrative Record Page 25734

Page 52: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

52Adminsitrative Record Page 25735

Page 53: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

53Adminsitrative Record Page 25736

Page 54: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

54Adminsitrative Record Page 25737

Page 55: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

55Adminsitrative Record Page 25738

Page 56: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

56Adminsitrative Record Page 25739

Page 57: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

57Adminsitrative Record Page 25740

Page 58: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

58Adminsitrative Record Page 25741

Page 59: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

59Adminsitrative Record Page 25742

Page 60: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

60Adminsitrative Record Page 25743

Page 61: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

61Adminsitrative Record Page 25744

Page 62: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

62Adminsitrative Record Page 25745

Page 63: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

63Adminsitrative Record Page 25746

Page 64: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

64Adminsitrative Record Page 25747

Page 65: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

65Adminsitrative Record Page 25748

Page 66: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

66Adminsitrative Record Page 25749

Page 67: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

67Adminsitrative Record Page 25750

Page 68: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

68Adminsitrative Record Page 25751

Page 69: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

69Adminsitrative Record Page 25752

Page 70: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

70Adminsitrative Record Page 25753

Page 71: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

71Adminsitrative Record Page 25754

Page 72: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

72Adminsitrative Record Page 25755

Page 73: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

73Adminsitrative Record Page 25756

Page 74: Adminsitrative Page 25684 · A Laboratory control spike (LCS) was used for quality assurance. Dimethoate recovered below the 68% lower control limit in the LCS at 55.6%. All other

74Adminsitrative Record Page 25757


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