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6107-09-0 December Mr. RaymRemediaBureau oState of C79 Elm SHartford, Re: E N H Dear Mr. F This letteevaluates Acceptabito the Con The CTDin closingcriteria foat the TirProtocol acriteria. Iindicated areas of fanalytes/pCriteria foto be usedlead. Thmilligramconcentra TCLP SA TCLP samwith the minitial planlead samCharacterlead data have a relForty-five
0004
r 15, 2009
mond Frigon ation Divisioof Water ProConnecticut
Street , CT 06106-
Evaluation of Non-Public PrHamden, Con
Frigon:
er presents a acceptability
ility Protocolnnecticut Dep
EP Material Ag the Tire Poor acceptance e Pond Landand comparedIn response tothe Departm
fill identifiedparameters pror mass analyd for fill at thhe Material A
ms per kilograation to be con
AMPLING ME
mples were comethodology nning stages,
mple results rization – Statset was then
latively unifore (45) sample
511 Cong
n tection and LDepartment
5127
Fill TCLP Lroperties, New
nnecticut
summary ofy of fill for usl numeric critpartment of E
Acceptabilityond (and Q P
of fill. The dfill” sent to Cd the NPP fillo MACTEC’
ment approvedd in Block F resented in tysis. The onlhe Tire Pond lAcceptability am (mg/kg) tnsidered non-
THODOLOGY
ollected in thdescribed in TCLP samplin ascendin
tistical Analydivided into rm distributio
e locations fro
gress Street, P.O. B207-775-540
Home Pag
Land Reuset of Environm
ead Data whall Street N
f the fill TCLse at the Tireteria (5 mg/L)nvironmental
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Protocol reqotal lead mu-hazardous.
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e spring and the October le locations wng order, aysis of May 2approximatel
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Box 7050, Portland01 ● Fax 207-77ge: www.mactec.c
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were determinas presented 2009 Samplinly equal grours of samplesht properties
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material with ss than 5 mil
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y of soils and) details the
Evaluation of a for the Matface (bgs) agaOlin dated Jun, namely that ill data set, thmeet the Tirptability of eLeaching Pro
concentratioligrams per l
s within the Nrization Workng the existinchnical memated June 29,o obtain a datnge of total leentified for c
PP (Figure 1)ata to the Ma
ubmitting this
d sediments fospecificationFill for Place
terial Acceptaainst these nune 19, 2008 wwhen the iso
he 90% UCLre Pond Chexcavated matcedure (TCLP
ons exceedingliter (mg/L) T
NPP in accork Plan. Durinng database ofmorandum “T, 2009. Thista set which wead concentracollection of T
), and aterial letter
or use ns and ement ability umeric which olated Ls for emical terials P) for g 250 TCLP
dance ng the f total TCLP s total would ations. TCLP
Mr. Raymond Frigon December 15, 2009 Page 2 of 3
lead samples. However, despite attempts by Olin and MACTEC to obtain access to properties for which access had not yet been obtained, five of the thirty-eight properties could not be accessed for proposed sampling, providing a total of 40 samples (plus two duplicates) from thirty-three properties for analysis. Examination of the spring 2009 TCLP lead data showed an anomalous result for sample N101801; the original sample had a TCLP value of 2.8 mg/L while the duplicate had only 0.18 mg/L, much more in line with the TCLP result for other samples with similar total and SPLP results. Since further inquiry with the laboratory could not resolve this apparent anomaly, MACTEC elected to delete this sample from the evaluation, resulting in 39 samples from the spring 2009 sampling event available for evaluation. Given the findings of the “TCLP Characterization – Statistical Analysis of May 2009 Sampling Results” dated June 29, 2009 that concluded use of the existing SPLP data would not be an adequate basis for determining soil would meet the TCLP Acceptability Criteria, an additional 70 fill samples were collected for TCLP lead analyses in the fall of 2009. The locations of these samples were selected randomly by first gridding the entire NPP site into approximately 50-ft by 50-ft cells and numbering the cells containing fill within each block. The information was then entered into a program called Visual Sampling Plan (created by Pacific Northwest Laboratories, Department of Energy), which generated random cell numbers for each Block based on the number of cells containing fill. Some of the randomly generated sampling locations were located within properties where access to conduct sampling was not granted, and these locations were shifted to other accessible properties. Figure 2 presents the locations of the 109 TCLP lead samples used to evaluate the acceptability of fill material for use as closure material at the Tire Pond Landfill. Table 1 presents the sample location information, including block, street, address, sampling date, and sampling depth. The analytical data generated by Accutest Laboratories in Marlborough, Massachusetts were validated in accordance with CTDEP guidelines (i.e., data was reviewed for completeness as well as the quality parameters provided in the RCP deliverables). Data quality review summaries are presented in Attachment 1. The Material Acceptability Protocol requires that the sampling frequency for placement of material at the Tire Pond Landfill must be no less than one sample per 1,000 cubic yards of material. Table 2 presents the estimated fill volume to be excavated from the NPP, which is approximately 107,000 cubic yards. The 109 TCLP lead samples collected is sufficient to meet the criteria of 1 sample per 1,000 cubic yards of material. TCLP DATA EVALUATION Validated TCLP lead results for the 109 samples are presented in Table 2. TCLP lead concentrations range from non-detect (<0.01 mg/L) to 203 mg/L. The locations of the 7 samples with concentrations greater than the 5 mg/L criteria for placement at the Tire Pond Landfill are indicated on Figure 3, and highlighted in Table 3.
CONCLUSIONS AND RECOMMENDATIONS 109 TCLP lead samples were collected from fill within the NPP in the spring and fall of 2009. Seven out of the 109 TCLP lead samples have concentrations exceeding the Tire Pond material acceptability criteria of 5 mg/L. The recommended approach for handling of the seven sampling locations with the TCLP lead concentrations greater than 5 mg/L is to sample the areas in the immediate vicinity of these seven locations for TCLP lead to bracket the concentrations exceeding 5 mg/L. Four samples would be
Mr. Raymond Frigon December 15, 2009 Page 3 of 3
collected (roughly north, south, east, and west) at a distance of approximately 10 feet from each of the existing seven sample location. Provided that all concentrations are less than 5 mg/L, the volume of fill containing concentrations greater than 5 mg/L would be estimated for each location and treated in place or disposed at an appropriate off-site disposal location. If any of the new samples have TCLP lead concentrations exceeding 5 mg/L, then additional sampling would be required. The results of the additional sampling would be provided in a memorandum to CTDEP. In this manner, these seven areas will be handled separately from the remainder of the NPP fill. The rest of the fill material in the NPP outside these seven areas meets the Tire Pond Material Acceptability Protocol for TCLP, and will be sent to the Tire Pond without additional sampling (note that the material with elevated lead concentrations [Block F outlier areas] identified in the February 14, 2008 letter would still require disposal at another location other than the Tire Pond). Please do not hesitate to contact me at (207) 651-0315 should you have any questions regarding this letter. Sincerely, MACTEC Engineering and Consulting, Inc.
MACTEC Electronic Signature MACTEC Electronic Signature
Nelson Walter, P.E. Rod Pendleton, P.G. Project Manager Principal Scientist
Enclosures cc: David Share (Olin)
C. Hunt (Olin) J. Gear (Olin) William Sigmund (CTDEP) Meg Harvey (CTDPH)
Alan Elia (Sevenson) Jill Barrett (Fitzgerald & Halliday, Inc.) Honorable Scott Jackson (Mayor of Hamden) Chris Harriman (Haley & Aldrich, Inc.) David Silverstone (Regional Water Authority) File
FIGURES
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Olin CorporationNewhall Street Neighborhood
Hamden, CT
Site Location Map
Project 6107090004 Figure 1
Connecticut1:24,000 scale digital topographic map obtainedfrom Environmental GIS Data for Connecticut -2003 Edition, State of Connecticut Departmentof EnvironmentalProtection.
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Document: C:\Documents and Settings\drpendleton\My Documents\_Projects\OLIN - Hamden\GIS\Mapdocuments\TCLP Characterization\TCLP_Sampling_Results_03Nov2009.mxd PDF: C:\Documents and Settings\drpendleton\My Documents\_Projects\OLIN - Hamden\TCLP Characterization\TCLP Characterization Memorandum\Draft_Dec2009\Figure 2_TCLP_SamplingLocs.pdf 12/03/2009 3:28 PM DRPendleton
Olin CorporationNewhall Street Neighborhood
Hamden, Connecticut
Checked/Date: MGV 12/03/09Prepared/Date: DRP 12/03/09
¯ 0 300 600 900150Feet
Legend
!A TCLP Sampling Locations
NPP Property BoundaryFill_Area_ExtentFill_Area_>_4_ft
TCLP Sampling Locations
Project 6107-09-0004 Figure 2
G
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Document: C:\Documents and Settings\drpendleton\My Documents\_Projects\OLIN - Hamden\GIS\Mapdocuments\TCLP Characterization\TCLP_Sampling_Results_03Nov2009.mxd PDF: C:\Documents and Settings\drpendleton\My Documents\_Projects\OLIN - Hamden\TCLP Characterization\TCLP Characterization Memorandum\Draft_Dec2009\Figure 3_TCLP_Lead_Concs.pdf 12/03/2009 3:30 PM DRPendleton
Olin CorporationNewhall Street Neighborhood
Hamden, Connecticut
Checked/Date: MGV 12/03/09Prepared/Date: DRP 12/03/09
¯ 0 300 600 900150Feet
Legend
!A TCLP Lead Concentrations > 5 mg/L (concentration in mg/L)
!A TCLP Sampling Locations
NPP Property BoundaryFill_Area_ExtentFill_Area_>_4_ft
TCLP Lead Concentrations > 5 mg/L
Project 6107-09-0004 Figure 3
TABLES
TABLE 1TCLP LEAD SAMPLE INFORMATION
NEWHALL STREET NEIGHBORHOODHAMDEN, CONNECTICUT
Block Street Number Street Name Location ID Field Sample ID Sample Date
Top Depth
(ft,bgs)
Bottom Depth (ft,bgs)
A 279 Morse St. A3004S1 A300401 05-May-09 0 1A 267 Morse St. A3011S1 A3011S101 05-May-09 0 1A 263 Morse St. A9001 A900102 10-Sep-09 0 2A 287 Morse St. A9002 A900224 10-Sep-09 2 4C 125 Bryden Terr. C1003 C100324 04-May-09 2 4C 117 Bryden Terr. C1004 C100424 05-May-09 2 4C 60 Wadsworth St. C1006 C100624 04-May-09 2 4C 60 Wadsworth St. C3001S1 C3001S101 04-May-09 0 1C 125 Bryden Terr. C9001 C900124 09-Sep-09 2 4C 117 Bryden Terr. C9002 C900224 15-Oct-09 2 4C 99 Bryden Terr. C9003 C900324 14-Oct-09 2 4C 99 Bryden Terr. C9004 C900424 14-Oct-09 2 4C 99 Bryden Terr. C9005 C900502 14-Oct-09 0 2C 1061 Winchester Ave. WIN-1061 WIN-106124 04-May-09 2 4E 513 Newhall St. E9001 E900124 15-Oct-09 2 4E 523 Newhall St. E9002 E900224 10-Sep-09 2 4E 513 Newhall St. E9003 E900324 15-Oct-09 2 4E 177 Morse St. E9004 E900424 15-Oct-09 2 4E 177 Morse St. E9005 E900502 15-Oct-09 0 2F 124 Bryden Terr. 124BT-HA1 124BT-HA112 04-May-09 1 2F 124 Bryden Terr. 124BT-HA5 124BT-HA512 04-May-09 1 2F 127 Morse St. 127MORSE-HA1 127MORSE-HA112 04-May-09 1 2F 127 Morse St. 127MORSE-HA2 127MORSE-HA212 04-May-09 1 2F 127 Morse St. 127MORSE-HA3 127MORSE-HA412 04-May-09 1 2F 127 Morse St. 127MORSE-HA4 267MORSE-HA512 05-May-09 1 2F 95 Morse St. 95-MS 95-MS01 04-May-09 0 1F 135 Morse St. F3002S1 F3002S101 04-May-09 0 1F 109 Morse St. F3003S1 F3003S101 04-May-09 0 1F 136 Bryden Terr. F3006S2 F3006S201 04-May-09 0 1F 1027 Winchester Ave. F9001 F900102 15-Oct-09 0 2F 127 Morse St. F9002 F900224 15-Oct-09 2 4F 84 Bryden Terr. F9003 F900324 15-Oct-09 2 4F 103 Morse St. F9004 F900402 09-Sep-09 0 2F 127 Morse St. F9005 F900524 15-Oct-09 2 4F 106 Bryden Terr. F9006 F900602 14-Oct-09 0 2F 1027 Winchester Ave. F9007 F900724 15-Oct-09 2 4F 84 Bryden Terr. F9008 F900824 15-Oct-09 2 4F 136 Bryden Terr. F9009 F900924 09-Sep-09 2 4F 84 Bryden Terr. F9010 F901002 15-Oct-09 0 2F 103 Morse St. F9011 F901102 09-Sep-09 0 2F 127 Morse St. F9012 F901224 15-Oct-09 2 4F 103 Morse St. F9013 F901302 09-Sep-09 0 2F 103 Morse St. F9014 F901424 09-Sep-09 2 4F 127 Morse St. F9015 F901524 15-Oct-09 2 4F 1027 Winchester Ave. F9016 F901602 15-Oct-09 0 2H 38 Edwards St. H1006 H100624 05-May-09 2 4H 38 Edwards St. H2002S H2002S23 05-May-09 2 3H 53 St. Mary St. H3001S3 H3001S301 05-May-09 0 1H 32 Edwards St. H3003S1 H3003S101 05-May-09 0 1H 27 St. Mary St. H3009S1 H3009S101 05-May-09 0 1
Page 1 of 3Prepared by: DRPChecked by: NW
TABLE 1TCLP LEAD SAMPLE INFORMATION
NEWHALL STREET NEIGHBORHOODHAMDEN, CONNECTICUT
Block Street Number Street Name Location ID Field Sample ID Sample Date
Top Depth
(ft,bgs)
Bottom Depth (ft,bgs)
H 21 St. Mary St. H9001 H900124 14-Oct-09 2 4H 308 Morse St. H9002 H900224 14-Oct-09 2 4H 330 Morse St. H9003 H900324 09-Sep-09 2 4H 27 St. Mary St. H9004 H900424 14-Oct-09 2 4H 308 Morse St. H9005 H900524 14-Oct-09 2 4H 308 Morse St. H9006 H900602 14-Oct-09 0 2H 308 Morse St. H9007 H900702 14-Oct-09 0 2H 308 Morse St. H9008 H900802 14-Oct-09 0 2H 29 St. Mary St. H9009 H900902 14-Oct-09 0 2H 16 Edwards St. H9010 H901024 14-Oct-09 2 4H 330 Morse St. H9011 H901102 09-Sep-09 0 2J 45 Edwards St. J1006 J100601 05-May-09 0 1J 59 Edwards St. J1010 J101012 05-May-09 1 2J 488 Shelton Ave. J9001 J900102 14-Oct-09 0 2J 476 Shelton Ave. J9002 J900224 14-Oct-09 2 4J 476 Shelton Ave. J9003 J900302 14-Oct-09 0 2J 59 Edwards St. J9004 J900424 14-Oct-09 2 4K 216 Morse St. K1038 K103801 05-May-09 0 1K 266 Morse St. K1117 K111701 05-May-09 0 1K 468 Newhall St. K9001 K900102 15-Oct-09 0 2K 468 Newhall St. K9002 K900202 15-Oct-09 0 2L 238 Butler St. L1002 L100201 05-May-09 0 1L 481 Shelton Ave. L1005 L100524 05-May-09 2 4L 265 Goodrich St. L1008 L100824 05-May-09 2 4L 481 Shelton Ave. L9001 L900102 09-Sep-09 0 2L 481 Shelton Ave. L9002 L900224 09-Sep-09 2 4L 265 Goodrich St. L9003 L900324 14-Oct-09 2 4L 481 Shelton Ave. L9004 L900424 09-Sep-09 2 4L 481 Shelton Ave. L9005 L900524 09-Sep-09 2 4L 461 Shelton Ave. L9006 L900602 10-Sep-09 0 2L 481 Shelton Ave. L9007 L900702 09-Sep-09 0 2M 168 Shepard St. M5030 M503002 05-May-09 0 2N 207-209 Goodrich St. N9001 N900124 14-Oct-09 2 4P 180 Morse St. P1005 P100524 04-May-09 2 4P 164 Morse St. P1039 P103901 04-May-09 0 1P 172 Morse St. P3001S3 P3001S301 04-May-09 0 1P 481 Newhall St. P9001 P900124 15-Oct-09 2 4P 176 Morse St. P9002 P900202 15-Oct-09 0 2P 21 Marlboro St. P9003 P900302 10-Sep-09 0 2P 176 Morse St. P9004 P900402 15-Oct-09 0 2Q 449 Newhall St. Q9001 Q900124 09-Sep-09 2 4Q 449 Newhall St. Q9002 Q900202 09-Sep-09 0 2Q 449 Newhall St. SB-13 SB-1324 04-May-09 2 4Q 449 Newhall St. SB-14 SB-1404 04-May-09 0 4R 979-981 Winchester Ave. R1031 R103102 05-May-09 0 2R 973 Winchester Ave. R9001 R900102 15-Oct-09 0 2S 29 North Sheffield St. S1039 S103924 06-May-09 2 4S 41 North Sheffield St. S1044 S104412 04-May-09 1 2S 98 Morse St. S1056 S105614 04-May-09 1 4S 92 Morse St. S9001 S900124 09-Sep-09 2 4
Page 2 of 3Prepared by: DRPChecked by: NW
TABLE 1TCLP LEAD SAMPLE INFORMATION
NEWHALL STREET NEIGHBORHOODHAMDEN, CONNECTICUT
Block Street Number Street Name Location ID Field Sample ID Sample Date
Top Depth
(ft,bgs)
Bottom Depth (ft,bgs)
S 35 North Sheffield St. S9002 S900224 09-Sep-09 2 4T 678 Newhall St. T9001 T900102 15-Oct-09 0 2T 339 Augur St. T9002 T900202 15-Oct-09 0 2T 672 Newhall St. T9003 T900324 15-Oct-09 2 4T 20 Harris St. T9004 T900424 10-Sep-09 2 4T 22 Remington St. T9005 T900524 15-Oct-09 2 4T 17 Harris St. T9006 T900602 15-Oct-09 0 2T 17 Harris St. T9007 T900702 15-Oct-09 0 2T 20 Harris St. T9008 T900824 10-Sep-09 2 4
Page 3 of 3Prepared by: DRPChecked by: NW
TABLE 2 ESTIMATED FILL EXCAVATION VOLUME BY BLOCK
NEWHALL STREET NEIGHBORHOODHAMDEN, CONNECTICUT
BlockEstimated Fill Excavation
Volumes1 (0‐4 ft bgs) in cu yds
A 2,355 C 16,010 E 7,298 F2 20,508
H 14,839 J 8,665 K 2,956 L 9,164 M 1,143 N 344 P 5,780 Q 7,115 R 446 S 1,834 T 8,975
Total 107,000
Notes: 1) Estimated fill excavation volumes are based on 1:1 slopes adjacent to streets and buildings
2) Excludes Block F Hot-Spots (2,606 cu yds) identified for disposal at a landfill other than the Tire Pond (see "Evaluation of Fill for Placement at the Tire Pond Landfill", February 14, 2008)
Page 1 of 1Prepared by: DRPChecked by: NW
TABLE 3TCLP LEAD ANALYTICAL RESULTS
NEWHALL STREET NEIGHBORHOODHAMDEN, CONNECTICUT
Block Street Number Street Name Location ID Field Sample
ID Sample Date Top Depth (ft,bgs)
Bottom Depth (ft,bgs)
Parameter Result Final Qualifier
Unit of Measure
A 279 Morse St. A3004S1 A300401 05-May-09 0 1 TCLP Lead 0.17 MG/LA 267 Morse St. A3011S1 A3011S101 05-May-09 0 1 TCLP Lead 0.24 MG/LA 263 Morse St. A9001 A900102 10-Sep-09 0 2 TCLP Lead 0.016 MG/LA 287 Morse St. A9002 A900224 10-Sep-09 2 4 TCLP Lead 1.4 J MG/LC 125 Bryden Terr. C1003 C100324 04-May-09 2 4 TCLP Lead 1.1 MG/LC 117 Bryden Terr. C1004 C100424 05-May-09 2 4 TCLP Lead 0.76 MG/LC 60 Wadsworth St. C1006 C100624 04-May-09 2 4 TCLP Lead 1 J MG/LC 60 Wadsworth St. C3001S1 C3001S101 04-May-09 0 1 TCLP Lead 1.3 J MG/LC 125 Bryden Terr. C9001 C900124 09-Sep-09 2 4 TCLP Lead 1.1 MG/LC 117 Bryden Terr. C9002 C900224 15-Oct-09 2 4 TCLP Lead 20.4 J MG/LC 99 Bryden Terr. C9003 C900324 14-Oct-09 2 4 TCLP Lead 0.16 J MG/LC 99 Bryden Terr. C9004 C900424 14-Oct-09 2 4 TCLP Lead 0.81 J MG/LC 99 Bryden Terr. C9005 C900502 14-Oct-09 0 2 TCLP Lead 0.2 J MG/LC 1061 Winchester Ave. WIN-1061 WIN-106124 04-May-09 2 4 TCLP Lead 0.3 MG/LE 513 Newhall St. E9001 E900124 15-Oct-09 2 4 TCLP Lead 2.7 J MG/LE 523 Newhall St. E9002 E900224 10-Sep-09 2 4 TCLP Lead 107 J MG/LE 513 Newhall St. E9003 E900324 15-Oct-09 2 4 TCLP Lead 0.015 J MG/LE 177 Morse St. E9004 E900424 15-Oct-09 2 4 TCLP Lead 0.3 J MG/LE 177 Morse St. E9005 E900502 15-Oct-09 0 2 TCLP Lead 0.027 J MG/LF 124 Bryden Terr. 124BT-HA1 124BT-HA112 04-May-09 1 2 TCLP Lead 0.25 J MG/LF 124 Bryden Terr. 124BT-HA5 124BT-HA512 04-May-09 1 2 TCLP Lead 0.014 J MG/LF 127 Morse St. 127MORSE-HA1 HA112 04-May-09 1 2 TCLP Lead 0.032 J MG/LF 127 Morse St. 127MORSE-HA2 HA212 04-May-09 1 2 TCLP Lead 2.1 J MG/LF 127 Morse St. 127MORSE-HA3 HA412 04-May-09 1 2 TCLP Lead 2.8 J MG/LF 127 Morse St. 127MORSE-HA4 HA512 05-May-09 1 2 TCLP Lead 0.081 MG/LF 95 Morse St. 95-MS 95-MS01 04-May-09 0 1 TCLP Lead 0.057 J MG/LF 135 Morse St. F3002S1 F3002S101 04-May-09 0 1 TCLP Lead 0.27 J MG/LF 109 Morse St. F3003S1 F3003S101 04-May-09 0 1 TCLP Lead 0.65 J MG/LF 136 Bryden Terr. F3006S2 F3006S201 04-May-09 0 1 TCLP Lead 0.23 MG/LF 1027 Winchester Ave. F9001 F900102 15-Oct-09 0 2 TCLP Lead 1 MG/LF 127 Morse St. F9002 F900224 15-Oct-09 2 4 TCLP Lead 0.94 J MG/LF 84 Bryden Terr. F9003 F900324 15-Oct-09 2 4 TCLP Lead 0.058 J MG/LF 103 Morse St. F9004 F900402 09-Sep-09 0 2 TCLP Lead 0.23 MG/LF 127 Morse St. F9005 F900524 15-Oct-09 2 4 TCLP Lead 0.24 J MG/LF 106 Bryden Terr. F9006 F900602 14-Oct-09 0 2 TCLP Lead 0.26 J MG/LF 1027 Winchester Ave. F9007 F900724 15-Oct-09 2 4 TCLP Lead 0.62 J MG/LF 84 Bryden Terr. F9008 F900824 15-Oct-09 2 4 TCLP Lead 0.069 J MG/LF 136 Bryden Terr. F9009 F900924 09-Sep-09 2 4 TCLP Lead 0.17 J MG/L
Page 1 of 3Prepared by: DRPChecked by : NW
TABLE 3TCLP LEAD ANALYTICAL RESULTS
NEWHALL STREET NEIGHBORHOODHAMDEN, CONNECTICUT
Block Street Number Street Name Location ID Field Sample
ID Sample Date Top Depth (ft,bgs)
Bottom Depth (ft,bgs)
Parameter Result Final Qualifier
Unit of Measure
F 84 Bryden Terr. F9010 F901002 15-Oct-09 0 2 TCLP Lead 0.37 J MG/LF 103 Morse St. F9011 F901102 09-Sep-09 0 2 TCLP Lead 1.2 MG/LF 127 Morse St. F9012 F901224 15-Oct-09 2 4 TCLP Lead 0.033 J MG/LF 103 Morse St. F9013 F901302 09-Sep-09 0 2 TCLP Lead 0.7 MG/LF 103 Morse St. F9014 F901424 09-Sep-09 2 4 TCLP Lead 0.36 MG/LF 127 Morse St. F9015 F901524 15-Oct-09 2 4 TCLP Lead 7.4 J MG/LF 1027 Winchester Ave. F9016 F901602 15-Oct-09 0 2 TCLP Lead 0.055 J MG/LH 38 Edwards St. H1006 H100624 05-May-09 2 4 TCLP Lead 147 J MG/LH 38 Edwards St. H2002S H2002S23 05-May-09 2 3 TCLP Lead 54.1 J MG/LH 53 St. Mary St. H3001S3 H3001S301 05-May-09 0 1 TCLP Lead 0.84 J MG/LH 32 Edwards St. H3003S1 H3003S101 05-May-09 0 1 TCLP Lead 0.17 MG/LH 27 St. Mary St. H3009S1 H3009S101 05-May-09 0 1 TCLP Lead 0.18 J MG/LH 21 St. Mary St. H9001 H900124 14-Oct-09 2 4 TCLP Lead 0.088 J MG/LH 308 Morse St. H9002 H900224 14-Oct-09 2 4 TCLP Lead 0.16 J MG/LH 330 Morse St. H9003 H900324 09-Sep-09 2 4 TCLP Lead 0.049 MG/LH 27 St. Mary St. H9004 H900424 14-Oct-09 2 4 TCLP Lead 0.021 J MG/LH 308 Morse St. H9005 H900524 14-Oct-09 2 4 TCLP Lead 0.01 UJ MG/LH 308 Morse St. H9006 H900602 14-Oct-09 0 2 TCLP Lead 0.057 J MG/LH 308 Morse St. H9007 H900702 14-Oct-09 0 2 TCLP Lead 0.068 J MG/LH 308 Morse St. H9008 H900802 14-Oct-09 0 2 TCLP Lead 0.18 J MG/LH 29 St. Mary St. H9009 H900902 14-Oct-09 0 2 TCLP Lead 0.063 J MG/LH 16 Edwards St. H9010 H901024 14-Oct-09 2 4 TCLP Lead 0.01 UJ MG/LH 330 Morse St. H9011 H901102 09-Sep-09 0 2 TCLP Lead 0.13 MG/LJ 45 Edwards St. J1006 J100601 05-May-09 0 1 TCLP Lead 0.11 J MG/LJ 59 Edwards St. J1010 J101012 05-May-09 1 2 TCLP Lead 2 J MG/LJ 488 Shelton Ave. J9001 J900102 14-Oct-09 0 2 TCLP Lead 0.39 J MG/LJ 476 Shelton Ave. J9002 J900224 14-Oct-09 2 4 TCLP Lead 0.12 J MG/LJ 476 Shelton Ave. J9003 J900302 14-Oct-09 0 2 TCLP Lead 0.17 J MG/LJ 59 Edwards St. J9004 J900424 14-Oct-09 2 4 TCLP Lead 0.27 J MG/LK 216 Morse St. K1038 K103801 05-May-09 0 1 TCLP Lead 0.7 MG/LK 266 Morse St. K1117 K111701 05-May-09 0 1 TCLP Lead 0.19 MG/LK 468 Newhall St. K9001 K900102 15-Oct-09 0 2 TCLP Lead 0.1 J MG/LK 468 Newhall St. K9002 K900202 15-Oct-09 0 2 TCLP Lead 0.075 J MG/LL 238 Butler St. L1002 L100201 05-May-09 0 1 TCLP Lead 0.18 MG/LL 481 Shelton Ave. L1005 L100524 05-May-09 2 4 TCLP Lead 2 MG/LL 265 Goodrich St. L1008 L100824 05-May-09 2 4 TCLP Lead 0.12 MG/LL 481 Shelton Ave. L9001 L900102 09-Sep-09 0 2 TCLP Lead 4.3 MG/LL 481 Shelton Ave. L9002 L900224 09-Sep-09 2 4 TCLP Lead 46.5 J MG/L
Page 2 of 3Prepared by: DRPChecked by : NW
TABLE 3TCLP LEAD ANALYTICAL RESULTS
NEWHALL STREET NEIGHBORHOODHAMDEN, CONNECTICUT
Block Street Number Street Name Location ID Field Sample
ID Sample Date Top Depth (ft,bgs)
Bottom Depth (ft,bgs)
Parameter Result Final Qualifier
Unit of Measure
L 265 Goodrich St. L9003 L900324 14-Oct-09 2 4 TCLP Lead 0.036 J MG/LL 481 Shelton Ave. L9004 L900424 09-Sep-09 2 4 TCLP Lead 0.43 MG/LL 481 Shelton Ave. L9005 L900524 09-Sep-09 2 4 TCLP Lead 0.01 U MG/LL 461 Shelton Ave. L9006 L900602 10-Sep-09 0 2 TCLP Lead 0.1 MG/LL 481 Shelton Ave. L9007 L900702 09-Sep-09 0 2 TCLP Lead 1.9 MG/LM 168 Shepard St. M5030 M503002 05-May-09 0 2 TCLP Lead 0.064 MG/LN 207-209 Goodrich St. N9001 N900124 14-Oct-09 2 4 TCLP Lead 0.061 J MG/LP 180 Morse St. P1005 P100524 04-May-09 2 4 TCLP Lead 0.058 MG/LP 164 Morse St. P1039 P103901 04-May-09 0 1 TCLP Lead 0.3 MG/LP 172 Morse St. P3001S3 P3001S301 04-May-09 0 1 TCLP Lead 0.36 MG/LP 481 Newhall St. P9001 P900124 15-Oct-09 2 4 TCLP Lead 0.82 J MG/LP 176 Morse St. P9002 P900202 15-Oct-09 0 2 TCLP Lead 0.073 J MG/LP 21 Marlboro St. P9003 P900302 10-Sep-09 0 2 TCLP Lead 0.15 J MG/LP 176 Morse St. P9004 P900402 15-Oct-09 0 2 TCLP Lead 0.45 J MG/LQ 449 Newhall St. Q9001 Q900124 09-Sep-09 2 4 TCLP Lead 0.074 MG/LQ 449 Newhall St. Q9002 Q900202 09-Sep-09 0 2 TCLP Lead 0.026 MG/LQ 449 Newhall St. SB-13 SB-1324 04-May-09 2 4 TCLP Lead 0.097 MG/LQ 449 Newhall St. SB-14 SB-1404 04-May-09 0 4 TCLP Lead 203 MG/LR 979-981 Winchester Ave. R1031 R103102 05-May-09 0 2 TCLP Lead 0.099 MG/LR 973 Winchester Ave. R9001 R900102 15-Oct-09 0 2 TCLP Lead 0.065 MG/LS 29 North Sheffield St. S1039 S103924 06-May-09 2 4 TCLP Lead 0.062 MG/LS 41 North Sheffield St. S1044 S104412 04-May-09 1 2 TCLP Lead 0.06 J MG/LS 98 Morse St. S1056 S105614 04-May-09 1 4 TCLP Lead 0.1 J MG/LS 92 Morse St. S9001 S900124 09-Sep-09 2 4 TCLP Lead 0.01 U MG/LS 35 North Sheffield St. S9002 S900224 09-Sep-09 2 4 TCLP Lead 0.4 MG/LT 678 Newhall St. T9001 T900102 15-Oct-09 0 2 TCLP Lead 0.017 MG/LT 339 Augur St. T9002 T900202 15-Oct-09 0 2 TCLP Lead 0.13 MG/LT 672 Newhall St. T9003 T900324 15-Oct-09 2 4 TCLP Lead 0.069 MG/LT 20 Harris St. T9004 T900424 10-Sep-09 2 4 TCLP Lead 0.025 J MG/LT 22 Remington St. T9005 T900524 15-Oct-09 2 4 TCLP Lead 0.01 U MG/LT 17 Harris St. T9006 T900602 15-Oct-09 0 2 TCLP Lead 0.014 MG/LT 17 Harris St. T9007 T900702 15-Oct-09 0 2 TCLP Lead 0.2 MG/LT 20 Harris St. T9008 T900824 10-Sep-09 2 4 TCLP Lead 0.017 J MG/L
Notes:1) Sample Concentration exceeds 5.0 mg/L Tire Pond disposal criteria
Page 3 of 3Prepared by: DRPChecked by : NW
ATTACHMENT 1
DATA QUALITY REVIEWS
05/20/09
Technical Report for
Olin CorporationMactec: Olin-Newhall St.-Hamden, CT
6107090004/01
Accutest Job Number: M82628
Sampling Dates: 05/04/09 - 05/06/09
Report to:
MacTec
drpendleton@mactec.com
ATTN: Rod Pendleton
Total number of pages in report:
Certifications: MA (M-MA136) CT (PH-0109) NH (2502) RI (00071) ME (MA0136) FL (E87579)NY (11791) NJ (MA926) PA (68-01121) NC (653) IL (200018) NAVY USACEThis report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.Test results relate only to samples analyzed.
New England • 495 Tech Center West • Building 1 • Marlborough, MA 01752 • tel: 508-481-6200 • fax: 508-481-7753 • http://www.accutest.com
Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Conference and/or state specific certification programs as applicable.
Client Service contact: Kristen Blanchard 508-481-6200
Reza TandLab Director
05/20/09
e-Hardcopy 2.0Automated Report
211
Accutest Laboratories is the sole authority for authorizing edits or modifications to thisdocument. Unauthorized modification of this report is strictly prohibited.
1 of 211
M82628
Table of Contents-1-
Sections:
Section 1: Sample Summary ................................................................................................... 6Section 2: Case Narrative/Conformance Summary .............................................................. 17Section 3: Sample Results ........................................................................................................ 20
3.1: M82628-1: SB-1324 ..................................................................................................... 213.2: M82628-1A: SB-1324 .................................................................................................. 223.3: M82628-1B: SB-1324 .................................................................................................. 233.4: M82628-2: SB-1404 ..................................................................................................... 243.5: M82628-2A: SB-1404 .................................................................................................. 253.6: M82628-2B: SB-1404 .................................................................................................. 263.7: M82628-3: P103901 ..................................................................................................... 273.8: M82628-3A: P103901 .................................................................................................. 283.9: M82628-3B: P103901 .................................................................................................. 293.10: M82628-4: P3001S301 ............................................................................................... 303.11: M82628-4A: P3001S301 ............................................................................................ 313.12: M82628-4B: P3001S301 ............................................................................................ 323.13: M82628-5: P100524 ................................................................................................... 333.14: M82628-5A: P100524 ................................................................................................ 343.15: M82628-5B: P100524 ................................................................................................ 353.16: M82628-6: F3006S201 ............................................................................................... 363.17: M82628-6A: F3006S201 ............................................................................................ 373.18: M82628-6B: F3006S201 ............................................................................................ 383.19: M82628-7: WIN-106124 ............................................................................................ 393.20: M82628-7A: WIN-106124 ......................................................................................... 403.21: M82628-7B: WIN-106124 ......................................................................................... 413.22: M82628-8: C100324 ................................................................................................... 423.23: M82628-8A: C100324 ................................................................................................ 433.24: M82628-8B: C100324 ................................................................................................ 443.25: M82628-9: 124BT-HA512 ......................................................................................... 453.26: M82628-9A: 124BT-HA512 ...................................................................................... 463.27: M82628-9B: 124BT-HA512 ...................................................................................... 473.28: M82628-10: 124BT-HA112 ....................................................................................... 483.29: M82628-10A: 124BT-HA112 .................................................................................... 493.30: M82628-10B: 124BT-HA112 .................................................................................... 503.31: M82628-11: 95-MS01 ................................................................................................ 513.32: M82628-11A: 95-MS01 ............................................................................................. 523.33: M82628-11B: 95-MS01 .............................................................................................. 533.34: M82628-12: F3002S101 ............................................................................................. 543.35: M82628-12A: F3002S101 .......................................................................................... 553.36: M82628-12B: F3002S101 .......................................................................................... 563.37: M82628-13: 127MORSE-HA412 .............................................................................. 573.38: M82628-13A: 127MORSE-HA412 ............................................................................ 583.39: M82628-13B: 127MORSE-HA412 ............................................................................ 59
12
34
5
2 of 211
M82628
Table of Contents-2-
Sections:
3.40: M82628-14: 127MORSE-HA112 .............................................................................. 603.41: M82628-14A: 127MORSE-HA112 ............................................................................ 613.42: M82628-14B: 127MORSE-HA112 ............................................................................ 623.43: M82628-15: 127MORSE-HA212 .............................................................................. 633.44: M82628-15A: 127MORSE-HA212 ............................................................................ 643.45: M82628-15B: 127MORSE-HA212 ............................................................................ 653.46: M82628-16: S104412 ................................................................................................. 663.47: M82628-16A: S104412 .............................................................................................. 673.48: M82628-16B: S104412 .............................................................................................. 683.49: M82628-17: S105614 ................................................................................................. 693.50: M82628-17A: S105614 .............................................................................................. 703.51: M82628-17B: S105614 .............................................................................................. 713.52: M82628-18: F3003S101 ............................................................................................. 723.53: M82628-18A: F3003S101 .......................................................................................... 733.54: M82628-18B: F3003S101 .......................................................................................... 743.55: M82628-19: C100624 ................................................................................................. 753.56: M82628-19A: C100624 .............................................................................................. 763.57: M82628-19B: C100624 .............................................................................................. 773.58: M82628-20: C3001S101 ............................................................................................ 783.59: M82628-20A: C3001S101 .......................................................................................... 793.60: M82628-20B: C3001S101 .......................................................................................... 803.61: M82628-21: N101801 ................................................................................................ 813.62: M82628-21A: N101801 .............................................................................................. 823.63: M82628-21B: N101801 .............................................................................................. 833.64: M82628-22: N101801DUP ........................................................................................ 843.65: M82628-22A: N101801DUP ...................................................................................... 853.66: M82628-22B: N101801DUP ...................................................................................... 863.67: M82628-23: H3009S101 ............................................................................................ 873.68: M82628-23A: H3009S101 ......................................................................................... 883.69: M82628-23B: H3009S101 .......................................................................................... 893.70: M82628-24: H3001S301 ............................................................................................ 903.71: M82628-24A: H3001S301 ......................................................................................... 913.72: M82628-24B: H3001S301 .......................................................................................... 923.73: M82628-25: J101012 .................................................................................................. 933.74: M82628-25A: J101012 ............................................................................................... 943.75: M82628-25B: J101012 ............................................................................................... 953.76: M82628-26: J100601 .................................................................................................. 963.77: M82628-26A: J100601 ............................................................................................... 973.78: M82628-26B: J100601 ............................................................................................... 983.79: M82628-27: H100624 ................................................................................................ 993.80: M82628-27A: H100624 .............................................................................................. 1003.81: M82628-27B: H100624 .............................................................................................. 101
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Table of Contents-3-
Sections:
3.82: M82628-28: H2002S23 .............................................................................................. 1023.83: M82628-28A: H2002S23 ........................................................................................... 1033.84: M82628-28B: H2002S23 ............................................................................................ 1043.85: M82628-29: H3003S101 ............................................................................................ 1053.86: M82628-29A: H3003S101 ......................................................................................... 1063.87: M82628-29B: H3003S101 .......................................................................................... 1073.88: M82628-30: A300401 ................................................................................................ 1083.89: M82628-30A: A300401 .............................................................................................. 1093.90: M82628-30B: A300401 .............................................................................................. 1103.91: M82628-31: A3011S101 ............................................................................................ 1113.92: M82628-31A: A3011S101 ......................................................................................... 1123.93: M82628-31B: A3011S101 .......................................................................................... 1133.94: M82628-32: 267MORSE-HA512 .............................................................................. 1143.95: M82628-32A: 267MORSE-HA512 ............................................................................ 1153.96: M82628-32B: 267MORSE-HA512 ............................................................................ 1163.97: M82628-33: K111701 ................................................................................................ 1173.98: M82628-33A: K111701 .............................................................................................. 1183.99: M82628-33B: K111701 .............................................................................................. 1193.100: M82628-34: L100201 ............................................................................................... 1203.101: M82628-34A: L100201 ............................................................................................ 1213.102: M82628-34B: L100201 ............................................................................................ 1223.103: M82628-35: L100524 ............................................................................................... 1233.104: M82628-35A: L100524 ............................................................................................ 1243.105: M82628-35B: L100524 ............................................................................................ 1253.106: M82628-36: L100824 ............................................................................................... 1263.107: M82628-36A: L100824 ............................................................................................ 1273.108: M82628-36B: L100824 ............................................................................................ 1283.109: M82628-37: L100824DUP ....................................................................................... 1293.110: M82628-37A: L100824DUP .................................................................................... 1303.111: M82628-37B: L100824DUP .................................................................................... 1313.112: M82628-38: K103801 .............................................................................................. 1323.113: M82628-38A: K103801 ............................................................................................ 1333.114: M82628-38B: K103801 ............................................................................................ 1343.115: M82628-39: C100424 ............................................................................................... 1353.116: M82628-39A: C100424 ............................................................................................ 1363.117: M82628-39B: C100424 ............................................................................................ 1373.118: M82628-40: R103102 ............................................................................................... 1383.119: M82628-40A: R103102 ............................................................................................ 1393.120: M82628-40B: R103102 ............................................................................................ 1403.121: M82628-41: M503002 .............................................................................................. 1413.122: M82628-41A: M503002 ........................................................................................... 1423.123: M82628-41B: M503002 ........................................................................................... 143
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Table of Contents-4-
Sections:
3.124: M82628-42: S103924 ............................................................................................... 1443.125: M82628-42A: S103924 ............................................................................................ 1453.126: M82628-42B: S103924 ............................................................................................ 146
Section 4: Misc. Forms ............................................................................................................ 1474.1: Chain of Custody ........................................................................................................... 1484.2: RCP Form ...................................................................................................................... 1534.3: Sample Tracking Chronicle ........................................................................................... 154
Section 5: Metals Analysis - QC Data Summaries ................................................................ 1715.1: Prep QC MP13454: Pb .................................................................................................. 1725.2: Prep QC MP13455: Pb .................................................................................................. 1785.3: Prep QC MP13463: Pb .................................................................................................. 1825.4: Prep QC MP13464: Pb .................................................................................................. 1875.5: Prep QC MP13466: Pb .................................................................................................. 1915.6: Prep QC MP13473: Pb .................................................................................................. 1965.7: Prep QC MP13476: Pb .................................................................................................. 2005.8: Prep QC MP13487: Pb .................................................................................................. 2045.9: Prep QC MP13488: Pb .................................................................................................. 208
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Accutest Laboratories
Sample Summary
Olin CorporationJob No:: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matr ix Client
Number Date Time By Received Code Type Sample ID
M82628-1 05/04/09 10:05 MV 05/06/09 SO Soil SB-1324
M82628-1A 05/04/09 10:05 MV 05/06/09 SO Soil SB-1324
M82628-1B 05/04/09 10:05 MV 05/06/09 SO Soil SB-1324
M82628-2 05/04/09 10:10 MV 05/06/09 SO Soil SB-1404
M82628-2A 05/04/09 10:10 MV 05/06/09 SO Soil SB-1404
M82628-2B 05/04/09 10:10 MV 05/06/09 SO Soil SB-1404
M82628-3 05/04/09 11:00 MV 05/06/09 SO Soil P103901
M82628-3A 05/04/09 11:00 MV 05/06/09 SO Soil P103901
M82628-3B 05/04/09 11:00 MV 05/06/09 SO Soil P103901
M82628-4 05/04/09 11:12 MV 05/06/09 SO Soil P3001S301
M82628-4A 05/04/09 11:12 MV 05/06/09 SO Soil P3001S301
M82628-4B 05/04/09 11:12 MV 05/06/09 SO Soil P3001S301
M82628-5 05/04/09 11:25 MV 05/06/09 SO Soil P100524
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Accutest Laboratories
Sample Summary(continued)
Olin CorporationJob No:: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matr ix Client
Number Date Time By Received Code Type Sample ID
M82628-5A 05/04/09 11:25 MV 05/06/09 SO Soil P100524
M82628-5B 05/04/09 11:25 MV 05/06/09 SO Soil P100524
M82628-6 05/04/09 11:55 MV 05/06/09 SO Soil F3006S201
M82628-6A 05/04/09 11:55 MV 05/06/09 SO Soil F3006S201
M82628-6B 05/04/09 11:55 MV 05/06/09 SO Soil F3006S201
M82628-7 05/04/09 12:10 MV 05/06/09 SO Soil WIN-106124
M82628-7A 05/04/09 12:10 MV 05/06/09 SO Soil WIN-106124
M82628-7B 05/04/09 12:10 MV 05/06/09 SO Soil WIN-106124
M82628-8 05/04/09 12:20 MV 05/06/09 SO Soil C100324
M82628-8A 05/04/09 12:20 MV 05/06/09 SO Soil C100324
M82628-8B 05/04/09 12:20 MV 05/06/09 SO Soil C100324
M82628-9 05/04/09 12:35 MV 05/06/09 SO Soil 124BT-HA512
M82628-9A 05/04/09 12:35 MV 05/06/09 SO Soil 124BT-HA512
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Accutest Laboratories
Sample Summary(continued)
Olin CorporationJob No:: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matr ix Client
Number Date Time By Received Code Type Sample ID
M82628-9B 05/04/09 12:35 MV 05/06/09 SO Soil 124BT-HA512
M82628-10 05/04/09 12:45 MV 05/06/09 SO Soil 124BT-HA112
M82628-10A 05/04/09 12:45 MV 05/06/09 SO Soil 124BT-HA112
M82628-10B 05/04/09 12:45 MV 05/06/09 SO Soil 124BT-HA112
M82628-11 05/04/09 12:58 MV 05/06/09 SO Soil 95-MS01
M82628-11A 05/04/09 12:58 MV 05/06/09 SO Soil 95-MS01
M82628-11B 05/04/09 12:58 MV 05/06/09 SO Soil 95-MS01
M82628-12 05/04/09 14:40 MV 05/06/09 SO Soil F3002S101
M82628-12A 05/04/09 14:40 MV 05/06/09 SO Soil F3002S101
M82628-12B 05/04/09 14:40 MV 05/06/09 SO Soil F3002S101
M82628-13 05/04/09 15:00 MV 05/06/09 SO Soil 127MORSE-HA412
M82628-13A 05/04/09 15:00 MV 05/06/09 SO Soil 127MORSE-HA412
M82628-13B 05/04/09 15:00 MV 05/06/09 SO Soil 127MORSE-HA412
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Accutest Laboratories
Sample Summary(continued)
Olin CorporationJob No:: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matr ix Client
Number Date Time By Received Code Type Sample ID
M82628-14 05/04/09 15:10 MV 05/06/09 SO Soil 127MORSE-HA112
M82628-14A 05/04/09 15:10 MV 05/06/09 SO Soil 127MORSE-HA112
M82628-14B 05/04/09 15:10 MV 05/06/09 SO Soil 127MORSE-HA112
M82628-15 05/04/09 15:13 MV 05/06/09 SO Soil 127MORSE-HA212
M82628-15A 05/04/09 15:13 MV 05/06/09 SO Soil 127MORSE-HA212
M82628-15B 05/04/09 15:13 MV 05/06/09 SO Soil 127MORSE-HA212
M82628-16 05/04/09 15:30 MV 05/06/09 SO Soil S104412
M82628-16A 05/04/09 15:30 MV 05/06/09 SO Soil S104412
M82628-16B 05/04/09 15:30 MV 05/06/09 SO Soil S104412
M82628-17 05/04/09 16:10 MV 05/06/09 SO Soil S105614
M82628-17A 05/04/09 16:10 MV 05/06/09 SO Soil S105614
M82628-17B 05/04/09 16:10 MV 05/06/09 SO Soil S105614
M82628-18 05/04/09 16:25 MV 05/06/09 SO Soil F3003S101
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Accutest Laboratories
Sample Summary(continued)
Olin CorporationJob No:: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matr ix Client
Number Date Time By Received Code Type Sample ID
M82628-18A 05/04/09 16:25 MV 05/06/09 SO Soil F3003S101
M82628-18B 05/04/09 16:25 MV 05/06/09 SO Soil F3003S101
M82628-19 05/04/09 16:45 MV 05/06/09 SO Soil C100624
M82628-19A 05/04/09 16:45 MV 05/06/09 SO Soil C100624
M82628-19B 05/04/09 16:45 MV 05/06/09 SO Soil C100624
M82628-20 05/04/09 17:00 MV 05/06/09 SO Soil C3001S101
M82628-20A 05/04/09 17:00 MV 05/06/09 SO Soil C3001S101
M82628-20B 05/04/09 17:00 MV 05/06/09 SO Soil C3001S101
M82628-21 05/04/09 17:40 MV 05/06/09 SO Soil N101801
M82628-21A 05/04/09 17:40 MV 05/06/09 SO Soil N101801
M82628-21AD05/04/09 17:40 MV 05/06/09 SO Soil Dup/MSD N101801
M82628-21AS05/04/09 17:40 MV 05/06/09 SO Soil Matrix Spike N101801
M82628-21B 05/04/09 17:40 MV 05/06/09 SO Soil N101801
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Accutest Laboratories
Sample Summary(continued)
Olin CorporationJob No:: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matr ix Client
Number Date Time By Received Code Type Sample ID
M82628-21BD05/04/09 17:40 MV 05/06/09 SO Soil Dup/MSD N101801
M82628-21BS 05/04/09 17:40 MV 05/06/09 SO Soil Matrix Spike N101801
M82628-21D 05/04/09 17:40 MV 05/06/09 SO Soil Dup/MSD N101801
M82628-21S 05/04/09 17:40 MV 05/06/09 SO Soil Matrix Spike N101801
M82628-22 05/04/09 17:40 MV 05/06/09 SO Soil N101801DUP
M82628-22A 05/04/09 17:40 MV 05/06/09 SO Soil N101801DUP
M82628-22B 05/04/09 17:40 MV 05/06/09 SO Soil N101801DUP
M82628-23 05/05/09 09:40 MV 05/06/09 SO Soil H3009S101
M82628-23A 05/05/09 09:40 MV 05/06/09 SO Soil H3009S101
M82628-23B 05/05/09 09:40 MV 05/06/09 SO Soil H3009S101
M82628-24 05/05/09 09:50 MV 05/06/09 SO Soil H3001S301
M82628-24A 05/05/09 09:50 MV 05/06/09 SO Soil H3001S301
M82628-24B 05/05/09 09:50 MV 05/06/09 SO Soil H3001S301
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Accutest Laboratories
Sample Summary(continued)
Olin CorporationJob No:: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matr ix Client
Number Date Time By Received Code Type Sample ID
M82628-25 05/05/09 10:02 MV 05/06/09 SO Soil J101012
M82628-25A 05/05/09 10:02 MV 05/06/09 SO Soil J101012
M82628-25B 05/05/09 10:02 MV 05/06/09 SO Soil J101012
M82628-26 05/05/09 10:13 MV 05/06/09 SO Soil J100601
M82628-26A 05/05/09 10:13 MV 05/06/09 SO Soil J100601
M82628-26B 05/05/09 10:13 MV 05/06/09 SO Soil J100601
M82628-27 05/05/09 10:25 MV 05/06/09 SO Soil H100624
M82628-27A 05/05/09 10:25 MV 05/06/09 SO Soil H100624
M82628-27B 05/05/09 10:25 MV 05/06/09 SO Soil H100624
M82628-28 05/05/09 10:32 MV 05/06/09 SO Soil H2002S23
M82628-28A 05/05/09 10:32 MV 05/06/09 SO Soil H2002S23
M82628-28B 05/05/09 10:32 MV 05/06/09 SO Soil H2002S23
M82628-29 05/05/09 11:00 MV 05/06/09 SO Soil H3003S101
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Accutest Laboratories
Sample Summary(continued)
Olin CorporationJob No:: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matr ix Client
Number Date Time By Received Code Type Sample ID
M82628-29A 05/05/09 11:00 MV 05/06/09 SO Soil H3003S101
M82628-29B 05/05/09 11:00 MV 05/06/09 SO Soil H3003S101
M82628-30 05/05/09 11:25 MV 05/06/09 SO Soil A300401
M82628-30A 05/05/09 11:25 MV 05/06/09 SO Soil A300401
M82628-30B 05/05/09 11:25 MV 05/06/09 SO Soil A300401
M82628-31 05/05/09 11:35 MV 05/06/09 SO Soil A3011S101
M82628-31A 05/05/09 11:35 MV 05/06/09 SO Soil A3011S101
M82628-31B 05/05/09 11:35 MV 05/06/09 SO Soil A3011S101
M82628-32 05/05/09 11:40 MV 05/06/09 SO Soil 267MORSE-HA512
M82628-32A 05/05/09 11:40 MV 05/06/09 SO Soil 267MORSE-HA512
M82628-32B 05/05/09 11:40 MV 05/06/09 SO Soil 267MORSE-HA512
M82628-33 05/05/09 11:55 MV 05/06/09 SO Soil K111701
M82628-33A 05/05/09 11:55 MV 05/06/09 SO Soil K111701
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Accutest Laboratories
Sample Summary(continued)
Olin CorporationJob No:: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matr ix Client
Number Date Time By Received Code Type Sample ID
M82628-33B 05/05/09 11:55 MV 05/06/09 SO Soil K111701
M82628-34 05/05/09 12:15 MV 05/06/09 SO Soil L100201
M82628-34A 05/05/09 12:15 MV 05/06/09 SO Soil L100201
M82628-34B 05/05/09 12:15 MV 05/06/09 SO Soil L100201
M82628-35 05/05/09 12:25 MV 05/06/09 SO Soil L100524
M82628-35A 05/05/09 12:25 MV 05/06/09 SO Soil L100524
M82628-35B 05/05/09 12:25 MV 05/06/09 SO Soil L100524
M82628-36 05/05/09 13:00 MV 05/06/09 SO Soil L100824
M82628-36A 05/05/09 13:00 MV 05/06/09 SO Soil L100824
M82628-36AD05/05/09 13:00 MV 05/06/09 SO Soil Dup/MSD L100824
M82628-36AS05/05/09 13:00 MV 05/06/09 SO Soil Matrix Spike L100824
M82628-36B 05/05/09 13:00 MV 05/06/09 SO Soil L100824
M82628-36BD05/05/09 13:00 MV 05/06/09 SO Soil Dup/MSD L100824
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Accutest Laboratories
Sample Summary(continued)
Olin CorporationJob No:: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matr ix Client
Number Date Time By Received Code Type Sample ID
M82628-36BS 05/05/09 13:00 MV 05/06/09 SO Soil Matrix Spike L100824
M82628-36D 05/05/09 13:00 MV 05/06/09 SO Soil Dup/MSD L100824
M82628-36S 05/05/09 13:00 MV 05/06/09 SO Soil Matrix Spike L100824
M82628-37 05/05/09 13:00 MV 05/06/09 SO Soil L100824DUP
M82628-37A 05/05/09 13:00 MV 05/06/09 SO Soil L100824DUP
M82628-37B 05/05/09 13:00 MV 05/06/09 SO Soil L100824DUP
M82628-38 05/05/09 14:20 MV 05/06/09 SO Soil K103801
M82628-38A 05/05/09 14:20 MV 05/06/09 SO Soil K103801
M82628-38B 05/05/09 14:20 MV 05/06/09 SO Soil K103801
M82628-39 05/05/09 14:40 MV 05/06/09 SO Soil C100424
M82628-39A 05/05/09 14:40 MV 05/06/09 SO Soil C100424
M82628-39B 05/05/09 14:40 MV 05/06/09 SO Soil C100424
M82628-40 05/05/09 15:10 MV 05/06/09 SO Soil R103102
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
15 of 211
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Accutest Laboratories
Sample Summary(continued)
Olin CorporationJob No:: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matr ix Client
Number Date Time By Received Code Type Sample ID
M82628-40A 05/05/09 15:10 MV 05/06/09 SO Soil R103102
M82628-40B 05/05/09 15:10 MV 05/06/09 SO Soil R103102
M82628-41 05/05/09 16:45 MV 05/06/09 SO Soil M503002
M82628-41A 05/05/09 16:45 MV 05/06/09 SO Soil M503002
M82628-41B 05/05/09 16:45 MV 05/06/09 SO Soil M503002
M82628-42 05/06/09 11:00 MV 05/06/09 SO Soil S103924
M82628-42A 05/06/09 11:00 MV 05/06/09 SO Soil S103924
M82628-42B 05/06/09 11:00 MV 05/06/09 SO Soil S103924
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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1
42 Sample(s) were collected on 05/04/2009 and were received at Accutest on 05/06/2009 properly preserved, at 2.3 Deg. C and
intact. These Samples received an Accutest job number of M82628. A listing of the Laboratory Sample ID, Client Sample ID and
dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more
information, please refer to QC summary pages.
Client: Olin Corporation
Site: Mactec: Olin-Newhall St.-Hamden, CT
Job No M82628
Repor t Date 5/20/2009 9:47:06 AM
SAMPLE DELIVERY GROUP CASE NARRATIVE
Metals By Method SW846 6010B
Matr ix LEACHATE Batch ID: MP13455
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) M82628-21ADUP, M82628-21AMS, M82628-21ASDL were used as the QC samples for metals.
Only Lead requested.
Matr ix LEACHATE Batch ID: MP13464
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) M82293-9TDUP, M82293-9TMS, M82293-9TSDL were used as the QC samples for metals.
RPD(s) for Serial Dilution for Lead are outside control limits for sample MP13464-SD1. Percent difference acceptable due to
low initial sample concentration (< 50 times IDL).
Only Lead requested.
Matr ix LEACHATE Batch ID: MP13473
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) M82628-21BDUP, M82628-21BSDL, M82628-21BMS were used as the QC samples for metals.
Matrix Spike Recovery(s) for Lead are outside control limits. Spike recovery indicates possible matrix interference.
Only Lead requested.
Matr ix LEACHATE Batch ID: MP13476
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) M82628-36ADUP, M82628-36AMS, M82628-36ASDL were used as the QC samples for metals.
Only Lead requested.
Matr ix LEACHATE Batch ID: MP13487
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
Wednesday, May 20, 2009 P age 1 of 3
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Metals By Method SW846 6010B
Matr ix LEACHATE Batch ID: MP13487
All method blanks for this batch meet method specific criteria.
Sample(s) M82689-1ADUP, M82689-1AMS, M82689-1ASDL were used as the QC samples for metals.
Only Lead requested.
Matr ix LEACHATE Batch ID: MP13488
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) M82628-36BDUP, M82628-36BMS, M82628-36BSDL were used as the QC samples for metals.
Only Lead requested.
Matr ix SO Batch ID: MP13454
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) M82628-21DUP, M82628-21PS, M82628-21SDL, M82628-21MS were used as the QC samples for metals.
Matrix Spike Recovery(s) for Lead are outside control limits. Spike recovery indicates possible matrix interference and/or sample
nonhomogeneity.Post spike within acceptable range.
Only Lead requested.
Matr ix SO Batch ID: MP13463
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) M82628-36DUP, M82628-36MS, M82628-36SDL were used as the QC samples for metals.
Only Lead requested.
Matr ix SO Batch ID: MP13466
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) M82651-1DUP, M82651-1MS, M82651-1SDL were used as the QC samples for metals.
Only Lead requested.
Wednesday, May 20, 2009 P age 2 of 3
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Matr ix SO Batch ID: GN28851
Sample(s) M82628-21DUP were used as the QC samples for Solids, Percent.
Matr ix SO Batch ID: GN28856
Sample(s) M82628-1DUP were used as the QC samples for Solids, Percent.
Matr ix SO Batch ID: GN28875
Sample(s) M82628-36DUP were used as the QC samples for Solids, Percent.
Matr ix SO Batch ID: GN28876
Sample(s) M82651-1DUP were used as the QC samples for Solids, Percent.
No specific RLs requested.
Note: Compounds whose reported QC limits are outside the CT Recommended Reasonable Confidence Protocol QC criteria are
QC criteria but exceed the RCP criteria (compounds exceeding Accutest QC criteria are flagged on the QC summary). Refer to
the QC summary pages.
Unless otherwise noted, sample dilutions are performed in order to report the result within the calibration range.
The Accutest Laboratories of New England certifies that all analysis were performed within method specification. It is further
recommended that this report to be used in its entirety.The Accutest Laboratories of NE, Laboratory Director or assignee as verified
by the signature on the cover page has authorized the release of this report(M82628).
Wednesday, May 20, 2009 P age 3 of 3
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Sample Results
Report of Analysis
Section 3
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: SB-1324
Lab Sample ID: M82628-1 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 91.0
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 40.8 2.1 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
21 of 211
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: SB-1324
Lab Sample ID: M82628-1A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 91.0
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.051 0.010 mg/l 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13455
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
22 of 211
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: SB-1324
Lab Sample ID: M82628-1B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 91.0
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.097 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
23 of 211
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: SB-1404
Lab Sample ID: M82628-2 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 89.7
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 8470 21 mg/kg 10 05/08/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13454
RL = Reporting Limit
24 of 211
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: SB-1404
Lab Sample ID: M82628-2A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 2.8 0.010 mg/l 1 05/08/09 05/12/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13455
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
25 of 211
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33.5
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: SB-1404
Lab Sample ID: M82628-2B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 203 D008 5.0 0.50 mg/l 50 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
26 of 211
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: P103901
Lab Sample ID: M82628-3 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 89.6
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 160 2.0 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
27 of 211
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33.7
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: P103901
Lab Sample ID: M82628-3A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 89.6
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.10 0.010 mg/l 1 05/08/09 05/12/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13455
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
28 of 211
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: P103901
Lab Sample ID: M82628-3B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 89.6
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.30 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
29 of 211
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: P3001S301
Lab Sample ID: M82628-4 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 155 2.1 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
30 of 211
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: P3001S301
Lab Sample ID: M82628-4A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.055 0.010 mg/l 1 05/08/09 05/12/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13455
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
31 of 211
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: P3001S301
Lab Sample ID: M82628-4B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.36 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
32 of 211
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: P100524
Lab Sample ID: M82628-5 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 86.0
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 159 2.1 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
33 of 211
M82628
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: P100524
Lab Sample ID: M82628-5A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 86.0
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.053 0.010 mg/l 1 05/08/09 05/12/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13455
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
34 of 211
M82628
33.14
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: P100524
Lab Sample ID: M82628-5B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 86.0
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.058 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
35 of 211
M82628
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F3006S201
Lab Sample ID: M82628-6 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 90.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 240 2.1 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
36 of 211
M82628
33.16
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F3006S201
Lab Sample ID: M82628-6A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 90.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.084 0.010 mg/l 1 05/08/09 05/12/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13455
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
37 of 211
M82628
33.17
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F3006S201
Lab Sample ID: M82628-6B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 90.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.23 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
38 of 211
M82628
33.18
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: WIN-106124
Lab Sample ID: M82628-7 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 77.9
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 360 2.4 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
39 of 211
M82628
33.19
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: WIN-106124
Lab Sample ID: M82628-7A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 77.9
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.082 0.010 mg/l 1 05/08/09 05/12/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13455
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
40 of 211
M82628
33.20
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: WIN-106124
Lab Sample ID: M82628-7B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 77.9
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.30 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
41 of 211
M82628
33.21
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C100324
Lab Sample ID: M82628-8 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 73.1
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 1140 2.5 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
42 of 211
M82628
33.22
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C100324
Lab Sample ID: M82628-8A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 73.1
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.15 0.010 mg/l 1 05/08/09 05/12/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13455
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
43 of 211
M82628
33.23
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C100324
Lab Sample ID: M82628-8B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 73.1
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 1.1 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
44 of 211
M82628
33.24
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 124BT-HA512
Lab Sample ID: M82628-9 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 93.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 14.1 2.0 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
45 of 211
M82628
33.25
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 124BT-HA512
Lab Sample ID: M82628-9A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 93.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead < 0.010 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
46 of 211
M82628
33.26
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 124BT-HA512
Lab Sample ID: M82628-9B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 93.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.014 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
47 of 211
M82628
33.27
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 124BT-HA112
Lab Sample ID: M82628-10 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 92.5
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 41.2 2.1 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
48 of 211
M82628
33.28
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 124BT-HA112
Lab Sample ID: M82628-10A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 92.5
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.031 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
49 of 211
M82628
33.29
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 124BT-HA112
Lab Sample ID: M82628-10B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 92.5
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.25 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
50 of 211
M82628
33.30
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 95-MS01
Lab Sample ID: M82628-11 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 92.1
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 58.9 2.0 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
51 of 211
M82628
33.31
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 95-MS01
Lab Sample ID: M82628-11A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 92.1
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.015 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
52 of 211
M82628
33.32
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 95-MS01
Lab Sample ID: M82628-11B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 92.1
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.057 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
53 of 211
M82628
33.33
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F3002S101
Lab Sample ID: M82628-12 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 82.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 551 2.3 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
54 of 211
M82628
33.34
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F3002S101
Lab Sample ID: M82628-12A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 82.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.095 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
55 of 211
M82628
33.35
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F3002S101
Lab Sample ID: M82628-12B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 82.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.27 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
56 of 211
M82628
33.36
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 127MORSE-HA412
Lab Sample ID: M82628-13 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 85.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 1470 2.2 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
57 of 211
M82628
33.37
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 127MORSE-HA412
Lab Sample ID: M82628-13A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 85.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.32 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
58 of 211
M82628
33.38
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 127MORSE-HA412
Lab Sample ID: M82628-13B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 85.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 2.8 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
59 of 211
M82628
33.39
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 127MORSE-HA112
Lab Sample ID: M82628-14 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 93.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 5.8 2.0 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
60 of 211
M82628
33.40
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 127MORSE-HA112
Lab Sample ID: M82628-14A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 93.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead < 0.010 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
61 of 211
M82628
33.41
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 127MORSE-HA112
Lab Sample ID: M82628-14B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 93.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.032 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
62 of 211
M82628
33.42
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 127MORSE-HA212
Lab Sample ID: M82628-15 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 77.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 1270 2.3 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
63 of 211
M82628
33.43
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 127MORSE-HA212
Lab Sample ID: M82628-15A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 77.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.21 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
64 of 211
M82628
33.44
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 127MORSE-HA212
Lab Sample ID: M82628-15B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 77.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 2.1 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
65 of 211
M82628
33.45
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: S104412
Lab Sample ID: M82628-16 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.9
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 43.0 2.1 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
66 of 211
M82628
33.46
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: S104412
Lab Sample ID: M82628-16A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.9
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.018 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
67 of 211
M82628
33.47
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: S104412
Lab Sample ID: M82628-16B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.9
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.060 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
68 of 211
M82628
33.48
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: S105614
Lab Sample ID: M82628-17 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 84.7
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 79.5 2.2 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
69 of 211
M82628
33.49
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: S105614
Lab Sample ID: M82628-17A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 84.7
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.025 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
70 of 211
M82628
33.50
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: S105614
Lab Sample ID: M82628-17B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 84.7
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.10 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
71 of 211
M82628
33.51
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F3003S101
Lab Sample ID: M82628-18 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 72.7
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 639 2.5 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
72 of 211
M82628
33.52
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F3003S101
Lab Sample ID: M82628-18A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 72.7
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.14 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
73 of 211
M82628
33.53
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F3003S101
Lab Sample ID: M82628-18B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 72.7
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.65 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
74 of 211
M82628
33.54
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C100624
Lab Sample ID: M82628-19 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 87.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 690 2.1 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
75 of 211
M82628
33.55
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C100624
Lab Sample ID: M82628-19A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 87.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.12 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
76 of 211
M82628
33.56
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C100624
Lab Sample ID: M82628-19B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 87.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 1.0 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
77 of 211
M82628
33.57
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C3001S101
Lab Sample ID: M82628-20 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 82.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 980 2.3 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
78 of 211
M82628
33.58
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C3001S101
Lab Sample ID: M82628-20A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 82.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.11 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
79 of 211
M82628
33.59
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C3001S101
Lab Sample ID: M82628-20B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 82.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 1.3 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
80 of 211
M82628
33.60
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: N101801
Lab Sample ID: M82628-21 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.5
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 359 2.1 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13454
RL = Reporting Limit
81 of 211
M82628
33.61
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: N101801
Lab Sample ID: M82628-21A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.5
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.066 0.010 mg/l 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13455
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
82 of 211
M82628
33.62
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: N101801
Lab Sample ID: M82628-21B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.5
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 2.8 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
83 of 211
M82628
33.63
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: N101801DUP
Lab Sample ID: M82628-22 Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 333 2.1 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
84 of 211
M82628
33.64
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: N101801DUP
Lab Sample ID: M82628-22A Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.068 0.010 mg/l 1 05/08/09 05/12/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10450
(2) Prep QC Batch: MP13455
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
85 of 211
M82628
33.65
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: N101801DUP
Lab Sample ID: M82628-22B Date Sampled: 05/04/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.18 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
86 of 211
M82628
33.66
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H3009S101
Lab Sample ID: M82628-23 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 83.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 335 2.2 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
87 of 211
M82628
33.67
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H3009S101
Lab Sample ID: M82628-23A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 83.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.076 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
88 of 211
M82628
33.68
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H3009S101
Lab Sample ID: M82628-23B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 83.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.18 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
89 of 211
M82628
33.69
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H3001S301
Lab Sample ID: M82628-24 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 85.7
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 547 2.2 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
90 of 211
M82628
33.70
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H3001S301
Lab Sample ID: M82628-24A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 85.7
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.19 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
91 of 211
M82628
33.71
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H3001S301
Lab Sample ID: M82628-24B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 85.7
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.84 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
92 of 211
M82628
33.72
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: J101012
Lab Sample ID: M82628-25 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.4
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 670 2.1 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
93 of 211
M82628
33.73
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: J101012
Lab Sample ID: M82628-25A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.4
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.14 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
94 of 211
M82628
33.74
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: J101012
Lab Sample ID: M82628-25B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.4
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 2.0 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
95 of 211
M82628
33.75
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: J100601
Lab Sample ID: M82628-26 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 84.1
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 316 2.2 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
96 of 211
M82628
33.76
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: J100601
Lab Sample ID: M82628-26A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 84.1
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.064 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
97 of 211
M82628
33.77
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: J100601
Lab Sample ID: M82628-26B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 84.1
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.11 D008 5.0 0.010 mg/l 1 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
98 of 211
M82628
33.78
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H100624
Lab Sample ID: M82628-27 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 74.0
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 28700 100 mg/kg 50 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
99 of 211
M82628
33.79
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H100624
Lab Sample ID: M82628-27A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 74.0
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 2.0 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
100 of 211
M82628
33.80
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H100624
Lab Sample ID: M82628-27B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 74.0
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 147 D008 5.0 0.20 mg/l 20 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
101 of 211
M82628
33.81
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H2002S23
Lab Sample ID: M82628-28 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 80.0
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 5010 12 mg/kg 5 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
102 of 211
M82628
33.82
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H2002S23
Lab Sample ID: M82628-28A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 80.0
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.86 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13464
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
103 of 211
M82628
33.83
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H2002S23
Lab Sample ID: M82628-28B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 80.0
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 54.1 D008 5.0 0.10 mg/l 10 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13473
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
104 of 211
M82628
33.84
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H3003S101
Lab Sample ID: M82628-29 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 87.1
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 376 2.1 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
105 of 211
M82628
33.85
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H3003S101
Lab Sample ID: M82628-29A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 87.1
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.070 0.010 mg/l 1 05/14/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13476
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
106 of 211
M82628
33.86
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H3003S101
Lab Sample ID: M82628-29B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 87.1
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.17 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
107 of 211
M82628
33.87
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: A300401
Lab Sample ID: M82628-30 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 85.5
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 252 2.2 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
108 of 211
M82628
33.88
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: A300401
Lab Sample ID: M82628-30A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 85.5
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.076 0.010 mg/l 1 05/14/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13476
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
109 of 211
M82628
33.89
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: A300401
Lab Sample ID: M82628-30B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 85.5
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.17 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
110 of 211
M82628
33.90
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: A3011S101
Lab Sample ID: M82628-31 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 87.9
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 75.2 2.1 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
111 of 211
M82628
33.91
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: A3011S101
Lab Sample ID: M82628-31A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 87.9
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.034 0.010 mg/l 1 05/14/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13476
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
112 of 211
M82628
33.92
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: A3011S101
Lab Sample ID: M82628-31B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 87.9
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.24 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
113 of 211
M82628
33.93
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 267MORSE-HA512
Lab Sample ID: M82628-32 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 86.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 356 2.2 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
114 of 211
M82628
33.94
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 267MORSE-HA512
Lab Sample ID: M82628-32A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 86.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.12 0.010 mg/l 1 05/14/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13476
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
115 of 211
M82628
33.95
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: 267MORSE-HA512
Lab Sample ID: M82628-32B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 86.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.081 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
116 of 211
M82628
33.96
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: K111701
Lab Sample ID: M82628-33 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 160 2.2 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
117 of 211
M82628
33.97
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: K111701
Lab Sample ID: M82628-33A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.055 0.010 mg/l 1 05/14/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13476
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
118 of 211
M82628
33.98
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: K111701
Lab Sample ID: M82628-33B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.19 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
119 of 211
M82628
33.99
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L100201
Lab Sample ID: M82628-34 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 86.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 303 2.2 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
120 of 211
M82628
33.100
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L100201
Lab Sample ID: M82628-34A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 86.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.15 0.010 mg/l 1 05/14/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13476
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
121 of 211
M82628
33.101
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L100201
Lab Sample ID: M82628-34B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 86.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.18 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
122 of 211
M82628
33.102
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L100524
Lab Sample ID: M82628-35 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 78.7
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 932 2.4 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
123 of 211
M82628
33.103
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L100524
Lab Sample ID: M82628-35A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 78.7
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.10 0.010 mg/l 1 05/14/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13476
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
124 of 211
M82628
33.104
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L100524
Lab Sample ID: M82628-35B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 78.7
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 2.0 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
125 of 211
M82628
33.105
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L100824
Lab Sample ID: M82628-36 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 85.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 429 2.2 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
126 of 211
M82628
33.106
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L100824
Lab Sample ID: M82628-36A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 85.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.099 0.010 mg/l 1 05/14/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10463
(2) Prep QC Batch: MP13476
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
127 of 211
M82628
33.107
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L100824
Lab Sample ID: M82628-36B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 85.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.12 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
128 of 211
M82628
33.108
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L100824DUP
Lab Sample ID: M82628-37 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 84.9
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 431 2.2 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
129 of 211
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33.109
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L100824DUP
Lab Sample ID: M82628-37A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 84.9
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.076 0.010 mg/l 1 05/14/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13476
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
130 of 211
M82628
33.110
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L100824DUP
Lab Sample ID: M82628-37B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 84.9
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.12 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
131 of 211
M82628
33.111
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: K103801
Lab Sample ID: M82628-38 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 87.4
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 500 2.2 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
132 of 211
M82628
33.112
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: K103801
Lab Sample ID: M82628-38A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 87.4
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.047 0.010 mg/l 1 05/14/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13476
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
133 of 211
M82628
33.113
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: K103801
Lab Sample ID: M82628-38B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 87.4
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.70 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
134 of 211
M82628
33.114
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C100424
Lab Sample ID: M82628-39 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 91.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 249 2.0 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
135 of 211
M82628
33.115
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C100424
Lab Sample ID: M82628-39A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 91.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.17 0.010 mg/l 1 05/14/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13476
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
136 of 211
M82628
33.116
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C100424
Lab Sample ID: M82628-39B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 91.8
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.76 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
137 of 211
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33.117
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: R103102
Lab Sample ID: M82628-40 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 92.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 63.5 2.0 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10453
(2) Prep QC Batch: MP13463
RL = Reporting Limit
138 of 211
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33.118
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: R103102
Lab Sample ID: M82628-40A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 92.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.027 0.010 mg/l 1 05/14/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13476
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
139 of 211
M82628
33.119
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: R103102
Lab Sample ID: M82628-40B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 92.2
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.099 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13488
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
140 of 211
M82628
33.120
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: M503002
Lab Sample ID: M82628-41 Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 273 2.1 mg/kg 1 05/12/09 05/13/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10458
(2) Prep QC Batch: MP13466
RL = Reporting Limit
141 of 211
M82628
33.121
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: M503002
Lab Sample ID: M82628-41A Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.050 0.010 mg/l 1 05/14/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13476
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
142 of 211
M82628
33.122
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: M503002
Lab Sample ID: M82628-41B Date Sampled: 05/05/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 88.3
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.064 D008 5.0 0.010 mg/l 1 05/15/09 05/15/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10470
(2) Prep QC Batch: MP13487
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
143 of 211
M82628
33.123
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: S103924
Lab Sample ID: M82628-42 Date Sampled: 05/06/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 86.6
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Lead 94.7 2.2 mg/kg 1 05/12/09 05/13/09 EAL SW846 6010B 1 SW846 3050B 2
(1) Instrument QC Batch: MA10458
(2) Prep QC Batch: MP13466
RL = Reporting Limit
144 of 211
M82628
33.124
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: S103924
Lab Sample ID: M82628-42A Date Sampled: 05/06/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 86.6
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, SPLP Leachate SW846 1312
Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.034 0.010 mg/l 1 05/14/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10475
(2) Prep QC Batch: MP13476
RL = Reporting Limit
MCL = Maximum Contamination Level (not available)
145 of 211
M82628
33.125
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: S103924
Lab Sample ID: M82628-42B Date Sampled: 05/06/09
Matrix: SO - Soil Date Received: 05/06/09
Percent Solids: 86.6
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.062 D008 5.0 0.010 mg/l 1 05/15/09 05/15/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10470
(2) Prep QC Batch: MP13487
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
146 of 211
M82628
33.126
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Certification Exceptions
• Certification Exceptions (CT)
• Chain of Custody
• RCP Form
• Sample Tracking Chronicle
Section 4
147 of 211
M82628
4
M82628: Chain of CustodyPage 1 of 5
148 of 211
M82628
44.1
M82628: Chain of CustodyPage 2 of 5
149 of 211
M82628
44.1
M82628: Chain of CustodyPage 3 of 5
150 of 211
M82628
44.1
M82628: Chain of CustodyPage 4 of 5
151 of 211
M82628
44.1
M82628: Chain of CustodyPage 5 of 5
152 of 211
M82628
44.1
Laboratory Name: Client:
Project Location: Project Number:
Sampling Date(s):
Laboratory Sample ID(s):
Methods:
1 Yes No
1A Yes No
1B Yes No
NA
2 Yes No
3 Yes No
4 Yes No
5 Yes No
Yes No
6 Yes No
7 Yes No
Authorized
Signature: Position: Lab Director
Printed Name: Reza Tand Date:
Accutest New England
5/20/2009
Reasonable Confidence Protocol
Where all the method specified preservation and holding time requirements met?
VPH and EPH mehods only: Was the VPH or EPH method conducted without
significant modifications (See section 11.3 of respective methods)
I, the undersigned, attest under pains and penalties of perjury that, to the best of my knowledge and belief
and based upon my personal inquiry of those responsible for providing the information contained in this
analytical report, such information is accurate and complete.
Were all QA/QC performance criteria specified in the CTDEP Reasonable
Confidence Protocol documents achieved?
EPA 160.3 M, SM21 2540 B MOD., SW846 6010B
For each analytical method referenced in this laboratory report package, were all
specified QA/QC performance criteria followed, including the requirement to explain any
criteria falling outside of acceptable guidelines, as specified in the CTDEP method-
specific Reasonable Confidence Protocol
documents)?
Were all samples received by the laboratory in a condition consistent with
that described on the associated chain-of-custody document(s)?
Laboratory Analysis
Reza Tand
a) Were reporting limits specified or referenced on the chain-of-custody?
b) Were these reporting limits met?
For each analytical method referenced in this laboratory report package,
were results reported for all constituents identified in the method-specific
analyte lists presented in the Reasonable Confidence Protocol documents?
Are project-specific matrix spikes and laboratory duplicates included in this
data set?
Note: For all questions to which the response was "No" (with the exception of question #7), additional
information must be provided in an attached narrative. If the answer to question #1, #1A or #1B is "No" , the
data package does not meet the requirements for "Reasonable Confidence" .
QA/QC Certification Form
Accutest New England
M82628-1 through M82628-42
5/4/2009
Olin Corporation
6107090004/01Mactec: Olin-Newhall St.-Hamden, CT
153 of 211
M82628
44.2
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-1 Collected: 04-MAY-09 10:05 By: MV Received: 06-MAY-09 By:
SB-1324
M82628-1 SM21 2540 B MOD. 11-MAY-09 NJ %SOL
M82628-1 SW846 6010B 11-MAY-09 16:28 PY 08-MAY-09 PY PB
M82628-2 Collected: 04-MAY-09 10:10 By: MV Received: 06-MAY-09 By:
SB-1404
M82628-2 SM21 2540 B MOD. 11-MAY-09 NJ %SOL
M82628-2 SW846 6010B 12-MAY-09 13:00 EAL 08-MAY-09 PY PB
M82628-3 Collected: 04-MAY-09 11:00 By: MV Received: 06-MAY-09 By:
P103901
M82628-3 SM21 2540 B MOD. 11-MAY-09 NJ %SOL
M82628-3 SW846 6010B 11-MAY-09 16:39 PY 08-MAY-09 PY PB
M82628-4 Collected: 04-MAY-09 11:12 By: MV Received: 06-MAY-09 By:
P3001S301
M82628-4 SM21 2540 B MOD. 11-MAY-09 NJ %SOL
M82628-4 SW846 6010B 11-MAY-09 16:44 PY 08-MAY-09 PY PB
M82628-5 Collected: 04-MAY-09 11:25 By: MV Received: 06-MAY-09 By:
P100524
M82628-5 SM21 2540 B MOD. 11-MAY-09 NJ %SOL
M82628-5 SW846 6010B 11-MAY-09 16:50 PY 08-MAY-09 PY PB
M82628-6 Collected: 04-MAY-09 11:55 By: MV Received: 06-MAY-09 By:
F3006S201
M82628-6 SW846 6010B 11-MAY-09 16:55 PY 08-MAY-09 PY PB
M82628-6 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-7 Collected: 04-MAY-09 12:10 By: MV Received: 06-MAY-09 By:
WIN-106124
M82628-7 SW846 6010B 11-MAY-09 17:00 PY 08-MAY-09 PY PB
Page 1 of 17
154 of 211
M82628
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-7 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-8 Collected: 04-MAY-09 12:20 By: MV Received: 06-MAY-09 By:
C100324
M82628-8 SW846 6010B 11-MAY-09 17:06 PY 08-MAY-09 PY PB
M82628-8 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-9 Collected: 04-MAY-09 12:35 By: MV Received: 06-MAY-09 By:
124BT-HA512
M82628-9 SW846 6010B 11-MAY-09 17:11 PY 08-MAY-09 PY PB
M82628-9 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-10 Collected: 04-MAY-09 12:45 By: MV Received: 06-MAY-09 By:
124BT-HA112
M82628-10 SW846 6010B 11-MAY-09 17:35 PY 08-MAY-09 PY PB
M82628-10 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-11 Collected: 04-MAY-09 12:58 By: MV Received: 06-MAY-09 By:
95-MS01
M82628-11 SW846 6010B 11-MAY-09 17:41 PY 08-MAY-09 PY PB
M82628-11 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-12 Collected: 04-MAY-09 14:40 By: MV Received: 06-MAY-09 By:
F3002S101
M82628-12 SW846 6010B 11-MAY-09 17:46 PY 08-MAY-09 PY PB
M82628-12 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-13 Collected: 04-MAY-09 15:00 By: MV Received: 06-MAY-09 By:
127MORSE-HA412
M82628-13 SW846 6010B 11-MAY-09 17:52 PY 08-MAY-09 PY PB
M82628-13 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
Page 2 of 17
155 of 211
M82628
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-14 Collected: 04-MAY-09 15:10 By: MV Received: 06-MAY-09 By:
127MORSE-HA112
M82628-14 SW846 6010B 11-MAY-09 17:57 PY 08-MAY-09 PY PB
M82628-14 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-15 Collected: 04-MAY-09 15:13 By: MV Received: 06-MAY-09 By:
127MORSE-HA212
M82628-15 SW846 6010B 11-MAY-09 18:02 PY 08-MAY-09 PY PB
M82628-15 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-16 Collected: 04-MAY-09 15:30 By: MV Received: 06-MAY-09 By:
S104412
M82628-16 SW846 6010B 11-MAY-09 18:08 PY 08-MAY-09 PY PB
M82628-16 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-17 Collected: 04-MAY-09 16:10 By: MV Received: 06-MAY-09 By:
S105614
M82628-17 SW846 6010B 11-MAY-09 18:13 PY 08-MAY-09 PY PB
M82628-17 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-18 Collected: 04-MAY-09 16:25 By: MV Received: 06-MAY-09 By:
F3003S101
M82628-18 SW846 6010B 11-MAY-09 18:19 PY 08-MAY-09 PY PB
M82628-18 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-19 Collected: 04-MAY-09 16:45 By: MV Received: 06-MAY-09 By:
C100624
M82628-19 SW846 6010B 11-MAY-09 18:24 PY 08-MAY-09 PY PB
M82628-19 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-1A Collected: 04-MAY-09 10:05 By: MV Received: 06-MAY-09 By:
SB-1324
Page 3 of 17
156 of 211
M82628
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-1A SW846 6010B 11-MAY-09 23:55 PY 08-MAY-09 PY EPB
M82628-1B Collected: 04-MAY-09 10:05 By: MV Received: 06-MAY-09 By:
SB-1324
M82628-1B SW846 6010B 18-MAY-09 11:30 EAL 15-MAY-09 PY EPB
M82628-20 Collected: 04-MAY-09 17:00 By: MV Received: 06-MAY-09 By:
C3001S101
M82628-20 SM21 2540 B MOD. 08-MAY-09 NJ %SOL
M82628-20 SW846 6010B 12-MAY-09 10:34 EAL 11-MAY-09 PY PB
M82628-21 Collected: 04-MAY-09 17:40 By: MV Received: 06-MAY-09 By:
N101801
M82628-21 SM21 2540 B MOD. 08-MAY-09 NJ %SOL
M82628-21 SW846 6010B 11-MAY-09 15:56 PY 08-MAY-09 PY PB
M82628-22 Collected: 04-MAY-09 17:40 By: MV Received: 06-MAY-09 By:
N101801DUP
M82628-22 SM21 2540 B MOD. 08-MAY-09 NJ %SOL
M82628-22 SW846 6010B 12-MAY-09 10:39 EAL 11-MAY-09 PY PB
M82628-23 Collected: 05-MAY-09 09:40 By: MV Received: 06-MAY-09 By:
H3009S101
M82628-23 SM21 2540 B MOD. 08-MAY-09 NJ %SOL
M82628-23 SW846 6010B 12-MAY-09 10:44 EAL 11-MAY-09 PY PB
M82628-24 Collected: 05-MAY-09 09:50 By: MV Received: 06-MAY-09 By:
H3001S301
M82628-24 SM21 2540 B MOD. 08-MAY-09 NJ %SOL
M82628-24 SW846 6010B 12-MAY-09 10:50 EAL 11-MAY-09 PY PB
M82628-25 Collected: 05-MAY-09 10:02 By: MV Received: 06-MAY-09 By:
J101012
Page 4 of 17
157 of 211
M82628
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-25 SM21 2540 B MOD. 08-MAY-09 NJ %SOL
M82628-25 SW846 6010B 12-MAY-09 10:55 EAL 11-MAY-09 PY PB
M82628-26 Collected: 05-MAY-09 10:13 By: MV Received: 06-MAY-09 By:
J100601
M82628-26 SM21 2540 B MOD. 08-MAY-09 NJ %SOL
M82628-26 SW846 6010B 12-MAY-09 11:01 EAL 11-MAY-09 PY PB
M82628-27 Collected: 05-MAY-09 10:25 By: MV Received: 06-MAY-09 By:
H100624
M82628-27 SM21 2540 B MOD. 08-MAY-09 NJ %SOL
M82628-27 SW846 6010B 12-MAY-09 12:48 EAL 11-MAY-09 PY PB
M82628-28 Collected: 05-MAY-09 10:32 By: MV Received: 06-MAY-09 By:
H2002S23
M82628-28 SM21 2540 B MOD. 08-MAY-09 NJ %SOL
M82628-28 SW846 6010B 12-MAY-09 12:54 EAL 11-MAY-09 PY PB
M82628-29 Collected: 05-MAY-09 11:00 By: MV Received: 06-MAY-09 By:
H3003S101
M82628-29 SM21 2540 B MOD. 08-MAY-09 NJ %SOL
M82628-29 SW846 6010B 12-MAY-09 11:17 EAL 11-MAY-09 PY PB
M82628-2A Collected: 04-MAY-09 10:10 By: MV Received: 06-MAY-09 By:
SB-1404
M82628-2A SW846 6010B 12-MAY-09 00:11 PY 08-MAY-09 PY EPB
M82628-2B Collected: 04-MAY-09 10:10 By: MV Received: 06-MAY-09 By:
SB-1404
M82628-2B SW846 6010B 18-MAY-09 15:06 EAL 15-MAY-09 PY EPB
M82628-30 Collected: 05-MAY-09 11:25 By: MV Received: 06-MAY-09 By:
A300401
Page 5 of 17
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44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-30 SM21 2540 B MOD. 08-MAY-09 NJ %SOL
M82628-30 SW846 6010B 12-MAY-09 11:33 EAL 11-MAY-09 PY PB
M82628-31 Collected: 05-MAY-09 11:35 By: MV Received: 06-MAY-09 By:
A3011S101
M82628-31 SM21 2540 B MOD. 08-MAY-09 NJ %SOL
M82628-31 SW846 6010B 12-MAY-09 11:39 EAL 11-MAY-09 PY PB
M82628-32 Collected: 05-MAY-09 11:40 By: MV Received: 06-MAY-09 By:
267MORSE-HA512
M82628-32 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-32 SW846 6010B 12-MAY-09 11:45 EAL 11-MAY-09 PY PB
M82628-33 Collected: 05-MAY-09 11:55 By: MV Received: 06-MAY-09 By:
K111701
M82628-33 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-33 SW846 6010B 12-MAY-09 11:53 EAL 11-MAY-09 PY PB
M82628-34 Collected: 05-MAY-09 12:15 By: MV Received: 06-MAY-09 By:
L100201
M82628-34 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-34 SW846 6010B 12-MAY-09 11:58 EAL 11-MAY-09 PY PB
M82628-35 Collected: 05-MAY-09 12:25 By: MV Received: 06-MAY-09 By:
L100524
M82628-35 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-35 SW846 6010B 12-MAY-09 12:04 EAL 11-MAY-09 PY PB
M82628-36 Collected: 05-MAY-09 13:00 By: MV Received: 06-MAY-09 By:
L100824
M82628-36 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-36 SW846 6010B 12-MAY-09 10:01 EAL 11-MAY-09 PY PB
Page 6 of 17
159 of 211
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44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-37 Collected: 05-MAY-09 13:00 By: MV Received: 06-MAY-09 By:
L100824DUP
M82628-37 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-37 SW846 6010B 12-MAY-09 12:09 EAL 11-MAY-09 PY PB
M82628-38 Collected: 05-MAY-09 14:20 By: MV Received: 06-MAY-09 By:
K103801
M82628-38 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-38 SW846 6010B 12-MAY-09 12:14 EAL 11-MAY-09 PY PB
M82628-39 Collected: 05-MAY-09 14:40 By: MV Received: 06-MAY-09 By:
C100424
M82628-39 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-39 SW846 6010B 12-MAY-09 12:20 EAL 11-MAY-09 PY PB
M82628-3A Collected: 04-MAY-09 11:00 By: MV Received: 06-MAY-09 By:
P103901
M82628-3A SW846 6010B 12-MAY-09 00:16 PY 08-MAY-09 PY EPB
M82628-3B Collected: 04-MAY-09 11:00 By: MV Received: 06-MAY-09 By:
P103901
M82628-3B SW846 6010B 18-MAY-09 13:05 EAL 15-MAY-09 PY EPB
M82628-40 Collected: 05-MAY-09 15:10 By: MV Received: 06-MAY-09 By:
R103102
M82628-40 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-40 SW846 6010B 12-MAY-09 12:25 EAL 11-MAY-09 PY PB
M82628-41 Collected: 05-MAY-09 16:45 By: MV Received: 06-MAY-09 By:
M503002
M82628-41 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-41 SW846 6010B 13-MAY-09 12:12 EAL 12-MAY-09 PY PB
Page 7 of 17
160 of 211
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44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-42 Collected: 06-MAY-09 11:00 By: MV Received: 06-MAY-09 By:
S103924
M82628-42 SM21 2540 B MOD. 12-MAY-09 NJ %SOL
M82628-42 SW846 6010B 13-MAY-09 12:18 EAL 12-MAY-09 PY PB
M82628-4A Collected: 04-MAY-09 11:12 By: MV Received: 06-MAY-09 By:
P3001S301
M82628-4A SW846 6010B 12-MAY-09 00:22 PY 08-MAY-09 PY EPB
M82628-4B Collected: 04-MAY-09 11:12 By: MV Received: 06-MAY-09 By:
P3001S301
M82628-4B SW846 6010B 18-MAY-09 12:54 EAL 15-MAY-09 PY EPB
M82628-5A Collected: 04-MAY-09 11:25 By: MV Received: 06-MAY-09 By:
P100524
M82628-5A SW846 6010B 12-MAY-09 00:27 PY 08-MAY-09 PY EPB
M82628-5B Collected: 04-MAY-09 11:25 By: MV Received: 06-MAY-09 By:
P100524
M82628-5B SW846 6010B 18-MAY-09 12:49 EAL 15-MAY-09 PY EPB
M82628-6A Collected: 04-MAY-09 11:55 By: MV Received: 06-MAY-09 By:
F3006S201
M82628-6A SW846 6010B 12-MAY-09 00:33 PY 08-MAY-09 PY EPB
M82628-6B Collected: 04-MAY-09 11:55 By: MV Received: 06-MAY-09 By:
F3006S201
M82628-6B SW846 6010B 18-MAY-09 12:43 EAL 15-MAY-09 PY EPB
M82628-7A Collected: 04-MAY-09 12:10 By: MV Received: 06-MAY-09 By:
WIN-106124
Page 8 of 17
161 of 211
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44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-7A SW846 6010B 12-MAY-09 00:38 PY 08-MAY-09 PY EPB
M82628-7B Collected: 04-MAY-09 12:10 By: MV Received: 06-MAY-09 By:
WIN-106124
M82628-7B SW846 6010B 18-MAY-09 13:16 EAL 15-MAY-09 PY EPB
M82628-8A Collected: 04-MAY-09 12:20 By: MV Received: 06-MAY-09 By:
C100324
M82628-8A SW846 6010B 12-MAY-09 00:44 PY 08-MAY-09 PY EPB
M82628-8B Collected: 04-MAY-09 12:20 By: MV Received: 06-MAY-09 By:
C100324
M82628-8B SW846 6010B 18-MAY-09 13:21 EAL 15-MAY-09 PY EPB
M82628-9A Collected: 04-MAY-09 12:35 By: MV Received: 06-MAY-09 By:
124BT-HA512
M82628-9A SW846 6010B 12-MAY-09 14:34 EAL 12-MAY-09 PY EPB
M82628-9B Collected: 04-MAY-09 12:35 By: MV Received: 06-MAY-09 By:
124BT-HA512
M82628-9B SW846 6010B 14-MAY-09 11:24 EAL 13-MAY-09 PY EPB
M82628-10ACollected: 04-MAY-09 12:45 By: MV Received: 06-MAY-09 By:
124BT-HA112
M82628-10ASW846 6010B 12-MAY-09 14:50 EAL 12-MAY-09 PY EPB
M82628-10BCollected: 04-MAY-09 12:45 By: MV Received: 06-MAY-09 By:
124BT-HA112
M82628-10BSW846 6010B 14-MAY-09 11:29 EAL 13-MAY-09 PY EPB
M82628-11ACollected: 04-MAY-09 12:58 By: MV Received: 06-MAY-09 By:
95-MS01
Page 9 of 17
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44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-11ASW846 6010B 12-MAY-09 14:56 EAL 12-MAY-09 PY EPB
M82628-11BCollected: 04-MAY-09 12:58 By: MV Received: 06-MAY-09 By:
95-MS01
M82628-11BSW846 6010B 14-MAY-09 11:35 EAL 13-MAY-09 PY EPB
M82628-12ACollected: 04-MAY-09 14:40 By: MV Received: 06-MAY-09 By:
F3002S101
M82628-12ASW846 6010B 12-MAY-09 15:01 EAL 12-MAY-09 PY EPB
M82628-12BCollected: 04-MAY-09 14:40 By: MV Received: 06-MAY-09 By:
F3002S101
M82628-12BSW846 6010B 14-MAY-09 11:41 EAL 13-MAY-09 PY EPB
M82628-13ACollected: 04-MAY-09 15:00 By: MV Received: 06-MAY-09 By:
127MORSE-HA412
M82628-13ASW846 6010B 12-MAY-09 15:06 EAL 12-MAY-09 PY EPB
M82628-13BCollected: 04-MAY-09 15:00 By: MV Received: 06-MAY-09 By:
127MORSE-HA412
M82628-13BSW846 6010B 14-MAY-09 11:46 EAL 13-MAY-09 PY EPB
M82628-14ACollected: 04-MAY-09 15:10 By: MV Received: 06-MAY-09 By:
127MORSE-HA112
M82628-14ASW846 6010B 12-MAY-09 15:12 EAL 12-MAY-09 PY EPB
M82628-14BCollected: 04-MAY-09 15:10 By: MV Received: 06-MAY-09 By:
127MORSE-HA112
M82628-14BSW846 6010B 14-MAY-09 11:52 EAL 13-MAY-09 PY EPB
M82628-15ACollected: 04-MAY-09 15:13 By: MV Received: 06-MAY-09 By:
127MORSE-HA212
Page 10 of 17
163 of 211
M82628
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-15ASW846 6010B 12-MAY-09 15:17 EAL 12-MAY-09 PY EPB
M82628-15BCollected: 04-MAY-09 15:13 By: MV Received: 06-MAY-09 By:
127MORSE-HA212
M82628-15BSW846 6010B 14-MAY-09 11:58 EAL 13-MAY-09 PY EPB
M82628-16ACollected: 04-MAY-09 15:30 By: MV Received: 06-MAY-09 By:
S104412
M82628-16ASW846 6010B 12-MAY-09 15:23 EAL 12-MAY-09 PY EPB
M82628-16BCollected: 04-MAY-09 15:30 By: MV Received: 06-MAY-09 By:
S104412
M82628-16BSW846 6010B 14-MAY-09 12:03 EAL 13-MAY-09 PY EPB
M82628-17ACollected: 04-MAY-09 16:10 By: MV Received: 06-MAY-09 By:
S105614
M82628-17ASW846 6010B 12-MAY-09 15:28 EAL 12-MAY-09 PY EPB
M82628-17BCollected: 04-MAY-09 16:10 By: MV Received: 06-MAY-09 By:
S105614
M82628-17BSW846 6010B 14-MAY-09 12:09 EAL 13-MAY-09 PY EPB
M82628-18ACollected: 04-MAY-09 16:25 By: MV Received: 06-MAY-09 By:
F3003S101
M82628-18ASW846 6010B 12-MAY-09 15:34 EAL 12-MAY-09 PY EPB
M82628-18BCollected: 04-MAY-09 16:25 By: MV Received: 06-MAY-09 By:
F3003S101
M82628-18BSW846 6010B 14-MAY-09 12:26 EAL 13-MAY-09 PY EPB
M82628-19ACollected: 04-MAY-09 16:45 By: MV Received: 06-MAY-09 By:
C100624
Page 11 of 17
164 of 211
M82628
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-19ASW846 6010B 12-MAY-09 15:39 EAL 12-MAY-09 PY EPB
M82628-19BCollected: 04-MAY-09 16:45 By: MV Received: 06-MAY-09 By:
C100624
M82628-19BSW846 6010B 14-MAY-09 12:31 EAL 13-MAY-09 PY EPB
M82628-20ACollected: 04-MAY-09 17:00 By: MV Received: 06-MAY-09 By:
C3001S101
M82628-20ASW846 6010B 12-MAY-09 15:59 EAL 12-MAY-09 PY EPB
M82628-20BCollected: 04-MAY-09 17:00 By: MV Received: 06-MAY-09 By:
C3001S101
M82628-20BSW846 6010B 14-MAY-09 12:37 EAL 13-MAY-09 PY EPB
M82628-21ACollected: 04-MAY-09 17:40 By: MV Received: 06-MAY-09 By:
N101801
M82628-21ASW846 6010B 11-MAY-09 22:28 PY 08-MAY-09 PY EPB
M82628-21BCollected: 04-MAY-09 17:40 By: MV Received: 06-MAY-09 By:
N101801
M82628-21BSW846 6010B 14-MAY-09 10:46 EAL 13-MAY-09 PY EPB
M82628-22ACollected: 04-MAY-09 17:40 By: MV Received: 06-MAY-09 By:
N101801DUP
M82628-22ASW846 6010B 12-MAY-09 00:49 PY 08-MAY-09 PY EPB
M82628-22BCollected: 04-MAY-09 17:40 By: MV Received: 06-MAY-09 By:
N101801DUP
M82628-22BSW846 6010B 14-MAY-09 12:43 EAL 13-MAY-09 PY EPB
M82628-23ACollected: 05-MAY-09 09:40 By: MV Received: 06-MAY-09 By:
H3009S101
Page 12 of 17
165 of 211
M82628
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-23ASW846 6010B 12-MAY-09 16:04 EAL 12-MAY-09 PY EPB
M82628-23BCollected: 05-MAY-09 09:40 By: MV Received: 06-MAY-09 By:
H3009S101
M82628-23BSW846 6010B 14-MAY-09 12:48 EAL 13-MAY-09 PY EPB
M82628-24ACollected: 05-MAY-09 09:50 By: MV Received: 06-MAY-09 By:
H3001S301
M82628-24ASW846 6010B 12-MAY-09 16:10 EAL 12-MAY-09 PY EPB
M82628-24BCollected: 05-MAY-09 09:50 By: MV Received: 06-MAY-09 By:
H3001S301
M82628-24BSW846 6010B 14-MAY-09 12:54 EAL 13-MAY-09 PY EPB
M82628-25ACollected: 05-MAY-09 10:02 By: MV Received: 06-MAY-09 By:
J101012
M82628-25ASW846 6010B 12-MAY-09 16:15 EAL 12-MAY-09 PY EPB
M82628-25BCollected: 05-MAY-09 10:02 By: MV Received: 06-MAY-09 By:
J101012
M82628-25BSW846 6010B 14-MAY-09 13:00 EAL 13-MAY-09 PY EPB
M82628-26ACollected: 05-MAY-09 10:13 By: MV Received: 06-MAY-09 By:
J100601
M82628-26ASW846 6010B 12-MAY-09 16:21 EAL 12-MAY-09 PY EPB
M82628-26BCollected: 05-MAY-09 10:13 By: MV Received: 06-MAY-09 By:
J100601
M82628-26BSW846 6010B 14-MAY-09 13:05 EAL 13-MAY-09 PY EPB
M82628-27ACollected: 05-MAY-09 10:25 By: MV Received: 06-MAY-09 By:
H100624
Page 13 of 17
166 of 211
M82628
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-27ASW846 6010B 12-MAY-09 16:26 EAL 12-MAY-09 PY EPB
M82628-27BCollected: 05-MAY-09 10:25 By: MV Received: 06-MAY-09 By:
H100624
M82628-27BSW846 6010B 14-MAY-09 13:49 EAL 13-MAY-09 PY EPB
M82628-28ACollected: 05-MAY-09 10:32 By: MV Received: 06-MAY-09 By:
H2002S23
M82628-28ASW846 6010B 12-MAY-09 16:31 EAL 12-MAY-09 PY EPB
M82628-28BCollected: 05-MAY-09 10:32 By: MV Received: 06-MAY-09 By:
H2002S23
M82628-28BSW846 6010B 14-MAY-09 13:55 EAL 13-MAY-09 PY EPB
M82628-29ACollected: 05-MAY-09 11:00 By: MV Received: 06-MAY-09 By:
H3003S101
M82628-29ASW846 6010B 18-MAY-09 13:45 EAL 14-MAY-09 EAL EPB
M82628-29BCollected: 05-MAY-09 11:00 By: MV Received: 06-MAY-09 By:
H3003S101
M82628-29BSW846 6010B 18-MAY-09 11:36 EAL 15-MAY-09 PY EPB
M82628-30ACollected: 05-MAY-09 11:25 By: MV Received: 06-MAY-09 By:
A300401
M82628-30ASW846 6010B 18-MAY-09 13:50 EAL 14-MAY-09 EAL EPB
M82628-30BCollected: 05-MAY-09 11:25 By: MV Received: 06-MAY-09 By:
A300401
M82628-30BSW846 6010B 18-MAY-09 11:49 EAL 15-MAY-09 PY EPB
M82628-31ACollected: 05-MAY-09 11:35 By: MV Received: 06-MAY-09 By:
A3011S101
Page 14 of 17
167 of 211
M82628
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-31ASW846 6010B 18-MAY-09 13:56 EAL 14-MAY-09 EAL EPB
M82628-31BCollected: 05-MAY-09 11:35 By: MV Received: 06-MAY-09 By:
A3011S101
M82628-31BSW846 6010B 18-MAY-09 11:54 EAL 15-MAY-09 PY EPB
M82628-32ACollected: 05-MAY-09 11:40 By: MV Received: 06-MAY-09 By:
267MORSE-HA512
M82628-32ASW846 6010B 18-MAY-09 14:01 EAL 14-MAY-09 EAL EPB
M82628-32BCollected: 05-MAY-09 11:40 By: MV Received: 06-MAY-09 By:
267MORSE-HA512
M82628-32BSW846 6010B 18-MAY-09 12:00 EAL 15-MAY-09 PY EPB
M82628-33ACollected: 05-MAY-09 11:55 By: MV Received: 06-MAY-09 By:
K111701
M82628-33ASW846 6010B 18-MAY-09 14:07 EAL 14-MAY-09 EAL EPB
M82628-33BCollected: 05-MAY-09 11:55 By: MV Received: 06-MAY-09 By:
K111701
M82628-33BSW846 6010B 18-MAY-09 12:05 EAL 15-MAY-09 PY EPB
M82628-34ACollected: 05-MAY-09 12:15 By: MV Received: 06-MAY-09 By:
L100201
M82628-34ASW846 6010B 18-MAY-09 14:12 EAL 14-MAY-09 EAL EPB
M82628-34BCollected: 05-MAY-09 12:15 By: MV Received: 06-MAY-09 By:
L100201
M82628-34BSW846 6010B 18-MAY-09 12:11 EAL 15-MAY-09 PY EPB
M82628-35ACollected: 05-MAY-09 12:25 By: MV Received: 06-MAY-09 By:
L100524
Page 15 of 17
168 of 211
M82628
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-35ASW846 6010B 18-MAY-09 14:17 EAL 14-MAY-09 EAL EPB
M82628-35BCollected: 05-MAY-09 12:25 By: MV Received: 06-MAY-09 By:
L100524
M82628-35BSW846 6010B 18-MAY-09 12:16 EAL 15-MAY-09 PY EPB
M82628-36ACollected: 05-MAY-09 13:00 By: MV Received: 06-MAY-09 By:
L100824
M82628-36ASW846 6010B 14-MAY-09 15:23 EAL 14-MAY-09 EAL EPB
M82628-36BCollected: 05-MAY-09 13:00 By: MV Received: 06-MAY-09 By:
L100824
M82628-36BSW846 6010B 18-MAY-09 10:55 EAL 15-MAY-09 PY EPB
M82628-37ACollected: 05-MAY-09 13:00 By: MV Received: 06-MAY-09 By:
L100824DUP
M82628-37ASW846 6010B 18-MAY-09 14:23 EAL 14-MAY-09 EAL EPB
M82628-37BCollected: 05-MAY-09 13:00 By: MV Received: 06-MAY-09 By:
L100824DUP
M82628-37BSW846 6010B 18-MAY-09 12:32 EAL 15-MAY-09 PY EPB
M82628-38ACollected: 05-MAY-09 14:20 By: MV Received: 06-MAY-09 By:
K103801
M82628-38ASW846 6010B 18-MAY-09 14:28 EAL 14-MAY-09 EAL EPB
M82628-38BCollected: 05-MAY-09 14:20 By: MV Received: 06-MAY-09 By:
K103801
M82628-38BSW846 6010B 18-MAY-09 12:38 EAL 15-MAY-09 PY EPB
M82628-39ACollected: 05-MAY-09 14:40 By: MV Received: 06-MAY-09 By:
C100424
Page 16 of 17
169 of 211
M82628
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M82628
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M82628-39ASW846 6010B 18-MAY-09 14:34 EAL 14-MAY-09 EAL EPB
M82628-39BCollected: 05-MAY-09 14:40 By: MV Received: 06-MAY-09 By:
C100424
M82628-39BSW846 6010B 18-MAY-09 13:10 EAL 15-MAY-09 PY EPB
M82628-40ACollected: 05-MAY-09 15:10 By: MV Received: 06-MAY-09 By:
R103102
M82628-40ASW846 6010B 18-MAY-09 14:50 EAL 14-MAY-09 EAL EPB
M82628-40BCollected: 05-MAY-09 15:10 By: MV Received: 06-MAY-09 By:
R103102
M82628-40BSW846 6010B 18-MAY-09 12:59 EAL 15-MAY-09 PY EPB
M82628-41ACollected: 05-MAY-09 16:45 By: MV Received: 06-MAY-09 By:
M503002
M82628-41ASW846 6010B 18-MAY-09 14:55 EAL 14-MAY-09 EAL EPB
M82628-41BCollected: 05-MAY-09 16:45 By: MV Received: 06-MAY-09 By:
M503002
M82628-41BSW846 6010B 15-MAY-09 14:47 EAL 15-MAY-09 PY EPB
M82628-42ACollected: 06-MAY-09 11:00 By: MV Received: 06-MAY-09 By:
S103924
M82628-42ASW846 6010B 18-MAY-09 15:01 EAL 14-MAY-09 EAL EPB
M82628-42BCollected: 06-MAY-09 11:00 By: MV Received: 06-MAY-09 By:
S103924
M82628-42BSW846 6010B 15-MAY-09 14:53 EAL 15-MAY-09 PY EPB
Page 17 of 17
170 of 211
M82628
44.3
Accutest Laboratories
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Matrix Spike and Duplicate Summaries
• Blank Spike and Lab Control Sample Summaries
• Serial Dilution Summaries
Section 5
171 of 211
M82628
5
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13454 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg
Prep Date: 05/08/09
MBMetal RL IDL MDL raw final
Aluminum 20 .86 2.1
Antimony 2.0 .16 .41
Arsenic 2.0 .23 .29
Barium 20 .06 .26
Beryllium 0.40 .015 .022
Boron 10 .13 .31
Cadmium 0.40 .022 .024
Calcium 500 .62 .74
Chromium 1.0 .072 .14
Cobalt 5.0 .054 .079
Copper 2.5 .064 .11
Iron 10 .66 2.5
Lead 2.0 .11 .16 0.19 <2.0
Magnesium 500 .51 .6
Manganese 1.5 .018 .031
Molybdenum 10 .088 .12
Nickel 4.0 .061 .13
Potassium 500 1.5 8.1
Selenium 2.0 .26 .34
Silver 0.50 .054 .076
Sodium 500 7.7 19
Strontium 1.0 .012 .022
Thallium 2.0 .29 .33
Tin 10 .4 .55
Titanium 5.0 .059 .5
Vanadium 3.0 .24 .26
Zinc 2.0 .061 .17
Associated samples MP13454: M82628-1, M82628-2, M82628-3, M82628-4, M82628-5, M82628-6, M82628-7, M82628-8, M82628-9, M82628-10, M82628-11, M82628-12, M82628-13, M82628-14, M82628-15, M82628-16, M82628-17,M82628-18, M82628-19, M82628-21
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
172 of 211
M82628
55.1.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13454 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg
Prep Date: 05/08/09 05/08/09
M82628-21 Spikelot QC M82628-21 QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 359 397 104 36.7 (a) 75-125 359 307 15.6 0-20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13454: M82628-1, M82628-2, M82628-3, M82628-4, M82628-5, M82628-6, M82628-7, M82628-8, M82628-9, M82628-10, M82628-11, M82628-12, M82628-13, M82628-14, M82628-15, M82628-16, M82628-17,M82628-18, M82628-19, M82628-21
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) Spike recovery indicates possible matrix interference and/or sample nonhomogeneity.Post spike within
acceptable range.
_________________________________________________________________________________________________________
Page 1
173 of 211
M82628
55.1.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13454 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg
Prep Date: 05/08/09 05/08/09
BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 96.9 100 96.9 80-120 96.0 100 96.0 0.9 20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13454: M82628-1, M82628-2, M82628-3, M82628-4, M82628-5, M82628-6, M82628-7, M82628-8, M82628-9, M82628-10, M82628-11, M82628-12, M82628-13, M82628-14, M82628-15, M82628-16, M82628-17,M82628-18, M82628-19, M82628-21
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
174 of 211
M82628
55.1.3
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13454 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg
Prep Date: 05/08/09
LCS Spikelot QCMetal Result MPLCS63 % Rec Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 201 223 90.1 82-118
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13454: M82628-1, M82628-2, M82628-3, M82628-4, M82628-5, M82628-6, M82628-7, M82628-8, M82628-9, M82628-10, M82628-11, M82628-12, M82628-13, M82628-14, M82628-15, M82628-16, M82628-17,M82628-18, M82628-19, M82628-21
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
175 of 211
M82628
55.1.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13454 Methods: SW846 6010B Matrix Type: SOLID Units: ug/l
Prep Date: 05/08/09
M82628-21 QCMetal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 3400 3590 5.6 0-10
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13454: M82628-1, M82628-2, M82628-3, M82628-4, M82628-5, M82628-6, M82628-7, M82628-8, M82628-9, M82628-10, M82628-11, M82628-12, M82628-13, M82628-14, M82628-15, M82628-16, M82628-17,M82628-18, M82628-19, M82628-21
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
176 of 211
M82628
55.1.4
POST DIGESTATE SPIKE SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13454 Methods: SW846 6010B Matrix Type: SOLID Units: ug/l
Prep Date: 05/08/09
Sample Final M82628-21 PS Spike Spike Spike QCMetal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 9.9 10 3399.98 3365.98 9338 .1 680 6800 87.8 -
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13454: M82628-1, M82628-2, M82628-3, M82628-4, M82628-5, M82628-6, M82628-7, M82628-8, M82628-9, M82628-10, M82628-11, M82628-12, M82628-13, M82628-14, M82628-15, M82628-16, M82628-17,M82628-18, M82628-19, M82628-21
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(**) Corr. sample result = Raw * (sample volume / final volume)(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
177 of 211
M82628
55.1.5
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13455 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/08/09
MBMetal RL IDL MDL raw final
Aluminum 0.20 .0086 .031
Antimony 0.0060 .0016 .003
Arsenic 0.025 .0023 .0032
Barium 0.50 .0006 .0012
Beryllium 0.0040 .00015 .0003
Boron 0.10 .0013 .0048
Cadmium 0.0040 .00022 .0003
Calcium 5.0 .0062 .04
Chromium 0.010 .00072 .0014
Cobalt 0.050 .00054 .001
Copper 0.025 .00064 .0018
Iron 0.10 .0066 .029
Lead 0.010 .0011 .0018 0.0010 <0.010
Magnesium 5.0 .0051 .01
Manganese 0.015 .00018 .0013
Molybdenum 0.10 .00088 .0014
Nickel 0.040 .00061 .001
Potassium 5.0 .015 .031
Selenium 0.025 .0026 .0033
Silver 0.0050 .00054 .0007
Sodium 5.0 .077 .21
Strontium 0.010 .00012 .0003
Thallium 0.0050 .0029 .0045
Tin 0.10 .004 .0099
Titanium 0.050 .00059 .0051
Vanadium 0.030 .0024 .0035
Zinc 0.10 .00061 .0013
Associated samples MP13455: M82628-1A, M82628-2A, M82628-3A, M82628-4A, M82628-5A, M82628-6A, M82628-7A,M82628-8A, M82628-21A, M82628-22A
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
178 of 211
M82628
55.2.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13455 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/08/09 05/08/09
M82628-21A Spikelot QC M82628-21A QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 0.066 1.1 1.0 103.4 75-125 0.066 0.066 0.0 0-20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13455: M82628-1A, M82628-2A, M82628-3A, M82628-4A, M82628-5A, M82628-6A, M82628-7A,M82628-8A, M82628-21A, M82628-22A
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
179 of 211
M82628
55.2.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13455 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/08/09 05/08/09
BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 1.0 1.0 100.0 80-120 1.0 1.0 100.0 0.0 20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13455: M82628-1A, M82628-2A, M82628-3A, M82628-4A, M82628-5A, M82628-6A, M82628-7A,M82628-8A, M82628-21A, M82628-22A
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
180 of 211
M82628
55.2.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13455 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date: 05/08/09
M82628-21A QCMetal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 66.0 72.5 9.9 0-10
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13455: M82628-1A, M82628-2A, M82628-3A, M82628-4A, M82628-5A, M82628-6A, M82628-7A,M82628-8A, M82628-21A, M82628-22A
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
181 of 211
M82628
55.2.4
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13463 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg
Prep Date: 05/11/09
MBMetal RL IDL MDL raw final
Aluminum 20 .86 2.1
Antimony 2.0 .16 .41
Arsenic 2.0 .23 .29
Barium 20 .06 .26
Beryllium 0.40 .015 .022
Boron 10 .13 .31
Cadmium 0.40 .022 .024
Calcium 500 .62 .74
Chromium 1.0 .072 .14
Cobalt 5.0 .054 .079
Copper 2.5 .064 .11
Iron 10 .66 2.5
Lead 2.0 .11 .16 0.24 <2.0
Magnesium 500 .51 .6
Manganese 1.5 .018 .031
Molybdenum 10 .088 .12
Nickel 4.0 .061 .13
Potassium 500 1.5 8.1
Selenium 2.0 .26 .34
Silver 0.50 .054 .076
Sodium 500 7.7 19
Strontium 1.0 .012 .022
Thallium 2.0 .29 .33
Tin 10 .4 .55
Titanium 5.0 .059 .5
Vanadium 3.0 .24 .26
Zinc 2.0 .061 .17
Associated samples MP13463: M82628-20, M82628-22, M82628-23, M82628-24, M82628-25, M82628-26, M82628-27,M82628-28, M82628-29, M82628-30, M82628-31, M82628-32, M82628-33, M82628-34, M82628-35, M82628-36,M82628-37, M82628-38, M82628-39, M82628-40
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
182 of 211
M82628
55.3.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13463 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg
Prep Date: 05/11/09 05/11/09
M82628-36 Spikelot QC M82628-36 QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 429 525 108 89.3 75-125 429 486 12.5 0-20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13463: M82628-20, M82628-22, M82628-23, M82628-24, M82628-25, M82628-26, M82628-27,M82628-28, M82628-29, M82628-30, M82628-31, M82628-32, M82628-33, M82628-34, M82628-35, M82628-36,M82628-37, M82628-38, M82628-39, M82628-40
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
183 of 211
M82628
55.3.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13463 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg
Prep Date: 05/11/09 05/11/09
BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 94.9 100 94.9 80-120 95.3 100 95.3 0.4 20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13463: M82628-20, M82628-22, M82628-23, M82628-24, M82628-25, M82628-26, M82628-27,M82628-28, M82628-29, M82628-30, M82628-31, M82628-32, M82628-33, M82628-34, M82628-35, M82628-36,M82628-37, M82628-38, M82628-39, M82628-40
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
184 of 211
M82628
55.3.3
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13463 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg
Prep Date: 05/11/09
LCS Spikelot QCMetal Result MPLCS63 % Rec Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 213 223 95.5 82-118
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13463: M82628-20, M82628-22, M82628-23, M82628-24, M82628-25, M82628-26, M82628-27,M82628-28, M82628-29, M82628-30, M82628-31, M82628-32, M82628-33, M82628-34, M82628-35, M82628-36,M82628-37, M82628-38, M82628-39, M82628-40
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
185 of 211
M82628
55.3.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13463 Methods: SW846 6010B Matrix Type: SOLID Units: ug/l
Prep Date: 05/11/09
M82628-36 QCMetal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 3950 4090 3.5 0-10
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13463: M82628-20, M82628-22, M82628-23, M82628-24, M82628-25, M82628-26, M82628-27,M82628-28, M82628-29, M82628-30, M82628-31, M82628-32, M82628-33, M82628-34, M82628-35, M82628-36,M82628-37, M82628-38, M82628-39, M82628-40
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
186 of 211
M82628
55.3.4
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13464 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/12/09
MBMetal RL IDL MDL raw final
Aluminum 0.20 .0086 .031
Antimony 0.0060 .0016 .003
Arsenic 0.025 .0023 .0032
Barium 0.50 .0006 .0012
Beryllium 0.0040 .00015 .0003
Boron 0.10 .0013 .0048
Cadmium 0.0040 .00022 .0003
Calcium 5.0 .0062 .04
Chromium 0.010 .00072 .0014
Cobalt 0.050 .00054 .001
Copper 0.025 .00064 .0018
Iron 0.10 .0066 .029
Lead 0.010 .0011 .0018 0.0015 <0.010
Magnesium 5.0 .0051 .01
Manganese 0.015 .00018 .0013
Molybdenum 0.10 .00088 .0014
Nickel 0.040 .00061 .001
Potassium 5.0 .015 .031
Selenium 0.025 .0026 .0033
Silver 0.0050 .00054 .0007
Sodium 5.0 .077 .21
Strontium 0.010 .00012 .0003
Thallium 0.0050 .0029 .0045
Tin 0.10 .004 .0099
Titanium 0.050 .00059 .0051
Vanadium 0.030 .0024 .0035
Zinc 0.10 .00061 .0013
Associated samples MP13464: M82628-9A, M82628-10A, M82628-11A, M82628-12A, M82628-13A, M82628-14A,M82628-15A, M82628-16A, M82628-17A, M82628-18A, M82628-19A, M82628-20A, M82628-23A, M82628-24A, M82628-25A, M82628-26A, M82628-27A, M82628-28A
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
187 of 211
M82628
55.4.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13464 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/12/09 05/12/09
M82293-9T Spikelot QC M82293-9T QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits
Aluminum
Antimony
Arsenic anr
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium anr
Cobalt
Copper anr
Iron
Lead 0.0043 1.0 1.0 99.6 75-125 0.0043 0.0043 0.0 0-20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium anr
Zinc
Associated samples MP13464: M82628-9A, M82628-10A, M82628-11A, M82628-12A, M82628-13A, M82628-14A,M82628-15A, M82628-16A, M82628-17A, M82628-18A, M82628-19A, M82628-20A, M82628-23A, M82628-24A, M82628-25A, M82628-26A, M82628-27A, M82628-28A
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
188 of 211
M82628
55.4.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13464 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/12/09 05/12/09
BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit
Aluminum
Antimony
Arsenic anr
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium anr
Cobalt
Copper anr
Iron
Lead 0.96 1.0 96.0 80-120 1.0 1.0 100.0 4.1 20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium anr
Zinc
Associated samples MP13464: M82628-9A, M82628-10A, M82628-11A, M82628-12A, M82628-13A, M82628-14A,M82628-15A, M82628-16A, M82628-17A, M82628-18A, M82628-19A, M82628-20A, M82628-23A, M82628-24A, M82628-25A, M82628-26A, M82628-27A, M82628-28A
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
189 of 211
M82628
55.4.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13464 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date: 05/12/09
M82293-9T QCMetal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic anr
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium anr
Cobalt
Copper anr
Iron
Lead 4.28 6.94 62.1 (a) 0-10
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium anr
Zinc
Associated samples MP13464: M82628-9A, M82628-10A, M82628-11A, M82628-12A, M82628-13A, M82628-14A,M82628-15A, M82628-16A, M82628-17A, M82628-18A, M82628-19A, M82628-20A, M82628-23A, M82628-24A, M82628-25A, M82628-26A, M82628-27A, M82628-28A
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
Page 1
190 of 211
M82628
55.4.4
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13466 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg
Prep Date: 05/12/09
MBMetal RL IDL MDL raw final
Aluminum 20 .86 2.1
Antimony 2.0 .16 .41
Arsenic 2.0 .23 .29
Barium 20 .06 .26
Beryllium 0.40 .015 .022
Boron 10 .13 .31
Cadmium 0.40 .022 .024
Calcium 500 .62 .74
Chromium 1.0 .072 .14
Cobalt 5.0 .054 .079
Copper 2.5 .064 .11
Iron 10 .66 2.5
Lead 2.0 .11 .16 -0.023 <2.0
Magnesium 500 .51 .6
Manganese 1.5 .018 .031
Molybdenum 10 .088 .12
Nickel 4.0 .061 .13
Potassium 500 1.5 8.1
Selenium 2.0 .26 .34
Silver 0.50 .054 .076
Sodium 500 7.7 19
Strontium 1.0 .012 .022
Thallium 2.0 .29 .33
Tin 10 .4 .55
Titanium 5.0 .059 .5
Vanadium 3.0 .24 .26
Zinc 2.0 .061 .17
Associated samples MP13466: M82628-41, M82628-42
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
191 of 211
M82628
55.5.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13466 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg
Prep Date: 05/12/09 05/12/09
M82651-1 Spikelot QC M82651-1 QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits
Aluminum
Antimony
Arsenic anr
Barium anr
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron
Lead 23.5 116 98.4 94.0 75-125 23.5 23.8 1.3 0-20
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc anr
Associated samples MP13466: M82628-41, M82628-42
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
192 of 211
M82628
55.5.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13466 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg
Prep Date: 05/12/09 05/12/09
BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit
Aluminum
Antimony
Arsenic anr
Barium anr
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron
Lead 97.9 100 97.9 80-120 95.4 100 95.4 2.6 20
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc anr
Associated samples MP13466: M82628-41, M82628-42
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
193 of 211
M82628
55.5.3
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13466 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg
Prep Date: 05/12/09
LCS Spikelot QCMetal Result MPLCS63 % Rec Limits
Aluminum
Antimony
Arsenic anr
Barium anr
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron
Lead 209 223 93.7 82-118
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc anr
Associated samples MP13466: M82628-41, M82628-42
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
194 of 211
M82628
55.5.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13466 Methods: SW846 6010B Matrix Type: SOLID Units: ug/l
Prep Date: 05/12/09
M82651-1 QCMetal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic anr
Barium anr
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron
Lead 235 244 3.7 0-10
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc anr
Associated samples MP13466: M82628-41, M82628-42
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
195 of 211
M82628
55.5.4
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13473 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/13/09
MBMetal RL IDL MDL raw final
Aluminum 0.20 .014 .031
Antimony 0.0060 .0029 .003
Arsenic 0.025 .0027 .0032
Barium 0.50 .00064 .0012
Beryllium 0.0040 .00017 .0003
Boron 0.10 .0023 .0048
Cadmium 0.0040 .00024 .0003
Calcium 5.0 .0047 .04
Chromium 0.010 .00051 .0014
Cobalt 0.050 .00076 .001
Copper 0.025 .0011 .0018
Iron 0.10 .011 .029
Lead 0.010 .0013 .0018 -0.00018 <0.010
Magnesium 5.0 .008 .01
Manganese 0.015 .00017 .0013
Molybdenum 0.10 .0005 .0014
Nickel 0.040 .00065 .001
Potassium 5.0 .025 .031
Selenium 0.025 .0016 .0033
Silver 0.0050 .00064 .0007
Sodium 5.0 .099 .21
Strontium 0.010 .00012 .0003
Thallium 0.0050 .002 .0045
Tin 0.10 .0016 .0099
Titanium 0.050 .0041 .0051
Tungsten 0.10 .0054 .007
Vanadium 0.030 .00065 .0035
Zinc 0.10 .0011 .0013
Associated samples MP13473: M82628-9B, M82628-10B, M82628-11B, M82628-12B, M82628-13B, M82628-14B,M82628-15B, M82628-16B, M82628-17B, M82628-18B, M82628-19B, M82628-20B, M82628-21B, M82628-22B, M82628-23B, M82628-24B, M82628-25B, M82628-26B, M82628-27B, M82628-28B
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
196 of 211
M82628
55.6.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13473 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/13/09 05/13/09
M82628-21B Spikelot QC M82628-21B QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 2.8 3.5 1.0 70.0 (a) 75-125 2.8 2.8 0.0 0-20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP13473: M82628-9B, M82628-10B, M82628-11B, M82628-12B, M82628-13B, M82628-14B,M82628-15B, M82628-16B, M82628-17B, M82628-18B, M82628-19B, M82628-20B, M82628-21B, M82628-22B, M82628-23B, M82628-24B, M82628-25B, M82628-26B, M82628-27B, M82628-28B
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) Spike recovery indicates possible matrix interference.
_________________________________________________________________________________________________________
Page 1
197 of 211
M82628
55.6.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13473 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/13/09 05/13/09
BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 1.0 1.0 100.0 80-120 0.99 1.0 99.0 1.0 20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP13473: M82628-9B, M82628-10B, M82628-11B, M82628-12B, M82628-13B, M82628-14B,M82628-15B, M82628-16B, M82628-17B, M82628-18B, M82628-19B, M82628-20B, M82628-21B, M82628-22B, M82628-23B, M82628-24B, M82628-25B, M82628-26B, M82628-27B, M82628-28B
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
198 of 211
M82628
55.6.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13473 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date: 05/13/09
M82628-21B QCMetal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 2780 2770 0.4 0-10
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP13473: M82628-9B, M82628-10B, M82628-11B, M82628-12B, M82628-13B, M82628-14B,M82628-15B, M82628-16B, M82628-17B, M82628-18B, M82628-19B, M82628-20B, M82628-21B, M82628-22B, M82628-23B, M82628-24B, M82628-25B, M82628-26B, M82628-27B, M82628-28B
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
199 of 211
M82628
55.6.4
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13476 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/14/09
MBMetal RL IDL MDL raw final
Aluminum 0.20 .014 .031
Antimony 0.0060 .0029 .003
Arsenic 0.025 .0027 .0032
Barium 0.50 .00064 .0012
Beryllium 0.0040 .00017 .0003
Boron 0.10 .0023 .0048
Cadmium 0.0040 .00024 .0003
Calcium 5.0 .0047 .04
Chromium 0.010 .00051 .0014
Cobalt 0.050 .00076 .001
Copper 0.025 .0011 .0018
Iron 0.10 .011 .029
Lead 0.010 .0013 .0018 0.00011 <0.010
Magnesium 5.0 .008 .01
Manganese 0.015 .00017 .0013
Molybdenum 0.10 .0005 .0014
Nickel 0.040 .00065 .001
Potassium 5.0 .025 .031
Selenium 0.025 .0016 .0033
Silver 0.0050 .00064 .0007
Sodium 5.0 .099 .21
Strontium 0.010 .00012 .0003
Thallium 0.0050 .002 .0045
Tin 0.10 .0016 .0099
Titanium 0.050 .0041 .0051
Tungsten 0.10 .0054 .007
Vanadium 0.030 .00065 .0035
Zinc 0.10 .0011 .0013
Associated samples MP13476: M82628-29A, M82628-30A, M82628-31A, M82628-32A, M82628-33A, M82628-34A,M82628-35A, M82628-36A, M82628-37A, M82628-38A, M82628-39A, M82628-40A, M82628-41A, M82628-42A
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
200 of 211
M82628
55.7.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13476 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/14/09 05/14/09
M82628-36A Spikelot QC M82628-36A QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits
Aluminum
Antimony
Arsenic anr
Barium
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron
Lead 0.099 1.2 1.0 110.1 75-125 0.099 0.10 1.0 0-20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP13476: M82628-29A, M82628-30A, M82628-31A, M82628-32A, M82628-33A, M82628-34A,M82628-35A, M82628-36A, M82628-37A, M82628-38A, M82628-39A, M82628-40A, M82628-41A, M82628-42A
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
201 of 211
M82628
55.7.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13476 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/14/09 05/14/09
BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit
Aluminum
Antimony
Arsenic anr
Barium
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron
Lead 1.0 1.0 100.0 80-120 1.0 1.0 100.0 0.0 20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP13476: M82628-29A, M82628-30A, M82628-31A, M82628-32A, M82628-33A, M82628-34A,M82628-35A, M82628-36A, M82628-37A, M82628-38A, M82628-39A, M82628-40A, M82628-41A, M82628-42A
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
202 of 211
M82628
55.7.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13476 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date: 05/14/09
M82628-36A QCMetal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic anr
Barium
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron
Lead 99.4 98.2 1.2 0-10
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP13476: M82628-29A, M82628-30A, M82628-31A, M82628-32A, M82628-33A, M82628-34A,M82628-35A, M82628-36A, M82628-37A, M82628-38A, M82628-39A, M82628-40A, M82628-41A, M82628-42A
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
203 of 211
M82628
55.7.4
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13487 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/15/09
MBMetal RL IDL MDL raw final
Aluminum 0.20 .014 .031
Antimony 0.0060 .0029 .003
Arsenic 0.025 .0027 .0032
Barium 0.50 .00064 .0012
Beryllium 0.0040 .00017 .0003
Boron 0.10 .0023 .0048
Cadmium 0.0040 .00024 .0003
Calcium 5.0 .0047 .04
Chromium 0.010 .00051 .0014
Cobalt 0.050 .00076 .001
Copper 0.025 .0011 .0018
Iron 0.10 .011 .029
Lead 0.010 .0013 .0018 0.00038 <0.010
Magnesium 5.0 .008 .01
Manganese 0.015 .00017 .0013
Molybdenum 0.10 .0005 .0014
Nickel 0.040 .00065 .001
Potassium 5.0 .025 .031
Selenium 0.025 .0016 .0033
Silver 0.0050 .00064 .0007
Sodium 5.0 .099 .21
Strontium 0.010 .00012 .0003
Thallium 0.0050 .002 .0045
Tin 0.10 .0016 .0099
Titanium 0.050 .0041 .0051
Tungsten 0.10 .0054 .007
Vanadium 0.030 .00065 .0035
Zinc 0.10 .0011 .0013
Associated samples MP13487: M82628-41B, M82628-42B
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
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M82628
55.8.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13487 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/15/09 05/15/09
M82689-1A Spikelot QC M82689-1A QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits
Aluminum
Antimony
Arsenic anr
Barium anr
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron
Lead 0.026 1.0 1.0 97.4 75-125 0.026 0.026 0.0 0-20
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc anr
Associated samples MP13487: M82628-41B, M82628-42B
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
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M82628
55.8.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13487 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/15/09 05/15/09
BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit
Aluminum
Antimony
Arsenic anr
Barium anr
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron
Lead 1.0 1.0 100.0 80-120 1.0 1.0 100.0 0.0 20
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc anr
Associated samples MP13487: M82628-41B, M82628-42B
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
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M82628
55.8.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13487 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date: 05/15/09
M82689-1A QCMetal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic anr
Barium anr
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper anr
Iron
Lead 25.6 24.0 6.4 0-10
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc anr
Associated samples MP13487: M82628-41B, M82628-42B
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
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M82628
55.8.4
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13488 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/15/09
MBMetal RL IDL MDL raw final
Aluminum 0.20 .0086 .031
Antimony 0.0060 .0016 .003
Arsenic 0.025 .0023 .0032
Barium 0.50 .0006 .0012
Beryllium 0.0040 .00015 .0003
Boron 0.10 .0013 .0048
Cadmium 0.0040 .00022 .0003
Calcium 5.0 .0062 .04
Chromium 0.010 .00072 .0014
Cobalt 0.050 .00054 .001
Copper 0.025 .00064 .0018
Iron 0.10 .0066 .029
Lead 0.010 .0011 .0018 -0.0013 <0.010
Magnesium 5.0 .0051 .01
Manganese 0.015 .00018 .0013
Molybdenum 0.10 .00088 .0014
Nickel 0.040 .00061 .001
Potassium 5.0 .015 .031
Selenium 0.025 .0026 .0033
Silver 0.0050 .00054 .0007
Sodium 5.0 .077 .21
Strontium 0.010 .00012 .0003
Thallium 0.0050 .0029 .0045
Tin 0.10 .004 .0099
Titanium 0.050 .00059 .0051
Vanadium 0.030 .0024 .0035
Zinc 0.10 .00061 .0013
Associated samples MP13488: M82628-1B, M82628-2B, M82628-3B, M82628-4B, M82628-5B, M82628-6B, M82628-7B,M82628-8B, M82628-29B, M82628-30B, M82628-31B, M82628-32B, M82628-33B, M82628-34B, M82628-35B, M82628-36B, M82628-37B, M82628-38B, M82628-39B, M82628-40B
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
208 of 211
M82628
55.9.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13488 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/15/09 05/15/09
M82628-36B Spikelot QC M82628-36B QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 0.12 1.1 1.0 98.0 75-125 0.12 0.13 8.0 0-20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13488: M82628-1B, M82628-2B, M82628-3B, M82628-4B, M82628-5B, M82628-6B, M82628-7B,M82628-8B, M82628-29B, M82628-30B, M82628-31B, M82628-32B, M82628-33B, M82628-34B, M82628-35B, M82628-36B, M82628-37B, M82628-38B, M82628-39B, M82628-40B
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
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M82628
55.9.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13488 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 05/15/09 05/15/09
BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 1.0 1.0 100.0 80-120 1.0 1.0 100.0 0.0 20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13488: M82628-1B, M82628-2B, M82628-3B, M82628-4B, M82628-5B, M82628-6B, M82628-7B,M82628-8B, M82628-29B, M82628-30B, M82628-31B, M82628-32B, M82628-33B, M82628-34B, M82628-35B, M82628-36B, M82628-37B, M82628-38B, M82628-39B, M82628-40B
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
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M82628
55.9.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: M82628 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP13488 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date: 05/15/09
M82628-36B QCMetal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 123 121 1.7 0-10
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP13488: M82628-1B, M82628-2B, M82628-3B, M82628-4B, M82628-5B, M82628-6B, M82628-7B,M82628-8B, M82628-29B, M82628-30B, M82628-31B, M82628-32B, M82628-33B, M82628-34B, M82628-35B, M82628-36B, M82628-37B, M82628-38B, M82628-39B, M82628-40B
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
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211 of 211
M82628
55.9.4
09/24/09
Technical Report for
Olin Corporation
Mactec: Olin-Newhall St.-Hamden, CT
6107090004/01
Accutest Job Number: M85762
Sampling Dates: 09/09/09 - 09/10/09
Report to:
Mactec1090 Elm Street Suite 201Rocky Hill, CT 06067mgvannoordennen@mactec.com
ATTN: Miles VanNoordennen
Total number of pages in report:
Certifications: MA (M-MA136) CT (PH-0109) NH (2502) RI (00071) ME (MA0136) FL (E87579)
NY (11791) NJ (MA926) NC (653) IL (200018) NAVY USACE
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
New England • 495 Tech Center West • Building 1 • Marlborough, MA 01752 • tel: 508-481-6200 • fax: 508-481-7753 • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Conference
and/or state specific certification programs as applicable.
Client Service contact: Kristen Blanchard 508-481-6200
Reza TandLab Director
09/24/09
e-Hardcopy 2.0Automated Report
54
Accutest Laboratories is the sole authority for authorizing edits or modifications to thisdocument. Unauthorized modification of this report is strictly prohibited.
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M85762
Table of Contents-1-
Sections:
Section 1: Sample Summary ................................................................................................... 3Section 2: Case Narrative/Conformance Summary .............................................................. 6Section 3: Sample Results ........................................................................................................ 7
3.1: M85762-1: L900424 ..................................................................................................... 83.2: M85762-2: L900524 ..................................................................................................... 93.3: M85762-3: L900702 ..................................................................................................... 103.4: M85762-4: L900102 ..................................................................................................... 113.5: M85762-5: H901102 .................................................................................................... 123.6: M85762-6: H900324 .................................................................................................... 133.7: M85762-7: L900602 ..................................................................................................... 143.8: M85762-8: A900102 .................................................................................................... 153.9: M85762-9: A900102DUP ............................................................................................ 163.10: M85762-10: C900124 ................................................................................................. 173.11: M85762-11: F901102 ................................................................................................. 183.12: M85762-12: F901424 ................................................................................................. 193.13: M85762-13: F901302 ................................................................................................. 203.14: M85762-14: F900402 ................................................................................................. 213.15: M85762-15: S900124 ................................................................................................. 223.16: M85762-16: S900224 ................................................................................................. 233.17: M85762-17: Q900202 ................................................................................................ 243.18: M85762-18: Q900124 ................................................................................................ 253.19: M85762-19: L900224 ................................................................................................. 263.20: M85762-20: A900224 ................................................................................................ 273.21: M85762-21: T900424 ................................................................................................. 283.22: M85762-22: T900824 ................................................................................................. 293.23: M85762-23: P900302 ................................................................................................. 303.24: M85762-24: E900224 ................................................................................................. 313.25: M85762-25: E900224DUP ......................................................................................... 323.26: M85762-26: F900924 ................................................................................................. 33
Section 4: Misc. Forms ............................................................................................................ 344.1: Chain of Custody ........................................................................................................... 354.2: RCP Form ...................................................................................................................... 384.3: Sample Tracking Chronicle ........................................................................................... 39
Section 5: Metals Analysis - QC Data Summaries ................................................................ 435.1: Prep QC MP14103: Pb .................................................................................................. 445.2: Prep QC MP14108: Pb .................................................................................................. 49
12
34
5
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Accutest Laboratories
Sample Summary
Olin CorporationJob No: M85762
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
M85762-1 09/09/09 13:55 MV 09/11/09 SO Soil L900424
M85762-2 09/09/09 14:00 MV 09/11/09 SO Soil L900524
M85762-3 09/09/09 14:10 MV 09/11/09 SO Soil L900702
M85762-4 09/09/09 14:40 MV 09/11/09 SO Soil L900102
M85762-5 09/09/09 15:25 MV 09/11/09 SO Soil H901102
M85762-6 09/09/09 15:35 MV 09/11/09 SO Soil H900324
M85762-7 09/10/09 09:15 MV 09/11/09 SO Soil L900602
M85762-8 09/10/09 09:25 MV 09/11/09 SO Soil A900102
M85762-8D 09/10/09 09:25 MV 09/11/09 SO Soil Dup/MSD A900102MSD
M85762-8S 09/10/09 09:25 MV 09/11/09 SO Soil Matrix Spike A900102MS
M85762-9 09/10/09 09:25 MV 09/11/09 SO Soil A900102DUP
M85762-10 09/09/09 10:10 MV 09/11/09 SO Soil C900124
M85762-11 09/09/09 10:25 MV 09/11/09 SO Soil F901102
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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M85762
1
Accutest Laboratories
Sample Summary(continued)
Olin CorporationJob No: M85762
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
M85762-12 09/09/09 10:30 MV 09/11/09 SO Soil F901424
M85762-13 09/09/09 10:40 MV 09/11/09 SO Soil F901302
M85762-14 09/09/09 11:00 MV 09/11/09 SO Soil F900402
M85762-15 09/09/09 11:15 MV 09/11/09 SO Soil S900124
M85762-16 09/09/09 11:30 MV 09/11/09 SO Soil S900224
M85762-17 09/09/09 13:05 MV 09/11/09 SO Soil Q900202
M85762-18 09/09/09 13:15 MV 09/11/09 SO Soil Q900124
M85762-19 09/09/09 13:50 MV 09/11/09 SO Soil L900224
M85762-20 09/10/09 09:55 MV 09/11/09 SO Soil A900224
M85762-21 09/10/09 10:50 MV 09/11/09 SO Soil T900424
M85762-22 09/10/09 11:15 MV 09/11/09 SO Soil T900824
M85762-23 09/10/09 11:35 MV 09/11/09 SO Soil P900302
M85762-24 09/10/09 12:10 MV 09/11/09 SO Soil E900224
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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1
Accutest Laboratories
Sample Summary(continued)
Olin CorporationJob No: M85762
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
M85762-24D 09/10/09 12:10 MV 09/11/09 SO Soil Dup/MSD E900224MSD
M85762-24S 09/10/09 12:10 MV 09/11/09 SO Soil Matrix Spike E900224MS
M85762-25 09/10/09 12:10 MV 09/11/09 SO Soil E900224DUP
M85762-26 09/09/09 09:50 MV 09/11/09 SO Soil F900924
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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1
26 Samples were collected on between 09/09/2009 and 09/10/2009 and were received at Accutest on 09/11/2009 properly preserved,
at 2.1 Deg. C and intact. These Samples received an Accutest job number of M85762. A listing of the Laboratory Sample ID, Client
Sample ID and dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more
information, please refer to QC summary pages.
Client: Olin Corporation
Site: Mactec: Olin-Newhall St.-Hamden, CT
Job No M85762
Repor t Date 9/24/2009 11:00:11 AM
SAMPLE DELIVERY GROUP CASE NARRATIVE
Metals By Method SW846 6010B
Matr ix LEACHATE Batch ID: MP14103
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) M85762-8DUP, M85762-8LS, M85767-1MS, M85767-1SDL were used as the QC samples for metals.
RPD(s) for Serial Dilution for Lead are outside control limits for sample MP14103-SD1. Percent difference acceptable due to
low initial sample concentration (< 50 times IDL).
Only Lead requested.
Matr ix LEACHATE Batch ID: MP14108
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) M85762-24DUP, M85762-24SDL, M85762-24MS were used as the QC samples for metals.
Matrix Spike Recovery(s) for Lead are outside control limits. Spike amount low relative to the sample amount. Refer to lab
control or spike blank for recovery information.
Only Lead requested.
The Accutest Laboratories of New England certifies that all analysis were performed within method specification. It is further
recommended that this report to be used in its entirety.The Accutest Laboratories of NE, Laboratory Director or assignee as verified
by the signature on the cover page has authorized the release of this report(M85762).
Thursday, September 24, 2009 P age 1 of 1
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2
Accutest Laboratories
Sample Results
Report of Analysis
Section 3
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3
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L900424
Lab Sample ID: M85762-1 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.43 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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33.1
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L900524
Lab Sample ID: M85762-2 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead < 0.010 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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33.2
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L900702
Lab Sample ID: M85762-3 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 1.9 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L900102
Lab Sample ID: M85762-4 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 4.3 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H901102
Lab Sample ID: M85762-5 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.13 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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33.5
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H900324
Lab Sample ID: M85762-6 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.049 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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M85762
33.6
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L900602
Lab Sample ID: M85762-7 Date Sampled: 09/10/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.10 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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33.7
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: A900102
Lab Sample ID: M85762-8 Date Sampled: 09/10/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.016 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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33.8
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: A900102DUP
Lab Sample ID: M85762-9 Date Sampled: 09/10/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.011 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Report of Analysis Page 1 of 1
Client Sample ID: C900124
Lab Sample ID: M85762-10 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 1.1 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
17 of 54
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Report of Analysis Page 1 of 1
Client Sample ID: F901102
Lab Sample ID: M85762-11 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 1.2 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
18 of 54
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Report of Analysis Page 1 of 1
Client Sample ID: F901424
Lab Sample ID: M85762-12 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.36 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
19 of 54
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Report of Analysis Page 1 of 1
Client Sample ID: F901302
Lab Sample ID: M85762-13 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.70 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Report of Analysis Page 1 of 1
Client Sample ID: F900402
Lab Sample ID: M85762-14 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.23 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
21 of 54
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: S900124
Lab Sample ID: M85762-15 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead < 0.010 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Report of Analysis Page 1 of 1
Client Sample ID: S900224
Lab Sample ID: M85762-16 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.40 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: Q900202
Lab Sample ID: M85762-17 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.026 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: Q900124
Lab Sample ID: M85762-18 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.074 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14103
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
25 of 54
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L900224
Lab Sample ID: M85762-19 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 46.5 D008 5.0 0.10 mg/l 10 09/16/09 09/17/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10966
(2) Prep QC Batch: MP14108
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: A900224
Lab Sample ID: M85762-20 Date Sampled: 09/10/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 1.4 D008 5.0 0.010 mg/l 1 09/16/09 09/17/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14108
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Report of Analysis Page 1 of 1
Client Sample ID: T900424
Lab Sample ID: M85762-21 Date Sampled: 09/10/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.025 D008 5.0 0.010 mg/l 1 09/16/09 09/17/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14108
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: T900824
Lab Sample ID: M85762-22 Date Sampled: 09/10/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.017 D008 5.0 0.010 mg/l 1 09/16/09 09/17/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14108
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Report of Analysis Page 1 of 1
Client Sample ID: P900302
Lab Sample ID: M85762-23 Date Sampled: 09/10/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.15 D008 5.0 0.010 mg/l 1 09/16/09 09/17/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14108
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: E900224
Lab Sample ID: M85762-24 Date Sampled: 09/10/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 107 D008 5.0 0.20 mg/l 20 09/16/09 09/17/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10966
(2) Prep QC Batch: MP14108
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: E900224DUP
Lab Sample ID: M85762-25 Date Sampled: 09/10/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 3.6 D008 5.0 0.010 mg/l 1 09/16/09 09/17/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14108
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Report of Analysis Page 1 of 1
Client Sample ID: F900924
Lab Sample ID: M85762-26 Date Sampled: 09/09/09
Matrix: SO - Soil Date Received: 09/11/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.17 D008 5.0 0.010 mg/l 1 09/16/09 09/17/09 EAL SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA10961
(2) Prep QC Batch: MP14108
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Certification Exceptions
• Certification Exceptions (CT)
• Chain of Custody
• RCP Form
• Sample Tracking Chronicle
Section 4
34 of 54
M85762
4
M85762: Chain of CustodyPage 1 of 3
35 of 54
M85762
44.1
M85762: Chain of CustodyPage 2 of 3
36 of 54
M85762
44.1
M85762: Chain of CustodyPage 3 of 3
37 of 54
M85762
44.1
Laboratory Name: Client:
Project Location: Project Number:
Sampling Date(s):
Laboratory Sample ID(s):
Methods:
1 Yes No
1A Yes No
1B Yes No
NA
2 Yes No
3 Yes No
4 Yes No
5 Yes No
Yes No
6 Yes No
7 Yes No
Authorized
Signature: Position: Lab Director
Printed Name: Reza Tand Date:
Accutest New England
9/24/2009
Reasonable Confidence Protocol
Where all the method specified preservation and holding time requirements met?
VPH and EPH mehods only: Was the VPH or EPH method conducted without
significant modifications (See section 11.3 of respective methods)
I, the undersigned, attest under pains and penalties of perjury that, to the best of my knowledge and belief
and based upon my personal inquiry of those responsible for providing the information contained in this
analytical report, such information is accurate and complete.
Were all QA/QC performance criteria specified in the CTDEP Reasonable
Confidence Protocol documents achieved?
SW846 6010B
For each analytical method referenced in this laboratory report package, were all
specified QA/QC performance criteria followed, including the requirement to explain any
criteria falling outside of acceptable guidelines, as specified in the CTDEP method-
specific Reasonable Confidence Protocol
documents)?
Were all samples received by the laboratory in a condition consistent with
that described on the associated chain-of-custody document(s)?
Laboratory Analysis
Reza Tand
a) Were reporting limits specified or referenced on the chain-of-custody?
b) Were these reporting limits met?
For each analytical method referenced in this laboratory report package,
were results reported for all constituents identified in the method-specific
analyte lists presented in the Reasonable Confidence Protocol documents?
Are project-specific matrix spikes and laboratory duplicates included in this
data set?
Note: For all questions to which the response was "No" (with the exception of question #7), additional
information must be provided in an attached narrative. If the answer to question #1, #1A or #1B is "No" , the
data package does not meet the requirements for "Reasonable Confidence" .
QA/QC Certification Form
Accutest New England
M85762-1, M85762-2, M85762-3, M85762-4, M85762-5, M85762-6, M85762-7, M85762-
8, M85762-9, M85762-10, M85762-11, M85762-12, M85762-13, M85762-14, M85762-15,
M85762-16, M85762-17, M85762-18, M85762-19, M85762-20, M85762-21, M85762-22,
M85762-23, M85762-24, M85762-25, M85762-26, M85762-8S, M85762-24S, M85762-
8D, M85762-24D
9/9/2009
Olin Corporation
6107090004/01Mactec: Olin-Newhall St.-Hamden, CT
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M85762
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Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M85762
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M85762-1 Collected: 09-SEP-09 13:55 By: MV Received: 11-SEP-09 By: SAP
L900424
M85762-1 SW846 6010B 16-SEP-09 18:24 EAL 15-SEP-09 EAL EPB
M85762-2 Collected: 09-SEP-09 14:00 By: MV Received: 11-SEP-09 By: SAP
L900524
M85762-2 SW846 6010B 16-SEP-09 18:30 EAL 15-SEP-09 EAL EPB
M85762-3 Collected: 09-SEP-09 14:10 By: MV Received: 11-SEP-09 By: SAP
L900702
M85762-3 SW846 6010B 16-SEP-09 18:37 EAL 15-SEP-09 EAL EPB
M85762-4 Collected: 09-SEP-09 14:40 By: MV Received: 11-SEP-09 By: SAP
L900102
M85762-4 SW846 6010B 16-SEP-09 18:43 EAL 15-SEP-09 EAL EPB
M85762-5 Collected: 09-SEP-09 15:25 By: MV Received: 11-SEP-09 By: SAP
H901102
M85762-5 SW846 6010B 16-SEP-09 18:49 EAL 15-SEP-09 EAL EPB
M85762-6 Collected: 09-SEP-09 15:35 By: MV Received: 11-SEP-09 By: SAP
H900324
M85762-6 SW846 6010B 16-SEP-09 18:56 EAL 15-SEP-09 EAL EPB
M85762-7 Collected: 10-SEP-09 09:15 By: MV Received: 11-SEP-09 By: SAP
L900602
M85762-7 SW846 6010B 16-SEP-09 19:02 EAL 15-SEP-09 EAL EPB
M85762-8 Collected: 10-SEP-09 09:25 By: MV Received: 11-SEP-09 By: SAP
A900102
M85762-8 SW846 6010B 16-SEP-09 18:17 EAL 15-SEP-09 EAL EPB
Page 1 of 4
39 of 54
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44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M85762
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M85762-9 Collected: 10-SEP-09 09:25 By: MV Received: 11-SEP-09 By: SAP
A900102DUP
M85762-9 SW846 6010B 16-SEP-09 19:22 EAL 15-SEP-09 EAL EPB
M85762-10 Collected: 09-SEP-09 10:10 By: MV Received: 11-SEP-09 By: SAP
C900124
M85762-10 SW846 6010B 16-SEP-09 19:28 EAL 15-SEP-09 EAL EPB
M85762-11 Collected: 09-SEP-09 10:25 By: MV Received: 11-SEP-09 By: SAP
F901102
M85762-11 SW846 6010B 16-SEP-09 19:34 EAL 15-SEP-09 EAL EPB
M85762-12 Collected: 09-SEP-09 10:30 By: MV Received: 11-SEP-09 By: SAP
F901424
M85762-12 SW846 6010B 16-SEP-09 19:41 EAL 15-SEP-09 EAL EPB
M85762-13 Collected: 09-SEP-09 10:40 By: MV Received: 11-SEP-09 By: SAP
F901302
M85762-13 SW846 6010B 16-SEP-09 19:47 EAL 15-SEP-09 EAL EPB
M85762-14 Collected: 09-SEP-09 11:00 By: MV Received: 11-SEP-09 By: SAP
F900402
M85762-14 SW846 6010B 16-SEP-09 19:54 EAL 15-SEP-09 EAL EPB
M85762-15 Collected: 09-SEP-09 11:15 By: MV Received: 11-SEP-09 By: SAP
S900124
M85762-15 SW846 6010B 16-SEP-09 20:00 EAL 15-SEP-09 EAL EPB
M85762-16 Collected: 09-SEP-09 11:30 By: MV Received: 11-SEP-09 By: SAP
S900224
M85762-16 SW846 6010B 16-SEP-09 20:07 EAL 15-SEP-09 EAL EPB
Page 2 of 4
40 of 54
M85762
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M85762
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M85762-17 Collected: 09-SEP-09 13:05 By: MV Received: 11-SEP-09 By: SAP
Q900202
M85762-17 SW846 6010B 16-SEP-09 20:13 EAL 15-SEP-09 EAL EPB
M85762-18 Collected: 09-SEP-09 13:15 By: MV Received: 11-SEP-09 By: SAP
Q900124
M85762-18 SW846 6010B 16-SEP-09 20:19 EAL 15-SEP-09 EAL EPB
M85762-19 Collected: 09-SEP-09 13:50 By: MV Received: 11-SEP-09 By: SAP
L900224
M85762-19 SW846 6010B 17-SEP-09 20:43 PY 16-SEP-09 EAL EPB
M85762-20 Collected: 10-SEP-09 09:55 By: MV Received: 11-SEP-09 By: SAP
A900224
M85762-20 SW846 6010B 17-SEP-09 03:44 EAL 16-SEP-09 EAL EPB
M85762-21 Collected: 10-SEP-09 10:50 By: MV Received: 11-SEP-09 By: SAP
T900424
M85762-21 SW846 6010B 17-SEP-09 03:51 EAL 16-SEP-09 EAL EPB
M85762-22 Collected: 10-SEP-09 11:15 By: MV Received: 11-SEP-09 By: SAP
T900824
M85762-22 SW846 6010B 17-SEP-09 03:57 EAL 16-SEP-09 EAL EPB
M85762-23 Collected: 10-SEP-09 11:35 By: MV Received: 11-SEP-09 By: SAP
P900302
M85762-23 SW846 6010B 17-SEP-09 04:04 EAL 16-SEP-09 EAL EPB
M85762-24 Collected: 10-SEP-09 12:10 By: MV Received: 11-SEP-09 By: SAP
E900224
M85762-24 SW846 6010B 17-SEP-09 20:34 PY 16-SEP-09 EAL EPB
Page 3 of 4
41 of 54
M85762
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M85762
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M85762-25 Collected: 10-SEP-09 12:10 By: MV Received: 11-SEP-09 By: SAP
E900224DUP
M85762-25 SW846 6010B 17-SEP-09 04:10 EAL 16-SEP-09 EAL EPB
M85762-26 Collected: 09-SEP-09 09:50 By: MV Received: 11-SEP-09 By: SAP
F900924
M85762-26 SW846 6010B 17-SEP-09 04:17 EAL 16-SEP-09 EAL EPB
Page 4 of 4
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M85762
44.3
Accutest Laboratories
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Matrix Spike and Duplicate Summaries
• Blank Spike and Lab Control Sample Summaries
• Serial Dilution Summaries
Section 5
43 of 54
M85762
5
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M85762 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14103 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 09/15/09
MBMetal RL IDL MDL raw final
Aluminum 0.20 .014 .031
Antimony 0.0060 .0029 .003
Arsenic 0.025 .0027 .0032
Barium 0.50 .00064 .0012
Beryllium 0.0040 .00017 .0003
Boron 0.10 .0023 .0048
Cadmium 0.0040 .00024 .0003
Calcium 5.0 .0047 .04
Chromium 0.010 .00051 .0014
Cobalt 0.050 .00076 .001
Copper 0.025 .0011 .0018
Iron 0.10 .011 .029
Lead 0.010 .0013 .0018 0.00055 <0.010
Magnesium 5.0 .008 .01
Manganese 0.015 .00017 .0013
Molybdenum 0.10 .0005 .0014
Nickel 0.040 .00065 .001
Potassium 5.0 .025 .031
Selenium 0.025 .0016 .0033
Silver 0.0050 .00064 .0007
Sodium 5.0 .099 .21
Strontium 0.010 .00012 .0003
Thallium 0.0050 .002 .0045
Tin 0.10 .0016 .0099
Titanium 0.050 .0041 .0051
Tungsten 0.10 .0054 .007
Vanadium 0.030 .00065 .0035
Zinc 0.10 .0011 .0013
Associated samples MP14103: M85762-1, M85762-2, M85762-3, M85762-4, M85762-5, M85762-6, M85762-7, M85762-8, M85762-9, M85762-10, M85762-11, M85762-12, M85762-13, M85762-14, M85762-15, M85762-16, M85762-17,M85762-18
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
44 of 54
M85762
55.1.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M85762 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14103 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 09/15/09 09/15/09
M85767-1 Spikelot QC M85762-8 Spikelot QCMetal Original MS MPICP % Rec Limits Original LS MPICP % Rec Limits
Aluminum
Antimony
Arsenic anr
Barium anr
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead 0.0020 1.0 1.0 99.8 75-125 0.016 1.0 1.0 98.4 75-125
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14103: M85762-1, M85762-2, M85762-3, M85762-4, M85762-5, M85762-6, M85762-7, M85762-8, M85762-9, M85762-10, M85762-11, M85762-12, M85762-13, M85762-14, M85762-15, M85762-16, M85762-17,M85762-18
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
45 of 54
M85762
55.1.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M85762 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14103 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 09/15/09
M85762-8 QCMetal Original DUP RPD Limits
Aluminum
Antimony
Arsenic anr
Barium anr
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead 0.016 0.017 6.1 0-20
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14103: M85762-1, M85762-2, M85762-3, M85762-4, M85762-5, M85762-6, M85762-7, M85762-8, M85762-9, M85762-10, M85762-11, M85762-12, M85762-13, M85762-14, M85762-15, M85762-16, M85762-17,M85762-18
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
46 of 54
M85762
55.1.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M85762 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14103 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 09/15/09 09/15/09
BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit
Aluminum
Antimony
Arsenic anr
Barium anr
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead 0.99 1.0 99.0 80-120 1.0 1.0 100.0 1.0 20
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14103: M85762-1, M85762-2, M85762-3, M85762-4, M85762-5, M85762-6, M85762-7, M85762-8, M85762-9, M85762-10, M85762-11, M85762-12, M85762-13, M85762-14, M85762-15, M85762-16, M85762-17,M85762-18
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
47 of 54
M85762
55.1.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: M85762 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14103 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date: 09/15/09
M85767-1 QCMetal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic anr
Barium anr
Beryllium
Boron
Cadmium anr
Calcium
Chromium anr
Cobalt
Copper
Iron
Lead 1.98 0.00 100.0(a) 0-10
Magnesium
Manganese
Molybdenum
Nickel anr
Potassium
Selenium anr
Silver anr
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14103: M85762-1, M85762-2, M85762-3, M85762-4, M85762-5, M85762-6, M85762-7, M85762-8, M85762-9, M85762-10, M85762-11, M85762-12, M85762-13, M85762-14, M85762-15, M85762-16, M85762-17,M85762-18
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
Page 1
48 of 54
M85762
55.1.4
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M85762 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14108 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 09/16/09
MBMetal RL IDL MDL raw final
Aluminum 0.20 .014 .031
Antimony 0.0060 .0029 .003
Arsenic 0.025 .0027 .0032
Barium 0.50 .00064 .0012
Beryllium 0.0040 .00017 .0003
Boron 0.10 .0023 .0048
Cadmium 0.0040 .00024 .0003
Calcium 5.0 .0047 .04
Chromium 0.010 .00051 .0014
Cobalt 0.050 .00076 .001
Copper 0.025 .0011 .0018
Iron 0.10 .011 .029
Lead 0.010 .0013 .0018 0.0020 <0.010
Magnesium 5.0 .008 .01
Manganese 0.015 .00017 .0013
Molybdenum 0.10 .0005 .0014
Nickel 0.040 .00065 .001
Potassium 5.0 .025 .031
Selenium 0.025 .0016 .0033
Silver 0.0050 .00064 .0007
Sodium 5.0 .099 .21
Strontium 0.010 .00012 .0003
Thallium 0.0050 .002 .0045
Tin 0.10 .0016 .0099
Titanium 0.050 .0041 .0051
Tungsten 0.10 .0054 .007
Vanadium 0.030 .00065 .0035
Zinc 0.10 .0011 .0013
Associated samples MP14108: M85762-19, M85762-20, M85762-21, M85762-22, M85762-23, M85762-24, M85762-25,M85762-26
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
49 of 54
M85762
55.2.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M85762 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14108 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 09/16/09 09/16/09
M85762-24 Spikelot QC M85762-24 QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Gold
Iron
Lead 107 103 1.00 -400.0(a 75-125 107 106 0.9 0-20
Magnesium
Manganese
Molybdenum
Nickel
Palladium
Platinum
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14108: M85762-19, M85762-20, M85762-21, M85762-22, M85762-23, M85762-24, M85762-25,M85762-26_________________________________________________________________________________________________________
Page 1
50 of 54
M85762
55.2.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M85762 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14108 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date:
Metal
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) Spike amount low relative to the sample amount. Refer to lab control or spike blank for recovery
information.
_________________________________________________________________________________________________________
Page 2
51 of 54
M85762
55.2.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M85762 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14108 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 09/16/09 09/16/09
BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead 1.0 1.0 100.0 80-120 1.0 1.0 100.0 0.0 20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14108: M85762-19, M85762-20, M85762-21, M85762-22, M85762-23, M85762-24, M85762-25,M85762-26
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
52 of 54
M85762
55.2.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: M85762 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14108 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date: 09/16/09
M85762-24 QCMetal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Gold
Iron
Lead 107000 106000 0.5 0-10
Magnesium
Manganese
Molybdenum
Nickel
Palladium
Platinum
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14108: M85762-19, M85762-20, M85762-21, M85762-22, M85762-23, M85762-24, M85762-25,M85762-26_________________________________________________________________________________________________________
Page 1
53 of 54
M85762
55.2.4
SERIAL DILUTION RESULTS SUMMARY
Login Number: M85762 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14108 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date:
Metal
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
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M85762
55.2.4
10/30/09
Technical Report for
Olin Corporation
Mactec: Olin-Newhall St.-Hamden, CT
6107090004/01
Accutest Job Number: M86571
Sampling Dates: 10/14/09 - 10/15/09
Report to:
Mactec1090 Elm Street Suite 201Rocky Hill, CT 06067mgvannoordennen@mactec.com
ATTN: Miles VanNoordennen
Total number of pages in report:
Certifications: MA (M-MA136) CT (PH-0109) NH (2502) RI (00071) ME (MA0136) FL (E87579)
NY (11791) NJ (MA926) NC (653) IL (200018) NAVY USACE
This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.
Test results relate only to samples analyzed.
New England • 495 Tech Center West • Building 1 • Marlborough, MA 01752 • tel: 508-481-6200 • fax: 508-481-7753 • http://www.accutest.com
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Conference
and/or state specific certification programs as applicable.
Client Service contact: Kristen Blanchard 508-481-6200
Reza TandLab Director
10/30/09
e-Hardcopy 2.0Automated Report
96
Accutest Laboratories is the sole authority for authorizing edits or modifications to thisdocument. Unauthorized modification of this report is strictly prohibited.
1 of 96
M86571
Table of Contents-1-
Sections:
Section 1: Sample Summary ................................................................................................... 4Section 2: Case Narrative/Conformance Summary .............................................................. 8Section 3: Sample Results ........................................................................................................ 9
3.1: M86571-1: H900424 .................................................................................................... 103.2: M86571-2: H900902 .................................................................................................... 113.3: M86571-3: H900524 .................................................................................................... 123.4: M86571-4: H900602 .................................................................................................... 133.5: M86571-5: H900702 .................................................................................................... 143.6: M86571-6: H900802 .................................................................................................... 153.7: M86571-7: H900224 .................................................................................................... 163.8: M86571-8: J900424 ...................................................................................................... 173.9: M86571-9: H901024 .................................................................................................... 183.10: M86571-10: H900124 ................................................................................................ 193.11: M86571-11: J900102 .................................................................................................. 203.12: M86571-12: J900102DUP .......................................................................................... 213.13: M86571-13: J900302 .................................................................................................. 223.14: M86571-14: J900224 .................................................................................................. 233.15: M86571-15: L900324 ................................................................................................. 243.16: M86571-16: N900124 ................................................................................................ 253.17: M86571-17: F900602 ................................................................................................. 263.18: M86571-18: C900324 ................................................................................................. 273.19: M86571-19: C900424 ................................................................................................. 283.20: M86571-20: C900502 ................................................................................................. 293.21: M86571-21: K900102 ................................................................................................ 303.22: M86571-22: K900102DUP ........................................................................................ 313.23: M86571-23: K900202 ................................................................................................ 323.24: M86571-24: P900124 ................................................................................................. 333.25: M86571-25: P900202 ................................................................................................. 343.26: M86571-26: P900402 ................................................................................................. 353.27: M86571-27: E900424 ................................................................................................. 363.28: M86571-28: E900502 ................................................................................................. 373.29: M86571-29: F901224 ................................................................................................. 383.30: M86571-30: F900224 ................................................................................................. 393.31: M86571-31: F901524 ................................................................................................. 403.32: M86571-32: F900524 ................................................................................................. 413.33: M86571-33: E900124 ................................................................................................. 423.34: M86571-34: E900324 ................................................................................................. 433.35: M86571-35: C900224 ................................................................................................. 443.36: M86571-36: F901002 ................................................................................................. 453.37: M86571-37: F900324 ................................................................................................. 463.38: M86571-38: F900824 ................................................................................................. 473.39: M86571-39: F901602 ................................................................................................. 48
12
34
5
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M86571
Table of Contents-2-
Sections:
3.40: M86571-40: F900724 ................................................................................................. 493.41: M86571-41: F900102 ................................................................................................. 503.42: M86571-42: R900102 ................................................................................................. 513.43: M86571-43: T900202 ................................................................................................. 523.44: M86571-44: T900102 ................................................................................................. 533.45: M86571-45: T900324 ................................................................................................. 543.46: M86571-46: T900524 ................................................................................................. 553.47: M86571-47: T900702 ................................................................................................. 563.48: M86571-48: T900602 ................................................................................................. 57
Section 4: Misc. Forms ............................................................................................................ 584.1: Chain of Custody ........................................................................................................... 594.2: RCP Form ...................................................................................................................... 654.3: Sample Tracking Chronicle ........................................................................................... 66
Section 5: Metals Analysis - QC Data Summaries ................................................................ 725.1: Prep QC MP14283: Pb .................................................................................................. 735.2: Prep QC MP14291: Pb .................................................................................................. 815.3: Prep QC MP14323: Pb .................................................................................................. 89
12
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5
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Accutest Laboratories
Sample Summary
Olin CorporationJob No: M86571
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
M86571-1 10/14/09 11:00 MV 10/16/09 SO Soil H900424
M86571-2 10/14/09 11:15 MV 10/16/09 SO Soil H900902
M86571-3 10/14/09 11:30 MV 10/16/09 SO Soil H900524
M86571-4 10/14/09 11:40 MV 10/16/09 SO Soil H900602
M86571-5 10/14/09 11:50 MV 10/16/09 SO Soil H900702
M86571-6 10/14/09 12:10 MV 10/16/09 SO Soil H900802
M86571-7 10/14/09 12:30 MV 10/16/09 SO Soil H900224
M86571-8 10/14/09 12:45 MV 10/16/09 SO Soil J900424
M86571-9 10/14/09 12:55 MV 10/16/09 SO Soil H901024
M86571-10 10/14/09 13:05 MV 10/16/09 SO Soil H900124
M86571-11 10/14/09 14:30 MV 10/16/09 SO Soil J900102
M86571-11D 10/14/09 14:30 MV 10/16/09 SO Soil Dup/MSD J900102 MSD
M86571-11S 10/14/09 14:30 MV 10/16/09 SO Soil Matrix Spike J900102 MS
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Sample Summary(continued)
Olin CorporationJob No: M86571
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
M86571-12 10/14/09 14:30 MV 10/16/09 SO Soil J900102DUP
M86571-13 10/14/09 14:45 MV 10/16/09 SO Soil J900302
M86571-14 10/14/09 14:50 MV 10/16/09 SO Soil J900224
M86571-15 10/14/09 15:10 MV 10/16/09 SO Soil L900324
M86571-16 10/14/09 15:45 MV 10/16/09 SO Soil N900124
M86571-17 10/14/09 16:00 MV 10/16/09 SO Soil F900602
M86571-18 10/14/09 16:15 MV 10/16/09 SO Soil C900324
M86571-19 10/14/09 16:20 MV 10/16/09 SO Soil C900424
M86571-20 10/14/09 16:40 MV 10/16/09 SO Soil C900502
M86571-21 10/15/09 09:20 MV 10/16/09 SO Soil K900102
M86571-21D 10/15/09 09:20 MV 10/16/09 SO Soil Dup/MSD K900102 MSD
M86571-21S 10/15/09 09:20 MV 10/16/09 SO Soil Matrix Spike K900102 MS
M86571-22 10/15/09 09:20 MV 10/16/09 SO Soil K900102DUP
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Accutest Laboratories
Sample Summary(continued)
Olin CorporationJob No: M86571
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
M86571-23 10/15/09 09:40 MV 10/16/09 SO Soil K900202
M86571-24 10/15/09 09:50 MV 10/16/09 SO Soil P900124
M86571-25 10/15/09 10:00 MV 10/16/09 SO Soil P900202
M86571-26 10/15/09 10:10 MV 10/16/09 SO Soil P900402
M86571-27 10/15/09 10:20 MV 10/16/09 SO Soil E900424
M86571-28 10/15/09 10:30 MV 10/16/09 SO Soil E900502
M86571-29 10/15/09 10:40 MV 10/16/09 SO Soil F901224
M86571-30 10/15/09 10:50 MV 10/16/09 SO Soil F900224
M86571-31 10/15/09 11:00 MV 10/16/09 SO Soil F901524
M86571-32 10/15/09 11:10 MV 10/16/09 SO Soil F900524
M86571-33 10/15/09 12:15 MV 10/16/09 SO Soil E900124
M86571-34 10/15/09 12:25 MV 10/16/09 SO Soil E900324
M86571-35 10/15/09 12:35 MV 10/16/09 SO Soil C900224
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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Accutest Laboratories
Sample Summary(continued)
Olin CorporationJob No: M86571
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
M86571-36 10/15/09 12:45 MV 10/16/09 SO Soil F901002
M86571-37 10/15/09 12:55 MV 10/16/09 SO Soil F900324
M86571-38 10/15/09 13:00 MV 10/16/09 SO Soil F900824
M86571-39 10/15/09 13:10 MV 10/16/09 SO Soil F901602
M86571-40 10/15/09 13:15 MV 10/16/09 SO Soil F900724
M86571-41 10/15/09 13:20 MV 10/16/09 SO Soil F900102
M86571-42 10/15/09 13:30 MV 10/16/09 SO Soil R900102
M86571-43 10/15/09 13:40 MV 10/16/09 SO Soil T900202
M86571-44 10/15/09 13:55 MV 10/16/09 SO Soil T900102
M86571-45 10/15/09 14:00 MV 10/16/09 SO Soil T900324
M86571-46 10/15/09 14:40 MV 10/16/09 SO Soil T900524
M86571-47 10/15/09 14:50 MV 10/16/09 SO Soil T900702
M86571-48 10/15/09 15:00 MV 10/16/09 SO Soil T900602
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
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1
48 Sample(s) were collected on between 10/14/2009 and 10/15/2009 and were received at Accutest on 10/16/2009 properly preserved,
at 1.8 Deg. C and intact. These Samples received an Accutest job number of M86571. A listing of the Laboratory Sample ID, Client
Sample ID and dates of collection are presented in the Results Summary Section of this report.
Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more
information, please refer to QC summary pages.
Client: Olin Corporation
Site: Mactec: Olin-Newhall St.-Hamden, CT
Job No M86571
Repor t Date 10/30/2009 12:52:00 PM
SAMPLE DELIVERY GROUP CASE NARRATIVE
Metals By Method SW846 6010B
Matr ix LEACHATE Batch ID: MP14283
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) M86571-11DUP, M86571-11MS, M86571-11SDL were used as the QC samples for metals.
Only Lead requested.
Matr ix LEACHATE Batch ID: MP14291
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) M86571-21DUP, M86571-21MS, M86571-21SDL were used as the QC samples for metals.
Only Lead requested.
Matr ix LEACHATE Batch ID: MP14323
All samples were digested within the recommended method holding time.
All samples were analyzed within the recommended method holding time.
All method blanks for this batch meet method specific criteria.
Sample(s) M86571-41DUP, M86571-41MS, M86571-41SDL were used as the QC samples for metals.
Only Lead requested.
The Accutest Laboratories of New England certifies that all analysis were performed within method specification. It is further
recommended that this report to be used in its entirety.The Accutest Laboratories of NE, Laboratory Director or assignee as verified
by the signature on the cover page has authorized the release of this report(M86571).
F riday, October 30, 2009 P age 1 of 1
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Sample Results
Report of Analysis
Section 3
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3
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Report of Analysis Page 1 of 1
Client Sample ID: H900424
Lab Sample ID: M86571-1 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.021 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
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33.1
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H900902
Lab Sample ID: M86571-2 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.063 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
11 of 96
M86571
33.2
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H900524
Lab Sample ID: M86571-3 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead < 0.010 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
12 of 96
M86571
33.3
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H900602
Lab Sample ID: M86571-4 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.057 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
13 of 96
M86571
33.4
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H900702
Lab Sample ID: M86571-5 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.068 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
14 of 96
M86571
33.5
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H900802
Lab Sample ID: M86571-6 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.18 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
15 of 96
M86571
33.6
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H900224
Lab Sample ID: M86571-7 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.16 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
16 of 96
M86571
33.7
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: J900424
Lab Sample ID: M86571-8 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.27 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
17 of 96
M86571
33.8
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H901024
Lab Sample ID: M86571-9 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead < 0.010 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
18 of 96
M86571
33.9
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: H900124
Lab Sample ID: M86571-10 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.088 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
19 of 96
M86571
33.10
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: J900102
Lab Sample ID: M86571-11 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.39 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
20 of 96
M86571
33.11
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: J900102DUP
Lab Sample ID: M86571-12 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.57 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
21 of 96
M86571
33.12
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: J900302
Lab Sample ID: M86571-13 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.17 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
22 of 96
M86571
33.13
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: J900224
Lab Sample ID: M86571-14 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.12 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
23 of 96
M86571
33.14
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: L900324
Lab Sample ID: M86571-15 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.036 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
24 of 96
M86571
33.15
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: N900124
Lab Sample ID: M86571-16 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.061 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
25 of 96
M86571
33.16
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F900602
Lab Sample ID: M86571-17 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.26 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
26 of 96
M86571
33.17
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C900324
Lab Sample ID: M86571-18 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.16 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
27 of 96
M86571
33.18
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C900424
Lab Sample ID: M86571-19 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.81 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
28 of 96
M86571
33.19
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C900502
Lab Sample ID: M86571-20 Date Sampled: 10/14/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.20 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11097
(2) Prep QC Batch: MP14283
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
29 of 96
M86571
33.20
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: K900102
Lab Sample ID: M86571-21 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.10 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
30 of 96
M86571
33.21
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: K900102DUP
Lab Sample ID: M86571-22 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.16 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
31 of 96
M86571
33.22
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: K900202
Lab Sample ID: M86571-23 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.075 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
32 of 96
M86571
33.23
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: P900124
Lab Sample ID: M86571-24 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.82 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
33 of 96
M86571
33.24
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: P900202
Lab Sample ID: M86571-25 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.073 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
34 of 96
M86571
33.25
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: P900402
Lab Sample ID: M86571-26 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.45 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
35 of 96
M86571
33.26
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: E900424
Lab Sample ID: M86571-27 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.30 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
36 of 96
M86571
33.27
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: E900502
Lab Sample ID: M86571-28 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.027 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
37 of 96
M86571
33.28
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F901224
Lab Sample ID: M86571-29 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.033 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
38 of 96
M86571
33.29
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F900224
Lab Sample ID: M86571-30 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.94 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
39 of 96
M86571
33.30
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F901524
Lab Sample ID: M86571-31 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 7.4 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
40 of 96
M86571
33.31
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F900524
Lab Sample ID: M86571-32 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.24 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
41 of 96
M86571
33.32
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: E900124
Lab Sample ID: M86571-33 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 2.7 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
42 of 96
M86571
33.33
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: E900324
Lab Sample ID: M86571-34 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.015 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
43 of 96
M86571
33.34
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: C900224
Lab Sample ID: M86571-35 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 20.4 D008 5.0 0.050 mg/l 5 10/22/09 10/23/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11102
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
44 of 96
M86571
33.35
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F901002
Lab Sample ID: M86571-36 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.37 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
45 of 96
M86571
33.36
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F900324
Lab Sample ID: M86571-37 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.058 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
46 of 96
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Report of Analysis Page 1 of 1
Client Sample ID: F900824
Lab Sample ID: M86571-38 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.069 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
47 of 96
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Report of Analysis Page 1 of 1
Client Sample ID: F901602
Lab Sample ID: M86571-39 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.055 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
48 of 96
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Report of Analysis Page 1 of 1
Client Sample ID: F900724
Lab Sample ID: M86571-40 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.62 D008 5.0 0.010 mg/l 1 10/22/09 10/22/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11101
(2) Prep QC Batch: MP14291
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
49 of 96
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: F900102
Lab Sample ID: M86571-41 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 1.0 D008 5.0 0.010 mg/l 1 10/28/09 10/29/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11120
(2) Prep QC Batch: MP14323
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
50 of 96
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: R900102
Lab Sample ID: M86571-42 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.065 D008 5.0 0.010 mg/l 1 10/28/09 10/29/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11120
(2) Prep QC Batch: MP14323
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
51 of 96
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Report of Analysis Page 1 of 1
Client Sample ID: T900202
Lab Sample ID: M86571-43 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.13 D008 5.0 0.010 mg/l 1 10/28/09 10/29/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11120
(2) Prep QC Batch: MP14323
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
52 of 96
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: T900102
Lab Sample ID: M86571-44 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.017 D008 5.0 0.010 mg/l 1 10/28/09 10/29/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11120
(2) Prep QC Batch: MP14323
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
53 of 96
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: T900324
Lab Sample ID: M86571-45 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.069 D008 5.0 0.010 mg/l 1 10/28/09 10/29/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11120
(2) Prep QC Batch: MP14323
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
54 of 96
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: T900524
Lab Sample ID: M86571-46 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead < 0.010 D008 5.0 0.010 mg/l 1 10/28/09 10/29/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11120
(2) Prep QC Batch: MP14323
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
55 of 96
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Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: T900702
Lab Sample ID: M86571-47 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.20 D008 5.0 0.010 mg/l 1 10/28/09 10/29/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11120
(2) Prep QC Batch: MP14323
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
56 of 96
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33.47
Accutest Laboratories
Report of Analysis Page 1 of 1
Client Sample ID: T900602
Lab Sample ID: M86571-48 Date Sampled: 10/15/09
Matrix: SO - Soil Date Received: 10/16/09
Percent Solids: n/a
Project: Mactec: Olin-Newhall St.-Hamden, CT
Metals Analysis, TCLP Leachate SW846 1311
Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method
Lead 0.014 D008 5.0 0.010 mg/l 1 10/28/09 10/29/09 PY SW846 6010B 1 SW846 3010A 2
(1) Instrument QC Batch: MA11120
(2) Prep QC Batch: MP14323
RL = Reporting Limit
MCL = Maximum Contamination Level (40 CFR 261 6/96)
57 of 96
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33.48
Accutest Laboratories
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Certification Exceptions
• Certification Exceptions (CT)
• Chain of Custody
• RCP Form
• Sample Tracking Chronicle
Section 4
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4
M86571: Chain of CustodyPage 1 of 6
59 of 96
M86571
44.1
M86571: Chain of CustodyPage 2 of 6
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44.1
M86571: Chain of CustodyPage 3 of 6
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44.1
M86571: Chain of CustodyPage 4 of 6
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M86571: Chain of CustodyPage 5 of 6
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M86571: Chain of CustodyPage 6 of 6
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44.1
Laboratory Name: Client:
Project Location: Project Number:
Sampling Date(s):
Laboratory Sample ID(s):
Methods:
1 Yes No
1A Yes No
1B Yes No
NA
2 Yes No
3 Yes No
4 Yes No
5 Yes No
Yes No
6 Yes No
7 Yes No
Authorized
Signature: Position: Lab Director
Printed Name: Reza Tand Date:
Accutest New England
10/14/2009
Olin Corporation
6107090004/01Mactec: Olin-Newhall St.-Hamden, CT
Laboratory Analysis
Reza Tand
a) Were reporting limits specified or referenced on the chain-of-custody?
b) Were these reporting limits met?
For each analytical method referenced in this laboratory report package,
were results reported for all constituents identified in the method-specific
analyte lists presented in the Reasonable Confidence Protocol documents?
Are project-specific matrix spikes and laboratory duplicates included in this
data set?
Note: For all questions to which the response was "No" (with the exception of question #7), additional
information must be provided in an attached narrative. If the answer to question #1, #1A or #1B is "No" , the
data package does not meet the requirements for "Reasonable Confidence" .
QA/QC Certification Form
Accutest New England
M86571-1, M86571-2, M86571-3, M86571-4, M86571-5, M86571-6, M86571-7, M86571-
8, M86571-9, M86571-10, M86571-11, M86571-12, M86571-13, M86571-14, M86571-15,
M86571-16, M86571-17, M86571-18, M86571-19, M86571-20, M86571-21, M86571-22,
M86571-23, M86571-24, M86571-25, M86571-26, M86571-27, M86571-28, M86571-29,
M86571-30, M86571-31, M86571-32, M86571-33, M86571-34, M86571-35, M86571-36,
M86571-37, M86571-38, M86571-39, M86571-40, M86571-41, M86571-42, M86571-43,
M86571-44, M86571-45, M86571-46, M86571-47, M86571-48, M86571-11S, M86571-
21S, M86571-11D, M86571-21D
10/30/2009
Reasonable Confidence Protocol
Where all the method specified preservation and holding time requirements met?
VPH and EPH mehods only: Was the VPH or EPH method conducted without
significant modifications (See section 11.3 of respective methods)
I, the undersigned, attest under pains and penalties of perjury that, to the best of my knowledge and belief
and based upon my personal inquiry of those responsible for providing the information contained in this
analytical report, such information is accurate and complete.
Were all QA/QC performance criteria specified in the CTDEP Reasonable
Confidence Protocol documents achieved?
EPA 160.3 M, SW846 6010B
For each analytical method referenced in this laboratory report package, were all
specified QA/QC performance criteria followed, including the requirement to explain any
criteria falling outside of acceptable guidelines, as specified in the CTDEP method-
specific Reasonable Confidence Protocol
documents)?
Were all samples received by the laboratory in a condition consistent with
that described on the associated chain-of-custody document(s)?
65 of 96
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44.2
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M86571
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M86571-1 Collected: 14-OCT-09 11:00 By: MV Received: 16-OCT-09 By: JB
H900424
M86571-1 SW846 6010B 21-OCT-09 21:05 PY 21-OCT-09 EAL EPB
M86571-2 Collected: 14-OCT-09 11:15 By: MV Received: 16-OCT-09 By: JB
H900902
M86571-2 SW846 6010B 21-OCT-09 21:18 PY 21-OCT-09 EAL EPB
M86571-3 Collected: 14-OCT-09 11:30 By: MV Received: 16-OCT-09 By: JB
H900524
M86571-3 SW846 6010B 21-OCT-09 21:22 PY 21-OCT-09 EAL EPB
M86571-4 Collected: 14-OCT-09 11:40 By: MV Received: 16-OCT-09 By: JB
H900602
M86571-4 SW846 6010B 21-OCT-09 21:27 PY 21-OCT-09 EAL EPB
M86571-5 Collected: 14-OCT-09 11:50 By: MV Received: 16-OCT-09 By: JB
H900702
M86571-5 SW846 6010B 21-OCT-09 21:31 PY 21-OCT-09 EAL EPB
M86571-6 Collected: 14-OCT-09 12:10 By: MV Received: 16-OCT-09 By: JB
H900802
M86571-6 SW846 6010B 21-OCT-09 21:36 PY 21-OCT-09 EAL EPB
M86571-7 Collected: 14-OCT-09 12:30 By: MV Received: 16-OCT-09 By: JB
H900224
M86571-7 SW846 6010B 21-OCT-09 21:40 PY 21-OCT-09 EAL EPB
M86571-8 Collected: 14-OCT-09 12:45 By: MV Received: 16-OCT-09 By: JB
J900424
M86571-8 SW846 6010B 21-OCT-09 21:45 PY 21-OCT-09 EAL EPB
Page 1 of 6
66 of 96
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44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M86571
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M86571-9 Collected: 14-OCT-09 12:55 By: MV Received: 16-OCT-09 By: JB
H901024
M86571-9 SW846 6010B 21-OCT-09 21:49 PY 21-OCT-09 EAL EPB
M86571-10 Collected: 14-OCT-09 13:05 By: MV Received: 16-OCT-09 By: JB
H900124
M86571-10 SW846 6010B 21-OCT-09 21:54 PY 21-OCT-09 EAL EPB
M86571-11 Collected: 14-OCT-09 14:30 By: MV Received: 16-OCT-09 By: JB
J900102
M86571-11 SW846 6010B 21-OCT-09 20:47 PY 21-OCT-09 EAL EPB
M86571-12 Collected: 14-OCT-09 14:30 By: MV Received: 16-OCT-09 By: JB
J900102DUP
M86571-12 SW846 6010B 21-OCT-09 21:58 PY 21-OCT-09 EAL EPB
M86571-13 Collected: 14-OCT-09 14:45 By: MV Received: 16-OCT-09 By: JB
J900302
M86571-13 SW846 6010B 21-OCT-09 22:11 PY 21-OCT-09 EAL EPB
M86571-14 Collected: 14-OCT-09 14:50 By: MV Received: 16-OCT-09 By: JB
J900224
M86571-14 SW846 6010B 21-OCT-09 22:16 PY 21-OCT-09 EAL EPB
M86571-15 Collected: 14-OCT-09 15:10 By: MV Received: 16-OCT-09 By: JB
L900324
M86571-15 SW846 6010B 21-OCT-09 22:20 PY 21-OCT-09 EAL EPB
M86571-16 Collected: 14-OCT-09 15:45 By: MV Received: 16-OCT-09 By: JB
N900124
M86571-16 SW846 6010B 21-OCT-09 22:24 PY 21-OCT-09 EAL EPB
Page 2 of 6
67 of 96
M86571
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M86571
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M86571-17 Collected: 14-OCT-09 16:00 By: MV Received: 16-OCT-09 By: JB
F900602
M86571-17 SW846 6010B 21-OCT-09 22:29 PY 21-OCT-09 EAL EPB
M86571-18 Collected: 14-OCT-09 16:15 By: MV Received: 16-OCT-09 By: JB
C900324
M86571-18 SW846 6010B 21-OCT-09 22:33 PY 21-OCT-09 EAL EPB
M86571-19 Collected: 14-OCT-09 16:20 By: MV Received: 16-OCT-09 By: JB
C900424
M86571-19 SW846 6010B 21-OCT-09 22:38 PY 21-OCT-09 EAL EPB
M86571-20 Collected: 14-OCT-09 16:40 By: MV Received: 16-OCT-09 By: JB
C900502
M86571-20 SW846 6010B 21-OCT-09 22:42 PY 21-OCT-09 EAL EPB
M86571-21 Collected: 15-OCT-09 09:20 By: MV Received: 16-OCT-09 By: JB
K900102
M86571-21 SW846 6010B 22-OCT-09 21:42 PY 22-OCT-09 EAL EPB
M86571-22 Collected: 15-OCT-09 09:20 By: MV Received: 16-OCT-09 By: JB
K900102DUP
M86571-22 SW846 6010B 22-OCT-09 22:08 PY 22-OCT-09 EAL EPB
M86571-23 Collected: 15-OCT-09 09:40 By: MV Received: 16-OCT-09 By: JB
K900202
M86571-23 SW846 6010B 22-OCT-09 22:12 PY 22-OCT-09 EAL EPB
M86571-24 Collected: 15-OCT-09 09:50 By: MV Received: 16-OCT-09 By: JB
P900124
M86571-24 SW846 6010B 22-OCT-09 22:17 PY 22-OCT-09 EAL EPB
Page 3 of 6
68 of 96
M86571
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M86571
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M86571-25 Collected: 15-OCT-09 10:00 By: MV Received: 16-OCT-09 By: JB
P900202
M86571-25 SW846 6010B 22-OCT-09 22:21 PY 22-OCT-09 EAL EPB
M86571-26 Collected: 15-OCT-09 10:10 By: MV Received: 16-OCT-09 By: JB
P900402
M86571-26 SW846 6010B 22-OCT-09 22:26 PY 22-OCT-09 EAL EPB
M86571-27 Collected: 15-OCT-09 10:20 By: MV Received: 16-OCT-09 By: JB
E900424
M86571-27 SW846 6010B 22-OCT-09 22:30 PY 22-OCT-09 EAL EPB
M86571-28 Collected: 15-OCT-09 10:30 By: MV Received: 16-OCT-09 By: JB
E900502
M86571-28 SW846 6010B 22-OCT-09 22:35 PY 22-OCT-09 EAL EPB
M86571-29 Collected: 15-OCT-09 10:40 By: MV Received: 16-OCT-09 By: JB
F901224
M86571-29 SW846 6010B 22-OCT-09 22:39 PY 22-OCT-09 EAL EPB
M86571-30 Collected: 15-OCT-09 10:50 By: MV Received: 16-OCT-09 By: JB
F900224
M86571-30 SW846 6010B 22-OCT-09 22:44 PY 22-OCT-09 EAL EPB
M86571-31 Collected: 15-OCT-09 11:00 By: MV Received: 16-OCT-09 By: JB
F901524
M86571-31 SW846 6010B 22-OCT-09 22:48 PY 22-OCT-09 EAL EPB
M86571-32 Collected: 15-OCT-09 11:10 By: MV Received: 16-OCT-09 By: JB
F900524
M86571-32 SW846 6010B 22-OCT-09 23:02 PY 22-OCT-09 EAL EPB
Page 4 of 6
69 of 96
M86571
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M86571
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M86571-33 Collected: 15-OCT-09 12:15 By: MV Received: 16-OCT-09 By: JB
E900124
M86571-33 SW846 6010B 22-OCT-09 23:06 PY 22-OCT-09 EAL EPB
M86571-34 Collected: 15-OCT-09 12:25 By: MV Received: 16-OCT-09 By: JB
E900324
M86571-34 SW846 6010B 22-OCT-09 23:11 PY 22-OCT-09 EAL EPB
M86571-35 Collected: 15-OCT-09 12:35 By: MV Received: 16-OCT-09 By: JB
C900224
M86571-35 SW846 6010B 23-OCT-09 14:07 PY 22-OCT-09 EAL EPB
M86571-36 Collected: 15-OCT-09 12:45 By: MV Received: 16-OCT-09 By: JB
F901002
M86571-36 SW846 6010B 22-OCT-09 23:20 PY 22-OCT-09 EAL EPB
M86571-37 Collected: 15-OCT-09 12:55 By: MV Received: 16-OCT-09 By: JB
F900324
M86571-37 SW846 6010B 22-OCT-09 23:24 PY 22-OCT-09 EAL EPB
M86571-38 Collected: 15-OCT-09 13:00 By: MV Received: 16-OCT-09 By: JB
F900824
M86571-38 SW846 6010B 22-OCT-09 23:28 PY 22-OCT-09 EAL EPB
M86571-39 Collected: 15-OCT-09 13:10 By: MV Received: 16-OCT-09 By: JB
F901602
M86571-39 SW846 6010B 22-OCT-09 23:33 PY 22-OCT-09 EAL EPB
M86571-40 Collected: 15-OCT-09 13:15 By: MV Received: 16-OCT-09 By: JB
F900724
M86571-40 SW846 6010B 22-OCT-09 23:37 PY 22-OCT-09 EAL EPB
Page 5 of 6
70 of 96
M86571
44.3
Accutest Laboratories
Internal Sample Tracking Chronicle
Olin CorporationJob No: M86571
Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01
Sample
Number Method Analyzed By Prepped By Test Codes
M86571-41 Collected: 15-OCT-09 13:20 By: MV Received: 16-OCT-09 By: JB
F900102
M86571-41 SW846 6010B 29-OCT-09 13:23 PY 28-OCT-09 EAL EPB
M86571-42 Collected: 15-OCT-09 13:30 By: MV Received: 16-OCT-09 By: JB
R900102
M86571-42 SW846 6010B 29-OCT-09 13:51 PY 28-OCT-09 EAL EPB
M86571-43 Collected: 15-OCT-09 13:40 By: MV Received: 16-OCT-09 By: JB
T900202
M86571-43 SW846 6010B 29-OCT-09 13:55 PY 28-OCT-09 EAL EPB
M86571-44 Collected: 15-OCT-09 13:55 By: MV Received: 16-OCT-09 By: JB
T900102
M86571-44 SW846 6010B 29-OCT-09 13:59 PY 28-OCT-09 EAL EPB
M86571-45 Collected: 15-OCT-09 14:00 By: MV Received: 16-OCT-09 By: JB
T900324
M86571-45 SW846 6010B 29-OCT-09 14:03 PY 28-OCT-09 EAL EPB
M86571-46 Collected: 15-OCT-09 14:40 By: MV Received: 16-OCT-09 By: JB
T900524
M86571-46 SW846 6010B 29-OCT-09 14:08 PY 28-OCT-09 EAL EPB
M86571-47 Collected: 15-OCT-09 14:50 By: MV Received: 16-OCT-09 By: JB
T900702
M86571-47 SW846 6010B 29-OCT-09 14:12 PY 28-OCT-09 EAL EPB
M86571-48 Collected: 15-OCT-09 15:00 By: MV Received: 16-OCT-09 By: JB
T900602
M86571-48 SW846 6010B 29-OCT-09 14:16 PY 28-OCT-09 EAL EPB
Page 6 of 6
71 of 96
M86571
44.3
Accutest Laboratories
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Matrix Spike and Duplicate Summaries
• Blank Spike and Lab Control Sample Summaries
• Serial Dilution Summaries
Section 5
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5
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14283 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 10/21/09
MBMetal RL IDL MDL raw final
Aluminum 0.20 .027 .04
Antimony 0.0060 .0014 .0016
Arsenic 0.025 .001 .0018
Barium 0.50 .00057 .0011
Beryllium 0.0040 .00015 .0004
Boron 0.10 .00065 .0023
Cadmium 0.0040 .00024 .0019
Calcium 5.0 .0076 .015
Chromium 0.010 .00081 .0011
Cobalt 0.050 .00025 .0003
Copper 0.025 .0022 .004
Gold 0.050 .0011 .0042
Iron 0.10 .0037 .013
Lead 0.010 .0011 .0027 -0.00020 <0.010
Magnesium 5.0 .037 .077
Manganese 0.015 .00012 .0011
Molybdenum 0.10 .00022 .0008
Nickel 0.040 .00024 .0013
Palladium 0.050 .0022 .004
Platinum 0.050 .0093 .013
Potassium 5.0 .039 .046
Selenium 0.025 .0019 .0035
Silicon 0.10 .0089 .036
Silver 0.0050 .00054 .0013
Sodium 5.0 .061 .16
Strontium 0.010 .00024 .0003
Thallium 0.0050 .0012 .0013
Tin 0.10 .00065 .0013
Titanium 0.050 .00074 .0008
Tungsten 0.10 .0056 .008
Vanadium 0.030 .00068 .0016
Zinc 0.10 .00074 .0015
Associated samples MP14283: M86571-1, M86571-2, M86571-3, M86571-4, M86571-5, M86571-6, M86571-7, M86571-8, M86571-9, M86571-10, M86571-11, M86571-12, M86571-13, M86571-14, M86571-15, M86571-16, M86571-17,_________________________________________________________________________________________________________
Page 1
73 of 96
M86571
55.1.1
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14283 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date:
Metal
M86571-18, M86571-19, M86571-20
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
74 of 96
M86571
55.1.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14283 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 10/21/09 10/21/09
M86571-11 Spikelot QC M86571-11 QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Gold
Iron
Lead 0.39 1.3 1.0 91.0 75-125 0.39 0.39 0.0 0-20
Magnesium
Manganese
Molybdenum
Nickel
Palladium
Platinum
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14283: M86571-1, M86571-2, M86571-3, M86571-4, M86571-5, M86571-6, M86571-7, M86571-8, M86571-9, M86571-10, M86571-11, M86571-12, M86571-13, M86571-14, M86571-15, M86571-16, M86571-17,_________________________________________________________________________________________________________
Page 1
75 of 96
M86571
55.1.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14283 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date:
Metal
M86571-18, M86571-19, M86571-20
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
76 of 96
M86571
55.1.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14283 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 10/21/09 10/21/09
BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Gold
Iron
Lead 0.92 1.0 92.0 80-120 0.91 1.0 91.0 1.1 20
Magnesium
Manganese
Molybdenum
Nickel
Palladium
Platinum
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14283: M86571-1, M86571-2, M86571-3, M86571-4, M86571-5, M86571-6, M86571-7, M86571-8, M86571-9, M86571-10, M86571-11, M86571-12, M86571-13, M86571-14, M86571-15, M86571-16, M86571-17,_________________________________________________________________________________________________________
Page 1
77 of 96
M86571
55.1.3
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14283 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date:
Metal
M86571-18, M86571-19, M86571-20
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
78 of 96
M86571
55.1.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14283 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date: 10/21/09
M86571-11 QCMetal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Gold
Iron
Lead 392 401 2.3 0-10
Magnesium
Manganese
Molybdenum
Nickel
Palladium
Platinum
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14283: M86571-1, M86571-2, M86571-3, M86571-4, M86571-5, M86571-6, M86571-7, M86571-8, M86571-9, M86571-10, M86571-11, M86571-12, M86571-13, M86571-14, M86571-15, M86571-16, M86571-17,_________________________________________________________________________________________________________
Page 1
79 of 96
M86571
55.1.4
SERIAL DILUTION RESULTS SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14283 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date:
Metal
M86571-18, M86571-19, M86571-20
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
80 of 96
M86571
55.1.4
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14291 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 10/22/09
MBMetal RL IDL MDL raw final
Aluminum 0.20 .027 .04
Antimony 0.0060 .0014 .0016
Arsenic 0.025 .001 .0018
Barium 0.50 .00057 .0011
Beryllium 0.0040 .00015 .0004
Boron 0.10 .00065 .0023
Cadmium 0.0040 .00024 .0019
Calcium 5.0 .0076 .015
Chromium 0.010 .00081 .0011
Cobalt 0.050 .00025 .0003
Copper 0.025 .0022 .004
Gold 0.050 .0011 .0042
Iron 0.10 .0037 .013
Lead 0.010 .0011 .0027 0.00020 <0.010
Magnesium 5.0 .037 .077
Manganese 0.015 .00012 .0011
Molybdenum 0.10 .00022 .0008
Nickel 0.040 .00024 .0013
Palladium 0.050 .0022 .004
Platinum 0.050 .0093 .013
Potassium 5.0 .039 .046
Selenium 0.025 .0019 .0035
Silicon 0.10 .0089 .036
Silver 0.0050 .00054 .0013
Sodium 5.0 .061 .16
Strontium 0.010 .00024 .0003
Thallium 0.0050 .0012 .0013
Tin 0.10 .00065 .0013
Titanium 0.050 .00074 .0008
Tungsten 0.10 .0056 .008
Vanadium 0.030 .00068 .0016
Zinc 0.10 .00074 .0015
Associated samples MP14291: M86571-21, M86571-22, M86571-23, M86571-24, M86571-25, M86571-26, M86571-27,M86571-28, M86571-29, M86571-30, M86571-31, M86571-32, M86571-33, M86571-34, M86571-35, M86571-36,_________________________________________________________________________________________________________
Page 1
81 of 96
M86571
55.2.1
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14291 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date:
Metal
M86571-37, M86571-38, M86571-39, M86571-40
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
82 of 96
M86571
55.2.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14291 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 10/22/09 10/22/09
M86571-21 Spikelot QC M86571-21 QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Gold
Iron
Lead 0.10 1.1 1.0 100.0 75-125 0.10 0.10 0.0 0-20
Magnesium
Manganese
Molybdenum
Nickel
Palladium
Platinum
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14291: M86571-21, M86571-22, M86571-23, M86571-24, M86571-25, M86571-26, M86571-27,M86571-28, M86571-29, M86571-30, M86571-31, M86571-32, M86571-33, M86571-34, M86571-35, M86571-36,_________________________________________________________________________________________________________
Page 1
83 of 96
M86571
55.2.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14291 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date:
Metal
M86571-37, M86571-38, M86571-39, M86571-40
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
84 of 96
M86571
55.2.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14291 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 10/22/09 10/22/09
BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Gold
Iron
Lead 0.94 1.0 94.0 80-120 0.95 1.0 95.0 1.1 20
Magnesium
Manganese
Molybdenum
Nickel
Palladium
Platinum
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14291: M86571-21, M86571-22, M86571-23, M86571-24, M86571-25, M86571-26, M86571-27,M86571-28, M86571-29, M86571-30, M86571-31, M86571-32, M86571-33, M86571-34, M86571-35, M86571-36,_________________________________________________________________________________________________________
Page 1
85 of 96
M86571
55.2.3
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14291 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date:
Metal
M86571-37, M86571-38, M86571-39, M86571-40
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
86 of 96
M86571
55.2.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14291 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date: 10/22/09
M86571-21 QCMetal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Gold
Iron
Lead 103 106 2.6 0-10
Magnesium
Manganese
Molybdenum
Nickel
Palladium
Platinum
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14291: M86571-21, M86571-22, M86571-23, M86571-24, M86571-25, M86571-26, M86571-27,M86571-28, M86571-29, M86571-30, M86571-31, M86571-32, M86571-33, M86571-34, M86571-35, M86571-36,_________________________________________________________________________________________________________
Page 1
87 of 96
M86571
55.2.4
SERIAL DILUTION RESULTS SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14291 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date:
Metal
M86571-37, M86571-38, M86571-39, M86571-40
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
88 of 96
M86571
55.2.4
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14323 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 10/28/09
MBMetal RL IDL MDL raw final
Aluminum 0.20 .027 .04
Antimony 0.0060 .0014 .0016
Arsenic 0.025 .001 .0018
Barium 0.50 .00057 .0011
Beryllium 0.0040 .00015 .0004
Boron 0.10 .00065 .0023
Cadmium 0.0040 .00024 .0019
Calcium 5.0 .0076 .015
Chromium 0.010 .00081 .0011
Cobalt 0.050 .00025 .0003
Copper 0.025 .0022 .004
Gold 0.050 .0011 .0042
Iron 0.10 .0037 .013
Lead 0.010 .0011 .0027 0.00060 <0.010
Magnesium 5.0 .037 .077
Manganese 0.015 .00012 .0011
Molybdenum 0.10 .00022 .0008
Nickel 0.040 .00024 .0013
Palladium 0.050 .0022 .004
Platinum 0.050 .0093 .013
Potassium 5.0 .039 .046
Selenium 0.025 .0019 .0035
Silicon 0.10 .0089 .036
Silver 0.0050 .00054 .0013
Sodium 5.0 .061 .16
Strontium 0.010 .00024 .0003
Thallium 0.0050 .0012 .0013
Tin 0.10 .00065 .0013
Titanium 0.050 .00074 .0008
Tungsten 0.10 .0056 .008
Vanadium 0.030 .00068 .0016
Zinc 0.10 .00074 .0015
Associated samples MP14323: M86571-41, M86571-42, M86571-43, M86571-44, M86571-45, M86571-46, M86571-47,M86571-48_________________________________________________________________________________________________________
Page 1
89 of 96
M86571
55.3.1
BLANK RESULTS SUMMARY Part 2 - Method Blanks
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14323 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date:
Metal
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
90 of 96
M86571
55.3.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14323 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 10/28/09 10/28/09
M86571-41 Spikelot QC M86571-41 QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Gold
Iron
Lead 1.0 2.0 1.0 100.0 75-125 1.0 1.0 0.0 0-20
Magnesium
Manganese
Molybdenum
Nickel
Palladium
Platinum
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14323: M86571-41, M86571-42, M86571-43, M86571-44, M86571-45, M86571-46, M86571-47,M86571-48_________________________________________________________________________________________________________
Page 1
91 of 96
M86571
55.3.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14323 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date:
Metal
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
92 of 96
M86571
55.3.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14323 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date: 10/28/09 10/28/09
BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Gold
Iron
Lead 0.94 1.0 94.0 80-120 0.91 1.0 91.0 3.2 20
Magnesium
Manganese
Molybdenum
Nickel
Palladium
Platinum
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14323: M86571-41, M86571-42, M86571-43, M86571-44, M86571-45, M86571-46, M86571-47,M86571-48_________________________________________________________________________________________________________
Page 1
93 of 96
M86571
55.3.3
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14323 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l
Prep Date:
Metal
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
94 of 96
M86571
55.3.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14323 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date: 10/28/09
M86571-41 QCMetal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Gold
Iron
Lead 1020 1070 4.4 0-10
Magnesium
Manganese
Molybdenum
Nickel
Palladium
Platinum
Potassium
Selenium
Silicon
Silver
Sodium
Strontium
Thallium
Tin
Titanium
Tungsten
Vanadium
Zinc
Associated samples MP14323: M86571-41, M86571-42, M86571-43, M86571-44, M86571-45, M86571-46, M86571-47,M86571-48_________________________________________________________________________________________________________
Page 1
95 of 96
M86571
55.3.4
SERIAL DILUTION RESULTS SUMMARY
Login Number: M86571 Account: OLINTN - Olin Corporation
Project: Mactec: Olin-Newhall St.-Hamden, CT
QC Batch ID: MP14323 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l
Prep Date:
Metal
Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
96 of 96
M86571
55.3.4
Recommended