Research Analysis Doc Implants

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Elements Not Analyzed: All Gases, C, S, Sc, In, Tb

Date Analyzed: 11-26-08

Note: the entire sample (0.0058 g) was mixed with 0.5 mL nitric acid and 0.5 mL hydrochloric acid and heated on ahotblock set at 110°C for 1 hour. The mixture was cooled, 0.5 mL 30% hydrogen peroxide added, and heated 30 min. Aportion remained undissolved; therefore, silicon or other elements that have low solubility in this acid mixture may bebiased low. The solution was mixed with internal standards, diluted to 10 g, and a 1:100 dilution also analyzed by ICPMS.

0.34.4Zirconium0.1NDMercury

244Zinc0.162Manganese

0.40.88Yttrium5890Magnesium

0.020.05Ytterbium0.5NDLutetium

121Vanadium1NDLithium

0.020.21Uranium0.11.3Lead

0.071.9Tungsten1NDLanthanum

0.320Titanium4460000Iron

0.16.5Tin0.053.6Iridium

0.02NDThulium0.9NDIodine

0.020.23Thorium0.02NDHolmium

0.2NDThallium0.020.10Hafnium0.1NDTellurium0.090.90Gold

0.07NDTantalum0.1300Germanium

0.210Strontium0.02130Gallium

10230Sodium0.020.13Gadolinium

0.02NDSilver0.020.03Europium

502700Silicon0.020.07Erbium

12.5Selenium0.020.11Dysprosium

0.020.13Samarium0.3170Copper

0.028.0Ruthenium0.092200Cobalt

0.020.15Rubidium0.213Chromium

0.022.8Rhodium0.02NDCesium

0.020.66Rhenium0.030.85Cerium

0.020.11Praseodymium301500Calcium

50NDPotassium0.09NDCadmium

0.0210Platinum5NDBromine

101600Phosphorus315Boron

0.023.3Palladium0.03NDBismuth

0.092.2Osmium0.05NDBeryllium

0.10.37Niobium0.196Barium

0.152000Nickel0.417Arsenic

0.020.39Neodymium0.20.37Antimony

0.059.3Molybdenum30260Aluminum

LimitppmLimitppm

DetectionDetection

Sample ID: SN Chunk 080911

Inductively Coupled Plasma - Mass Spectrometry

Trace Impurities by SOP 7040, Rev 9

Client: A&S Research IncJob Number: 110609

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11-26-08Date Analyzed:

821431722Zinc

98168172NDVanadium

99170172NDTitanium

95164172NDThallium103177172NDStrontium

1001720017200NDSodium

97167172NDSilver

891530017200NDSilicon

7412701720NDSelenium

1001720017200NDPotassium

871490017200NDPhosphorus

100172172NDNickel

101173172NDMolybdenum9215.917.20.06Mercury

99170172NDManganese

1001720017200NDMagnesium

99171172NDLithium

95164172NDLead

991710017200NDIron

95163172NDCopper

98168172NDCobalt

98169172NDChromium

1011730017200NDCalcium

90155172NDCadmium

891551722.4Boron

90155172NDBeryllium

98168172NDBarium

83142172NDArsenic

88152172NDAntimony

9919817228Aluminum

% RecResultConcResultAnalyte

SpikeSpikeSpikeBlank

Parts Per Million (µg/g)

Laboratory Fortified BlankSample:

Quality Control Summary

Client: A&S Research IncJob Number: 110609