TCLP Characterization NPP sent CTDEP 15Dec2009 · 2019-12-15 · The rest of the fill material in the NPP outside these seven areas meets the Tire Pond Material Acceptability Protocol

6107-09-0 December Mr. RaymRemediaBureau oState of C79 Elm SHartford, Re: E N H Dear Mr. F This letteevaluates Acceptabito the Con The CTDin closingcriteria foat the TirProtocol acriteria. Iindicated areas of fanalytes/pCriteria foto be usedlead. Thmilligramconcentra TCLP SA TCLP samwith the minitial planlead samCharacterlead data have a relForty-five

0004

r 15, 2009

mond Frigon ation Divisioof Water ProConnecticut

Street , CT 06106-

Evaluation of Non-Public PrHamden, Con

Frigon:

er presents a acceptability

ility Protocolnnecticut Dep

EP Material Ag the Tire Poor acceptance e Pond Landand comparedIn response tothe Departm

fill identifiedparameters pror mass analyd for fill at thhe Material A

ms per kilograation to be con

AMPLING ME

mples were comethodology nning stages,

mple results rization – Statset was then

latively unifore (45) sample

511 Cong

n tection and LDepartment

5127

Fill TCLP Lroperties, New

nnecticut

summary ofy of fill for usl numeric critpartment of E

Acceptabilityond (and Q P

of fill. The dfill” sent to Cd the NPP fillo MACTEC’

ment approvedd in Block F resented in tysis. The onlhe Tire Pond lAcceptability am (mg/kg) tnsidered non-

THODOLOGY

ollected in thdescribed in TCLP samplin ascendin

tistical Analydivided into rm distributio

e locations fro

gress Street, P.O. B207-775-540

Home Pag

Land Reuset of Environm

ead Data whall Street N

f the fill TCLse at the Tireteria (5 mg/L)nvironmental

y Protocol forPark) LandfilMACTEC Fe

CTDEP presel data from 0s letter, CTD

d of the conclare removed

the Material ly test remainlandfill is the

Protocol reqotal lead mu-hazardous.

Y

e spring and the October le locations wng order, aysis of May 2approximatel

on (of numberom thirty-eigh

Box 7050, Portland01 ● Fax 207-77ge: www.mactec.c

mental Prote

Neighborhoo

LP lead datae Pond by com) for leachingl Protection (C

r determiningll (dated Marebruary 14, 2ented the che-4 feet below

DEP submittedlusion of the

d from the 0-Acceptabilit

ning to determ Toxicity Chaquires that mst meet a les

fall of 2009 f21, 2008 TCL

were determinas presented 2009 Samplinly equal grours of samplesht properties

d, Maine 04112-72-4762 com

ection

od

a collected wmparing the Tg of lead. MACTDEP) on O

g acceptabilityrch 14, 2007)2008 letter “Emical criteria

w ground surfd a letter to Oletter report,

-4 feet bgs fity Protocol mmine the acceparacteristics L

material with ss than 5 mil

from fill areaLP Character

ned by orderinin the tec

ng Results” daups in order tos) over the ranwere thus id

7050

within the NPTCLP lead dACTEC is suOlin’s behalf.

y of soils and) details the

Evaluation of a for the Matface (bgs) agaOlin dated Jun, namely that ill data set, thmeet the Tirptability of eLeaching Pro

concentratioligrams per l

s within the Nrization Workng the existinchnical memated June 29,o obtain a datnge of total leentified for c

PP (Figure 1)ata to the Ma

ubmitting this

d sediments fospecificationFill for Place

terial Acceptaainst these nune 19, 2008 wwhen the iso

he 90% UCLre Pond Chexcavated matcedure (TCLP

ons exceedingliter (mg/L) T

NPP in accork Plan. Durinng database ofmorandum “T, 2009. Thista set which wead concentracollection of T

), and aterial letter

or use ns and ement ability umeric which olated Ls for emical terials P) for g 250 TCLP

dance ng the f total TCLP s total would ations. TCLP

Mr. Raymond Frigon December 15, 2009 Page 2 of 3

lead samples. However, despite attempts by Olin and MACTEC to obtain access to properties for which access had not yet been obtained, five of the thirty-eight properties could not be accessed for proposed sampling, providing a total of 40 samples (plus two duplicates) from thirty-three properties for analysis. Examination of the spring 2009 TCLP lead data showed an anomalous result for sample N101801; the original sample had a TCLP value of 2.8 mg/L while the duplicate had only 0.18 mg/L, much more in line with the TCLP result for other samples with similar total and SPLP results. Since further inquiry with the laboratory could not resolve this apparent anomaly, MACTEC elected to delete this sample from the evaluation, resulting in 39 samples from the spring 2009 sampling event available for evaluation. Given the findings of the “TCLP Characterization – Statistical Analysis of May 2009 Sampling Results” dated June 29, 2009 that concluded use of the existing SPLP data would not be an adequate basis for determining soil would meet the TCLP Acceptability Criteria, an additional 70 fill samples were collected for TCLP lead analyses in the fall of 2009. The locations of these samples were selected randomly by first gridding the entire NPP site into approximately 50-ft by 50-ft cells and numbering the cells containing fill within each block. The information was then entered into a program called Visual Sampling Plan (created by Pacific Northwest Laboratories, Department of Energy), which generated random cell numbers for each Block based on the number of cells containing fill. Some of the randomly generated sampling locations were located within properties where access to conduct sampling was not granted, and these locations were shifted to other accessible properties. Figure 2 presents the locations of the 109 TCLP lead samples used to evaluate the acceptability of fill material for use as closure material at the Tire Pond Landfill. Table 1 presents the sample location information, including block, street, address, sampling date, and sampling depth. The analytical data generated by Accutest Laboratories in Marlborough, Massachusetts were validated in accordance with CTDEP guidelines (i.e., data was reviewed for completeness as well as the quality parameters provided in the RCP deliverables). Data quality review summaries are presented in Attachment 1. The Material Acceptability Protocol requires that the sampling frequency for placement of material at the Tire Pond Landfill must be no less than one sample per 1,000 cubic yards of material. Table 2 presents the estimated fill volume to be excavated from the NPP, which is approximately 107,000 cubic yards. The 109 TCLP lead samples collected is sufficient to meet the criteria of 1 sample per 1,000 cubic yards of material. TCLP DATA EVALUATION Validated TCLP lead results for the 109 samples are presented in Table 2. TCLP lead concentrations range from non-detect (<0.01 mg/L) to 203 mg/L. The locations of the 7 samples with concentrations greater than the 5 mg/L criteria for placement at the Tire Pond Landfill are indicated on Figure 3, and highlighted in Table 3.

CONCLUSIONS AND RECOMMENDATIONS 109 TCLP lead samples were collected from fill within the NPP in the spring and fall of 2009. Seven out of the 109 TCLP lead samples have concentrations exceeding the Tire Pond material acceptability criteria of 5 mg/L. The recommended approach for handling of the seven sampling locations with the TCLP lead concentrations greater than 5 mg/L is to sample the areas in the immediate vicinity of these seven locations for TCLP lead to bracket the concentrations exceeding 5 mg/L. Four samples would be

Mr. Raymond Frigon December 15, 2009 Page 3 of 3

collected (roughly north, south, east, and west) at a distance of approximately 10 feet from each of the existing seven sample location. Provided that all concentrations are less than 5 mg/L, the volume of fill containing concentrations greater than 5 mg/L would be estimated for each location and treated in place or disposed at an appropriate off-site disposal location. If any of the new samples have TCLP lead concentrations exceeding 5 mg/L, then additional sampling would be required. The results of the additional sampling would be provided in a memorandum to CTDEP. In this manner, these seven areas will be handled separately from the remainder of the NPP fill. The rest of the fill material in the NPP outside these seven areas meets the Tire Pond Material Acceptability Protocol for TCLP, and will be sent to the Tire Pond without additional sampling (note that the material with elevated lead concentrations [Block F outlier areas] identified in the February 14, 2008 letter would still require disposal at another location other than the Tire Pond). Please do not hesitate to contact me at (207) 651-0315 should you have any questions regarding this letter. Sincerely, MACTEC Engineering and Consulting, Inc.

MACTEC Electronic Signature MACTEC Electronic Signature

Nelson Walter, P.E. Rod Pendleton, P.G. Project Manager Principal Scientist

Enclosures cc: David Share (Olin)

C. Hunt (Olin) J. Gear (Olin) William Sigmund (CTDEP) Meg Harvey (CTDPH)

Alan Elia (Sevenson) Jill Barrett (Fitzgerald & Halliday, Inc.) Honorable Scott Jackson (Mayor of Hamden) Chris Harriman (Haley & Aldrich, Inc.) David Silverstone (Regional Water Authority) File

FIGURES

Checked/Date: MGV 12/04/09Prepared/Date: BRP 12/04/07¯ 0 2,0001,000

Feet

Doc

umen

t: P

:\Pro

ject

s\O

lin H

amde

n N

ewha

ll S

t\GIS

\Map

docu

men

ts\S

iteLo

catio

nMap

_8x1

1P.m

xd

PD

F: P

:\Pro

ject

s\O

lin H

amde

n N

ewha

ll S

t\GIS

\Fig

ures

\22

Pro

perti

es W

ork

Pla

n\Fi

gure

1.pd

f 1

2/04

/200

7 1

1:22

AM

b

rpet

ers

Olin CorporationNewhall Street Neighborhood

Hamden, CT

Site Location Map

Project 6107090004 Figure 1

Connecticut1:24,000 scale digital topographic map obtainedfrom Environmental GIS Data for Connecticut -2003 Edition, State of Connecticut Departmentof EnvironmentalProtection.

SITELOCATION

SITELOCATION

G

T

F

B

KH J

S

E

QL

D

A

R

P

C

M N

HAMDEN PARK DRIVE

HAMDEN PARK INDUSTRIAL CIRCLE

HA

MD

EN

PA

RK

DR

IVE

HAMDEN PARK DRIVE

AUGUR STREET

MORSE STREET

HARRIS STREET

RE

MIN

GTO

N

STREET

CO

LUM

BU

S S

TRE

ET

MILL ROCK ROAD

HA

MD

EN

PA

RK

DR

IVE

BUTL

ER S

TREE

T

SHEP

ARD

STR

EET

SHEL

TON

AVE

NU

E

EDW

AR

DS

STR

EE

T

ST M

AR

Y S

TRE

ET

MARLBORO STREET

GOODRICH STREET

NE

WH

ALL

STR

EE

T

DU

DLE

Y C

OU

RT

GOODRICH STREET

GE

M S

T.

ALLING STREET

DUDLEY STREET

MORSE STREET

GO

OD

YEAR

LAMKIN STREET

GILE

S S

TRE

ET

RO

LFE RO

AD

FARN

SWO

RTH

STREET

PAC

IFIC S

TRE

ET

BLAKE ROADBLAKE CIRCLE

MILL ROCK ROAD

NE

WH

ALL

STR

EE

T

AUGUR STREET

MARLBORO STREET

NO

RTH

SH

EFF

IELD

STR

EE

T

LANE

HO

ME

LAN

DS

TE

RR

AC

E

MORSE STREET

PROSPECT COURT

PRO

SP

EC

T S

TRE

ET

BRYDEN TERRACE

WA

DS

WO

RTH

STR

EE

T

WIN

CH

ES

TER

AV

EN

UE

GOODRICH STREET

MORSE STREET

BLAKE CIRCLE

NEWBURY STREET

WIN

CH

ES

TER

AV

EN

UE

BRYDEN TERRACE

PROSPECT

PRO

SP

EC

T S

TRE

ET

NEW

HALL

STR

EET

!A!A!A!A!A!A

!A !A

!A

!A!A

!A

!A

!A!A

!A

!A

!A

!A!A

!A

!A

!A!A!A

!A!A

!A!A

!A!A

!A

!A!A

!A

!A!A!A!A

!A

!A

!A

!A!A!A

!A!A

!A !A!A

!A

!A!A

!A !A!A

!A

!A !A

!A

!A

!A!A

!A

!A

!A!A!A

!A!A!A!A

!A

!A

!A!A

!A!A!A

!A

!A!A

!A!A

!A

!A!A

!A

!A

!A

!A

!A!A!A

!A

!A

!A

!A

!A

!A

!A

!A!A

!A!A!A

!A

!A

!AS1056

S1039

R1031

SB-14SB-13

P1005

P1039

L1005

L1008

L1002

K1117

K1038

J1010

H1006

95-MS

C1006

C1003

C1004

T9003T9001

C9005

C9004

C9003

C9002

C9001

F9006

F9010

F9008

F9003

F9014F9013

F9011F9015

F9012

F9005

F9002

F9016

F9007 F9001

F9009

S9001

R9001

E9005

E9004

E9003E9001

P9003

P9004P9001

Q9002Q9001

E9002

K9002J9001

H9001 J9003

J9002

H9004H9009

H9010

J9004

L9007

L9005L9004 L9002

L9001

L9003

L9006

N9001

T9005

T9007

T9008T9004

A9001

A9002

H9008

H9007

H9006

H9005

H9002

H9011

H9003

T9002

M5030

H3009S1

H3003S1

H3001S3

F3006S2

F3003S1

F3002S1

A3011S1A3004S1

WIN-1061

124BT-HA5124BT-HA1

127MORSE-HA4127MORSE-HA1

266

48164

308330

20

20

99

449

40

26

163

596

41

79

49

44

26 22

49

3526

18

118

18

53

112

42

46311

105

34

48

117

499

124

16

293

106

131

94

303

98

95

125

22

90

92

54

60

13

84

35

28

99

16

14

12

163 29

90

23

59

30

39

50

32

26

155

56

115

44

17

38

45

10

18

109

15

121222

171

177

38

630

1035

17

20

61116

523

274

984

478

12673 69

130

21

634

105

30

83

10229108

299

123

474

142

150

502

17

45

117

49

39

125

973311

1048

965

155

238 33

214

453

421

159

115

1061

993

517

34

999

507

121

319

985

161

105

11

1067

425-431

5

9

994

338642

51

329

230

322

271295

263

279

259

291

267

275513

149

17-19

950

606

602

976

610

333

1002

1042

1036

1071

168

185

257

650

331

334

323

109

325

339

496

956

50-52

670

678

618

80

481

477

84

304

176

323

469

168

438

296

88

1005

452

300

82

342

160

319-321

473

245

297

461

465

29

960962

672

1032

203 199

1006

966

1028

515-517

492

1030

229

237

453

622

626

509-511

35-37

957-959

231234-236

25-27

968-970213-215

217-219164-166

156-158

484-486

21-23

972-974

460-462

S1044

J1006

F9004

S9002

P9002

K9001

T9006

H2002S P3001S3

C3001S1

127MORSE-HA3127MORSE-HA2

113

127

27

103

29

2125

136

135

1027

283287

32

337

265

16

87172

91

461

253

164

327

180

1019

267

488

241

197

321

165-167

233

220

237

216

457

979-981

466

315-317301-303

432-434

468

284-286290-292

424

476

221-223

160-162

472470466

462-464

508-510

207-209211-213

482-484

478-480

229-231

Document: C:\Documents and Settings\drpendleton\My Documents\_Projects\OLIN - Hamden\GIS\Mapdocuments\TCLP Characterization\TCLP_Sampling_Results_03Nov2009.mxd PDF: C:\Documents and Settings\drpendleton\My Documents\_Projects\OLIN - Hamden\TCLP Characterization\TCLP Characterization Memorandum\Draft_Dec2009\Figure 2_TCLP_SamplingLocs.pdf 12/03/2009 3:28 PM DRPendleton


Hamden, Connecticut

Checked/Date: MGV 12/03/09Prepared/Date: DRP 12/03/09

¯ 0 300 600 900150Feet

Legend

!A TCLP Sampling Locations

NPP Property BoundaryFill_Area_ExtentFill_Area_>_4_ft

TCLP Sampling Locations

Project 6107-09-0004 Figure 2

G

T

F

B

KH J

S

E

QL

D

A

R

P

C

M N

HAMDEN PARK DRIVE

HAMDEN PARK INDUSTRIAL CIRCLE

HA

MD

EN

PA

RK

DR

IVE

HAMDEN PARK DRIVE

AUGUR STREET

MORSE STREET

HARRIS STREET

RE

MIN

GTO

N

STREET

CO

LUM

BU

S S

TRE

ET

MILL ROCK ROAD

HA

MD

EN

PA

RK

DR

IVE

BUTL

ER S

TREE

T

SHEP

ARD

STR

EET

SHEL

TON

AVE

NU

E

EDW

AR

DS

STR

EE

T

ST M

AR

Y S

TRE

ET

MARLBORO STREET

GOODRICH STREET

NE

WH

ALL

STR

EE

T

DU

DLE

Y C

OU

RT

GOODRICH STREET

GE

M S

T.

ALLING STREET

DUDLEY STREET

MORSE STREET

GO

OD

YEAR

LAMKIN STREET

GILE

S S

TRE

ET

RO

LFE RO

AD

FARN

SWO

RTH

STREET

PAC

IFIC S

TRE

ET

BLAKE ROADBLAKE CIRCLE

MILL ROCK ROAD

NE

WH

ALL

STR

EE

T

AUGUR STREET

MARLBORO STREET

NO

RTH

SH

EFF

IELD

STR

EE

T

LANE

HO

ME

LAN

DS

TE

RR

AC

E

MORSE STREET

PROSPECT COURT

PRO

SP

EC

T S

TRE

ET

BRYDEN TERRACE

WA

DS

WO

RTH

STR

EE

T

WIN

CH

ES

TER

AV

EN

UE

GOODRICH STREET

MORSE STREET

BLAKE CIRCLE

NEWBURY STREET

WIN

CH

ES

TER

AV

EN

UE

BRYDEN TERRACE

PROSPECT

PRO

SP

EC

T S

TRE

ET

NEW

HALL

STR

EET

!A!A!A!A!A!A

!A !A

!A

!A!A

!A

!A

!A!A

!A

!A

!A

!A!A

!A

!A

!A!A!A

!A!A

!A!A

!A!A

!A

!A!A

!A

!A!A!A!A

!A

!A

!A

!A!A!A

!A!A

!A !A!A

!A

!A!A

!A !A!A

!A

!A !A

!A

!A

!A!A

!A

!A

!A!A!A

!A!A!A!A

!A

!A

!A!A

!A!A!A

!A

!A!A

!A!A

!A

!A!A

!A

!A

!A

!A

!A!A!A

!A

!A

!A

!A

!A

!A

!A

!A!A

!A!A!A

!A

!A

!A

!A

!A

!A

!A

!A!A

!A203203

1471477 .47 .4

107107

54 .154 .1

20 .420 .4

46 .546 .5

266

48164

308330

20

20

99

449

40

26

163

596

41

79

49

44

26 22

49

3526

18

118

18

53

112

46311

105

34

48

117

499

124

16

293

106

131

94

303

98

95

125

22

90

92

54

60

13

84

35

28

99

16

14

12

163 29

90

23

59

30

39

50

32

26

155

56

115

44

17

38

45

10

18

109

15

121222

171

177

630

1035

17

20

61116

523

274

984

478

12673 69

130

21

634

105

30

83

10229108

299

123

474

142

150

502

17

45

117

49

39

125

973311

1048

965

155

238 33

214

421

159

115

1061

993

517

34

999

507

121

319

985

161

105

11

1067

425-431

5

9

994

338642

51

329

230

322

271295

263

279

259

291

267

275 513

149

17-19

950

606

602

976

610

333

1002

1042

1036

1071

168

185

257

650

331

334

323

109

325

339

496

956

50-52

670

678

618

80

481

477

84

304

176

323

469

168

438

296

88

1005

452

300

82

342

160

319-321

473

245

297

461

465

29

960962

672

1032

203 199

1006

966

1028

515-517

492

1030

229

453

622

626

509-511

35-37

957-959

234-23625-27

968-970213-215

217-219164-166

156-158

484-486

21-23

972-974

460-462

113

42

127

27

103

29

38

2125

136

453

135

1027

283287

32

337

265

16

87172

91

461

253

164

327

180

1019

267

488

241

197

321

165-167

233

220

237

216

237

457

979-981

231

466

315-317301-303

432-434

468

284-286290-292

424

476

221-223

160-162

472470466

462-464

508-510

207-209211-213

482-484

478-480

229-231

Document: C:\Documents and Settings\drpendleton\My Documents\_Projects\OLIN - Hamden\GIS\Mapdocuments\TCLP Characterization\TCLP_Sampling_Results_03Nov2009.mxd PDF: C:\Documents and Settings\drpendleton\My Documents\_Projects\OLIN - Hamden\TCLP Characterization\TCLP Characterization Memorandum\Draft_Dec2009\Figure 3_TCLP_Lead_Concs.pdf 12/03/2009 3:30 PM DRPendleton


Hamden, Connecticut

Checked/Date: MGV 12/03/09Prepared/Date: DRP 12/03/09

¯ 0 300 600 900150Feet

Legend

!A TCLP Lead Concentrations > 5 mg/L (concentration in mg/L)

!A TCLP Sampling Locations

NPP Property BoundaryFill_Area_ExtentFill_Area_>_4_ft

TCLP Lead Concentrations > 5 mg/L

Project 6107-09-0004 Figure 3

TABLES

TABLE 1TCLP LEAD SAMPLE INFORMATION

NEWHALL STREET NEIGHBORHOODHAMDEN, CONNECTICUT

Block Street Number Street Name Location ID Field Sample ID Sample Date

Top Depth

(ft,bgs)

Bottom Depth (ft,bgs)

A 279 Morse St. A3004S1 A300401 05-May-09 0 1A 267 Morse St. A3011S1 A3011S101 05-May-09 0 1A 263 Morse St. A9001 A900102 10-Sep-09 0 2A 287 Morse St. A9002 A900224 10-Sep-09 2 4C 125 Bryden Terr. C1003 C100324 04-May-09 2 4C 117 Bryden Terr. C1004 C100424 05-May-09 2 4C 60 Wadsworth St. C1006 C100624 04-May-09 2 4C 60 Wadsworth St. C3001S1 C3001S101 04-May-09 0 1C 125 Bryden Terr. C9001 C900124 09-Sep-09 2 4C 117 Bryden Terr. C9002 C900224 15-Oct-09 2 4C 99 Bryden Terr. C9003 C900324 14-Oct-09 2 4C 99 Bryden Terr. C9004 C900424 14-Oct-09 2 4C 99 Bryden Terr. C9005 C900502 14-Oct-09 0 2C 1061 Winchester Ave. WIN-1061 WIN-106124 04-May-09 2 4E 513 Newhall St. E9001 E900124 15-Oct-09 2 4E 523 Newhall St. E9002 E900224 10-Sep-09 2 4E 513 Newhall St. E9003 E900324 15-Oct-09 2 4E 177 Morse St. E9004 E900424 15-Oct-09 2 4E 177 Morse St. E9005 E900502 15-Oct-09 0 2F 124 Bryden Terr. 124BT-HA1 124BT-HA112 04-May-09 1 2F 124 Bryden Terr. 124BT-HA5 124BT-HA512 04-May-09 1 2F 127 Morse St. 127MORSE-HA1 127MORSE-HA112 04-May-09 1 2F 127 Morse St. 127MORSE-HA2 127MORSE-HA212 04-May-09 1 2F 127 Morse St. 127MORSE-HA3 127MORSE-HA412 04-May-09 1 2F 127 Morse St. 127MORSE-HA4 267MORSE-HA512 05-May-09 1 2F 95 Morse St. 95-MS 95-MS01 04-May-09 0 1F 135 Morse St. F3002S1 F3002S101 04-May-09 0 1F 109 Morse St. F3003S1 F3003S101 04-May-09 0 1F 136 Bryden Terr. F3006S2 F3006S201 04-May-09 0 1F 1027 Winchester Ave. F9001 F900102 15-Oct-09 0 2F 127 Morse St. F9002 F900224 15-Oct-09 2 4F 84 Bryden Terr. F9003 F900324 15-Oct-09 2 4F 103 Morse St. F9004 F900402 09-Sep-09 0 2F 127 Morse St. F9005 F900524 15-Oct-09 2 4F 106 Bryden Terr. F9006 F900602 14-Oct-09 0 2F 1027 Winchester Ave. F9007 F900724 15-Oct-09 2 4F 84 Bryden Terr. F9008 F900824 15-Oct-09 2 4F 136 Bryden Terr. F9009 F900924 09-Sep-09 2 4F 84 Bryden Terr. F9010 F901002 15-Oct-09 0 2F 103 Morse St. F9011 F901102 09-Sep-09 0 2F 127 Morse St. F9012 F901224 15-Oct-09 2 4F 103 Morse St. F9013 F901302 09-Sep-09 0 2F 103 Morse St. F9014 F901424 09-Sep-09 2 4F 127 Morse St. F9015 F901524 15-Oct-09 2 4F 1027 Winchester Ave. F9016 F901602 15-Oct-09 0 2H 38 Edwards St. H1006 H100624 05-May-09 2 4H 38 Edwards St. H2002S H2002S23 05-May-09 2 3H 53 St. Mary St. H3001S3 H3001S301 05-May-09 0 1H 32 Edwards St. H3003S1 H3003S101 05-May-09 0 1H 27 St. Mary St. H3009S1 H3009S101 05-May-09 0 1

Page 1 of 3Prepared by: DRPChecked by: NW




Top Depth

(ft,bgs)


H 21 St. Mary St. H9001 H900124 14-Oct-09 2 4H 308 Morse St. H9002 H900224 14-Oct-09 2 4H 330 Morse St. H9003 H900324 09-Sep-09 2 4H 27 St. Mary St. H9004 H900424 14-Oct-09 2 4H 308 Morse St. H9005 H900524 14-Oct-09 2 4H 308 Morse St. H9006 H900602 14-Oct-09 0 2H 308 Morse St. H9007 H900702 14-Oct-09 0 2H 308 Morse St. H9008 H900802 14-Oct-09 0 2H 29 St. Mary St. H9009 H900902 14-Oct-09 0 2H 16 Edwards St. H9010 H901024 14-Oct-09 2 4H 330 Morse St. H9011 H901102 09-Sep-09 0 2J 45 Edwards St. J1006 J100601 05-May-09 0 1J 59 Edwards St. J1010 J101012 05-May-09 1 2J 488 Shelton Ave. J9001 J900102 14-Oct-09 0 2J 476 Shelton Ave. J9002 J900224 14-Oct-09 2 4J 476 Shelton Ave. J9003 J900302 14-Oct-09 0 2J 59 Edwards St. J9004 J900424 14-Oct-09 2 4K 216 Morse St. K1038 K103801 05-May-09 0 1K 266 Morse St. K1117 K111701 05-May-09 0 1K 468 Newhall St. K9001 K900102 15-Oct-09 0 2K 468 Newhall St. K9002 K900202 15-Oct-09 0 2L 238 Butler St. L1002 L100201 05-May-09 0 1L 481 Shelton Ave. L1005 L100524 05-May-09 2 4L 265 Goodrich St. L1008 L100824 05-May-09 2 4L 481 Shelton Ave. L9001 L900102 09-Sep-09 0 2L 481 Shelton Ave. L9002 L900224 09-Sep-09 2 4L 265 Goodrich St. L9003 L900324 14-Oct-09 2 4L 481 Shelton Ave. L9004 L900424 09-Sep-09 2 4L 481 Shelton Ave. L9005 L900524 09-Sep-09 2 4L 461 Shelton Ave. L9006 L900602 10-Sep-09 0 2L 481 Shelton Ave. L9007 L900702 09-Sep-09 0 2M 168 Shepard St. M5030 M503002 05-May-09 0 2N 207-209 Goodrich St. N9001 N900124 14-Oct-09 2 4P 180 Morse St. P1005 P100524 04-May-09 2 4P 164 Morse St. P1039 P103901 04-May-09 0 1P 172 Morse St. P3001S3 P3001S301 04-May-09 0 1P 481 Newhall St. P9001 P900124 15-Oct-09 2 4P 176 Morse St. P9002 P900202 15-Oct-09 0 2P 21 Marlboro St. P9003 P900302 10-Sep-09 0 2P 176 Morse St. P9004 P900402 15-Oct-09 0 2Q 449 Newhall St. Q9001 Q900124 09-Sep-09 2 4Q 449 Newhall St. Q9002 Q900202 09-Sep-09 0 2Q 449 Newhall St. SB-13 SB-1324 04-May-09 2 4Q 449 Newhall St. SB-14 SB-1404 04-May-09 0 4R 979-981 Winchester Ave. R1031 R103102 05-May-09 0 2R 973 Winchester Ave. R9001 R900102 15-Oct-09 0 2S 29 North Sheffield St. S1039 S103924 06-May-09 2 4S 41 North Sheffield St. S1044 S104412 04-May-09 1 2S 98 Morse St. S1056 S105614 04-May-09 1 4S 92 Morse St. S9001 S900124 09-Sep-09 2 4





Top Depth

(ft,bgs)


S 35 North Sheffield St. S9002 S900224 09-Sep-09 2 4T 678 Newhall St. T9001 T900102 15-Oct-09 0 2T 339 Augur St. T9002 T900202 15-Oct-09 0 2T 672 Newhall St. T9003 T900324 15-Oct-09 2 4T 20 Harris St. T9004 T900424 10-Sep-09 2 4T 22 Remington St. T9005 T900524 15-Oct-09 2 4T 17 Harris St. T9006 T900602 15-Oct-09 0 2T 17 Harris St. T9007 T900702 15-Oct-09 0 2T 20 Harris St. T9008 T900824 10-Sep-09 2 4


TABLE 2 ESTIMATED FILL EXCAVATION VOLUME BY BLOCK


BlockEstimated Fill Excavation

Volumes1 (0‐4 ft bgs) in cu yds

A 2,355 C 16,010 E 7,298 F2 20,508

H 14,839 J 8,665 K 2,956 L 9,164 M 1,143 N 344 P 5,780 Q 7,115 R 446 S 1,834 T 8,975

Total 107,000

Notes: 1) Estimated fill excavation volumes are based on 1:1 slopes adjacent to streets and buildings

2) Excludes Block F Hot-Spots (2,606 cu yds) identified for disposal at a landfill other than the Tire Pond (see "Evaluation of Fill for Placement at the Tire Pond Landfill", February 14, 2008)


TABLE 3TCLP LEAD ANALYTICAL RESULTS


Block Street Number Street Name Location ID Field Sample

ID Sample Date Top Depth (ft,bgs)


Parameter Result Final Qualifier

Unit of Measure

A 279 Morse St. A3004S1 A300401 05-May-09 0 1 TCLP Lead 0.17 MG/LA 267 Morse St. A3011S1 A3011S101 05-May-09 0 1 TCLP Lead 0.24 MG/LA 263 Morse St. A9001 A900102 10-Sep-09 0 2 TCLP Lead 0.016 MG/LA 287 Morse St. A9002 A900224 10-Sep-09 2 4 TCLP Lead 1.4 J MG/LC 125 Bryden Terr. C1003 C100324 04-May-09 2 4 TCLP Lead 1.1 MG/LC 117 Bryden Terr. C1004 C100424 05-May-09 2 4 TCLP Lead 0.76 MG/LC 60 Wadsworth St. C1006 C100624 04-May-09 2 4 TCLP Lead 1 J MG/LC 60 Wadsworth St. C3001S1 C3001S101 04-May-09 0 1 TCLP Lead 1.3 J MG/LC 125 Bryden Terr. C9001 C900124 09-Sep-09 2 4 TCLP Lead 1.1 MG/LC 117 Bryden Terr. C9002 C900224 15-Oct-09 2 4 TCLP Lead 20.4 J MG/LC 99 Bryden Terr. C9003 C900324 14-Oct-09 2 4 TCLP Lead 0.16 J MG/LC 99 Bryden Terr. C9004 C900424 14-Oct-09 2 4 TCLP Lead 0.81 J MG/LC 99 Bryden Terr. C9005 C900502 14-Oct-09 0 2 TCLP Lead 0.2 J MG/LC 1061 Winchester Ave. WIN-1061 WIN-106124 04-May-09 2 4 TCLP Lead 0.3 MG/LE 513 Newhall St. E9001 E900124 15-Oct-09 2 4 TCLP Lead 2.7 J MG/LE 523 Newhall St. E9002 E900224 10-Sep-09 2 4 TCLP Lead 107 J MG/LE 513 Newhall St. E9003 E900324 15-Oct-09 2 4 TCLP Lead 0.015 J MG/LE 177 Morse St. E9004 E900424 15-Oct-09 2 4 TCLP Lead 0.3 J MG/LE 177 Morse St. E9005 E900502 15-Oct-09 0 2 TCLP Lead 0.027 J MG/LF 124 Bryden Terr. 124BT-HA1 124BT-HA112 04-May-09 1 2 TCLP Lead 0.25 J MG/LF 124 Bryden Terr. 124BT-HA5 124BT-HA512 04-May-09 1 2 TCLP Lead 0.014 J MG/LF 127 Morse St. 127MORSE-HA1 HA112 04-May-09 1 2 TCLP Lead 0.032 J MG/LF 127 Morse St. 127MORSE-HA2 HA212 04-May-09 1 2 TCLP Lead 2.1 J MG/LF 127 Morse St. 127MORSE-HA3 HA412 04-May-09 1 2 TCLP Lead 2.8 J MG/LF 127 Morse St. 127MORSE-HA4 HA512 05-May-09 1 2 TCLP Lead 0.081 MG/LF 95 Morse St. 95-MS 95-MS01 04-May-09 0 1 TCLP Lead 0.057 J MG/LF 135 Morse St. F3002S1 F3002S101 04-May-09 0 1 TCLP Lead 0.27 J MG/LF 109 Morse St. F3003S1 F3003S101 04-May-09 0 1 TCLP Lead 0.65 J MG/LF 136 Bryden Terr. F3006S2 F3006S201 04-May-09 0 1 TCLP Lead 0.23 MG/LF 1027 Winchester Ave. F9001 F900102 15-Oct-09 0 2 TCLP Lead 1 MG/LF 127 Morse St. F9002 F900224 15-Oct-09 2 4 TCLP Lead 0.94 J MG/LF 84 Bryden Terr. F9003 F900324 15-Oct-09 2 4 TCLP Lead 0.058 J MG/LF 103 Morse St. F9004 F900402 09-Sep-09 0 2 TCLP Lead 0.23 MG/LF 127 Morse St. F9005 F900524 15-Oct-09 2 4 TCLP Lead 0.24 J MG/LF 106 Bryden Terr. F9006 F900602 14-Oct-09 0 2 TCLP Lead 0.26 J MG/LF 1027 Winchester Ave. F9007 F900724 15-Oct-09 2 4 TCLP Lead 0.62 J MG/LF 84 Bryden Terr. F9008 F900824 15-Oct-09 2 4 TCLP Lead 0.069 J MG/LF 136 Bryden Terr. F9009 F900924 09-Sep-09 2 4 TCLP Lead 0.17 J MG/L

Page 1 of 3Prepared by: DRPChecked by : NW







Unit of Measure

F 84 Bryden Terr. F9010 F901002 15-Oct-09 0 2 TCLP Lead 0.37 J MG/LF 103 Morse St. F9011 F901102 09-Sep-09 0 2 TCLP Lead 1.2 MG/LF 127 Morse St. F9012 F901224 15-Oct-09 2 4 TCLP Lead 0.033 J MG/LF 103 Morse St. F9013 F901302 09-Sep-09 0 2 TCLP Lead 0.7 MG/LF 103 Morse St. F9014 F901424 09-Sep-09 2 4 TCLP Lead 0.36 MG/LF 127 Morse St. F9015 F901524 15-Oct-09 2 4 TCLP Lead 7.4 J MG/LF 1027 Winchester Ave. F9016 F901602 15-Oct-09 0 2 TCLP Lead 0.055 J MG/LH 38 Edwards St. H1006 H100624 05-May-09 2 4 TCLP Lead 147 J MG/LH 38 Edwards St. H2002S H2002S23 05-May-09 2 3 TCLP Lead 54.1 J MG/LH 53 St. Mary St. H3001S3 H3001S301 05-May-09 0 1 TCLP Lead 0.84 J MG/LH 32 Edwards St. H3003S1 H3003S101 05-May-09 0 1 TCLP Lead 0.17 MG/LH 27 St. Mary St. H3009S1 H3009S101 05-May-09 0 1 TCLP Lead 0.18 J MG/LH 21 St. Mary St. H9001 H900124 14-Oct-09 2 4 TCLP Lead 0.088 J MG/LH 308 Morse St. H9002 H900224 14-Oct-09 2 4 TCLP Lead 0.16 J MG/LH 330 Morse St. H9003 H900324 09-Sep-09 2 4 TCLP Lead 0.049 MG/LH 27 St. Mary St. H9004 H900424 14-Oct-09 2 4 TCLP Lead 0.021 J MG/LH 308 Morse St. H9005 H900524 14-Oct-09 2 4 TCLP Lead 0.01 UJ MG/LH 308 Morse St. H9006 H900602 14-Oct-09 0 2 TCLP Lead 0.057 J MG/LH 308 Morse St. H9007 H900702 14-Oct-09 0 2 TCLP Lead 0.068 J MG/LH 308 Morse St. H9008 H900802 14-Oct-09 0 2 TCLP Lead 0.18 J MG/LH 29 St. Mary St. H9009 H900902 14-Oct-09 0 2 TCLP Lead 0.063 J MG/LH 16 Edwards St. H9010 H901024 14-Oct-09 2 4 TCLP Lead 0.01 UJ MG/LH 330 Morse St. H9011 H901102 09-Sep-09 0 2 TCLP Lead 0.13 MG/LJ 45 Edwards St. J1006 J100601 05-May-09 0 1 TCLP Lead 0.11 J MG/LJ 59 Edwards St. J1010 J101012 05-May-09 1 2 TCLP Lead 2 J MG/LJ 488 Shelton Ave. J9001 J900102 14-Oct-09 0 2 TCLP Lead 0.39 J MG/LJ 476 Shelton Ave. J9002 J900224 14-Oct-09 2 4 TCLP Lead 0.12 J MG/LJ 476 Shelton Ave. J9003 J900302 14-Oct-09 0 2 TCLP Lead 0.17 J MG/LJ 59 Edwards St. J9004 J900424 14-Oct-09 2 4 TCLP Lead 0.27 J MG/LK 216 Morse St. K1038 K103801 05-May-09 0 1 TCLP Lead 0.7 MG/LK 266 Morse St. K1117 K111701 05-May-09 0 1 TCLP Lead 0.19 MG/LK 468 Newhall St. K9001 K900102 15-Oct-09 0 2 TCLP Lead 0.1 J MG/LK 468 Newhall St. K9002 K900202 15-Oct-09 0 2 TCLP Lead 0.075 J MG/LL 238 Butler St. L1002 L100201 05-May-09 0 1 TCLP Lead 0.18 MG/LL 481 Shelton Ave. L1005 L100524 05-May-09 2 4 TCLP Lead 2 MG/LL 265 Goodrich St. L1008 L100824 05-May-09 2 4 TCLP Lead 0.12 MG/LL 481 Shelton Ave. L9001 L900102 09-Sep-09 0 2 TCLP Lead 4.3 MG/LL 481 Shelton Ave. L9002 L900224 09-Sep-09 2 4 TCLP Lead 46.5 J MG/L








Unit of Measure

L 265 Goodrich St. L9003 L900324 14-Oct-09 2 4 TCLP Lead 0.036 J MG/LL 481 Shelton Ave. L9004 L900424 09-Sep-09 2 4 TCLP Lead 0.43 MG/LL 481 Shelton Ave. L9005 L900524 09-Sep-09 2 4 TCLP Lead 0.01 U MG/LL 461 Shelton Ave. L9006 L900602 10-Sep-09 0 2 TCLP Lead 0.1 MG/LL 481 Shelton Ave. L9007 L900702 09-Sep-09 0 2 TCLP Lead 1.9 MG/LM 168 Shepard St. M5030 M503002 05-May-09 0 2 TCLP Lead 0.064 MG/LN 207-209 Goodrich St. N9001 N900124 14-Oct-09 2 4 TCLP Lead 0.061 J MG/LP 180 Morse St. P1005 P100524 04-May-09 2 4 TCLP Lead 0.058 MG/LP 164 Morse St. P1039 P103901 04-May-09 0 1 TCLP Lead 0.3 MG/LP 172 Morse St. P3001S3 P3001S301 04-May-09 0 1 TCLP Lead 0.36 MG/LP 481 Newhall St. P9001 P900124 15-Oct-09 2 4 TCLP Lead 0.82 J MG/LP 176 Morse St. P9002 P900202 15-Oct-09 0 2 TCLP Lead 0.073 J MG/LP 21 Marlboro St. P9003 P900302 10-Sep-09 0 2 TCLP Lead 0.15 J MG/LP 176 Morse St. P9004 P900402 15-Oct-09 0 2 TCLP Lead 0.45 J MG/LQ 449 Newhall St. Q9001 Q900124 09-Sep-09 2 4 TCLP Lead 0.074 MG/LQ 449 Newhall St. Q9002 Q900202 09-Sep-09 0 2 TCLP Lead 0.026 MG/LQ 449 Newhall St. SB-13 SB-1324 04-May-09 2 4 TCLP Lead 0.097 MG/LQ 449 Newhall St. SB-14 SB-1404 04-May-09 0 4 TCLP Lead 203 MG/LR 979-981 Winchester Ave. R1031 R103102 05-May-09 0 2 TCLP Lead 0.099 MG/LR 973 Winchester Ave. R9001 R900102 15-Oct-09 0 2 TCLP Lead 0.065 MG/LS 29 North Sheffield St. S1039 S103924 06-May-09 2 4 TCLP Lead 0.062 MG/LS 41 North Sheffield St. S1044 S104412 04-May-09 1 2 TCLP Lead 0.06 J MG/LS 98 Morse St. S1056 S105614 04-May-09 1 4 TCLP Lead 0.1 J MG/LS 92 Morse St. S9001 S900124 09-Sep-09 2 4 TCLP Lead 0.01 U MG/LS 35 North Sheffield St. S9002 S900224 09-Sep-09 2 4 TCLP Lead 0.4 MG/LT 678 Newhall St. T9001 T900102 15-Oct-09 0 2 TCLP Lead 0.017 MG/LT 339 Augur St. T9002 T900202 15-Oct-09 0 2 TCLP Lead 0.13 MG/LT 672 Newhall St. T9003 T900324 15-Oct-09 2 4 TCLP Lead 0.069 MG/LT 20 Harris St. T9004 T900424 10-Sep-09 2 4 TCLP Lead 0.025 J MG/LT 22 Remington St. T9005 T900524 15-Oct-09 2 4 TCLP Lead 0.01 U MG/LT 17 Harris St. T9006 T900602 15-Oct-09 0 2 TCLP Lead 0.014 MG/LT 17 Harris St. T9007 T900702 15-Oct-09 0 2 TCLP Lead 0.2 MG/LT 20 Harris St. T9008 T900824 10-Sep-09 2 4 TCLP Lead 0.017 J MG/L

Notes:1) Sample Concentration exceeds 5.0 mg/L Tire Pond disposal criteria


ATTACHMENT 1

DATA QUALITY REVIEWS

05/20/09

Technical Report for

Olin CorporationMactec: Olin-Newhall St.-Hamden, CT

6107090004/01

Accutest Job Number: M82628

Sampling Dates: 05/04/09 - 05/06/09

Report to:

MacTec

[email protected]

ATTN: Rod Pendleton

Total number of pages in report:

Certifications: MA (M-MA136) CT (PH-0109) NH (2502) RI (00071) ME (MA0136) FL (E87579)NY (11791) NJ (MA926) PA (68-01121) NC (653) IL (200018) NAVY USACEThis report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.Test results relate only to samples analyzed.

New England • 495 Tech Center West • Building 1 • Marlborough, MA 01752 • tel: 508-481-6200 • fax: 508-481-7753 • http://www.accutest.com

Test results contained within this data package meet the requirements of the National Environmental Laboratory Accreditation Conference and/or state specific certification programs as applicable.

Client Service contact: Kristen Blanchard 508-481-6200

Reza TandLab Director

05/20/09

e-Hardcopy 2.0Automated Report

211

Accutest Laboratories is the sole authority for authorizing edits or modifications to thisdocument. Unauthorized modification of this report is strictly prohibited.

1 of 211

M82628

Table of Contents-1-

Sections:

Section 1: Sample Summary ................................................................................................... 6Section 2: Case Narrative/Conformance Summary .............................................................. 17Section 3: Sample Results ........................................................................................................ 20

3.1: M82628-1: SB-1324 ..................................................................................................... 213.2: M82628-1A: SB-1324 .................................................................................................. 223.3: M82628-1B: SB-1324 .................................................................................................. 233.4: M82628-2: SB-1404 ..................................................................................................... 243.5: M82628-2A: SB-1404 .................................................................................................. 253.6: M82628-2B: SB-1404 .................................................................................................. 263.7: M82628-3: P103901 ..................................................................................................... 273.8: M82628-3A: P103901 .................................................................................................. 283.9: M82628-3B: P103901 .................................................................................................. 293.10: M82628-4: P3001S301 ............................................................................................... 303.11: M82628-4A: P3001S301 ............................................................................................ 313.12: M82628-4B: P3001S301 ............................................................................................ 323.13: M82628-5: P100524 ................................................................................................... 333.14: M82628-5A: P100524 ................................................................................................ 343.15: M82628-5B: P100524 ................................................................................................ 353.16: M82628-6: F3006S201 ............................................................................................... 363.17: M82628-6A: F3006S201 ............................................................................................ 373.18: M82628-6B: F3006S201 ............................................................................................ 383.19: M82628-7: WIN-106124 ............................................................................................ 393.20: M82628-7A: WIN-106124 ......................................................................................... 403.21: M82628-7B: WIN-106124 ......................................................................................... 413.22: M82628-8: C100324 ................................................................................................... 423.23: M82628-8A: C100324 ................................................................................................ 433.24: M82628-8B: C100324 ................................................................................................ 443.25: M82628-9: 124BT-HA512 ......................................................................................... 453.26: M82628-9A: 124BT-HA512 ...................................................................................... 463.27: M82628-9B: 124BT-HA512 ...................................................................................... 473.28: M82628-10: 124BT-HA112 ....................................................................................... 483.29: M82628-10A: 124BT-HA112 .................................................................................... 493.30: M82628-10B: 124BT-HA112 .................................................................................... 503.31: M82628-11: 95-MS01 ................................................................................................ 513.32: M82628-11A: 95-MS01 ............................................................................................. 523.33: M82628-11B: 95-MS01 .............................................................................................. 533.34: M82628-12: F3002S101 ............................................................................................. 543.35: M82628-12A: F3002S101 .......................................................................................... 553.36: M82628-12B: F3002S101 .......................................................................................... 563.37: M82628-13: 127MORSE-HA412 .............................................................................. 573.38: M82628-13A: 127MORSE-HA412 ............................................................................ 583.39: M82628-13B: 127MORSE-HA412 ............................................................................ 59

12

34

5

2 of 211

M82628


Sections:

3.40: M82628-14: 127MORSE-HA112 .............................................................................. 603.41: M82628-14A: 127MORSE-HA112 ............................................................................ 613.42: M82628-14B: 127MORSE-HA112 ............................................................................ 623.43: M82628-15: 127MORSE-HA212 .............................................................................. 633.44: M82628-15A: 127MORSE-HA212 ............................................................................ 643.45: M82628-15B: 127MORSE-HA212 ............................................................................ 653.46: M82628-16: S104412 ................................................................................................. 663.47: M82628-16A: S104412 .............................................................................................. 673.48: M82628-16B: S104412 .............................................................................................. 683.49: M82628-17: S105614 ................................................................................................. 693.50: M82628-17A: S105614 .............................................................................................. 703.51: M82628-17B: S105614 .............................................................................................. 713.52: M82628-18: F3003S101 ............................................................................................. 723.53: M82628-18A: F3003S101 .......................................................................................... 733.54: M82628-18B: F3003S101 .......................................................................................... 743.55: M82628-19: C100624 ................................................................................................. 753.56: M82628-19A: C100624 .............................................................................................. 763.57: M82628-19B: C100624 .............................................................................................. 773.58: M82628-20: C3001S101 ............................................................................................ 783.59: M82628-20A: C3001S101 .......................................................................................... 793.60: M82628-20B: C3001S101 .......................................................................................... 803.61: M82628-21: N101801 ................................................................................................ 813.62: M82628-21A: N101801 .............................................................................................. 823.63: M82628-21B: N101801 .............................................................................................. 833.64: M82628-22: N101801DUP ........................................................................................ 843.65: M82628-22A: N101801DUP ...................................................................................... 853.66: M82628-22B: N101801DUP ...................................................................................... 863.67: M82628-23: H3009S101 ............................................................................................ 873.68: M82628-23A: H3009S101 ......................................................................................... 883.69: M82628-23B: H3009S101 .......................................................................................... 893.70: M82628-24: H3001S301 ............................................................................................ 903.71: M82628-24A: H3001S301 ......................................................................................... 913.72: M82628-24B: H3001S301 .......................................................................................... 923.73: M82628-25: J101012 .................................................................................................. 933.74: M82628-25A: J101012 ............................................................................................... 943.75: M82628-25B: J101012 ............................................................................................... 953.76: M82628-26: J100601 .................................................................................................. 963.77: M82628-26A: J100601 ............................................................................................... 973.78: M82628-26B: J100601 ............................................................................................... 983.79: M82628-27: H100624 ................................................................................................ 993.80: M82628-27A: H100624 .............................................................................................. 1003.81: M82628-27B: H100624 .............................................................................................. 101

12

34

5

3 of 211

M82628


Sections:

3.82: M82628-28: H2002S23 .............................................................................................. 1023.83: M82628-28A: H2002S23 ........................................................................................... 1033.84: M82628-28B: H2002S23 ............................................................................................ 1043.85: M82628-29: H3003S101 ............................................................................................ 1053.86: M82628-29A: H3003S101 ......................................................................................... 1063.87: M82628-29B: H3003S101 .......................................................................................... 1073.88: M82628-30: A300401 ................................................................................................ 1083.89: M82628-30A: A300401 .............................................................................................. 1093.90: M82628-30B: A300401 .............................................................................................. 1103.91: M82628-31: A3011S101 ............................................................................................ 1113.92: M82628-31A: A3011S101 ......................................................................................... 1123.93: M82628-31B: A3011S101 .......................................................................................... 1133.94: M82628-32: 267MORSE-HA512 .............................................................................. 1143.95: M82628-32A: 267MORSE-HA512 ............................................................................ 1153.96: M82628-32B: 267MORSE-HA512 ............................................................................ 1163.97: M82628-33: K111701 ................................................................................................ 1173.98: M82628-33A: K111701 .............................................................................................. 1183.99: M82628-33B: K111701 .............................................................................................. 1193.100: M82628-34: L100201 ............................................................................................... 1203.101: M82628-34A: L100201 ............................................................................................ 1213.102: M82628-34B: L100201 ............................................................................................ 1223.103: M82628-35: L100524 ............................................................................................... 1233.104: M82628-35A: L100524 ............................................................................................ 1243.105: M82628-35B: L100524 ............................................................................................ 1253.106: M82628-36: L100824 ............................................................................................... 1263.107: M82628-36A: L100824 ............................................................................................ 1273.108: M82628-36B: L100824 ............................................................................................ 1283.109: M82628-37: L100824DUP ....................................................................................... 1293.110: M82628-37A: L100824DUP .................................................................................... 1303.111: M82628-37B: L100824DUP .................................................................................... 1313.112: M82628-38: K103801 .............................................................................................. 1323.113: M82628-38A: K103801 ............................................................................................ 1333.114: M82628-38B: K103801 ............................................................................................ 1343.115: M82628-39: C100424 ............................................................................................... 1353.116: M82628-39A: C100424 ............................................................................................ 1363.117: M82628-39B: C100424 ............................................................................................ 1373.118: M82628-40: R103102 ............................................................................................... 1383.119: M82628-40A: R103102 ............................................................................................ 1393.120: M82628-40B: R103102 ............................................................................................ 1403.121: M82628-41: M503002 .............................................................................................. 1413.122: M82628-41A: M503002 ........................................................................................... 1423.123: M82628-41B: M503002 ........................................................................................... 143

12

34

5

4 of 211

M82628


Sections:

3.124: M82628-42: S103924 ............................................................................................... 1443.125: M82628-42A: S103924 ............................................................................................ 1453.126: M82628-42B: S103924 ............................................................................................ 146

Section 4: Misc. Forms ............................................................................................................ 1474.1: Chain of Custody ........................................................................................................... 1484.2: RCP Form ...................................................................................................................... 1534.3: Sample Tracking Chronicle ........................................................................................... 154

Section 5: Metals Analysis - QC Data Summaries ................................................................ 1715.1: Prep QC MP13454: Pb .................................................................................................. 1725.2: Prep QC MP13455: Pb .................................................................................................. 1785.3: Prep QC MP13463: Pb .................................................................................................. 1825.4: Prep QC MP13464: Pb .................................................................................................. 1875.5: Prep QC MP13466: Pb .................................................................................................. 1915.6: Prep QC MP13473: Pb .................................................................................................. 1965.7: Prep QC MP13476: Pb .................................................................................................. 2005.8: Prep QC MP13487: Pb .................................................................................................. 2045.9: Prep QC MP13488: Pb .................................................................................................. 208

12

34

5

5 of 211

M82628

Accutest Laboratories

Sample Summary

Olin CorporationJob No:: M82628

Mactec: Olin-Newhall St.-Hamden, CTProject No: 6107090004/01

Sample Collected Matr ix Client

Number Date Time By Received Code Type Sample ID

M82628-1 05/04/09 10:05 MV 05/06/09 SO Soil SB-1324

M82628-1A 05/04/09 10:05 MV 05/06/09 SO Soil SB-1324

M82628-1B 05/04/09 10:05 MV 05/06/09 SO Soil SB-1324

M82628-2 05/04/09 10:10 MV 05/06/09 SO Soil SB-1404

M82628-2A 05/04/09 10:10 MV 05/06/09 SO Soil SB-1404

M82628-2B 05/04/09 10:10 MV 05/06/09 SO Soil SB-1404

M82628-3 05/04/09 11:00 MV 05/06/09 SO Soil P103901

M82628-3A 05/04/09 11:00 MV 05/06/09 SO Soil P103901

M82628-3B 05/04/09 11:00 MV 05/06/09 SO Soil P103901

M82628-4 05/04/09 11:12 MV 05/06/09 SO Soil P3001S301

M82628-4A 05/04/09 11:12 MV 05/06/09 SO Soil P3001S301

M82628-4B 05/04/09 11:12 MV 05/06/09 SO Soil P3001S301

M82628-5 05/04/09 11:25 MV 05/06/09 SO Soil P100524

Soil samples reported on a dry weight basis unless otherwise indicated on result page.

6 of 211

M82628

1


Sample Summary(continued)





M82628-5A 05/04/09 11:25 MV 05/06/09 SO Soil P100524

M82628-5B 05/04/09 11:25 MV 05/06/09 SO Soil P100524

M82628-6 05/04/09 11:55 MV 05/06/09 SO Soil F3006S201

M82628-6A 05/04/09 11:55 MV 05/06/09 SO Soil F3006S201

M82628-6B 05/04/09 11:55 MV 05/06/09 SO Soil F3006S201

M82628-7 05/04/09 12:10 MV 05/06/09 SO Soil WIN-106124

M82628-7A 05/04/09 12:10 MV 05/06/09 SO Soil WIN-106124

M82628-7B 05/04/09 12:10 MV 05/06/09 SO Soil WIN-106124

M82628-8 05/04/09 12:20 MV 05/06/09 SO Soil C100324

M82628-8A 05/04/09 12:20 MV 05/06/09 SO Soil C100324

M82628-8B 05/04/09 12:20 MV 05/06/09 SO Soil C100324

M82628-9 05/04/09 12:35 MV 05/06/09 SO Soil 124BT-HA512

M82628-9A 05/04/09 12:35 MV 05/06/09 SO Soil 124BT-HA512


7 of 211

M82628

1







M82628-9B 05/04/09 12:35 MV 05/06/09 SO Soil 124BT-HA512

M82628-10 05/04/09 12:45 MV 05/06/09 SO Soil 124BT-HA112

M82628-10A 05/04/09 12:45 MV 05/06/09 SO Soil 124BT-HA112

M82628-10B 05/04/09 12:45 MV 05/06/09 SO Soil 124BT-HA112

M82628-11 05/04/09 12:58 MV 05/06/09 SO Soil 95-MS01

M82628-11A 05/04/09 12:58 MV 05/06/09 SO Soil 95-MS01

M82628-11B 05/04/09 12:58 MV 05/06/09 SO Soil 95-MS01

M82628-12 05/04/09 14:40 MV 05/06/09 SO Soil F3002S101

M82628-12A 05/04/09 14:40 MV 05/06/09 SO Soil F3002S101

M82628-12B 05/04/09 14:40 MV 05/06/09 SO Soil F3002S101

M82628-13 05/04/09 15:00 MV 05/06/09 SO Soil 127MORSE-HA412

M82628-13A 05/04/09 15:00 MV 05/06/09 SO Soil 127MORSE-HA412

M82628-13B 05/04/09 15:00 MV 05/06/09 SO Soil 127MORSE-HA412


8 of 211

M82628

1













M82628-16 05/04/09 15:30 MV 05/06/09 SO Soil S104412

M82628-16A 05/04/09 15:30 MV 05/06/09 SO Soil S104412

M82628-16B 05/04/09 15:30 MV 05/06/09 SO Soil S104412

M82628-17 05/04/09 16:10 MV 05/06/09 SO Soil S105614

M82628-17A 05/04/09 16:10 MV 05/06/09 SO Soil S105614

M82628-17B 05/04/09 16:10 MV 05/06/09 SO Soil S105614

M82628-18 05/04/09 16:25 MV 05/06/09 SO Soil F3003S101


9 of 211

M82628

1







M82628-18A 05/04/09 16:25 MV 05/06/09 SO Soil F3003S101

M82628-18B 05/04/09 16:25 MV 05/06/09 SO Soil F3003S101

M82628-19 05/04/09 16:45 MV 05/06/09 SO Soil C100624

M82628-19A 05/04/09 16:45 MV 05/06/09 SO Soil C100624

M82628-19B 05/04/09 16:45 MV 05/06/09 SO Soil C100624

M82628-20 05/04/09 17:00 MV 05/06/09 SO Soil C3001S101

M82628-20A 05/04/09 17:00 MV 05/06/09 SO Soil C3001S101

M82628-20B 05/04/09 17:00 MV 05/06/09 SO Soil C3001S101

M82628-21 05/04/09 17:40 MV 05/06/09 SO Soil N101801

M82628-21A 05/04/09 17:40 MV 05/06/09 SO Soil N101801

M82628-21AD05/04/09 17:40 MV 05/06/09 SO Soil Dup/MSD N101801

M82628-21AS05/04/09 17:40 MV 05/06/09 SO Soil Matrix Spike N101801

M82628-21B 05/04/09 17:40 MV 05/06/09 SO Soil N101801


10 of 211

M82628

1







M82628-21BD05/04/09 17:40 MV 05/06/09 SO Soil Dup/MSD N101801

M82628-21BS 05/04/09 17:40 MV 05/06/09 SO Soil Matrix Spike N101801

M82628-21D 05/04/09 17:40 MV 05/06/09 SO Soil Dup/MSD N101801

M82628-21S 05/04/09 17:40 MV 05/06/09 SO Soil Matrix Spike N101801

M82628-22 05/04/09 17:40 MV 05/06/09 SO Soil N101801DUP

M82628-22A 05/04/09 17:40 MV 05/06/09 SO Soil N101801DUP

M82628-22B 05/04/09 17:40 MV 05/06/09 SO Soil N101801DUP

M82628-23 05/05/09 09:40 MV 05/06/09 SO Soil H3009S101

M82628-23A 05/05/09 09:40 MV 05/06/09 SO Soil H3009S101

M82628-23B 05/05/09 09:40 MV 05/06/09 SO Soil H3009S101

M82628-24 05/05/09 09:50 MV 05/06/09 SO Soil H3001S301

M82628-24A 05/05/09 09:50 MV 05/06/09 SO Soil H3001S301

M82628-24B 05/05/09 09:50 MV 05/06/09 SO Soil H3001S301


11 of 211

M82628

1







M82628-25 05/05/09 10:02 MV 05/06/09 SO Soil J101012

M82628-25A 05/05/09 10:02 MV 05/06/09 SO Soil J101012

M82628-25B 05/05/09 10:02 MV 05/06/09 SO Soil J101012

M82628-26 05/05/09 10:13 MV 05/06/09 SO Soil J100601

M82628-26A 05/05/09 10:13 MV 05/06/09 SO Soil J100601

M82628-26B 05/05/09 10:13 MV 05/06/09 SO Soil J100601

M82628-27 05/05/09 10:25 MV 05/06/09 SO Soil H100624

M82628-27A 05/05/09 10:25 MV 05/06/09 SO Soil H100624

M82628-27B 05/05/09 10:25 MV 05/06/09 SO Soil H100624

M82628-28 05/05/09 10:32 MV 05/06/09 SO Soil H2002S23

M82628-28A 05/05/09 10:32 MV 05/06/09 SO Soil H2002S23

M82628-28B 05/05/09 10:32 MV 05/06/09 SO Soil H2002S23

M82628-29 05/05/09 11:00 MV 05/06/09 SO Soil H3003S101


12 of 211

M82628

1







M82628-29A 05/05/09 11:00 MV 05/06/09 SO Soil H3003S101

M82628-29B 05/05/09 11:00 MV 05/06/09 SO Soil H3003S101

M82628-30 05/05/09 11:25 MV 05/06/09 SO Soil A300401

M82628-30A 05/05/09 11:25 MV 05/06/09 SO Soil A300401

M82628-30B 05/05/09 11:25 MV 05/06/09 SO Soil A300401

M82628-31 05/05/09 11:35 MV 05/06/09 SO Soil A3011S101

M82628-31A 05/05/09 11:35 MV 05/06/09 SO Soil A3011S101

M82628-31B 05/05/09 11:35 MV 05/06/09 SO Soil A3011S101




M82628-33 05/05/09 11:55 MV 05/06/09 SO Soil K111701

M82628-33A 05/05/09 11:55 MV 05/06/09 SO Soil K111701


13 of 211

M82628

1







M82628-33B 05/05/09 11:55 MV 05/06/09 SO Soil K111701

M82628-34 05/05/09 12:15 MV 05/06/09 SO Soil L100201

M82628-34A 05/05/09 12:15 MV 05/06/09 SO Soil L100201

M82628-34B 05/05/09 12:15 MV 05/06/09 SO Soil L100201

M82628-35 05/05/09 12:25 MV 05/06/09 SO Soil L100524

M82628-35A 05/05/09 12:25 MV 05/06/09 SO Soil L100524

M82628-35B 05/05/09 12:25 MV 05/06/09 SO Soil L100524

M82628-36 05/05/09 13:00 MV 05/06/09 SO Soil L100824

M82628-36A 05/05/09 13:00 MV 05/06/09 SO Soil L100824

M82628-36AD05/05/09 13:00 MV 05/06/09 SO Soil Dup/MSD L100824

M82628-36AS05/05/09 13:00 MV 05/06/09 SO Soil Matrix Spike L100824

M82628-36B 05/05/09 13:00 MV 05/06/09 SO Soil L100824

M82628-36BD05/05/09 13:00 MV 05/06/09 SO Soil Dup/MSD L100824


14 of 211

M82628

1







M82628-36BS 05/05/09 13:00 MV 05/06/09 SO Soil Matrix Spike L100824

M82628-36D 05/05/09 13:00 MV 05/06/09 SO Soil Dup/MSD L100824

M82628-36S 05/05/09 13:00 MV 05/06/09 SO Soil Matrix Spike L100824

M82628-37 05/05/09 13:00 MV 05/06/09 SO Soil L100824DUP

M82628-37A 05/05/09 13:00 MV 05/06/09 SO Soil L100824DUP

M82628-37B 05/05/09 13:00 MV 05/06/09 SO Soil L100824DUP

M82628-38 05/05/09 14:20 MV 05/06/09 SO Soil K103801

M82628-38A 05/05/09 14:20 MV 05/06/09 SO Soil K103801

M82628-38B 05/05/09 14:20 MV 05/06/09 SO Soil K103801

M82628-39 05/05/09 14:40 MV 05/06/09 SO Soil C100424

M82628-39A 05/05/09 14:40 MV 05/06/09 SO Soil C100424

M82628-39B 05/05/09 14:40 MV 05/06/09 SO Soil C100424

M82628-40 05/05/09 15:10 MV 05/06/09 SO Soil R103102


15 of 211

M82628

1







M82628-40A 05/05/09 15:10 MV 05/06/09 SO Soil R103102

M82628-40B 05/05/09 15:10 MV 05/06/09 SO Soil R103102

M82628-41 05/05/09 16:45 MV 05/06/09 SO Soil M503002

M82628-41A 05/05/09 16:45 MV 05/06/09 SO Soil M503002

M82628-41B 05/05/09 16:45 MV 05/06/09 SO Soil M503002

M82628-42 05/06/09 11:00 MV 05/06/09 SO Soil S103924

M82628-42A 05/06/09 11:00 MV 05/06/09 SO Soil S103924

M82628-42B 05/06/09 11:00 MV 05/06/09 SO Soil S103924


16 of 211

M82628

1

42 Sample(s) were collected on 05/04/2009 and were received at Accutest on 05/06/2009 properly preserved, at 2.3 Deg. C and

intact. These Samples received an Accutest job number of M82628. A listing of the Laboratory Sample ID, Client Sample ID and

dates of collection are presented in the Results Summary Section of this report.

Except as noted below, all method specified calibrations and quality control performance criteria were met for this job. For more

information, please refer to QC summary pages.

Client: Olin Corporation

Site: Mactec: Olin-Newhall St.-Hamden, CT

Job No M82628

Repor t Date 5/20/2009 9:47:06 AM

SAMPLE DELIVERY GROUP CASE NARRATIVE

Metals By Method SW846 6010B

Matr ix LEACHATE Batch ID: MP13455

All samples were digested within the recommended method holding time.

All samples were analyzed within the recommended method holding time.

All method blanks for this batch meet method specific criteria.

Sample(s) M82628-21ADUP, M82628-21AMS, M82628-21ASDL were used as the QC samples for metals.

Only Lead requested.





Sample(s) M82293-9TDUP, M82293-9TMS, M82293-9TSDL were used as the QC samples for metals.

RPD(s) for Serial Dilution for Lead are outside control limits for sample MP13464-SD1. Percent difference acceptable due to

low initial sample concentration (< 50 times IDL).






Sample(s) M82628-21BDUP, M82628-21BSDL, M82628-21BMS were used as the QC samples for metals.

Matrix Spike Recovery(s) for Lead are outside control limits. Spike recovery indicates possible matrix interference.











Wednesday, May 20, 2009 P age 1 of 3

17 of 211

M82628

2










Sample(s) M82628-36BDUP, M82628-36BMS, M82628-36BSDL were used as the QC samples for metals.


Matr ix SO Batch ID: MP13454




Sample(s) M82628-21DUP, M82628-21PS, M82628-21SDL, M82628-21MS were used as the QC samples for metals.

Matrix Spike Recovery(s) for Lead are outside control limits. Spike recovery indicates possible matrix interference and/or sample

nonhomogeneity.Post spike within acceptable range.






Sample(s) M82628-36DUP, M82628-36MS, M82628-36SDL were used as the QC samples for metals.









18 of 211

M82628

2

Wet Chemistry By Method SM21 2540 B MOD.

Matr ix SO Batch ID: GN28851

Sample(s) M82628-21DUP were used as the QC samples for Solids, Percent.







No specific RLs requested.

Note: Compounds whose reported QC limits are outside the CT Recommended Reasonable Confidence Protocol QC criteria are

QC criteria but exceed the RCP criteria (compounds exceeding Accutest QC criteria are flagged on the QC summary). Refer to

the QC summary pages.

Unless otherwise noted, sample dilutions are performed in order to report the result within the calibration range.

The Accutest Laboratories of New England certifies that all analysis were performed within method specification. It is further

recommended that this report to be used in its entirety.The Accutest Laboratories of NE, Laboratory Director or assignee as verified

by the signature on the cover page has authorized the release of this report(M82628).


19 of 211

M82628

2


Sample Results

Report of Analysis

Section 3

20 of 211

M82628

3


Report of Analysis Page 1 of 1

Client Sample ID: SB-1324

Lab Sample ID: M82628-1 Date Sampled: 05/04/09

Matrix: SO - Soil Date Received: 05/06/09

Percent Solids: 91.0

Project: Mactec: Olin-Newhall St.-Hamden, CT

Metals Analysis

Analyte Result RL Units DF Prep Analyzed By Method Prep Method

Lead 40.8 2.1 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2

(1) Instrument QC Batch: MA10450

(2) Prep QC Batch: MP13454

RL = Reporting Limit

21 of 211

M82628

33.1




Lab Sample ID: M82628-1A Date Sampled: 05/04/09




Metals Analysis, SPLP Leachate SW846 1312

Analyte Result MCL RL Units DF Prep Analyzed By Method Prep Method

Lead 0.051 0.010 mg/l 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3010A 2




MCL = Maximum Contamination Level (not available)

22 of 211

M82628

33.2




Lab Sample ID: M82628-1B Date Sampled: 05/04/09




Metals Analysis, TCLP Leachate SW846 1311

Analyte Result HW# MCL RL Units DF Prep Analyzed By Method Prep Method

Lead 0.097 D008 5.0 0.010 mg/l 1 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2




MCL = Maximum Contamination Level (40 CFR 261 6/96)

23 of 211

M82628

33.3








Metals Analysis


Lead 8470 21 mg/kg 10 05/08/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2




24 of 211

M82628

33.4






Percent Solids: n/a









25 of 211

M82628

33.5






Percent Solids: n/a




Lead 203 D008 5.0 0.50 mg/l 50 05/15/09 05/18/09 EAL SW846 6010B 1 SW846 3010A 2





26 of 211

M82628

33.6



Client Sample ID: P103901





Metals Analysis


Lead 160 2.0 mg/kg 1 05/08/09 05/11/09 PY SW846 6010B 1 SW846 3050B 2




27 of 211

M82628

33.7















28 of 211

M82628

33.8















29 of 211

M82628

33.9



Client Sample ID: P3001S301





Metals Analysis






30 of 211

M82628

33.10















31 of 211

M82628

33.11















32 of 211

M82628

33.12








Metals Analysis






33 of 211

M82628

33.13















34 of 211

M82628

33.14















35 of 211

M82628

33.15



Client Sample ID: F3006S201





Metals Analysis






36 of 211

M82628

33.16















37 of 211

M82628

33.17















38 of 211

M82628

33.18



Client Sample ID: WIN-106124





Metals Analysis






39 of 211

M82628

33.19















40 of 211

M82628

33.20















41 of 211

M82628

33.21



Client Sample ID: C100324





Metals Analysis






42 of 211

M82628

33.22















43 of 211

M82628

33.23















44 of 211

M82628

33.24



Client Sample ID: 124BT-HA512





Metals Analysis






45 of 211

M82628

33.25










Lead < 0.010 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2





46 of 211

M82628

33.26















47 of 211

M82628

33.27








Metals Analysis






48 of 211

M82628

33.28










Lead 0.031 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2





49 of 211

M82628

33.29















50 of 211

M82628

33.30



Client Sample ID: 95-MS01





Metals Analysis






51 of 211

M82628

33.31















52 of 211

M82628

33.32















53 of 211

M82628

33.33








Metals Analysis






54 of 211

M82628

33.34















55 of 211

M82628

33.35















56 of 211

M82628

33.36



Client Sample ID: 127MORSE-HA412





Metals Analysis






57 of 211

M82628

33.37















58 of 211

M82628

33.38















59 of 211

M82628

33.39








Metals Analysis






60 of 211

M82628

33.40










Lead < 0.010 0.010 mg/l 1 05/12/09 05/12/09 EAL SW846 6010B 1 SW846 3010A 2





61 of 211

M82628

33.41















62 of 211

M82628

33.42








Metals Analysis






63 of 211

M82628

33.43















64 of 211

M82628

33.44















65 of 211

M82628

33.45



Client Sample ID: S104412





Metals Analysis






66 of 211

M82628

33.46















67 of 211

M82628

33.47















68 of 211

M82628

33.48








Metals Analysis






69 of 211

M82628

33.49















70 of 211

M82628

33.50















71 of 211

M82628

33.51








Metals Analysis






72 of 211

M82628

33.52















73 of 211

M82628

33.53















74 of 211

M82628

33.54








Metals Analysis






75 of 211

M82628

33.55















76 of 211

M82628

33.56















77 of 211

M82628

33.57



Client Sample ID: C3001S101





Metals Analysis


Lead 980 2.3 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2




78 of 211

M82628

33.58















79 of 211

M82628

33.59















80 of 211

M82628

33.60



Client Sample ID: N101801





Metals Analysis






81 of 211

M82628

33.61















82 of 211

M82628

33.62















83 of 211

M82628

33.63



Client Sample ID: N101801DUP





Metals Analysis






84 of 211

M82628

33.64















85 of 211

M82628

33.65















86 of 211

M82628

33.66



Client Sample ID: H3009S101





Metals Analysis






87 of 211

M82628

33.67















88 of 211

M82628

33.68















89 of 211

M82628

33.69








Metals Analysis






90 of 211

M82628

33.70















91 of 211

M82628

33.71















92 of 211

M82628

33.72



Client Sample ID: J101012





Metals Analysis






93 of 211

M82628

33.73















94 of 211

M82628

33.74















95 of 211

M82628

33.75








Metals Analysis






96 of 211

M82628

33.76















97 of 211

M82628

33.77















98 of 211

M82628

33.78



Client Sample ID: H100624





Metals Analysis






99 of 211

M82628

33.79















100 of 211

M82628

33.80










Lead 147 D008 5.0 0.20 mg/l 20 05/13/09 05/14/09 EAL SW846 6010B 1 SW846 3010A 2





101 of 211

M82628

33.81








Metals Analysis






102 of 211

M82628

33.82















103 of 211

M82628

33.83















104 of 211

M82628

33.84








Metals Analysis






105 of 211

M82628

33.85















106 of 211

M82628

33.86















107 of 211

M82628

33.87



Client Sample ID: A300401





Metals Analysis






108 of 211

M82628

33.88















109 of 211

M82628

33.89















110 of 211

M82628

33.90



Client Sample ID: A3011S101





Metals Analysis


Lead 75.2 2.1 mg/kg 1 05/11/09 05/12/09 EAL SW846 6010B 1 SW846 3050B 2




111 of 211

M82628

33.91















112 of 211

M82628

33.92















113 of 211

M82628

33.93








Metals Analysis






114 of 211

M82628

33.94















115 of 211

M82628

33.95















116 of 211

M82628

33.96



Client Sample ID: K111701





Metals Analysis






117 of 211

M82628

33.97















118 of 211

M82628

33.98















119 of 211

M82628

33.99



Client Sample ID: L100201





Metals Analysis






120 of 211

M82628

33.100















121 of 211

M82628

33.101















122 of 211

M82628

33.102








Metals Analysis






123 of 211

M82628

33.103















124 of 211

M82628

33.104















125 of 211

M82628

33.105








Metals Analysis






126 of 211

M82628

33.106















127 of 211

M82628

33.107















128 of 211

M82628

33.108



Client Sample ID: L100824DUP





Metals Analysis






129 of 211

M82628

33.109















130 of 211

M82628

33.110















131 of 211

M82628

33.111








Metals Analysis






132 of 211

M82628

33.112















133 of 211

M82628

33.113















134 of 211

M82628

33.114








Metals Analysis






135 of 211

M82628

33.115















136 of 211

M82628

33.116















137 of 211

M82628

33.117



Client Sample ID: R103102





Metals Analysis






138 of 211

M82628

33.118















139 of 211

M82628

33.119















140 of 211

M82628

33.120



Client Sample ID: M503002





Metals Analysis






141 of 211

M82628

33.121















142 of 211

M82628

33.122















143 of 211

M82628

33.123








Metals Analysis






144 of 211

M82628

33.124















145 of 211

M82628

33.125















146 of 211

M82628

33.126


Misc. Forms

Custody Documents and Other Forms

Includes the following where applicable:

• Certification Exceptions

• Certification Exceptions (CT)

• Chain of Custody

• RCP Form

• Sample Tracking Chronicle

Section 4

147 of 211

M82628

4

M82628: Chain of CustodyPage 1 of 5

148 of 211

M82628

44.1


149 of 211

M82628

44.1


150 of 211

M82628

44.1


151 of 211

M82628

44.1


152 of 211

M82628

44.1

Laboratory Name: Client:

Project Location: Project Number:

Sampling Date(s):

Laboratory Sample ID(s):

Methods:

1 Yes No

1A Yes No

1B Yes No

NA

2 Yes No

3 Yes No

4 Yes No

5 Yes No

Yes No

6 Yes No

7 Yes No

Authorized

Signature: Position: Lab Director

Printed Name: Reza Tand Date:

Accutest New England

5/20/2009

Reasonable Confidence Protocol

Where all the method specified preservation and holding time requirements met?

VPH and EPH mehods only: Was the VPH or EPH method conducted without

significant modifications (See section 11.3 of respective methods)

I, the undersigned, attest under pains and penalties of perjury that, to the best of my knowledge and belief

and based upon my personal inquiry of those responsible for providing the information contained in this

analytical report, such information is accurate and complete.

Were all QA/QC performance criteria specified in the CTDEP Reasonable

Confidence Protocol documents achieved?

EPA 160.3 M, SM21 2540 B MOD., SW846 6010B

For each analytical method referenced in this laboratory report package, were all

specified QA/QC performance criteria followed, including the requirement to explain any

criteria falling outside of acceptable guidelines, as specified in the CTDEP method-

specific Reasonable Confidence Protocol

documents)?

Were all samples received by the laboratory in a condition consistent with

that described on the associated chain-of-custody document(s)?

Laboratory Analysis

Reza Tand

a) Were reporting limits specified or referenced on the chain-of-custody?

b) Were these reporting limits met?

For each analytical method referenced in this laboratory report package,

were results reported for all constituents identified in the method-specific

analyte lists presented in the Reasonable Confidence Protocol documents?

Are project-specific matrix spikes and laboratory duplicates included in this

data set?

Note: For all questions to which the response was "No" (with the exception of question #7), additional

information must be provided in an attached narrative. If the answer to question #1, #1A or #1B is "No" , the

data package does not meet the requirements for "Reasonable Confidence" .

QA/QC Certification Form


M82628-1 through M82628-42

5/4/2009

Olin Corporation

6107090004/01Mactec: Olin-Newhall St.-Hamden, CT

153 of 211

M82628

44.2


Internal Sample Tracking Chronicle

Olin CorporationJob No: M82628


Sample

Number Method Analyzed By Prepped By Test Codes

M82628-1 Collected: 04-MAY-09 10:05 By: MV Received: 06-MAY-09 By:

SB-1324

M82628-1 SM21 2540 B MOD. 11-MAY-09 NJ %SOL

M82628-1 SW846 6010B 11-MAY-09 16:28 PY 08-MAY-09 PY PB


SB-1404


M82628-2 SW846 6010B 12-MAY-09 13:00 EAL 08-MAY-09 PY PB


P103901




P3001S301




P100524




F3006S201




WIN-106124


Page 1 of 17

154 of 211

M82628

44.3





Sample




C100324




124BT-HA512




124BT-HA112




95-MS01




F3002S101




127MORSE-HA412



Page 2 of 17

155 of 211

M82628

44.3





Sample



127MORSE-HA112




127MORSE-HA212




S104412




S105614




F3003S101




C100624



M82628-1A Collected: 04-MAY-09 10:05 By: MV Received: 06-MAY-09 By:

SB-1324

Page 3 of 17

156 of 211

M82628

44.3





Sample


M82628-1A SW846 6010B 11-MAY-09 23:55 PY 08-MAY-09 PY EPB

M82628-1B Collected: 04-MAY-09 10:05 By: MV Received: 06-MAY-09 By:

SB-1324

M82628-1B SW846 6010B 18-MAY-09 11:30 EAL 15-MAY-09 PY EPB


C3001S101




N101801




N101801DUP




H3009S101




H3001S301




J101012

Page 4 of 17

157 of 211

M82628

44.3





Sample





J100601




H100624




H2002S23




H3003S101




SB-1404



SB-1404



A300401

Page 5 of 17

158 of 211

M82628

44.3





Sample





A3011S101




267MORSE-HA512




K111701




L100201




L100524




L100824



Page 6 of 17

159 of 211

M82628

44.3





Sample



L100824DUP




K103801




C100424




P103901



P103901



R103102




M503002



Page 7 of 17

160 of 211

M82628

44.3





Sample



S103924




P3001S301



P3001S301



P100524



P100524



F3006S201



F3006S201



WIN-106124

Page 8 of 17

161 of 211

M82628

44.3





Sample




WIN-106124



C100324



C100324



124BT-HA512

M82628-9A SW846 6010B 12-MAY-09 14:34 EAL 12-MAY-09 PY EPB


124BT-HA512


M82628-10ACollected: 04-MAY-09 12:45 By: MV Received: 06-MAY-09 By:

124BT-HA112

M82628-10ASW846 6010B 12-MAY-09 14:50 EAL 12-MAY-09 PY EPB

M82628-10BCollected: 04-MAY-09 12:45 By: MV Received: 06-MAY-09 By:

124BT-HA112

M82628-10BSW846 6010B 14-MAY-09 11:29 EAL 13-MAY-09 PY EPB


95-MS01

Page 9 of 17

162 of 211

M82628

44.3





Sample




95-MS01



F3002S101



F3002S101



127MORSE-HA412



127MORSE-HA412



127MORSE-HA112



127MORSE-HA112



127MORSE-HA212

Page 10 of 17

163 of 211

M82628

44.3





Sample




127MORSE-HA212



S104412



S104412



S105614



S105614



F3003S101



F3003S101



C100624

Page 11 of 17

164 of 211

M82628

44.3





Sample




C100624



C3001S101



C3001S101



N101801

M82628-21ASW846 6010B 11-MAY-09 22:28 PY 08-MAY-09 PY EPB


N101801



N101801DUP

M82628-22ASW846 6010B 12-MAY-09 00:49 PY 08-MAY-09 PY EPB


N101801DUP



H3009S101

Page 12 of 17

165 of 211

M82628

44.3





Sample




H3009S101



H3001S301



H3001S301



J101012



J101012



J100601



J100601



H100624

Page 13 of 17

166 of 211

M82628

44.3





Sample




H100624



H2002S23



H2002S23



H3003S101

M82628-29ASW846 6010B 18-MAY-09 13:45 EAL 14-MAY-09 EAL EPB


H3003S101



A300401



A300401



A3011S101

Page 14 of 17

167 of 211

M82628

44.3





Sample




A3011S101



267MORSE-HA512



267MORSE-HA512



K111701



K111701



L100201



L100201



L100524

Page 15 of 17

168 of 211

M82628

44.3





Sample




L100524



L100824



L100824



L100824DUP



L100824DUP



K103801



K103801



C100424

Page 16 of 17

169 of 211

M82628

44.3





Sample




C100424



R103102



R103102



M503002



M503002



S103924



S103924


Page 17 of 17

170 of 211

M82628

44.3


Metals Analysis

QC Data Summaries


• Method Blank Summaries

• Matrix Spike and Duplicate Summaries

• Blank Spike and Lab Control Sample Summaries

• Serial Dilution Summaries

Section 5

171 of 211

M82628

5

BLANK RESULTS SUMMARY Part 2 - Method Blanks

Login Number: M82628 Account: OLINTN - Olin Corporation


QC Batch ID: MP13454 Methods: SW846 6010B Matrix Type: SOLID Units: mg/kg

Prep Date: 05/08/09

MBMetal RL IDL MDL raw final

Aluminum 20 .86 2.1

Antimony 2.0 .16 .41

Arsenic 2.0 .23 .29

Barium 20 .06 .26

Beryllium 0.40 .015 .022

Boron 10 .13 .31

Cadmium 0.40 .022 .024

Calcium 500 .62 .74

Chromium 1.0 .072 .14

Cobalt 5.0 .054 .079

Copper 2.5 .064 .11

Iron 10 .66 2.5

Lead 2.0 .11 .16 0.19 <2.0

Magnesium 500 .51 .6

Manganese 1.5 .018 .031

Molybdenum 10 .088 .12

Nickel 4.0 .061 .13

Potassium 500 1.5 8.1

Selenium 2.0 .26 .34

Silver 0.50 .054 .076

Sodium 500 7.7 19

Strontium 1.0 .012 .022

Thallium 2.0 .29 .33

Tin 10 .4 .55

Titanium 5.0 .059 .5

Vanadium 3.0 .24 .26

Zinc 2.0 .061 .17

Associated samples MP13454: M82628-1, M82628-2, M82628-3, M82628-4, M82628-5, M82628-6, M82628-7, M82628-8, M82628-9, M82628-10, M82628-11, M82628-12, M82628-13, M82628-14, M82628-15, M82628-16, M82628-17,M82628-18, M82628-19, M82628-21

Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested

_________________________________________________________________________________________________________

Page 1

172 of 211

M82628

55.1.1

MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY




Prep Date: 05/08/09 05/08/09

M82628-21 Spikelot QC M82628-21 QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits

Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 359 397 104 36.7 (a) 75-125 359 307 15.6 0-20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) Spike recovery indicates possible matrix interference and/or sample nonhomogeneity.Post spike within

acceptable range.

_________________________________________________________________________________________________________

Page 1

173 of 211

M82628

55.1.2

SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY




Prep Date: 05/08/09 05/08/09

BSP Spikelot QC BSD Spikelot BSD QCMetal Result MPICP % Rec Limits Result MPICP % Rec RPD Limit

Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 96.9 100 96.9 80-120 96.0 100 96.0 0.9 20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

174 of 211

M82628

55.1.3





Prep Date: 05/08/09

LCS Spikelot QCMetal Result MPLCS63 % Rec Limits

Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 201 223 90.1 82-118

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 2

175 of 211

M82628

55.1.3

SERIAL DILUTION RESULTS SUMMARY



QC Batch ID: MP13454 Methods: SW846 6010B Matrix Type: SOLID Units: ug/l

Prep Date: 05/08/09

M82628-21 QCMetal Original SDL 1:5 %DIF Limits

Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 3400 3590 5.6 0-10

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

176 of 211

M82628

55.1.4

POST DIGESTATE SPIKE SUMMARY




Prep Date: 05/08/09

Sample Final M82628-21 PS Spike Spike Spike QCMetal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits

Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 9.9 10 3399.98 3365.98 9338 .1 680 6800 87.8 -

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(**) Corr. sample result = Raw * (sample volume / final volume)(anr) Analyte not requested

_________________________________________________________________________________________________________

Page 1

177 of 211

M82628

55.1.5




QC Batch ID: MP13455 Methods: SW846 6010B Matrix Type: LEACHATE Units: mg/l

Prep Date: 05/08/09


Aluminum 0.20 .0086 .031

Antimony 0.0060 .0016 .003

Arsenic 0.025 .0023 .0032

Barium 0.50 .0006 .0012

Beryllium 0.0040 .00015 .0003

Boron 0.10 .0013 .0048

Cadmium 0.0040 .00022 .0003

Calcium 5.0 .0062 .04

Chromium 0.010 .00072 .0014

Cobalt 0.050 .00054 .001

Copper 0.025 .00064 .0018

Iron 0.10 .0066 .029

Lead 0.010 .0011 .0018 0.0010 <0.010

Magnesium 5.0 .0051 .01

Manganese 0.015 .00018 .0013

Molybdenum 0.10 .00088 .0014

Nickel 0.040 .00061 .001

Potassium 5.0 .015 .031

Selenium 0.025 .0026 .0033

Silver 0.0050 .00054 .0007

Sodium 5.0 .077 .21

Strontium 0.010 .00012 .0003

Thallium 0.0050 .0029 .0045

Tin 0.10 .004 .0099

Titanium 0.050 .00059 .0051

Vanadium 0.030 .0024 .0035

Zinc 0.10 .00061 .0013

Associated samples MP13455: M82628-1A, M82628-2A, M82628-3A, M82628-4A, M82628-5A, M82628-6A, M82628-7A,M82628-8A, M82628-21A, M82628-22A


_________________________________________________________________________________________________________

Page 1

178 of 211

M82628

55.2.1





Prep Date: 05/08/09 05/08/09

M82628-21A Spikelot QC M82628-21A QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits

Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 0.066 1.1 1.0 103.4 75-125 0.066 0.066 0.0 0-20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested

_________________________________________________________________________________________________________

Page 1

179 of 211

M82628

55.2.2





Prep Date: 05/08/09 05/08/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 1.0 1.0 100.0 80-120 1.0 1.0 100.0 0.0 20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

180 of 211

M82628

55.2.3




QC Batch ID: MP13455 Methods: SW846 6010B Matrix Type: LEACHATE Units: ug/l

Prep Date: 05/08/09

M82628-21A QCMetal Original SDL 1:5 %DIF Limits

Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 66.0 72.5 9.9 0-10

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

181 of 211

M82628

55.2.4





Prep Date: 05/11/09


Aluminum 20 .86 2.1


Arsenic 2.0 .23 .29

Barium 20 .06 .26

Beryllium 0.40 .015 .022

Boron 10 .13 .31

Cadmium 0.40 .022 .024

Calcium 500 .62 .74

Chromium 1.0 .072 .14

Cobalt 5.0 .054 .079

Copper 2.5 .064 .11

Iron 10 .66 2.5

Lead 2.0 .11 .16 0.24 <2.0


Manganese 1.5 .018 .031


Nickel 4.0 .061 .13



Silver 0.50 .054 .076

Sodium 500 7.7 19

Strontium 1.0 .012 .022


Tin 10 .4 .55



Zinc 2.0 .061 .17

Associated samples MP13463: M82628-20, M82628-22, M82628-23, M82628-24, M82628-25, M82628-26, M82628-27,M82628-28, M82628-29, M82628-30, M82628-31, M82628-32, M82628-33, M82628-34, M82628-35, M82628-36,M82628-37, M82628-38, M82628-39, M82628-40


_________________________________________________________________________________________________________

Page 1

182 of 211

M82628

55.3.1





Prep Date: 05/11/09 05/11/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 429 525 108 89.3 75-125 429 486 12.5 0-20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

183 of 211

M82628

55.3.2





Prep Date: 05/11/09 05/11/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 94.9 100 94.9 80-120 95.3 100 95.3 0.4 20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

184 of 211

M82628

55.3.3





Prep Date: 05/11/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 213 223 95.5 82-118

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 2

185 of 211

M82628

55.3.3





Prep Date: 05/11/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 3950 4090 3.5 0-10

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

186 of 211

M82628

55.3.4





Prep Date: 05/12/09


Aluminum 0.20 .0086 .031

Antimony 0.0060 .0016 .003

Arsenic 0.025 .0023 .0032

Barium 0.50 .0006 .0012

Beryllium 0.0040 .00015 .0003

Boron 0.10 .0013 .0048

Cadmium 0.0040 .00022 .0003

Calcium 5.0 .0062 .04

Chromium 0.010 .00072 .0014

Cobalt 0.050 .00054 .001

Copper 0.025 .00064 .0018

Iron 0.10 .0066 .029

Lead 0.010 .0011 .0018 0.0015 <0.010

Magnesium 5.0 .0051 .01

Manganese 0.015 .00018 .0013

Molybdenum 0.10 .00088 .0014

Nickel 0.040 .00061 .001

Potassium 5.0 .015 .031

Selenium 0.025 .0026 .0033

Silver 0.0050 .00054 .0007

Sodium 5.0 .077 .21

Strontium 0.010 .00012 .0003

Thallium 0.0050 .0029 .0045

Tin 0.10 .004 .0099

Titanium 0.050 .00059 .0051

Vanadium 0.030 .0024 .0035

Zinc 0.10 .00061 .0013

Associated samples MP13464: M82628-9A, M82628-10A, M82628-11A, M82628-12A, M82628-13A, M82628-14A,M82628-15A, M82628-16A, M82628-17A, M82628-18A, M82628-19A, M82628-20A, M82628-23A, M82628-24A, M82628-25A, M82628-26A, M82628-27A, M82628-28A


_________________________________________________________________________________________________________

Page 1

187 of 211

M82628

55.4.1





Prep Date: 05/12/09 05/12/09

M82293-9T Spikelot QC M82293-9T QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits

Aluminum

Antimony

Arsenic anr

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium anr

Cobalt

Copper anr

Iron

Lead 0.0043 1.0 1.0 99.6 75-125 0.0043 0.0043 0.0 0-20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium anr

Zinc



_________________________________________________________________________________________________________

Page 1

188 of 211

M82628

55.4.2





Prep Date: 05/12/09 05/12/09


Aluminum

Antimony

Arsenic anr

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium anr

Cobalt

Copper anr

Iron

Lead 0.96 1.0 96.0 80-120 1.0 1.0 100.0 4.1 20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium anr

Zinc



_________________________________________________________________________________________________________

Page 1

189 of 211

M82628

55.4.3





Prep Date: 05/12/09

M82293-9T QCMetal Original SDL 1:5 %DIF Limits

Aluminum

Antimony

Arsenic anr

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium anr

Cobalt

Copper anr

Iron

Lead 4.28 6.94 62.1 (a) 0-10

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium anr

Zinc


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).

_________________________________________________________________________________________________________

Page 1

190 of 211

M82628

55.4.4





Prep Date: 05/12/09


Aluminum 20 .86 2.1


Arsenic 2.0 .23 .29

Barium 20 .06 .26

Beryllium 0.40 .015 .022

Boron 10 .13 .31

Cadmium 0.40 .022 .024

Calcium 500 .62 .74

Chromium 1.0 .072 .14

Cobalt 5.0 .054 .079

Copper 2.5 .064 .11

Iron 10 .66 2.5

Lead 2.0 .11 .16 -0.023 <2.0


Manganese 1.5 .018 .031


Nickel 4.0 .061 .13



Silver 0.50 .054 .076

Sodium 500 7.7 19

Strontium 1.0 .012 .022


Tin 10 .4 .55



Zinc 2.0 .061 .17

Associated samples MP13466: M82628-41, M82628-42


_________________________________________________________________________________________________________

Page 1

191 of 211

M82628

55.5.1





Prep Date: 05/12/09 05/12/09


Aluminum

Antimony

Arsenic anr

Barium anr

Beryllium

Boron

Cadmium anr

Calcium

Chromium anr

Cobalt

Copper anr

Iron

Lead 23.5 116 98.4 94.0 75-125 23.5 23.8 1.3 0-20

Magnesium

Manganese

Molybdenum

Nickel anr

Potassium

Selenium anr

Silver anr

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc anr



_________________________________________________________________________________________________________

Page 1

192 of 211

M82628

55.5.2





Prep Date: 05/12/09 05/12/09


Aluminum

Antimony

Arsenic anr

Barium anr

Beryllium

Boron

Cadmium anr

Calcium

Chromium anr

Cobalt

Copper anr

Iron

Lead 97.9 100 97.9 80-120 95.4 100 95.4 2.6 20

Magnesium

Manganese

Molybdenum

Nickel anr

Potassium

Selenium anr

Silver anr

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc anr



_________________________________________________________________________________________________________

Page 1

193 of 211

M82628

55.5.3





Prep Date: 05/12/09


Aluminum

Antimony

Arsenic anr

Barium anr

Beryllium

Boron

Cadmium anr

Calcium

Chromium anr

Cobalt

Copper anr

Iron

Lead 209 223 93.7 82-118

Magnesium

Manganese

Molybdenum

Nickel anr

Potassium

Selenium anr

Silver anr

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc anr



_________________________________________________________________________________________________________

Page 2

194 of 211

M82628

55.5.3





Prep Date: 05/12/09


Aluminum

Antimony

Arsenic anr

Barium anr

Beryllium

Boron

Cadmium anr

Calcium

Chromium anr

Cobalt

Copper anr

Iron

Lead 235 244 3.7 0-10

Magnesium

Manganese

Molybdenum

Nickel anr

Potassium

Selenium anr

Silver anr

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc anr



_________________________________________________________________________________________________________

Page 1

195 of 211

M82628

55.5.4





Prep Date: 05/13/09


Aluminum 0.20 .014 .031

Antimony 0.0060 .0029 .003

Arsenic 0.025 .0027 .0032

Barium 0.50 .00064 .0012

Beryllium 0.0040 .00017 .0003

Boron 0.10 .0023 .0048

Cadmium 0.0040 .00024 .0003

Calcium 5.0 .0047 .04

Chromium 0.010 .00051 .0014

Cobalt 0.050 .00076 .001

Copper 0.025 .0011 .0018

Iron 0.10 .011 .029

Lead 0.010 .0013 .0018 -0.00018 <0.010

Magnesium 5.0 .008 .01

Manganese 0.015 .00017 .0013

Molybdenum 0.10 .0005 .0014

Nickel 0.040 .00065 .001

Potassium 5.0 .025 .031

Selenium 0.025 .0016 .0033

Silver 0.0050 .00064 .0007

Sodium 5.0 .099 .21

Strontium 0.010 .00012 .0003

Thallium 0.0050 .002 .0045

Tin 0.10 .0016 .0099

Titanium 0.050 .0041 .0051

Tungsten 0.10 .0054 .007

Vanadium 0.030 .00065 .0035

Zinc 0.10 .0011 .0013

Associated samples MP13473: M82628-9B, M82628-10B, M82628-11B, M82628-12B, M82628-13B, M82628-14B,M82628-15B, M82628-16B, M82628-17B, M82628-18B, M82628-19B, M82628-20B, M82628-21B, M82628-22B, M82628-23B, M82628-24B, M82628-25B, M82628-26B, M82628-27B, M82628-28B


_________________________________________________________________________________________________________

Page 1

196 of 211

M82628

55.6.1





Prep Date: 05/13/09 05/13/09

M82628-21B Spikelot QC M82628-21B QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits

Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 2.8 3.5 1.0 70.0 (a) 75-125 2.8 2.8 0.0 0-20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) Spike recovery indicates possible matrix interference.

_________________________________________________________________________________________________________

Page 1

197 of 211

M82628

55.6.2





Prep Date: 05/13/09 05/13/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 1.0 1.0 100.0 80-120 0.99 1.0 99.0 1.0 20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

198 of 211

M82628

55.6.3





Prep Date: 05/13/09

M82628-21B QCMetal Original SDL 1:5 %DIF Limits

Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 2780 2770 0.4 0-10

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

199 of 211

M82628

55.6.4





Prep Date: 05/14/09


Aluminum 0.20 .014 .031

Antimony 0.0060 .0029 .003

Arsenic 0.025 .0027 .0032

Barium 0.50 .00064 .0012

Beryllium 0.0040 .00017 .0003

Boron 0.10 .0023 .0048

Cadmium 0.0040 .00024 .0003

Calcium 5.0 .0047 .04

Chromium 0.010 .00051 .0014

Cobalt 0.050 .00076 .001

Copper 0.025 .0011 .0018

Iron 0.10 .011 .029

Lead 0.010 .0013 .0018 0.00011 <0.010


Manganese 0.015 .00017 .0013

Molybdenum 0.10 .0005 .0014

Nickel 0.040 .00065 .001

Potassium 5.0 .025 .031

Selenium 0.025 .0016 .0033

Silver 0.0050 .00064 .0007

Sodium 5.0 .099 .21

Strontium 0.010 .00012 .0003

Thallium 0.0050 .002 .0045

Tin 0.10 .0016 .0099

Titanium 0.050 .0041 .0051

Tungsten 0.10 .0054 .007

Vanadium 0.030 .00065 .0035

Zinc 0.10 .0011 .0013

Associated samples MP13476: M82628-29A, M82628-30A, M82628-31A, M82628-32A, M82628-33A, M82628-34A,M82628-35A, M82628-36A, M82628-37A, M82628-38A, M82628-39A, M82628-40A, M82628-41A, M82628-42A


_________________________________________________________________________________________________________

Page 1

200 of 211

M82628

55.7.1





Prep Date: 05/14/09 05/14/09


Aluminum

Antimony

Arsenic anr

Barium

Beryllium

Boron

Cadmium anr

Calcium

Chromium anr

Cobalt

Copper anr

Iron

Lead 0.099 1.2 1.0 110.1 75-125 0.099 0.10 1.0 0-20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

201 of 211

M82628

55.7.2





Prep Date: 05/14/09 05/14/09


Aluminum

Antimony

Arsenic anr

Barium

Beryllium

Boron

Cadmium anr

Calcium

Chromium anr

Cobalt

Copper anr

Iron

Lead 1.0 1.0 100.0 80-120 1.0 1.0 100.0 0.0 20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

202 of 211

M82628

55.7.3





Prep Date: 05/14/09


Aluminum

Antimony

Arsenic anr

Barium

Beryllium

Boron

Cadmium anr

Calcium

Chromium anr

Cobalt

Copper anr

Iron

Lead 99.4 98.2 1.2 0-10

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

203 of 211

M82628

55.7.4





Prep Date: 05/15/09


Aluminum 0.20 .014 .031

Antimony 0.0060 .0029 .003

Arsenic 0.025 .0027 .0032

Barium 0.50 .00064 .0012

Beryllium 0.0040 .00017 .0003

Boron 0.10 .0023 .0048

Cadmium 0.0040 .00024 .0003

Calcium 5.0 .0047 .04

Chromium 0.010 .00051 .0014

Cobalt 0.050 .00076 .001

Copper 0.025 .0011 .0018

Iron 0.10 .011 .029

Lead 0.010 .0013 .0018 0.00038 <0.010


Manganese 0.015 .00017 .0013

Molybdenum 0.10 .0005 .0014

Nickel 0.040 .00065 .001

Potassium 5.0 .025 .031

Selenium 0.025 .0016 .0033

Silver 0.0050 .00064 .0007

Sodium 5.0 .099 .21

Strontium 0.010 .00012 .0003

Thallium 0.0050 .002 .0045

Tin 0.10 .0016 .0099

Titanium 0.050 .0041 .0051

Tungsten 0.10 .0054 .007

Vanadium 0.030 .00065 .0035

Zinc 0.10 .0011 .0013

Associated samples MP13487: M82628-41B, M82628-42B


_________________________________________________________________________________________________________

Page 1

204 of 211

M82628

55.8.1





Prep Date: 05/15/09 05/15/09


Aluminum

Antimony

Arsenic anr

Barium anr

Beryllium

Boron

Cadmium anr

Calcium

Chromium anr

Cobalt

Copper anr

Iron

Lead 0.026 1.0 1.0 97.4 75-125 0.026 0.026 0.0 0-20

Magnesium

Manganese

Molybdenum

Nickel anr

Potassium

Selenium anr

Silver anr

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc anr



_________________________________________________________________________________________________________

Page 1

205 of 211

M82628

55.8.2





Prep Date: 05/15/09 05/15/09


Aluminum

Antimony

Arsenic anr

Barium anr

Beryllium

Boron

Cadmium anr

Calcium

Chromium anr

Cobalt

Copper anr

Iron

Lead 1.0 1.0 100.0 80-120 1.0 1.0 100.0 0.0 20

Magnesium

Manganese

Molybdenum

Nickel anr

Potassium

Selenium anr

Silver anr

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc anr



_________________________________________________________________________________________________________

Page 1

206 of 211

M82628

55.8.3





Prep Date: 05/15/09


Aluminum

Antimony

Arsenic anr

Barium anr

Beryllium

Boron

Cadmium anr

Calcium

Chromium anr

Cobalt

Copper anr

Iron

Lead 25.6 24.0 6.4 0-10

Magnesium

Manganese

Molybdenum

Nickel anr

Potassium

Selenium anr

Silver anr

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc anr



_________________________________________________________________________________________________________

Page 1

207 of 211

M82628

55.8.4





Prep Date: 05/15/09


Aluminum 0.20 .0086 .031

Antimony 0.0060 .0016 .003

Arsenic 0.025 .0023 .0032

Barium 0.50 .0006 .0012

Beryllium 0.0040 .00015 .0003

Boron 0.10 .0013 .0048

Cadmium 0.0040 .00022 .0003

Calcium 5.0 .0062 .04

Chromium 0.010 .00072 .0014

Cobalt 0.050 .00054 .001

Copper 0.025 .00064 .0018

Iron 0.10 .0066 .029

Lead 0.010 .0011 .0018 -0.0013 <0.010

Magnesium 5.0 .0051 .01

Manganese 0.015 .00018 .0013

Molybdenum 0.10 .00088 .0014

Nickel 0.040 .00061 .001

Potassium 5.0 .015 .031

Selenium 0.025 .0026 .0033

Silver 0.0050 .00054 .0007

Sodium 5.0 .077 .21

Strontium 0.010 .00012 .0003

Thallium 0.0050 .0029 .0045

Tin 0.10 .004 .0099

Titanium 0.050 .00059 .0051

Vanadium 0.030 .0024 .0035

Zinc 0.10 .00061 .0013

Associated samples MP13488: M82628-1B, M82628-2B, M82628-3B, M82628-4B, M82628-5B, M82628-6B, M82628-7B,M82628-8B, M82628-29B, M82628-30B, M82628-31B, M82628-32B, M82628-33B, M82628-34B, M82628-35B, M82628-36B, M82628-37B, M82628-38B, M82628-39B, M82628-40B


_________________________________________________________________________________________________________

Page 1

208 of 211

M82628

55.9.1





Prep Date: 05/15/09 05/15/09

M82628-36B Spikelot QC M82628-36B QCMetal Original MS MPICP % Rec Limits Original DUP RPD Limits

Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 0.12 1.1 1.0 98.0 75-125 0.12 0.13 8.0 0-20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

209 of 211

M82628

55.9.2





Prep Date: 05/15/09 05/15/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 1.0 1.0 100.0 80-120 1.0 1.0 100.0 0.0 20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

210 of 211

M82628

55.9.3





Prep Date: 05/15/09

M82628-36B QCMetal Original SDL 1:5 %DIF Limits

Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 123 121 1.7 0-10

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

211 of 211

M82628

55.9.4

09/24/09


Olin Corporation

Mactec: Olin-Newhall St.-Hamden, CT

6107090004/01


Sampling Dates: 09/09/09 - 09/10/09

Report to:

Mactec1090 Elm Street Suite 201Rocky Hill, CT [email protected]

ATTN: Miles VanNoordennen


Certifications: MA (M-MA136) CT (PH-0109) NH (2502) RI (00071) ME (MA0136) FL (E87579)

NY (11791) NJ (MA926) NC (653) IL (200018) NAVY USACE

This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.

Test results relate only to samples analyzed.


Test results contained within this data package meet the requirements

of the National Environmental Laboratory Accreditation Conference

and/or state specific certification programs as applicable.



09/24/09


54


1 of 54

M85762


Sections:


3.1: M85762-1: L900424 ..................................................................................................... 83.2: M85762-2: L900524 ..................................................................................................... 93.3: M85762-3: L900702 ..................................................................................................... 103.4: M85762-4: L900102 ..................................................................................................... 113.5: M85762-5: H901102 .................................................................................................... 123.6: M85762-6: H900324 .................................................................................................... 133.7: M85762-7: L900602 ..................................................................................................... 143.8: M85762-8: A900102 .................................................................................................... 153.9: M85762-9: A900102DUP ............................................................................................ 163.10: M85762-10: C900124 ................................................................................................. 173.11: M85762-11: F901102 ................................................................................................. 183.12: M85762-12: F901424 ................................................................................................. 193.13: M85762-13: F901302 ................................................................................................. 203.14: M85762-14: F900402 ................................................................................................. 213.15: M85762-15: S900124 ................................................................................................. 223.16: M85762-16: S900224 ................................................................................................. 233.17: M85762-17: Q900202 ................................................................................................ 243.18: M85762-18: Q900124 ................................................................................................ 253.19: M85762-19: L900224 ................................................................................................. 263.20: M85762-20: A900224 ................................................................................................ 273.21: M85762-21: T900424 ................................................................................................. 283.22: M85762-22: T900824 ................................................................................................. 293.23: M85762-23: P900302 ................................................................................................. 303.24: M85762-24: E900224 ................................................................................................. 313.25: M85762-25: E900224DUP ......................................................................................... 323.26: M85762-26: F900924 ................................................................................................. 33


Section 5: Metals Analysis - QC Data Summaries ................................................................ 435.1: Prep QC MP14103: Pb .................................................................................................. 445.2: Prep QC MP14108: Pb .................................................................................................. 49

12

34

5

2 of 54

M85762


Sample Summary



Sample Collected Matrix Client


M85762-1 09/09/09 13:55 MV 09/11/09 SO Soil L900424

M85762-2 09/09/09 14:00 MV 09/11/09 SO Soil L900524

M85762-3 09/09/09 14:10 MV 09/11/09 SO Soil L900702

M85762-4 09/09/09 14:40 MV 09/11/09 SO Soil L900102

M85762-5 09/09/09 15:25 MV 09/11/09 SO Soil H901102

M85762-6 09/09/09 15:35 MV 09/11/09 SO Soil H900324

M85762-7 09/10/09 09:15 MV 09/11/09 SO Soil L900602

M85762-8 09/10/09 09:25 MV 09/11/09 SO Soil A900102

M85762-8D 09/10/09 09:25 MV 09/11/09 SO Soil Dup/MSD A900102MSD

M85762-8S 09/10/09 09:25 MV 09/11/09 SO Soil Matrix Spike A900102MS

M85762-9 09/10/09 09:25 MV 09/11/09 SO Soil A900102DUP

M85762-10 09/09/09 10:10 MV 09/11/09 SO Soil C900124

M85762-11 09/09/09 10:25 MV 09/11/09 SO Soil F901102


3 of 54

M85762

1







M85762-12 09/09/09 10:30 MV 09/11/09 SO Soil F901424

M85762-13 09/09/09 10:40 MV 09/11/09 SO Soil F901302

M85762-14 09/09/09 11:00 MV 09/11/09 SO Soil F900402

M85762-15 09/09/09 11:15 MV 09/11/09 SO Soil S900124

M85762-16 09/09/09 11:30 MV 09/11/09 SO Soil S900224

M85762-17 09/09/09 13:05 MV 09/11/09 SO Soil Q900202

M85762-18 09/09/09 13:15 MV 09/11/09 SO Soil Q900124

M85762-19 09/09/09 13:50 MV 09/11/09 SO Soil L900224

M85762-20 09/10/09 09:55 MV 09/11/09 SO Soil A900224

M85762-21 09/10/09 10:50 MV 09/11/09 SO Soil T900424

M85762-22 09/10/09 11:15 MV 09/11/09 SO Soil T900824

M85762-23 09/10/09 11:35 MV 09/11/09 SO Soil P900302

M85762-24 09/10/09 12:10 MV 09/11/09 SO Soil E900224


4 of 54

M85762

1







M85762-24D 09/10/09 12:10 MV 09/11/09 SO Soil Dup/MSD E900224MSD

M85762-24S 09/10/09 12:10 MV 09/11/09 SO Soil Matrix Spike E900224MS

M85762-25 09/10/09 12:10 MV 09/11/09 SO Soil E900224DUP

M85762-26 09/09/09 09:50 MV 09/11/09 SO Soil F900924


5 of 54

M85762

1

26 Samples were collected on between 09/09/2009 and 09/10/2009 and were received at Accutest on 09/11/2009 properly preserved,

at 2.1 Deg. C and intact. These Samples received an Accutest job number of M85762. A listing of the Laboratory Sample ID, Client

Sample ID and dates of collection are presented in the Results Summary Section of this report.





Job No M85762

Repor t Date 9/24/2009 11:00:11 AM







Sample(s) M85762-8DUP, M85762-8LS, M85767-1MS, M85767-1SDL were used as the QC samples for metals.

RPD(s) for Serial Dilution for Lead are outside control limits for sample MP14103-SD1. Percent difference acceptable due to

low initial sample concentration (< 50 times IDL).






Sample(s) M85762-24DUP, M85762-24SDL, M85762-24MS were used as the QC samples for metals.

Matrix Spike Recovery(s) for Lead are outside control limits. Spike amount low relative to the sample amount. Refer to lab

control or spike blank for recovery information.





Thursday, September 24, 2009 P age 1 of 1

6 of 54

M85762

2


Sample Results

Report of Analysis

Section 3

7 of 54

M85762

3






Percent Solids: n/a









8 of 54

M85762

33.1






Percent Solids: n/a




Lead < 0.010 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2





9 of 54

M85762

33.2






Percent Solids: n/a









10 of 54

M85762

33.3






Percent Solids: n/a









11 of 54

M85762

33.4






Percent Solids: n/a









12 of 54

M85762

33.5






Percent Solids: n/a









13 of 54

M85762

33.6






Percent Solids: n/a









14 of 54

M85762

33.7






Percent Solids: n/a









15 of 54

M85762

33.8



Client Sample ID: A900102DUP



Percent Solids: n/a









16 of 54

M85762

33.9






Percent Solids: n/a









17 of 54

M85762

33.10



Client Sample ID: F901102



Percent Solids: n/a









18 of 54

M85762

33.11






Percent Solids: n/a









19 of 54

M85762

33.12






Percent Solids: n/a









20 of 54

M85762

33.13






Percent Solids: n/a









21 of 54

M85762

33.14






Percent Solids: n/a




Lead < 0.010 D008 5.0 0.010 mg/l 1 09/15/09 09/16/09 EAL SW846 6010B 1 SW846 3010A 2





22 of 54

M85762

33.15






Percent Solids: n/a









23 of 54

M85762

33.16



Client Sample ID: Q900202



Percent Solids: n/a









24 of 54

M85762

33.17



Client Sample ID: Q900124



Percent Solids: n/a









25 of 54

M85762

33.18






Percent Solids: n/a




Lead 46.5 D008 5.0 0.10 mg/l 10 09/16/09 09/17/09 PY SW846 6010B 1 SW846 3010A 2





26 of 54

M85762

33.19






Percent Solids: n/a









27 of 54

M85762

33.20



Client Sample ID: T900424



Percent Solids: n/a









28 of 54

M85762

33.21






Percent Solids: n/a









29 of 54

M85762

33.22






Percent Solids: n/a









30 of 54

M85762

33.23



Client Sample ID: E900224



Percent Solids: n/a




Lead 107 D008 5.0 0.20 mg/l 20 09/16/09 09/17/09 PY SW846 6010B 1 SW846 3010A 2





31 of 54

M85762

33.24



Client Sample ID: E900224DUP



Percent Solids: n/a









32 of 54

M85762

33.25






Percent Solids: n/a









33 of 54

M85762

33.26


Misc. Forms






• RCP Form


Section 4

34 of 54

M85762

4


35 of 54

M85762

44.1


36 of 54

M85762

44.1


37 of 54

M85762

44.1



Sampling Date(s):


Methods:

1 Yes No

1A Yes No

1B Yes No

NA

2 Yes No

3 Yes No

4 Yes No

5 Yes No

Yes No

6 Yes No

7 Yes No

Authorized




9/24/2009










SW846 6010B





documents)?



Laboratory Analysis

Reza Tand







data set?






M85762-1, M85762-2, M85762-3, M85762-4, M85762-5, M85762-6, M85762-7, M85762-

8, M85762-9, M85762-10, M85762-11, M85762-12, M85762-13, M85762-14, M85762-15,

M85762-16, M85762-17, M85762-18, M85762-19, M85762-20, M85762-21, M85762-22,

M85762-23, M85762-24, M85762-25, M85762-26, M85762-8S, M85762-24S, M85762-

8D, M85762-24D

9/9/2009

Olin Corporation


38 of 54

M85762

44.2





Sample


M85762-1 Collected: 09-SEP-09 13:55 By: MV Received: 11-SEP-09 By: SAP

L900424

M85762-1 SW846 6010B 16-SEP-09 18:24 EAL 15-SEP-09 EAL EPB


L900524



L900702



L900102



H901102



H900324



L900602



A900102


Page 1 of 4

39 of 54

M85762

44.3





Sample



A900102DUP



C900124



F901102



F901424



F901302



F900402



S900124



S900224


Page 2 of 4

40 of 54

M85762

44.3





Sample



Q900202



Q900124



L900224

M85762-19 SW846 6010B 17-SEP-09 20:43 PY 16-SEP-09 EAL EPB


A900224



T900424



T900824



P900302



E900224

M85762-24 SW846 6010B 17-SEP-09 20:34 PY 16-SEP-09 EAL EPB

Page 3 of 4

41 of 54

M85762

44.3





Sample



E900224DUP



F900924


Page 4 of 4

42 of 54

M85762

44.3


Metals Analysis

QC Data Summaries






Section 5

43 of 54

M85762

5





Prep Date: 09/15/09


Aluminum 0.20 .014 .031

Antimony 0.0060 .0029 .003

Arsenic 0.025 .0027 .0032

Barium 0.50 .00064 .0012

Beryllium 0.0040 .00017 .0003

Boron 0.10 .0023 .0048

Cadmium 0.0040 .00024 .0003

Calcium 5.0 .0047 .04

Chromium 0.010 .00051 .0014

Cobalt 0.050 .00076 .001

Copper 0.025 .0011 .0018

Iron 0.10 .011 .029

Lead 0.010 .0013 .0018 0.00055 <0.010


Manganese 0.015 .00017 .0013

Molybdenum 0.10 .0005 .0014

Nickel 0.040 .00065 .001

Potassium 5.0 .025 .031

Selenium 0.025 .0016 .0033

Silver 0.0050 .00064 .0007

Sodium 5.0 .099 .21

Strontium 0.010 .00012 .0003

Thallium 0.0050 .002 .0045

Tin 0.10 .0016 .0099

Titanium 0.050 .0041 .0051

Tungsten 0.10 .0054 .007

Vanadium 0.030 .00065 .0035

Zinc 0.10 .0011 .0013

Associated samples MP14103: M85762-1, M85762-2, M85762-3, M85762-4, M85762-5, M85762-6, M85762-7, M85762-8, M85762-9, M85762-10, M85762-11, M85762-12, M85762-13, M85762-14, M85762-15, M85762-16, M85762-17,M85762-18


_________________________________________________________________________________________________________

Page 1

44 of 54

M85762

55.1.1





Prep Date: 09/15/09 09/15/09

M85767-1 Spikelot QC M85762-8 Spikelot QCMetal Original MS MPICP % Rec Limits Original LS MPICP % Rec Limits

Aluminum

Antimony

Arsenic anr

Barium anr

Beryllium

Boron

Cadmium anr

Calcium

Chromium anr

Cobalt

Copper

Iron

Lead 0.0020 1.0 1.0 99.8 75-125 0.016 1.0 1.0 98.4 75-125

Magnesium

Manganese

Molybdenum

Nickel anr

Potassium

Selenium anr

Silver anr

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

45 of 54

M85762

55.1.2





Prep Date: 09/15/09

M85762-8 QCMetal Original DUP RPD Limits

Aluminum

Antimony

Arsenic anr

Barium anr

Beryllium

Boron

Cadmium anr

Calcium

Chromium anr

Cobalt

Copper

Iron

Lead 0.016 0.017 6.1 0-20

Magnesium

Manganese

Molybdenum

Nickel anr

Potassium

Selenium anr

Silver anr

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 2

46 of 54

M85762

55.1.2





Prep Date: 09/15/09 09/15/09


Aluminum

Antimony

Arsenic anr

Barium anr

Beryllium

Boron

Cadmium anr

Calcium

Chromium anr

Cobalt

Copper

Iron

Lead 0.99 1.0 99.0 80-120 1.0 1.0 100.0 1.0 20

Magnesium

Manganese

Molybdenum

Nickel anr

Potassium

Selenium anr

Silver anr

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc



_________________________________________________________________________________________________________

Page 1

47 of 54

M85762

55.1.3





Prep Date: 09/15/09


Aluminum

Antimony

Arsenic anr

Barium anr

Beryllium

Boron

Cadmium anr

Calcium

Chromium anr

Cobalt

Copper

Iron

Lead 1.98 0.00 100.0(a) 0-10

Magnesium

Manganese

Molybdenum

Nickel anr

Potassium

Selenium anr

Silver anr

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc


Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(anr) Analyte not requested(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).

_________________________________________________________________________________________________________

Page 1

48 of 54

M85762

55.1.4





Prep Date: 09/16/09


Aluminum 0.20 .014 .031

Antimony 0.0060 .0029 .003

Arsenic 0.025 .0027 .0032

Barium 0.50 .00064 .0012

Beryllium 0.0040 .00017 .0003

Boron 0.10 .0023 .0048

Cadmium 0.0040 .00024 .0003

Calcium 5.0 .0047 .04

Chromium 0.010 .00051 .0014

Cobalt 0.050 .00076 .001

Copper 0.025 .0011 .0018

Iron 0.10 .011 .029

Lead 0.010 .0013 .0018 0.0020 <0.010


Manganese 0.015 .00017 .0013

Molybdenum 0.10 .0005 .0014

Nickel 0.040 .00065 .001

Potassium 5.0 .025 .031

Selenium 0.025 .0016 .0033

Silver 0.0050 .00064 .0007

Sodium 5.0 .099 .21

Strontium 0.010 .00012 .0003

Thallium 0.0050 .002 .0045

Tin 0.10 .0016 .0099

Titanium 0.050 .0041 .0051

Tungsten 0.10 .0054 .007

Vanadium 0.030 .00065 .0035

Zinc 0.10 .0011 .0013

Associated samples MP14108: M85762-19, M85762-20, M85762-21, M85762-22, M85762-23, M85762-24, M85762-25,M85762-26


_________________________________________________________________________________________________________

Page 1

49 of 54

M85762

55.2.1





Prep Date: 09/16/09 09/16/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Gold

Iron

Lead 107 103 1.00 -400.0(a 75-125 107 106 0.9 0-20

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium

Silicon

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc

Associated samples MP14108: M85762-19, M85762-20, M85762-21, M85762-22, M85762-23, M85762-24, M85762-25,M85762-26_________________________________________________________________________________________________________

Page 1

50 of 54

M85762

55.2.2





Prep Date:

Metal

Results < IDL are shown as zero for calculation purposes(*) Outside of QC limits(N) Matrix Spike Rec. outside of QC limits(anr) Analyte not requested(a) Spike amount low relative to the sample amount. Refer to lab control or spike blank for recovery

information.

_________________________________________________________________________________________________________

Page 2

51 of 54

M85762

55.2.2





Prep Date: 09/16/09 09/16/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Iron

Lead 1.0 1.0 100.0 80-120 1.0 1.0 100.0 0.0 20

Magnesium

Manganese

Molybdenum

Nickel

Potassium

Selenium

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc

Associated samples MP14108: M85762-19, M85762-20, M85762-21, M85762-22, M85762-23, M85762-24, M85762-25,M85762-26


_________________________________________________________________________________________________________

Page 1

52 of 54

M85762

55.2.3





Prep Date: 09/16/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Gold

Iron

Lead 107000 106000 0.5 0-10

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium

Silicon

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc


Page 1

53 of 54

M85762

55.2.4





Prep Date:

Metal


_________________________________________________________________________________________________________

Page 2

54 of 54

M85762

55.2.4

10/30/09


Olin Corporation

Mactec: Olin-Newhall St.-Hamden, CT

6107090004/01


Sampling Dates: 10/14/09 - 10/15/09

Report to:

Mactec1090 Elm Street Suite 201Rocky Hill, CT [email protected]

ATTN: Miles VanNoordennen


Certifications: MA (M-MA136) CT (PH-0109) NH (2502) RI (00071) ME (MA0136) FL (E87579)

NY (11791) NJ (MA926) NC (653) IL (200018) NAVY USACE

This report shall not be reproduced, except in its entirety, without the written approval of Accutest Laboratories.

Test results relate only to samples analyzed.


Test results contained within this data package meet the requirements

of the National Environmental Laboratory Accreditation Conference

and/or state specific certification programs as applicable.



10/30/09


96


1 of 96

M86571


Sections:


3.1: M86571-1: H900424 .................................................................................................... 103.2: M86571-2: H900902 .................................................................................................... 113.3: M86571-3: H900524 .................................................................................................... 123.4: M86571-4: H900602 .................................................................................................... 133.5: M86571-5: H900702 .................................................................................................... 143.6: M86571-6: H900802 .................................................................................................... 153.7: M86571-7: H900224 .................................................................................................... 163.8: M86571-8: J900424 ...................................................................................................... 173.9: M86571-9: H901024 .................................................................................................... 183.10: M86571-10: H900124 ................................................................................................ 193.11: M86571-11: J900102 .................................................................................................. 203.12: M86571-12: J900102DUP .......................................................................................... 213.13: M86571-13: J900302 .................................................................................................. 223.14: M86571-14: J900224 .................................................................................................. 233.15: M86571-15: L900324 ................................................................................................. 243.16: M86571-16: N900124 ................................................................................................ 253.17: M86571-17: F900602 ................................................................................................. 263.18: M86571-18: C900324 ................................................................................................. 273.19: M86571-19: C900424 ................................................................................................. 283.20: M86571-20: C900502 ................................................................................................. 293.21: M86571-21: K900102 ................................................................................................ 303.22: M86571-22: K900102DUP ........................................................................................ 313.23: M86571-23: K900202 ................................................................................................ 323.24: M86571-24: P900124 ................................................................................................. 333.25: M86571-25: P900202 ................................................................................................. 343.26: M86571-26: P900402 ................................................................................................. 353.27: M86571-27: E900424 ................................................................................................. 363.28: M86571-28: E900502 ................................................................................................. 373.29: M86571-29: F901224 ................................................................................................. 383.30: M86571-30: F900224 ................................................................................................. 393.31: M86571-31: F901524 ................................................................................................. 403.32: M86571-32: F900524 ................................................................................................. 413.33: M86571-33: E900124 ................................................................................................. 423.34: M86571-34: E900324 ................................................................................................. 433.35: M86571-35: C900224 ................................................................................................. 443.36: M86571-36: F901002 ................................................................................................. 453.37: M86571-37: F900324 ................................................................................................. 463.38: M86571-38: F900824 ................................................................................................. 473.39: M86571-39: F901602 ................................................................................................. 48

12

34

5

2 of 96

M86571


Sections:

3.40: M86571-40: F900724 ................................................................................................. 493.41: M86571-41: F900102 ................................................................................................. 503.42: M86571-42: R900102 ................................................................................................. 513.43: M86571-43: T900202 ................................................................................................. 523.44: M86571-44: T900102 ................................................................................................. 533.45: M86571-45: T900324 ................................................................................................. 543.46: M86571-46: T900524 ................................................................................................. 553.47: M86571-47: T900702 ................................................................................................. 563.48: M86571-48: T900602 ................................................................................................. 57


Section 5: Metals Analysis - QC Data Summaries ................................................................ 725.1: Prep QC MP14283: Pb .................................................................................................. 735.2: Prep QC MP14291: Pb .................................................................................................. 815.3: Prep QC MP14323: Pb .................................................................................................. 89

12

34

5

3 of 96

M86571


Sample Summary





M86571-1 10/14/09 11:00 MV 10/16/09 SO Soil H900424

M86571-2 10/14/09 11:15 MV 10/16/09 SO Soil H900902

M86571-3 10/14/09 11:30 MV 10/16/09 SO Soil H900524

M86571-4 10/14/09 11:40 MV 10/16/09 SO Soil H900602

M86571-5 10/14/09 11:50 MV 10/16/09 SO Soil H900702

M86571-6 10/14/09 12:10 MV 10/16/09 SO Soil H900802

M86571-7 10/14/09 12:30 MV 10/16/09 SO Soil H900224

M86571-8 10/14/09 12:45 MV 10/16/09 SO Soil J900424

M86571-9 10/14/09 12:55 MV 10/16/09 SO Soil H901024

M86571-10 10/14/09 13:05 MV 10/16/09 SO Soil H900124

M86571-11 10/14/09 14:30 MV 10/16/09 SO Soil J900102

M86571-11D 10/14/09 14:30 MV 10/16/09 SO Soil Dup/MSD J900102 MSD

M86571-11S 10/14/09 14:30 MV 10/16/09 SO Soil Matrix Spike J900102 MS


4 of 96

M86571

1







M86571-12 10/14/09 14:30 MV 10/16/09 SO Soil J900102DUP

M86571-13 10/14/09 14:45 MV 10/16/09 SO Soil J900302

M86571-14 10/14/09 14:50 MV 10/16/09 SO Soil J900224

M86571-15 10/14/09 15:10 MV 10/16/09 SO Soil L900324

M86571-16 10/14/09 15:45 MV 10/16/09 SO Soil N900124

M86571-17 10/14/09 16:00 MV 10/16/09 SO Soil F900602

M86571-18 10/14/09 16:15 MV 10/16/09 SO Soil C900324

M86571-19 10/14/09 16:20 MV 10/16/09 SO Soil C900424

M86571-20 10/14/09 16:40 MV 10/16/09 SO Soil C900502

M86571-21 10/15/09 09:20 MV 10/16/09 SO Soil K900102

M86571-21D 10/15/09 09:20 MV 10/16/09 SO Soil Dup/MSD K900102 MSD

M86571-21S 10/15/09 09:20 MV 10/16/09 SO Soil Matrix Spike K900102 MS

M86571-22 10/15/09 09:20 MV 10/16/09 SO Soil K900102DUP


5 of 96

M86571

1







M86571-23 10/15/09 09:40 MV 10/16/09 SO Soil K900202

M86571-24 10/15/09 09:50 MV 10/16/09 SO Soil P900124

M86571-25 10/15/09 10:00 MV 10/16/09 SO Soil P900202

M86571-26 10/15/09 10:10 MV 10/16/09 SO Soil P900402

M86571-27 10/15/09 10:20 MV 10/16/09 SO Soil E900424

M86571-28 10/15/09 10:30 MV 10/16/09 SO Soil E900502

M86571-29 10/15/09 10:40 MV 10/16/09 SO Soil F901224

M86571-30 10/15/09 10:50 MV 10/16/09 SO Soil F900224

M86571-31 10/15/09 11:00 MV 10/16/09 SO Soil F901524

M86571-32 10/15/09 11:10 MV 10/16/09 SO Soil F900524

M86571-33 10/15/09 12:15 MV 10/16/09 SO Soil E900124

M86571-34 10/15/09 12:25 MV 10/16/09 SO Soil E900324

M86571-35 10/15/09 12:35 MV 10/16/09 SO Soil C900224


6 of 96

M86571

1







M86571-36 10/15/09 12:45 MV 10/16/09 SO Soil F901002

M86571-37 10/15/09 12:55 MV 10/16/09 SO Soil F900324

M86571-38 10/15/09 13:00 MV 10/16/09 SO Soil F900824

M86571-39 10/15/09 13:10 MV 10/16/09 SO Soil F901602

M86571-40 10/15/09 13:15 MV 10/16/09 SO Soil F900724

M86571-41 10/15/09 13:20 MV 10/16/09 SO Soil F900102

M86571-42 10/15/09 13:30 MV 10/16/09 SO Soil R900102

M86571-43 10/15/09 13:40 MV 10/16/09 SO Soil T900202

M86571-44 10/15/09 13:55 MV 10/16/09 SO Soil T900102

M86571-45 10/15/09 14:00 MV 10/16/09 SO Soil T900324

M86571-46 10/15/09 14:40 MV 10/16/09 SO Soil T900524

M86571-47 10/15/09 14:50 MV 10/16/09 SO Soil T900702

M86571-48 10/15/09 15:00 MV 10/16/09 SO Soil T900602


7 of 96

M86571

1

48 Sample(s) were collected on between 10/14/2009 and 10/15/2009 and were received at Accutest on 10/16/2009 properly preserved,

at 1.8 Deg. C and intact. These Samples received an Accutest job number of M86571. A listing of the Laboratory Sample ID, Client

Sample ID and dates of collection are presented in the Results Summary Section of this report.





Job No M86571

Repor t Date 10/30/2009 12:52:00 PM
























F riday, October 30, 2009 P age 1 of 1

8 of 96

M86571

2


Sample Results

Report of Analysis

Section 3

9 of 96

M86571

3






Percent Solids: n/a









10 of 96

M86571

33.1






Percent Solids: n/a









11 of 96

M86571

33.2






Percent Solids: n/a




Lead < 0.010 D008 5.0 0.010 mg/l 1 10/21/09 10/21/09 PY SW846 6010B 1 SW846 3010A 2





12 of 96

M86571

33.3






Percent Solids: n/a









13 of 96

M86571

33.4






Percent Solids: n/a









14 of 96

M86571

33.5






Percent Solids: n/a









15 of 96

M86571

33.6






Percent Solids: n/a









16 of 96

M86571

33.7






Percent Solids: n/a









17 of 96

M86571

33.8






Percent Solids: n/a









18 of 96

M86571

33.9






Percent Solids: n/a









19 of 96

M86571

33.10






Percent Solids: n/a









20 of 96

M86571

33.11



Client Sample ID: J900102DUP



Percent Solids: n/a









21 of 96

M86571

33.12






Percent Solids: n/a









22 of 96

M86571

33.13






Percent Solids: n/a









23 of 96

M86571

33.14






Percent Solids: n/a









24 of 96

M86571

33.15






Percent Solids: n/a









25 of 96

M86571

33.16






Percent Solids: n/a









26 of 96

M86571

33.17






Percent Solids: n/a









27 of 96

M86571

33.18






Percent Solids: n/a









28 of 96

M86571

33.19






Percent Solids: n/a









29 of 96

M86571

33.20






Percent Solids: n/a









30 of 96

M86571

33.21



Client Sample ID: K900102DUP



Percent Solids: n/a









31 of 96

M86571

33.22






Percent Solids: n/a









32 of 96

M86571

33.23






Percent Solids: n/a









33 of 96

M86571

33.24






Percent Solids: n/a









34 of 96

M86571

33.25






Percent Solids: n/a









35 of 96

M86571

33.26






Percent Solids: n/a









36 of 96

M86571

33.27






Percent Solids: n/a









37 of 96

M86571

33.28






Percent Solids: n/a









38 of 96

M86571

33.29






Percent Solids: n/a









39 of 96

M86571

33.30






Percent Solids: n/a









40 of 96

M86571

33.31






Percent Solids: n/a









41 of 96

M86571

33.32






Percent Solids: n/a









42 of 96

M86571

33.33






Percent Solids: n/a









43 of 96

M86571

33.34






Percent Solids: n/a









44 of 96

M86571

33.35






Percent Solids: n/a









45 of 96

M86571

33.36






Percent Solids: n/a









46 of 96

M86571

33.37






Percent Solids: n/a









47 of 96

M86571

33.38






Percent Solids: n/a









48 of 96

M86571

33.39






Percent Solids: n/a









49 of 96

M86571

33.40






Percent Solids: n/a









50 of 96

M86571

33.41






Percent Solids: n/a









51 of 96

M86571

33.42






Percent Solids: n/a









52 of 96

M86571

33.43






Percent Solids: n/a









53 of 96

M86571

33.44






Percent Solids: n/a









54 of 96

M86571

33.45






Percent Solids: n/a









55 of 96

M86571

33.46






Percent Solids: n/a









56 of 96

M86571

33.47






Percent Solids: n/a









57 of 96

M86571

33.48


Misc. Forms






• RCP Form


Section 4

58 of 96

M86571

4


59 of 96

M86571

44.1


60 of 96

M86571

44.1


61 of 96

M86571

44.1


62 of 96

M86571

44.1


63 of 96

M86571

44.1


64 of 96

M86571

44.1



Sampling Date(s):


Methods:

1 Yes No

1A Yes No

1B Yes No

NA

2 Yes No

3 Yes No

4 Yes No

5 Yes No

Yes No

6 Yes No

7 Yes No

Authorized




10/14/2009

Olin Corporation


Laboratory Analysis

Reza Tand







data set?






M86571-1, M86571-2, M86571-3, M86571-4, M86571-5, M86571-6, M86571-7, M86571-

8, M86571-9, M86571-10, M86571-11, M86571-12, M86571-13, M86571-14, M86571-15,

M86571-16, M86571-17, M86571-18, M86571-19, M86571-20, M86571-21, M86571-22,

M86571-23, M86571-24, M86571-25, M86571-26, M86571-27, M86571-28, M86571-29,

M86571-30, M86571-31, M86571-32, M86571-33, M86571-34, M86571-35, M86571-36,

M86571-37, M86571-38, M86571-39, M86571-40, M86571-41, M86571-42, M86571-43,

M86571-44, M86571-45, M86571-46, M86571-47, M86571-48, M86571-11S, M86571-

21S, M86571-11D, M86571-21D

10/30/2009










EPA 160.3 M, SW846 6010B





documents)?



65 of 96

M86571

44.2





Sample


M86571-1 Collected: 14-OCT-09 11:00 By: MV Received: 16-OCT-09 By: JB

H900424

M86571-1 SW846 6010B 21-OCT-09 21:05 PY 21-OCT-09 EAL EPB


H900902



H900524



H900602



H900702



H900802



H900224



J900424


Page 1 of 6

66 of 96

M86571

44.3





Sample



H901024



H900124



J900102



J900102DUP



J900302



J900224



L900324



N900124


Page 2 of 6

67 of 96

M86571

44.3





Sample



F900602



C900324



C900424



C900502



K900102



K900102DUP



K900202



P900124


Page 3 of 6

68 of 96

M86571

44.3





Sample



P900202



P900402



E900424



E900502



F901224



F900224



F901524



F900524


Page 4 of 6

69 of 96

M86571

44.3





Sample



E900124



E900324



C900224



F901002



F900324



F900824



F901602



F900724


Page 5 of 6

70 of 96

M86571

44.3





Sample



F900102



R900102



T900202



T900102



T900324



T900524



T900702



T900602


Page 6 of 6

71 of 96

M86571

44.3


Metals Analysis

QC Data Summaries






Section 5

72 of 96

M86571

5





Prep Date: 10/21/09


Aluminum 0.20 .027 .04

Antimony 0.0060 .0014 .0016

Arsenic 0.025 .001 .0018

Barium 0.50 .00057 .0011

Beryllium 0.0040 .00015 .0004

Boron 0.10 .00065 .0023

Cadmium 0.0040 .00024 .0019

Calcium 5.0 .0076 .015

Chromium 0.010 .00081 .0011

Cobalt 0.050 .00025 .0003

Copper 0.025 .0022 .004

Gold 0.050 .0011 .0042

Iron 0.10 .0037 .013

Lead 0.010 .0011 .0027 -0.00020 <0.010

Magnesium 5.0 .037 .077

Manganese 0.015 .00012 .0011

Molybdenum 0.10 .00022 .0008

Nickel 0.040 .00024 .0013

Palladium 0.050 .0022 .004

Platinum 0.050 .0093 .013

Potassium 5.0 .039 .046

Selenium 0.025 .0019 .0035

Silicon 0.10 .0089 .036

Silver 0.0050 .00054 .0013

Sodium 5.0 .061 .16

Strontium 0.010 .00024 .0003

Thallium 0.0050 .0012 .0013

Tin 0.10 .00065 .0013

Titanium 0.050 .00074 .0008

Tungsten 0.10 .0056 .008

Vanadium 0.030 .00068 .0016

Zinc 0.10 .00074 .0015

Associated samples MP14283: M86571-1, M86571-2, M86571-3, M86571-4, M86571-5, M86571-6, M86571-7, M86571-8, M86571-9, M86571-10, M86571-11, M86571-12, M86571-13, M86571-14, M86571-15, M86571-16, M86571-17,_________________________________________________________________________________________________________

Page 1

73 of 96

M86571

55.1.1





Prep Date:

Metal

M86571-18, M86571-19, M86571-20


_________________________________________________________________________________________________________

Page 2

74 of 96

M86571

55.1.1





Prep Date: 10/21/09 10/21/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Gold

Iron

Lead 0.39 1.3 1.0 91.0 75-125 0.39 0.39 0.0 0-20

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium

Silicon

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc


Page 1

75 of 96

M86571

55.1.2





Prep Date:

Metal

M86571-18, M86571-19, M86571-20


_________________________________________________________________________________________________________

Page 2

76 of 96

M86571

55.1.2





Prep Date: 10/21/09 10/21/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Gold

Iron

Lead 0.92 1.0 92.0 80-120 0.91 1.0 91.0 1.1 20

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium

Silicon

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc


Page 1

77 of 96

M86571

55.1.3





Prep Date:

Metal

M86571-18, M86571-19, M86571-20


_________________________________________________________________________________________________________

Page 2

78 of 96

M86571

55.1.3





Prep Date: 10/21/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Gold

Iron

Lead 392 401 2.3 0-10

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium

Silicon

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc


Page 1

79 of 96

M86571

55.1.4





Prep Date:

Metal

M86571-18, M86571-19, M86571-20


_________________________________________________________________________________________________________

Page 2

80 of 96

M86571

55.1.4





Prep Date: 10/22/09


Aluminum 0.20 .027 .04

Antimony 0.0060 .0014 .0016

Arsenic 0.025 .001 .0018

Barium 0.50 .00057 .0011

Beryllium 0.0040 .00015 .0004

Boron 0.10 .00065 .0023

Cadmium 0.0040 .00024 .0019

Calcium 5.0 .0076 .015

Chromium 0.010 .00081 .0011

Cobalt 0.050 .00025 .0003

Copper 0.025 .0022 .004

Gold 0.050 .0011 .0042

Iron 0.10 .0037 .013

Lead 0.010 .0011 .0027 0.00020 <0.010

Magnesium 5.0 .037 .077

Manganese 0.015 .00012 .0011

Molybdenum 0.10 .00022 .0008

Nickel 0.040 .00024 .0013

Palladium 0.050 .0022 .004

Platinum 0.050 .0093 .013

Potassium 5.0 .039 .046

Selenium 0.025 .0019 .0035

Silicon 0.10 .0089 .036

Silver 0.0050 .00054 .0013

Sodium 5.0 .061 .16

Strontium 0.010 .00024 .0003

Thallium 0.0050 .0012 .0013

Tin 0.10 .00065 .0013

Titanium 0.050 .00074 .0008

Tungsten 0.10 .0056 .008

Vanadium 0.030 .00068 .0016

Zinc 0.10 .00074 .0015

Associated samples MP14291: M86571-21, M86571-22, M86571-23, M86571-24, M86571-25, M86571-26, M86571-27,M86571-28, M86571-29, M86571-30, M86571-31, M86571-32, M86571-33, M86571-34, M86571-35, M86571-36,_________________________________________________________________________________________________________

Page 1

81 of 96

M86571

55.2.1





Prep Date:

Metal

M86571-37, M86571-38, M86571-39, M86571-40


_________________________________________________________________________________________________________

Page 2

82 of 96

M86571

55.2.1





Prep Date: 10/22/09 10/22/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Gold

Iron

Lead 0.10 1.1 1.0 100.0 75-125 0.10 0.10 0.0 0-20

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium

Silicon

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc


Page 1

83 of 96

M86571

55.2.2





Prep Date:

Metal

M86571-37, M86571-38, M86571-39, M86571-40


_________________________________________________________________________________________________________

Page 2

84 of 96

M86571

55.2.2





Prep Date: 10/22/09 10/22/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Gold

Iron

Lead 0.94 1.0 94.0 80-120 0.95 1.0 95.0 1.1 20

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium

Silicon

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc


Page 1

85 of 96

M86571

55.2.3





Prep Date:

Metal

M86571-37, M86571-38, M86571-39, M86571-40


_________________________________________________________________________________________________________

Page 2

86 of 96

M86571

55.2.3





Prep Date: 10/22/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Gold

Iron

Lead 103 106 2.6 0-10

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium

Silicon

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc


Page 1

87 of 96

M86571

55.2.4





Prep Date:

Metal

M86571-37, M86571-38, M86571-39, M86571-40


_________________________________________________________________________________________________________

Page 2

88 of 96

M86571

55.2.4





Prep Date: 10/28/09


Aluminum 0.20 .027 .04

Antimony 0.0060 .0014 .0016

Arsenic 0.025 .001 .0018

Barium 0.50 .00057 .0011

Beryllium 0.0040 .00015 .0004

Boron 0.10 .00065 .0023

Cadmium 0.0040 .00024 .0019

Calcium 5.0 .0076 .015

Chromium 0.010 .00081 .0011

Cobalt 0.050 .00025 .0003

Copper 0.025 .0022 .004

Gold 0.050 .0011 .0042

Iron 0.10 .0037 .013

Lead 0.010 .0011 .0027 0.00060 <0.010

Magnesium 5.0 .037 .077

Manganese 0.015 .00012 .0011

Molybdenum 0.10 .00022 .0008

Nickel 0.040 .00024 .0013

Palladium 0.050 .0022 .004

Platinum 0.050 .0093 .013

Potassium 5.0 .039 .046

Selenium 0.025 .0019 .0035

Silicon 0.10 .0089 .036

Silver 0.0050 .00054 .0013

Sodium 5.0 .061 .16

Strontium 0.010 .00024 .0003

Thallium 0.0050 .0012 .0013

Tin 0.10 .00065 .0013

Titanium 0.050 .00074 .0008

Tungsten 0.10 .0056 .008

Vanadium 0.030 .00068 .0016

Zinc 0.10 .00074 .0015


Page 1

89 of 96

M86571

55.3.1





Prep Date:

Metal


_________________________________________________________________________________________________________

Page 2

90 of 96

M86571

55.3.1





Prep Date: 10/28/09 10/28/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Gold

Iron

Lead 1.0 2.0 1.0 100.0 75-125 1.0 1.0 0.0 0-20

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium

Silicon

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc


Page 1

91 of 96

M86571

55.3.2





Prep Date:

Metal


_________________________________________________________________________________________________________

Page 2

92 of 96

M86571

55.3.2





Prep Date: 10/28/09 10/28/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Gold

Iron

Lead 0.94 1.0 94.0 80-120 0.91 1.0 91.0 3.2 20

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium

Silicon

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc


Page 1

93 of 96

M86571

55.3.3





Prep Date:

Metal


_________________________________________________________________________________________________________

Page 2

94 of 96

M86571

55.3.3





Prep Date: 10/28/09


Aluminum

Antimony

Arsenic

Barium

Beryllium

Boron

Cadmium

Calcium

Chromium

Cobalt

Copper

Gold

Iron

Lead 1020 1070 4.4 0-10

Magnesium

Manganese

Molybdenum

Nickel

Palladium

Platinum

Potassium

Selenium

Silicon

Silver

Sodium

Strontium

Thallium

Tin

Titanium

Tungsten

Vanadium

Zinc


Page 1

95 of 96

M86571

55.3.4





Prep Date:

Metal


_________________________________________________________________________________________________________

Page 2

96 of 96

M86571

55.3.4