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Reboiler Methanol
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The reboiler had been filed with Methanol
The reboiler had been filed with Methanol. The trays had been drained of most of the liquid on them. They had had MeOH-Water mixtures on them.
Below is a graph of the time response of the temperatures in the column.
At point A, the Reboiler temperature is rising. It rises to around 67(C and slowly rises over the rest of the experiment.
At point B, the upper trays' temperatures are rising and they rise to up to 80(C. One thing I'd like for students to explain is how the vapors from the Reboiler at about 70(C can heat the upper trays so that they have temperatures HOTTER than the Reboiler vapor.
At point C, finally, the top tray (Tray 1) reaches its peak temperature. The trays with water on them apparently condense the MeOH vapors from below, diluting the mixture with MeOH and lowering its boiling point. So, the temperature peaks and then falls off.
The liquid on the upper trays (with their water content) then drain down to the lower trays, making the lower trays' boiling point to rise. This is displayed by the humps in the curves at point D.
By the time at point E, The trays have all
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Distillate
Reboiler
T2
T1
T4
T6
T7
T11
T10
T12
A
B
C
D
E
T(D)
T1
T2
T4
T6
T7
T(F)
T10
T11
T12
T(R)
Sept-16-data
Run TimeT(D)T1T2T4T6T7T(F)T10T11T12T(R)CWSCWRLOOSE 9/16/97 - - - 2:50 PM
0.63323.61122.84222.86124.42622.40922.29722.84323.4921.82724.84325.31824.51125.43622.956
1.63323.61722.84122.86724.41322.4122.30522.85823.48421.83424.82725.76524.55625.44322.704
2.63323.61622.83722.86324.40822.41722.31422.84123.4821.79924.8327.66824.55225.48422.693
3.63323.63222.84122.88424.41622.47122.25422.85723.4621.78324.85530.14724.55125.4722.719
4.63323.61222.8522.86324.43122.43822.28322.85723.44221.79424.9532.40124.5525.46422.656
5.63323.61122.83522.88224.43822.47422.25322.86923.44121.85125.14734.59924.53725.46522.692
6.63323.61822.83222.86824.49422.4522.26422.83623.47121.78625.2236.76524.53325.45622.723
7.63323.59722.82222.88824.51122.43722.23522.8923.55321.7925.38738.74624.56225.50122.605
8.63323.61222.8422.88424.55322.45322.27222.88323.56521.79425.56440.59424.59125.50622.448
9.63323.59422.84622.89324.59522.4522.26122.87223.6221.7925.92942.32324.60225.51222.481
10.63323.60522.8622.89624.6422.43622.2522.88523.62821.81826.22343.99824.60525.53522.467
11.63323.60522.85122.90724.63822.45222.24622.87223.68121.81726.69445.62924.59625.52622.452
12.63323.59622.85222.91824.68422.4522.24722.88423.64721.87927.08647.15224.61125.52722.56
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179.66762.78264.25464.70965.82266.14865.1266.61764.39565.32567.11169.15624.92327.67723.316
180.66762.79164.25364.69865.73566.07665.06366.58864.3665.2667.10769.14824.92127.71423.322
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