Waste Plastic to Oil

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Pyrolysis Machine Converting Waste Plastic into Oil

ADITYA RECYCLINGBangalore

www.adityahitechmachines.com


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The Project Converting Waste Plastics into Oil

Model => Batch Type ECP-2011




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Depletion of Fossil Energy

High efficiency (average80%) High quality (light oil level)

The Value of Business!

Intensified Regulation of Greenhouse Gas Emissions

Rapid Increase of the need to Improve Nvironmental Pollution

The plan to Overcome New Regulations

Protection of the Earth, the Nation,

the Environment

Creation of New Energy


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Bio Energy

Alternatives for the Future!

Solar Energy Wind Power Generation Energy

Nuclear Energy


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Vinyl Waste

Creation of Renewable energy!

Waste Fishing Net, Fishing Gear

Used Waste Lubricating Oil Wasted Tires

Cracked Oil from Wasted Tire Cracked Oil from Household Waste Vinyl


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The Relative Value of Oil Conversion Projects

# TOE : Tonnage of Oil Equivalent

Refinery Equipment


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Use and Value of Produced Oil from Pyrolysis

Waste Plastics, Waste Oil Conversion to Fuel Oil


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Simple Process, Low Investment

The Best Stability, Safety

The Best Oil Conversion Profitability

Leader of environment-friendly technology, Ecocreation !!

Ecocreation is an environment-friendly

company that cares about future environment of the earth and is a global leading company that opens a new era of low carbon green growth by reducing

CO2 emission for invigoration of resource circulation and prevention of global warming through production of

environment-friendly products.


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폐기물

Oil

Reforming R.P.F( Solid Polymer ) Reforming Waste Plastic

Nitrogen, Atmospheric Pressure Condition Pyrolysis Emulsion ( 380~480℃ Heating Fluid )

Apply liquefaction, Separation TTechnology Based Catalyst

Typical yields : Polymer Waste Kerosene, Diesel more than 80%, Naphtha around 15%, Gas around 3%, CHAR (Coke) around 3%

Pyrolysis Refined Oil

Hybrid Cracking Emulsion Technology

PP(Poly-Propylene), PE( Poly-Ethylene ) PS(Poly-Styrene), PPT( Polyphenylene Terephthalate )


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Process The first pyrolysis of waste and secondary catalytic cracking with catalyst

Operation Type Batch type

Input Plastics PP, PE, PS

Yield Approx. 75 ~ 80 % (It can be different according to the waste plastics type)

Electric Capacity Three-Phases (220V or 380V)

Produced Oil Component

Naphtha, Kerosene & Diesel Fraction

Operating Cost Low operating cost due to the use of recycled oil and waste gas from self production

Safety Less risk of explosion and fire due to nitrogen substitution

It is not necessary to separate, shred and clean the waste plastics.

Plant Size by 12,000mm(W) X 10,000(L) X 7,000(H)

Space required for installation => Variable for capacities Notice => Waterproof / Protection against wind must in roof

Period required for installation by within 10 days site installation


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Power Start ON

Gas Collector ON


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The Main Process Flow Diagram 1

Input

(Waste Plastic) (Compress) (Compressed Stuff)

(Separation/Cooling) (Contact Catalytic Reforming Cracking) (Pyrolysis) (Refining/Storage)


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Catalyst Column secondary catalytic cracking

Primary classification process

Primary cooling process

Storage / Ship

Material Screening Compression

input Material and Melting

Primary fusion

decomposition

Input liquid cracking catalyst

Input coking inhibitor

Decomposition of chlorine compounds, Input inhibitory catalyst

Input GUM inhibitor,

Neutralization reagent

The primary classification, NAPTHA, GAS

Utilization of Process fuel

Environmental Process Dust Collection,

Adsorption of odor

Air emissions

Secondary Classification

Secondary classification NAPTHA, GAS

Vapor catalytic cracking catalyst column

Process Flow Diagram 2 Reactor , Process fuel

Molten Material,

Pressing Heat Supply


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Machine under manufacturing (Currently available daily capacity by 1 ton, 2 tons and 3 tons)

Process Chamber Placement Pictures


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1. Production Process

Section System Configuration / Characteristics Remarks

Heating Furnace( Heater ) Indirectly Heated => Combustion Gas Transfer Heat to the Reactor

High Efficiency =>

Utilize Waste Gas, Apply Waste Heat Recovery System

Automation =>

Autoignition, Automatic Temperature Control Burner System

Safety / Cooling =>

Explosion Prevention, Forced Quick Exhaust Cooling

Using Liquid

Gas Fuel( Option )

Pyrolysis Reactor

Completed the iIspection of B.T.

Special Material of Explosion Proof,

Anti-Corrosion( SUS )

High Efficiency Catalyst Layer Built-In,

External Apply Coking prevention Technology

Apply Anti-Corrosion( H2S / HCl ) Technology

Pyrolysis Reactor

Splitter / Condenser Apply Splitter,

Condenser Integrated Structure Facility

Adoption of 3( Three-Phase )( Solid,Gaseous,Liquid)

Fractionator

Heat Exchanger

Application System ofAanti-Corrosion Material and

Neutralizing Agent


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2. Process Support

Section System Configuration / Method Option

Cooling Equipment System Apply Water-Cooling Type Cooling System

=> Apply Cooling Water anti-Corrosion System

=> Apply Cooling Water Scale Prevention System

Cooling Air-Cooled Furnace

=> Apply Cooling Heating Medium Reactor by

Cooling Heat Recovery

Separate

Chemical

Nitrogen Injection Safety System Nitrogen Injection Around Process Operation

=> For Cooling

=> The Inhibition of Oxidization

=> Self-Nitrogen Generator can be Adopted

Anti-Corrosion Chemical Injection System

Apply Special Corrosion Inhibitor

( Apply to the Target of Process Cooling Classification System )

=> Prevention of Hydrochloric Acid Corrosion

=> Prevention of Organic Acid Corrosion

Heat Recovery System Recovery

Utilization of Exhaust Waste Heat from Heating Furnace Chimney

=> Recycling of OFF Gas by Economizer System

=> Separate Heating Furnace by Operate Reactor

Option Equipment


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3. Safety and Environmental Equipment

Section System Configuration / Method Remarks

Reactor Explosion Proof Safety System

Satisfy National Safety Standards Material & Facility

Required Government Agencies Verify

Adopt Pressure Relief System in an Emergency

Adopt National Standard Explosion Proof Equipment

Explosion Proof Electrical System

Apply Pipe interlocking Device Against Vibration

Apply Reactor Interlocking Device

Emergency Response System in case of Power Failure

Apply Emergency Private Power Station System

Apply Process Generated Gas Continuous

Processing System

Incineration of OFF-Gas Apply Flare Stack

Option of Small Diesel Generator

Oil Spill Response System Apply Preparing Process for Oil Spill

Loss Prevention System

=> Compliance with Government Standard

Precipitator Deodorizing

Adsorption Removal

Post Processing of Emission Combustion Gas

from Incinerator by Heating Furnace

=> Precipitator, Odor Adsorption Column

=> Precautionary Investment Prepared for Emergency

Facility more than

3 Tons

Process Waste Treatment System Solid Waste Consignment Process for General Landfill

Development of a Separate Solid and Sale


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Characteristic of our Development Process

Section Material

Separation Process Characteristic Remarks

Our Company Process

Polymer Resin of

PP, PE, PS, ABS, etc Complex of Single Substance or Mixture

Excellent Yield

=> Kerosene, Diesel Grade

Excellent Separation Process

High Quality Oil Production

=> Minimize of Wax Component

=> Excellent Low Temperature Fluidity

In the case of Catalytic Cracking of Mixture,

the Process Efficiency of Solid Liquid Mixtures

Is Twice.

Other Company Process

Solid Waste RPF

Low yield

=> The Yield of Naphtha is about

60% at least

Fixed Separation Decline

Low Quality Oil Production

=> Contain Large Amounts of Wax

Very Poor Low Temperature Fluidity

Process Operating Time Is Long

Cause Energy Mass

Consumption form or

Product Quality

Becomes Degraded

It is inevitable that

Light Naphtha Occurs

in Bulk because of

Reflux reaction to

Reduce Wax


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Section Process Operating Condition

Relative Comparison of Operating Hour

( Based 5 Tons Reactor)

Main Products

Our Company Process

Normal Pressure Indirect Heating Type

=> 380~480℃

=> Normal Pressure 0.5 Kgf

( Gassing Pressure Standard )

In case of Solid Liquid

Mixture Process Around 10 hours

( Shorten Operating Hour )

Boiling Point Range

130~385℃ of

Fuel Oil and Similar to Kerosene and Diesel


Normal Pressure

High Pressure Indirect Heating Type

=> 400~500℃

In case of Solid Single

Material Process

=> 20 hours

=> Prolonged Operating

Hours According to

Reflux Reaction

Fuel Oil Containing Large Amounts of

Waste Naphtha, Gas and Wax

=> Room Temperature

Low Temperature

Fluidity is very Bad

because of Wax Containing

Normal Pressure

High Pressure Indirect Heating Type

450~700℃

In case of Solid Single

Material Process

15 hours


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Section Reactor Process Characteristics Remarks

Our Company Process

Horizontal STOP Reactor

Semi Automatic Medium Sized Reactor

It is possible to Input more than 80% of the Material

=> Equipped with Catalyst Column

Remove Wax and Foreign Material

Apply Technology

=> Apply self Development Isomerization

Catalyst

=> Excellent Thermal Efficiency

=> Coking Prevention and

Easy Operation Management

Isomerization Catalyst As the Catalyst which Changes the Structure of Paraffin with It Changes the Structure of Wax and Makes

It very good Fluidity

Material


Rotary Fluid Reactor

Limited less than 50% of Raw Material Charging Quantity by Based on Liquid

Law Material

=> Thermal Efficiency is Disadvantage

Heat Loss is Great

=> Coking Management is Difficult

=> Front Coking Phenomenon Occurs At 360°C

=> Concern about Mechanical Durability

Problems According to Reactor Fluid


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Our Competitive Technology

Process Risk Other Company

Existing Technology Our Technology Remarks

Reactor Coking

Extended Maintenance time

=> Heat Transfer Decline

=> No Chemicals to Remove

Independently Developed

Application of Anti Coking and

so Expected a Patent Application

Dramatically Improved Process

As the

Highest Level

of Technology at Home and

Abroad,

No other

Companies

Commercial

Pracactes

Distiller Tube Clogged (Wax / Saponification substance)

Impurities Occur Wax Occurs Frequently Piping Blockage Poor Quality in Winter

Applied Independently Developed Inhibitors for Impurities Occur

=> Expected Patent Application

=> Wax Cracking Catalyst Development => Expected Patent Application

Dramatically Improve Fuel Quality

Product Quality Degradation

Caused by Wax

Product Quality Degradation due to Facility Hydrochloric Acid Corrosionby PVC and Salt

Exposure to Corrosive Hydrochloric Acid,

Difficult for Screening Material -Shorten Equipment Life

-VCM Monomer Occurs and

Fuel Quality Degradation

-Applied VCM Monomer Dechlorination Catalyst Development ( Expected Patent Application)

-Suppress Interference Reaction by Salt (The same patented item)


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Our Competitive Technology

Select Fuel Additive Based On the Same Refineries

Applied Technology

=> Fully Improved Combustion Efficiency

=> Other Functionality

Possible to Provide Leading High

Performance Reforming Catalyst

Facilities due to having Independent Catalyst Development Efforts

Engineering Technique

=> Contribute to Improving Future Productivity

► Profitability


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Pyrolysis Yield according to Material

Material Section Pyrolysis Yield Remarks

Pure PE, PP, PS Standard

=> Except of PVC

• Gas => 2~3%

• Naphtha => Around 15%

• Kerosene & Diesel Fuel

=> More than 80%

• Coke( ASH ) => Below 1~3%

• Distillation Appearance

( Boiling Point )

=> 130 ℃ ~ 385℃

=> In the case of RPF

=> Yield Change Depending

on the Foreign Content


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Our Technical Characteristics

Cost of Equipment Superior Economic Compared to other Company Gas uses Its Own Fuel

Minimize Investment

Maximize Thermal efficiency of Approx. 8 % No limited material is Single Operation of High Molecule and Waste Oil

Minimize Operation Cost

HDPE Standard Diesel Level can be Produced more than 75% of Pyrolysis Oil Minimize 2nd Waste Material => Dangerous Substances like Gas, Naphtha, etc => Generated Gas and Naphtha are used for its Own Fuel.

Maximize Profitability

Maximize the Stability of Pyrolysis Furnace due to the Secure of Low Pyrolysis Temperature Decomposition of Chlorine Compounds Input Neutralization Catalyst Minimize the Occurrence of Chlorine Gas Causing Equipment Corrosion to Adoption of Anti-Corrosion Minimize Simplify Production Process Facility to Minimize

Minimize Disposal Dangerous Material Stability due to Low temperature Pyrolysis Stable Operation due to Minimize the Occurrence of Wax and Regular Maintenance and Stable Shut down in case of Abnormal Condition and Easy Process Maintenance

Secured Economic Secured Stability

The Best Catalyst Control Technology of the World Liquid Catalytic Cracking, Vapor Catalytic Cracking, Decomposition of Chlorine Compounds, Neutralization Catalyst Technology, Apply Suppression Technology of Wax, Gum, Coking

Facility

Stability

Operation Stability


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Material => Waste Plastics 100%( RPF RDF, Recycling Chip )

Operating Hour is Variable Depending on the Characteristics of Materials

=> Operating Hour is Very Variable Depending on Foreign Content and

Content of the Pure Polymer

It is very General to Operate One Time a Day

( Normal Operating 12 hours )

=> In the case of much Foreign Content

=> ASH Removal Time Occurs by Increasing after Reaction

Recommended Maximum One Time a Day

Our Process Operating Characteristics - Case 2


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기존 상용 촉매

당사 개질 RDF 촉매

RPF PYROYSIS OIL @ ASTM D86

Comparison of Produced Oil based on our Technology


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Hybrid Cracking Process Product Quality

Classification (Red is Standard) Diesel (Oil Company’s Diesel) Waste Lubricating Oil

Cracking Oil (NO Catalyst) Our Pyrolysis Oil of Waste Plastics

Flash Point(℃) Above 40

(Above 30℃ of Pyrolysis Oil ) 30~60 : Variable According to Process

Pour Point(℃) Below 0(Apr. ~ Sep.),

Below -17.5 (Oct. ~ Mar.) -30 -10

Residual Carbon, Wt% Below 0.15 0.17 0.05

ASH, Wt% Below 0.05 0.001 0.001

Distillation 90%, ℃ Below 360 395 350

Centistoke @ 40℃, cSt 2.0~5.8 5.2 2

SULFUR, Wt% Below 0.2 0.08 0.005

Moisture & Precipitate, VOL% Below 0.5 0.07 0.05

Cetane index Above 45 - 40~55

Lubricative, HRRR W.S.D 400 MAX Red Orange B&C 300

@15℃ DENSITY, g/㎤ Above 0.815~below 0.855 0.82~0.84 0.79~0.81

Contents of Heavy Metals

Pb Below 1 ppm None None

Cr Below 1 ppm None None

Cd) Below 1 ppm None None

As) Below 1 ppm None None


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Minimize of Heavy Oil Fraction

Maximize of Kerosene & Diesel Grade

Technology Outline( Catalyst Performance )


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High Molecule PP,PE,PVC

Decomposition & isomerization ,

Reaction of dechlorination

Pour point Below -25℃ Becomes High Quality Fuel

http://image.search.daum.net/dsa/search?w=imgviewer&q=%C6%E4%BA%F1%B4%D2&page_offset=16&page=2&shape=default&size=0&color=0&SortType=3&lpp=28&cp=&od=SguUz10


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Technology Outline Infrared Analysis of Kerosene & Diesel at General Gas Station

Aromatics

High Quality Hydrocarbon



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Technology Outline Infrared Analysis Comparison of Our Catalyst Pyrolysis Oil

Fully meets as Petroleum fuel based on Analysis of the chemical structure

HDPE 촉매 분해유

FT-IR CHART

Hydrocarbon Double Bond Substance

Aromatics High Quality Hydrocarbon



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RPF(PE ,PS 등) 촉매 분해유

FT-IR CHART

Plasticizer Line C-O Combination

Hydro Carbon Double Bond Substance

Hydro Carbon Aromatic

High Quality Hydro Carbon

High Quality Hydro Carbon

Unrefined Moisture

Fully meets as petroleum fuel based on analysis of the chemical structure

Infrared Analysis Comparison of R.P.F Catalyst Cracking Oil


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Throughput => 3 Tons / day X 20days / Month Operation

Output => Gross 75% Recovery Rate /2500 Liter( Reflected by a Reduction in Fuel use Itself )

Raw Material => Waste Plastic / RPF 100% Handling Economic Evaluation of Refined Oil Production

Leased Plant Standard


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Reasonable Price Range (Based Kerosene KRW 1400) Standard Price => Selling Price of Gas Station Jan. 2012

Economic Evaluation of Refined Oil Production


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[ The Purpose of Emulsified Recycle Business ] 1. Reduce Emission Amount of Co2 { Reduce by Approx. ¼ Compared to Incineration Treatment } 2. Reduce Incineration Treatment or Reclaiming Disposal Cost 3. Create a New Business and Profit by Selling Recycled Oil 4. Thorough Information Management of Wastes

[ The Purpose of Product ] ▶ Fuel for Diesel => Industrial fuel, Agricultural Boiler, Incinerator, Diesel engine generator, Vessel& heavy machinery fuel, etc ▶ Residue is Available as a Heating Fuel for Cement Furnace Fuel, Heating Fuel of Iron Works and Foundry{ Cokes 4500Kcal }

[ Recommend Type of Business ] Main Agent of Administration( City ) Recycling Resources Enterprise => Recycle Center, Plastics Recycling Resources Enterprise, Mineral Resources Enterprise Waste Disposal Enterprise => General Waste, Industrial Waste, Agricultural Waste Plastics Industry Product processing industry, Film printing industry Chemical Industry Polymer Ingredient Manufacturing Industry Chemicals Industry


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Q&A about Catalytic Cracker of Waste Plastics

Q.1. What is the Characteristic of this Device? A ① Low Operation Cost due to Pyrolysis using the Fuel of Recycled Oil and Waste Gas. ② This Device Realized Low Cost Compared to Former Emulsification Device Q.2. What is the Processing Capacity of this Device? A ① Processing Capacity => 1.000kg, 2.000kg, 3.000kg, 4.000kg, 5.000kg / Day Q.3. What is the Processing Progress of this Device? A ① Input a Batch of Waste Plastics in the Preprocessing Stage. ② Heat the Raw Materials of Waste Plastics and Gasify Inside a Furnace. ③ Obtained Cracked Gas is Reformed into Gasoline Grade and Diesel Grade by a Catalyst Column and save in each Cracked Oil Tank Q.4. What is different from General Method until now? A ① Existing Emulsification Device Safety Matter Operation Cost and our Emulsification device needs a Gaseous Reforming Catalyst and there is No Risks of Explosion and Fire because of using Nitrogen and Low Operation Cost by using the Fuel of our Own Produced Recycled Oil and Gas


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Q&A about Catalytic Cracker of Waste Plastics

Q.5. What is the Influence on Safety and Environment? A ① Block the Emission of Harmful Gas with the Installation of Gas Washer and Storage Tank ② Not necessary of Measures and like a Silencer and etc Specially even though there are Operation Sounds like Motor Sounds and Cooling Pump Sounds, etc ③ Not necessary of Measures because we perceive almost No Vibrations even though we are near to the Device ④ It is possible for draining and Waterproofing Entirely without Polluting because Drainage is only for Circulating Cooling Water


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Vitalization of Regional Economy through Regional

Energy Supply

Creation for Clean Streets And Clear Regional Society

Environment

Change of Environmental Friendly Awareness by Region

Name of Parts

Fuel Gas Storage Tank 1EA

Burner 1EA Spiral Heat Exchanger 2EA

Damper Noxious Gas Neutralizing Tank

1EA

Catalyst Reforming Column

1EA Cooling Tower

Collect Wax Column 1EA Fuel Heater 2EA

Naphtha Separation Tank

1EA Nitrogen Generator 1EA

Overpressure Gas Tank 1EA Gas Vein Pump 1EA

Naphtha Tank 1EA Micro Pressure Gauge

Diesel Grade Storage Tank 1EA Micro Thermometer

Gasoline Grade Storage Tank 1EA Valves & Pipes


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Relay Part

Electricity is used to Operate Burner Pump & Lamp and to Measure the Gauge

Maximum Load => 2.2 kw( Based on 1 Ton ) Average Electric Consumption => 1 ~ 2 kw / hr Average Daily Operating Hours => 10 ~ 12 hours/day


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Relay Part Main Control Panel


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Main Device Status Indirect Heating Furnace & Burner

Indirect Heating Furnace & Burner


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Melting Pyrolysis Reactor Main Device Status

Melting Pyrolysis Reactor


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Main Device Status DUFJ

Various Tank


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Main Device Status

Power Start ON

Gas Collector ON

Various Tank


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Main Device Status


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Main Device Status


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Main Device Status ( Sight Glass )

Sight Glass


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Other Major Device


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Other Major Device


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Other Major Device


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Nitrogen Generator Gas Compressor

Despite being compact in size and light in weight vertical Air Cooled Oil Free Reciprocating Compressor is as Highly reliable as any industrial version used in utility supply plants and the product is used to Supply High Pressure Gas as required by increasing and the Pressure of a Low Pressure Gas operation speed of Compressor It should not operate at 820rpm or Higher or at 200 rpm or Lower

Electricity Single Phase AC 220V 50 / 60Hz

Specification

Flow 98% by the purity of the Nitrogen Generated( Nm3/hr )

Discharge Pressure of the Nitrogen Generated( kg/㎠g )

Inflow Air Volume( nm3/hr )

Inflow air Generated( kg/㎠g )

Voltage ( V, AC )

Frequency(Hz)

Number of Phase

Current( Ampere )

Discharge Port Diameter of the Nitrogen Generated( PT )


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Burner

Technical and Functional Features • Diesel Burner / Oil Burner, OFF GAS Incineration Burner • Single Stage Operation( ON / OFF ) • Compatible with Any type of Combustion Chamber • High Pressure Mechanical Atomization of Fuel using Nozzle • Ability to Obtain Optimal Combustion Values by Regulating Combustion Air and Blast Pipe • Maintenance Facilitated by the fact that the Atomization unit can be removed without having to remove the Burner from the Boiler • Manual Air Flow Adjustment

Technical Data


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No. ITEM UNIT CONTENT

1 Inner Volume M³ 1.0

2 Name of the Fluid to be used Air

3 Design Pressure Mpa G 0.97

Temperature ℃ 60

4 Operation

Pressure Mpa G 0.88

Temperature ℃ AMB.

5 Inner Diameter of fuselage mm I.D 898.4 x 1264h

6 Corrosion Tolerance mm 1.0

7 Radiation Inspection(S/H) NO / N.A

8 Welding Efficiency

Fuselage % 70

Flat End Plate % 85

9 Post Heat Treatment NO

10 Used Material

Fuselage and Flat End Plate SS400

Support SS400

Anchor Bolt SS400

11 Permissible Stress

Fuselage and Flat End Plate N/㎟ 100

Support N/㎟ 100

Anchor Bolt N/㎟ 61

12 Water-Pressure Test Pressure Mpa G 1.261

13 Wind Load/Earthquake Load ㎧ 45/ZONE 2A(1.15)

14 Weight

In installation Kg 383

In operation Kg 383

In Water-Pressure Kg 1393

15 Installation Place OUTDOOR

No. ITEM UNIT CONTENT

1 Inner Volume M³ 2.0

2 Name of the Fluid to be used Air

3 Design Pressure Mpa G 0.97

Temperature ℃ 60

4 Operation

Pressure Mpa G 0.882

Temperature ℃ AMB.

5 Inner Diameter of fuselage mm I.D 1130 x 1584h

6 Corrosion Tolerance mm 1.0

7 Radiation Inspection(S/H) NO / N.A

8 Welding Efficiency

Fuselage % 70

Flat End Plate % 85

9 Post Heat Treatment NO

10 Used Material

Fuselage and Flat End Plate SS400

Support SS400

Anchor Bolt SS400

11 Permissible Stress

Fuselage and Flat End Plate N/㎟ 100

Support N/㎟ 100

Anchor Bolt N/㎟ 61

12 Water-Pressure Test Pressure Mpa G 1.261

13 Wind Load/Earthquake Load ㎧ 45/ZONE 2A(1.15)

14 Weight

In installation Kg 739

In operation Kg 739

In Water-Pressure Kg 2794

15 Installation Place OUTDOOR


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Patent Status


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Certificate of Test for Pyrolysis Oil


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Thanks So Much to You

New Technology by Ecocreation Industries keeps running forward for more Clear and Cleaner World

