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XRF Sample Preparation Specialists

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Page 1: Lab Supply Tradeshow Presentation

XRF Sample Preparation Specialists

Page 2: Lab Supply Tradeshow Presentation

www.premierlabsupply.com

Profile & Mission

PREMIER is a Florida based manufacturer and supplier specializing in XRF Sample Preparation

PREMIER is committed to a primary market focus of Applications, Products, Service and Solutions for the XRF Sample Preparation Industry.  

One of the Fastest Growing Manufacturer & Supplier of XRF Sample Preparations Solutions 

Our steady growth & success is directly attributed to ensuring complete customer satisfaction for products & services it provides.

Page 3: Lab Supply Tradeshow Presentation

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Platinum Labware

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Services Our company’s commitment to clients extends beyond the initial

supply of labware as it can offer a complete range of services:

Metal Exchange Program  Repair and Reshaping Service  Cleaning & Polishing   Engraving Service  Refining Services  Technical Support  Custom Items 

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Materials Platinum and its alloys are widely utilized in the analytical

laboratory because of their unique properties. Items offered are as follows: 

Platinum Platinum 5% Gold  Platinum 3% Rhodium  Platinum 10% Rhodium  Platinum Gold Rhodium (87/3/10)

Other Metals 

Gold Silver

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Crucibles Standard Form 

2.5 – 700ml  Larger sizes made to order  Lids   Reinforce rims and/or bases 

Low Form Crucibles 

8 – 125ml  Larger sizes made to order  Lids   Reinforce rims and/or bases

Low Form

Standard Form

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Dishes Reinforced rim and heavy base optional. The additional cost for reinforcement is

far outweighed by longer life and ease of handling.

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Fusion Labware Manufacturers:

Claisse® Herzog Leco ® Perl’X Phoenix Shoeps Universal/Multi Vulcan

Claisse ®

Vulcan

Perl’X

Phoenix

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Specialty Items Premier can supply a wide range of specialty items to supplement

our product range of labware: 

Boats Electrodes  Filter Cones  Foil Sheets  Gauze  Inoculating Loops Tongs  Reshapers Pan Kits  Tweezers   Wire

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AA/ICP Preparation Sample Cups Test Tubes

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Applications for a wide range of industry:

• Cement• Lime• Limestone• Sand• Kiln Feed• Clinker• Mild Meal

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Fusion Applications for a Wide Range of Industry:

Iron Ores & Steel Manufacturers, Bauxite - Alumina & Aluminum industry, Mineral Sands including Rutile - Ilmenite - Zircon Glass & Ceramics Cement industry Industrial minerals - lime, limestone, dolomite, magnesite &

magnesia Geological materials such as aluminosilicates, Base metal (Pb, Zn, Cu, Ni) sulphides, sinters, silicate slags,

mattes, Ferro Alloys.

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Fusion Apparatus Multiple Position Fusion Machines:

Features: Up to 6 Samples simultaneously Auto shutdown in case of loss of pressure Individual burner selection Separate mould timer Variable speed swirling/mixing Adjustable pour delay Auto locking crucible holder Reset at any time Capable of heating heavy duty moulds (up to 150gm)

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Fusion Single Position Fusion Machines

Ideal for: Intro-Fusion Machine R & D Educational Institutions Back up Low Cost

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Fusion Fluxes Fusion Re-agents

Anhydrous, Homogenous, Pre-Fused Fluxes  Easy to Handle & Weigh; Ideal fro Automatic Weighing Systems Defined Geometry & Low Loss of Ignition Non Hydroscopic Dust Free >99.98% Purity ( please ask for analysis) Specials Mixes and Fluxes on Request

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Sample Storage Sample Storage containers choices suitable for

all your reference materials prepared as pellets, glass beads or cups

Ideal for the XRF user Dust Free Dry Storage Easy Labeling for Organization

Page 17: Lab Supply Tradeshow Presentation

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Glassware Charging Columns Cylinders FIA Flasks Glassware repair service MCRT Vials Rams Bottom RTFO Bottles Viscometers

D-86 Flask

Rams Bottom 524

MCRT Vials

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Applications for a wide range of industry:

• Iron Ore Manufacturers• Steel Manufacturers• Slag• Silicate Slag• Magnesites• Base Metals• Sinters

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Press Powder Technique

Samples are prepared as pressed powders to improve producibility.

Tools and Accessories required:  Aluminum Caps  Binding/Grinding Additives  Die Sets  Grinder/Mixer Mill  Filling Tool for Boric Acid  Pellet Film  Press

*Ask about our application note “Press Powder Technique”

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Hydraulic Presses for XRF Ideal for briquetting samples for XRF, XRD and Halide disks for

Infrared analysis.

Product Specifications: Max Pressure 15 / 25 tons, electrical 25 tons Pressure display 0 - 20 t / 0 - 30 t Piston 108 mm Piston Stroke, max 25 mm Bolster Screw diameter 30 mm Bolster Screw Travel, max 90 mm Minimum Distance Between Pressing Faces 35 mm Maximum Distance Between Pressing Faces 125 mm Area size D310 x W290 mm Weight 50.5 kg, electrical 60 kg

Manual

Electric

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Die SetsPremier Stainless Steel Die Sets are complete sets which

include: Detachable main body Integrated valve port A base "O" ring and plunger Two polished Stainless Steel Pellets

Applications at a Glance: Ideal for briquetting samples for XRF and XRD

analysis   Ideal for briquetting Halide disks for infrared analysis  Fits into most commonly used presses.  High Quality Stainless Steel Material allowing Load

Limits of Up to 50 tons.   Pellets offered in Stainless Steel and Tungsten Carbide

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Filling Tool/Backing Method The backing technique is commonly utilized for low quantity

samples

Tool Highlights:  Ensures the sample is “centered” when poured into the die.  A piston presses before filling the cellulose or boric acid on top.  Produces Picture Perfect Pellets  Fast Easy Clean up

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Aluminum Caps Aluminum Caps are utilized to stabilize samples from both sides. Features at a Glance: 

Finest Quality  Thin Wall Material ensures minimal back pressure   Resistance to accidental damage   Easy to handle, label and store

Taper Design

Straight-Wall Design

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Pellet Film XRD and XRF Press Pellet Advantages:

Avoids sample sticking of the die set  Eliminates Chromium contamination from the die  Eliminates sample dusting in Instrument  Clean up is fast & easy

Hot Pressing Advantages: The use of PelletFilm allows pressing polymers using

a standard die set and press. It is not necessary to buy a hot plate  Clean up is fast & easy

Page 25: Lab Supply Tradeshow Presentation

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Grinding & Binding Additives

Typical industries used in:

Cement Industry Sand Limestone Kiln Feed Clinker Milled Meal

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Grinding & Binding Additives

Typical industries used in: Glass & Ceramic Industry Refractories Steel Industry

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Applications for a wide range of industry:• Energy/Power• Environmental• Petrochemical• Plastics • Refineries

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Liquid Preparation XRF Sample Cups: Manufactured In-House Ability to fit many Spectrometers Contaminant - free polyethylene Disposable Standard universal sizes of:

32, 35, 40, & 45mm.

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SOP 3000 Series

1. To prepare your sample cup for analysis, you will require• an Inner Ring

(1)• an Outer Ring

(2)• and a Cap

2. Place Ring (1) with the larger end downward onto the table. Then, place the film on top.

3. Place the Outer Ring (2) on top of the Inner (1) Ring...

...And now use the PREMIER Tool to push the Ring all the way down. The hole in the middle of the Tool allows air to escape, preventing sagging of the film.

4. be certain that there are no folds or creases in the Film. It should look perfect. Now fill your cup with a liquid or solid sample. The Inner Ring contains a "Fill Line" (SC-3345: 5.5ml or 11ml; SC-3340: 9.3ml).

5. Finally, close your sample cup with the snap on cap. There is a "Labeling Area" for you to write your sample description right on the cap.

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