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Al6061 NI resultsNIST Project
Ali KhosravaniJordan Weaver
4
5
6
7
8
x 10-3
50
55
60
65
70-0.1
0
0.1
0.2
0.3
0.4
0.5
0.6
Fit4 Average Abs ResidualEeff
h-c
han
ge
Fit
4 M
ax A
bs
Res
idu
al
0.014
0.015
0.016
0.017
0.018
0.019
0.02
0.021
0.022
0.023
Aged at 400F for 2hrs_ 100micron tip_001
AR_ 100micron tip_ test 001
65 70 75 800
20
40
Modulus [GPa]
0.96 0.98 1 1.020
20
40
R2
40 60 80 1000
20
40
Modulus Length [#points]-0.7 -0.6 -0.5 -0.4 -0.30
20
40
Hr [nm]
0.009 0.01 0.011 0.012 0.0130
50
Fit1 Avg.Abs.Res.0.02 0.03 0.04 0.05 0.060
20
40
Fit1 Max.Abs.Res.0.1 0.11 0.12 0.130
20
40
Fit2 Avg.Abs.Res.0.25 0.3 0.35 0.4 0.450
20
40
Fit2 Max.Abs.Res.
0.5 0.6 0.7 0.8 0.90
50
h change [nm/nm]0.4 0.5 0.6 0.7
0
20
40
P change [mN/mN]6 6.5 7 7.5
x 10-3
0
20
40
Fit4 Avg.Abs.Res.0.018 0.02 0.022 0.0240
20
40
Fit4 Max.Abs.Res.
0.2 0.21 0.22 0.230
20
40
P* [mN]
18.5 19 19.50
20
40
h* [nm]
0 1 2 3
x 10-3
0
10
20
dP [mN]-0.2 -0.1 0 0.1 0.20
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
AR_ 100micron tip_ test 001Estat = mean: 74.0953 median: 74.5196 stdev: 1.4504 min: 70.4381 max: 75.9712
Ystat = mean: 0.5090 median: 0.5134 stdev: 0.0169 min: 0.4678 max: 0.5321
Hstat = mean: 26.4590 median: 26.6196 stdev: 0.5423 min: 25.0907 max: 27.1902
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.5
1
1.5
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=70.4792; Bunge=0, 0, 0; Strength=0.50739; Hardening=26.4099
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
0 200 400 600 8000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 5 10 15
x 104
-2.5
-2
-1.5
-1
-0.5
0x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.2 0.4 0.6 0.8-2
0
2
4
6
8
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
AR_ 100micron tip_ test 003
66 68 70 72 74 760
20
40
Modulus [GPa]
0.95 0.96 0.97 0.98 0.99 10
100
200
R2
0 50 100 1500
50
100
Modulus Length [#points]-2 -1.5 -1 -0.5 0
0
50
100
Hr [nm]
0 0.01 0.02 0.03 0.040
50
100
Fit1 Avg.Abs.Res.0 0.05 0.1 0.15 0.2
0
100
200
Fit1 Max.Abs.Res.0 0.1 0.2 0.3 0.4
0
50
100
Fit2 Avg.Abs.Res.0 0.5 1 1.5
0
50
100
Fit2 Max.Abs.Res.
0 0.2 0.4 0.6 0.80
50
100
h change [nm/nm]0.1 0.2 0.3 0.4 0.5 0.60
50
100
P change [mN/mN]4 5 6 7 8
x 10-3
0
50
100
Fit4 Avg.Abs.Res.0.012 0.014 0.016 0.018 0.02 0.0220
50
100
Fit4 Max.Abs.Res.
0.2 0.4 0.6 0.8 10
50
100
P* [mN]
14 16 18 20 22 240
50
100
h* [nm]
0 1 2 3 4
x 10-3
0
20
40
dP [mN]-0.6 -0.4 -0.2 0 0.2 0.40
50
100
dH [nm]
effective
sample
Fit1
Fit2
Fit3
AR_ 100micron tip_ test 003Estat = mean: 72.8881 median: 72.7568 stdev: 1.7132 min: 70.0032 max: 75.9966
Ystat = mean: 0.5726 median: 0.5718 stdev: 0.0247 min: 0.4797 max: 0.6337
Hstat = mean: 25.9397 median: 25.8888 stdev: 0.6667 min: 24.6468 max: 27.2296
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.2
0.4
0.6
0.8
1
1.2
1.4
1.6
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.4139; Bunge=0, 0, 0; Strength=0.58068; Hardening=25.8184
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-200 0 200 400 600 8000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 0.5 1 1.5 2 2.5
x 105
-6
-5
-4
-3
-2
-1
0
1x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2-5
0
5
10
15
20
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
AR_ 100micron tip_ test 004
65 70 75 800
10
20
Modulus [GPa]
0.99 0.995 1 1.0050
20
40
R2
110 120 130 140 1500
20
40
Modulus Length [#points]-1.4 -1.2 -1 -0.8 -0.60
10
20
Hr [nm]
0.008 0.01 0.012 0.0140
20
40
Fit1 Avg.Abs.Res.0.02 0.04 0.06 0.080
20
40
Fit1 Max.Abs.Res.0.2 0.25 0.3 0.35
0
20
40
Fit2 Avg.Abs.Res.0.5 1 1.50
20
40
Fit2 Max.Abs.Res.
-0.1 0 0.1 0.2 0.30
20
40
h change [nm/nm]0 0.05 0.1 0.15 0.2
0
10
20
P change [mN/mN]3.8 4 4.2 4.4 4.6
x 10-3
0
10
20
Fit4 Avg.Abs.Res.0.011 0.012 0.013 0.014 0.0150
50
Fit4 Max.Abs.Res.
0.35 0.4 0.45 0.50
20
40
P* [mN]
22 22.5 23 23.5 240
20
40
h* [nm]
0 1 2 3 4
x 10-3
0
10
20
dP [mN]-0.2 0 0.2 0.4 0.60
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
AR_ 100micron tip_ test 004Estat = mean: 72.9264 median: 72.7957 stdev: 1.7328 min: 70.0236 max: 75.9430
Ystat = mean: 0.5620 median: 0.5603 stdev: 0.0253 min: 0.5206 max: 0.6081
Hstat = mean: 25.3096 median: 25.2949 stdev: 0.6958 min: 24.1726 max: 26.5177
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.5
1
1.5
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.3459; Bunge=0, 0, 0; Strength=0.55924; Hardening=25.3294
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-200 0 200 400 600 8000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
x 105
-6
-5
-4
-3
-2
-1
0
1x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 20
5
10
15
20
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
AR_ 100micron tip_ test 005
66 68 70 72 74 760
10
20
Modulus [GPa]
0.95 0.96 0.97 0.98 0.99 10
50
100
R2
20 40 60 80 100 1200
20
40
Modulus Length [#points]-0.7 -0.6 -0.5 -0.4 -0.30
50
Hr [nm]
4 6 8 10
x 10-3
0
50
Fit1 Avg.Abs.Res.0.01 0.02 0.03 0.04 0.050
50
100
Fit1 Max.Abs.Res.0.08 0.1 0.12 0.14 0.160
50
100
Fit2 Avg.Abs.Res.0.25 0.3 0.35 0.4 0.450
100
200
Fit2 Max.Abs.Res.
0 0.2 0.4 0.6 0.80
20
40
h change [nm/nm]0 0.1 0.2 0.3 0.4 0.5
0
20
40
P change [mN/mN]4 5 6 7 8
x 10-3
0
20
40
Fit4 Avg.Abs.Res.0.016 0.018 0.02 0.0220
20
40
Fit4 Max.Abs.Res.
0.25 0.3 0.35 0.4 0.450
50
P* [mN]
18.5 19 19.5 20 20.5 210
50
100
h* [nm]
0 1 2 3 4
x 10-3
0
10
20
dP [mN]-0.4 -0.2 0 0.2 0.40
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
AR_ 100micron tip_ test 005Estat = mean: 72.9738 median: 73.0464 stdev: 1.7727 min: 70.0284 max: 75.9751
Ystat = mean: 0.5677 median: 0.5668 stdev: 0.0264 min: 0.5105 max: 0.6133
Hstat = mean: 24.2864 median: 24.3030 stdev: 0.6177 min: 23.2218 max: 25.3615
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.5
1
1.5
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.4103; Bunge=0, 0, 0; Strength=0.56771; Hardening=24.2611
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-500 0 500 10000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 5 10 15
x 104
-3
-2.5
-2
-1.5
-1
-0.5
0
0.5x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1-2
0
2
4
6
8
10
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
AR_ 100micron tip_ test 006
65 70 75 800
5
10
Modulus [GPa]
0.94 0.96 0.98 10
10
20
R2
20 30 40 50 600
5
10
Modulus Length [#points]-0.6 -0.5 -0.4 -0.3 -0.20
10
20
Hr [nm]
4 5 6 7
x 10-3
0
10
20
Fit1 Avg.Abs.Res.0.005 0.01 0.015 0.02 0.0250
10
20
Fit1 Max.Abs.Res.0.08 0.1 0.12 0.140
10
20
Fit2 Avg.Abs.Res.0.2 0.3 0.4 0.50
5
10
Fit2 Max.Abs.Res.
-0.5 0 0.5 10
10
20
h change [nm/nm]0 0.2 0.4 0.6 0.8
0
10
20
P change [mN/mN]4 5 6 7
x 10-3
0
10
20
Fit4 Avg.Abs.Res.0.01 0.015 0.020
5
10
Fit4 Max.Abs.Res.
0.2 0.25 0.3 0.35 0.40
10
20
P* [mN]
10 11 12 13 140
10
20
h* [nm]
0 1 2 3 4
x 10-3
0
5
10
dP [mN]-0.2 0 0.2 0.4 0.60
10
20
dH [nm]
effective
sample
Fit1
Fit2
Fit3
AR_ 100micron tip_ test 006Estat = mean: 72.7770 median: 72.6317 stdev: 1.6269 min: 70.0297 max: 75.9841
Ystat = mean: 1.3887 median: 0.5726 stdev: 0.8684 min: 0.4794 max: 2.3706
Hstat = mean: -20.5747 median: 24.3717 stdev: 46.3225 min: -68.8533 max: 25.6614
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.2
0.4
0.6
0.8
1
1.2
1.4
1.6
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.1032; Bunge=0, 0, 0; Strength=0.55979; Hardening=25.303
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
0 200 400 600 8000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 5 10 15
x 104
-2
-1.5
-1
-0.5
0x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.2 0.4 0.6 0.8-2
0
2
4
6
8
10
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
AR_ 100micron tip_ test 007
65 70 75 800
10
20
Modulus [GPa]
0.985 0.99 0.995 1 1.0050
20
40
R2
90 100 110 1200
10
20
Modulus Length [#points]-0.9 -0.8 -0.7 -0.6 -0.50
10
20
Hr [nm]
0.01 0.015 0.020
10
20
Fit1 Avg.Abs.Res.0.03 0.04 0.05 0.060
10
20
Fit1 Max.Abs.Res.0.2 0.25 0.3 0.35
0
10
20
Fit2 Avg.Abs.Res.0 0.5 1 1.5
0
10
20
Fit2 Max.Abs.Res.
0 0.1 0.2 0.3 0.40
10
20
h change [nm/nm]0 0.05 0.1 0.15 0.2
0
10
20
P change [mN/mN]5.5 6 6.5 7
x 10-3
0
20
40
Fit4 Avg.Abs.Res.0.016 0.018 0.02 0.0220
10
20
Fit4 Max.Abs.Res.
0.48 0.5 0.52 0.54 0.560
10
20
P* [mN]
18 18.5 19 19.50
10
20
h* [nm]
0 2 4 6
x 10-3
0
10
20
dP [mN]-0.5 0 0.50
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
AR_ 100micron tip_ test 007Estat = mean: 72.2464 median: 71.9764 stdev: 1.6662 min: 70.0129 max: 75.9662
Ystat = mean: 0.5074 median: 0.5047 stdev: 0.0193 min: 0.4798 max: 0.5531
Hstat = mean: 25.7443 median: 25.7191 stdev: 0.7086 min: 24.5450 max: 27.1741
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.5
1
1.5
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=68.7734; Bunge=0, 0, 0; Strength=0.50939; Hardening=25.8316
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-200 0 200 400 600 8000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
x 105
-5
-4
-3
-2
-1
0
1x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 20
5
10
15
20
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
AR_ 100micron tip_ test 009
66 68 70 72 74 760
10
20
Modulus [GPa]
0.96 0.97 0.98 0.99 1 1.010
20
40
R2
40 60 80 100 1200
10
20
Modulus Length [#points]-0.8 -0.6 -0.4 -0.2 00
10
20
Hr [nm]
5 6 7 8 9 10
x 10-3
0
10
20
Fit1 Avg.Abs.Res.0.01 0.02 0.03 0.04 0.050
50
Fit1 Max.Abs.Res.0.11 0.12 0.13 0.14 0.15 0.160
10
20
Fit2 Avg.Abs.Res.0.2 0.4 0.6 0.8 10
10
20
Fit2 Max.Abs.Res.
-0.05 0 0.05 0.1 0.15 0.20
5
10
h change [nm/nm]0 0.05 0.1 0.15 0.2
0
5
10
P change [mN/mN]4 5 6 7
x 10-3
0
10
20
Fit4 Avg.Abs.Res.0.014 0.016 0.018 0.02 0.022 0.0240
5
10
Fit4 Max.Abs.Res.
0.25 0.3 0.35 0.4 0.450
20
40
P* [mN]
14 15 16 17 180
20
40
h* [nm]
0 1 2 3 4
x 10-3
0
5
10
dP [mN]-0.4 -0.2 0 0.2 0.40
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
AR_ 100micron tip_ test 009Estat = mean: 72.3650 median: 72.3985 stdev: 1.6707 min: 70.0855 max: 75.9545
Ystat = mean: 0.6027 median: 0.6021 stdev: 0.0314 min: 0.5364 max: 0.6666
Hstat = mean: 25.0466 median: 25.0440 stdev: 0.5939 min: 24.1868 max: 26.2760
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.5
1
1.5
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=68.8635; Bunge=0, 0, 0; Strength=0.60705; Hardening=25.0446
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-200 0 200 400 600 8000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
x 105
-4
-3
-2
-1
0
1x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.50
2
4
6
8
10
12
14
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
AR_ 100micron tip_ test 010
AR_ 100micron tip_ test 010Estat = mean: 72.5138 median: 72.2047 stdev: 1.5804 min: 70.0063 max: 75.9970
Ystat = mean: 1.1205 median: 1.1902 stdev: 0.2391 min: 0.3946 max: 1.3185
Hstat = mean: 10.6983 median: 8.5662 stdev: 5.5002 min: 8.2477 max: 27.3548
400F_ 100micron tip_ test 001
66 68 70 72 74 760
20
40
Modulus [GPa]
0.95 0.96 0.97 0.98 0.99 10
200
400
R2
60 80 100 1200
20
40
Modulus Length [#points]-6 -4 -2 0
0
20
40
Hr [nm]
0 0.05 0.1 0.15 0.2 0.250
50
100
Fit1 Avg.Abs.Res.0 0.2 0.4 0.6 0.8
0
50
100
Fit1 Max.Abs.Res.0 0.2 0.4 0.6 0.8 1
0
50
100
Fit2 Avg.Abs.Res.0 1 2 3 4
0
50
Fit2 Max.Abs.Res.
0 0.1 0.2 0.3 0.40
50
h change [nm/nm]0 0.1 0.2 0.3 0.4
0
50
P change [mN/mN]0.005 0.01 0.015 0.020
50
100
Fit4 Avg.Abs.Res.0.01 0.02 0.03 0.04 0.050
20
40
Fit4 Max.Abs.Res.
0 2 4 6 80
50
P* [mN]
0 20 40 600
50
h* [nm]
0 0.01 0.02 0.03 0.04 0.050
20
40
dP [mN]-1.5 -1 -0.5 0 0.5 10
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
Estat = mean: 72.7560 median: 72.6725 stdev: 1.7194 min: 70.0141 max: 75.9311
Ystat = mean: 0.5800 median: 0.5799 stdev: 0.0273 min: 0.5142 max: 0.6424
Hstat = mean: 25.7733 median: 25.7376 stdev: 0.8190 min: 23.9460 max: 27.7413
400F_ 100micron tip_ test 001
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.5
1
1.5
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.1823; Bunge=0, 0, 0; Strength=0.60068; Hardening=25.4006
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-200 0 200 400 600 8000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
-1 0 1 2 3
x 105
-15
-10
-5
0
5x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 3 40
10
20
30
40
50
P 2/3
h
Modulus Fit
Data
Elastic
0 0.02 0.04 0.06 0.08 0.10
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
400F_ 100micron tip_ test 002
66 68 70 72 74 760
20
40
Modulus [GPa]
0.95 0.96 0.97 0.98 0.99 10
100
200
R2
60 80 100 1200
50
Modulus Length [#points]-6 -4 -2 0
0
50
Hr [nm]
0 0.05 0.1 0.15 0.20
50
100
Fit1 Avg.Abs.Res.0 0.2 0.4 0.6 0.8
0
50
Fit1 Max.Abs.Res.0 0.2 0.4 0.6 0.8 1
0
50
100
Fit2 Avg.Abs.Res.0 1 2 3 4
0
50
Fit2 Max.Abs.Res.
0 0.1 0.2 0.3 0.4 0.50
50
h change [nm/nm]0 0.1 0.2 0.3 0.4
0
50
P change [mN/mN]0.005 0.01 0.015 0.020
50
100
Fit4 Avg.Abs.Res.0.015 0.02 0.025 0.03 0.035 0.040
20
40
Fit4 Max.Abs.Res.
0 2 4 60
20
40
P* [mN]
0 10 20 30 40 500
20
40
h* [nm]
0 0.01 0.02 0.03 0.04 0.050
20
40
dP [mN]-2 -1 0 1 2
0
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
400F_ 100micron tip_ test 002Estat = mean: 72.5480 median: 72.3265 stdev: 1.7056 min: 70.0063 max: 75.9879
Ystat = mean: 0.6048 median: 0.6052 stdev: 0.0245 min: 0.5445 max: 0.6608
Hstat = mean: 26.2425 median: 26.1201 stdev: 0.7859 min: 24.9040 max: 28.0767
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.5
1
1.5
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=68.8711; Bunge=0, 0, 0; Strength=0.61391; Hardening=25.8814
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-200 0 200 400 600 8000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
-1 0 1 2 3
x 105
-12
-10
-8
-6
-4
-2
0
2x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 3 40
10
20
30
40
P 2/3
h
Modulus Fit
Data
Elastic
0 0.2 0.4 0.60
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
400F_ 100micron tip_ test 003
65 70 75 800
10
20
Modulus [GPa]
0.94 0.96 0.98 10
50
100
R2
80 90 100 110 1200
20
40
Modulus Length [#points]-4 -3 -2 -1 0
0
20
40
Hr [nm]
0 0.02 0.04 0.06 0.080
20
40
Fit1 Avg.Abs.Res.0 0.1 0.2 0.3 0.4
0
20
40
Fit1 Max.Abs.Res.0 0.2 0.4 0.6 0.8
0
50
Fit2 Avg.Abs.Res.0 1 2 3
0
20
40
Fit2 Max.Abs.Res.
0 0.1 0.2 0.3 0.40
20
40
h change [nm/nm]0 0.05 0.1 0.15 0.2
0
50
100
P change [mN/mN]0.005 0.01 0.0150
20
40
Fit4 Avg.Abs.Res.0.01 0.02 0.03 0.040
20
40
Fit4 Max.Abs.Res.
0 1 2 3 40
10
20
P* [mN]
0 10 20 30 400
20
40
h* [nm]
0 0.02 0.04 0.060
20
40
dP [mN]-0.5 0 0.5 1 1.50
10
20
dH [nm]
effective
sample
Fit1
Fit2
Fit3
400F_ 100micron tip_ test 003
Estat = mean: 73.0235 median: 73.0678 stdev: 1.7908 min: 70.0025 max: 75.9985
Ystat = mean: 0.5911 median: 0.5877 stdev: 0.0241 min: 0.5384 max: 0.6472
Hstat = mean: 26.7180 median: 26.7403 stdev: 0.7762 min: 25.1076 max: 28.2214
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.2
0.4
0.6
0.8
1
1.2
1.4
1.6
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.6973; Bunge=0, 0, 0; Strength=0.57997; Hardening=27.0297
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-500 0 500 10000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
-2 0 2 4
x 105
-20
-15
-10
-5
0
5x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 2 4 6-10
0
10
20
30
40
50
P 2/3
h
Modulus Fit
Data
Elastic
0 0.1 0.2 0.30
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
400F_ 100micron tip_ test 004
66 68 70 72 74 760
10
20
Modulus [GPa]
0.97 0.98 0.99 1 1.010
20
40
R2
80 90 100 110 1200
20
40
Modulus Length [#points]-3.5 -3 -2.5 -2 -1.5 -10
20
40
Hr [nm]
0.02 0.04 0.06 0.080
20
40
Fit1 Avg.Abs.Res.0.05 0.1 0.15 0.2 0.250
20
40
Fit1 Max.Abs.Res.0.2 0.3 0.4 0.5 0.6 0.70
20
40
Fit2 Avg.Abs.Res.1 1.5 2 2.5 3
0
20
40
Fit2 Max.Abs.Res.
0 0.05 0.1 0.15 0.2 0.250
20
40
h change [nm/nm]0 0.05 0.1 0.15 0.2
0
20
40
P change [mN/mN]4 6 8 10 12
x 10-3
0
20
40
Fit4 Avg.Abs.Res.0.01 0.015 0.02 0.025 0.030
20
40
Fit4 Max.Abs.Res.
0.5 1 1.5 2 2.5 30
20
40
P* [mN]
10 15 20 25 300
20
40
h* [nm]
0 0.005 0.01 0.015 0.020
20
40
dP [mN]-0.5 0 0.5 10
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
400F_ 100micron tip_ test 004Estat = mean: 72.9889 median: 73.1361 stdev: 1.8000 min: 70.0546 max: 75.9991
Ystat = mean: 0.6103 median: 0.6072 stdev: 0.0260 min: 0.5609 max: 0.6650
Hstat = mean: 26.9273 median: 26.9275 stdev: 0.7568 min: 25.5735 max: 28.3435
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.2
0.4
0.6
0.8
1
1.2
1.4
1.6
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.4253; Bunge=0, 0, 0; Strength=0.6109; Hardening=26.7417
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-500 0 500 10000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
-1 0 1 2 3
x 105
-8
-6
-4
-2
0
2x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 30
5
10
15
20
25
30
P 2/3
h
Modulus Fit
Data
Elastic
0 0.05 0.10
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
400F_ 100micron tip_ test 005
66 68 70 72 74 760
20
40
Modulus [GPa]
0.95 0.96 0.97 0.98 0.99 10
50
100
R2
60 80 100 1200
20
40
Modulus Length [#points]-4 -3 -2 -1 0
0
50
100
Hr [nm]
0 0.02 0.04 0.06 0.08 0.10
50
100
Fit1 Avg.Abs.Res.0 0.05 0.1 0.15 0.2 0.25
0
50
100
Fit1 Max.Abs.Res.0 0.2 0.4 0.6 0.8
0
50
100
Fit2 Avg.Abs.Res.0 1 2 3 4
0
20
40
Fit2 Max.Abs.Res.
-0.1 0 0.1 0.2 0.30
20
40
h change [nm/nm]0 0.05 0.1 0.15 0.2
0
20
40
P change [mN/mN]4 6 8 10 12
x 10-3
0
20
40
Fit4 Avg.Abs.Res.0.01 0.015 0.02 0.0250
20
40
Fit4 Max.Abs.Res.
0 1 2 3 40
50
100
P* [mN]
0 10 20 30 400
50
100
h* [nm]
0 0.005 0.01 0.015 0.020
50
dP [mN]-0.5 0 0.5 10
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
400F_ 100micron tip_ test 005Estat = mean: 72.4187 median: 72.3209 stdev: 1.5646 min: 70.0299 max: 75.9694
Ystat = mean: 0.5981 median: 0.5954 stdev: 0.0208 min: 0.5477 max: 0.6574
Hstat =
mean: 25.8628 median: 25.7550 stdev: 0.6907 min: 24.7395 max: 27.5316
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.5
1
1.5
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=68.8299; Bunge=0, 0, 0; Strength=0.58431; Hardening=25.9528
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-500 0 500 10000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 1 2 3
x 105
-12
-10
-8
-6
-4
-2
0
2x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 3 40
10
20
30
40
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
400F_ 100micron tip_ test 006
66 68 70 72 74 760
10
20
Modulus [GPa]
0.95 0.96 0.97 0.98 0.99 10
100
200
R2
60 70 80 90 100 1100
10
20
Modulus Length [#points]-4 -3 -2 -1 0
0
20
40
Hr [nm]
0 0.02 0.04 0.06 0.080
20
40
Fit1 Avg.Abs.Res.0 0.05 0.1 0.15 0.2 0.25
0
20
40
Fit1 Max.Abs.Res.0 0.2 0.4 0.6 0.8
0
50
100
Fit2 Avg.Abs.Res.0 1 2 3
0
20
40
Fit2 Max.Abs.Res.
0 0.1 0.2 0.3 0.4 0.50
50
100
h change [nm/nm]0 0.1 0.2 0.3 0.4
0
50
100
P change [mN/mN]5 6 7 8 9 10
x 10-3
0
20
40
Fit4 Avg.Abs.Res.0.015 0.02 0.025 0.030
20
40
Fit4 Max.Abs.Res.
0 1 2 3 40
20
40
P* [mN]
0 10 20 30 400
20
40
h* [nm]
0 0.005 0.01 0.015 0.020
20
40
dP [mN]-0.5 0 0.5 10
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
400F_ 100micron tip_ test 006Estat = mean: 72.5387 median: 72.3448 stdev: 1.6706 min: 70.0031 max: 75.9708
Ystat = mean: 0.6235 median: 0.6197 stdev: 0.0376 min: 0.5521 max: 0.7019
Hstat = mean: 25.2648 median: 25.1910 stdev: 0.6441 min: 24.1051 max: 26.5741
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.2
0.4
0.6
0.8
1
1.2
1.4
1.6
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=68.9125; Bunge=0, 0, 0; Strength=0.64253; Hardening=25.1394
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-500 0 500 10000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 1 2 3
x 105
-15
-10
-5
0
5x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 3 40
10
20
30
40
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
400F_ 100micron tip_ test 007
66 68 70 72 74 760
10
20
Modulus [GPa]
0.95 0.96 0.97 0.98 0.99 10
20
40
R2
95 100 105 110 115 1200
10
20
Modulus Length [#points]-3 -2.5 -2 -1.5 -1
0
10
20
Hr [nm]
0.02 0.03 0.04 0.05 0.060
10
20
Fit1 Avg.Abs.Res.0.05 0.1 0.15 0.2 0.250
10
20
Fit1 Max.Abs.Res.0.35 0.4 0.45 0.5 0.55 0.6
0
10
20
Fit2 Avg.Abs.Res.1 1.5 2 2.5 3
0
10
20
Fit2 Max.Abs.Res.
-0.05 0 0.05 0.1 0.150
20
40
h change [nm/nm]0 0.02 0.04 0.06 0.08 0.1
0
20
40
P change [mN/mN]5 6 7 8 9 10
x 10-3
0
20
40
Fit4 Avg.Abs.Res.0.015 0.02 0.025 0.030
10
20
Fit4 Max.Abs.Res.
0.5 1 1.5 2 2.50
10
20
P* [mN]
10 15 20 250
10
20
h* [nm]
0 0.005 0.01 0.015 0.020
10
20
dP [mN]-0.5 0 0.5 10
10
20
dH [nm]
effective
sample
Fit1
Fit2
Fit3
400F_ 100micron tip_ test 007
Estat = mean: 72.5940 median: 72.4691 stdev: 1.6808 min: 70.0073 max: 75.9954
Ystat = mean: 0.6301 median: 0.6262 stdev: 0.0239 min: 0.5901 max: 0.6833
Hstat = mean: 24.2083 median: 24.1450 stdev: 0.6232 min: 23.2490 max: 25.4870
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.5
1
1.5
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=68.9381; Bunge=0, 0, 0; Strength=0.62268; Hardening=24.145
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-500 0 500 10000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 1 2 3
x 105
-15
-10
-5
0
5x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 3 40
10
20
30
40
50
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
2000
4000
6000
8000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
400F_ 100micron tip_ test 008
65 70 75 800
5
10
Modulus [GPa]
0.94 0.96 0.98 10
5
10
R2
70 75 80 85 900
5
10
Modulus Length [#points]-3 -2.5 -2 -1.5 -1
0
10
20
Hr [nm]
0.03 0.04 0.05 0.060
5
10
Fit1 Avg.Abs.Res.0.08 0.1 0.12 0.14 0.160
5
10
Fit1 Max.Abs.Res.0.35 0.4 0.45 0.5
0
5
10
Fit2 Avg.Abs.Res.1 1.5 2 2.5
0
10
20
Fit2 Max.Abs.Res.
0 0.05 0.1 0.15 0.20
10
20
h change [nm/nm]0 0.05 0.1 0.15 0.2
0
20
40
P change [mN/mN]6 8 10 12
x 10-3
0
5
10
Fit4 Avg.Abs.Res.0.018 0.02 0.022 0.024 0.0260
5
10
Fit4 Max.Abs.Res.
1.4 1.6 1.8 2 2.20
5
10
P* [mN]
16 18 20 22 240
5
10
h* [nm]
0 0.005 0.01 0.015 0.020
5
10
dP [mN]-0.5 0 0.5 10
5
10
dH [nm]
effective
sample
Fit1
Fit2
Fit3
400F_ 100micron tip_ test 008Estat = mean: 72.8347 median: 72.7764 stdev: 1.7629 min: 70.0515 max: 75.9819
Ystat = mean: 0.6153 median: 0.6150 stdev: 0.0243 min: 0.5745 max: 0.6635
Hstat = mean: 25.5687 median: 25.5641 stdev: 0.6504 min: 24.5436 max: 26.8152
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.2
0.4
0.6
0.8
1
1.2
1.4
1.6
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.3031; Bunge=0, 0, 0; Strength=0.61882; Hardening=25.6051
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-500 0 500 10000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
-1 0 1 2 3
x 105
-10
-8
-6
-4
-2
0
2x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 3-10
0
10
20
30
40
P 2/3
h
Modulus Fit
Data
Elastic
0 0.1 0.20
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
400F_ 100micron tip_ test 009
65 70 75 800
10
20
Modulus [GPa]
0.94 0.96 0.98 10
10
20
R2
90 100 110 1200
20
40
Modulus Length [#points]-2 -1.5 -1 -0.5
0
10
20
Hr [nm]
0.02 0.03 0.04 0.050
20
40
Fit1 Avg.Abs.Res.0.05 0.1 0.150
10
20
Fit1 Max.Abs.Res.0.35 0.4 0.45 0.5
0
10
20
Fit2 Avg.Abs.Res.1 1.5 2 2.5
0
10
20
Fit2 Max.Abs.Res.
-0.05 0 0.05 0.1 0.150
10
20
h change [nm/nm]0 0.05 0.1
0
10
20
P change [mN/mN]4 6 8 10
x 10-3
0
20
40
Fit4 Avg.Abs.Res.0.015 0.02 0.025 0.030
10
20
Fit4 Max.Abs.Res.
0.5 1 1.5 20
10
20
P* [mN]
10 15 200
10
20
h* [nm]
0 0.005 0.01 0.015 0.020
10
20
dP [mN]0.2 0.4 0.6 0.8 10
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
400F_ 100micron tip_ test 009Estat = mean: 72.7375 median: 72.5867 stdev: 1.7351 min: 70.0108 max: 75.9380
Ystat = mean: 0.5990 median: 0.5987 stdev: 0.0244 min: 0.5534 max: 0.6502
Hstat = mean: 25.0370 median: 25.0045 stdev: 0.6484 min: 23.9826 max: 26.3593
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.5
1
1.5
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.186; Bunge=0, 0, 0; Strength=0.60556; Hardening=25.147
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-200 0 200 400 600 8000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
-1 0 1 2 3
x 105
-10
-8
-6
-4
-2
0
2x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 1 2 30
5
10
15
20
25
30
35
P 2/3
h
Modulus Fit
Data
Elastic
0 0.2 0.4 0.6 0.80
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
400F_ 100micron tip_ test 010
65 70 75 800
10
20
Modulus [GPa]
0.94 0.96 0.98 10
10
20
R2
10 20 30 40 500
20
40
Modulus Length [#points]-2 -1.5 -1 -0.5
0
10
20
Hr [nm]
0 0.02 0.04 0.060
20
40
Fit1 Avg.Abs.Res.0 0.05 0.1 0.15 0.2
0
10
20
Fit1 Max.Abs.Res.0 0.1 0.2 0.3 0.4
0
10
20
Fit2 Avg.Abs.Res.0.2 0.4 0.6 0.8 10
10
20
Fit2 Max.Abs.Res.
0.5 0.6 0.7 0.8 0.90
10
20
h change [nm/nm]0.4 0.6 0.8 10
20
40
P change [mN/mN]0.006 0.008 0.01 0.012 0.0140
10
20
Fit4 Avg.Abs.Res.0.015 0.02 0.025 0.030
10
20
Fit4 Max.Abs.Res.
0 0.5 1 1.50
10
20
P* [mN]
5 10 15 20 250
10
20
h* [nm]
0 0.005 0.01 0.015 0.020
10
20
dP [mN]-1 -0.5 0 0.5
0
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
400F_ 100micron tip_ test 010Estat = mean: 72.9543 median: 72.9222 stdev: 1.6266 min: 70.0865 max: 75.9163
Ystat = mean: 0.4556 median: 0.4465 stdev: 0.0448 min: 0.3839 max: 0.5389
Hstat = mean: 28.2196 median: 28.1243 stdev: 0.8397 min: 26.5468 max: 29.9858
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.5
1
1.5
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.3707; Bunge=0, 0, 0; Strength=0.53241; Hardening=27.4405
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
0 200 400 600 8000
50
100
150
200
250
300
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0.5 1 1.5 2 2.5
x 105
-8
-6
-4
-2
0x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2 2.5-5
0
5
10
15
20
25
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
525F_ 100micron tip_ test 001
65 70 75 800
10
20
Modulus [GPa]
0.94 0.96 0.98 10
20
40
R2
80 90 100 110 1200
20
40
Modulus Length [#points]-1 -0.8 -0.6 -0.4 -0.2
0
10
20
Hr [nm]
0.005 0.01 0.015 0.020
10
20
Fit1 Avg.Abs.Res.0.02 0.03 0.04 0.05 0.060
10
20
Fit1 Max.Abs.Res.0.1 0.15 0.2 0.250
20
40
Fit2 Avg.Abs.Res.0.4 0.5 0.6 0.7
0
10
20
Fit2 Max.Abs.Res.
0.2 0.3 0.4 0.50
10
20
h change [nm/nm]0.2 0.25 0.3 0.35
0
20
40
P change [mN/mN]7 8 9 10
x 10-3
0
20
40
Fit4 Avg.Abs.Res.0.02 0.025 0.03 0.035 0.040
20
40
Fit4 Max.Abs.Res.
0.05 0.1 0.15 0.2 0.250
20
40
P* [mN]
3 4 5 6 70
20
40
h* [nm]
0 0.5 1 1.5 2
x 10-3
0
10
20
dP [mN]-0.6 -0.4 -0.2 0 0.20
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
Estat = mean: 72.8279 median: 73.1006 stdev: 1.7629 min: 70.0003 max: 75.9999
Ystat = mean: 0.3439 median: 0.3420 stdev: 0.0158 min: 0.3150 max: 0.3783
Hstat = mean: 17.3318 median: 17.3867 stdev: 0.4754 min: 16.5865 max: 18.4025
525F_ 100micron tip_ test 001
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.2875; Bunge=0, 0, 0; Strength=0.34963; Hardening=17.2816
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
0 200 400 600 8000
50
100
150
200
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
x 105
-2
-1.5
-1
-0.5
0x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.2 0.4 0.6 0.8 1-2
0
2
4
6
8
10
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
2000
4000
6000
8000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
525F_ 100micron tip_ test 002
66 68 70 72 74 760
20
40
Modulus [GPa]
0.95 0.96 0.97 0.98 0.99 10
100
200
R2
50 100 1500
50
100
Modulus Length [#points]-1.2 -1 -0.8 -0.6 -0.4 -0.20
50
100
Hr [nm]
0.005 0.01 0.015 0.020
50
100
Fit1 Avg.Abs.Res.0 0.02 0.04 0.06 0.08 0.1
0
100
200
Fit1 Max.Abs.Res.0.1 0.15 0.2 0.25 0.3 0.350
50
100
Fit2 Avg.Abs.Res.0.2 0.4 0.6 0.8 1 1.20
100
200
Fit2 Max.Abs.Res.
-0.2 0 0.2 0.4 0.60
100
200
h change [nm/nm]0 0.1 0.2 0.3 0.4
0
100
200
P change [mN/mN]5 6 7 8 9 10
x 10-3
0
50
100
Fit4 Avg.Abs.Res.0.01 0.02 0.03 0.04 0.05 0.060
50
100
Fit4 Max.Abs.Res.
0.1 0.2 0.3 0.4 0.50
50
100
P* [mN]
6 7 8 9 10 110
50
100
h* [nm]
0 0.5 1 1.5 2 2.5
x 10-3
0
50
dP [mN]-0.4 -0.2 0 0.2 0.4 0.60
50
100
dH [nm]
effective
sample
Fit1
Fit2
Fit3
525F_ 100micron tip_ test 002Estat = mean: 73.0168 median: 72.9951 stdev: 1.7580 min: 70.0013 max: 75.9956
Ystat = mean: 0.3923 median: 0.3923 stdev: 0.0185 min: 0.3468 max: 0.4306
Hstat = mean: 18.0153 median: 17.8977 stdev: 0.6708 min: 17.0777 max: 19.5268
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.2
0.4
0.6
0.8
1
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.4679; Bunge=0, 0, 0; Strength=0.36933; Hardening=18.023
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
0 500 10000
50
100
150
200
250
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
x 105
-3.5
-3
-2.5
-2
-1.5
-1
-0.5
0x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.50
5
10
15
20
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
2000
4000
6000
8000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
525F_ 100micron tip_ test 003
65 70 75 800
10
20
Modulus [GPa]
0.94 0.96 0.98 10
50
R2
50 100 1500
10
20
Modulus Length [#points]-0.9 -0.8 -0.7 -0.6 -0.50
10
20
Hr [nm]
0.005 0.01 0.0150
20
40
Fit1 Avg.Abs.Res.0.025 0.03 0.035 0.04 0.0450
20
40
Fit1 Max.Abs.Res.0.1 0.11 0.12 0.130
20
40
Fit2 Avg.Abs.Res.0.4 0.5 0.6 0.7
0
20
40
Fit2 Max.Abs.Res.
0.1 0.2 0.3 0.4 0.50
20
40
h change [nm/nm]0.1 0.2 0.3 0.4 0.50
10
20
P change [mN/mN]6 7 8 9 10
x 10-3
0
20
40
Fit4 Avg.Abs.Res.0.025 0.03 0.035 0.040
50
100
Fit4 Max.Abs.Res.
0.12 0.14 0.16 0.180
10
20
P* [mN]
4.5 5 5.5 60
10
20
h* [nm]
0 0.5 1 1.5 2
x 10-3
0
10
20
dP [mN]-1 -0.5 0 0.5
0
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
525F_ 100micron tip_ test 003Estat = mean: 72.8329 median: 72.6625 stdev: 1.6899 min: 70.0091 max: 75.9662
Ystat = mean: 0.4241 median: 0.4226 stdev: 0.0182 min: 0.3933 max: 0.4577
Hstat = mean: 17.1184 median: 17.0781 stdev: 0.4141 min: 16.4184 max: 17.9105
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.2
0.4
0.6
0.8
1
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.3119; Bunge=0, 0, 0; Strength=0.42218; Hardening=17.1288
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-500 0 500 10000
50
100
150
200
250
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 5 10 15
x 104
-10
-8
-6
-4
-2
0
2x 10
5
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.2 0.4 0.6 0.8-1
0
1
2
3
4
5
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
2000
4000
6000
8000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
525F_ 100micron tip_ test 004
65 70 75 8010
20
30
Modulus [GPa]
0.94 0.96 0.98 10
100
200
R2
0 50 100 1500
50
Modulus Length [#points]-1.5 -1 -0.5 00
50
100
Hr [nm]
0 0.01 0.02 0.030
50
100
Fit1 Avg.Abs.Res.0 0.02 0.04 0.06 0.08
0
50
100
Fit1 Max.Abs.Res.0.05 0.1 0.15 0.2 0.250
50
100
Fit2 Avg.Abs.Res.0.2 0.4 0.6 0.8 10
50
Fit2 Max.Abs.Res.
0.2 0.4 0.6 0.80
50
h change [nm/nm]0.1 0.2 0.3 0.4 0.50
50
P change [mN/mN]4 6 8 10
x 10-3
0
50
100
Fit4 Avg.Abs.Res.0.01 0.02 0.03 0.040
50
100
Fit4 Max.Abs.Res.
0 0.1 0.2 0.3 0.40
50
100
P* [mN]
6 8 10 120
50
100
h* [nm]
0 1 2 3 4
x 10-3
0
20
40
dP [mN]-1 -0.5 0 0.5
0
50
100
dH [nm]
effective
sample
Fit1
Fit2
Fit3
525F_ 100micron tip_ test 004Estat = mean: 72.9655 median: 72.8722 stdev: 1.7495 min: 70.0414 max: 75.9761
Ystat = mean: 0.3900 median: 0.3888 stdev: 0.0169 min: 0.3590 max: 0.4202
Hstat = mean: 17.9959 median: 17.9677 stdev: 0.4532 min: 17.2153 max: 18.7965
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.2
0.4
0.6
0.8
1
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.4561; Bunge=0, 0, 0; Strength=0.38674; Hardening=18.0079
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
0 200 400 600 8000
50
100
150
200
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
x 105
-4
-3
-2
-1
0x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2-5
0
5
10
15
20
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
2000
4000
6000
8000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
525F_ 100micron tip_ test 005
66 68 70 72 74 760
10
20
Modulus [GPa]
0.95 0.96 0.97 0.98 0.99 10
20
40
R2
70 80 90 100 110 1200
20
40
Modulus Length [#points]-1.5 -1 -0.5 00
20
40
Hr [nm]
0.005 0.01 0.015 0.020
20
40
Fit1 Avg.Abs.Res.0.02 0.04 0.06 0.08 0.10
20
40
Fit1 Max.Abs.Res.0.1 0.15 0.2 0.25 0.3 0.350
50
Fit2 Avg.Abs.Res.0.2 0.4 0.6 0.8 1 1.20
20
40
Fit2 Max.Abs.Res.
0.2 0.3 0.4 0.50
10
20
h change [nm/nm]0.2 0.25 0.3 0.35
0
20
40
P change [mN/mN]7 8 9 10
x 10-3
0
20
40
Fit4 Avg.Abs.Res.0.02 0.025 0.03 0.035 0.040
50
Fit4 Max.Abs.Res.
0 0.1 0.2 0.3 0.4 0.50
50
P* [mN]
2 4 6 8 100
20
40
h* [nm]
0 1 2 3 4 5
x 10-3
0
20
40
dP [mN]-0.6 -0.4 -0.2 0 0.2 0.40
20
40
dH [nm]
effective
sample
Fit1
Fit2
Fit3
525F_ 100micron tip_ test 005Estat = mean: 72.9610 median: 73.1697 stdev: 1.8039 min: 70.0003 max: 75.9999
Ystat = mean: 0.3449 median: 0.3440 stdev: 0.0155 min: 0.3150 max: 0.3783
Hstat = mean: 17.3682 median: 17.4043 stdev: 0.4815 min: 16.5865 max: 18.4025
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
0.9
1
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.4314; Bunge=0, 0, 0; Strength=0.3375; Hardening=17.4237
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
0 200 400 600 8000
50
100
150
200
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 0.5 1 1.5 2
x 105
-3
-2.5
-2
-1.5
-1
-0.5
0x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5-5
0
5
10
15
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
2000
4000
6000
8000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
650F_ 100micron tip_ test 002
65 70 75 800
10
20
Modulus [GPa]
0.98 0.99 1 1.010
50
R2
20 40 60 800
10
20
Modulus Length [#points]-2 -1 0 1
0
10
20
Hr [nm]
0.08 0.1 0.12 0.14 0.160
20
40
Fit1 Avg.Abs.Res.0.2 0.3 0.4 0.50
20
40
Fit1 Max.Abs.Res.0 0.1 0.2 0.3 0.4
0
10
20
Fit2 Avg.Abs.Res.0 0.5 1 1.5
0
10
20
Fit2 Max.Abs.Res.
0.7 0.8 0.9 10
10
20
h change [nm/nm]0.4 0.5 0.6 0.7 0.80
20
40
P change [mN/mN]0.02 0.03 0.04 0.050
10
20
Fit4 Avg.Abs.Res.0.04 0.05 0.06 0.07 0.080
10
20
Fit4 Max.Abs.Res.
0.8 1 1.2 1.40
10
20
P* [mN]
30 35 40 450
10
20
h* [nm]
0 0.005 0.01 0.0150
10
20
dP [mN]-0.5 0 0.5 1 1.50
10
20
dH [nm]
effective
sample
Fit1
Fit2
Fit3
650F_ 100micron tip_ test 002Estat = mean: 73.0756 median: 72.9917 stdev: 1.6628 min: 70.1255 max: 75.9698
Ystat = mean: 0.2518 median: 0.2515 stdev: 0.0119 min: 0.2208 max: 0.2790
Hstat = mean: 12.9052 median: 12.8873 stdev: 0.7722 min: 11.7981 max: 14.2977
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.1
0.2
0.3
0.4
0.5
0.6
0.7
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.4988; Bunge=0, 0, 0; Strength=0.25718; Hardening=12.4377
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
0 200 400 600 8000
20
40
60
80
100
120
140
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 1 2 3
x 105
-12
-10
-8
-6
-4
-2
0x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2-5
0
5
10
15
20
25
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.030
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
650F_ 100micron tip_ test 003
650F_ 100micron tip_ test 003Estat = mean: 72.8141 median: 72.5877 stdev: 1.7410 min: 70.0232 max: 75.9629
Ystat = mean: 0.2503 median: 0.2504 stdev: 0.0100 min: 0.2326 max: 0.2741
Hstat = mean: 13.3240 median: 13.2591 stdev: 0.4620 min: 12.0619 max: 14.2475
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.1
0.2
0.3
0.4
0.5
0.6
0.7
0.8
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.2711; Bunge=0, 0, 0; Strength=0.25215; Hardening=13.2591
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
0 500 10000
50
100
150
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 1 2 3
x 105
-14
-12
-10
-8
-6
-4
-2
0x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2-5
0
5
10
15
20
25
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.03 0.040
2000
4000
6000
8000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
650F_ 100micron tip_ test 004
65 70 75 800
5
10
Modulus [GPa]
0.98 0.99 1 1.010
20
40
R2
20 40 60 800
10
20
Modulus Length [#points]-2 -1 0 1
0
10
20
Hr [nm]
0.1 0.12 0.14 0.160
20
40
Fit1 Avg.Abs.Res.0.25 0.3 0.35 0.4 0.450
10
20
Fit1 Max.Abs.Res.0 0.1 0.2 0.3 0.4
0
10
20
Fit2 Avg.Abs.Res.0 0.5 1 1.5
0
10
20
Fit2 Max.Abs.Res.
0.75 0.8 0.85 0.9 0.950
5
10
h change [nm/nm]0.4 0.5 0.6 0.7 0.80
10
20
P change [mN/mN]0.02 0.03 0.04 0.050
5
10
Fit4 Avg.Abs.Res.0.045 0.05 0.055 0.060
5
10
Fit4 Max.Abs.Res.
0.7 0.8 0.9 10
5
10
P* [mN]
54 56 58 600
5
10
h* [nm]
0 0.005 0.010
10
20
dP [mN]-0.5 0 0.5 10
10
20
dH [nm]
effective
sample
Fit1
Fit2
Fit3
650F_ 100micron tip_ test 004Estat = mean: 72.7263 median: 72.4234 stdev: 1.7910 min: 70.0506 max: 75.9400
Ystat = mean: 0.2271 median: 0.2261 stdev: 0.0108 min: 0.1959 max: 0.2459
Hstat = mean: 12.3714 median: 12.0507 stdev: 0.6598 min: 11.5263 max: 13.4687
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.1
0.2
0.3
0.4
0.5
0.6
0.7
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.1896; Bunge=0, 0, 0; Strength=0.23049; Hardening=12.0506
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
0 200 400 600 8000
20
40
60
80
100
120
140
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 1 2 3
x 105
-14
-12
-10
-8
-6
-4
-2
0x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 2-5
0
5
10
15
20
25
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.030
2000
4000
6000
8000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
650F_ 100micron tip_ test 005
65 70 75 800
5
10
Modulus [GPa]
0.96 0.98 1 1.020
20
40
R2
20 40 60 800
5
10
Modulus Length [#points]-1 -0.5 0 0.5
0
5
10
Hr [nm]
0.08 0.1 0.12 0.14 0.160
10
20
Fit1 Avg.Abs.Res.0.2 0.25 0.3 0.35 0.40
10
20
Fit1 Max.Abs.Res.0.05 0.1 0.15 0.2 0.250
5
10
Fit2 Avg.Abs.Res.0 0.5 1
0
10
20
Fit2 Max.Abs.Res.
0.75 0.8 0.85 0.9 0.950
5
10
h change [nm/nm]0.4 0.5 0.6 0.7 0.80
5
10
P change [mN/mN]0.025 0.03 0.035 0.04 0.0450
5
10
Fit4 Avg.Abs.Res.0.05 0.055 0.06 0.0650
5
10
Fit4 Max.Abs.Res.
0.55 0.6 0.65 0.7 0.750
5
10
P* [mN]
31 32 33 34 350
5
10
h* [nm]
0 2 4 6 8
x 10-3
0
5
10
dP [mN]-0.5 0 0.5 10
5
10
dH [nm]
effective
sample
Fit1
Fit2
Fit3
650F_ 100micron tip_ test 005
Estat = mean: 73.0497 median: 72.7548 stdev: 1.8111 min: 70.0597 max: 75.9970
Ystat = mean: 0.2244 median: 0.2263 stdev: 0.0123 min: 0.1897 max: 0.2476
Hstat = mean: 13.1493 median: 13.0770 stdev: 0.4404 min: 12.2847 max: 13.9221
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.1
0.2
0.3
0.4
0.5
0.6
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.467; Bunge=0, 0, 0; Strength=0.23406; Hardening=12.931
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
0 200 400 6000
20
40
60
80
100
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 0.5 1 1.5 2 2.5
x 105
-8
-6
-4
-2
0x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5-5
0
5
10
15
20
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.030
1000
2000
3000
4000
5000
6000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
650F_ 100micron tip_ test 006
66 68 70 72 74 760
10
20
Modulus [GPa]
0.95 0.96 0.97 0.98 0.99 10
20
40
R2
20 25 30 35 40 450
10
20
Modulus Length [#points]-1 -0.5 0 0.5 1
0
10
20
Hr [nm]
0.1 0.2 0.3 0.4 0.50
10
20
Fit1 Avg.Abs.Res.0 0.5 1 1.5 2
0
10
20
Fit1 Max.Abs.Res.0.1 0.2 0.3 0.4 0.5 0.60
10
20
Fit2 Avg.Abs.Res.0 0.5 1 1.5 2
0
10
20
Fit2 Max.Abs.Res.
0.75 0.8 0.85 0.9 0.950
20
40
h change [nm/nm]0.65 0.7 0.75 0.8
0
10
20
P change [mN/mN]0.045 0.05 0.055 0.06 0.065 0.070
10
20
Fit4 Avg.Abs.Res.0.06 0.07 0.08 0.09 0.1 0.110
10
20
Fit4 Max.Abs.Res.
0 1 2 3 4 50
10
20
P* [mN]
60 70 80 90 100 1100
10
20
h* [nm]
0 0.01 0.02 0.030
10
20
dP [mN]0 0.5 1 1.5 2 2.5
0
10
20
dH [nm]
effective
sample
Fit1
Fit2
Fit3
650F_ 100micron tip_ test 006
Estat = mean: 72.5025 median: 72.0208 stdev: 1.7646 min: 70.0303 max: 75.9951
Ystat = mean: 0.1528 median: 0.1565 stdev: 0.0120 min: 0.1219 max: 0.1704
Hstat = mean: 14.1212 median: 13.9646 stdev: 0.8057 min: 12.9491 max: 15.8711
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.1
0.2
0.3
0.4
0.5
0.6
0.7
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=68.9422; Bunge=0, 0, 0; Strength=0.16582; Hardening=13.5432
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
-200 0 200 400 600 8000
20
40
60
80
100
120
140
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 1 2 3 4
x 105
-2.5
-2
-1.5
-1
-0.5
0
0.5x 10
7
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5 20
5
10
15
20
25
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.030
2000
4000
6000
8000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
775F_ 100micron tip_ test 002
66 68 70 72 74 760
5
10
Modulus [GPa]
0.95 0.96 0.97 0.98 0.99 10
10
20
R2
30 35 40 45 50 550
5
10
Modulus Length [#points]-1 -0.5 0 0.5 1
0
5
10
Hr [nm]
0.08 0.1 0.12 0.14 0.160
10
20
Fit1 Avg.Abs.Res.0.3 0.32 0.34 0.36 0.38
0
10
20
Fit1 Max.Abs.Res.0.1 0.15 0.2 0.250
5
10
Fit2 Avg.Abs.Res.0.2 0.4 0.6 0.8 10
10
20
Fit2 Max.Abs.Res.
0.86 0.88 0.9 0.92 0.940
5
10
h change [nm/nm]0.55 0.6 0.65 0.7 0.750
5
10
P change [mN/mN]0.02 0.03 0.04 0.05 0.06 0.070
5
10
Fit4 Avg.Abs.Res.0.04 0.06 0.08 0.10
10
20
Fit4 Max.Abs.Res.
0.5 0.6 0.7 0.8 0.9 10
5
10
P* [mN]
56 58 60 62 64 660
5
10
h* [nm]
0 0.002 0.004 0.006 0.008 0.010
5
10
dP [mN]-0.5 0 0.5 1 1.5 20
5
10
dH [nm]
effective
sample
Fit1
Fit2
Fit3
775F_ 100micron tip_ test 002
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.1
0.2
0.3
0.4
0.5
0.6
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.0392; Bunge=0, 0, 0; Strength=0.15987; Hardening=11.39
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
0 200 400 600 8000
20
40
60
80
100
120
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 0.5 1 1.5 2 2.5
x 105
-14
-12
-10
-8
-6
-4
-2
0x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.5-5
0
5
10
15
20
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.030
2000
4000
6000
8000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
Estat = mean: 72.6774 median: 72.4660 stdev: 1.5328 min: 70.1452 max: 75.7897
Ystat = mean: 0.1801 median: 0.1808 stdev: 0.0080 min: 0.1588 max: 0.2022
Hstat = mean: 10.8999 median: 10.8444 stdev: 0.3716 min: 10.1605 max: 11.7637
775F_ 100micron tip_ test 004
66 68 70 72 74 760
5
10
Modulus [GPa]
0.96 0.97 0.98 0.99 1 1.010
10
20
R2
20 30 40 50 60 700
5
10
Modulus Length [#points]-1.5 -1 -0.5 0 0.5 10
5
10
Hr [nm]
0.1 0.12 0.14 0.160
5
10
Fit1 Avg.Abs.Res.0.25 0.3 0.35 0.4 0.450
5
10
Fit1 Max.Abs.Res.0.1 0.15 0.2 0.250
5
10
Fit2 Avg.Abs.Res.0.4 0.5 0.6 0.7
0
5
10
Fit2 Max.Abs.Res.
0.8 0.85 0.9 0.95 10
2
4
h change [nm/nm]0.5 0.6 0.7 0.8 0.90
5
10
P change [mN/mN]0.02 0.03 0.04 0.05 0.06 0.070
10
20
Fit4 Avg.Abs.Res.0.04 0.05 0.06 0.07 0.08 0.090
10
20
Fit4 Max.Abs.Res.
0.7 0.8 0.9 1 1.10
10
20
P* [mN]
44 46 48 50 52 540
5
10
h* [nm]
0 0.002 0.004 0.006 0.008 0.010
5
10
dP [mN]-1 -0.5 0 0.5 1 1.5
0
5
10
dH [nm]
effective
sample
Fit1
Fit2
Fit3
775F_ 100micron tip_ test 004Estat = mean: 72.9440 median: 72.5348 stdev: 1.7310 min: 70.2726 max: 75.8985
Ystat = mean: 0.1815 median: 0.1793 stdev: 0.0162 min: 0.1483 max: 0.2122
Hstat = mean: 11.4562 median: 11.0910 stdev: 0.7168 min: 10.4900 max: 12.6142
0 0.005 0.01 0.015 0.02 0.025 0.03 0.035 0.040
0.1
0.2
0.3
0.4
0.5
0.6
Ind. Strain
Ind.
Str
ess
[GP
a]
Es=69.1715; Bunge=0, 0, 0; Strength=0.18232; Hardening=10.8001
Stress-StrainModulus Line
Hardening Fit
Strain Offset
Modulus Fit Data
Hardening Fit DataYield Point
0 200 400 600 8000
20
40
60
80
100
120
displacement / nm
load
/ m
N
Load Vs. Displacement
Raw Data
0 Pt. Data
0 0.5 1 1.5 2 2.5
x 105
-12
-10
-8
-6
-4
-2
0x 10
6
S
P2/
3-S
h
Zero Point Fit
Raw Data
0 Pt. Data
0 0.5 1 1.50
5
10
15
20
P 2/3
h
Modulus Fit
Data
Elastic
0 0.01 0.02 0.030
1000
2000
3000
4000
5000
6000
7000
Strain
Con
tact
Rad
ius
/ nm
Strain Vs. Contact Radius
Data
Elastic
775F_ 100micron tip_ test 005
775F_ 100micron tip_ test 005Estat = mean: 73.0240 median: 73.0903 stdev: 1.7293 min: 70.0061 max: 75.9250
Ystat = mean: 0.2102 median: 0.2100 stdev: 0.0102 min: 0.1834 max: 0.2314
Hstat = mean: 9.9928 median: 9.9663 stdev: 0.2857 min: 9.4651 max: 10.6556
775F_ 100micron tip_ test 007
775F_ 100micron tip_ test 007
775F_ 100micron tip_ test 010
775F_ 100micron tip_ test 010
Elastic module Yield strength (GPa) HardeningAs received
400 F 55.73153 0.422567 20.59428525 F 56.33968 0.2724 14.30632650 F775 F
