21
WWW.OZM.CZ VERSION 2014 TESTING INSTRUMENTS FOR ENERGETIC MATERIALS LABORATORIES

2014 ozm catalog

Embed Size (px)

DESCRIPTION

 

Citation preview

Page 1: 2014 ozm catalog

WWW.OZM.CZ

VERSION 2014

TESTING INSTRUMENTSFOR ENERGETIC MATERIALS LABORATORIES

Page 2: 2014 ozm catalog

CONTENTABOUT US

TOP QUALIFICATION OZM Research is a knowledge-based company formed by experienced explosives scientists and engineers with advanced academic degrees in this very special branch of chemical engineering. The company’s core business consists of testing instruments, technologies and expert services for energetic materials – explosives, propellants, pyrotechnics, and ammunition.

CUSTOMER-SUPPORTOur services do not end with sale and delivery. Our product managers are PhDs in explosives science and technology with extensive laboratory praxis and international experience in development and applications of new testing methods and instruments. This allows us to provide our customers the maximum assistance in selection and implementation of the testing instruments. Customer-oriented approach involves modifications of the standard products for better fitting the customer’s needs or development of completely new instruments tailored for a specific project. Having the high expertise in the field of explosives and munitions, we are able to provide full assistance to the customers with fitting the products into the customer’s projects, with testing methodologies, personnel training and other expert services.

EXPORT-ORIENTEDSince 1997 we have exported our products to more than 40 countries on all continents. Our major clients include military research & development centres, forensic institutes, international certification bodies, universities, explosives and ammunition manufacturers, nuclear power plants and other related industries. Our company is fully licensed for handling explosive materials and ammunition, as well as for foreign trade with these specific products.

P.15High Performance Calorimeter

P.281 m3 Explosion Chamber

P.27Minimum Ignition Energy Apparatus

P.31Sustained Combustibility Tester

OZM RESEARCH IS READY TO HELP YOU WITH YOUR TASKS IN ENERGETIC MATERIALS!

ENERGETIC MATERIALS TESTING INSTRUMENTSInstruments Application Reference Table 4

SENSITIVITY TESTS

Small-Scale Electrostatic Spark Sensitivity Tester ESD 2008A 5

Large-Scale Electrostatic Discharge Sensitivity Tester ESD LS30-MIL 6

BAM Friction Apparatus FSKM 10 7

Improved BAM Fall Hammer (Impact Tester) BFH 12 8

Consumables for BAM Friction and Fall Hammer testers 9

Koenen Test 9

THERMAL STABILITY TESTS

Vacuum Stability Tester for Explosives STABIL VI 10

Automatic Explosion Temperature Tester AET 402 11

Differential Thermal Analyzer DTA 552-Ex 12

Heating Blocks 13

Detonation Velocity Measuring System VOD 812 14

High Performance Calorimeter for Energetic Materials BCA 500 15

Detonation Calorimeter DCA5 and DCA50 16

PERFORMANCE TESTS

Laboratory Detonation Chambers 17

Industrial Detonation Chambers 18

Remote Cnc Machining for Explsoives and Rocket Fuels XSM-01 19

Time-Pressure Test Apparatus/Test for Oxidizing Liquids TPT Series 20

Software for Calculation of Detonation Parameters EXPLO5 Current version: 6.02 21

Pressure Wave Analyzer and Quantifier Prewaq 22

INTERIOR BALLISTIC TESTS

Closed vessels NV series 23

Closed Vessels RB series 23

Stojan Vessel SV-2 24

Rocket Motor Ballistic Measurement RMM 25

Subscale Rocket Motor Measurement TRM 35 25

GAS & DUST TESTING INSTRUMENTSMeasurement of Minimum Ignition Energy of Dust Dispersions MIE-D 1.2 27

Explosion Chambers for Gas and Dusts 28

Autoignition Temperature of Liquid and Solid Chemicals AIT 551 29

Self Heating Substances Tester SHT 150 30

Sustained Combustibility Tester SCT 100 31

Minimum Ignition Temperature Tester MIT 1000 32

Dust Layer Ignition Temperature Tester LIT 400 32

EXPLOSION-RESISTANT STORAGESafe Laboratory Storage of Small Explosive Samples

PORTABLE GAS-TIGHT EXPLOSION-RESISTANT CONTAINERS 34

Safe Storage Of Larger Stocks Of Explosive Samples

EXPLOSION-RESISTANT STORAGE CONTAINERS (5 – 10 kg TNT eq.) 35

Safe Storage of Larger Stocks of Explosive Samples

STORAGE MODULES FOR EXPANDING CAPACITY OF STORAGE ROOMS (10 – 1000 kg TNT eq.) 35

EXPLOSIVE PROCESSING OF METALS 37

SELECTED REFERENCES 38

Page 3: 2014 ozm catalog

INSTRUMENTS APPLICATIONS REFERENCE TABLE 5

TEST METHOD OZM INSTRUMENT

EXPLOSIVE MATERIALS APPLICATIONS

Prim

ary

Ex

plo

sive

s

Mili

tary

Hig

h Ex

plo

sive

s

Ind

ustr

ial E

xp

losi

ves

Py

rote

chni

cs

Gun

Pro

pel

lant

s

Ro

cket

Pro

pel

lant

s

Exp

losi

ve S

ubst

anc

es

Exp

losi

ve D

evic

es

Mili

tary

Qua

lifica

tio

n

Mili

tary

Sur

veill

anc

e

Pro

duc

t Qua

lity

Co

ntro

l

R&

D

Sto

rag

e &

Tra

nsp

ort

Safe

ty E

ngin

eeri

ng

Abel Test ABT-01 x x x o x o

Accelerated Ageing HBA-01, heating boxes x x x x x x x x

Bergmann-Junk Test BeJu-01 x x x x o

Differential Thermal Analysis (DTA) DTA 552-Ex x x x x x x x x x x x x x

Dutch Weight Loss Test at 90 oC (Holland Test)

HOLLAND TEST x x x x o

Explosion Temperature Test AET 402 o x x x o o o x o x o o

Heat Storage Test at 100 °C CH100-01 x x x x x

Chemical Compatibility by DTA DTA 552-Ex x x x x o o x x x x

Chemical Compatibility by VST STABIL VI x x o x x x x x x

Methyl Violet Test MVT-01 x x x x o

Thermal Stability test at 75 oC TST75-01 x x x x x x o x

Time-to-explosion Test AET 402 x x x x x x x x

Vacuum Stability Test (VST) STABIL VI o x x o x x x x x x x x

Cook-off Tests (slow, fast) SCO, FCO o x x x x x x x x x x

Friction Sensitivity TestFSKM 10 (BFST-BAM6A) o x x x x x x x x x x x

FSKM 10 (BFST-PEX3A) x o x x x x x x

Gap Tests (shock wave sensitivity) Water & UN GAP Test o x x o o o x o x x x x x

Impact Sensitivity TestBFH 10, BFH 12 o x x x x x x o x x x x x

BFH PEx x x x x x x x

Koenen Test Koenen tester o x x x x x x x x x x x

Large Scale Electrostatic Discharge Sensitivity Test

ESD LS30-MIL x o x x x o x x x x x

Small Scale Electrostatic Discharge Sensitivity Test

ESD 2008A x x x x x x x x x x x x

Time-pressure Test TPT series o x x x x x x x x x

Explosive Strength (power) Ballistic mortars BM 310,BM 765 o x x o x x

Explosive Strength (power) Trauzl test, detonation chambers o x x o x x

Explosive Brisance Tests Hess test, Kast test, detonation chambers o x x o x x

Detonation Velocity VOD 812, detonation chambers o x x o o x x x x x

Detonation Properties Calculation EXPLO5 x x x x x x x x x

Heat of Detonation DCA 5, DCA 50 x x x x x x

Shock Wave Pressure and Heat Flow in Air Blast, Closed Structures, Underwater Tests

PREWAQ, detonation chambers x x x x x x x x x

Heat of Combustion/Explosion BCA 500 x x x x x x x x x x x

Closed Vessel TestsNV series x x x x x x x x x

RB series x x x x x

Burning Rate Tests STOJAN VESSEL SV-2 x x x x x

Sub-scale Rocket Motor Tests TRM 35 x x x x x

Rocket Motor Burning Parameters RMM x x x x x x

CNC Remote Sampling and Machining

XSM-01 o x o x x x x x x

5

Chem

ica

l and

The

rma

l St

ab

ility

Tes

tsSe

nsit

ivit

y to

Ex

tern

al

Stim

uli T

ests

Exp

losi

ve P

erfo

rma

nce

Test

sIn

teri

or

Ba

llist

ic

Per

form

an

ce

Test

s

Sam

plin

g

and

Sa

mp

le

Prep

ara

tio

n

x

O

Applicable

Limited usage

Not applicable

ENERGETIC MATERIALS TESTING INSTRUMENTSFOR THERMAL STABILITY, SENSITIVITY AND PERFORMANCE TESTS

3 4

Page 4: 2014 ozm catalog

SEN

SIT

IVIT

Y T

ESTS

SEN

SITIV

ITY TES

TS

SMALL-SCALE ELECTROSTATIC SPARK SENSITIVITY TESTER

ESD 2008A

APPLICATIONElectrostatic discharge is one of the most frequent and the least characterized cause of accidental initiation of energetic materials. Sensitivity to electrostatic discharge (spark) is one of the main safety parameter crucial for the handling, processing and transportation of the energetic materials. A small-scale electrostatic spark sensitivity test determines the amount of the discharge energy required for the initiation of the tested sample. ESD 2008A is suitable for the wide range of applications ranging from the quality control of explosives processing and manufacturing to the research and development of the new explosive materials.

Designed to comply with the requirements of the following standards:

• EN 13938-2 Explosives for civil uses – Propellants and rocket propellants – Part 2: Determination of resistance to electrostatic energy

• STANAG 4490: Explosives, Electrostatic Discharge Sensitivity • MIL-STD-1751A: Safety and Performance Tests for the Qualification

of Explosives - Methods 1031, 1032 & 1033

FEATURES• ESD 2008A allows precise measurement of the spark energy

which is entirely absorbed by the sample and is capable to initiate it. Depending on the applied test method are results presented in the form of Minimum Initiation Energy (threshold) or energy level representing 50 % probability (E50).

• Tester is designed to work with the crystalline/granular high explosives, propellants, pyrotechnics and as well primary explosives.

• Tester is equipped with the two automatically operated testing stands:

• First testing stand is designed for the fixed distance of electrodes; • Second testing stand is designed for the approaching anode.• External testing assemblies is designed for the testing of the larger

amount of explosive sample.• Tester is supplied with the wide range of internal and auxiliary

capacitors allowing to carry testing within the wide range of energies at the arbitrary energy levels.

• Voltage from HV source can be driven outside of machine as an alternative HV source for an alternative application.

• Tester is not suitable for testing of the Electro Explosive Devices or simulation of electrostatic environment as well as examination of the large compact samples (eg. rocket propellant grains).

ACCESSORIES

• Designed for the precise measurement of the initiation energy of energetic materials in the range of discharge energies (from 25 μJ to 25 J).

• Apparatus can operate in the two discharge regimes – Oscillating & Damping – allowing to test sensitivity to electrostatic spark (discharge) of the various classes of energetic materials.

• Several designs of the spark gap assemblies designed according to the requirements of different standards or testing methods.

Fixed electrode testing stand Approaching anode testing stand

Left to right:ESD-30133-TA Spark gap assembly acc. to MIL-STD-1751A methods 1031 & 1033ESD-FE-TA Spark gap assembly acc. to MIL-PRF-46676B (AR)ESD-32-TA Spark gap assembly acc. to MIL-ST D-1751A methods 1032ESD-OZM-TA Spark gap assembly acc. to OZM/TNO /DTTX

LARGE-SCALE ELECTROSTATIC DISCHARGE SENSITIVITY TESTER

ESD LS30-MIL

APPLICATIONThis tester is applicable for the testing of the ESD susceptibility of the large size solid materials (typically bulk propellant grains) as well as other ESD sensitive items and munitions elements. Tester can be used to test resistance to energy in the form of ESD event of the Electro Explosive Devices and related electronics. Tester is not suitable to examine exact energy levels necessary to initiate granular energetic materials samples. Tester is capable to operate in the mode generating human body equivalent discharges.

Designed to comply with the requirements of the following standards:

• STANAG 4235, STANAG 4239, STANAG 4490 • AECTP-500, AECTP-250 • MIL-STD-331B • MIL-STD-1576 • MIL-STD-1751A

FEATURES• Tester produces discharges in the two basic testing modes: • For large-scale testing of resistance to electrostatic discharge

of energetic materials. • For the testing to determine resistance of explosive materials,

ammunition or electronic elements against electrostatic discharge generated by the human body.

• Remote controlled operation of the apparatus using optical communication for safe distance operation up to several hundreds of meters.

• Variable setting of discharge parameters and energy by the combination of external HV resistors and capacitors.

• Simple reversion of electrical polarity of the high voltage output.• Robust case with IP54 protection for easy handling and outdoor

applications.• Testing samples weighing up to several kilograms by a series or

individual discharges with constant spark energy of up to 17 J.• The instrument can be used for evaluation of influence of

temperature on the spark sensitivity.

ACCESSORIES

• Designed for the determination of the resistance of high explosives, propellants, ammunition elements or electronic devices to electrostatic discharge. Discharge parameters are adjustable in the range of 0 - 30 kV voltage and 0 - 17 J spark energy.

• Two modes of testing – Oscillating & Damping.

• Single or consecutive repeated discharges.

• Set of changeable inbuilt capacitors and resistors.

• Capable of testing various type and amount of solid or granular form of samples up to several kilograms.

High voltage probe Remote control Set-up of testing container

5 6

Page 5: 2014 ozm catalog

{

SEN

SIT

IVIT

Y T

ESTS

SEN

SITIV

ITY TES

TS

BAM FRICTION APPARATUS

FSKM 10

APPLICATIONFriction of explosives between hard surfaces is one of the most frequent causes of accidental explosions. Determination of friction sensitivity is thus a necessary part of characterization of new explosives, modified formulations or manufacturing conditions, as well as for defining influences of impurities or ageing. It is also used in quality control of manufactured explosives, surveillance of in-service explosives and transport/storage classification of explosive materials.

Designed to comply with the requirements of the following standards of testing:

• UN Recommendation on the Transport of Dangerous Goods, Manual of Tests and Criteria, 2010 - Test 3 (b) (i)

• STANAG 4487: Explosives, Friction Sensitivity Tests• MIL-STD-1751A: Safety and Performance Tests for the Qualification

of Explosives – Method 1024• EN 13631-3:2004 Explosives for Civil Uses – High Explosives

– Part 3: Determination of Sensitiveness to Friction of Explosives• European Commission Directive 92/69/EEC, Method A14:

Explosive Properties

FEATURES• Completely stainless-steel design (friction device, loading arms,

all sets of weights and even working table frame).• A unique ability to interchange the entire loading arm.• Standard 6-position loading arm along with two sets of weights

provides loads from 0.5 N to 360 N.• Light 3-position loading arm, specially designed for testing highly

sensitive substances, along with two sets of weights provides loads from 0.1 N to 60 N.

• Protective shield to protect the personnel against fragments arise out of porcelain plate or peg.

• Digitally-controlled step motor allows to achieve high precision and control of the porcelain plate movement.

• Working table covered by electrostatic conductive surface.• Wide range of accessories.• Premium consumables at reasonable prices.

ACCESSORIES

• Designed for determination of friction sensitivity of energetic materials in a wide range of friction loads (from 0.1 to 360 N) in accordance with the BAM procedure.

• Robust stainless steel design.

• Two loading arms are available – for sensitivity testing of highly sensitive explosives as well as less sensitive explosives at one apparatus.

Standard 6-position loading arm in storage case Porcelain Plate and Peg Set of weights PEx-5 Set of weights PEx-14

IMPROVED BAM FALL HAMMER (IMPACT TESTER)

BFH 12

APPLICATIONImpact sensitivity is one of the most important characteristics of energetic materials defining their safety in handling, processing or transportation. Its determination is a necessary part of characterization of new explosives, modified formulations or manufacturing conditions, as well as for defining influences of impurities or ageing. It is also used in quality control of manufactured explosives, surveillance of in-service explosives and transport/storage classification of explosive materials.

FEATURES• Unique Drop Weight Exchange Window.• Protective box with standard instrument parts.• Wide range of impact energies from 0.25 J to 100 J.• Six drop weights from 0.25 kg to 10 kg available.• Drop weights with brass grooves for friction reduction.• Electromagnetic or pneumatic releasing device operated via remote controller.• Steel file plates for alternative testing of impact stimuli.• Wide range of accessories.• Premium consumables at reasonable prices.

Designed to comply with the requirements of the following standards of testing:

• UN Recommendation on the Transport of Dangerous Goods, Manual of Tests and Criteria, 2010 - Test 3 (a) (ii)

• STANAG 4489: Explosives, Impact Sensitivity Tests • MIL-STD-1751A: Safety and Performance Tests for the Qualification

of Explosives – Method 1015• EN 13631-4:2002 Explosives for Civil Uses – High Explosives – Part 4:

Determination of Sensitiveness to Impact of Explosives• European Commission Directive 92/69/EEC, Method A14: Explosive Properties

Other available versions:

• Standard BAM Fall Hammer BFH-10 • Automated BAM Fall Hammer BFH-12A equipped with automated lifting mechanism• Small BAM Fall Hammer BFH-PEx designed for testing highly sensitive substances

ACCESSORIES

• Designed for determination of impact sensitivity of energetic materials in accordance with the BAM procedure.

• Unique Drop Weight Exchange Window.

Steel guide rings and cylinders

Sampling spoonsSet of drop weightsFile plate holder

Drop Weight Exchange Window

87

Page 6: 2014 ozm catalog

THER

MA

L S

TAB

ILIT

Y T

ESTS

SEN

SITIV

ITY TES

TS

ACCESSORIES

VACUUM STABILITY TESTER FOR EXPLOSIVES

STABIL VI

APPLICATIONVacuum stability test is frequently used for determination of chemical stability and compatibility of energetic materials and for quality tests of energetic ingredients. The test is able to discover chemical instability of energetic materials due to the presence of destabilizing impurities, incompatibility with surrounding materials, or ageing, with high sensitivity, precision and reproducibility. Vacuum stability test finds its wide application in qualification, surveillance, manufacture, quality control and research & development of a wide range of energetic materials.

Designed to comply with the requirements of the following standards of testing:

• STANAG 4556, 4147, 4022/4, 4023, 4230, 4284 and 4566

FEATURES• Fully replaces old apparatuses with mercury-containing

manometer tubes.• User-friendly software WINSTAB, automatic measurement

and evaluation.• Continuous volume-time record as a result of testing.• Adaptable design of instrument and software according

to customer’s needs.• Calibrated volumes of the test tubes and pressure sensors.• Automatic temperature calibration.• Up to 20 simultaneous independent measurements

in two heating blocks.

WINSTAB software : Examples of experiment evaluation

Pressure transducer and test tube

KOENEN TEST

CONSUMABLES FOR BAM FRICTION AND FALL HAMMER TESTERS

• Designed for determination of thermal sensitivity of solid and liquid substances.

APPLICATIONKoenen test is used to determine the sensitiveness of solid and liquid substances to the effect of intense heat under high confinement. Samples of the test material are confined in a steel tube fitted with an orifice plate at the top end.

Data obtained from the Koenen test can be used in determining a substance’s shipping classification and for evaluating the degree of venting required to avoid an explosion during processing operations.

FEATURES• Durable design –body of the protective welded

box is made of stainless steel.• Remotely controlled.• Full set of accessories and consumables.

Designed to comply with the requirements of the following standards of testing:

• STANAG 4491: Explosives, Thermal Sensitiveness and Explosiveness Tests

• UN Recommendations on the Transport of Dangerous Goods, Manual of Tests and Criteria, 2010 - Test 1 (b)

• European Commission Directive 92/69/EEC, Method A14: Explosive Properties

ACCESSORIES

Koenen tube(before/after test)

All our consumables are manufactured in EU with emphasis on compliance with requests all related standards, as are:

• UN Recommendation on Transport of Dangerous Goods

• STANAGs

• MIL-STD

• EN standards

Part-No. Description BFST-Pt-100 Porcelain Plates, 25 x 25 x 5 mm, Set of 100 pcs

BFST-Pn-400 Porcelain Pegs, Ø10 x 15 mm, Set of 400 pcs

Part-No. Description

BFH-SC-100 Steel Guide Rings, Ø16/10 x 13mm, Set of 100 pcs

BFH-SR-200 Steel Cylinders, Ø10 x 10 mm, Set of 200 pcs

BFH-FP-100 File Plates, 20 x 20 x 5 mm, Set of 100 pcs

Porcelain plates and Porcelain pegs for BAM Friction testers

Steel guide rings and Steel cylinders for BAM Fall Hammers (Impact testers)

• Unique design of test tubes and transducer connections.

• Long tradition – first electronic VST tester developed over 40 years ago.

• Automatic measurement and evaluation.

• High precision and long term accuracy of pressure measurement.

109

Page 7: 2014 ozm catalog

DETAIL OF FURNACE

THER

MA

L S

TAB

ILIT

Y T

ESTS

THER

MA

L STA

BILITY

TESTS

APPLICATION DTA 552-Ex was developed specifically for evaluation of thermal stability, purity, compatibility and decomposition parameters of energetic materials, which explosion may cause damage to standard commercial analyzers.

DTA as a method is applied for evaluation of thermal stability of explosive materials, their purity (melting point, solidification point), compatibility, thermal decomposition parameters. It is used in quality control of manufactured explosives, characterization and qualification of new explosives, surveillance of in-service explosives, research & development, and many other testing programs.

FEATURES• Robust design resistant against explosion of up

to several hundred milligrams of explosives. • High sensitivity due to direct contact of one thermocouple

with each sample.• High precision and accuracy.• Large variety of accessories.• User-friendly software for data acquisition, analysis and archiving.• Low costs of investment and operation.

Designed to comply with the requirements of the following standards of testing:

• STANAG 4515: Explosives, Thermal Characterization by Differencial Thermal Analysis, Differention Scanning Calorimetry and Thermogravimetric Analysis

DETAIL OF FURNACE

APPLICATION Explosion (ignition) temperature is defined as the temperature at which an explosive sample explodes (deflagrates, ignites) when heated with constant rating rate. AET 402 can also be used for determination of time-to-explosion. It is defined as the time needed for ignition of a sample at a given constant temperature. The tester consists of a temperature controller and a heating block with multiple holes.

FEATURES• Measures up to 5 samples simultaneously.• Automatic determination of the explosion

temperature using an explosion sensor.• Saves operator’s time by eliminating the need to continuously

watch the whole experiment and manually record the explosion temperature.

Designed to comply with the requirements of the following standards of testing:

• STANAG 4491: Explosives, Thermal Sensitiveness and Explosiveness Tests

• Thermal stability testing instrument designed specifically for differential thermal analysis of explosive materials which explosion may cause damage to standard commercial analyzers.

• Designed for determination of the explosion (ignition) temperature at constant heating rate or time-to-explosion in isothermal mode.

AUTOMATIC EXPLOSION TEMPERATURE TESTER

AET 402

DIFFERENTIAL THERMAL ANALYZER

DTA 552-EX

1211

Page 8: 2014 ozm catalog

• Designed for wide range of thermal stability tests.

PER

FOR

MA

NC

E TE

STS

THER

MA

L STA

BILITY

TESTS

APPLICATIONDetonation velocity is one of the main explosion parameter. The determination of the detonation velocity is based upon the measurement of the time interval needed for the detonation wave to travel a known distance through the explosive being tested.

This method is based on the ability of the optical fibre to accept a light signal when the detonation wave arrives, and to transmit that signal to suitable measuring equipment, which enables precise recording of the time interval between the two signals. From the measured time interval and the corresponding distance travelled by the detonation wave, the detonation velocity is calculated.

FEATURES • Battery charged instrument equipped by internal memory

for storage of 100 results, 4-line LCD display and water-proof keyboard.

• Supplied accessories include optical extension line, optical probes, USB communication cable and software WinVOD for data acquisition.

• Impact resistant and water proof transport case. • 7 independent timers measuring the time intervals

between the illuminations of 8 optical probes.• Simple operation.

Designed to comply with the requirements of the following standards of testing:

• EN 13631-14 Explosives for civil uses – High explosives – Part 14: Determination of velocity of detonation

• Instrument is designed for precise measurement of detonation velocity and/or the burning rate of explosives based on optical fibre method.

• Optical probes are resistant against humidity and RF disturbances and allow simple operation and fast setup of measurement.

PRODUCT DETAILS

DETONATION VELOCITY MEASURING SYSTEM

VOD 812

HEATING BLOCKS

Abel Heat Tester

Bergmann-Junk Tester Heating Block for Accelerated Ageing Details of transport case

APPLICATIONTraditional tests for determination of chemical stability of energetic materials (mainly propellants) are based on heating samples at elevated temperatures and detecting their reactive decomposition products (NOX). This detection can be based on visual identification of colored gases above the sample (Heat Storage Test at 100 °C), color change of indicator papers (Abel Test, Methyl Violet Test), titration of acidity in water extract of the gases (Bergmann-Junk Test) or determination of weight loss (Holland Test). Heating at elevated temperatures is also used in artificial ageing of propellants (STANAG 4117, AOP-48).

Instruments for the heat tests consist of temperature controllers and heating blocks, each containing multiple (4 – 45) holes for the test tubes of appropriate size. Glass test tubes used for each different test are supplied with the instruments as well.

Standard models of heating blocks with the given number of holes are supplied, and further models with different number or dimensions of holes are available upon request.

FEATURES• High precision of temperature control.• High safety (independent limit controller including switches against

exceeding safety temperature).• Robust stainless steel design and long-term reliability.

LIST OF AVAILABLE HEATING BLOCKS• ABEL HEAT TESTER - ABT-01• BERGMANN-JUNK TESTER - BeJu-01• METHYL VIOLET TESTER - MVT-01• HEATING BLOCK FOR ACCELERATED AGEING - HBA-01• DUTCH WEIGHT LOSS TEST (HOLLAND TEST)• INSTRUMENT FOR HEAT STORAGE TEST AT 100 °C - CH100-01• other upon request

The instruments comply with relevant standards for particular heat tests and can be further modified upon customer’s request or designed type-specific.

1413

Page 9: 2014 ozm catalog

THER

MA

L S

TAB

ILIT

Y T

ESTS

PER

FOR

MA

NC

E TESTS BCA500 PRESENTS ONLY ONE UNIT WITH

FOLLOWING PARTS INCLUDED: •Calorimetric bath with fixed bucket and precise level sensors• True static (isoperibolic) jacket with electronic regulation• Temperature measuring system• Microprocessor controller for device operation

with interface for PC, balance and LAN• PC interface with 6.5” LCD color touch screen,

wireless keyboard and mouse• 2 water tanks for simultaneous conditioning and testing• Thermostat for water chilling and stirrer for circulation

DETONATION CALORIMETER

DCA5 AND DCA50

PRODUCT DETAILS

• DCA5 and DCA50 are large scale calorimeters for determination of detonation heat of explosive samples.

APPLICATIONTypical application of DCA5 and DCA50 is in research, development and quality control assurance in civil and military institutions such as universities, academies, research laboratories, production companies, ammunition acceptance laboratories and others. Testing vessels with volume 5 and 14.5 liters provides excellent option for investigation of• Single and double based gun propellants• Double based rocket fuels• Composite rocket fuels• Military grade high explosives

(TNT, PETN, RDX, HMX, FOX-7 etc)• Industrial explosives (dynamites, emulsions, slurries, ANFO, etc)• Sample can have weight of 50 g of high explosives in liquid,

powder or pressed form.

FEATURES•High resolution of thermometers 0.00001 °C.•Inbuilt data acquisition with 2 MHz sampling rate.• High strength stainless steel detonation chamber for testing

in vacuum, air, nitrogen, argon, oxygen etc.• Fully automatic operation, data acquisition and results evaluation

with inbuilt friendly interface.• Advanced system for water conditioning, dosing, emptying is

integrated into main unit and includes all water tanks, valves, heaters, chillers, level and temperature sensors.

•Inbuilt manipulator for bomb positioning and detachable cart.

• BCA 500 is an advanced bomb calorimeter designed for rapid determination of gross calorific values of solid and liquid samples.

• BCA500 and its accessories were designed according to highest industrial demands and always respect the best possible output according to application.

APPLICATION• Fuels – oil, coal, wood and many others• Waste material – plastics, water containing samples,

PVC and others• Polymers and other industrial materials• Metal powders and high energy composite materials with AP• Energetic materials – propellants, pyrotechnics, and other

ignitable explosives

TOP FEATURES OF CALORIMETRIC SYSTEM BCA500 ARE:• Tailored design of accessories and consumables provides

excellent solution for any application especially in industry of fuels and energetic materials.

• High resolution of thermometers - 0.00001 °C.• All systems are implemented into one unit. • Calorimeter needs no water supply and all process water is

stored inside inner tanks.• Two tanks for non-stop testing and operation time minimizing.• Advanced water management with integrated chillers provides

conditioning and precise dosing.• Operation interface is easy to operate with LCD touch screen,

wireless keyboard and mouse.• Fully automated data acquisition, evaluation and management

with remote access features.

HIGH PERFORMANCE CALORIMETER FOR ENERGETIC MATERIALS

BCA 500

ACCESSORIES

Inbuilt water conditioning system Filling arrangement for vessels EX-1/2 Bomb DC-1Bomb OX-1

Testing conditions in BCA500 bombs

BombConditions

Use(No detonation regime allowed)

Vacuum Air Oxygen Inert

OX-1/2 NO NO YES YES Fuels and other combustible materials.Bayonet lock for fast and easy operation.

DC-1 YES YES NO YES Pyrotechnic mixtures. High pressure design.

EX-1/2 YES YES NO YES Fuels and other combustible materials. Ignitable explosives and propellants. Rigid design with thread lock.

Dynamic Pressure Record of pressed TNT charge DCA 5 on-site

1615

Page 10: 2014 ozm catalog

PER

FOR

MA

NC

E TE

STS

PER

FOR

MA

NC

E TESTS

LABORATORY DETONATION CHAMBERS

Laboratory detonation chambers allow to safely carry out detonation experiments directly inside explosives laboratories. They can be used for scientific investigations, research, development and testing in the area of energetic materials, confined explosions and related applications such as explosive forming of metals or safe disposal of laboratory explosive wastes.

Laboratory detonation chambers are designed to withstand repeated detonations of up to 250 g TNT. The explosive charges are installed on a working table inside the chambers (KV-series) or hanged through the top lid (LDC-series) and safely fired by electric detonators connected to firing contacts. Gas-tight valves on the chamber body enable creating different gas atmospheres within the chamber, as well as sampling, evacuation and flushing of the post-explosion gases. The chambers are furthermore equipped with multiple ports, which can be used for installing various optical or electrical measuring instruments for investigations of the detonation processes.

Several full-scale performance and sensitivity tests can be safely executed within the chambers such as measurement of detonation velocity, pressure-time and temperature-time records of confined explosions, brisance and explosive power tests (Hess, Kast, PDT, Trauzl), high-speed optical and X-ray photography, gap tests, cook-off tests, electrostatic discharge sensitivity tests, large-scale thermal stability tests etc.

INDUSTRIAL DETONATION CHAMBERS

Industrial detonation chambers are automated machinery designed to withstand repeated detonations with equivalent of 2 - 16 kg TNT and applied in various programs, such as: • Large-scale or frequent scientific

detonation experiments.

• Quality control tests in explosives or ammunition manufacture.

• Explosive working of metals (hardening, cladding, welding, cutting, pressing).

• Environmentally friendly disposal of explosive wastes.

• Forensic investigation and safe disposal of improvised explosive devices.

During more than 40 years of service, these industrial detonation chambers have proven to have a long service life (> 100,000 detonations) and reliable, safe and simple operation with low investment and operating costs. The industrial detonation chambers are manufactured in two design lines – vertical and horizontal – both equipped with hydraulic systems, control panels for fully automatic remote operations and, where required, with appropriate pollution abatement systems for off-gases. Electrical and optical measuring equipment for investigation of the explosion processes can be installed in the multiple ports at the chamber body.

VERTICAL DETONATION CHAMBERS

• For 2 – 5 kg TNT

• Open and close with back-folded cupola

• Suitable for compact charges

• Equipped with anti-fragment shields

Laboratory detonation chamber LDC25

Laboratory Detonation Chambers

Type TNT Equivalent (g) Weight (kg) Material Atmosphere

LDC-10 10 30

Stainless steelVacuum, air, inert gas

or oxygen (up to 30 bar)

LDC-25 25 60

LDC-50 50 190

KV-150M2 150 1100Steel Air or inert gas

(up to 1 bar) KV-250M4 250 2200

PRESSING TOOLSSeveral sensitivity or performance tests (gap tests, brisance tests, detonation velocity, etc) require the use of samples of high explosives or pyrotechnics in a form of pressed pellets. OZM Research offers a wide range of pressing tools for preparation of the charges, ranging from 5 mm to 100 mm charge diameter and creating pellets with flat surfaces, detonator entries, central holes or conical shapes. We can also provide a complete pressing station equipped with remote control hydraulic press and installed within an explosion-proof bunker. Design of the pressing tools and complete station originates from long-term experience with these manufacturing tools in the explosives and ammunition industry.

Pressing tools

KV-250M4 (250 g TNT)

Vertical detonation chamber KV-2 Control panel of the detonation chambers

HORIZONTAL DETONATION CHAMBERS

• For 8 – 16 kg TNT

• Open and close by a cover moving on rails

• Suitable for elongated charges.

• Best for explosive metalworking operations

Horizontal detonation chamber KV-16

1817

Page 11: 2014 ozm catalog

PER

FOR

MA

NC

E TE

STS

PER

FOR

MA

NC

E TESTS

REMOTE CNC MACHINING FOR EXPLSOIVES AND ROCKET FUELS

XSM-01

APPLICATIONSampling of explosive materials from live ammunition and preparation of compact samples for mechanical, sensitivity or performance tests and sample preparation procedures are however one of the most dangerous operations with inherent risks of accidental explosions. OZM Research develops and supplies remotely operated multi spindle vertical and horizontal CNC machining units for cutting, milling, and drilling of energetic materials such as rocket propellants and high explosives in 4 axes. These techniques are typically used for: • Cutting of large rocket propellant grains to smaller blocks for

artificial ageing or mechanical properties tests.• Machining of the rocket propellant grains to obtain samples for

chemical stability testing (insulation, outer and inner surface and whole diameter – all in adjustable chip size).

• Precise sampling of the rocket propellants by automated drilling from predefined spots for plasticizer migration.

• Precise sampling of high explosives from the warheads and grenades by automated drilling in predefined spots (fine powder).

• Machining of the propellant blocks to “dog-bones” or other specific shapes for mechanical, sensitivity and performance tests (gap tests, spark tests, Stojan vessel tests).

• Machining of ammunition parts as a part of disassembling process.

FEATURES• CNC units XSM-01 are developed with consideration of all risky

situations leading to accidental initiation such as excessive friction on moving parts, electric or mechanical sparks and hot surfaces.

• All the electrical components used are appropriately protected, hard friction areas or moving contacts of sparking metals are minimized, explosive dust is continuously removed, temperature of tools are continuously measured and operation carefully observed by cameras, fire detectors and fire extinguishers.

• System is installed in explosion-proof bunker, with support of technological container and control room. Auxiliary equipment is located in nearby buildings or mobile containers.

DETAILS OF SAMPLING

• CNC machining system XSM-01 was developed as an integral part of research & development, quality control and surveillance programs for new, regularly manufactured or in-service energetic materials and ammunition.

TIME-PRESSURE TEST APPARATUS/TEST FOR OXIDIZING LIQUIDS

TPT SERIES

APPLICATION Time/Pressure Test and Test for Oxidizing Liquids Apparatus serve for evaluation of transfer ignition to deflagration process under confinement or measure the potential for a liquid substance to increase the burning rate or burning intensity is important for hazard assessment of combustible substances.

TPT series apparatus are used to study of burning process and oxidizing properties of flammable substances if the ignition leads to a deflagration. Obtained results (max. pressure, pressure rise time, burning rate. etc) serve for hazard classification of energetic materials, pyrotechnic substances, oxidizing solids and liquids.

Designed to comply with requirements of the following standard of testing:

• UN Recommendation on the Transport of Dangerous Goods, Manual of Tests and Criteria, 2010 - Test 1(c)(i), Test 2(c)(i), Test C.1: Time/pressure test, or Test O.2: Test for oxidizing liquids

• European Commission Directive 2004/73/EC - the classification, packing and labeling of dangerous substances, method A.21: Oxidizing properties (Liquids)

• UN Recommendation on the Transport of Dangerous Goods - HSL Flash Composition Test

• Power source for UN Recommendation on the Transport of Dangerous Goods -Test O.1: Test for oxidizing solids

FEATURES• Universal testing pressure vessel and set of adapters for whole

group of standardized testing procedures.• Corrosion resistant material of pressure vessel parts.• Easier use – right/left hand using stand, connector directly

on transducer, etc.• Precise and robust measurement of pressure/time rise.• One box design – speed data acquisition, transducer conditioner,

ignition current unit, safety switch, USB output.• Simple operation and evaluation of results – SW for control,

measurement, calibration and results evaluation. • Starting kit included – equipment and tools for assembling and

cleaning.

ACCESSORIES

Live ammunition samplingDefined grain size sampling

Ammunition parts clamped for machining

TPT vessel parts

• R&D, quality control or hazard classification of flammable substances, energetic materials or igniters.

2019

Page 12: 2014 ozm catalog

PER

FOR

MA

NC

E TE

STS

PER

FOR

MA

NC

E TESTS

SOFTWARE FOR CALCULATION OF DETONATION PARAMETERS

EXPLO5 CURRENT VERSION: 6.02

EXPLO5 is a thermo-chemical computer code that predicts detonation properties (such as composition of detonation products, detonation velocity, pressure, temperature, heat, etc) of high explosives, and combustion properties of propellants under constant volume or constant pressure conditions (such as composition of combustion products, pressure in closed vessel, heat and temperature of combustion, specific impulse, force, etc). As such, EXPLO5 is important tool in synthesis, formulation, and numerical modelling of energetic materials.

The calculation of detonation parameters in EXPLO5 is based on the chemical equilibrium, steady-state model of detonation. The equilibrium composition of detonation products is calculated applying free energy minimization technique.

The program uses Becker-Kistiakowsky-Wilson (BKW) and Jacobs-Cowperthwaite-Zwisler (JCZ3) equations of state for gaseous detonation products, and Murnaghan equation of state for solids products.

The program is designed so that it enables the calculation of chemical equilibrium composition and thermodynamic parameters of state

along shock adiabate of detonation products, the CJ state and detonation parameters at the CJ state, as well as parameters of state along the expansion isentrope.

It uses non-linear curve fitting subroutine to fit relative volume-pressure data along expansion isentrope according to Jones-Wilkins-Lee (JWL) model, enabling the calculation of detonation energy available for performing mechanical work.

For the calculation of combustion performances under constant pressure or under constant volume conditions, the program uses the ideal gas or the virial equation of state. The virial coefficients of individual gaseous species are calculated from the intermolecular potential equations.

EXPLO5’s database contains 32 chemical elements, about 270 reactants, and more than 300 products being in different phase states.

THE EXPLO5 SOFTWARE IS DEVELOPED BY DR. MUHAMED SUCESKA.

PRODUCT DATA

CURRENT VERSION: 6.02Operation of EXPLO5 is simple and the program run starts with only one edit window. The easy and intuitive program operation can be viewed via the screenshot of the EXPLO5’s edit window below.

Example of summary results of calculationExample of reactant information

Instrumentation for pressure and heat flux measurement inside detonation chamber

Pressure and coaxial thermocouple record from detonation chamber KV-250

Coaxial thermocouple MCT 19 with Voltage Amplifier MVA 10 MHz and 1 MHz filter

APPLICATION The measuring system PREWAQ offers measurement of pressure wave parameters generated by any kind of explosion. This universal tool could be applied not only under open sky but could be also designed for measurement in closed space (e.g. explosion chamber).

The DT modification of the system is used for measurement of extremely fast explosions driven by detonation mechanism and parameters change in order up to tens of nanoseconds for pressure and microseconds in case of temperature.

The DF modification is intended for measurement of explosions driven by deflagration mechanism so the change of parameters happen in order of microseconds.

According to required measurements (type, speed and maximal measured values) the PREWAQ is equipped by the set of sensors together with appropriate cables and perhaps even with stands or holders.

FEATURES• Standard measurement on either 4 or 8 input channels according

to user needs.• Simultaneous measurement of pressure, temperature

(heat radiation), velocity of detonation and/or light.• System is intended for measurement, storage and evaluation

of explosion parameters.• Standard measurement rate is since 3 Ms/s/channel

up to 25 Ms/s/channel.• Graphical output of measured data in formats suitable

for spreadsheet and database editors is a standard.• User-friendly software for apparatus operation, data recording

and evaluation.

ACCESSORIES

• One unique system for measurement of various explosion parameters.

• Portable and simple-to-use design fulfilling specific customer s requirements.

• Measurement of explosion parameters for both detonation and deflagration.

PRESSURE WAVE ANALYZER AND QUANTIFIER

PREWAQ

21 22

Page 13: 2014 ozm catalog

CLOSED VESSELS

RB SERIES

• Measurement of ballistic parameters of gun propellant in closed vessel up to 700 ccm volume.

INTE

RIO

R B

ALL

ISTI

C T

ESTS

INTER

IOR

BA

LLISTIC

TESTS

Pressure - time p(t) plots measuredPressure gradient dp/dt - pressure p plots calculated from experimental data

Vivacity - p/pmax plots calculated from experimental data

Example of customized Electro-explosive Device Analyzer (EDA)

Pressure p - time t dependencies measured using STOJAN VESSEL

Burning rate u [m/s] - pressure p [MPa] dependencies calculated from experimental data measured using STOJAN VESSEL

Comparison of burning rate/pressure curve obtaining by STOJAN VESSEL (line) and by Small Testing Rocket Motor (points)

APPLICATION Determination of burning rate of solid rocket propellants is usually carried out in a Strand Burner or in a sub-scale rocket motor at constant pressures. With Strand Burner, about 10 individual shots are necessary to get the required burning rate plot in the whole pressure range, while using very complicated and expensive instrumentation. The newly developed Stojan Vessel is a much simpler and safer instrument applying advanced mathematical procedure for calculation of pressure dependency of burning rate from experimental data of a single shot only. The mathematical procedure has proved to be in very good correlation with experimental results from multiple-shot measurements in the Strand Burner or in the sub-scale rocket motor.

FEATURES

• Quick assessment of burning rate of new or modified rocket propellant formulations in their research, development and testing.

OZM can supply all equipment and procedure for sample preparation and conditioning for both SV-2 and TRM-35 instruments (hydraulic press, pressing tools, molds for casting, cutting machines, cutting tools, temperature and climatic chambers, etc).

Detail of Stojan Vessel

SV-2 on movable stand

CLOSED VESSELS

NV SERIES

STOJAN VESSEL

SV-2

• The principle of this method is based on the most modern computational and ballistic procedures for determination of burning behavior of double-based solid rocket propellants.

• A single shot is sufficient for plotting burning rates in the whole pressure range. Sample similar as for Subscale Rocket Motor.

• This unique simple-to-use instrument is capable of fully replacing the complicated Strand Burner equipment.

APPLICATION Closed Vessel RB series is used for the measuring of pressure increase curve during burning of the different gun propellant types in constant volume. Behavior of propellant is predicted (e.g. max pressure, vivacity, pressure gradient, covolume, burning rate, etc). Thus, by using the Closed Vessel, the number of shots from a real weapon is minimized. Data obtained from tests in the Closed Vessel are also necessary for the development of new propellants and for

the control of regular produced powder types.

FEATURES• High-pressure vessel up to 5000 bars, standard volumes

40, 80, 200, 400 and 700 ccm.• Two outlet valves, cooling jacket, temperature conditioning unit,

temperature sensor, positioning stand.• Electrical or mechanical ignition.• Precise and high-speed measurement of pressure/time rise.• Simple operation and evaluation of results.

Designed to comply with the requirements of the following standards of testing:

• MIL-STD-286 • STANAG 4115

PRODUCT DATA

APPLICATION Closed Vessels NV series are used for measuring of pressure increase during burning of sample (powder, compact materials, and igniters) in constant volume. Obtained results (max. pressure, burning time, ignition delay time, pressure gradient, pressure rise time, burning rate etc) serve for quality control, safety testing, research and development of energetic materials including primary explosives, propellants and pyrotechnic substances.

Complex solution usually involves customized ignition and measurement control unit named EDA (Electro-explosive Device Analyzer). EDA usually contains adjustable pulse constant current source (for ignition or safety testing), safety switch, ignition current and voltage measurement, pressure rise measurement and PC communication. Typical application is testing (with controlled supply and measurement) of electric initiators like squibs, fuses, etc.

FEATURES• High-pressure vessel up to 5000 bars,

standard volumes 3, 5, 10 and 20 ccm.• Electrical ignition.• EDA – Electro-explosive Device Analyzer – control unit with

adjustable pulse current supply and speed measurement.• Simple operation and evaluation of results – control and

evaluation SW.• Customization is typical.• Simpler and cheaper possibility for determination of ballistic

properties of small-caliber gun powders.

• Determination of ignition and burning parameters of energetic materials in closed vessel up to 20 ccm volume.

2423

Page 14: 2014 ozm catalog

GA

SES

& D

US

TSIN

TERIO

R B

ALLIS

TIC TES

TS

APPLICATION RMM is used for the measuring of pressure inside rocket motor chamber and thrust of rocket motor with time during burning different types of solid propellant rocket motors mounted on stand. RMM can be also used for measurement of different types of closed vessels, pyro-cartridges for aircraft ejection systems, etc.

FEATURES• Robust pressure and thrust measurement with time

– Pressure up to 100 MPa. Thrust up to 1000 kN.• Electrical ignition unit – safety switch, ignition current pulse. • Simple operation and evaluation of results

– measurement and evaluation SW.• Modification upon customer requests

(adapters, evaluation, data sheet, etc)

• Instrument for measurement and evaluation of parameters of solid propellant rocket motor on stand.

Measured pressure and thrust evaluation

Rocket motor on stand

Example of pressure/time curves measured in Small Testing Rocket Motor

Burning rate/pressure dependence evaluated from Small Testing Rocket Motor measurement

SUBSCALE ROCKET MOTOR MEASUREMENTTRM 35

ROCKET MOTOR BALLISTIC MEASUREMENT

RMM

APPLICATION Sub-scale rocket motors are newly introduced procedure in NATO STANAG standards. More individual shots are necessary to get the required parameters (e.g. burning rate, erosion influence, etc) in the whole pressure range. Subscale Rocket Motor is recommended as more universal but more risky supporting method. Measurement and evaluation by RMM is generally included.

FEATURES• Wider assessment of ballistic behavior of new or modified rocket

propellant formulations in their research, development and testing.

• Instrument for measurement of burning parameters of solid rocket propellants in a rocket motor.

• Design and results close to real rocket motor.

• Simple operation and wide range of testing conditions.

GAS & DUST TESTING INSTRUMENTS FOR EXPLOSIBILITY TESTING

OF INDUSTRIAL EXPLOSIVE ATMOSPHERES

2625

Page 15: 2014 ozm catalog

Explosion Chamber 20 L1 m3 Explosion Chamber

GA

SES

, V

AP

OU

RS

& D

US

TS

DU

STS

MEASUREMENT OF MINIMUM IGNITION ENERGY OF DUST DISPERSIONS

MIE-D 1.2

APPLICATIONThe minimum ignition energy of dust dispersions is the key parameter for an assessment of the hazard situation in this plants establishing the extent and, hence, the cost of protective measures. A MIE test determines the amount of energy required for an electric spark to cause a tested dust dispersion sample to initiate. This testing method is essential part of a standard set of tests used by certified bodies, Universities and other research organizations to characterize the dust.

Designed to comply with the requirements of the following standards of testing:

• EN 13821:2002 Potentially explosive atmospheres - Explosion prevention and protection - Determination of minimum ignition energy of dust/air mixtures

FEATURES• Standard measurement on only seven pre-set energy levels up to

1 J, optionally on user specified level in the range of 1 mJ to 3 J.• MIE-D 1.2 could by equipped by the measurement of the real spark

energy.• Two mode of spark triggering: high-voltage switch

or moving electrode.• Pneumatically operated and automatically controlled instrument.• Resistant stainless steel case.

PRODUCT DETAILS

• The minimum ignition energy (MIE) of a combustible substance is the lowest value of the electrical energy stored in a capacitor, which upon discharge, just suffices to ignite the most readily ignitable fuel/air/mixture at atmospheric pressure and room temperature.

APPLICATIONExplosion chambers are used for measurement of basic explosion characteristic of flammable dusts, gases and vapors. These characteristics are maximum explosion pressure, maximum rate of pressure rise, lower and upper explosibility limits and limiting oxygen concentration. Two sizes of explosion chamber are setup by international standards for dust explosion – 1 m3 (our CA 1M3) and 20 l (our CA 20L). The explosion chamber for gas and vapor has to be larger than 5 l so CA 20l is recommended.Testing methods using our CA 1M3 and CA 20L are essential part of standard are essential part of a standard set of tests used by certified bodies, Universities and other research organizations to characterize the dust, gas and vapors. Design of mitigating and protective measures, such as explosion venting device, automatic suppression or partial inerting, without knowledge of these explosion parameters is unimaginable.

FEATURES• Fully automated and remote-controlled machinery.• Robust design with 30 barg of operating and 40 barg of testing

pressures.• Under customer´s requirements could be equipped with heating

for measurements under elevated temperatures up to 200 °C.

Designed to comply with the requirements of the following standards:

• EN 14034 (1-4) sets up 1 m3 explosion chamber (our CA 1M3) as a standard instrument for measurement of maximum pressure, rate of pressure rise, lower explosion limit (LEL) and limiting oxygen concentration (LOC) of dust dispersions. 20 l sphere (our CA 20L) is an alternative of 1 m3 explosion chamber given by EN 14034 (1-4)

• Both CA 1M3 and CA 20L could be delivered with instrumentation for measurement of explosion parameters of gases and vapors according to EN 15967 (maximum pressure and rate of pressure rise), according to EN 14756 (LOC) and EN 1839 (explosion limits)

PRODUCT DETAILS

EXPLOSION CHAMBERS FOR GAS AND DUSTS

CA1M3 software

2827

Page 16: 2014 ozm catalog

DU

STS

VA

PO

UR

S

AUTOIGNITION TEMPERATURE OF LIQUID AND SOLID CHEMICALS

AIT 551

PRODUCT DETAILS

APPLICATIONOutcomes of the testing are used for classification of solid substances or mixtures flammability. This classification is important for transport of these materials according to ARD, RID and, ADN regulations and storage of these materials according to CLP regulations.

FEATURES• Temperature range: up to 140 °C.• Accuracy of temperature: ± 2 °C.• Typical sample volume: 15.63 cm3 and 1000 cm3.• Evaluation of temperature records using the software.• Resistant stainless steel case.

Designed to comply with the requirements of the following standards:

• Regulation (ec) no 1272/2008 of the European Parliament and of the Council on classification, labeling and packaging of substances and mixtures, amending and repealing (CPL)

• UN Recommendation on the Transport of Dangerous Goods, Manual of Tests and Criteria, United Nations, New York, 2010, chapter 32.5.2 Test L.2

• European Agreement Concerning the International Carriage of Dangerous Goods by Road (ADR) (2013)

• Convention concerning International Carriage by Rail (COTIF) Regulations concerning the International Carriage of Dangerous Goods by Rail (RID) (2013)

• European agreement concerning the international carriage of dangerous goods by inland waterways (ADN) (2013)

PRODUCT DETAILS

SELF HEATING SUBSTANCES TESTER

SHT 150

Instrument setup according to ASTM E659 – 78 Instrument setup according to EN 14522 Instrument setup according to UN Recommendation on the transport of dangerous goods

• This temperature is an important parameter for determining the physical and chemical properties according to Globally Harmonized System of Classification and Labeling of Chemicals (GHS) regulation (European CLP Regulation (EC) No 1272/2008).

APPLICATIONAutoignition temperature is the lowest temperature at atmospheric pressure which a substance burst into flame with the absence of an external source of ignition (spark or flame). It is the lowest temperature to which a combustible mixture must be raised, so that the rate of heat evolved by the exothermic oxidation reaction will overbalance the rate at which heat is lost to the surroundings and cause ignition. This property of the substance must be known for especially plants or technologies where there are high temperature of operation. In addition, this property identifies the possible ignition source in technological units under operating conditions.

FEATURES• Possibility of testing auto-ignition temperature of substances into

850 °C (1 562 °F).• Detection of the homogeneity of the temperature on the surface of

the test flasks using three thermocouples and temperature inside the flask.

• Automatic regulation temperature around test flask.• Uniform heating of the flask tested by circulating hot air in the oven.• Accurate batching of the liquid.• Evaluation of temperature records using the software.• Resistant stainless steel case.

Designed to comply with the requirements of the following standards of testing:

• ASTM E659 – 78: Standard Test Method for Autoignition Temperature of Liquid Chemicals

• EN 14522: Determination of the auto ignition temperature of gases and vapours

• NF T 20-036: Chemical products for industrial use. Determination of the relative temperature of the spontaneous flammability of solids

• Self-heating test characterizes ability of substances to self oxidative heating and decomposition. This test is based on the determination of exothermal decomposition of sample directly exposed to hot air at elevated temperatures.

3029

Page 17: 2014 ozm catalog

SUSTAINED COMBUSTIBILITY TESTER

SCT 100

PRODUCT DETAILS

MINIMUM IGNITION TEMPERATURE TESTER

MIT 1000

APPLICATIONThe procedure is applicable to paints (including water-borne paints), varnishes, paint binders, solvents, petroleum or related products and adhesives, which have a flash point. It is not applicable to painted surfaces in respect of assessing their potential fire hazards.

FEATURES• Temperature range: 25 - 75 °C. • Accuracy: ±0.1 °C. • Step for setup of temperature: 0.1 °C. • Typical sample volume: 2.0 ml. • Flame size: 5 mm (diameter).

Designed to comply with the requirements of the following standards:

• ISO 9038:2013 Determination of sustained combustibility of liquids • Regulation (ec) no 1272/2008 of the European Parliament and of

the Council on classification, labelling and packaging of substances and mixtures, amending and repealing (CPL)

• UN Recommendation on the Transport of Dangerous Goods, Manual of Tests and Criteria, United Nations, New York, 2010, chapter 32.5.2 Test L.2

• European Agreement Concerning the International Carriage of Dangerous Goods by Road (ADR) (2013)

• Convention concerning International Carriage by Rail (COTIF) Regulations concerning the International Carriage of Dangerous Goods by Rail (RID) (2013)

• European agreement concerning the international carriage of dangerous goods by inland waterways (ADN) (2013)

• Determination of the minimum temperature of hot surface causing degradation or ignition of dispersed dust.

• Measurement of minimum temperature of hot surface leading to degradation or ignition of dust layers.

• Instrument for determination whether or not a liquid product that would be classified as „flammable“ by virtue of its flash point has the ability to sustain combustion at the temperature or temperatures specified in the appropriate regulations.

APPLICATIONDetermining the minimum temperature of the hot surface has applications in process industry where the presence of combustible dust clouds near the hot surfaces exists. Knowledge of these dust clouds ignition temperature allows assessment whether the hot surfaces in the process are able to ignite dispersion of presented dust or not. Then it is possible to design and apply effective measures to prevent damage to industrial technologies caused by dust cloud explosion.

FEATURES• Minimum temperature of the hot furnace surface

in the range from 20 °C to 1 000 °C.• Accuracy of ± 1% over the whole temperature range. • Identification of the ignition of dispersed dust is realized using

a flexible mirror.• Recording, archiving and measured data analysis on the PC.• This method is suitable as a complementary method to the device

LITTA-400.

Designed to comply with the requirements of the following standards:

• EN 50281-2-1 Methods of determining minimum ignition temperature

APPLICATIONThe minimum temperature of the hot surface igniteing the dust layer provides important information for the prevention of fires in process industry producing dust. It shows thermal resistance of occurring dust to thermal stress. Places in the plant with increased surface temperature are identified during risk analysis continuing with assessing the level of risk generated by ignition of dust. Suggesting preventive measures against the ignition is then much more efficient and easier.

FEATURES• Minimum temperature of the hot surface in the range

from 20 °C to 400 °C. at which changes occurs in the dust layer.

• Changes can be monitoring using either by recording equipment (temperature change) or by optical detection.

• Stable temperature conditions ± 2 °C.• Recording, archiving and measured data analysis on the PC.

Design to comply with the requirements of the following standards:

• EN 50281-2-1 Methods of determining minimum ignition temperature

DU

STS

LIQU

IDS

DUST LAYER IGNITION TEMPERATURE TESTERLIT 400

?

?

SCT 100 tester with remote control

3231

Page 18: 2014 ozm catalog

PRODUCT DETAILS

J-200G

J-120G2

J-025G J-500G

LAB

OR

ATO

RY

STO

RA

GE

OF

EXP

LOS

IVES

INTER

MED

IATE S

TOR

AG

E OF EX

PLO

SIV

ES

Product No. J-025G J-120G2 J-200G J-500GCapacity [g TNT] 20 120 200 500

Weight [kg] 7 25 95 390

Outside dimensions L x W x H [mm]

160 x 160 x 440 330 x 330 x 770 600 x 600 x 1040 1250 x 720 x 830

Internal space L x W x H [mm]

150 x Ø 40 330 x Ø 70 560 x Ø 125 500 x 300 x 300

FEATURES• Safe storage of sensitive or unstable samples.• All explosion effects contained inside, no release of shock wave,

fragments, flame or toxic gases, overpressure safely released through manually opened valves.

• Full protection of life and property in case of accidental explosion of stored explosive samples.

• Zero safety distances: they can be stored directly inside laboratories.

• Portable for transport of the explosive samples outside laboratories.• Interior made of antistatic rubber for eliminating risks of friction

or spark discharge.• Quick opening and closing mechanisms.

SAFE LABORATORY STORAGE OF SMALL EXPLOSIVE SAMPLES

PORTABLE GAS-TIGHT EXPLOSION-RESISTANT CONTAINERS

EXPLOSION-RESISTANT STORAGEFOR SAFE STORAGE OF EXPLOSIVES FROM SMALL

SAMPLES TO LARGER STOCKS

3433

Page 19: 2014 ozm catalog

SAFE STORAGE OF LARGER STOCKS OF EXPLOSIVE SAMPLES

EXPLOSION-RESISTANT STORAGE CONTAINERS (5 – 10 kg TNT eq.)

SAFE STORAGE OF LARGER STOCKS OF EXPLOSIVE SAMPLES

STORAGE MODULES FOR EXPANDING CAPACITY OF STORAGE ROOMS (10 – 1000 kg TNT eq.)

FEATURES• Wider assessment of ballistic behavior of new or modified rocket

propellant formulations in their research, development and testing.• Small magazines for explosive samples attached directly

to laboratory buildings.• Safety distances from 2 meters to buildings and public roads.• All fragments caught, shock wave reduced to safe levels and

overpressure released through ventilating chimneys, without moving the container from its position.

• Tested to full TNT capacity and fragment resistance (122 mm – 152 mm cal. HEF projectiles).

• Safety locks against unauthorized access. • Containers can be transported on trailers or light trucks.

FEATURES• Storage modules protecting against transfer of explosion

(sympathetic detonation). • Safety distances corresponding to the content of one module

only (up to 2.5 kg TNT) despite total stored amount in the storage room (up to several tons).

• Minimization of safety distances / maximization of storage capacity of existing storage rooms.

• Storage of otherwise incompatible classes of explosive materials in one room (e.g. detonators together with high explosives).

• Modules designed for mounting to walls with variable heights and widths.

• Non-sparking and water-tight lids, antistatic rubber seals.

EXP

LOS

IVE

PR

OC

ESS

ING

MET

ALS

INTER

MED

IATE S

TOR

AG

E OF EX

PLO

SIV

ES Product No. J-5KV J-10KVCapacity [g TNT] 5 10

Weight [kg] 1500 2800

Outside dimensions L x W x H [mm]

2100 x 1310 x 1910 2350 x 1670 x 2000

Internal space L x W x H [mm]

700 x 450 x 250 750 x 450 x 250

Product No. ISS

Capacity [g TNT] 2 x 2.5 kg

Weight [kg] 245

Outside dimensions L x W x H [mm]

588 x 400 x 803

Internal dimensions of one tube Ø x L [mm]

324 x 500

EXPLOSIVE PROCESING OF METALS PROCESSING OF METALLIC AND NON-METALLIC

MATERIALS USING EXPLOSIVES

3635

Page 20: 2014 ozm catalog

EXPLOSIVE PROCESSING OF METALS

APPLICATION

One specific field where the energy of explosive is successfully

utilized is explosive processing of metallic and non-metallic

materials. The activities of OZM Research are concentrated

to developing and manufacturing explosion-clad bimetallic

and multilayer metallic materials, explosive hardening and

to a lesser extent OZM Research cooperates in the field of explosive

forming, compaction of powder materials and other application.

Half-finished products, structural elements, and components are

produced in cooperation with the respective customer.

OZM Research offers counselling applicability of explosive

processing of metallic and non-metallic materials.

MAIN FOCUS OF ACTIVITIES:

• Bimetallic or multilayer sheets.

• Semi-products for manufacturing the tube plates for heat exchangers.

• Workpieces to be rolled down.

• Bearing materials and wear resistant materials.

• Structural transition joints.

• Semi-products for glass moulds.

• Lining-up of the socket pipes and sheathing of the rods or the shafts.

• Tube to tube-plate explosive welding and fixing.

• Labyrint coolers.

• Explosive hardening of manganese-steel construction elements.

SELECTED REFERENCES

EXP

LOS

IVE P

RO

CES

SIN

G O

F META

LS

Albania• Ministry of Defence

Algeria• Ministry of Defence

Australia• ORICA

Austria• Austin Powder• Josef Köhler Pyrotechnik

Azerbaijan• Ministry of Defence

Belgium• Royal Military Academy

Brazil• IBQ Industrias Quimicas• Institute of Aeronautics and Space

Bulgaria• Arcus Co.

Canada• Canadian Explosives Research Laboratory• General Dynamics• ORICA• Public Works and Government

Services Canada

China• Beijing Institute of Technology• China Academy of Safety Science

and Technology Beijing• National Registration Center

for Chemicals, SAWS (NRCC)• Shenhua Group Zhungeer Energy Co.• Xi´an Modern Chemistry Research Institute

Croatia• Ministry of Defence• University of Zagreb

Czech Republic• Austin Detonator• Explosia• Indet Safety Systems • Ministry of Defence• Nuclear Research Institute• Zeveta Ammunition

Egypt• Ministry of Defence

Finland• PVTT

France• CEA Le Ripault • CNRS• French-German Research Institute

of Saint-Louis• Herakles - Groupe Safran• INERIS• ONERA – French Aerospace Lab• OUTREAU TECHNOLOGIES

Georgia• Express Diagnostic

Germany• BWB• DIEHL• Fisher-Scientific• Fraunhofer-Institut für Chemische

Technologie ICT• Ludwig-Maximilians University of Munich• Rheinmetall

Greece• National Technical University

of Athens

Hungary• HM Arzenal• TÜV Rheinland

India• HEMRL • TBRL• VSSC

Italy• AVIO Aerospace Propulsion

Jordan• Ministry of Defence

Kazakhstan• Ministry of Defence

Malaysia• STRIDE Weapons Technology Division

NATO• NAMSA

Netherlands• TNO Prins Maurits Laboratory

Peru• EXSA• FAMESA

Poland• Bumar Amunicja • Instytut Przemyslu Organicznego• Military Institute of Armament Technology• Warsaw University of Technology• Zaklady Chemiczne “Nitro-Chem”

Romania• Military Technical Academy

Russia• Altai State Technical University • Central Scientific Research Institute of

Chemistry and Mechanics

Serbia• Evaco International• Ministry of Defence

Singapore• Advanced Material Engineering• Advanced Technology Research Centre• Nanyang Technological University• National University of Singapore

Slovakia• Konštrukta Defence• Ministry of Defence• ZVS Holding

South Africa• African Explosives Limited • Denel Land Systems

South Korea• Agency for Defence Development• Hanwha• Poongsan

Spain• IBATECH Technologia

Sweden• Dyno Nobel Sweden• Fisher Scientific GTF• FOI• Nammo LIAB• Swedish Defence Research Agency

Switzerland• Armasuisse

Taiwan• Precision International Corp.

Turkey• Roketsan Missile Industries• Tubitak Mam• Tubitak Sage

UK• BREXCO• Chemring Energetics UK• Eley Limited• University of Warwick

UN• International Atomic Energy Agency

USA• Air Force Research Laboratory• Alliant Techsystems Inc. • ATK• Fauske & Associates• Los Alamos National Laboratories• McAlester Army Ammunition Plant• University of Southern California• US Army ARDEC Picatinny Arsenal• UTC Aerospace Systems

Vietnam• Military Technical Academy• Ministry of Defence• Institute of Propellant and Explosive• Chemical Manufacture 21 • Industry Explosive Material Centre

37

Page 21: 2014 ozm catalog

CONTACT US OZM Research s.r.o.Bliznovice 32, 538 62 Hrochuv Tynec Czech Republic, European UnionTel.: +420 469 692 341 Mobile: +420 608 742 777 Fax: +420 469 692 882E-mail: [email protected]

www.ozm.czScan QR code

CHINAIdea Science Technology CorporationBeijing, P. R. ChinaTel.: +86 10 84775602, 84775603Fax: +86 10 84786587E-mail: [email protected]

EGYPTNoor Scientific & Trade Cairo, EgyptTel.: +202 432 9148Fax: +202 203 4350E-mail: [email protected]

GERMANY, ÖSTERREICH, SWITZERLANDDr. Müller Instruments Oberursel, GermanyTel.: +49 6172 380 37 27Fax: +49 6172 177 07 74E-mail: [email protected]

INDIAVenture Technologies Bangalore, IndiaTel.: +91 80 65727320, 41715022, 4400 4111Fax: +91 80 4400 4104E-mail: [email protected]

INDONESIAPT. Radin Nusa Digna Surabaya, IndonesiaContact: Widyanto Budihardjo Tel.: +62 31 732 9088Fax: +62 31 732 5588E-mail: [email protected]

MALAYSIASII MalaysiaSubang Jaya, MalaysiaTel.: +60 3 5633 1432Fax: +60 3 5633 0811E-mail: [email protected]

PAKISTANBlue Chip International Rawalpindi, PakistanTel.: +92 21 2538811, 2538833Mobile: +92 300 522 1637, 314 200 2393Fax: +92 21 4841779E-mail: [email protected]

SERBIA, BOSNIA & HERZEGOVINA, MONTENEGROLab Systems SupportBelgrade, SerbiaTel/Fax: +381 11 2893 182Mobile: +381 63 554 742Mobile: +381 64 130 22 34E-mail: [email protected], dragan.jovanovic@labsystemssupport.co.rswww.labsystemssupport.co.rs

SOUTH KOREABaroin co., Ltd.#2-320, 160, Daehwa-ro, Daedeok-gu,Daejeon 306-754 rep. of KoreaTel.: +82 70 4010 7476Fax: +82 42 336 7467Mobile: +82 10 2565 0526

VIETNAM, CAMBODIA, LAOSHienquang Co.Hanoi, VietnamTel.: +84 4 761 77 53Mobile: +84 913 537 940 Fax: +84 4 761 76 91E-mail: [email protected]

INTERNATIONAL SALES REPRESENTATIVES