2020 SPRING Semester · 2020-03-30 · 2020 SPRING Semester. General Chemistry Lab II (CH104)...

2020 SPRING Semester

General Chemistry Lab II (CH104)Exp.0. Orientation

Department of Chemistry

2020. 3.

Class:

TA Name: My office: Extension Number: E-mail:

Introduction Lab Schedule Method of Evaluation / Grading Additional Information

Today’s Topics

Introduction

• CourseInformation• CourseObjective• CourseRequirement

1. Course Information

1) Course Number: CH104

2) Lecture: Experiment: credit = 0:3 h:1

-Lab: 402, 406 & 704(Goong-Ni Laboratory Building, E6-5)

2. Course Objective

1) To teach basic laboratory techniques

2) To introduce to elementary methods of assessingthe significance of experimental measurements

3) To provide experiences that enable the studentsto acquire positive attitude toward CHEMISTRY,or SCIENCE

1) Preparation in advance for experimental work.• Pre-laboratory reading preparation for successful

experimentation.• Pre-lab quizzes are or pre-lab reports are required

relating to the experimental details.

2) Wearing of eye protection and lab clothing at all timeswhile in the laboratory.

3. Course Requirement

3) Writing up and submission of lab reports.

Includes the following (but see evaluation):

Observations and experimental detail.

Detailed method of processing the experimentaldata. (For Quantitative analytical experiments)

Calculations and Conclusions regarding theaccuracy and the precision of experimental resultsand errors and the inherent errors based on themeasurements.

Lab Schedule LaboratoryExperiments TimeTable Manual General ChemistryWebsite

Online Lab class (March 30 ~ April 24, Exp.0 ~ 3)-Video & Q & A board: klms.kaist.ac.kr-Homework & Report Submission: www.turnitin.com

Offline Lab class (May 11 ~ June 26, Exp.4 ~ 10)

-Q & A board: klms.kaist.ac.kr-Homework & Report Submission: www.turnitin.com

1. Laboratory Experiment(Experiment # in the lab manual)

Exp.0. Introduction, Schedule, and Method of Evaluation-Online ClassExp.1. Factors Affecting Reaction Rates (Experiment 23) -Online ClassExp.2. A Rate Law and Activation Energy (Experiment 24) -Online ClassExp.3. Natural and Synthetic Polymers: The Preparation of Nylon -Online ClassExp.4. Aspirin Synthesis and Analysis I: IR Spectroscopy (Experiment 19)Exp.5. Aspirin Synthesis and Analysis II: Proton NMR Spectroscopy (Experiment 19)Exp.6. Paper Chromatography (Experiment 21)Exp.7. Transition Metal Complexes (Experiment 36)Exp.8. Spectrophotometric Metal in Analysis (Experiment 35)Exp.9. Enzyme Kinetics Exp.10. Hard Water Analysis (Experiment 21)

2. Time Table Date

(Friday)

Experiment #/ Lab#

Mon Tue Wed Thu Fri

3/20 [No lab]

3/27 [No lab]

4/3 [Exp.0.]/ online

4/10 [Exp.1.]/ online

4/17 [Exp.2.]/ online

4/24 [Exp.3.]/ online

5/1

5/4-5/8 Mid-term Examination period

Period

(Friday)

Experiment #/Lab #

Mon Tue Wed Thu Fri

5/15 [Exp.4.]/ Lab 402

5/22 [Exp.5.]/ Lab 402

5/29 [Exp.6.]/ Lab 406

6/5 [Exp.7.]/ Lab 704

6/12 [Exp.8.]/ Lab 402

6/19 [Exp.9.]/ Lab 406

6/26 [Exp.10.]/ Lab 704

7/3 Final Examination Period

3. Manual

Laboratory Manual for Principles of General Chemistry, 10th Edition, J. A. Beran, John Wiley & Sons, Inc.

You can purchase the lab manual at the bookstore of main library (E9).

4. General Chemistry Website

www.gencheminkaist.pe.kr

The experimental procedure file with photos will be uploadedcontinually at a link, [Experimental Procedure] of left frame on thegeneral chemistry website. Please look over the procedure on themanual and the file in advance sothat you can complete your worksuccessfully.

Method of Evaluation and Grading

• Grading&ExaminationInfo• Pointdistribution

1. Grading & Examination Info

Total 10 Experiments X 100 pts = 1000 pts :A(45-50%), B (45-50%), C-D (5%), F

F Grade;• Unexcused absence from more than 3 times.• Score range below 550 points

Examination Information: No examination.

2. Point Distribution2-1) For online lab class: Exp. 1 ~3

Point distribution per One Experiment = 100 points1. Pre-Laboratory Assignment (30 pts)2. Laboratory Reports (40 Pts)

a. Introduction b. Result c. Discussion Summary Assessing the results Conclusions

d. Reference 3. Post-Laboratory Assignment: Questions (30 pts)

Part A. Pre-lab Assignment (30 pts)

□ Theory (10 pts) and Procedure( 10 pts) Summary□ Question ( 10 pts)Teaching assistant will let you know #s of the problems to be submitted out of Pre-lab Assignment of each topic on the lab manual.

Part B. Laboratory Report (40 Points)

Date (If missing,-3 pts)Name (If missing, -3 pts)Co-worker (If missing, -3 pts)Introduction (~10 lines) Summary of introduction on the lab manual. (If missing, -5 pts)Results 0 Data orAnalysis

0 Calculations (with units)0 Graphs0Tables

Discussion (20~40 lines) 0 Summary0 Assessing the results ( Analysis)0 Conclusions

Reference (If missing, -3 pts)

□ Report Template

Part C. Laboratory Questions

□ Points: 0 ~ 30 pt□ Explanations

Teaching assistant will choose and assign the number of problems out of Laboratory Question of each topic on the lab manual.

2-2) For Offline lab class: Exp. 4 ~10Point distribution per One Experiment = 100 points

1. Pre-and post-Laboratory quizzes (30 pts)2. Attitude (20 pts)

a. Lateness (5 pts)b. Lab Safety or Cleanup (10 pts)c. Concentration or Comprehension (5 pts)

3. Laboratory Reports (40 Pts)a. Introduction b. Result c. Discussion

Summary Assessing the results Conclusions

d. Reference 4. Laboratory Questions (10 pts)

Part A. QUIZ (30 points)

□ # of Problems: 8 ~ 10 questions□ Sources Pre-Laboratory Assignment Lab Report Laboratory Questions

Part B. Attitude (20 points)

□ Section: Attendance-Late Coming□ Penalty points: -2 ~ -5 pts□ Explanations

Whenyouarriveat thelabbeforeTAcallsyour name, youget a fullscore, 5pts. If youarrive10minlateafterthebeginningof thelab, youget 3pts. Whenyouarrivebetween10minand20min, youwill get thescore, 0pts. Forbeing20minuteslate, youcan't participateinthelabexperiment. (Nochanceanymore.)

Part C. Attitude

□ Section: Attendance-Absencewithout notice□ Penaltypoints: -100pts□ Explanations

If you are absent 3 times without any notices, F credit will berecorded.

Thelabexperiment isONLYpermittedinregisteredclass. Only valid excuses are illness (with a valid doctor's excuse) or

unusual circumstancebeyondyourcontrol (deathinfamily), etc. Thestudent must submit writtenverificationof themfor anexcused

absence.

□ Section: Lab Safety & Cleanup□ Penalty points: -5, -10 pts□ Explanations

Personal Protective Equipment: Safety glasses, Attire (lab coat) Wear approved eyeprotectionat all timeswhileinthelaboratory. Thepenaltyis-5ptsforthis.

Careof balance: Anyonefoundtobe leavingspilledchemicals inthebalancearea orbenchwill lose5pts foreachviolation. Anychemicalsspilledonthebenchtoporthebalancepanduringtransferaretobecleanedupimmediatelybythestudent.

Cleanup of Lab Bench: The students are responsible for cleaning up their immediatelab bench area before leaving lab. Thismeans wiping up any spillsand disposing ofany paper towelsfromthebenchtopandsink. Failuretodothisresult inadeductionof -5pts.

Disposal of chemicals: DONOTdiscardchemicalsdownthelaboratorysink. Thepenaltyis-5ptsforthis.

□ Section: Concentration & Comprehension□ Penalty points: -5 pt□ Explanations

Checklists playingwithgossiping cell phone(touching, ringing, chatting), andsoon Repeatedfailureof thesameexperiment

Thepenaltyis-5ptspereachcase.

Part D. Laboratory Report (40 Points)□ Report Template

Date (If missing,-3 pts)Name (If missing, -3 pts)Co-worker (If missing, -3 pts)Introduction (~10 lines) Summary of introduction on the lab manual. (If missing, -5 pts)Results 0 Data orAnalysis

0 Calculations (with units)0 Graphs0Tables

Discussion (20~40 lines) 0 Summary0 Assessing the results ( Analysis)0 Conclusions

Reference (If missing, -3 pts)

Student must submit Result SummarytoTAbeforeleaving lab.

Labpartner will sharedata, however separate labreport must bewrittenbyeachstudent.

Duplicatereportswill begivenazero.

Allowing someone to submit or resubmit your work as theirs willresultsinazeroforbothparties.

Part E. Laboratory Questions

□ Points: 0 ~ 10 pt□ Explanations

You should solve the questions and submit them in lab class to your TA. Identical question answers will receive a zero.

Additional Information

• Homework&Labreportsubmission• Latereportpolicy• LaboratoryMakeuppolicy

1. Homework & Report Submission

1) Onlinesubmission: www.turnitin.com2) Createyouraccount. EnterClassIDandPassword(providedbyTA).3) EnteryournameinKoreanorEnglish.4) Submissiondue: Beforethenextexperiment5) Postinggrade: Within7daysfromduedateof thereport6) Plagiarism results in zero for all reports involved (determined by

Chief TAandInstructor).7) Late submission is not allowed in Turnitin website. You should send

yourlabreport toyourTA.

•Blue - No matching text•Green - One word to 24% matching text•Yellow - 25-49% matching text•Orange - 50-74% matching text•Red -75-100% matching text

8) Student should create and upload only one MS-word file for each experiment in Turnitin.

Turnitinaccepts submissions in this format: Microsoft Word™ (DOC and DOCX)

Experiment 1 ~ 3 Experiment 4 ~ 10

• Pre-lab assignment• Laboratory Report

• Post-lab Assignment

• Laboratory Report• Post-lab Assignment

2. Policy regarding late lab reports

Labreportsaredueat thestart of thescheduledexperiment, unlessotherwiseinstructed. Yourscoreonthat report will bereducedby apercentage, basedonwhenyourTAreceivedyourreport.

Within24hours: -10pointsMorethan24hours: -40points

3. Laboratory Makeup Policy Make-ups are only for those who missed labs for a legitimate reason and got TA’s

permission to make up lab. (Give a written documentation to your lab TA during the next lab or bring it to his lab and ask permission to make up the missed lab)

Missed labs without a valid excuse, shall count as zero (0) and the student will not be allowed to make up this missed lab.

Students are not allowed to make up late lab reports or to make up more than two experiments during the scheduled lab make-up time. Re-doing labs is not possible.

Missed scheduled make-ups will be counted as zero and will not be rescheduled unless exceptional circumstances exist.

If more than three labs are missed with or without valid excused student shall fail the course.

Your lab TA will let you know the make-up schedule and the due dates for make-up reports.

Comments

• Familiarizeyourselfwith…• Think about these for both students

andTA• Duedateof labreport• Experimental Group

1. Familiarize yourself withthe following items

a. The nearest telephoneb. Eye wash & Shower Locationc. Fire blanket Locationd. Fire Extinguisher Locatione. Safety glasses holderf. Chemical Fume & Arm Hood

2. Familiarize yourself with the following Safety Concerns

a. Report all injuriesb. Attire: Safety glasses….c. Acid and Basesd. Cleanup

3. Think about these…..

1) A Successful Student…a. Responsible and activeb. Ask questionsc. Are good time managers

2) A Good Teaching Assistant………..a. Grades lab reports correctly and fairlyb. Gives feedback on the lab report that is helpful c. Isenthusiastic about teaching the lab

4. Due Date of Lab Report

The submission will close at 23:59 on the day before next lab class begins

5. Experimental Group

One or Two Student(s)Per One Experimental Group

There are four objectives for you, thestudent, in the laboratory:

Todeveloptheskillsnecessarytoobtainandevaluateareliableoriginal result. Torecordyourresultsforfutureuse. To be able to drawconclusions regarding your results (with the aid of some coaching and

readinginthebeginning). Tolearntocommunicateyourresultscriticallyandknowledgeably

By attentively reading over the experiments in advance, and by carefully following directions andworkingsafelyinthelaboratory, youwill beabletoaccomplishall theseobjectives.