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A PARADIGM SHIFT IN CRITICAL (DYNAMIC) ASSETS CARE – FUNCTIONAL
PROPERTIES PROCESS ANALYZERS
Pareto Principle and Critical Dynamic Assets Care
Typical Lubrication Oil Process Properties Monitored
Process Properties
Kinematic viscosity (40°C and 100°C) Water content/activity Temperature Blotter spot test Oxidation Sulfation Organic contamination Wear and additive elements (AES) Total wear (ferous & non ferouos) - Particle quantifier index (PQI)
Process Analyzers FundamentalsPROCESS MONITORING = INSTRUMENTS
Options available in the marketA. Property inferred via direct measurement
Pressure Temperature Density Viscosity TAN
Options available in the marketB. Property inferred via correlation measurement
NIR//FTIR MRA RAMAN
Process Analyzers FundamentalsPROCESS MONITORING = INSTRUMENTS
Analyzers FundamentalsELECTROMAGNETIC SPECTRUM
Property inferred via correlation measurement
SPECTROSCOPY nmr / esr / microwave IR / vis / UV X-ray
WAVELENGTH 10m 100cm 1cm 100m 1m 10nm
cm-1 100 500 2000 5000 10,000 20,000 30,000m 100 20 5 2 1 0.5 0.33
far-IR mid-IR near-IR visible/UV
Diesel Fuel Spectra
-1
0
1
2
3
4
5
6
7
6500.0 5921.5 5342.9 4764.4 4185.8 3607.3 3028.8 2450.2 1871.7 1293.1
46.3 clr-prod47.5 boost30048.2 boost60048.9 boost900
SPECTRA OF FOUR SAMPLESmid-IR range: 6500 to 1000cm-1
clear product CN = 46.3+ 300ppm booster CN = 47.5+ 600ppm booster CN = 48.2+ 900ppm booster CN = 48.9
measured by engine
mid-IR range accessible by usingINTERFEROMETER
area zoomed
LaborChemieConsulting
NIR - Technik
Options available in the marketB. Property inferred via correlation measurement
NIR//FTIR
Process Analyzers FundamentalsPROCESS MONITORING = FUNCTIONAL PROPERTIES ANALYZERS
Diesel Fuel zoomed mid-IR
0
0.2
0.4
0.6
0.8
1
1.2
1800.3 1761.7 1723.2 1684.6 1646.0 1607.5 1568.9
clr-prodboost300boost600boost900
SPECTRA OF FOUR SAMPLESzoomed mid-IR : 1800 to 1500cm-1
clear product CN = 46.3+ 300ppm booster CN = 47.5+ 600ppm booster CN = 48.2+ 900ppm booster CN = 48.9
measured by engine
mid-IR range shows clear peakcaused by Alkyl-Nitrate booster
Calibration in mid-IR rangegives good CN predictionboth on clear product and
on addivated product
LaborChemieConsulting
NIR - Technik
Options available in the marketB. Property inferred via correlation measurement
NIR//FTIR
Process Analyzers FundamentalsPROCESS MONITORING = FUNCTIONAL PROPERTIES ANALYZERS
Lubrication Oil Aging
LUBRICATION OIL AGINGN AS SEEN IN IR
Oil Aging Sensor - ηνραΤ
OIL AGING SENSOR
SENSOR SIZE 36 x 38 MM !
Sensor mounting Ø100 mm pipe
Sensor mounting Ø30 mm pipe
Oil Aging Sensor
Calibrated ranges
Density: 600 kg.m-3 ... 1500 kg.m-3
Viscosity: 0.3 cP ... 400 cP (500 cSt)Water activity: 0 aw ... 1 awTemperature: 0 °C ... 85 °C
Accuracy(typical, max)
Density: 0.1 %F.S. (typ) 0.5 %F.S. (max)Viscosity: 0.8 %F.S. (typ) 2 %F.S. (max)Water activity: 1 %F.S. (typ) 3 %F.S. (max)Temperature: 0.2 °C 0.5 °C
Repeatability
Density: 0.1 %F.S.Viscosity: 0.5 %F.S.Water activity: 0.5 %F.S.Temperature: 0.2 °C
Real-time calibrated output Density (kg.m-3), Viscosity (cP - cSt), Water activity (aw), Temperature (°C)
Operating conditions Temperature: -40 °C ... 125 °CPressure: Atm ... 10 bar (burst pressure 50 bar)
Water and Lubrication Oils
WATER ACTIVITY AND LUBRICATION OILS
Water and Lubrication Oils
WATER ACTIVITY AND LUBRICATION OILS
Water and Lubrication Oils
WATER ACTIVITY AND LUBRICATION OILS
Water and Lubrication Oils
WATER ACTIVITY AND LUBRICATION OILS
Water Activity Sensor
Water Activity Sensor
Out
er la
yer
40 n
m fi
ness
e
Water Activity Sensor
Calibrated ranges Water activity: 0 aw ... 1 aw
Temperature: 0 °C ... 85 °C
Accuracy(typical, max)
Water activity: 1 %F.S. (typ) 3 %F.S. (max)Temperature: 0.2 °C (typ) 0.5°C (max)
Repeatibility Water activity: 0.5%F.S.
Temperature: 0.2°C
Real-time calibrated output Water activity (aw), Temperature (°C)
Operating conditions Temperature: -40°C ... +120 °CPressure: Atm ... 50 bar
Wireless P & T Sensor
Pressure & Temperature Sensor
Out
er la
yer
40 n
m fi
ness
e
Moubray PrincipleW
ear p
artic
le c
once
ntra
tion
Wear particle size being generated, microns
1 10 100 1000Source Moubray et. all
On-line metallic wear debris
ON-LINE METALLIC WEAR DEBRIS SENSOR
ON-LINE METALLIC WEAR DEBRIS SENSOR
On-line metallic wear debris
Total Wear Metalic Debris
Detection Range: >40 μm Ferrous & >135 μm Non-Ferrous Metallic. Simultaneous quantification of metallic composition, size category & particle count
Fluid Compatibility: Petroleum, synthetic oils and water/oil emulsionsFluid environment: <10 Bar @ -20°C to 65°C, 0.28 m/s (1.3 Litres/minute) to
4.5 m/s (21 Litres/minute), <500 cST @ 40oCConnections 3/8" BSPP female, 10 mm ID x 120 mm L boreAmbient Temperature: -20°C to 65°CAnalogue Outputs: 2 x Opto isolated 4-20 mA, 1 x Alarm contacts (0.1A max),
RS232, RS485, Modbus RTU (over RS485), CANopenInput: +24 VDC +/- 10%, Calibration Push ButtonOther: IP66ATEX Marking: II 2 G, Ex mb IIB T6, Ta = -20ºC to + 55ºC
Total Wear Ferous Debris
Range: 0 - 2000 ppmDetection: Total Ferrous Wear DebrisFluid Compatibility: Petroleum, synthetic oils and water/oil.Connections: Oil 1/8” (Inlet BSP female, outlet BSP female)Communications: CAN, RS232, RS485Analogue Output: Opto isolated 4 - 20mAFluid Temperature: -20°C to 65°C (-4°F to 149°F)Max. Fluid Pressure: 10 Bar (145 psi)Power Supply: 18 - 30 VDCProtection: IP65Ambient temperature: -20°C to 65°C
Alconex Corporate Outline
Staff: 30 people
(28 university graduates)
Founded August 1990
Romanian Private
Company
2011 Turnover € 3.5 million
Main Lines of Activity
Technology provider for the Oil Patch
Meter checking and
proving
Oilfield equipment packager
Project integrator
Core ExpertiseGas and crude processing : separation,
dehydration, filtration
System integrator; equipment packager
Liquids & gas metering solutions provider; extensive knowledge on custody transfer
Industrial Metrology (liquids & gas). Meter checking, proving and calibration
Metering systems condition monitoring and maintenance
Consulting : metering and processing
Oilfield Equipment Packager
ROMGAZ – Sâncel Gas Processing Unit - 2009
Oilfield Equipment Packager
ROMGAZ – Tămăşeşti Gas Processing Unit - 2010
PETROFAC UK – CPI Separator - 2011
Oilfield Equipment Packager
PETROFAC UK – Backwash Water Filtration Skid - 2011
Oilfield Equipment Packager
MOBILE CFF UNIT
Pump
Control unit
Filtration Equipment Packager
FILTER HOUSINGS
CERAMIC MEMBRANE FILTRATION UNIT
Crossflow Filtration Packager
Metering Solutions
Oil Terminal Romania - Crude Oil Carrier Custody Transfer Unloading Terminal. 2000
OMV Petrom – Fuel Depots Custody Transfer Metering
Skids - 2005
Metering Solutions
SNGN Romgaz SA – 240 Custody transfer metering points
SNGN Romgaz Custody transfer gas stations
Process GC
Water Dewpoint Monitor
GC & Dewpoint Sampling Points
OMV PetromWaterflooding monitoring –
400 units
Metering Solutions
Metering Solution-Gas Quality Monitoring Process GC
Sitrans CVSiemens
Danalyzer 700Emerson
FXi 930Hamilton-S.
Metering Solutions
OMV PETROM – Custody Transfer Skids-2008
Mobile Calibration Unit -2008
Industrial Metrology Services
Licensed Metrology Laboratory
Laboratory traceable to Romanian and German W&M
2 Mobile calibration units
Legal Metrology proving & checking
Industrial metrology portfolio: pressure, temperature, density, water cut
Consulting : metering and checking
THANK YOU !
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