2
Elements Not Analyzed: All Gases, C, S, Sc, In, Tb Date Analyzed: 11-26-08 Note: the entire sample (0.0058 g) was mixed with 0.5 mL nitric acid and 0.5 mL hydrochloric acid and heated on a hotblock set at 110° C for 1 hour. The mixture was cooled, 0.5 mL 30% hydrogen peroxide added, and heated 30 min. A portion remained undissolved; therefore, silicon or other elements that have low solubility in this acid mixture may be biased low. The solution was mixed with inter nal standards, diluted to 10 g, and a 1:100 dilution also analyzed by ICPMS. 0.3 4.4 Zirconium 0.1 ND Mercury 2 44 Zinc 0.1 62 Manganese 0.4 0.88 Yttrium 5 890 Magnesium 0.02 0.05 Ytterbium 0.5 ND Lutetium 1 21 Vanadium 1 ND Lithium 0.02 0.21 Uranium 0.1 1.3 Lead 0.07 1.9 Tungsten 1 ND Lanthanum 0.3 20 Titanium 4 460000 Iron 0.1 6.5 Tin 0.05 3.6 Iridium 0.02 ND Thulium 0.9 ND Iodine 0.02 0.23 Thorium 0.02 ND Holmium 0.2 ND Thallium 0.02 0.10 Hafnium 0.1 ND Tellurium 0.09 0.90 Gold 0.07 ND Tantalum 0.1 300 Germanium 0.2 10 Strontium 0.02 130 Gallium 10 230 Sodium 0.02 0.13 Gadolinium 0.02 ND Silver 0.02 0.03 Europium 50 2700 Silicon 0.02 0.07 Erbium 1 2.5 Selenium 0.02 0.11 Dysprosium 0.02 0.13 Samarium 0.3 170 Copper 0.02 8.0 Ruthenium 0.09 2200 Cobalt 0.02 0.15 Rubidium 0.2 13 Chromium 0.02 2.8 Rhodium 0.02 ND Cesium 0.02 0.66 Rhenium 0.03 0.85 Cerium 0.02 0.11 Praseodymium 30 1500 Calcium 50 ND Potassium 0.09 ND Cadmium 0.02 10 Platinum 5 ND Bromine 10 1600 Phosphorus 3 15 Boron 0.02 3.3 Palladium 0.03 ND Bismuth 0.09 2.2 Osmium 0.05 ND Beryllium 0.1 0.37 Niobium 0.1 96 Barium 0.1 52000 Nickel 0.4 17 Arsenic 0.02 0.39 Neodymium 0.2 0.37 Antimony 0.05 9.3 Molybdenum 30 260 Aluminum Limit ppm Limit ppm Detection Detection Sample ID: SN Chunk 080911 Inductively Coupled Plasma - Mass Spectrometry Trace Impurities by SOP 7040, Rev 9 Client: A&S Research Inc Job Number: 110609

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Elements Not Analyzed: All Gases, C, S, Sc, In, Tb

Date Analyzed: 11-26-08

Note: the entire sample (0.0058 g) was mixed with 0.5 mL nitric acid and 0.5 mL hydrochloric acid and heated on ahotblock set at 110°C for 1 hour. The mixture was cooled, 0.5 mL 30% hydrogen peroxide added, and heated 30 min. Aportion remained undissolved; therefore, silicon or other elements that have low solubility in this acid mixture may bebiased low. The solution was mixed with internal standards, diluted to 10 g, and a 1:100 dilution also analyzed by ICPMS.

0.34.4Zirconium0.1NDMercury

244Zinc0.162Manganese

0.40.88Yttrium5890Magnesium

0.020.05Ytterbium0.5NDLutetium

121Vanadium1NDLithium

0.020.21Uranium0.11.3Lead

0.071.9Tungsten1NDLanthanum

0.320Titanium4460000Iron

0.16.5Tin0.053.6Iridium

0.02NDThulium0.9NDIodine

0.020.23Thorium0.02NDHolmium

0.2NDThallium0.020.10Hafnium0.1NDTellurium0.090.90Gold

0.07NDTantalum0.1300Germanium

0.210Strontium0.02130Gallium

10230Sodium0.020.13Gadolinium

0.02NDSilver0.020.03Europium

502700Silicon0.020.07Erbium

12.5Selenium0.020.11Dysprosium

0.020.13Samarium0.3170Copper

0.028.0Ruthenium0.092200Cobalt

0.020.15Rubidium0.213Chromium

0.022.8Rhodium0.02NDCesium

0.020.66Rhenium0.030.85Cerium

0.020.11Praseodymium301500Calcium

50NDPotassium0.09NDCadmium

0.0210Platinum5NDBromine

101600Phosphorus315Boron

0.023.3Palladium0.03NDBismuth

0.092.2Osmium0.05NDBeryllium

0.10.37Niobium0.196Barium

0.152000Nickel0.417Arsenic

0.020.39Neodymium0.20.37Antimony

0.059.3Molybdenum30260Aluminum

LimitppmLimitppm

DetectionDetection

Sample ID: SN Chunk 080911

Inductively Coupled Plasma - Mass Spectrometry

Trace Impurities by SOP 7040, Rev 9

Client: A&S Research IncJob Number: 110609

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11-26-08Date Analyzed:

821431722Zinc

98168172NDVanadium

99170172NDTitanium

95164172NDThallium103177172NDStrontium

1001720017200NDSodium

97167172NDSilver

891530017200NDSilicon

7412701720NDSelenium

1001720017200NDPotassium

871490017200NDPhosphorus

100172172NDNickel

101173172NDMolybdenum9215.917.20.06Mercury

99170172NDManganese

1001720017200NDMagnesium

99171172NDLithium

95164172NDLead

991710017200NDIron

95163172NDCopper

98168172NDCobalt

98169172NDChromium

1011730017200NDCalcium

90155172NDCadmium

891551722.4Boron

90155172NDBeryllium

98168172NDBarium

83142172NDArsenic

88152172NDAntimony

9919817228Aluminum

% RecResultConcResultAnalyte

SpikeSpikeSpikeBlank

Parts Per Million (µg/g)

Laboratory Fortified BlankSample:

Quality Control Summary

Client: A&S Research IncJob Number: 110609