Today’s Outline - February 19, 2015csrri.iit.edu/~segre/phys570/15S/lecture_10.pdfToday’s...

Today’s Outline - February 19, 2015

• Homework #2 solutions

• Refractive optics

• Research papers

Homework Assignment #03:Chapter 3: 1, 3, 4, 6, 8due Thursday, February 26, 2015

C. Segre (IIT) PHYS 570 - Spring 2015 February 19, 2015 1 / 18

• Research papers

Homework 02 - Problem 1

Knowing that the photoelectric absorption of an element scales as theinverse of the energy cubed, calculate

(a) The absorption coefficient at 10keV for copper when the value at5keV is 1698.3 cm−1.

(b) The actual absorption coefficient of copper at 10keV is 1942.1 cm−1,why is this so different than your calculated value?

(a) We are given the energy de-pendence of the absorption co-efficient and its value at 5 keV.

(b) The calculation does nottake into account the Cu K ab-sorption edge at 8.98 keV.

µ10keVµ5kev

=1/103

µ10keV = µ5keV

= 1698.3 cm−1

)= 212 cm−1

µ10keVµ5kev

=1/103

µ10keV = µ5keV

= 1698.3 cm−1

)= 212 cm−1

µ10keVµ5kev

=1/103

µ10keV = µ5keV

= 1698.3 cm−1

)= 212 cm−1

µ10keVµ5kev

=1/103

µ10keV = µ5keV

= 1698.3 cm−1

)= 212 cm−1

µ10keVµ5kev

=1/103

µ10keV = µ5keV

= 1698.3 cm−1

= 212 cm−1

µ10keVµ5kev

=1/103

µ10keV = µ5keV

= 1698.3 cm−1

)= 212 cm−1

µ10keVµ5kev

=1/103

µ10keV = µ5keV

= 1698.3 cm−1

)= 212 cm−1

A 30 cm long, ionization chamber, filled with 80% helium and 20%nitrogen gases at 1 atmosphere, is being used to measure the photon rate(photons/sec) in a synchrotron beamline at 12 keV. If a current ofi =10 nA is measured, what is the photon flux entering the ionizationchamber?

The number of free electrons per second generated in the ion chamber bythe beam is given by

dt= [f (E ) Φ]

]where f (E ) is the fraction of the beam absorbed, Φ is the total flux

incident on the ion chamber, E is the energy of a single photon, and W isthe energy required to produce a free electron in the gas mixture. Thefraction of photons absorbed is given by

f (E ) =I0 − I (L)

I0= 1− e−µL

dt= [f (E ) Φ]

f (E ) =I0 − I (L)

I0= 1− e−µL

dt= [f (E ) Φ]

where f (E ) is the fraction of the beam absorbed, Φ is the total fluxincident on the ion chamber, E is the energy of a single photon, and W isthe energy required to produce a free electron in the gas mixture. Thefraction of photons absorbed is given by

f (E ) =I0 − I (L)

I0= 1− e−µL

dt= [f (E ) Φ]

incident on the ion chamber, E is the energy of a single photon, and W isthe energy required to produce a free electron in the gas mixture.

Thefraction of photons absorbed is given by

f (E ) =I0 − I (L)

I0= 1− e−µL

dt= [f (E ) Φ]

f (E ) =I0 − I (L)

I0= 1− e−µL

dt= [f (E ) Φ]

f (E ) =I0 − I (L)

= 1− e−µL

dt= [f (E ) Φ]

f (E ) =I0 − I (L)

I0= 1− e−µL

Homework 02 - Problem 2 (cont.)

The total absorption coefficient µis a weighted sum of the absorp-tion of the substance in the ionchamber.

Where the quantity µican be computed from the absorp-tion cross section of each compo-nent (σa,i ), its mass density (ρm,i ),molar mass (Mi ), and Avogadro’snumber (NA).

µ =N∑i=1

(ρm,iNA

)σa,i

These values can be computed orlooked up in the orange book or onthe MuCal online calculator for theenergy desired. For E = 12 keV,the photoelectric cross-section is

µHe = 2.0× 10−6 cm−1 µN2 = 2.29× 10−3

µ = 0.8µHe + 0.2µN2 = 0.8 · 2.0× 10−6 + 0.2 · 2.29× 10−3

= 4.60× 10−4 cm−1

The total absorption coefficient µis a weighted sum of the absorp-tion of the substance in the ionchamber.

Where the quantity µican be computed from the absorp-tion cross section of each compo-nent (σa,i ), its mass density (ρm,i ),molar mass (Mi ), and Avogadro’snumber (NA).

µ =N∑i=1

(ρm,iNA

)σa,i

µHe = 2.0× 10−6 cm−1 µN2 = 2.29× 10−3

µ = 0.8µHe + 0.2µN2 = 0.8 · 2.0× 10−6 + 0.2 · 2.29× 10−3

= 4.60× 10−4 cm−1

The total absorption coefficient µis a weighted sum of the absorp-tion of the substance in the ionchamber. Where the quantity µican be computed from the absorp-tion cross section of each compo-nent (σa,i ), its mass density (ρm,i ),molar mass (Mi ), and Avogadro’snumber (NA).

µ =N∑i=1

(ρm,iNA

)σa,i

µHe = 2.0× 10−6 cm−1 µN2 = 2.29× 10−3

µ = 0.8µHe + 0.2µN2 = 0.8 · 2.0× 10−6 + 0.2 · 2.29× 10−3

= 4.60× 10−4 cm−1

µ =N∑i=1

(ρm,iNA

)σa,i

µHe = 2.0× 10−6 cm−1 µN2 = 2.29× 10−3

µ = 0.8µHe + 0.2µN2 = 0.8 · 2.0× 10−6 + 0.2 · 2.29× 10−3

= 4.60× 10−4 cm−1

µ =N∑i=1

(ρm,iNA

)σa,i

µHe = 2.0× 10−6 cm−1 µN2 = 2.29× 10−3

µ = 0.8µHe + 0.2µN2 = 0.8 · 2.0× 10−6 + 0.2 · 2.29× 10−3

= 4.60× 10−4 cm−1

µ =N∑i=1

(ρm,iNA

)σa,i

µHe = 2.0× 10−6 cm−1

µN2 = 2.29× 10−3

µ = 0.8µHe + 0.2µN2 = 0.8 · 2.0× 10−6 + 0.2 · 2.29× 10−3

= 4.60× 10−4 cm−1

µ =N∑i=1

(ρm,iNA

)σa,i

µHe = 2.0× 10−6 cm−1 µN2 = 2.29× 10−3

µ = 0.8µHe + 0.2µN2 = 0.8 · 2.0× 10−6 + 0.2 · 2.29× 10−3

= 4.60× 10−4 cm−1

µ =N∑i=1

(ρm,iNA

)σa,i

µHe = 2.0× 10−6 cm−1 µN2 = 2.29× 10−3

µ = 0.8µHe + 0.2µN2

= 0.8 · 2.0× 10−6 + 0.2 · 2.29× 10−3

= 4.60× 10−4 cm−1

µ =N∑i=1

(ρm,iNA

)σa,i

µHe = 2.0× 10−6 cm−1 µN2 = 2.29× 10−3

µ = 0.8µHe + 0.2µN2 = 0.8 · 2.0× 10−6 + 0.2 · 2.29× 10−3

= 4.60× 10−4 cm−1

µ =N∑i=1

(ρm,iNA

)σa,i

µHe = 2.0× 10−6 cm−1 µN2 = 2.29× 10−3

µ = 0.8µHe + 0.2µN2 = 0.8 · 2.0× 10−6 + 0.2 · 2.29× 10−3

= 4.60× 10−4 cm−1

Now we use this to calculate thefraction of photons absorbed in thechamber

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

Finally, we look up in the orangebook the energy required to make afree electron by inoization for eachgas and take a weighted average

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

The number of electrons per secondcan be computed directly from themeasured current

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Putting it all together

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

(0.0136)(12× 103 eV/photon)= 1.53× 1010 photon/s

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL

= 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

=10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36

= 40 eV

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Φ =dN

f (E )E

=(6.24×10 s−1)(40 eV)

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

(0.0136)(12× 103 eV/photon)

= 1.53× 1010 photon/s

10× 10−9

1.602× 10−19

= 6.24× 1010 s−1

µ = 4.60× 10−4 cm−1

f (E ) = 1− e−µL = 1− e−4.60×−4·30

= 0.0136 = 1.36%

WHe = 41 eV WN2 = 36 eV

W = 0.8 · 41 + 0.2 · 36 = 40 eV

Φ =dN

f (E )E=

(6.24×10 s−1)(40 eV)

A 5 cm deep ionization chamber is used to measure the fluorescence froma sample containing arsenic (As). Using any noble gases or nitrogen,determine a gas fill (at 1 atmosphere) for this chamber which absorbs atleast 60% of the incident photons. How does this change if you aremeasuring the fluorescence from ruthenium (Ru)?

The energy of the arsenic fluores-ence line can be obtained fromMuCal or from Hephaestus and is10.54 keV. We would like to haveat least 60% absorption in the 5 cmchamber. This can give us the de-sired value of µ.

This is the minimum value of theabsorption that we require.

f (E ) = 1− e−µL

e−µL = [1− f (E )]

− µL = ln[1− f (E )]

µ =− ln[1− F (E )]

=− ln[1− 0.6]

5 cm= 0.183 cm−1

f (E ) = 1− e−µL

e−µL = [1− f (E )]

− µL = ln[1− f (E )]

µ =− ln[1− F (E )]

=− ln[1− 0.6]

5 cm= 0.183 cm−1

f (E ) = 1− e−µL

e−µL = [1− f (E )]

− µL = ln[1− f (E )]

µ =− ln[1− F (E )]

=− ln[1− 0.6]

5 cm= 0.183 cm−1

f (E ) = 1− e−µL

e−µL = [1− f (E )]

− µL = ln[1− f (E )]

µ =− ln[1− F (E )]

=− ln[1− 0.6]

5 cm= 0.183 cm−1

f (E ) = 1− e−µL

e−µL = [1− f (E )]

− µL = ln[1− f (E )]

µ =− ln[1− F (E )]

=− ln[1− 0.6]

5 cm= 0.183 cm−1

f (E ) = 1− e−µL

e−µL = [1− f (E )]

− µL = ln[1− f (E )]

µ =− ln[1− F (E )]

=− ln[1− 0.6]

5 cm= 0.183 cm−1

f (E ) = 1− e−µL

e−µL = [1− f (E )]

− µL = ln[1− f (E )]

µ =− ln[1− F (E )]

=− ln[1− 0.6]

= 0.183 cm−1

f (E ) = 1− e−µL

e−µL = [1− f (E )]

− µL = ln[1− f (E )]

µ =− ln[1− F (E )]

=− ln[1− 0.6]

5 cm= 0.183 cm−1

f (E ) = 1− e−µL

e−µL = [1− f (E )]

− µL = ln[1− f (E )]

µ =− ln[1− F (E )]

=− ln[1− 0.6]

5 cm= 0.183 cm−1

Looking at tabulated values of the absorption coefficient for various gasesat this energy (from MuCal, total cross-section):

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

µAr = 0.098 cm−1 µKr = 0.17 cm−1 µXe = 0.89 cm−1 µRn = 1.3 cm−1

Thus for the most likely candidates we have

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

For the Ru K-edge at 19.28 keV, we have

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1

µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1

µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

µAr = 0.098 cm−1

µKr = 0.17 cm−1 µXe = 0.89 cm−1 µRn = 1.3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

µAr = 0.098 cm−1 µKr = 0.17 cm−1

µXe = 0.89 cm−1 µRn = 1.3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

µAr = 0.098 cm−1 µKr = 0.17 cm−1 µXe = 0.89 cm−1

µRn = 1.3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5)

= 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5)

= 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

µAr = 0.017 cm−1

µKr = 0.23 cm−1 µXe = 0.17 cm−1 µRn = 0.99 cm−1

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

µAr = 0.017 cm−1 µKr = 0.23 cm−1

µXe = 0.17 cm−1 µRn = 0.99 cm−1

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

µAr = 0.017 cm−1 µKr = 0.23 cm−1 µXe = 0.17 cm−1

µRn = 0.99 cm−1

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5)

= 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5)

= 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5)

= 1− 0.01 = 99%

µHe = 4.2× 10−5 cm−1 µN2 = 3.9× 10−3 cm−1 µNe = 8.8× 10−3 cm−1

f (E )Kr = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Xe = 1− e−(0.89)(5) = 1− 0.01 = 99%

f (E )Kr = 1− e−(0.23)(5) = 1− 0.32 = 68%

f (E )Xe = 1− e−(0.17)(5) = 1− 0.43 = 57%

f (E )Rn = 1− e−(0.99)(5) = 1− 0.01 = 99%

Calculate the characteristic angle of reflection of 10keV and 30keV x-raysfor:

(a) A slab of glass (SiO2)

(b) A thick chromium mirror;

(c) A thick platinum mirror.

(d) If the incident x-ray beam is 2mm high, what length of mirror isrequired to reflect the entire beam for each material?

Calculate the characteristic angle of reflection of 10keV and 30keV x-raysfor:

(a) A slab of glass (SiO2)

(b) A thick chromium mirror;

(c) A thick platinum mirror.

(d) If the incident x-ray beam is 2mm high, what length of mirror isrequired to reflect the entire beam for each material?

Calculate the fraction of silver (Ag) fluorescence x-rays which are absorbedin a 1 mm thick silicon (Si) detector and the charge pulse expected foreach absorbed photon. Repeat the calculation for a 1 mm thickgermanium (Ge) detector.

How to make a Fresnel lens

The ideal refracting lens has a parabolicshape (actually elliptical) but this is imprac-tical to make.

h(x) = Λ

2λo f

when h(x) = 100Λ ∼ 1000µm

x = 10√

2λo f ∼ 100µm

aspect ratio too large for a stable structureand absorption would be too large!

h(x) = Λ

2λo f

when h(x) = 100Λ ∼ 1000µm

x = 10√

2λo f ∼ 100µm

h(x) = Λ

2λo f

when h(x) = 100Λ ∼ 1000µm

x = 10√

2λo f ∼ 100µm

h(x) = Λ

2λo f

when h(x) = 100Λ ∼ 1000µm

x = 10√

2λo f ∼ 100µm

h(x) = Λ

2λo f

when h(x) = 100Λ ∼ 1000µm

x = 10√

2λo f ∼ 100µm

7ΛMark off the longitudinal zones (of thicknessΛ) where the waves inside and outside thematerial are in phase.

Each block of thickness Λ serves nopurpose for refraction but only attenuatesthe wave.

This material can be removed and theremaining material collapsed to producea Fresnel lens which has the same opticalproperties as the parabolic lens as long asf � NΛ where N is the number of zones.

7 Mark off the longitudinal zones (of thicknessΛ) where the waves inside and outside thematerial are in phase.

Fresnel lens dimensions

The outermost zones become very small andthus limit the overall aperture of the zoneplate. The dimensions of outermost zone, Ncan be calculated by first defining a scaledheight and lateral dimension

ν =h(x)

Λξ =

x√2λo f

Since ν = ξ2, the position of the Nth zoneis ξN =

√N and the scaled width of the Nth

(outermost) zone is

∆ξN = ξN − ξN−1 =√N −

√N − 1

ν =h(x)

ξ =x√

2λo f

(outermost) zone is

∆ξN = ξN − ξN−1 =√N −

√N − 1

ν =h(x)

Λξ =

x√2λo f

(outermost) zone is

∆ξN = ξN − ξN−1 =√N −

√N − 1

ν =h(x)

Λξ =

x√2λo f

(outermost) zone is

∆ξN = ξN − ξN−1 =√N −

√N − 1

ν =h(x)

Λξ =

x√2λo f

(outermost) zone is

∆ξN = ξN − ξN−1 =√N −

√N − 1

∆ξN = ξN − ξN−1 =√N −

√N − 1

√1− 1

≈√N

[1− 1

])∆ξN ≈

The diameter of the entire lens is thus

2ξN = 2√N =

∆ξN

∆ξN = ξN − ξN−1 =√N −

√N − 1

√1− 1

≈√N

[1− 1

])∆ξN ≈

2ξN = 2√N =

∆ξN

∆ξN = ξN − ξN−1 =√N −

√N − 1

√1− 1

≈√N

[1− 1

∆ξN ≈1

2ξN = 2√N =

∆ξN

∆ξN = ξN − ξN−1 =√N −

√N − 1

√1− 1

≈√N

[1− 1

])∆ξN ≈

2ξN = 2√N =

∆ξN

∆ξN = ξN − ξN−1 =√N −

√N − 1

√1− 1

≈√N

[1− 1

])∆ξN ≈

2ξN = 2√N =

∆ξN

Fresnel lens example

In terms of the unscaled variables

∆xN = ∆ξN√

2λo f

√λo f

dN = 2ξN =

√2λo f

∆ξN= 2√N√

2λo f =√

2Nλo f

If we take

λo = 1A = 1× 10−10m

f = 50cm = 0.5m

N = 100

∆xN = 5× 10−7m = 500nm dN = 2× 10−4m = 100µm

∆xN = ∆ξN√

2λo f =

√λo f

dN = 2ξN =

√2λo f

∆ξN= 2√N√

2λo f =√

2Nλo f

If we take

λo = 1A = 1× 10−10m

f = 50cm = 0.5m

N = 100

∆xN = 5× 10−7m = 500nm dN = 2× 10−4m = 100µm

∆xN = ∆ξN√

2λo f =

√λo f

dN = 2ξN

√2λo f

∆ξN= 2√N√

2λo f =√

2Nλo f

If we take

λo = 1A = 1× 10−10m

f = 50cm = 0.5m

N = 100

∆xN = 5× 10−7m = 500nm dN = 2× 10−4m = 100µm

∆xN = ∆ξN√

2λo f =

√λo f

dN = 2ξN =

√2λo f

∆ξN

= 2√N√

2λo f =√

2Nλo f

If we take

λo = 1A = 1× 10−10m

f = 50cm = 0.5m

N = 100

∆xN = 5× 10−7m = 500nm dN = 2× 10−4m = 100µm

∆xN = ∆ξN√

2λo f =

√λo f

dN = 2ξN =

√2λo f

∆ξN= 2√N√

2λo f =√

2Nλo f

If we take

λo = 1A = 1× 10−10m

f = 50cm = 0.5m

N = 100

∆xN = 5× 10−7m = 500nm dN = 2× 10−4m = 100µm

∆xN = ∆ξN√

2λo f =

√λo f

dN = 2ξN =

√2λo f

∆ξN= 2√N√

2λo f =√

2Nλo f

If we take

λo = 1A = 1× 10−10m

f = 50cm = 0.5m

N = 100

∆xN = 5× 10−7m = 500nm dN = 2× 10−4m = 100µm

∆xN = ∆ξN√

2λo f =

√λo f

dN = 2ξN =

√2λo f

∆ξN= 2√N√

2λo f =√

2Nλo f

If we take

λo = 1A = 1× 10−10m

f = 50cm = 0.5m

N = 100

∆xN = 5× 10−7m = 500nm

dN = 2× 10−4m = 100µm

∆xN = ∆ξN√

2λo f =

√λo f

dN = 2ξN =

√2λo f

∆ξN= 2√N√

2λo f =√

2Nλo f

If we take

λo = 1A = 1× 10−10m

f = 50cm = 0.5m

N = 100

∆xN = 5× 10−7m = 500nm dN = 2× 10−4m = 100µm

Making a Fresnel zone plate

The specific shape required for a zone plateis difficult to fabricate, consequently, itis convenient to approximate the nearlytriangular zones with a rectangular profile.

In practice, since the outermost zonesare very small, zone plates are generallyfabricated as alternating zones (rings for2D) of materials with a large Z-contrast,such as Au/Si or W/C.

This kind of zone plate is not as effi-cient as a true Fresnel lens would be in thex-ray regime. Nevertheless, efficiencies upto 35% have been achieved.

Variable focal length CRL

The compound refractive lenses (CRL) are useful for fixed focus but aredifficult to use if a variable focal distance and a long focal length isrequired.

Start with a 2 hole CRL. Rotate byan angle χ about vertical axis giv-ing an effective change in the num-ber of “lenses” by a factor 1/ cosχ.

at E = 5.5keV and χ = 0◦, heightis over 120µm

At χ = 30◦, it is under 50µm

Optimal focus is 20µm at χ = 40◦

B. Adams and C. Rose-Petruck, “Hybrid len/mirror x-ray focusing scheme and beam stabilization”, in prepration (2013).

Start with a 2 hole CRL.

Rotate byan angle χ about vertical axis giv-ing an effective change in the num-ber of “lenses” by a factor 1/ cosχ.

Start with a 2 hole CRL. Rotate byan angle χ about vertical axis

giv-ing an effective change in the num-ber of “lenses” by a factor 1/ cosχ.

Start with a 2 hole CRL. Rotate byan angle χ about vertical axis giv-ing an effective change in the num-ber of “lenses” by a factor 1/ cosχ.

The compound refractive lenses (CRL) are useful for fixed focus but aredifficult to use if a variable focal distance and a long focal length isrequired.Start with a 2 hole CRL. Rotate byan angle χ about vertical axis giv-ing an effective change in the num-ber of “lenses” by a factor 1/ cosχ.

Zone plate fabrication

Making high aspect ratio zone plates is challenging but a new process hasbeen developed to make plates with an aspect ratio as high as 25.

Start with Ultra nano crystallinediamond (UNCD) films on SiN.Coat with hydrogen silsesquioxane(HSQ). Pattern and develop theHSQ layer. Reactive ion etch theUNCD to the substrate. Plate withgold to make final zone plate.

The whole 150nm diameter zoneplate

Detail view of outer zones

M. Wojick et al., “High Aspect Ratio Zone Plate Fabrication Using a Bilayer Mold”, EIBPN 2011.

Start with Ultra nano crystallinediamond (UNCD) films on SiN.

Coat with hydrogen silsesquioxane(HSQ). Pattern and develop theHSQ layer. Reactive ion etch theUNCD to the substrate. Plate withgold to make final zone plate.

Start with Ultra nano crystallinediamond (UNCD) films on SiN.Coat with hydrogen silsesquioxane(HSQ).

Pattern and develop theHSQ layer. Reactive ion etch theUNCD to the substrate. Plate withgold to make final zone plate.

Start with Ultra nano crystallinediamond (UNCD) films on SiN.Coat with hydrogen silsesquioxane(HSQ). Pattern and develop theHSQ layer.

Reactive ion etch theUNCD to the substrate. Plate withgold to make final zone plate.

Start with Ultra nano crystallinediamond (UNCD) films on SiN.Coat with hydrogen silsesquioxane(HSQ). Pattern and develop theHSQ layer. Reactive ion etch theUNCD to the substrate.

Plate withgold to make final zone plate.

Alligator-type lenses

Perhaps one of the most original x-ray lenses has been made by using oldvinyl records in an “alligator” configuration.

Bjorn Cederstrom et al., “Focusing hard X-rays with old LPs”, Nature 404, 951 (2000).

This design has also beenused to make lenses out oflithium metal.

E.M. Dufresne et al., “Lithium metal for x-ray refractive optics”, Appl. Phys. Lett. 79, 4085 (2001).

Alligator-type lenses

Perhaps one of the most original x-ray lenses has been made by using oldvinyl records in an “alligator” configuration.

Bjorn Cederstrom et al., “Focusing hard X-rays with old LPs”, Nature 404, 951 (2000).

This design has also beenused to make lenses out oflithium metal.

E.M. Dufresne et al., “Lithium metal for x-ray refractive optics”, Appl. Phys. Lett. 79, 4085 (2001).

Today’s Outline - February 19, 2015csrri.iit.edu/~segre/phys570/15S/lecture_10.pdfToday’s...

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