The reboiler had been filed with Methanol

The reboiler had been filed with Methanol. The trays had been drained of most of the liquid on them. They had had MeOH-Water mixtures on them.

Below is a graph of the time response of the temperatures in the column.

At point A, the Reboiler temperature is rising. It rises to around 67(C and slowly rises over the rest of the experiment.

At point B, the upper trays' temperatures are rising and they rise to up to 80(C. One thing I'd like for students to explain is how the vapors from the Reboiler at about 70(C can heat the upper trays so that they have temperatures HOTTER than the Reboiler vapor.

At point C, finally, the top tray (Tray 1) reaches its peak temperature. The trays with water on them apparently condense the MeOH vapors from below, diluting the mixture with MeOH and lowering its boiling point. So, the temperature peaks and then falls off.

The liquid on the upper trays (with their water content) then drain down to the lower trays, making the lower trays' boiling point to rise. This is displayed by the humps in the curves at point D.

By the time at point E, The trays have all

EMBED Excel.Sheet.8

_936008972.xlsChart1

23.61122.84222.86124.42622.40922.29722.84323.4921.82724.84325.318

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23.61622.83722.86324.40822.41722.31422.84123.4821.79924.8327.668

23.63222.84122.88424.41622.47122.25422.85723.4621.78324.85530.147

23.61222.8522.86324.43122.43822.28322.85723.44221.79424.9532.401

23.61122.83522.88224.43822.47422.25322.86923.44121.85125.14734.599

23.61822.83222.86824.49422.4522.26422.83623.47121.78625.2236.765

23.59722.82222.88824.51122.43722.23522.8923.55321.7925.38738.746

23.61222.8422.88424.55322.45322.27222.88323.56521.79425.56440.594

23.59422.84622.89324.59522.4522.26122.87223.6221.7925.92942.323

23.60522.8622.89624.6422.43622.2522.88523.62821.81826.22343.998

23.60522.85122.90724.63822.45222.24622.87223.68121.81726.69445.629

23.59622.85222.91824.68422.4522.24722.88423.64721.87927.08647.152

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23.44122.84622.90324.85622.90122.33223.51323.152437.45559.53

23.42622.83322.89224.88822.89622.30823.59423.1124.30137.65960.332

23.40822.8322.89424.89122.88822.29823.70523.09924.65238.0961.077

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23.20522.77322.83825.46822.94222.33330.96422.91544.99368.03667.403

23.18422.76722.8425.50622.98322.33434.3922.90651.92369.51767.657

23.17122.75722.83625.52723.07622.34351.10222.95156.55168.79467.776

23.15222.75222.8325.57823.32822.33964.74523.06960.49269.20567.724

23.1222.74722.83125.68627.21822.41364.97423.07362.8469.13967.813

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23.08522.74222.84325.87965.1952.90665.20323.15463.83768.88367.934

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23.02722.75422.88426.50765.30764.34565.27823.07564.14868.767.807

23.01222.7622.87927.16865.3664.3765.34423.11764.17868.57667.748

22.98522.75122.89629.35565.32464.47765.35423.11864.2268.42967.825

22.95122.74222.88264.93665.39964.40865.36523.10864.14768.28667.895

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22.86722.75422.89475.98868.52472.8566.11449.3664.57667.92167.934

22.86722.73322.90875.83769.9173.28866.69570.27464.93867.83868.043

22.83222.74222.91175.54270.58373.82567.01673.91965.28767.80968.102

22.81222.75823.10975.43371.19674.29567.36773.49365.70367.77468.061

22.79822.7523.77275.38571.75474.40867.8273.35666.27667.74168.052

22.77522.79625.19475.42872.17274.5468.25373.22266.71267.72968.233

22.75123.13434.73175.54572.54774.90268.57273.45267.15367.68268.158

22.72523.89372.90575.64372.85974.82269.05873.02867.6367.66968.263

23.01629.50379.28976.10873.19974.89969.35473.50167.7767.6968.208

23.67550.66480.50676.43573.45675.07369.58973.50968.0367.67868.296

24.72963.58880.72576.10173.57875.25770.06773.27868.27767.67268.189

26.161.71381.40775.98273.85975.40870.4773.07268.54967.74268.204

27.61161.72181.62375.99774.12575.40870.71773.12568.74367.78368.131

28.56860.51981.25675.99574.27875.46370.85473.12668.86967.81668.108

29.73661.13580.5777674.39875.46671.01273.10469.00267.8568.064

30.67760.81680.3476.02874.4675.33271.05473.07969.14967.86668.058

33.14260.07379.95575.99874.53575.28471.0672.90969.18367.87368.073

34.87560.26979.39875.98274.59375.21471.09773.13769.26167.88468.036

35.7259.72277.73676.0374.60475.13271.14673.03669.30467.92768.103

36.2959.72977.16776.10174.64575.05271.19972.99969.37667.96668.066

36.88659.89576.43275.97674.67975.01971.2272.9169.45267.98968.068

37.22461.88776.91875.85274.66574.92871.26272.969.52168.02168.106

37.74562.93777.28575.82874.65474.86671.28572.93769.54868.04268.162

38.40663.22377.11975.8674.62774.76871.27472.85469.50868.06868.135

38.99962.89176.90175.88374.5974.72171.27872.84969.52568.09368.127

39.23862.69176.63575.74774.54974.64871.29372.67669.55468.12268.103

39.74762.72776.42275.73974.54274.5671.22772.68669.49768.1368.171

40.03963.32576.29275.66474.50274.47771.26572.69269.48868.13268.197

40.22364.57276.93275.58974.48674.41571.28672.63469.50768.14268.127

40.82364.41377.49475.51174.44674.34771.23972.52769.47468.13768.131

41.3566.08978.08275.38474.35474.26371.24772.4269.45568.12968.179

41.89865.678.29775.27174.29874.19171.21372.40169.46868.10568.223

42.32565.94678.49775.2374.21574.1471.18272.45469.37668.08968.179

42.80464.83878.54875.09174.20574.06571.15672.41869.29668.08868.238

42.83366.11378.65175.09374.12974.02771.16572.30169.28968.07168.168

43.43964.93178.4975.06674.07673.93571.17272.19169.25268.06368.186

44.01866.49678.59675.05274.05573.85571.01872.19369.19668.06268.167

44.43667.68878.76374.93874.01473.85371.08172.24469.22468.06468.145

44.69868.38978.8674.94773.91573.78371.05572.16969.23468.07168.287

45.26166.91778.87574.87173.85973.76871.06172.06969.268.02868.183

45.53367.34378.87574.88173.8573.70371.03172.04869.21467.98868.286

45.89267.11378.66274.81773.77873.6770.97472.19369.22967.97968.183

46.32967.47578.61374.76573.73373.57770.99472.04669.19267.8968.2

46.5767.23378.55774.70773.72373.54970.99672.03969.18567.88168.217

47.14365.83878.35374.72973.66673.47571.00171.94969.20267.86568.233

47.20965.84178.22174.73273.59873.44470.99271.88769.20467.85768.26

47.06365.8978.05174.66673.58673.37170.9487571.91569.18267.84468.284

47.28964.86477.84774.61673.33373.37770.97971.94969.16667.87868.274

47.26463.9477.59374.67172.65773.32371.00571.85469.10867.82368.315

47.36765.86477.46274.57673.4373.29571.00871.84369.19267.83168.281

47.62266.26477.50274.50273.38173.27270.99171.76169.11567.82968.31

47.77666.68677.4874.40673.33773.23171.00471.78569.1267.79468.359

47.71267.06977.58874.38373.3273.17971.01771.77269.04867.81968.317

48.01166.14577.43174.32973.22473.12370.96471.74369.06967.76668.315

48.26371.6178.05474.50373.30773.17570.92671.69269.03167.74868.397

53.18375.25679.09174.40173.27573.14270.70171.8369.06967.7168.433

60.29576.15478.91274.5473.17973.18170.66872.10869.4967.67168.43

65.33476.25378.60274.7373.14473.25570.6372.19169.53967.63368.479

67.56875.85177.87474.77173.1373.29770.62572.16369.58967.61768.578

67.70375.29577.45874.82473.12573.38470.65372.27269.60267.62868.519

67.69374.8877.18674.96873.19273.60370.77372.23969.68867.56268.541

67.7574.21376.51875.07373.24673.64770.88872.44469.80667.54868.595

67.58373.63775.87875.11273.29273.69870.94872.33769.84967.54568.584

67.33872.99475.28975.1973.39673.75870.9872.38269.92367.53468.607

67.1272.37674.49775.15973.4773.86771.09672.3170.01267.52468.628

66.82171.77473.85775.22173.54973.88871.24572.29170.15367.52268.554

66.58971.20873.26575.2273.61173.94271.27372.41870.17867.51468.609

66.39670.79172.73475.26373.66773.98271.32372.35970.27667.49568.744

66.60370.19972.15775.22373.72673.98771.43272.20970.37567.49568.712

66.1469.82671.74275.18573.78573.98271.4972.10170.38267.49468.706

65.75469.31571.28775.14673.85673.97371.53672.04270.45967.50768.714

65.5368.90670.83175.07273.8473.88771.63871.99670.54367.50968.697

65.26868.64370.41674.97173.87673.8571.72271.85870.62567.50268.626

65.33968.28570.03574.8273.86673.74771.72971.74570.72467.52368.689

65.06267.95969.67174.66873.84273.64171.78971.44770.72467.52168.726

64.81267.65269.31574.46973.80273.5271.89471.19370.72467.51268.703

64.68767.38668.97774.27873.73573.37171.85770.98970.77567.51668.709

64.5967.09168.65374.07173.70573.22571.83270.71470.70867.52568.815

64.466.72268.35273.80173.60173.03671.8370.43470.74767.52268.795

64.2366.67968.07173.56273.50672.8671.83270.16770.67767.52568.713

64.11466.49467.84173.2973.38372.66771.80569.83770.64767.52368.87

64.23466.25567.60672.99373.2472.48171.73269.62870.53867.51268.825

63.98866.11767.38972.74373.10272.25771.74269.4570.58967.52568.854

63.85966.0767.17372.43872.95971.99771.76269.18670.49567.49968.88

63.7465.80267.00372.14372.78971.78671.57468.96170.43867.50868.952

63.84365.66466.80371.90972.63971.55271.46668.64170.2767.53168.937

63.64365.54266.64571.54272.43271.2771.39368.4970.18967.50168.92

63.56865.42166.50171.28372.22471.03271.3368.20370.14867.50468.795

63.47565.32266.33970.98872.00470.77271.22467.99670.02367.568.929

63.52365.23866.23470.71371.78370.49871.10967.75569.91167.49968.956

63.39865.14166.07970.40871.58570.21571.0167.58169.77867.49668.944

63.31765.07865.96970.14471.34569.92970.85267.37569.65567.49268.891

63.32664.98965.85869.90271.1169.66470.72167.17369.47367.47468.878

63.24764.92665.7669.6270.87469.41670.5846769.33367.48468.97

63.21564.86965.67969.38970.65569.18370.45366.77369.21767.46468.986

63.14964.81365.59569.15970.42368.97670.2966.61269.07567.47368.904

63.14164.75965.52968.92870.20868.72970.1566.46568.91967.44968.987

63.11364.71865.45368.74569.98868.50769.99366.27768.74167.43569.021

63.11564.67365.37868.52669.77568.2869.83766.17668.58667.41868.984

63.0664.63465.3368.25869.55468.0669.65466.00168.41867.41369.025

63.03564.58665.27368.11369.33467.81269.52365.87668.26167.41269.054

63.06164.57365.22267.9669.14667.6369.37265.74768.10767.39868.96

63.00564.53665.18567.77468.92567.44469.20465.62967.97767.38269.085

62.99764.51465.12967.62468.74367.27769.06165.52867.79867.37568.971

62.98564.49665.09467.47768.54667.08568.89965.41167.64467.36769.134

62.9464.47365.05667.33668.37966.94268.7665.32467.48767.34969.043

62.91464.44565.02467.19768.19966.78268.59465.25767.31867.33568.979

62.9164.42765.00467.07468.02566.60968.4565.16267.19367.31569.071

62.8964.41164.96166.95167.85366.48868.32865.0867.06267.31469.147

62.90464.38264.9366.83967.69166.35968.18565.00666.967.29669.092

62.87964.36564.91366.74567.56466.24468.02764.93866.73267.29169.134

62.83164.34764.89866.64767.39966.11167.89564.88666.63467.28369.066

62.85564.3564.86366.53867.26966.00267.7764.81966.46267.25369.074

62.84364.33564.83966.39267.12865.89967.63364.76966.35267.23769.075

62.8464.31664.83766.3867.00265.81367.49764.73466.23167.22669.019

62.83364.3164.80166.26666.87565.66267.37664.66466.15867.22569.092

62.84564.30264.78766.18666.77165.58767.2764.59965.9967.21769.037

62.80764.28664.77966.14366.65265.51867.14964.56965.93667.20169.111

62.82164.2864.75866.06366.56165.43467.06964.5165.77867.19769.097

62.82264.29164.73866.01266.48365.3666.9764.47665.67467.17469.016

62.82164.27864.74665.94466.37865.30666.87564.4465.62867.16169.075

62.79264.26464.74865.91466.29565.23266.78864.41365.53667.16269.029

62.79764.2664.71665.85366.22365.17366.69964.38165.4467.13869.145

62.78264.25464.70965.82266.14865.1266.61764.39565.32567.11169.156

62.79164.25364.69865.73566.07665.06366.58864.3665.2667.10769.148

62.78964.23464.68765.68866.01565.01766.4764.30465.19167.09369.067

62.77264.21564.68365.70865.92564.97466.37864.33165.15667.05569.084

62.78464.22164.68265.67665.88164.92966.31464.27865.05267.04569.135

62.79464.22264.67765.62765.84264.88266.25464.25764.98367.02969.208

62.77464.24964.65865.57265.7964.8466.20464.32664.89467.00169.082

62.7764.21564.6765.57965.72464.80766.14964.21564.86966.98769.149

62.7664.21564.6565.52165.68164.79966.08464.19664.77966.96969.171

62.77564.21564.65165.50865.63764.73366.03964.19364.78266.95169.141

62.77564.22264.66265.49365.59164.69565.98364.16864.67766.92869.144

62.79364.22964.64565.45565.54364.67965.94464.16464.65366.92669.192

62.75964.22664.64665.44365.52864.65765.964.15364.61666.90869.183

62.75364.21564.66365.45665.49264.64665.84864.15464.58466.89569.208

62.75664.21264.62465.4265.46864.60865.81564.13264.55266.87169.201

62.77264.20764.64665.41365.44564.58365.80364.12664.51766.8669.263

62.75864.19864.62965.4165.41264.55565.74264.11364.49666.82769.158

Distillate

Reboiler

T2

T1

T4

T6

T7

T11

T10

T12

A

B

C

D

E

T(D)

T1

T2

T4

T6

T7

T(F)

T10

T11

T12

T(R)

Sept-16-data

Run TimeT(D)T1T2T4T6T7T(F)T10T11T12T(R)CWSCWRLOOSE 9/16/97 - - - 2:50 PM

0.63323.61122.84222.86124.42622.40922.29722.84323.4921.82724.84325.31824.51125.43622.956

1.63323.61722.84122.86724.41322.4122.30522.85823.48421.83424.82725.76524.55625.44322.704

2.63323.61622.83722.86324.40822.41722.31422.84123.4821.79924.8327.66824.55225.48422.693

3.63323.63222.84122.88424.41622.47122.25422.85723.4621.78324.85530.14724.55125.4722.719

4.63323.61222.8522.86324.43122.43822.28322.85723.44221.79424.9532.40124.5525.46422.656

5.63323.61122.83522.88224.43822.47422.25322.86923.44121.85125.14734.59924.53725.46522.692

6.63323.61822.83222.86824.49422.4522.26422.83623.47121.78625.2236.76524.53325.45622.723

7.63323.59722.82222.88824.51122.43722.23522.8923.55321.7925.38738.74624.56225.50122.605

8.63323.61222.8422.88424.55322.45322.27222.88323.56521.79425.56440.59424.59125.50622.448

9.63323.59422.84622.89324.59522.4522.26122.87223.6221.7925.92942.32324.60225.51222.481

10.63323.60522.8622.89624.6422.43622.2522.88523.62821.81826.22343.99824.60525.53522.467

11.63323.60522.85122.90724.63822.45222.24622.87223.68121.81726.69445.62924.59625.52622.452

12.63323.59622.85222.91824.68422.4522.24722.88423.64721.87927.08647.15224.61125.52722.56

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179.66762.78264.25464.70965.82266.14865.1266.61764.39565.32567.11169.15624.92327.67723.316

180.66762.79164.25364.69865.73566.07665.06366.58864.3665.2667.10769.14824.92127.71423.322

181.66762.78964.23464.68765.68866.01565.01766.4764.30465.19167.09369.06724.91627.61223.315

182.66762.77264.21564.68365.70865.92564.97466.37864.33165.15667.05569.08424.90527.68623.306

183.66762.78464.22164.68265.67665.88164.92966.31464.27865.05267.04569.13524.88427.80123.33

184.66762.79464.22264.67765.62765.84264.88266.25464.25764.98367.02969.20824.87227.63823.355

185.66762.77464.24964.65865.57265.7964.8466.20464.32664.89467.00169.08224.85127.82323.299

186.66762.7764.21564.6765.57965.72464.80766.14964.21564.86966.98769.14924.83827.823.276

187.66762.7664.21564.6565.52165.68164.79966.08464.19664.77966.96969.17124.84227.73523.315

188.66762.77564.21564.65165.50865.63764.73366.03964.19364.78266.95169.14124.84227.75923.281

189.66762.77564.22264.66265.49365.59164.69565.98364.16864.67766.92869.14424.84827.66623.226

190.66762.79364.22964.64565.45565.54364.67965.94464.16464.65366.92669.19224.85827.76623.286

191.66762.75964.22664.64665.44365.52864.65765.964.15364.61666.90869.18324.87427.92423.306

192.66762.75364.21564.66365.45665.49264.64665.84864.15464.58466.89569.20824.89927.88623.294

193.66762.75664.21264.62465.4265.46864.60865.81564.13264.55266.87169.20124.90428.01523.315

194.66762.77264.20764.64665.41365.44564.58365.80364.12664.51766.8669.26324.93928.09123.115

195.86762.75864.19864.62965.4165.41264.55565.74264.11364.49666.82769.15824.96127.84523.196