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d^5* OREGON
Environmental Laboratory Accreditation Program
TestAmerica Denver 4025
4955 Yarrow St. ,Arvada, CO 80002 ! '
IS GRANTED APPROVAL BY ORELAP UNDER THE 2009 TNI STANDARDS, TO PERFORM ANALYSES ON ENVIRONMENTAL SAMPLES IN MATRICES AS LISTED BELOW :
J;^?i§rmS0f
NELAP Recognized
Air Drinking WaterNon Potable
WaterSolids and
Cbem. Waste Tissue
Chemistry Chemistry Chemistry
AND AS RECORDED IN THE LIST OF APPROVED ANALYTES, METHODS, ANALYTICAL TECHNIQUES, AND FIELDS OF TESTING ISSUED CONCURRENTLY WITH THIS CERTIFICATE AND REVISED AS NECESSARY.
ACCREDITED STATUS DEPENDS ON SUCCESSFUL ONGOING PARTICIPATION IN THE PROGRAM AND CONTINUED COMPLIANCE WITH THE STANDARDS. ,
CUSTOMERS ARE URGED TO VERIFY THE LABORATORY’S CURRENT ACCREDITATION STATUS IN OREGON.v/ J sJ~<Pr'
Gary fc'. Ward, MS Oregon State Public Health Laboratory ORELAP Administrator 3150 NW. 229th Ave, Suite 100 Hillsboro, OR 97124
EFFECTIVE DATE : 01/9/2017
EXPIRATION DATE : 01/8/2018
Certificate No : 4025 - 006
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«ELiOREGON
Environmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002
ORELAP ID: 4025
C000026EPA CODE:
Certificate: 4025-006
Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.
MATRIX Reference Code Analyte Code DescriptionDrinkingWater DV-LC-0012 i 60036035 TestAmerica Denver - PFOA in NPW
and SCM by HPLC-MS-MS
7044 Ammonium Perfluorooctanoate (APFO)
6911 Perfluorobutane Sulfonate (PFBS)
6915 Perfluorobutyric acid (PFBA)
9562 Perfluorodecane Sulfonate (PFDS)
6905 Perfluorodecanoic acid (PFDA)
6903 Perfluorododecanoic (PFDDA)
6908 Perfluoroheptanoic acid (PFHA)
6910 Perfluorohexane Sulfonate (PFHS)
6913 Perfluorohexanoic acid (PFHXA)
6906 Perfluorononanoic acid (PFNA)
6917 Perfluorooctane Sulfonamide (PFOSA)
6912 Perfluorooctanoic acid (6909 Perfluorooctanoic Sulfonate (PFOS)
6914 Perfluoropentanoic acid (PFPEA)
6902 Perfluorotetradecanoic acid (PFTDA)
9563 Perfluorotridecanoic (PFTRIA)
6904 Perfluoroundecanoic acid (PFUDA)
Non-Potable ASTM D5057- 30032134 Screening Apparent Specific GravityWater 10 and Bulk Density of Waste
8042 Specific Gravity (Relative Density)
ASTM D7065- 30032918 Nonylphenol by GC/MS06
6513 4-Nonylphenol
9466 4-Nonylphenol diethoxylate
6512 4-tert-Octylphenol
9301 Bisphenol A
9592 Nonyl phenol monoethoxylate
CA HML 939-M 90016765 Determination of Organic LeadCompounds by Graphite FurnaceAbsorption Spectrometry
1208 Organic Lead
D1429-08 30023439 Standard Test Methods for SpecificGravity of Water and Brine
8042 Specific Gravity (Relative Density)
DV-LC-0012 60036035 TestAmerica Denver - PFOA in NPW .and SCM by HPLC-MS-MS M
7044 Ammonium Perfluorooctanoate (APFO)
6911 Perfluorobutane Sulfonate (PFBS)
6915 Perfluorobutyric acid (PFBA)
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 1 Of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002
EPACODE: C000026
Certificate: 4025 - 006
Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Perfluorodecane Sulfonate (PFDS)
Perfluorodecanoic acid (PFDA)
Perfluorododecanoic (PFDDA)
,J)f(----- ItJ .
Non- DV-LC-0012 9562
Potable 6905
Water 6903
6908
6910
6913
6906
r in ’ fr - f6910 Perflubrohexarie-Sulfonate (PFHS)/
^ 691.7 .Vtr
'^',6912^
i'. '6909
’6914
>Perfluorooctane Sulfonamide (PFOSA)
Perfluorooctanoic acid
Perfluorooctanoic Sulfonate (PFOS)
Perfluoropentanoic acid (PFPEA)
'dj f/t\ O
!; / /[/J- Z7, i'V, <HV.
6902 Perfluorotetradecanoic acid (PFTDA)
V—’-V9563 Perfluorotridecanoic (PFTRIA)
6904 Perfluoroundecanoic acid (PFUDA)
DV-LC-0020 3
6119 Disodium Inimodiacetate
60036013 TestAmerica Denver - Disodium Iminodiacetate (IDA) by LC/MS/MS (modified EPA 8321 A)
DV-WC-0077
9378 1,1-Dimethyl hydrazine
60036046 TestAmerica Denver - Determination of Hydrazine, Monomethyl Hydrazine, and Unsymmetrical Dimethylhydrazine by IC
9486 Hydrazine
9495 Methyl hydrazine (MMH)
EPA 1010 10116606 Pensky-Martens Closed-Cup Method for Determining Ignitability
" \(L.!0 ' 1780 IgnitabilityEPA 1010A SJV~
K10234807 , i Pensky-Martens Closed-Cup Method for
Determining Ignitability? 1780':., Ignitability
EPA 1311 ^ j , S- "0)
8031 ■ - -T--•- Extraction'/l?i;eparation;L j ‘| ,/?”V
10118806r-A ^
- "Toxicity Characteristic Leaching Procedure
EPA 1312 j'U-fj 11 Ij.'i -',' - J 13 10119003 Synthetic Precipitation Leaching Procedure
8031 Extraction/Preparation
EPA 160.4
1947 Residue - Fixed
10010409 Total Volatile Solids, ignition @ 550 C.
1948 Residue - Fixed, Nonfilterable (FSS)
2070 Volatile suspended solids
EPA 160.4
1970 Residue-volatile
10010409 Total Volatile Solids, ignition @ 550 C.
EPA1664A(HEM)
1803 n-Hexane Extractable Material (O&G)
10127807 N-Hexane Extractable Material (Oil and Grease) by Extraction and Gravimetry
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
2 of 70
oEL«CESS* OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields ofAccreditation ORELAP ID: 4025
TestAmerica Denver EPA CODE: C000026
4955 Yarrow St. Certificate: 4025- 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- Potable Water
EPA 1664A (HEM)
1860 Oil & Grease
EPA 1664A 10261606 Silica Gen Treated N-Hexane(SGT-HEM)
2050
Tr?'- pi—, fT"- ” /v’tn
TotaLPetroleum-Hydrocarbons (TPW) )1Extractable Material (Oil and Grease)
EPA1664B i V“-‘- i/, —3 \
V-J/ /.<•( I fjN-Hexane Extractable Material (Oil and Grease) by Extraction and Gravimetry
. 1803 n-Hexane Extractable Material (O&G)U I £j .
yv 1860 - Oil & Grease ' .e r.
EPA1664B CO 10260628 \ Silica Gel Treated n-Hexane Extractable(SGT-HEM)---- o'- X' vMaterial(Oil & Grease)
‘ - 2050 Total Petroleum Hydrocarbons (TPH)
EPA 180.1 2 10011800 Tur6jdity: Nephelometric
2055 Turbidity
EPA 200.7 4.4
1000 Aluminum
10013806 ICP - metals
1005 Antimony 11010 Arsenic
1015 Barium
1020 Beryllium
1025 Boron
1030 Cadmium
1035 Calcium
1040 Chromium
1050 Cobalt
Qy* . 1055 Copperi: r 1760 Hardness (calc.) '•x-
- f |1070 Iron , r—.
1075 5 •'.Lead /h;:
1080// /Lithium ' __ '
1085 ‘ Magnesium / ,J / ; ~1 f.fi 'r~i H i ^ | ’t 'i .•4
1090 Manganese-' ; .; i 1 '
1100 Molybdenum
1105 Nickel
1910 Phosphorus, total
1125 Potassium
1140 Selenium
1990 Silica as Si02
1145 Silicon
1150 Silver 11155 Sodium
1160 Strontium
2017 Sulfur
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 3 of 70
oEUo'SSS OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025-006
Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-PotableWater
EPA 200.7 4.4
EPA 200.8 5.4
1165
1175
1180
1185
1190
i1005
.1010.»■> \.10.15
’1*620
1030
Thallium
Tin
Titanium
Vanadium
Zinc-!:
. \
Antimony ^ Arsenic
Barium
Beryllium
Cadmium
to fft -SI, ‘I I If l ff'I. !■ -- „[i, •■lL'LIjJ:, 'lin ifp0014605 Metals by ICP-MS
/>
\SC. Oi H
1040
1050
Chromium
Cobalt■A A
>->- —1/
1055 Copper
1075 Lead
1090 Manganese
1100 Molybdenum
1105 Nickel
1140 Selenium
1150 Silver
1165 Thallium
1170 Thorium
1175 Tin
3035 Uranium h
1185 Vanadium
-.1190 ZincEPA 245.1 3 ^ 10036609. . Z ^Mercury by Cold Vapor Atomic
, Absorption
-1,095 C J,Mercury
EPA 300.0 ' i'
1540'■Cj, 1 - ,1 f 1 ^ i-v T.t- cr-Brorhide-'/ <,( )' 1 Jr]-!: i
i ! 10053006' Ion chromatography - anions.
1! 7 ■ f Aii- -
1575 Chloride vl !•;' AA 1 i_.' ---
1730 Fluoride
1810 Nitrate as N
1820 Nitrate-nitrite
1840 Nitrite as N
1870 Orthophosphate as P
2000 Sulfate
EPA 3005A 10133207 Acid Digestion of waters for TotalRecoverable or Dissolved Metals
9822 Extraction/Preparation
EPA 3010A 10133605 Acid Digestion of Aqueous samples and Extracts for Total Metals
9822 Extraction/Preparation
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
4 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPACODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-PotableWater
EPA 3020A
9822 Extraction/Preparation
10134404 Acid Digestion of Aqueous samples and Extracts for Total Metals for Analysis by GFAA
EPA 335.1 _ ^ - t— (V"' S 10060001i | i>^ "'p
Cyanides, amenable to chlorination
1510 t Amenable cyanide'O
EPA 335.4 I
t VL L.\ ,1 J S'. »-- < -■ *1' 1645 Total cyanide
!‘s4.0061402 ,r> Methods for the Determination of ,»lnorganic Substances in Environmental .'‘Samples
EPA 350.1 2 10063602 ' Ammonia Nitrogen - Colorimetric, Auto Rhe'nate':
-O 1515 Ammonia as N '• j
EPA 351.2 2
1795 Kjeldahl nitrogen - total
10065404 Total Kjeldahl Nitrogen - Block Digest, Phenate_; v
EPA 351.2 minus EPA
10238207 Organic Nitrogen by AutomatedPhenate (Calculated)
350.1 1865 Organic nitrogen •EPA 3510C
9822 Extraction/Preparation
10138202 Separatory Funnel Liquid-liquid extraction
EPA 3520C
9822 Extraction/Preparation
10139001 Continuous Liquid-liquid extraction
EPA 353.2 2 10067604 Nitrate/Nitrite Nitrogen - Automated, Cadmium
- 1810 Nitrate as N•
- 1820 Nitrate-nitrite ^ --
M 1825 Total nitrate+nitrite_
:EPA 3535A rV
L /.10139409 ~ ,'Solid-Phase Extraction (SPE)
9822' ' Extraction/Preparation'’.'s'.y''"
EPA 3580A J 1 . J J • 1 .l.. 10143007 Waste Dilution
8031 ' / ’ • ' 1 j' ‘lExtraction/Pfepal'dtion 1 11 1 ilr ' S:
EPA 3620B
9822 Extraction/Preparation
10145809 Florisil Cleanup
EPA 365.1 2
1870 Orthophosphate as P
10070005 Phosphorous - Colorimetric, Automated persulfate
1910 Phosphorus, total
EPA 3660B 10148400 Sulfur cleanup
8031 Extraction/Preparation £
EPA 3665A 10148808 Sulfuric Acid / permanganate Cleanup
9822 Extraction/Preparation
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 5 Of 70
oELt OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields ofAccreditation ORELAP ID: 4025
TestAmerica Denver EPA CODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number._________Non-PotableWater
EPA 410.4 2 10077404 Chemical Oxygen Demand ■ Colorimetric, Automated.
1565 Chemical oxygen demand
EPA 420.1
1905 Total phenolics pp
10079400-ftdn , „'fr$ —
U . ! 'V -
Phenolics - Spectrophotometric, manual.
EPA 420.4
S?•V*19,05
F i Jw b ~-J ^3 ~
ir.T ^,-pTotal phenolics
J [ [10080203.1 J | jTH~(/M
il- / S
Phenolics, Total Recoverable by Semi- Automated Colorimetry
vEPA 5030B -A
'OO't/ \r
,9822 Extraction/Preparation
10153409 :3/. .Burge and trap for aqueous samples
EPA 5030C V. 10284603 Purge-ancHTrap for Aqueous Samples
8031 Extraction/Preparation
EPA 6010B
1000 Aluminum
10155609 ICP - AES '
1005 Antimony
1010 Arsenic
1015 Barium
1020 Beryllium
1025 Boron
1030 Cadmium
1035 Calcium
1040 Chromium
1050 Cobalt
1055 Copper
r1070
1075"[1080
1085'
Iron
Lead
>_ Lithium
Pd, MagnesiumJ; Manganese
Molybdenbrp,!
j
’v. r*"'V>: r
1090
1100
.. V"’
1105
1910
Nickel [[ [I,
Phosphorus, total
It 3-
1125 Potassium
1140 Selenium
1990 Silica as Si02
1145 Silicon
1150 Silver
1155 Sodium
1160 Strontium
2017 Sulfur
1165 Thallium
1175 Tin
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
6 of 70
oEU(CT4 OREGON
Environmental Laboratory Accreditation Program
ORELAP Fields of ^„I_1 _Accreditation ORELAP ID: 4025
TestAmerica Denver EPA CODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 6010B 1180 Titanium
Potable 1185 Vanadium
Water 1190 Zinc
EPA 6010C^ fOi
1000r'
Aluminuhii f r-y\: \ 1*, M
1005 \ ^Antimony
1010 ' Arsenic^Barium
,, ■. .1020' Beryllium__ .”'1025
/ - jBoron
1030 Cadmium
1035 Calcium
1040 Chromium
1050 Cobalt
1055 Copper
1070 Iron
1075 Lead
1080 Lithium
1085 Magnesium
1090 Manganese
1100 Molybdenum
1105 Nickel
1910 Phosphorus, total
1125 Potassiumr,l- 1140 Selenium
-1990 Silica as Si02^ >145
Silicon! 1150. . . Silver
} -1155: Sodjum1160 lj ^Strontium
2017 Sulfur ■ r} i | ’
Thallium i >1165
1175 Tin
1180 Titanium
1185 Vanadium
1190 Zinc
_ J10155803
f(p/>H J .1 j t
ICP - AES
riM:
EPA 6010D 10155916 Metals by ICP - AES
1000 Aluminum
1005 Antimony
1010 Arsenic
1015 Barium
1020 Beryllium
1025 Boron
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 7 Of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2C
As of 1/9/2017 this list supercedes all previous lists for thiiNon- EPA 6010D 1030 Cadmium
Potable 1035 Calcium
Water 1040 Chromium
1050 Cobalt
1055 Copper .
1070 Iron
1075 Lead •'
1080 Lithium
1085 Magnesium
1090 Manganese
1100 Molybdenum
1105 Nickel
1910 Phosphorus, total
1125 Potassium
1140 Selenium
1990 Silica as Si02( 1145 Silicon
1150 Silver
1155 Sodium
1160 Strontium
2017 Sulfur
1165 Thallium
1175 Tin
1180 Titanium
1185 Vanadium
1190 Zinc
EPA 602
4610 1,2-Dichlorobenzene
4615 1,3-Dichlorobenzene
4620 1,4-Dichlorobenzene
4375 Benzene
4475 Chlorobenzene
4765 Ethylbenzene
5240 m+p-xylene
5000 Methyl tert-butyl ether (MTBE)
5250 o-Xylene
5140 Toluene
5260 Xylene (total)
ORELAP ID: 4025
EPA CODE: C000026
Certificate: 4025-006
EPA 6020
10102202 Purgeable Aromatics by GC/PID Purge & Trap
10156000 Inductively Coupled Plasma-Mass Spectrometry
1005
1010
1015
Antimony
Arsenic
Barium
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 8 of 70
fH OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
ORELAP ID:
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002
4025
C000026EPA CODE:
Certificate: 4025 - 006
Expiration Date: 1/8/2018Issue Date: 1/9/2017
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 6020 1020 Beryllium
Potable 1030 Cadmium
Water 1040 Chromium
1050 Cobalt
1055 Copper
1075 Lead
1090 Manganese
1100 Molybdenum
1105 Nickel
1140 Selenium
1150 Silver
1165 Thallium
1170 Thorium
1175 Tin
3035 Uranium
1185 Vanadium
| 1190 Zinc
EPA 6020A
1005 Antimony
1010 Arsenic
1015 Barium
1020 Beryllium
1030 Cadmium
1040 Chromium
1050 Cobalt
1055 Copper
1075 Lead
1090 Manganese
1100 Molybdenum
1105 Nickel
1140 Selenium
1150 Silver
1165 Thallium
1170 Thorium
1175 Tin
3035 Uranium
1185 Vanadium
1190 Zinc
>EPA 6020B2014
1005 Antimony
1010 Arsenic
1015 Barium
i‘
10156408 Inductively Coupled Plasma-Mass Spectrometry
10156420 Inductively Coupled Plasma-Mass Spectrometry
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 9 Of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPACODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-PotableWater
EPA 6020B 2014
1020
1030
1040
1050
1055
1075
1090
1100
1105
1140
1150
1165
1170
1175
3035
1185
1190
Beryllium
Cadmium
Chromium
Cobalt ,
Copper
Lead
Manganese
Molybdenum
Nickel
Selenium
Silver
Thallium
Thorium
Tin
Uranium
Vanadium
Zinc
EPA 608 10103603
7355 4,4'-DDD
7360 4,4-DDE
7365 4,4-DDT
7025 Aldrin
7110 alpha-BHC (alpha-Hexachlorocyclohexane)
7240 alpha-Chlordane
8880 Aroclor-1016 (PCB-1016)
8885 Aroclor-1221 (PCB-1221)
8890 . Aroclor-1232 (PCB-1232)
8895 Aroclor-1242 (PCB-1242)
8900 Aroclor-1248 (PCB-1248)
8905 Aroclor-1254 (PCB-1254)
8910 Aroclor-1260 (PCB-1260)
7115 beta-BHC (beta-Hexachlorocyclohexane)
7250
7105
7470
7510
7515
7520
7540
7530
7535
Chlordane (tech.)
delta-BHC
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Endrin ketone
Organochlorine Pesticides & PCBs by GC/ECD
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
10 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPACODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 608PotableWater
7120
7245
7685
gamma-BHC (Lindane, gamma- HexachlorocyclohexanE)
gamma-Chlordane
Heptachlor
7690 Heptachlor epoxide
7810 Methoxychlor , .
8250 Toxaphene (Chlorinated camphene)
EPA 610 (HPLC)
10297004 , Polynuclear Hydrocarbons by HPLC/UV-VIS
6380 1-Methylnaphthalene
6385 2-Methylnaphthalene
5500 Acenaphthene
5505 Acenaphthylene
5555 Anthracene
5575 Benzo(a)anthracene
5580 Benzo(a)pyrene
_ 5590 Benzo(g,h,i)perylenew 5600 Benzo(k)fluoranthene
5585 Benzo[b]fluoranthene
5855 Chrysene
5895 Dibenz(a.h) anthracene
6265 Fluoranthene
6270 Fluorene
6315 lndeno(1,2,3-cd) pyrene
5005 Naphthalene
6615 Phenanthrene
6665 Pyrene
EPA 614 10105201 Organophosphorous Pesticides by Liquid/Liquid Extraction and GC/NPD
7075 Azinphos-methyl (Guthion)
7410 Diazinon
8625 Disulfoton
7770 Malathion
7825 Methyl parathion (Parathion, methyl)
7955 Parathion, ethyl
EPA 614 10105201 Organophosphorous Pesticides by Liquid/Liquid Extraction and GC/NPD
7390 Demeton
7395 Demeton-o
7385 Demeton-s
EPA 624 10107207 Volatile Organic Compounds by purge and trap GC/MS
5105 1,1,1,2-Tetrachloroethane
5160 1,1,1 -Trichloroethane
5110 1,1,2,2-Tetrachloroethane
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
11 Of 70
aEU OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPA CODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 624 5165 1,1,2-Trichloroethane
Potable 4630 1,1-Dichloroethane
Water 4640 1,1 -Dichloroethylene
5180 1,2,3-Trichloropropane
4570 1,2-Dibromo-3-chloropropane (DBCP)
4585 1,2-Dibromoethane (EDB, Ethylene, dibromide)
4610 1,2-Dichlorobenzene
4635 1,2-Dichloroethane (Ethylene dichloride)
4655 1,2-Dichloropropane
4615 1,3-Dichlorobenzene
4620 1,4-Dichlorobenzene
4735 1,4-Dioxane (1,4- Diethyleneoxide)
4410 2-Butanone (Methyl ethyl ketone, MEK)
4500 2-Chloroethyl vinyl ether
4860 2-Hexanone (MBK)
4995 4-Methyl-2-pentanone (MIBK)
4315 Acetone
4325 Acrolein (Propenal)
4340 Acrylonitrile
4375 Benzene
4395 Bromodichloromethane
4400 Bromoform
4450 Carbon disulfide
4455 Carbon tetrachloride
4475 Chlorobenzene
4575 Chlorodibromomethane
4485 . Chloroethane (Ethyl chloride)
4505 Chloroform
4645 cis-1,2-Dichloroethylene
4680' cis-1,3-Dichloropropene
4595 Dibromomethane (Methylene bromide)
4625 Dichlorodifluoromethane (Freon-12)
4765 Ethylbenzene
5240 m+p-xylene
4950 Methyl bromide (Bromomethane)
4960 Methyl chloride (Chloromethane)
5000 Methyl tert-butyl ether (MTBE)
4975 Methylene chloride (Dichloromethane)
5005 Naphthalenei 4855 n-Hexane
5250 o-Xylene
5100 Styrene
5115 Tetrachloroethylene (Perchloroethylene)
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 12 Of 70
o!SS5o OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of A r,Accreditation ORELAP ID: 4025
TestAmerica Denver EPA CODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 624 5140 Toluene
Potable 5205 Total trihalomethanes
Water 4700 trans-1,2-Dichloroethylene
4685 trans-1,3-Dichloropropylene 4
5170 Trichloroethene (Trichloroethylene)
5175 Trichlorofluoromethane -(Fluorotrichloromethane, Freon 11)
5225 . Vinyl acetate
5235 Vinyl chloride
5260 Xylene (total)
EPA 625
6715 1,2,4,5-Tetrachlorobenzene
5155 1,2,4-Trichlorobenzene
4610 1,2-Dichlorobenzene
6221 1,2-Diphenylhydrazine
4615 1,3-Dichlorobenzene
\ 4620 1,4-Dichlorobenzene
4735 1,4-Dioxane (1,4- Diethyleneoxide)
4659 2,2-Oxybis(1 -chloropropane)
6835 2,4,5-T richlorophenol
6840 2,4,6-Trichlorophenol
5880 2,4-Diaminotoluene
6000 2,4-Dichlorophenol
6130 2,4-Dimethylphenol
6175 2,4-Dinitrophenol
6185 2,4-Dinitrotoluene (2,4-DNT)
6183 2,6-Diaminotoluene
6005 2,6-Dichlorophenol
6190 2,6-Dinitrotoluene (2,6-DNT)
5795 2-Chloronaphthalene
5800 2-Chlorophenol
6360 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2 -methylphenol)
6400 2-Methylphenol (o-Cresol)
6490 2-Nitrophenol
6412 3 & 4 Methylphenol
5945 3,3'-Dichlorobenzidine
5660 4-Bromophenyl phenyl ether (BDE-3)
5700 4-Chloro-3-methylphenol
5825 4-Chlorophenyl phenylether
I 6410 4-Methylphenol (p-Cresol)
6500 4-Nitrophenol
5500 Acenaphthene
5505 Acenaphthylene
10300002 Base/Neutrals and Acids by GC/MS
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
13 Of 70
oEUOW4 OREGON
Environmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 625
Potable Water
5510 Acetophenone
4330 Acrylamide
6700 alpha-Terpineol
5545 Aniline
5555 Anthracene
5562 Azobenzene - -
5565 Benzal chloride
5595 Benzidine
5575 Benzo(a)anthracene
5580 Benzo(a)pyrene
5590 Benzo(g,h,i)perylene
5600 Benzo(k)fluoranthene
5585 Benzo[b]fluoranthene
5610 Benzoic acid
5760 bis(2-Chloroethoxy)methane
5765 bis(2-Chloroethyl) ether
5780 bis(2-Chloroisopropyl) ether
5670 Butyl benzyl phthalate
5680 Carbazole
7210 Carbofuran phenol
5855 Chrysene
6065 Di(2-ethylhexyl) phthalate (bis(2- Ethylhexyl)phthalate, DEHP)
5895 Dibenz(a,h) anthracene
6070 Diethyl phthalate
6135 Dimethyl phthalate
5925 Di-n-butyl phthalate
6200 Di-n-octyl phthalate
6265 Fluoranthene
6270 Fluorene
6275 Hexachlorobenzene
4835 Hexachlorobutadiene
6285 Hexachlorocyclopentadiene
4840 Hexachloroethane
6315 lndeno(1,2,3-cd) pyrene
6320 Isophorone
5005 Naphthalene
5875 n-Decane
5015 Nitrobenzene
6530 n-Nitrosodimethylamine
6545 n-Nitrosodi-n-propylamine
6535 n-Nitrosodiphenylamine
6580 n-Octadecane
6590 Pentachlorobenzene
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 14 Of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPACODE: C000026
4955 Yarrow st. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 625 6605 Pentachlorophenol
Potable 6615 Phenanthrene
Water 6625 Phenol
6640 Phthalic anhydride
6665 Pyrene , l5095 Pyridine . • ■5200 Triethylamine
EPA 6860
1895 Perchlorate
10304800 ' Perchlorate in Water, Soils and Solid Wastes Using Ion Chromatography/Electrospray
‘ lonization/Mass Spectrometry
EPA7196A
1045 Chromium VI
10162400 Chromium Hexavalent colorimetric
EPA 7470A
1095 Mercury
10165807 Mercury in Liquid Waste by Cold Vapor Atomic Absorption
• EPA 8011 10173009 1,2-Dibromoethane and 1,2-Dibromo-3- chloropropane by Microextraction and GC/ECD
5180 1,2,3-Trichloropropane
4585 1,2-Dibromoethane (EDB, Ethylene dibromide)
4580 Dibromochloropropane
EPA 8015B
9369 Diesel range organics (DRO)
10173601 Non-halogenated organics usingGC/FID
4750 Ethanol
9408 Gasoline range organics (GRO)
4875 . Isobutyl alcohol (2-Methyl-1-propanol)
4895 •Isopropyl alcohol (2-Propanol, Isopropanol)
9488 Jet Fuel
4930 Methanol
9499 Motor Oil
4425 n-Butyl alcohol (1-Butanol, n-Butanol)
5055 n-Propanol
EPA8015C 10173805 Non-halogenated organics using GC/FID
9369
4720
4750
4785
9408
4875
Diesel range organics (DRO)
Diethylene glycol (2,2-Oxybisethanol)
Ethanol
Ethylene glycol
Gasoline range organics (GRO)
Isobutyl alcohol (2-Methyl-1 -propanol)
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 15 Of 70
aEUOW4 OREGON
Environmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
ORELAP ID: 4025
EPACODE: C000026
4955 Yarrow St. Certificate: 4025-006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.EPA8015C
PotableWater
4895
9488
4930
Isopropyl alcohol (2-Propanol,Isopropanol)
Jet Fuel
Methanol
9499 Motor Oil |
4425 n-Butyl alcohol (1-Butanol, n-Butanol)
5055 ; ; n-Propanol
6657 Propylene Glycol
9646 Triethylene Glycol
EPA8015D 10305609 Nonhalogenated Organics UsingGC/FID
9369 Diesel range organics (DRO)
4750 Ethanol
9408 Gasoline range organics (GRO)
4875 Isobutyl alcohol (2-Methyl-1-propanol)
4895 Isopropyl alcohol (2-Propanol,Isopropanol)
) 9488 Jet Fuel
4930 Methanol
9499 Motor Oil
4425 n-Butyl alcohol (1 -Butanol, n-Butanol)
5055 n-Propanol
EPA 8021B 10174808 Aromatic and Halogenated Volatiles byGC with PID and/or ECD Purge & Trap
4610 1,2-Dichlorobenzene
4615 1,3-Dichlorobenzene
4620 1,4-Dichlorobenzene
4375 Benzene
4475 Chlorobenzene
4765 Ethylbenzene
5240 m+p-xylene
5000 Methyl tert-butyl ether (MTBE) ;
5005 Naphthalene
5250 o-Xylene
5140 Toluene
5260 Xylene (total)
EPA 8081A 10178606 Organochlorine Pesticides by GC/ECD
8580 2,4'-DDD
8585 2,4-DDE
8590 2,4-DDT
7355 4,4-DDD9
7360 4,4-DDE
7365 4,4'-DDT
7025 Aldrin
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 16 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
As of 1/9/2017 this list supercedes all previous lists for this cerEPA 8081A 7110 alpha-BHC (alpha-
PotableHexachlorocyclohexane)
7240 aloha-ChlordaneWater 7115 beta-BHC (beta-
Hexachlorocyclohexane)
7250 Chlordane (tech.)
7260 Chlorobenzilate
7300 Chlorpyrifos
7105 delta-BHC
7405 Diallate
7460 Dicofol
7470 Dieldrin
7510 Endosulfan I
7515 Endosulfan II
7520 Endosulfan sulfate
7540 Endrin
7530 Endrin aldehyde1
7535 Endrin ketone
7120 gamma-BHC (Lindane, gamma- HexachlorocyclohexanE)
7245 gamma-Chlordane
7685 Heptachlor
7690 Heptachlor epoxide
6275 Hexachlorobenzene
6280 Hexachlorocyclohexanes
7725 Isodrin
7740 Kepone
7810 Methoxychlor
7870 Mirex
8045 Propachlor (Ramrod)
8250 Toxaphene (Chlorinated camphene)
EPA 8081B
8580 2,4-DDD
8585 2,4-DDE
8590 2,4-DDT
7355 4,4-DDD
7360 4,4'-DDE
7365 4,4'-DDT
7025 Aldrin
7110 alpha-BHC (alpha- Hexachlorocyclohexane)
¥ 7240 alpha-Chlordane
7115 beta-BHC (beta- Hexachlorocyclohexane)
7250 Chlordane (tech.)
EPACODE: C000026
Certificate: 4025 - 006
Expiration Date: 1/8/2018
10.178800 Organochlorine Pesticides by GC/ECD
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 17 of 70
oEL« OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
Test America Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
As of 1/9/2017 this list supercedes all previous lists for this cerEPA 8081B 7260 Chlorobenzilate
Potable 7300 Chlorpyrifos
Water 7105 delta-BHC
7405 Diallate r ; ,
7460 DicofOl ' ;
7470 ■ - Dieldrin - - --- -
7510 Endosulfan I
7515 Endosulfan II
7520 Endosulfan sulfate
7540 Endrin
7530 Endrin aldehyde
7535 Endrin ketone
7120 gamma-BHC (Lindane, gamma- HexachlorocyclohexanE)
7245 gamma-Chlordane
7685 Heptachlor
j 7690 Heptachlor epoxide
6275 Hexachlorobenzene
6280 Hexachlorocyclohexanes
7725 Isodrin
7740 Kepone
7810 Methoxychlor
7870 Mirex
8045 Propachlor (Ramrod)
8250 Toxaphene (Chlorinated camphene)
EPA 8082
8880 Aroclor-1016 (PCB-1016)
8885 Aroclor-1221 (PCB-1221)
8890 Aroclor-1232 (PCB-1232)
8895 Aroclor-1242 (PCB-1242)
8900 Aroclor-1248 (PCB-1248)
8905 Aroclor-1254 (PCB-1254)
8910 Aroclor-1260 (PCB-1260)
8912 Aroclor-1262 (PCB-1262)
8913 Aroclor-1268 (PCB-1268)
ORELAP ID: 4025
EPA CODE: C000026
Certificate: 4025-006
Expiration Date: 1/8/2018
10179007 Polychlorinated Biphenyls (PCBs) by GC/ECD
EPA 8082A 10179201 Polychlorinated Biphenyls (PCBs) by GC/ECD
8880 Aroclor-1016 (PCB-1016)
8885 Aroclor-1221 (PCB-1221)
8890 Aroclor-1232 (PCB-1232)
8895 Aroclor-1242 (PCB-1242)
8900 Aroclor-1248 (PCB-1248)
8905 Aroclor-1254 (PCB-1254)
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 18 of 70
aEU OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields ofAccreditation ORELAP ID. 4025
TestAmerica Denver EPA CODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-PotableWater
EPA 8082A
EPA 8141A
/‘f'V-
%
8910
8912
8913
7045
7065
7070
7075.
, 7125
;> 7220
7300
7315
7390
7395
7385
7410
8610
7475
8625
7550
7570
7580
7600
7605
7770
'7785
•7825
Aroclor-1260 (PCB-1260)
Aroclor-1262 (PCB-1262)
Aroclor-1268 (PCB-1268)
Cr’,-Anilazine:
-k
I”T—'*^1XO:-' f10182000
g)'Atrazihe
iljjiziriphos-ethyl (Ethyl guthion)
' Azinphos-methyl (Guthion)
Bolstar (Sulprofos)
Carbophenothion
Chlorpyrifos
Coumaphos
Demeton
Demeton-o
Demeton-s
Diazinon
Dichlorovos (DDVP, Dichlorvos)
Dimethoate
Disulfoton
EPN
Ethoprop
Famphur
Fensulfothion
Fenthion
Malathion
Merphos
Methyl parathion (Parathion, methyl)
Organophosphorous Pesticides by GC/NPD
m tif.nr ,fSIT-
_r:_s
Crib -VI.
a
!!>7850V^'Mevinphos
7905)
8290
7955
7985
8000
8060
8110
8125
8155
8200
8235
8245
8275
ji ii Naled . ti r-
6,0,0/Triethyl phosphorothioateA
If 4> I.
Q l;. I:
■ fi JParathion,"ethyl
Phorate
Phosmet (Imidan)
Propazine
Ronnel
Simazine
Sulfotepp
Tetrachlorvinphos (Stirophos, Gardona) Z-isomer
Thionazin (Zinophos)
Tokuthion (Prothiophos)
Trichloronate
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
19 Of 70
o£S5* OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002
EPACODE: C000026
Certificate: 4025 - 006
Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-PotableWater
EPA8141B 10182204 Organophosphorous Pesticides by GC/NPD
7045 Anilazine
7065 AtrazineT '-..si,Azinphos-ethy) .(Ethyl
£ p~-7070 guthion)f
7075 Azinphos-methyl (Gut
7125^ ^Bolstaf^Sulprofos)
„ 7220f.-f V-;:• . 7300.
Carbophenothion-TV
Chlorpyrifos^'’.^7315 CoumaphosXl ;: 7390 Demeton
7395 Demeton-o
7385 Demeton-s
7410 Diazinon
8610 Dichlorovos (DDVP, Dichlorvos)
7475 Dimethoate
8625 Disulfoton
7550 EPN
7570 Ethoprop
7580 Famphur
7600 Fensulfothion
7605 Fenthion
7770 Malathion
7785 Merphos
7825 Methyl parathion (Parathion, methyl)
7850 Mevinphos
‘ 7905 Naled
. L , 79551 i7985‘
Parathion, ethyl
' Phorate
^ lit
/ J"/
8000 i
8110
8125
8155
8200
8235
8245
8275
Phosrpet (Imidan)
Rorinel f'\-- SimStzine 'V ' I i Tfi.V' •*i ‘tSulfotepp ;i. j 1
Tetrachlorvinphos (Stirophos, Gardona) Z-isomer
Thionazin (Zinophos)
Tokuthion (Prothiophos)
Trichloronate
EPA 8151A 10183207 Chlorinated Herbicides by GC/ECD
8655
8545
8560
8555
8595
2,4,5-T
2.4- D
2.4- DB
Dalapon
Dicamba
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 20 Of 70
ttEUOREGON
Environmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025-006
Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-PotableWater
EPA 8151A 8605
8620
7775
7780
8645
8650
Dichloroprop (Dichlorprop)
Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)
MCPA
MCPB—,
EPA 8260B •t^tA"
'V
^Picloram'.!w...... .!jSilvexL{2,4,5-TP) vu A
——i!" A I I j'v101848024///
?
N.’
%-■ Q 'if
:5,105■‘'5185
5160
5110
5195
5165
5167
5172
5171
4630
4640
4670
5150
5180
5182
5155
,5210
4570
’• l, *3 f v //4695 J
i4697
4610
4635
4655
6800
5215
4615
4660
4675
4620
4735
4919
4510
1.1.1.2- Tetrachloroethane
1,1,1 -Trichloro-2,2,2-trifluoroethane
1.1.1- Trichloroethane
1.1.2.2- Tetrachloroethane
1.1.2- Trichloro-1,2,2-trifluoroethane (Freon 113)
1.1.2- T richloroethane
1.1.2- Trichlorofluoroethane
1.1.2- Trifluoroethane
1.1- Dichloro-1-fluoroethane
1.1- Dichloroethane
1.1- Dichloroethylene
1.1- Dichloropropene
1.2.3- Trichlorobenzene
1.2.3- Trichloropropane
1.2.3- T rimethylbenzene
1.2.4- T richlorobenzene
1.2.4- Trimethylbenzene
1.2- Dibromo-3-chloropropane (DBCP)
1.2- Dibromoethane (EDB, Ethylene 'T’dibromide)
",1\2-Dichloro-1,1,2,2-tetrafluoroethane(^reon‘11'4) J IT-.-, c-p |.\
fluoroethane ] f l 7.!u y
/.Volatile Organic Compounds by purge •' and trap GC/MS
'S-v
Yi.
cc,
Vl
■ i • i i f J — r,-J F-7., cr pj L it,',2-DjchjQtbr1,1,2j-trifluprpethanp ] ; I. _; “t (Y i'1' £ ji'7 J ’i,i Tj
1('-. I < '• if —1.2- DichlorobenzeneT ~t-
1.2- Dichloroethane (Ethylene dichloride)
1.2- Dichloropropane
1.3.5- Trichlorobenzene
1.3.5- Trimethylbenzene
1.3- Dichlorobenzene
1.3- Dichloropropane
1.3- Dichloropropene
1.4- Dichlorobenzene
1.4- Dioxane (1,4- Diethyleneoxide)
1 -Chloro-1,1 -difluoroethane
1-Chlorohexane
- 5 --,Af'^ji t - jyM"1
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 21 of 70
«EUOREGON
Environmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
EPACODE: C000026
Certificate: 4025-006
Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-PotableWater
EPA 8260B 5222
4665
4410
4411
4500
4535
-v 4860^ 50201
O’. 5045
Ly 4540
4910
4995
4315
4320
4325
4340
4355
4375
4385
4390
4395
4400
4450
4455
4475
4575
4577 '4485
; :
U
2.2- Dichloro-1,1,1 -trifluoroethane (Freon 123)
2.2- Dichloropropane
2-Butanone (Methyl ethylketone. MEK)2-Chloro-1,1,1-trif|.uoroethanie tf?
r v-1, ■; . i;.p~ fl 'r'_- 2-Chjoraethyl yinvhgther ~ ' y ,
'.grChlorotoluene
'l 2-Hexanone (MBK)
• 2-Nitropropane
2-Pentanone
4-Chlorotoluene
4-lsopropyltoluene (p-Cymene)
4-Methyl-2-pentanone (MIBK)
Acetone
Acetonitrile
Acrolein (Propenal)
Acrylonitrile
Allyl chloride (3-Chloropropene)
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chlorodifluoromethane (Freon-22)
- Chloroethane (Ethyl chloride)
1/ ; l, /?,L.L;—I / rVf r /e
ii/yy
r •i'-yt. ■
44861, - . ’ ' 'nChlorqfluoromethane4505'J Chloroform .. — y,
4522- — i . * ,i t , f , ■1 j ( l. i L <Chloropentafluorbethane || I1.’
4525 Chloroprene (2-Chldro-1,3-butadiene)
4526 Chlorotrifluoroethene
4705 cis & trans-1,2-Dichloroethene
4645 cis-1,2-Dichloroethylene
4680 cis-1,3-Dichloropropene
4600 cis-1,4-Dichloro-2-butene
4555 Cyclohexane
4560 Cyclohexanone
4595 Dibromomethane (Methylene bromide)
4625 Dichlorodifluoromethane (Freon-12)
4627 Dichlorofluoromethane (Freon 21)
4725 Diethyl ether
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 22 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-PotableWater
EPA 8260B 9375
4750
4755
4810
4765
4795
4770
Di-isopropylether (DIPE)
Ethanol
Ethyl acetate
Ethyl methacrylate, pp3EthyJbgnzenelO':-' ij p? iff
A7
77't
-1-- \ V ^$Tlpr-4835
4870
4875
4895
4900
5240
4925
4940
4950
4960
4990
5000
4965
4975
5245
5005
-4425Vi4435
V ^yieh#bxide^J ««--- 'H“J-'■‘feVH ^ ^\!iEthyJ^f-fautyIether (ETBE) (2-Ethoxy-2- ’S^rV/Y | 7?
' Sjr 1It! 7
(fs:
Ijriethylpropane)
Fluoromethane (Freon 41)
Hexachlorobutadiene
lodomethane (Methyl iodide)
Isobutyl alcohol (2-Methyl-1-propanol)
Isopropyl alcohol (2-Propanol, Isopropanol)
Isopropylbenzene (Cumene)
m+p-xylene
Methacrylonitrile
Methyl acetate
Methyl bromide (Bromomethane)
Methyl chloride (Chloromethane)
Methyl methacrylate
Methyl tert-butyl ether (MTBE)
Methylcyclohexane
Methylene chloride (Dichloromethane)
m-Xylene
Naphthalene
n-Butyl alcohol (1-Butanol, n-Butanol)
n-Butylbenzene
\sOil
s?
48550. n-Hexane
50965250t-Y
5035
5080
9579
5255
9607
4440
5100
4370
4420
4445
5115
5120
9574
n^P-ropylbenzene
i o-Xylene - f jr _n- | |Pentachloroethane
O fp, fl,/3,\ f i -Propionitrile(Ethyl cySnide)1:'
Propylene oxide
p-Xylene
sec-Butyl Alcohol (2-Butanol)
sec-Butylbenzene
Styrene
T-amylmethylether (TAME)
tert-Butyl alcohol
tert-Butylbenzene
Tetrachloroethylene (Perchloroethylene)
Tetrahydrofuran (THF)
Tetrahydrothiophene
ff*-.X 7
;s
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
23 of 70
ItELtOREGON
Environmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPA CODE: C000026
4955 Yarrow St. Certificate: 4025-006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA8260B 5140 Toluene
Potable 4027 Total BTEX
Water 5205 Total trihalomethanes
4700 trans-1,2-Dichloroethylgne'r, 1’■ i* ;,.. f’:r~ '
4685 tranp=1,3-Dichjoropropylenelj ^ jl s4605 r '.trans;13-Dichloro-2-butene J V----
hVv i1 Trichloroethene (Trichloroethylene)5170
y- Si'75 ,.,oT richlorofluoromethaneV,r (Fluorotrichloromethane, Freon 11)
! -’5225 Vinyl acetate
.f—5235 Vinyl chloride
5237 Vinyl Fluoride
5260 Xylene (total)
EPA 8260B SIM
5180 1,2,3-Trichloropropane
4570 1,2-Dibromo-3-chloropropane (DBCP)
4585 1,2-Dibromoethane (EDB, Ethylene dibromide)
4735 1,4-Dioxane (1,4- Diethyleneoxide)
4325 Acrolein (Propenal)
4340 Acrylonitrile
4375 Benzene
4925 Methacrylonitrile
4420 tert-Butyl alcohol
- - .I 5235 Vinyl chloride
EPA 8270C y 'u' . — •
I, i ’t-,6703 1,1-Biphenyl (BZ-0)
6715 1,2,4,5-Tetrachlorobenzene
5155,1, 1,2,4-Trichlorobenzene4610 1,2-Dichldrobe’nzepe , ■ , —p| V6221 1,2-DipheriyihVd^azine ] || 1 '
6885 1,3,5-Trinitroberizene (1 ;3,5-TNB)
4615 1,3-Dichlorobenzene
6160 1,3-Dinitrobenzene (1,3-DNB)
4679 1,3-phenylenediamine
4620 1,4-Dichlorobenzene
6165 1,4-Dinitrobenzene
4735 1,4-Dioxane (1,4- Diethyleneoxide)
6420 1,4-Naphthoquinone
6630 1,4-Phenylenediamine
5790 1 -Chloronaphthalene
6380 1 -Methylnaphthalene
6425 1-Naphthylamine
!'■ Cs Jf ■'t \:-J , /r; !
' 1 1 l j
wI '1.
10184904 Volatile Organic Compounds by purge and trap GC/MS-SIM
10185805 -Semivolatile Organic compounds by -GC/MS
’tW'/h
Department ol Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 24 of 70
oELd OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPA CODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 8270C 4659 2,2-Oxybis(1 -chloropropane)
Potable 6735 2,3,4,6-Tetrachlorophenol
Water 6835 2,4,5-T richlorophenol
6840 2,4,6-Trichlorophenolf:>^„ s-n,--- ri—i • rpfr
6000 VCAL. {* i
6130 rt2i4-pirnethylph^inol-- ’ ■ - ~ *^3 Xr—'X1
6175 r';2;4jDinitrophenol -«j?2,4-Dinitrotoluene (2,4-DNT)6185
2,6-Dichlorophenol1 <0:61 90 2,6-Dinitrotoluene (2,6-DNT)
V-—-' 5515 2-Acetylaminofluorene
9322 2-Butoxyethanol
5795 2-Chloronaphthalene
5800 2-Chlorophenol
5866 2-Ethoxyethanol (cellosolve)
6360 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2 -methylphenol)
P5145 2-Methylaniline (o-Toluidine)
6385 2-Methylnaphthalene
6400 2-Methylphenol (o-Cresol)
6430 2-Naphthylamine
6460 2-Nitroaniline
6490 2-Nitrophenol
5050 2-Picoline (2-Methylpyridine)
6412 3 & 4 Methylphenol
5945 3,3'-Dichlorobenzidiner>' j—~ •„• // 6J20
'4 .-6355 ,f .^6405^
3,3'-Dimethylbenzidine
3-Methylcholanthrene
' “| 3-Methylphenol (m-Cresol)
6465 J f:'^3-Nitroaniline
6365“1 ;V4,4':Methylenebis(2-chloroaniline)^
4-AminobipKenyf j j | llf'.1^' J"'! J J ,1
4-Bromophenyl phehyl ether! (BDE-3) “5540
5660
5700 4-Chloro-3-methylphenol
5745 4-Chloroaniline
5825 4-Chlorophenyl phenylether
6105 4-Dimethyl aminoazobenzene
6410 4-Methylphenol (p-Cresol)
6470 4-Nitroaniline
6500 4-Nitrophenol\
6510 4-Nitroquinoline 1 -oxide
6570 5-Nitro-o-toluidine
6112 6-Methylchrysene
6115 7,12-Dimethylbenz(a) anthracene
' ! J iE?- -/7|
f '■& ,1* r _\x.
\\U -r t
\ - —'V
- V "■VI
& i?
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 25 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPACODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 8270C 6125 a-a-Dimethylphenethylamine
Potable 5500 Acenaphthene
Water 5505 Acenaphthylene
5510 Acetophenone.—4330 Acrylamide lj r=’ l[{
7005 r'^AIacKlori ’ \
I i V-5. 1 '4357 1'alplja-Methylstyrene
,y>: 5545 ^ciAnlline r -■ y
,/j' . \ . ' I r J' / ‘•y 6555 ^ Anthracene v" __1
/P
■\n c . V-1WH,/=w
,5560 Aramite
7065 Atrazine
5562 Azobenzene
5570 Benzaldehyde
5567 Benzenethiol (Phenylmercaptan)
5595 Benzidine
5575 Benzo(a)anthracene
5580 Benzo(a)pyrene
5605 Benzo(e)pyrene
5590 Benzo(g,h,i)perylene
5600 Benzo(k)fluoranthene
5585 Benzo[b]fluoranthene
5610 Benzoic acid
5630 Benzyl alcohol
5760 bis(2-Chloroethoxy)methane
5765 bis(2-Chloroethyl) ether
5780 bis(2-Chloroisopropyl) ether
5670 Butyl benzyl phthalate
--<*,
03 O Caprolactam
5680 y Carbazole7210,’i
1Carbofuran phenol
7260 - Chlorobenzilate \ r PP
5855• 1 t • ‘ 1 ’ ItChrysene \ i • _ ^ II , i
5862 Cresols, Total
6065 Di(2-ethylhexyl) phthalate (bis(2- Ethylhexyl)phthalate, DEHP)
7405 Diallate
9354 Dibenzfa, h) acridine
5900 Dibenz(a, j) acridine
5895 Dibenz(a.h) anthracene
5890 Dibenzo(a.e) pyrene
5905 Dibenzofuran
6070 Diethyl phthalate
7475 Dimethoate
6135 Dimethyl phthalate
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 26 Of 70
oEUO’SiJo OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
EPACODE: C000026
Certificate: 4025 - 006
Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-PotableWater
EPA 8270C
y0
-----fi!
5925
6200
8620
6205
8625
62607580
6265;
6270
6275
4835
6285
4840
6295
6312
6315
7725
6320
6325
6345
6375
7825
5010
5005
5875
63000 - ■A y5015
('6525^
Di-n-butyl phthalate
Di-n-octyl phthalate
Dinoseb (2-sec-butyl-4,6-dinitrophenol DNBP) _ j—,
Diphenylaminei; j,? I j—-j iff' ' ff y.DisulfoJtqn ^ g Ll ^!,Ethyl methanesulfonate
i^Famphur
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachlorobutadiene
Hexachlorocyclopentadiene
Hexachloroethane
Hexachloropropene
Indene
lndeno(1,2,3-cd) pyrene
Isodrin
Isophorone
Isosafrole
Methapyrilene
Methyl methanesulfonate
Methyl parathion (Parathion, methyl)
n, n-Dimethyl formamide
Naphthalene
n-Decane
n-Hexadecane
Nitrobenzene
y n-Nitrosodiethylamine
"1
00)
.A
cV/?=..■< v-'
6530 5025!
6545
6535
6550
6555
6560
6565
8290
5550
5553
7955
6590
5035
6600
$ n-Nitrosodimethylamine
fi;Nitroso-di-njbutylamine t—-p
n-Nitrosddi-n{pro,plylamihe jn-Nitrosodiphenylamihell'i t
n-Nitrosomethylethalamine
n-Nitrosomorpholine
n-Nitrosopiperidine
n-Nitrosopyrrolidine
o,o,o-Triethyl phosphorothioate
o-Anisidine
Octachlorostyrene
Parathion, ethyl
Pentachlorobenzene
Pentachloroethane
Pentachloronitrobenzene
'',f0A
jj
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 27 of 70
oEUOREGON
Environmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002
ORELAP ID: 4025
C000026
Issue Date: 1/9/2017
EPA CODE:
Certificate: 4025 - 006
Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA8270C 6605 Pentachlorophenol
Perylene
Phenacetin
Phenanthren^-—-
Phe^'-'
PotableWater
6608
6610
6615
6625
7985 r Phofate-Yi .nr..
/?
EPA 8270C SIM
6635 *1 V v
Phthalic acid
^ 6640 ^ iPhthalic anhydride
s---> 9663- ' p-Phenylenediamine
.6650 Pronamide (Kerb)
- 6665 Pyrene
5095 Pyridine
6670 Quinoline
6685 Safrole
8155 Sulfotepp
8235 Thionazin (Zinophos)
8262 Tributyl phosphate
5200 Triethylamine
8310 tris-(2,3-Dibromopropyl) phosphate (tris- BP)
4735 1,4-Dioxane (1,4- Diethyleneoxide)
6380 1 -Methylnaphthalene
6385 2-Methylnaphthalene
5500 Acenaphthene
\ 5505 Acenaphthylene
5555 Anthracene' [ 5575.';. Benzo(a)anthracene
5580 . Benzo(a)pyrene
5605-J Benzo’(e)pyrene y - -
5590 Benzd(g,h,i)perylene ;' )" ' I 1 'f
5600 Benzo(k)fluorantheri!S — ; j >! -
5585 Benzo[b]fluoranthene
5670 Butyl benzyl phthalate
5855 Chrysene
6065 Di(2-ethylhexyl) phthalate (bis(2- Ethylhexyl)phthalate, DEHP)
5895 Dibenz(a.h) anthracene
5905 Dibenzofuran
6070 Diethyl phthalate
6135 Dimethyl phthalate
5925 Di-n-butyl phthalate
6200 Di-n-octyl phthalate
'// f 7
'{fr,
/ je'S
%./ _..'V
10242407 Semivolatile Organic GC/MS Selective Ion
compounds by Monitoring
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 28 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
Test America Denver EPACODE: C000026
4955 Yarrow St. Certificate: 4025-006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-Potable
EPA 8270CSIM
6265
6270
Fluoranthene
Fluorene
Water 6315 lndeno(1,2,3-cd) pyrene
5005 Naphthalene, f
6525 n-Nitrosodiethylamine
6530 : n-Nitrosodimethylamine—‘
6545 n-Nitrosodi-n-propylamine
6535 n-Nitrosodiphenylamine
6615 Phenanthrene
6665 Pyrene
EPA 8270D.
6703 1,1'-Biphenyl (BZ-0)
6715 1,2,4,5-Tetrachlorobenzene
5155 1,2,4-T richlorobenzene
4610 1,2-Dichlorobenzene
6221 1,2-DiphenylhydrazineP
6885 1,3,5-Trinitrobenzene (1,3,5-TNB)
4615 1,3-Dichlorobenzene
6160 1,3-Dinitrobenzene (1,3-DNB)
4620 1,4-Dichlorobenzene
6165 1,4-Dinitrobenzene
4735 1,4-Dioxane (1,4- Diethyleneoxide)
6420 1,4-Naphthoquinone
6630 1,4-Phenylenediamine
5790 1 -Chloronaphthalene
6380 1 -Methylnaphthalene
6425 1-Naphthylamine
4659 2,2-Oxybis(1 -chloropropane)
6735 2,3,4,6-Tetrachlorophenol
6835 2,4,5-Trichlorophenol
6840 2,4,6-Trichlorophenol ' s
6000 2,4-Dichlorophenol
6130 2,4-Dimethylphenol
6175 2,4-Dinitrophenol
6185 2,4-Dinitrotoluene (2,4-DNT)
6005 2,6-Dichlorophenol
6190 2,6-Dinitrotoluene (2,6-DNT)
5515 2-Acetylaminofluorene
5795 2-Chloronaphthalene| 5800 2-Chlorophenol
6360 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2 -methylphenol)
5145 2-Methylaniline (o-Toluidine)
10186002 Semivolatile Organic compounds by GC/MS
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 29 of 70
oELtOW4 OREGON
Environmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
As of 1/9/2017 this list supercedes all previous lists for this certNon- EPA 82700 6385 2-Methylnaphthalene
Potable 6400 2-Methylphenol (o-Cresol)
Water 6430 2-Naphthylamine
6460 2-Nitroaniline,
6490 2-Nitrophenol
5050 2-Picoline (2-Methylpyridine)
6412 3 & 4 Methylphenol
5945 3,3'-Dichlorobenzidine
6120 3,3'-Dimethylbenzidine
6355 3-Methylcholanthrene
6405 3-Methylphenol (m-Cresol)
6465 3-Nitroaniline
6365 4,4-Methylenebis(2-chloroaniline)
5540 4-Aminobiphenyl
5660 4-Bromophenyl phenyl ether (BDE-3)
5700 4-Chloro-3-methylphenol
5745 4-Chloroaniline
5825 4-Chlorophenyl phenylether
6105 4-Dimethyl aminoazobenzene
6410 4-Methylphenol (p-Cresol)
6470 4-Nitroaniline
6500 4-Nitrophenol
6510 4-Nitroquinoline 1-oxide
6570 5-Nitro-o-toluidine
6115 7,12-Dimethylbenz(a) anthracene
6125 a-a-Dimethylphenethylamine
5500 Acenaphthene
5505 Acenaphthylene
5510 Acetophenone
5545 Aniline
5555 Anthracene
5560 Aramite
5562 Azobenzene
5570 Benzaldehyde
5595 Benzidine
5575 Benzo(a)anthracene
5580 Benzo(a)pyrene
5590 Benzo(g,h,i)perylene
5600 Benzo(k)fluoranthene
5585 Benzo[b]fluoranthene
5610 Benzoic acid
5630 Benzyl alcohol
5760 bis(2-Chloroethoxy)methane
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025-006
Expiration Date: 1/8/2018
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 30 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPACODE: C000026
4955 Yarrow St. Certificate: 4025-006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 8270D 5765 bis(2-Chloroethyl) ether
Potable 5780 bis(2-Chloroisopropyl) ether
Water 5670 Butyl benzyl phthalate
7180 Caprolactam, ,
5680 Carbazole
7260 Chlorobenzilate - ■
5855 Chrysene
8906 Coelution - 3-Chlorophenol + 4- Chlorophenol
5862 Cresols, Total
6065 Di(2-ethylhexyl) phthalate (bis(2- Ethylhexyl)phthalate, DEHP)
7405 Diallate
5900 Dibenz(a, j) acridine
5895 Dibenz(a,h) anthracene
5905 Dibenzofuran
6070 Diethyl phthalate
• 7475 Dimethoate
6135 Dimethyl phthalate
5925 Di-n-butyl phthalate
6200 Di-n-octyl phthalate
8620 Dinoseb (2-sec-butyl-4,6-dinitrophenol DNBP)
6205 Diphenylamine
8625 Disulfoton
6260 Ethyl methanesulfonate
7580 Famphur
6265 Fluoranthene
6270' Fluorene
6275 Hexachlorobenzene
4835 Hexachlorobutadiene
6285 Hexachlorocyclopentadiene
4840 Hexachloroethane
6295 Hexachloropropene
6315 lndeno(1,2,3-cd) pyrene
7725 Isodrin
6320 Isophorone
6325 Isosafrole
6345 Methapyrilene
6375 Methyl methanesulfonate
•7825 Methyl parathion (Parathion, methyl)
5005 Naphthalene
5015 Nitrobenzene
6525 n-Nitrosodiethylamine
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
31 Of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields ofAccreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
As of 1/9/2017 this list supercedes all previous lists for this ceNon- epa 82700 6530 n-Nitrosodimethylamine
Potable 5025 n-Nitroso-di-n-butylamine
Water 6545 n-Nitrosodi-n-propylamine
6535 n-Nitrosodiphenylamine
6550 n-Nitrosomethylethalamine
6555 n-Nitrosomorpholine
6560 n-Nitrosopiperidine
6565 n-Nitrosopyrrolidine
8290 0,0,0-Triethyl phosphorothioate
7955 Parathion, ethyl
6590 Pentachlorobenzene
5035 Pentachloroethane
6600 Pentachloronitrobenzene
6605 Pentachlorophenol
6610 Phenacetin
6615 Phenanthrene
6625 Phenol
7985 Phorate
9663 p-Phenylenediamine
6650 Pronamide (Kerb)
6665 Pyrene
5095 Pyridine
6685 Safrole
8155 Sulfotepp
8235 Thionazin (Zinophos)
EPA 8270DSIM
4735 1,4-Dioxane (1,4- Diethyleneoxide)
6380 1 -Methylnaphthalene
6385 2-Methylnaphthalene
5500 Acenaphthene
5505 Acenaphthylene
5555 Anthracene
5575 Benzo(a)anthracene
5580 Benzo(a)pyrene
5590 Benzo(g,h,i)perylene
5600 Benzo(k)fluoranthene
5585 Benzo[b]fluoranthene
5670 Butyl benzyl phthalate
5855 Chrysene
6065 Di(2-ethylhexyl) phthalate (bis(2- Ethylhexyl)phthalate, DEHP)
5895 Dibenz(a,h) anthracene
5905 Dibenzofuran
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Expiration Date: 1/8/2018
10242509 Semivolatile Organic compounds by GC/MS Selective Ion Monitoring
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 32 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 8270D 6070 Diethyl phthalate
SIMPotableWater
Dimethyl phthalate
Di-n-butyl phthalate
Di-n-octyl phttjalate Fluoranthene IQ.;
6135
5925
6200
6265 . . ..6270 rfiFJuoferie'1 Ui
6315
5005 ,jy ,,V . -v6530-'
I ./L>. S t-]. !lndeno(-l ,2,3-cd) pyreneh r
^Naphthalene
n-Nitrosodimethylamine
EPA 8310
."-.6535 n-Nitrosodiphenylamine
L 6615 Phenanthrene
6665 Pyrene
6380 1 -Methylnaphthalene
6385 2-Methylnaphthalene
5500 Acenaphthene
5505 Acenaphthylene
5555 Anthracene
5575 Benzo(a)anthracene
5580 Benzo(a)pyrene
5590 Benzo(g,h,i)perylene
5600 Benzo(k)fluoranthene
5585 Benzo[b]fluoranthene
5855 Chrysene
5895 Dibenz(a,h) anthracene
! “ 6265 Fluoranthene
, *46270''ff1 6315*
r~_
s Fluorene■J,-Q~Hndeno(1 ,2,3-cd) pyrene
10187607 Polynuclear Aromatic Hydrocarbons by HPLC/UVrVIS
6615
6665
NaphthaleneiPheninthfanei!:
Pyrene-
%
%.
:v)i .jL“L -fZ
EPA 8321A "" M 7 Li ’!4 " '
6885 1,3,5-Trinitrobenzene (1,3,5-TNB)
6160 1,3-Dinitrobenzene (1,3-DNB)
6014 2,3-Dinitrotoluene
8655 2,4,5-T
9651 2,4,6-Trinitrotoluene (2,4,6-TNT)
8545 2,4-D
8560 2,4-DB
6185 2,4-Dinitrotoluene (2,4-DNT)
6190 2,6-Dinitrotoluene (2,6-DNT)
9303 2-Amino-4,6-dinitrotoluene (2-am-dnt)
10189001 Solvent Extractable non-volatile compounds by HPLC/TS/MS
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 33 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St. I
Arvada, CO 80002 Issue Date: 1/9/2017 E
As of 1/9/2017 this list supercedes all previous lists for this certiNon- EPA 8321A 9507 2-Nitrotoluene
Potable 9510 3-Nitrotoluene
Water 9306 4-Amino-2,6-dinitrotoluene (4-am-dnt)
9513 4-Nitrotoluene
7010 Aldicarb (Temjk)
7040 Aminocarb
7195 Carbaryl (Sevin)
7205 Carbofuran (Furaden)
7275 Chloropropham
8555 Dalapon
8595 Dicamba
8605 Dichloroprop (Dichlorprop)
8620 Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)
7505 Diuron
7610 Fenuron
7630 Fluometuron
7765 Linuron (Lorox)
7775 MCPA
7780 MCPP
7800 Methiocarb (Mesurol)
7805 Methomyl (Lannate)
6415 Methyl-2,4,6-trinitrophenylnitramine (tetryl)
7855 Mexacarbate
7885 Monuron
7915 Neburon
5015 Nitrobenzene
6485 Nitroglycerin
9522 Octahydro-1,3,5,7-tetranitro-1,3,5,7- tetrazocine (HMX)
6605 Pentachlorophenol
9558 Pentaerythritoltetranitrate (PETN)
8075 Propham
8080 Propoxur (Baygon)
9432 RDX (hexahydro-1,3,5-trinitro-1,3,5- triazine)
8120 Siduron
8650 Silvex (2,4,5-TP)
EPA 8321B
6885 1,3,5-Trinitrobenzene (1,3,5-TNB)
6160 1,3-Dinitrobenzene (1,3-DNB)
6014 2,3-Dinitrotoluene
8655 2,4,5-T
ORELAP ID: 4025
EPACODE: C000026
tificate: 4025 - 006
10189205 Solvent Extractable non-volatile compounds by HPLC/TS/MS
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 34 of 70
c8S5* OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Expiration Date: 1/8/2018Issue Date: 1/9/2017
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 8321B 9651 2,4,6-Trinitrotoluene (2,4,6-TNT)
Potable 8545 2,4-D
Water 8560 2,4-DB
6185 2,4-Dinitrotoluene (2,4-DNT) "
6190 2,6-Dinitrotoluene (2,6-DNT)
9303 2-Amino-4,6-dinitrotoluene (2-am-dnt)
9507 2-Nitrotoluene
9510 3-Nitrotoluene
9306 4-Amino-2,6-dinitrotoluene (4-am-dnt)
9513 4-Nitrotoluene
7010 Aldicarb (Temik)
7040 Aminocarb
7195 Carbaryl (Sevin)
7205 Carbofuran (Furaden)
7275 Chloropropham
8555 Dalapon( 8595 Dicamba
8605 Dichloroprop (Dichlorprop)
8620 Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)
7505 Diuron
7610 Fenuron
7630 Fluometuron
7765 Linuron (Lorox)
7775 MCPA
7780 MCPP
7800 Methiocarb (Mesurol)
7805 Methomyl (Lannate)
6415 Methyl-2,4,6-trinitrophenylnitramine (tetryl)
7855 Mexacarbate ,
7885 Monuron ’
7915 Neburon
5015 Nitrobenzene
6485 Nitroglycerin
9522 Octahydro-1,3,5,7-tetranitro-1,3,5,7- tetrazocine (HMX)
6605 Pentachlorophenol
9558 Pentaerythritoltetranitrate (PETN)
8075 Propham
| 8080 Propoxur (Baygon)¥ 9432 RDX (hexahydro-1,3,5-trinitro-1,3,5-
triazine)
8120 Siduron
8650 Silvex (2,4,5-TP)
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 35 of 70
«EL«OREGON
Environmental Laboratory Accreditation Program
6160 1,3-Dinitroberizene (1,,3-DNB)
9651 2,4,6-Trinitrotoluene (2,4,6-TNT)
5882 2,4-diamino-6-nitrotoluene
6185 2,4-Dinitrotoluene (2,4-DNT)
6181 2,6-diamino-4-nitrotoluene
6190 2,6-Dinitrotoiuene (2,6-DNT)
9303 2-Amino-4,6-dinitrotoluene (2-am-dnt)
9507 2-Nitrotoluene
9510 3-Nitrotoluene
9306 4-Amino-2,6-dinitrotoluene (4-am-dnt)
9513 4-Nitrotoluene
7046 Ammonium Picrate
6415 Methyl-2,4,6-trinitrophenylnitramine(tetryl)
5015 Nitrobenzene
6485 Nitroglycerin
9522 Octahydro-1,3,5,7-tetranitro-1,3,5,7- tetrazocine (HMX)
9558 Pentaerythritoltetranitrate (PETN)
1899 Picric Acid (2,4,6-Trinitrophenol)
9432 RDX (hexahydro-1,3,5-trinitro-1,3,5- triazine)
6885 1,3,5-Trinitrobenzene (1,3,5-TNB)
6160 1,3-Dinitrobenzene (1,3-DNB)
9651 2,4,6-Trinitrotoluene (2,4,6-TNT)
5882 2,4-diamino-6-nitrotoluene
6185 2,4-Dinitrotoluene (2,4-DNT)
6181 2,6-diamino-4-nitrotoluene
6190 2,6-Dinitrotoluene (2,6-DNT)
9303 2-Amino-4,6-dinitrotoluene (2-am-dnt)
9507 2-Nitrotoluene
6150 3,5-Dinitroaniline
9510 3-Nitrotoluene
9306 4-Amino-2,6-dinitrotoluene (4-am-dnt)
9513 4-Nitrotoluene
7046 Ammonium Picrate
6415 Methyl-2,4,6-trinitrophenylnitramine(tetryl)
5015 Nitrobenzene
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
EPACODE: C000026
Certificate: 4025 - 006
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-PotableWater
EPA 8330A 10190008 Nitroaromatics and Nitramines by HighPerformance Liquid Chromatography (HPLC)
6885 1,3,5-Trinitrobenzene (1,3,5-TNB)
EPA 8330B 10308006 Nitroaromatics, Nitramines and NitrateEsters by High Performance Liquid Chromatography (HPLC)
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 36 Of 70
ow-o OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non- EPA 8330B 6485 Nitroglycerin
Potable 9522 Octahydro-1,3,5,7-tetranitro-1,3,5,7- tetrazocine (HMX)
Water9558 Pentaerythritoltetranitrate (PETN)
1899 Picric Acid (2,4,6-Trinitrophenol)
9432 RDX (hexahydro-1,3,5-tr!nitro-1,3,5- triazine)
i
• ' i
EPA 9012A 10193405 Total and Amenable Cyanide (automated colorimetric with off-line
■ distillation)
1510 Amenable cyanide ' '
_1645 Total cyanide
EPA 9012B
1510 Amenable cyanide
10243206 Total and Amenable Cyanide (automated colorimetric with off-line distillation)
1645 Total cyanide
EPA 9020B 10194408 Total Organic Halides
• 2045 Total organic halides (TOX)
EPA 9030B
2005 Sulfide
10195605 Acid-Soluble and Acid-Insoluble sulfides: Distillation
EPA 9034
2005 Sulfide
10196006 Titrimetric Procedure for Acid-Soluble and Acid-Insoluble Sulfides
EPA 9040B
1900 pH
10197203 pH Electrometric Measurement
EPA 9040C
,1900 pH
10244403 pH Electrometric Measurement
EPA 9050A
1610 Conductivity
10198808 Specific Conductance
EPA 9056
1540 Bromide
10199005 Determination of Inorganic Anions byIon Chromatography
1575 Chloride
1730 Fluoride
1805 Nitrate
1835 Nitrite
1870 Orthophosphate as P
2000 Sulfate
_1825 Total nitrate+nitrite
• EPA 9056A
1540 Bromide
10199607 Determination of Inorganic Anions byIon Chromatography
1575 Chloride
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 37 of 70
«ELdOREGON
Environmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver
4955 Yarrow St. Certificate: 4025-006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.EPA 9056A 1730 Fluoride
Potable 1805 Nitrate
Water 1820 Nitrate-nitrite
1835 Nitrite
1870 Orthophosphate as P
2000 Sulfate
EPA 9060
1710 Dissolved organic carbon (DOC)
10200201 Total Organic Carbon
2040 Total organic carbon
EPA 9060A
1710 Dissolved organic carbon (DOC)
10244801 Total Organic Carbon
2040 Total organic carbon
EPA 9066
1905 Total phenolics
10200609 Phenolics (Colorimetric, Automated 4- AAP with Distillation)
EPA RSK-175 10212905 Methane, Ethane, and Ethene in water(GC-FID)
4323 Acetylene
by Headspace GC/FID
4747 Ethane
4752 Ethene
4877 Isobutylene
4926 Methane
5007 n-Butane
5028 n-Pentane
5029 n-Propane
FLDEP SOP 90015820 Calculation of Un-ionized Ammonia in02/12/01
2058 Un-ionized Ammonia
Fresh Water
NWTPH-Dx
9369 Diesel range organics (DRO)
90018409 Oregon DEQ TPH Diesel Range
9499 Motor Oil
9506 Residual Range Organics (RRO)
2050 Total Petroleum Hydrocarbons (TPH)
NWTPH-Gx
9408 Gasoline range organics (GRO)
90018603 Oregon DEQ TPH Gasoline RangeOrganics by GC/FID-PID Purge & Trap
SM 2120 B- 2001 online
1605 Color
20039309 Color by Visual Comparison
SM 2120 B- 20039310 Color2011
1605 Color •SM 2310 B-97 online
1500 Acidity, as CaC03
20044604 Acidity by Titration Method
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 38 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-Potable
SM 2320 B- 2011
1505 Alkalinity as CaC03
20045618 Alkalinity as CaC03
Water SM 2320 B-97 online
1505i ,
Alkalinity as CaC03 ,
20045607 Alkalinity by Titration Method
SM 2340 B- 2011
1750
• _ ■ * • *
Hardness
20046611 Hardness
SM 2340 B-97 online
1550 Calcium hardness as CaC03
20046600 Hardness by calculation
- 1750 Hardness
1755 Total hardness as CaC03
SM 2340 C-97 online
1755 Total hardness as CaC03
20047603 Hardness by EDTA Titration Method
SM 2510 B-97 online
1610 Conductivity
20048606 Conductivity by Probe
§ SM 2540 B-97 online
1950 Residue-total
20049405 Total Solids Dried at 103 - 105C
SM 2540 C- 2011
1955 Residue-filterable (TDS)
20050413 Residue-filterable (TDS)
SM 2540 C-97 online
1955 Residue-filterable (TDS)
20050402 Total Dissolved Solids Dried at 180C
SM 2540 D-97 online
1960 Residue-nonfilterable (TSS)
20051201 Total Suspended Solids Dried at 103 - 105C’
SM 2540 F-97 online
1965 Residue-settleable
20052204 Settleable Solids
SM 3500-Cr B- 2009 online
1045 Chromium VI
20066255 Chromium by Colorimetric Method
SM 3500-Cr D 19th ED
1045 Chromium VI
20067009 Chromium by Colorimetric Method
SM 3500-Fe B 20th ED
1070 Iron
20068604 Iron by Colorimetric Method
SM 3500-Fe B- 97 online
1070 Iron
20069005 Iron by Phenanthroline Method
£
SM 3500-Fe D 19th ED
1070 Iron
20069209 Iron by Phenanthroline Method
SM 4500-CN E- 20096417 Cyanide by Colorimetric Method1999
1645 Total cyanide
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 39 of 70
OW4 OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPA CODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Non-Potable
SM 4500-CN E- 2011 2011
1645 Total cyanide
20096428 Cyanide by Colormetric Method
Water SM 4500-CN G- 1999 online
1510 Amenable cyanide
20097216 Cyanide Amenable to Chlorination after Distillation
SM 4500-CN' C-97 online
20095607 Cyanide by Total Cyanide afterDistillation
1645 Total cyanide
SM 4500-CN' I- 97 online
2074 Weak Acid Dissociable Cyanide
20098004 Cyanide by Weak Acid Dissociable Cyanide
SM 4500-H+ B- 2000 online
1900 pH
20105219 pH Value by Electrometric Method .
SM 4500-H+ B- 2011
1900 pH
20105220 pH - Electrometric Measurement
SM 4500-N02" B-2000 online
1835 Nitrite
20113104 Nitrite by Colorimetric Determination
1840 Nitrite as N
SM 4500-S2 D- 2000
2005 Sulfide
20125853 Sulfide by Methylene Blue Method
SM 4500-S2' F-2000 online
2005 Sulfide
20126652 Sulfide by lodometric Method
SM 4500-S03' B-2000 online
2015 Sulfite-S03
20130625 Sulfite by lodometric Method
SM 5210 B- 2001 online
1530 Biochemical oxygen demand
20135255 Biochemical Oxygen Demand (BOD), 5- Day
1555 Carbonaceous BOD, CBOD
SM 5210 B- 2011
1530 Biochemical oxygen demand
20135266 Biochemical Oxygen Demand (5 days @ 20 C).
SM 5310 B- 2000
1710 Dissolved organic carbon (DOC)
20137819 Total Organic Carbon (TOC) by Combustion Infra-red Method
2040 Total organic carbon
SM 5310 B- 2011 2011
1710 Dissolved organic carbon (DOC)
20137820 TOC by High-Temperature Combustion Method
Solids
ASTM D2216- 10 10
8641 Percent Moisture
30025106 Standard Test Methods for Laboratory Determination of Water (Moisture)Content of Soil and Rock by Mass
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 40 Of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of AAccreditation ORELAP ID: 4025
TestAmerica Denver EPA CODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
CA HML 939-M
1208 Organic Lead
90016765 Determination of Organic Lead Compounds by Graphite Furnace Absorption Spectrometry
DV-LC-0012
7044 • Ammonium Perfluorooctanoate (APFO)
60036035 TestAmerica Denver - PFOA in NPW and SCM by HPLC-MS-MS
6911 Perfluorobutane Sulfonate (PFBS)
6915 Perfluorobutyric acid (PFBA)
9562 Perfluorodecane Sulfonate (PFDS)
6905 Perfluorodecanoic acid (PFDA)
6903 Perfluorododecanoic (PFDDA)
6908 Perfluoroheptanoic acid (PFHA) -
6910 Perfluorohexane Sulfonate (PFHS)
6913 Perfluorohexanoic acid (PFHXA)
6906 Perfluorononanoic acid (PFNA)
6917 Perfluorooctane Sulfonamide (PFOSA)
6912 Perfluorooctanoic acid
6909 Perfluorooctanoic Sulfonate (PFOS)
6914 Perfluoropentanoic acid (PFPEA)
6902 Perfluorotetradecanoic acid (PFTDA)
9563 Perfluorotridecanoic (PFTRIA)
6904 Perfluoroundecanoic acid (PFUDA)
DV-LC-0020 3
6119 Disodium Inimodiacetate
60036013 TestAmerica Denver - Disodium Iminodiacetate (IDA) by LC/MS/MS (modified EPA 8321 A)
DV-WC-0077
9378 1,1-Dimethyl hydrazine
60036046 TestAmerica Denver - Determination of Hydrazine, Monomethyl Hydrazine, and Unsymmetrical Dimethylhydrazine by IC
9486 Hydrazine
9495 Methyl hydrazine (MMH)
EPA 1010
1780 Ignitability
10116606 Pensky-Martens Closed-Cup Method for Determining Ignitability
EPA 1010A
1780 Ignitability
10234807 Pensky-Martens Closed-Cup Method for Determining Ignitability
EPA 1311
9822 Extraction/Preparation
10118806 Toxicity Characteristic Leaching Procedure
EPA 1312
9822 Extraction/Preparation
10119003 Synthetic Precipitation Leaching Procedure
Solids
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 41 Of 70
oEUOWO OREGON
Environmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002
EPACODE: C000026
Certificate: 4025 - 006
Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 160.4
1970 Residue-volatile
10010409 Total Volatile Solids, ignition @ 550 C.
EPA 3050B
9822-Extradion/Preparation (— !
10135601
ff
Acid Digestion of Sediments, Sludges, and soils
EPA 335.4
//'V\
■-1645-
L i x \ i
..J”" "
Total cyanide
V'-Lt;1 110061208'v._J i/r>\'■oh
L
Methods for the Determination of j-, Inorganic Substances in Environmental '/ ^Samples
EPA 350.1 , v \
1515 Ammonia as N
10063204' Jc \Ammbnia Nitrogen - Colorimetric, AutoVPhenate,
v/t-i S
EPA 350.1 2 10063602 Ammonia Nitrogen - Colorimetric, Auto Phenate j i
1515 Ammonia as N —
EPA 351.2
1790 Kjeldahl nitrogen
10065006 Total Kjeldahl Nitrogen - Block Digest, Phenate
M
EPA 353.2 2
1820 Nitrate-nitrite
10067604 Nitrate/Nitrite Nitrogen - Automated, ^
Cadmium
1825 Total nitrate+nitrite
EPA 3540C
9822 Extraction/Preparation
10140202 Soxhlet Extraction
EPA 3546
8031 Extraction/Preparation
10141205 Microwave Extraction
EPA 3550C . • .Kt‘ /' . -
10142004 ^Ultrasonic Extraction
I r8031 Extraction/Preparation
EPA 3580A ‘ l I , 10143007 ‘ Waste Dilution
8031 '1, Extraction/Preparation i -i ■ ■
EPA 3620B "ji 1 ,,^0145809 Florisil Cleanup
8031■ — -■ / I ' -1! i '
Extradion/Preparation •_ ■Ij ‘'7.7
EPA 3660B
8031 Extraction/Preparation
10148400 Sulfur cleanup
EPA 3665A
9822 Extraction/Preparation
10148808 Sulfuric Acid / permanganate Cleanup
EPA 5035 10154004 Closed-System Purge-and-Trap and Extraction for Volatile Organics in Soil and Waste Samples
9822 Extraction/Preparation M
EPA 5035A
8031 Extraction/Preparation
10284807 Closed-System Purge-and-Trap and ^ Extraction for Volatile Organics in Soil and Waste Samples
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 42 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPACODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number. _______SolidS EPA 6010B 10155609 ICP - AES
1000 Aluminum
1005 Antimony
1010 Arsenic ' -
1015 Barium
1020 Beryllium
1025 Boron ’
1030 Cadmium
1035 Calcium
1040 Chromium
1050 Cobalt
1055 Copper
1070 Iron
1075 Lead
1080 Lithium
1085 Magnesium
1090 Manganese
1100 Molybdenum
1105 Nickel
1910 Phosphorus, total
1125 Potassium
1140 Selenium
1990 Silica as Si02
1145 Silicon
1150 Silver
1155 Sodium
1160 Strontium
2017- Sulfur
1165 Thallium
1175 Tin ,
1180 Titanium
1185 Vanadium
1190 Zinc
EPA 6010C 10155803 ICP - AES
1000 Aluminum
1005 Antimony
1010 Arsenic
1015 Barium
1020 Beryllium
1025 Boron
1030 Cadmium
1035 Calcium
1040 Chromium
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 43 of 70
«EL«OREGON
Environmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002
EPACODE: C000026
Certificate: 4025-006
Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 6010C 1050 Cobalt
EPA 6010D
1105 " Nickel
.1910 Phosphorus, total
1125 Potassium
1140 Selenium
1990 Silica as Si02
1145 Silicon
1150 Silver
1155 Sodium
1160 Strontium
2017 Sulfur
1165 Thallium
1175 Tin
1180 Titanium
1185 Vanadium
1190 Zinc
1000 Aluminum
.1005 Antimony
r.1010 Arsenic
1015 Bariumf02*)* Beryllium
1025 -J Boron,Cadmium t .i111 |1030
1035 Calcium u ! i
1040 Chromium
1050 Cobalt
1055 Copper
1070 Iron
1075 Lead
1080 Lithium
1085 Magnesium
1090 Manganese
1100 Molybdenum
1105 Nickel
1910 Phosphorus, total
10155916 Metals by ICP - AES
7-;--
;k1: r ir. i >
I Si, ~;-r'
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 44 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPACODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number. Solids EPA 6010D
EPA 6020
EPA 6020A
1125 Potassium
1140 Selenium
1990 Silica as Si02
1145 Silicon
1150 Silver
1155 Sodium
1160 Strontium
2017 Sulfur
1165 Thallium
1175 Tin
1180 Titanium
1185 Vanadium
1190 Zinc
1005 Antimony
1010 Arsenic
1015 Barium
1020 Beryllium
1030 Cadmium
1040 Chromium
1050 Cobalt
1055 Copper
1075 Lead
1090 Manganese
1100 Molybdenum
1105 Nickel
1140 , Selenium
1150 Silver
1165 Thallium
1170 Thorium
1175 Tin
3035 Uranium
1185 Vanadium
1190 Zinc
1005 Antimony
1010 Arsenic
1015 Barium
1020 Beryllium
1030 Cadmium
1040 Chromium
1050 Cobalt
10156000
10156408
Inductively Coupled Plasma-Mass Spectrometry
Inductively Coupled Plasma-Mass Spectrometry
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
45 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPACODE: C000026
4955 Yarrow St. Certificate: 4025-006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this listSoMdS ERA 6020A
EPA 6020B 2014
supercedes all previous lists for this certificate number.1055 Copper
1075 Lead
1090 Manganese
1100 Molybdenum
1105 Nickel
1140 Selenium - -
1150 Silver •
1165 Thallium
1170 Thorium
1175 Tin
3035 Uranium
1185 Vanadium
1190 Zinc
10156420
1005 Antimony
1010 Arsenic
1015 Barium
1020 Beryllium
1030 Cadmium
1040 Chromium
1050 Cobalt
1055 Copper
1075 Lead
1090 Manganese
1100 Molybdenum
1105 Nickel
1140 Selenium
1150 Silver
1165 Thallium
1170 Thorium
1175 Tin
3035 Uranium
1185 Vanadium
1190 Zinc
Inductively Coupled Plasma-Mass Spectrometry
EPA 6860
1895 Perchlorate
10304800 Perchlorate in Water, Soils and Solid Wastes Using Ion Chromatography/Electrospray lonization/Mass Spectrometry
EPA 7471A
1095 Mercury
IUIDOCUO mercury in ounu was it? uyAtomic Absorption
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 46 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002
EPACODE: C000026
Certificate: 4025-006
Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 7471B
1095 Mercury
10166402 Mercury by Cold Vapor AtomicAbsorption
EPA 8011;•
10173009 1,2-Dibromoethane and 1,2-Dibromo-3- chloropropane by Microextraction and GC/ECD
5180 1,2,3-Trichloropropane - ■
4585 1,2-Dibromoethane (EDB, Ethylene dibromide)
4580 Dibromochloropropane
EPA 8015B
9369 Diesel range organics (DRO)
10173601 Non-halogenated organics usingGC/FID
4750 Ethanol
9408 Gasoline range organics (GRO)
4875 Isobutyl alcohol (2-Methyl-1-propanol)
4895 Isopropyl alcohol (2-Propanol, Isopropanol)
9488 Jet Fuel
4930 Methanol
9499 Motor Oil
4425 n-Butyl alcohol (1-Butanol, n-Butanol)
5055 n-Propanol
EPA 8015C
9369 Diesel range organics (DRO)
10173805 Non-halogenated organics usingGC/FID
4720 Diethylene glycol (2,2-Oxybisethanol)
4750 Ethanol
4785 Ethylene glycol
9408 Gasoline range organics (GRO)
4875 Isobutyl alcohol (2-Methyl-1-propanol)
4895 Isopropyl alcohol (2-Propanol, Isopropanol)
9488 Jet Fuel
4930 Methanol
9499 Motor Oil
4425 n-Butyl alcohol (1-Butanol, n-Butanol)
5055 n-Propanol
6657 Propylene Glycol
9646 Triethylene Glycol
EPA 8015D
9369 Diesel range organics (DRO)
10305609 Nonhalogenated Organics UsingGC/FID
4750 Ethanol
9408 Gasoline range organics (GRO)
4875 Isobutyl alcohol (2-Methyl-1-propanol)
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
47 Of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPACODE: C000026
4955 Yarrow St. Certificate: 4025-006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this listSolidS EPA8015D
EPA 8021B
EPA 8081A
supercedes all previous lists for this certificate number.4895 Isopropyl alcohol (2-Propanol,
Isopropanol)
9488 Jet Fuel
4930 Methanol
9499 Motor Oil
4425 n-Butyl alcohol (1-Butanol, n-Butanol)
5055 n-Propanol
10174808
4610 1,2-Dichlorobenzene
4615 1,3-Dichlorobenzene
4620 1,4-Dichlorobenzene
4375 Benzene
4475 Chlorobenzene
4765 Ethylbenzene
5240 m+p-xylene
5000 Methyl tert-butyl ether (MTBE)
5005 Naphthalene
5250 o-Xylene
5140 Toluene
5260 Xylene (total)
10178606
8580 2,4'-DDD
8585 2,4'-DDE
8590 2,4'-DDT
7355 4,4-DDD
7360 4,4'-DDE
7365 4,4'-DDT
7025 Aldrin
7110 alpha-BHC (alpha-Hexachlorocyclohexane)
7240 alpha-Chlordane
7115 beta-BHC (beta-Hexachlorocyclohexane)
7250 Chlordane (tech.)
7260 Chlorobenzilate
7105 delta-BHC
7405 Diallate
7470 Dieldrin
7510 Endosulfan I
7515 Endosulfan II
7520 Endosulfan sulfate
7540 Endrin
7530 Endrin aldehyde
Aromatic and Halogenated Volatiles by GC with PID and/or ECD Purge & Trap
Organochlorine Pesticides by GC/ECD
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 48 Of 70
o*“2U OREGONEnvironmental Laboratory Accreditation Program
ORELAPID: 4025ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
EPACODE: C000026
Certificate: 4025 - 006
Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8081A 7535 Endrin ketone
7120 gamma-BHC (Lindane, gamma- HexachlorocyclohexanE)
7245 gamma-Chlordane ,
7685 Heptachlor
7690 Heptachlor epoxide^
6275 Hexachlorobenzene
6280 Hexachlorocyclohexanes
7725 Isodrin
7740 Kepone
7810 Methoxychlor
7870 Mirex
8250 Toxaphene (Chlorinated camphene)
8310 tris-(2,3-Dibromopropyl) phosphate (tris-BP)
EPA 8081B 10178800 Organochlorine Pesticides by GC/ECD
8580 2,4'-DDD
8585 2,4'-DDE
8590 2,4'-DDT
7355 4,4-DDD
7360 4,4'-DDE
7365 4,4-DDT
7025 Aldrin
7110 alpha-BHC (alpha- Hexachlorocyclohexane)
7240 alpha-Chlordane
7115 beta-BHC (beta- Hexachlorocyclohexane)
7250 Chlordane (tech.)
7260 Chlorobenzilate
7105 delta-BHC
7405 Diallate
7470 Dieldrin
7510 Endosulfan I
7515 Endosulfan II
7520 Endosulfan sulfate
7540 Endrin
7530 Endrin aldehyde
7535 Endrin ketone
7120 gamma-BHC (Lindane, gamma- HexachlorocyclohexanE)
7245 gamma-Chlordane
7685 Heptachlor
7690 Heptachlor epoxide
6275 Hexachlorobenzene
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 49 of 70
nELt OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8081B
EPA 8082
6280 Hexachlorocyclohexanes
7725 Isodrin
7740 Kepone
7810 Methoxychlor
7870 Mirex
8250 Toxaphene (Chlorinated camphene)
8310 tris-(2,3-Dibromopropyl) phosphate (tris-BP)
10179007
8880 Aroclor-1016 (PCB-1016)
8885 Aroclor-1221 (PCB-1221)
8890 Aroclor-1232 (PCB-1232)
8895 Aroclor-1242 (PCB-1242)
8900 Aroclor-1248 (PCB-1248)
8905 Aroclor-1254 (PCB-1254)
8910 Aroclor-1260 (PCB-1260)
8912 Aroclor-1262 (PCB-1262)
8913 Aroclor-1268 (PCB-1268)
EPA 8082A 10179201
8880
8885
8890
8895
8900
8905
8910
8912
_________________ 8913
EPA 8141A
Aroclor-1016 (PCB-1016)
Aroclor-1221 (PCB-1221)
Aroclor-1232 (PCB-1232)
Aroclor-1242 (PCB-1242)
Aroclor-1248 (PCB-1248)
Aroclor-1254 (PCB-1254)
Aroclor-1260 (PCB-1260)
Aroclor-1262 (PCB-1262)
Aroclor-1268 (PCB-1268)
10182000
7045 Anilazine
7065 Atrazine
7070 Azinphos-ethyl (Ethyl guthion)
7075 Azinphos-methyl (Guthion)
7125 Bolstar (Sulprofos)
7220 Carbophenothion
7300 Chlorpyrifos
7315 Coumaphos
7390 Demeton
7395 Demeton-o
7385 Demeton-s
7410 Diazinon
8610 Dichlorovos (DDVP, Dichlorvos)
Polychlorinated Biphenyls (PCBs) by GC/ECD
Polychlorinated Biphenyls (PCBs) by GC/ECD
Organophosphorous Pesticides byGC/NPD
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 50 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
TestAmerica Denver EPACODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8141A
EPA 8141B
7475 Dimethoate
8625 Disulfoton
7550 EPN
7570 Ethoprop , '
7580 Famphur
7600 Fensulfothion 1
7605 Fenthion
7770 Malathion
7785 Merphos
7825 Methyl parathion (Parathion, methyl)
7850 Mevinphos
7905 Naled
8290 0,0,0-Triethyl phosphorothioate
7955 Parathion, ethyl
7985 Phorate
8000 Phosmet (Imidan)
8060 Propazine
8110 Ronnel
8125 Simazine
8155 Sulfotepp
8200 Tetrachlorvinphos (Stirophos, Gardona) Z-isomer
8235 Thionazin (Zinophos)
8245 Tokuthion (Prothiophos)
8275 Trichloronate
7045 Anilazine
7065 Atrazine
7070 Azinphos-ethyl (Ethyl guthion)
7075 Azinphos-methyl (Guthion)
7125 Bolstar (Sulprofos)
7220 Carbophenothion
7300 Chlorpyrifos
7315 Coumaphos
7390 Demeton
7395 Demeton-o
7385 Demeton-s
7410 Diazinon
8610 Dichlorovos (DDVP, Dichlorvos)
7475 Dimethoate
8625 Disulfoton
7550 EPN
7570 Ethoprop
10182204 Organophosphorous Pesticides by GC/NPD
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
51 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation ORELAP ID: 4025
Test America Denver EPACODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8141B 7580 Famphur
7600 Fensulfothion
7605 Fenthion
7770 Malathion
7785 Merphos >
7825 Methyl parathion (Parathion, methyl)
7850 Mevinphos
7905 Naled
7955 Parathion, ethyl
7985 Phorate
8000 Phosmet (Imidan)
8110 Ronnel
8125 Simazine
8155 Sulfotepp
8200 Tetrachlorvinphos (Stirophos, Gardona) Z-isomer
8235 Thionazin (Zinophos)
8245 Tokuthion (Prothiophos)
8275 Trichloronate
EPA 8151A
8655 2,4,5-T
10183207
8545 2,4-D
8560 2,4-DB
8555 Dalapon
8595 Dicamba
8605 Dichloroprop (Dichlorprop)
7775 MCPA
7780 MCPP
8645 Picloram
8650 Silvex (2,4,5-TP)
Chlorinated Herbicides by GC/ECD
EPA 8260B
5105 1,1,1,2-Tetrachloroethane
5185 1,1,1 -T richloro-2,2,2-trifluoroethane
5160 1,1,1-Trichloroethane
5110 1,1,2,2-T etrachloroethane
5195 1,1,2-Trichloro-1,2,2-trifluoroethane(Freon 113)
5165 1,1,2-Trichloroethane
5167 1,1,2-Trichlorofluoroethane
5172 1,1,2-Trifluoroethane
5171 1,1-Dichloro-1-fluoroethane
4630 1,1-Dichloroethane
4640 1,1 -Dichloroethylene
10184802 Volatile Organic Compounds by purge and trap GC/MS
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 52 of 70
«EU OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number. SolidS EPA8260B 4670 1,1-Dichloropropene
1,2,3-T richlorobenzene
1.2.3- T richloropropane
1.2.3- Trimethylbenzene1.2.4- Trichloroberizene •- ') i
‘1,2,4-Trimethylbenzene ' ' -
1,2rDibromo-3-chloropropane (DBCP)
1.2- Dibromoethane (EDB, Ethylene dibromide)
1.2- Dichloro-1,1,2,2-tetrafluoroethane (Freon-114)
1.2- Dichloro-1,1,2-trifluoroethane
1.2- Dichlorobenzene
1.2- Dichloroethane (Ethylene dichloride)
1.2- Dichloropropane
1.3.5- Trichlorobenzene
1.3.5- Trimethylbenzene
1.3- Dichlorobenzene
1.3- Dichloropropane
1.3- Dichloropropene
1.4- Dichlorobenzene
1.4- Dioxane (1,4- Diethyleneoxide)
1 -Chloro-1,1 -difluoroethane
1-Chlorohexane
2,2-Dichloro-1,1,1 -trifluoroethane (Freon 123)
4665 2,2-Dichloropropane
4410 2-Butanone (Methyl ethyl ketone, MEK)
4411 2-Chloro-1,1,1-trifluoroethane
4500 2-Ghloroethyl vinyl ether ;
4535 2-Chlorotoluene
4860 2-Hexanone (MBK)
5020 2-Nitropropane
5045 2-Pentanone
4540 4-Chlorotoluene
4910 4-lsopropyltoluene (p-Cymene)
4995 4-Methyl-2-pentanone (MIBK)
4315 Acetone
4320 Acetonitrile
4325 Acrolein (Propenal)
4340 Acrylonitrile
4355 Allyl chloride (3-Chloropropene)
4375 Benzene
4385 Bromobenzene
5150
5180
5182
51555210'
4570
4585
4695
4697
4610
4635
4655
6800
5215
4615
4660
4675
4620
4735
4919
4510
5222
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
53 Of 70
aEL4
ORELAPID: 4025
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver EPA CODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8260B 4390 Bromochloromethane
4395 Bromodichloromethane
4400 Bromoform
„ 4450 Carbon disulfide ,r
4455 Carbon tetrachloride i .
4475 Chlorobenzene, -- ~ V ,
4575 Chlorodibromomethane
4577 Chlorodifluoromethane (Freon-22)
4485 Chloroethane (Ethyl chloride) _ .
4486 Chlorofluoromethane
4505 Chloroform
4522 Chloropentafluoroethane
4525 Chloroprene (2-Chloro-1,3-butadiene)
4526 Chlorotrifluoroethene /
4705 cis & trans-1,2-Dichloroethene
4645 cis-1,2-Dichloroethylene
4680 cis-1,3-Dichloropropene
4600 cis-1,4-Dichloro-2-butene
4555 Cyclohexane
4560 Cyclohexanone
4595 Dibromomethane (Methylene bromide)
4625 Dichlorodifluoromethane (Freon-12)
4627 Dichlorofluoromethane (Freon 21)
4725 Diethyl ether
9375 Di-isopropylether (DIPE)
4750 Ethanol
4755 Ethyl acetate
4810 Ethyl methacrylate
4765 Ethylbenzene
4795 Ethylene oxide
4770 Ethyl-t-butylether (ETBE) (2-Ethoxy-2- methylpropane)
4772 . Fluoromethane (Freon 41)
4835 Hexachlorobutadiene
4870 lodomethane (Methyl iodide)
4875 Isobutyl alcohol (2-Methyl-1-propanol)
4895 Isopropyl alcohol (2-Propanol,Isopropanol)
4900 Isopropylbenzene (Cumene)
5240 m+p-xylene
4925 Methacrylonitrile
4940 Methyl acetate
4950 Methyl bromide (Bromomethane)
4960 Methyl chloride (Chloromethane)
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
54 Of 70
ow« OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.SoMdS EPA8260B 4990 Methylmethacrylate
5000 Methyl tert-butyl ether (MTBE)
4965 Methylcyclohexane
4975 Methylene chloride (Dichloromethane)
5245 m-Xylene ‘ ( ; ~
5005 Naphthalene
4425 n-Butyl alcohol (1-Butanol, n-Butanol)
; 4435 n-Butylbenzene
4855 n-Hexane
EPA 8260B SIM
5090 n-Propylbenzene
5250 o-Xylene
5035 Pentachloroethane
5080 Propionitrile (Ethyl cyanide)
9579 Propylene oxide
5255 p-Xylene
9607 sec-Butyl Alcohol (2-Butanol)
4440 sec-Butylbenzene
5100 Styrene
4370 T-amylmethylether (TAME)
4420 tert-Butyl alcohol
4445 tert-Butylbenzene
5115 Tetrachloroethylene (Perchloroethylene)
5120 Tetrahydrofuran (THF)
9574 Tetrahydrothiophene
5140 Toluene
4027 Total BTEX
5205 Total trihalomethanes
4700 trans-1,2-Dichloroethylene
4685 irans-1,3-Dichloropropylene
4605 trans-1,4-Dichloro-2-butene
5170 Trichloroethene (Trichloroethylene)
5175 Trichlorofluoromethane(Fluorotrichloromethane, Freon 11)
5225 Vinyl acetate
5235 Vinyl chloride
5237 Vinyl Fluoride
5260 Xylene (total)
10184904
4735 1,4-Dioxane (1,4- Diethyleneoxide)
EPA 8270C 10185805
6703 1,1'-Biphenyl (BZ-0)
6715 1,2,4,5-Tetrachlorobenzene
Volatile Organic Compounds by purge and trap GC/MS-SIM
Semivolatile Organic compounds by GC/MS
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
55 Of 70
oEU
ORELAPID: 4025
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of^Accreditation
TestAmerica Denver EPA CODE: C000026
4955 Yarrow st. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.SolidS EPA8270C. 5155 1,2,4-Trichlorobenzene
4610 1,2-Dichlorobenzene
6221 1,2-Diphenylhydrazine
6885 1,3,5-Trinitrobenzene'(1,3,5-TNB)
4615 1,3-Dichlorobenzene :
6160 1,3-Dinitrobenzene (1,3-DNB)-
4620 1,4-Dichlorobenzene , , /
/ 6165 1,4-Dinitrobenzene .
4735 1,4-Dioxane (1,4-Diethyleneoxide)
. 6420 1,4-Naphthoquinone
6630 1,4-Phenylenediamine
5790 1-Chloronaphthalene
6380 1-Methylnaphthalene
6425 1-Naphthylamine
4659 2,2-Oxybis(1-chloropropane)
6735 2,3,4,6-Tetrachlorophenol
6835 2,4,5-Trichlorophenol
6840 2,4,6-TrichlOrophenol
6000 2,4-Dichlorophenol
6130 2,4-Dimethylphenol
6175 2,4-Dinitrophenol
6185 2,4-Dinitrotoluene (2,4-DNT)
6005 2,6-Dichlorophenol
6190 2,6-Dinitrotoluene (2,6-DNT)
5515 2-Acetylaminofluorene
9322 2-Butoxyethanol
5795 2-Chloronaphthalene
5800 2-Chlorophenol
5866 2-Ethoxyethanol (cellosolve)
6360 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2-methylphenol)
5145 2-Methylaniline (o-Toluidine)1
6385 2-Methylnaphthalene
6400 2-Methylphenol (o-Cresol)
6430 2-Naphthylamine
6460 2-Nitroaniline
6490 2-Nitrophenol
5050 2-Picoline (2-Methylpyridine)
6412 3 & 4 Methylphenol
5945 3,3'-Dichlorobenzidine
6120 3,3'-Dimethylbenzidine
6355 3-Methylcholanthrene
6405 3-Methylphenol (m-Cresol)
6465 3-Nitroaniline
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
56 Of 70
HEUOWO OREGON
Environmental Laboratory Accreditation Program
ORELAP Fields of „noi:Accreditation ORELAP ID: 4025
TestAmerica Denver EPA CODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8270C 6365 4,4-Methylenebis(2-chloroaniline)
5540 4-Aminobiphenyl
5660 4-Bromophenyl phenyl ether (BDE-
5700 4-Chloro-3-methylphenol
5745 4-Chloroaniline -
5825 ) \4-Chlorophenyl phenylether
6105 4-Dimethyt aminoazobenzene
6410 . 4-Methylphenol (p-Cresol)
6470 4-Nitroaniline
6500 4-Nitrophenol
6510 4-Nitroquinoline 1 -oxide
6570 5-Nitro-o-toluidine
6112 6-Methylchrysene
6115 7,12-Dimethylbenz(a) anthracene
6125 a-a-Dimethylphenethylamine
5500 Acenaphthene
5505 Acenaphthylene
5510 Acetophenone
4330 Acrylamide
7005 Alachlor
4357 alpha-Methytstyrene
5545 Aniline
5555 Anthracene
5560 Aramite
7065 Atrazine
5562 Azobenzene
5570 Benzaldehyde
5567 Benzenethiol (Phenylmercaptan)
5595 Benzidine
5575 Benzo(a)anthracene
5580 Benzo(a)pyrene
5605 Benzo(e)pyrene
5590 Benzo(g,h,i)perylene
5600 Benzo(k)fluoranthene
5585 Benzo[b]fluoranthene
5610 Benzoic acid
5630 Benzyl alcohol
5760 bis(2-Chloroethoxy)methane
5765 bis(2-Chloroethyl) ether
5780 bis(2-Chloroisopropyl) ether
5670 Butyl benzyl phthalate
7180 Caprolactam
5680 Carbazole
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
57 of 70
HELt0^sb3* OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA8270C 7210 Carbofuran phenol
7260 Chlorobenzilate
5855 Chrysene
5862 Cresols, Total -
6065 Di(2-ethylhexyl) phthalate (bis(2- Ethylhexyl)phthalate, DEHP)
7405 Diallate
9354 , Dibenz(a, h) acridine
5900 Dibenz(a, j) acridine
5895 Dibenz(a.h) anthracene
5890 Dibenzo(a.e) pyrene
5905 Dibenzofuran
6070 Diethyl phthalate
7475 Dimethoate
6135 Dimethyl phthalate
5925 Di-n-butyl phthalate
6200 Di-n-octyl phthalate
8620 Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)
6205 Diphenylamine
8625 Disulfoton
6260 Ethyl methanesulfonate
7580 Famphur
6265 Fluoranthene
6270 Fluorene
6275 Hexachiorobenzene
4835 Hexachlorobutadiene
6285 Hexachlorocyclopentadiene
4840 Hexachloroethane
6295 Hexachloropropene
6312 Indene
6315 lndeno(1,2,3-cd) pyrene
7725 Isodrin
6320 Isophorone
6325 Isosafrole
6345 MethapyrileneI6375 Methyl methanesulfonate
7825 Methyl parathion (Parathion, methyl)
5010 n, n-Dimethyl formamide
5005 Naphthalene
5875 n-Decane
6300 n-Hexadecane
5015 Nitrobenzene
6525 n-Nitrosodiethylamine
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
58 Of 70
aEU OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.SoMdS EPA8270C 6530
5025
6545
6535
6550
6555
6560
6565
8290
5550
5553
7955
6590
5035
6600
6605
6615
6625
7985
6635
6640
9663
6650
6665
6670
6685
8155
8235
5200
8310
EPA 8270C SIM
n-Nitrosodimethyl amine
n-Nitroso-di-n-butyl amine
n-Nitrosodi-n-propylamine
n-Nitrosodiphenylamirie , . n-Nitrosomethylethalamine ' , -,
n-Nitrosomorpholirie' '—’ ' - ,x - " \ \ - ■n-Nitrosopiperidine ■ , .
n-Nitrosopyrrolidine ,
o,o,o-Triethyl phosphorothioate
o-Anisidine
Octachlorostyrene
Parathion, ethyl
Pentachlorobenzene '
Pentachloroethane
Pentachloronitrobenzene
Pentachlorophenol
Perylene
Phenacetin
Phenanthrene
Phenol
Phorate
Phthalic acid
Phthalic anhydride
p-Phenylenediamine
Pronamide (Kerb)
Pyrene
Pyridine
Quinoline
Safrole
Sulfotepp
Thioriazin (Zinophos) .
Triethylamine
tris-(2,3-Dibromopropyl) phosphate (tris- BP)
10242407
4735
6380
6385
5500
5505
5555
5575
5580
1,4-Dioxane (1,4- Diethyleneoxide)
1 -Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Semivolatile Organic compounds by GC/MS Selective Ion Monitoring
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
59 of 70
oELd OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.SoMdS EPA8270C 5605 Benzo(e)pyrene
SIM 5590 Benzo(g,h,i)perylene
5600 Benzo(k)fluoranthene
5585 Benzo[b]fluoranthene'
5670 Butyl benzyl phthalate
5855 Chrysene ' ' • ' ■ • ’ - .
6065 Di(2-ethylhexyl) phthalate (bis(2- Ethylhexyl)phthalate, DEHP)
5895
5905
6070
6135
5925
6200
6265
6270
6315
5005
6525
6530
6545
6535
6615
6665
Dibenz(a,h) anthracene
Dibenzofuran
Diethyl phthalate
Dimethyl phthalate
Di-n-butyl phthalate
Di-n-octyl phthalate
Fluoranthene
Fluorene
lndeno(1,2,3-cd) pyrene
Naphthalene ^
n-Nitrosodiethylamine
n-Nitrosodimethylamine
n-Nitrosodi-n-propyl amine
n-Nitrosodiphenylamine
Phenanthrene
Pyrene
EPA 8270D 10186002
6703
6715
5155
4610
6221
6885
4615
6160
4620
6165
4735
6420
6630
5790
6380
6425
4659
6735
1,1’-Biphenyl (BZ-0)
1,2,4,5-Tetrachlorobenzene
1.2.4- Trichlorobenzene
1.2- Dichlorobenzene
1.2- Diphenylhydrazine
1.3.5- Trinitrobenzene (1,3,5-TNB)
1.3- Dichlorobenzene
1.3- Dinitrobenzene (1,3-DNB)
1.4- Dichlorobenzene
1.4- Dinitrobenzene
1.4- Dioxane (1,4- Diethyleneoxide)
1.4- Naphthoquinone
1.4- Phenylenediamine
1 -Chloronaphthalene
1 -Methylnaphthalene
1-Naphthylamine
2,2-Oxybis(1 -chloropropane)
2,3,4,6-Tetrachlorophenol
Semivolatile Organic compounds by GC/MS
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
60 Of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.SoMdS EPA8270D 6835 2,4,5-Trichlorophenol
6840 2,4,6-Trichlorophenol
6000 2,4-Dichlorophenol
6130 2,4-Dimethylphenol ;
6175 2,4-Dinitrophenol
6185 2,4-Dinitrotoluene (2,4-DNT) - ' ; . ' ■'
6005 ■ 2,6-Dichlorophenol
6190 ' 2,6-Dinitrotoluene (2,6-DNT)
5515 2-Acetylaminofluorene /
5795 2-Chloronaphthalene
5800 2-Chlorophenol
6360 2-Methyl-4,6-dinitrophenol (4,6-Dinitro-2 -methylphenol)
5145 2-Methylaniline (o-Toluidine)
6385 2-Methylnaphthalene
6400 2-Methylphenol (o-Cresol)
6430 2-Naphthylamine
6460 2-Nitroaniline
6490 2-Nitrophenol
5050 2-Picoline (2-Methylpyridine)
6412 3 & 4 Methylphenol
5945 3,3’-Dichlorobenzidine
6120 3,3'-Dimethylbenzidine
6355 3-Methylcholanthrene
6405 3-Methylphenol (m-Cresol)
6465 3-Nitroaniline
6365 4,4-Methylenebis(2-chloroaniline)
5540. 4-Aminobiphenyl
5660 4-Bromophenyl phenyl ether (BDE-3)
5700 4-Chloro-3-methylphenol
5745 4-Chloroaniline
5825 4-Chlorophenyl phenylether ■
6105 4-Dimethyl aminoazobenzene
6410 4-Methylphenol (p-Cresol)
6470 4-Nitroaniline
6500 4-Nitrophenol
6510 4-Nitroquinoline 1-oxide
6570 5-Nitro-o-toluidine
6115 7,12-Dimethylbenz(a) anthracene
6125 a-a-Dimethylphenethylamine
5500 Acenaphthene
5505 Acenaphthylene
5510 Acetophenone
5545 Aniline
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
61 Of 70
owo OREGONEnvironmental Laboratory Accreditation Program
ORELAPID: 4025ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
EPACODE: C000026
Certificate: 4025 - 006
Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.SoMdS EPA 8270D
5560 Aramite
5562 Azobenzene
5570 Benzaldehyde .
5595 Benzidine
5575 Benzo(a)anthracene ---- -
5580 Benzo(a)pyrene
5590 Benzo(g,h,i)perylene
5600 Benzo(k)fluoranthene
5585 Benzo[b]fluoranthene
5610 Benzoic acid
5630 Benzyl alcohol
5760 bis(2-Chloroethoxy)methane
5765 bis(2-Chloroethyl) ether
5780 bis(2-Chloroisopropyl) ether
5670 Butyl benzyl phthalate
7180 Caprolactam
5680 Carbazole
7260 Chlorobenzilate
5855 Chrysene
8906 Coelution - 3-Chlorophenol + 4- Chlorophenol
5862 Cresols, Total
6065 Di(2-ethylhexyl) phthalate (bis(2- Ethylhexyl)phthalate, DEHP)
7405 Diallate
5900 Dibenz(a, j) acridine
5895 Dibenz(a.h) anthracene
5905 Dibenzofuran
6070 Diethyl phthalate
7475 Dimethoate
6135 Dimethyl phthalate
5925 Di-n-butyl phthalate
6200 Di-n-octyl phthalate
8620 Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)
6205 Diphenylamine
8625 Disulfoton
6260 Ethyl methanesulfonate
7580 Famphur
6265 Fluoranthene
6270 Fluorene
6275 Hexachlorobenzene
4835 Hexachlorobutadiene
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
62 Of 70
HEU OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025-006
Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA8270D 6285 Hexachlorocyclopentadiene
4840 Hexachloroethane
6295 Hexachloropropene
6315 lndeno(1,2.3-cd) pyrene .. .....
7725 Isodrin ' '6320 Isophorone -----J . ' y';
6325 Isosafrole
, 6345 Methapyrilene
x 6375 Methyl methanesulfonate
7825 Methyl parathion (Parathion, methyl)
- 5005 Naphthalene
5015 Nitrobenzene
6525 n-Nitrosodiethylamine
6530 n-Nitrosodimethylamine
5025 n-Nitroso-di-n-butylamine
6545 n-Nitrosodi-n-propylamine
6535 n-NitrosodiphenylamineI 6550 n-Nitrosomethylethalamine
6555 n-Nitrosomorpholine
6560 n-Nitrosopiperidine
6565 n-Nitrosopyrrolidine
8290 o,o,o-Triethyl phosphorothioate
7955 Parathion, ethyl
6590 Pentachlorobenzene
5035 'Pentachloroethane
6600 Pentachloronitrobenzene
6605 Pentachlorophenol
6610 Phenacetin
6615 Phenanthrene
6625 Phenol ,
7985 Phorate .
9663 p-Phenylenediamine
6650 Pronamide (Kerb)
6665 Pyrene
5095 Pyridine
6685 Safrole
8155 Sulfotepp
8235 Thionazin (Zinophos)
EPA8270D 10242509SIM
4735
6380
6385
5500
1,4-Dioxane (1,4- Diethyleneoxide)
1 -Methylnaphthalene
2-Methylnaphthalene
Acenaphthene
Semivolatile Organic compounds by GC/MS Selective Ion Monitoring
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
63 Of 70
owo OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8270D
SIM5505 Acenaphthylene
EPA 8310
5555 Anthracene
5575 Benzo(a)anthracene
5580 Benzo(a)pyrene I f
5590 Benzo(g,h,i)perylene
5600 Benzo(k)fluoranthene ~ - -
5585 Berizo[b]fluoranthene
5670 Butyl benzyl phthalate
5855 Chrysene
6065 Di(2-ethylhexyl) phthalate (bis(2- Ethylhexyl)phthalate, DEHP)
5895 Dibenz(a,h) anthracene
5905 Dibenzofuran
6070 Diethyl phthalate
6135 Dimethyl phthalate
5925 Di-n-butyl phthalate
6200 Di-n-octyl phthalate
6265 Fluoranthene
6270 Fluorene
6315 lndeno(1,2,3-cd) pyrene
5005 Naphthalene
6530 n-Nitrosodimethylamine
6535 n-Nitrosodiphenylamine
6615 Phenanthrene
6665 Pyrene
6380 1-Methylnaphthalene
6385 2-Methylnaphthalene
5500 Acenaphthene
5505 Acenaphthylene
5555 Anthracene r
5575 Benzo(a)anthracene
5580 Benzo(a)pyrene
5590 Benzo(g,h,i)perylene
5600 Benzo(k)fluoranthene
5585 Benzo[b]fluoranthene
5855 Chrysene
5895 Dibenz(a,h) anthracene
6265 Fluoranthene
6270 Fluorene
6315 lndeno(1,2,3-cd) pyrene
5005 Naphthalene
6615 Phenanthrene
10187607 Polynuclear Aromatic Hydrocarbons by HPLC/UV-VIS
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
64 Of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields ofAccreditation ORELAP ID: 4025
TestAmerica Denver EPA CODE: C000026
4955 Yarrow St. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids EPA 8310 6665 Pyrene
EPA 8321A
6885 1,3,5-Tririitrobehzene (1,3,5-TNB) /
6160 7 1,3-Dinitrobenzene (1;3-DNB) ~ - V
6014 ’ 2,3-Dinitrotoluene
/-, 8655 . - 2,4,5-T
' 9651 2,4,6-Trinitrotoluene (2,4,6-TNT)
8545 2,4-D
~ 8560 2,4-DB
6185 2,4-Dinitrotoluene (2,4-DNT)
6190 2,6-Dinitrotoluene (2,6-DNT)
9303 2-Amino-4,6-dinitrotoluene (2-am-dnt)
9507 2-Nitrotoluene
9510 3-Nitrotoluene
9306 4-Amino-2,6-dinitrotoluene (4-am-dnt)
9513 4-Nitrotoluene
7010 Aldicarb (Temik)
, 7040 Aminocarb
7195 Carbaryl (Sevin)
7205 Carbofuran (Furaden)
7275 Chloropropham
8555 Dalapon
8595 Dicamba
8605 Dichloroprop (Dichlorprop)
8620 Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)
7505 ': Djuron
7610 1 Fenuron
7630 Fluometuron
7765 Linuron (Lorox) ' '
7775 MCPA •:
7780 MCPP
7800 Methiocarb (Mesurol)
7805 Methomyl (Lannate)
6415 Methyl-2,4,6-trinitrophenylnitramine (tetryl)
7855 Mexacarbate)
7885 Monuron
7915 Neburon
5015 Nitrobenzene
6485 Nitroglycerin
10189001 Solvent Extractable non-volatile compounds by HPLC/TS/MS
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division 65 Of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow St.
Arvada, CO 80002 Issue Date: 1/9/2017
ORELAP ID: 4025
EPACODE: C000026
Certificate: 4025 - 006
Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.Solids ERA 8321A 9522 Octahydro-1,3,5,7-tetranitro-1,3,5,7-
tetrazocine (HMX)
EPA 8321B
6605 Pentachlorophenol
9558 Pentaeryth ritoltetran itrate (P ETN)
8075 Propham •
8080 Propoxur (Baygon) .;
9432 RDX (hexahydro-1,3,5-trinitro-1,3,5- triazine)
.8120 ; Siduron
8650 Silvex (2,4,5-TP)
6885 1,3,5-Trinitrobenzene(1,3,5-TNB)
6160 1,3-Dinitrobenzene (1,3-DNB)
6014 2,3-Dinitrotoluene
8655 2,4,5-T
9651 2,4,6-Trinitrotoluene (2,4,6-TNT)
8545 2,4-D
8560 2,4-DB
6185 2,4-Dinitrotoluene (2,4-DNT)
6190 2,6-Dinitrotoluene (2,6-DNT)
9303 2-Amino-4,6-dinitrotoluene (2-am-dnt)
9507 2-Nitrotoluene
9510 3-Nitrotoluene
9306 4-Amino-2,6-dinitrotoluene (4-am-dnt)
9513 4-Nitrotoluene
7010 Aldicarb (Temik)
7040 Aminocarb
7195 Carbaryl (Sevin)
7205 Carbofuran (Furaden)
7275 , Chloropropham
8555 Dalapon
8595 Dicamba
8605 Dichloroprop (Dichlorprop)
8620 Dinoseb (2-sec-butyl-4,6-dinitrophenol, DNBP)
7505 Diuron
7610 Fenuron
7630 Fluometuron
7765 Linuron (Lorox)
7775 MCPA
7780 MCPP
7800 Methiocarb (Mesurol)
7805 Methomyl (Lannate)
10189205 Solvent Extractable non-volatile compounds by HPLC/TS/MS
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
66 Of 70
aELa OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields ofAccreditation ORELAP ID: 4025
TestAmerica Denver EPA CODE: C000026
4955 Yarrow st. Certificate: 4025-006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.SoMdS EPA 8321B 6415 Methyl-2,4,6-trinitrophenylnitramine
(tetryl)
7855 Mexacarbate
7885 Monuron
7915 Neburon
5015 Nitrobenzene ___ i '
6485 Nitroglycerin
9522 Octahydro-1,3,5,7-tetranitro-1,3,5,7- tetrazocine (HMX)
6605' Pentachlorophenol
9558 Pentaerythritoltetranitrate (PETN)
8075 Propham
8080 Propoxur (Baygon)
9432 RDX (hexahydro-1,3,5-trinitro-1,3,5- triazine)
8120 Siduron
8650 Silvex (2,4,5-TP)
EPA 8330A 10190008
6885
6160
9651
5882
6185
6181
6190
9303
9507
9510
9306
9513
7046
6415
5015
6485
9522
9558
1899
9432
1.3.5- Trinitrobenzene (1,3,5-TNB)
1.3- Dinitrobenzene (1,3-DNB)
2.4.6- Trinitrotoluene (2,4,6-TNT)
2.4- diamino-6-nitrotoluene
2.4- Dinitrotoluene (2,4-DNT)
2.6- diamino-4-nitrotoluene
2.6- Dinitrotoluene (2,6-DNT)
2-Amino-4,6-dinitrotoluene (2-am-dnt)
2- Nitrotoluene
3- Nitrotoluene
4- Amino-2,6-dinitrotoluene (4-am-dnt)
4-Nitrotoluene
Ammonium Picrate
Methyt-2,4,6-trinitrophenylnitramine — (tetryl)
Nitrobenzene
Nitroglycerin
Octahydro-1,3,5,7-tetranitro-1,3,5,7- tetrazocine (HMX)
Pentaerythritoltetranitrate (PETN)
Picric Acid (2,4,6-Trinitrophenol)
RDX (hexahydro-1,3,5-trinitro-1,3,5- triazine)
Nitroaromatics and Nitramines by High Performance Liquid Chromatography (HPLC)
)
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
67 of 70
«EU OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
TestAmerica Denver
4955 Yarrow st. Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number._________
ORELAP ID: 4025
EPACODE: C000026
Solids EPA 8330B 10308006 Nitroaromatics, Nitramines and Nitrate Esters by High Performance Liquid Chromatography (HPLC)
6885 1,3,5-Trinitrobenzene (1,3,5-TNB)
6160 1,3-Dinitrobenzene (1',3-DNBj,
9651 2,4,6-Trinitrotoluene (2,4,6-TNT) /' - -5882 , 2,4-diamino-6-nitrotoluene
6185 2,4-Dinitrotoluene (2,4-DNT)' 6181 2,6-diamino-4-nitrotoluene
v 6190 2,6-Dinitrotoluene (2,6-DNT)
9303 2-Amino-4,6-dinitrotoluene (2-am-dnt)
9507 2-Nitrotoluene
6150 3,5-Dinitroaniline j
9510 3-Nitrotoluene
9306 4-Amino-2,6-dinitrotoluene (4-am-dnt)
9513 4-Nitrotoluene
7046 Ammonium Picrate
6415 Methyl-2,4,6-trinitrophenylnitr amine (tetryl)
5015 Nitrobenzene
6485 Nitroglycerin
9522 Octahydro-1,3,5,7-tetranitro-1,3,5,7- tetrazocine (HMX)
9558 Pentaerythritoltetranitrate (PETN)
1899 Picric Acid (2,4,6-Trinitrophenol)
>' ,9432 RDX (hexahydro-1,3,5-trinitro-1,3,5-
triazine)
EPA 9012A -
1645 : Total cyanide
10193405 Total and Amenable Cyanide (automated colorimetric with off-line distillation)
EPA 9012B • ' % .10243206 Total and Amenable Cyanide (automated colorimetric with off-linedistillation)
1645 Total cyanide
EPA 9030BJ
10195605 Acid-Soluble and Acid-Insoluble sulfides: Distillation
2005 Sulfide
EPA 9034
2005 Sulfide
10196006 Titrimetric Procedure for Acid-Soluble and Acid-Insoluble Sulfides
EPA 9045C
1900 pH
10198400 Soil and Waste pH
EPA 9045D
1900 pH
10244607 Soil and Waste pH
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
68 of 70
OREGONEnvironmental Laboratory Accreditation Program
ORELAP Fields of Accreditation
ORELAP ID: 4025
TestAmerica Denver
4955 Yarrow St.
EPACODE: C000026
Certificate: 4025 - 006
Arvada, CO 80002 Issue Date: 1/9/2017 Expiration Date: 1/8/2018
As of 1/9/2017 this list supercedes all previous lists for this certificate number.SoMdS EPA 9050A
1610 Conductivity
10198808 Specific Conductance
EPA 9056r " ■. rv ■-
10199005 Determination of Inorganic Anions byIon Chromatography
1540 Bromide '• ' ' • ~ . j ' ;
1575 Chloride ..... /N
1730 t fluoride "■ ' j «' -... 1805 Nitrate
1835 Nitrite
1870 Orthophosphate as P
2000 Sulfate
1825 Total nitrate+nitrite
EPA 9056A
1540 Bromide
10199607 Determination of Inorganic Anions byIon Chromatography
1575 Chloride
1730 Fluoride
•1805 Nitrate
1820 Nitrate-nitrite
1835 Nitrite
1870 Orthophosphate as P
2000 Sulfate
EPA 9060
2040 Total organic carbon
10200201 Total Organic Carbon
EPA 9060A '
I 2040 Total organic carbon
10244801 Total Organic Carbon
EPA 9071B-
10201602 Oil and Grease Extraction Method for sludge and sediment samples
1803 n-Hexane Extractable Material (O&G)
1860 Oil & Grease
EPA 9095A
9822 Extraction/Preparation .
10204203 Paint Filter Liquids Test
NWTPH-Dx
9369 Diesel range organics (DRO)
90018409 Oregon DEQ TPH Diesel Range
9499 Motor Oil
8641 Percent Moisture
9506 Residual Range Organics (RRO)
2050 Total Petroleum Hydrocarbons (TPH)
NWTPH-Gx
•90018603 Oregon DEQ TPH Gasoline Range
Organics by GC/FID-PID Purge & Trap
9408 Gasoline range organics (GRO)
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
69 of 70
SM 2320 B-97 online
1505 Alkalinity as CaC03
20045607 Alkalinity by Titration Method
SM 251 OB-97 online
1610 Conductivity '< ; ‘ ' /
20048606 Conductivity by Probe
SM 2540 B-97 online
1950 Residue-total
, , ; , 20049405 Total Solids Dried at 103 - 105C
SM 4500-CN C- 1999
1635 Cyanide
20095652/ Cyanide (Total) after Distillation/
SM 4500-CN E- 1999 ' "
1645 Total cyanide
20096417 Cyanide by Colorimetric Method
SM 4500-CN E- 2011 2011
1645 Total cyanide
20096428 Cyanide by Colormetric Method
SM 4500-CN'C-97 online
1645 Total cyanide
20095607 Cyanide by Total Cyanide afterDistillation
SM 4500-N02" 20113104 Nitrite by Colorimetric DeterminationB-2000 online
1835 Nitrite
1840 Nitrite as N
Department of Agriculture, Laboratory DivisionDepartment of Environmental Quality, Laboratory DivisionOregon Health Authority, Public Health Division
70 Of 70
TestAmericaTHE LEADER IN ENVIRONMENTAL TESTING
TestAmerica Denver
Electronic Document Cover
The electronic copy of this document, as maintained on the TestAmerica Denver computer network, is the controlled copy. Any printed copy becomes uncontrolled,
and all work performed should ultimately reference the controlled electronic version.
Any printed or electronic copy of this document that is distributed external to TestAmerica Denver becomes uncontrolled; To arrange for automatic updates to
this document, contact TestAmerica Denver.
TestAmerica Laboratories, Inc. TestAmerica Denver 4955 Yarrow Street Arvada, CO 80002
Phone: 303-736-0100 Fax: 303-431-7171
DenverTestAmericaTHE LEADER IN ENVIRONMENTAL TESTING
SOP No. DV-QA-003P, Rev. 11Effective Date: 10/31/2016
Page No.: 1 of 35
Electronic Copy Only
Title: Quality Control Program
Copyright Information:This documentation has been prepared by TestAmerica Laboratories, Inc. and its affiliates (“TestAmerica”), solely for their own use and the use of their customers in evaluating their qualifications and capabilities in connection with a particular project. The user of this document agrees by its acceptance to return it to TestAmerica upon request and not to reproduce, copy, lend, or otherwise disclose its contents, directly or indirectly, and not to use it for any other purpose other than that for which it was specifically provided. The user also agrees that where consultants or other outside parties are involved in the evaluation process, access to these documents shall not be given to said parties unless those parties also specifically agree to these conditions.
THIS DOCUMENT CONTAINS VALUABLE CONFIDENTIAL AND PROPRIETARY INFORMATION. DISCLOSURE, USE OR REPRODUCTION OF THESE MATERIALS WITHOUT THE WRITTEN AUTHORIZATION OF TESTAMERICA IS STRICTLY PROHIBITED. THIS UNPUBLISHED WORK BY TESTAMERICA IS PROTECTED BY STATE AND FEDERAL LAW OF THE UNITED STATES. IF PUBLICATION OF THIS WORK SHOULD OCCUR THE FOLLOWING NOTICE SHALL APPLY:
©COPYRIGHT 2016 TESTAMERICA LABORATORIES, INC. ALL RIGHTS RESERVED.
Facility Distribution No. Distributed To:
SOP No. DV-QA-003P, Rev. 11Effective Date: 10/31/2016
Page No.: 2 of 35
1.0 Purpose /
1.1 The purpose of this policy is to describe TestAmerica Denver’s program of routine analytical quality control (QC) activities. The objective is to generate QC data that demonstrate that the analytical process is in control and that the data meet client and method requirements.
1.2 The policy outlines QC requirements for a variety of regulatory programs, with the stipulation that lacking specific direction from our clients, TestAmerica Denver will default to routine “commercial” QC requirements as described in this policy.
2.0 Scope
2.1 This procedure provides a consistent approach for evaluating and maintaining routine analytical QC activities. This document has been prepared to assure compliance with The NELAC Institute (TNI) Standard, dated 2009, Volume 1 Modules 2 and 4, and the ISO/IEC Guide 17025:2005(E). All requirements established here are to be enforced and followed throughout the laboratory.
2.2 Every staff member at TestAmerica Denver plays an integral part in quality control activities and is held responsible and accountable for the quality of their work. It is, therefore, required that all laboratory personnel are trained and agree to comply with applicable procedures and requirements established by this document.
2.3 Federal program requirements are not covered in this procedure. SOP DV-QA- 024P, Requirements for Federal programs provides specific requirements for the Department of Defense Environmental Accreditation Program (DoD ELAP) and the Department of Energy (DOE) programs. When performing analyses for DoD ELAP, or DOE projects, DV-QA-024P shall be consulted to ensure that program- specific requirements are met.
3.0 Safety
3.1 There are no specific safety hazards associated with this SOP.
3.2 During the course of performing this procedure it may be necessary to go into laboratory areas to consult with appropriate staff members, therefore employees performing this procedure must be familiar with the Laboratory Health & Safety Plan, and take appropriate precautions and wear appropriate attire and safety glasses.
4.0 Definitions
4.1 Acceptance Criteria: The specified limits placed on characteristics of an item, process, or service defined in requirement documents.
4.2 Accuracy: The degree of agreement between an observed value and anaccepted reference value. Accuracy includes a combination of random error (precision) and systematic error (bias) components which are due to sampling and analytical operations; a data quality indicator.
COMPANY CONFIDENTIAL AND PROPRIETARY
SOP No. DV-QA-003P, Rev. 11Effective Date: 10/31/2016
Page No.: 3 of 35■©
4.3 Batch: Environmental samples that are prepared and/or analyzed together with the same process and personnel, using the same lot(s) of reagents.
4.3.1 A preparation batch is composed of one (1) to twenty (20) environmental samples of the same quality systems matrix, meeting the above mentioned criteria and with a maximum time between the start of processing of the first and last sample in the batch to be twenty-four (24) hours. When a batch is closed and a new batch is opened, QC samples must not be shared across multiple LIMS batch numbers that are prepared at different times. Each LIMS preparation batch must have its own QC samples.
NOTE 1: Field samples prepared at different dilutions (initial volume < nominal volume specified in the method) are not duplicates and must be counted as separate samples toward the batch count of20.
NOTE 2: For some procedures where the analytical results from the same extract can be reported using different analysis method codes, the samples are prepared in the same QC batch and then assigned to a different TALS prep batch number. Traceability to the analyst, original reagents, materials, and equipment must be maintained.
NOTE 3: When samples need to be filtered by the lab, the samples and associated batch QC must all be filtered. A filtration batch must not exceed 20 samples.
4.3.2 An analytical batch is composed of prepared environmental samples (extracts, digestates or concentrates) which are analyzed together as a group. An analytical batch can include prepared samples originating from various quality system matrices and can exceed twenty (20) samples. (Analyses with no separate preparation are limited to 20 field samples.)
4.4 QC Batch: The QC batch is a set of up to 20 field samples plus associatedlaboratory QC samples (both positive and negative controls) that are similar in composition (matrix) and that are processed within the same time period using the same reagents and standard lots. )
4.5 Calibration: A set of operations that establish, under specified conditions, the relationship between values of quantities indicated by a measuring instrument or measuring system, or values represented by a material measure or a reference material, and the corresponding values realized by standards.
4.6 Corrective Action: The action taken to eliminate the causes of an existingnonconformity, defect, or other undesirable situation in order to prevent recurrence.
4.7 Detection Limits and Quantitation Limits
NOTE: DoD ELAP program delineates three detections limits (DL, LOD and LOQ) see SOP DV-QA-024P for additional information.
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4.7.1 Limit(s) of Detection (LOD) [a.k.a., Method Detection Limit (MDL)]: Alaboratory's estimate of the minimum amount of an analyte in a given matrix that an analytical process can reliably detect in their facility. This is defined as the minimum concentration of a substance (an analyte) that can be measured and reported with 99% confidence that the analyte concentration is greater than zero and is determined from analysis of a sample in a given matrix containing the analyte.
4.7.2 Limit(s) of Quantitation (LOQ) [a.k.a., Reporting Limit]: The minimum levels, concentrations, or quantities of a target variable (e.g., target analyte) that can be reported with a specified degree of confidence.
4.7.3 Lower Limit of Quantitation (LLOQ): The lowest concentration at which the laboratory has demonstrated target analytes can be reliably measured and reported with a certain degree of confidence, which must be > the lowest point in the calibration curve. The LLOQ is equivalent to the standard reporting limit. The required LLOQ verification is performed at a concentration of 1-2 times the LLOQ (or RL).
4.8 Instrument/Calibration Blank: A clean sample (e.g., distilled water, hexane, methylene chloride, etc.) processed through the instrumental steps of the measurement process; used to determine instrument contamination.
NOTE: For procedures without a separate preparation step for aqueous samples, an instrument blank is equivalent to the method blank, and serves the same purpose.
4.9 Laboratory Control Sample (however named, such as laboratory fortified blank, spiked blank, or QC check sample): A sample matrix, free from the analytes of interest, spiked with verified known amounts of analytes or a material containing known and verified amounts of analytes, taken through all preparation and analysis steps of the procedure unless otherwise noted in a reference method. It is generally used to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system.
, 4.9.1 An LCS shall be prepared at a minimum of one per batch of 20 or fewersamples per matrix type per sample extraction or preparation method.
4.9.2 QC samples are purchased and used as an LCS for methods that are not easily spiked into solution such as total suspended solids, total dissolved solids, pH or turbidity.
4.9.3 Sample duplicates serve as the batch QC for methods where spiking solutions are not available such as total volatile solids, total solids, color, dissolved oxygen, settable solids or moisture. An LCS is not prepared for these methods.
4.10 Laboratory Control Sample Duplicate (LCSD): A duplicate laboratory control sample must be prepared if there is insufficient sample volume received to prepare and analyze an MS/MSD pair or sample duplicate. Some clients may require an
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LCSD to be reported for their samples. LCS/LCSD pairs provide information regarding the precision of the measurement process.
4.11 Matrix Spike (spiked sample or fortified sample): A sample prepared, takenthrough all sample preparation and analytical steps of the procedure unless otherwise noted in a referenced method, by adding a known amount of target analyte to a specified amount of a field sample for which an independent test result of targetanalyte concentration is available. Matrix spikes are used, for example, to determine the effect of the matrix on a method's recovery efficiency..
4.12 Matrix Spike Duplicate (spiked sample or fortified sample duplicate): Areplicate matrix spike prepared and analyzed to obtain a measure of the precision of the recovery for each analyte.
NOTE: Due to the potential variability of the matrix of each sample, the MS and MSD results may not have immediate bearing on any samples except the one spiked and possible for samples from the same site.
4.13 Measurement System: An analysis or test method, as implemented at aparticular laboratory, which includes the equipment and reagents used to perform the method.
4.14 Method Blank: A sample of a matrix similar to the batch of associated samples (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences are present at concentrations that impact the analytical results for sample analyses.
4.15 Precision: The degree to which a set of observations or measurements of the same property obtained under similar conditions, conform to themselves; a data quality indicator. Precision is usually expressed as standard deviation, variance or range, whether absolute or in relative terms.
4.16 Sample Duplicate: A sample duplicate is a second aliquot of a field sample, taken from the same sample container when possible, that is processed with the first aliquot of that sample. That is, sample duplicates, using the same size aliquot from the sample container for each replicate, are processed as independent samples within the same QC batch. The sample duplicate does not count toward the maximum batch count of 20 samples. The sample and duplicate results are compared to determine the effect of the sample matrix on the precision of the analytical process.
NOTE: Field samples that go thorough a preparation process at different dilutions are not considered duplicates and must be counted as separate samples toward the batch count of 20.
4.17 Spike: A known amount of target analyte added to a blank sample or sub-sample; used to determine recovery efficiency or for other quality purposes.
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4.18 Surrogate: A substance with properties that mimic the analyte of interest. It is unlikely to be found in environment samples and is added to them for quality control purposes.
4.18.1 Surrogate compounds must be added to air samples, standards, and blanks, for all organic chromatography methods except when the matrix precludes its use or when a surrogate is not available. Poor surrogate recovery may indicate a problem with sample composition and shall be reported to the client whose sample produced poor recovery.
4.19 Working Range: The difference between the Limit of Quantitation and the upper limit of measurement system calibration.
Procedure
5.1 Assessments of QC data relative to established control limits determine the acceptability of sample test results. Whenever control criteria are not met, the data must be evaluated to determine appropriate corrective action. Corrective action decisions, particularly whether or not to reanalyze samples, should be done in consultation with the client to the extent possible when operating under project- specific QA plans.
5.2 TestAmerica Denver’s standard QC program shall be communicated to the client prior to acceptance of work. Alternative QC procedures may be required depending on the clients’ special project requirements. In the event that alternative QC procedures are not specified by our clients, the standard QC protocols specified in this policy must be followed to ensure the generation of legally and scientifically defensible analytical data.
5.3 TestAmerica Denver’s QC Program applies to the following:
5.3.1 RCRA and SW-846 Projects - All routine analytical projects performed using SW-846 methods must comply with the requirements described in TestAmerica Denver’s Quality Assurance Manual (QAM) and this policy. The Quality Control sections of analytical standard operating procedures (SOPs) referencing SW-846 methods must be consistent with the requirements in this policy.
5.3.2 CWA and 40 CFR Part 136 Projects - Any analytical work conducted in support of an NPDES permit or other Clean Water Act (CWA) compliance activities, must meet applicable quality control specifications as summarized in the QAM. The quality control requirements listed in the QAM define the minimum requirements that must be given in laboratory analytical SOPs.
5.3.3 Method specific QC requirements that are more restrictive than the requirements defined in this policy take precedence. For example, a method that requires the MS/MSD be performed every 10 samples sets the number of samples in the QC batch to 10, not 20.
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Other Programs or Projects with Clearly Defined QC Requirements
5.4.1 The differences between TestAmerica Denver’s standard QC program and special project requirements must be specified in project documents. These documents may include Quality Assurance Project Plans (QAPPs), Sampling and Analysis Plans (SAPs), project-specific Quality Assurance Summaries (QASs), SOPs, contracts, protocols, or other approved documents.
NOTE: Specific requirements for federal programs are not covered in this document and can be found in TestAmerica Denver’s SOP DV- QA-024P QA/QC Requirements for Federal Programs.
5.4.2 Documents describing special project requirements must be reviewed and approved by appropriate QA and operations staff.
5.4.3 If the special project requirements appear to result in modifications that contradict TestAmerica policies or procedures, a variance must be requested in writing and communicated to the client. A record of this communication and acceptance of the variance must be retained as a permanent part of the project file.
5.4.4 Any special client’s project requirements must be communicated to TestAmerica Denver’s analysts in advance of releasing samples for analysis, and the work must be clearly differentiated in the analytical documentation, otherwise this policy’s requirements will be followed.
Laboratory QC Method Requirements
NOTE: Analytical SOPs must include a quality control section that addresses these general QC requirements as well as method-specific requirements. Method-specific requirements are given precedence to these general requirements and are noted accordingly.
5.5.1 The proficiency of a method is defined by its precision, bias (accuracy), limit of quantitation, limit of detection, and working range.
5.5.2 The limit of quantitation (LOQ) is established as the standard reporting limit at the time of calibration and is typically defined as the lowest level standard that is used in the method calibration. Alternatively, the LOQ may be defined in relation to an established lower limit of detection (LOD), i.e., method detection limit (MDL). See SOP DV-QA-009P, Reporting Limits, for additional information.
5.5.3 The working range is established by the difference between the Limit of Quantitation and the upper limit of measurement system calibration.
5.5.4 The method detection limit (MDL) must be initially determined in accordance with Policy DV-QA-005P. The MDL must be verified annually at a minimum. Quarterly verification is required for specific programs (DOD ELAP and Texas TRRP).
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5.5.5 Prior to using a method for actual samples and at any time there is a change in instrument type, personnel, or test method, a NELAC-compliant demonstration of capability (IDOC) must be performed by the analyst(s) who will be performing the method in accordance with SOP DV-QA-0024. The analyst must analyze spiked control samples and achieve recoveries within prescribed acceptance criteria. For methods where spiked samples are not appropriate, the DOC consists of demonstration of a properly performed QC batch. Acceptable results from analysis of blind PTs or QC samples may also be used for the CDOC. Analysts performing a method must demonstrate their continued proficiency annually.
5.5.6 Evaluation of LCS data over the long term establishes the precision and bias of the analytical method free of any matrix interference. See section5.9 for details on the determination of limits.
Batch QC Elements and Batch Processing
5.6.1 A QC batch is designed to allow assessment of the quality, in terms of accuracy and precision, of the analytical results obtained for a group of up to 20 field samples. Every batch must include both accuracy and precision. With some exceptions as described in Sections 5.6.6 and 5.6.7 below, the minimum QC elements for each QC batch consist of the following:
• one method blank (MB),
• one laboratory control sample (LCS),
• one sample duplicate (DUP) [where applicable],
• one matrix spike (MS), and
• one matrix spike duplicate (MSD).
NOTE: If there is insufficient sample for an MS/MSD or sample duplicate, an LCSD must be performed.
5.6.2 The identity of each QC batch must be documented and traceable, i.e., each batch of field samples must be clearly associated with the applicable QC samples.
5.6.3 To the extent possible, samples that require a preparation step should be analyzed together with their associated QC samples. If the samples in a given QC batch require separate analytical runs, the minimum batch QC in each run is an acceptable MB or instrument/calibration blank. To the extent possible, the QC samples should not be analyzed independently of the field samples on a different instrument.
5.6.4 For analytical procedures that do not include a separate extraction or digestion (e.g., volatile organic analysis by purge and trap), the QC batch must be analyzed sequentially using the same instrument and instrument configuration within the same calibration event. That is, the same calibration curve, calibration factors, or response factors must be in effect throughout the analysis.
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5.6.5 Field QC samples (e.g., trip blanks, equipment rinsates, and field duplicates) count as individual samples, therefore, they add to the QC batch count. Samples that require simple reanalysis (e.g., dilutions to adjust a sample extract to the working range of the instrument), as opposed to re-extraction or digestion and reanalysis, do not count as additional samples in the QC batch. For procedures without a separate preparation, a reanalysis within the same calibration event (as defined in Section 5.6.4) does not add to the batch count.
5.6.6 Although MS/MSD pairs are the preferred measure of precision, they are not the only acceptable means of demonstrating precision.
5.6.6.1 As requested by clients or as method required, batch precision may also be demonstrated through the analysis of sample duplicates. The client should be advised that a sample duplicate is less likely to provide usable precision statistics depending on the likelihood of finding concentrations above reporting limits.
5.6.6.2 A duplicate LCS (LCSD) may be used to demonstrate method batch precision independent of the client’s matrix. LCSDs may be prepared at the client’s request, but must be used when there is no client specified MS and MSD, or sample duplicate in the batch.
5.6.6.3 On-going monitoring of LCS results can be used to determine long-term precision and accuracy for a method independent of matrix effects.
5.6.6.4 MS and MSDs are to be prepared, analyzed and reported at the same dilution as the parent sample.
5.6.7 Some methods, including isotope-dilution methods, pH, and ignitability, for example, do not use all of the QC elements listed in Section 5.6.1. Method exceptions to these requirements are listed in the laboratory’s analytical SOPs.
5.6.8 Deviations from these QC elements must be noted either in project planning documents (QAPPs, SAPs, SOWs, QAS, or equivalent) or in a nonconformance memo (see SOP DV-QA-0031 for details).
Data Evaluation and Corrective Action)
5.7.1 General Guidelines\
5.7.1.1 Any QC component that fails acceptance criteria is considered an out-of-control event. All out-of-control events must be documented and the associated data evaluated. Depending on the specific circumstances, evaluation can lead to a variety of actions. The following sections and the flowcharts (Figures 1-4) describe the appropriate corrective actions for the most common QC failures. However, it is not possible to address all possible data evaluation scenarios in this policy. The guiding principle for
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all evaluations is that the data and corrective action decisions must be defensible using TestAmerica Denver policies, procedures, or scientific evidence, and justified in the project records.
5.7.1.2 If reanalysis for QC failures is conducted and the second analysis confirms a QC problem that is outside of the laboratory’s control, further testing is not necessary. The problem must be documented and the data properly qualified in. the analytical report.
5.7.1.3 QC failures that require reanalysis are documented in TestAmerica Denver’s electronic nonconformance system, as described in SOP DV-QA-0031.
5.7.1.4 QC failures due to sample matrix interferences (particularly sample duplicate, and sample surrogate failures) must be documented and the data properly qualified in the analytical report.
5.7.1.5 The laboratory does not control on MS/MSD recoveries or RPDs. However, the laboratory must ensure that significant failures are not due to laboratory error such as a missed spike, double spike or incorrect integration. MS/MSD failures due to laboratory error must be corrected. See Section 5.7.6.2 for additional corrective actions.
5.7.1.6 When ongoing, systematic problems are identified, work must stop until it can be demonstrated that the system is in control again.
5.7.2 Method Blank (MB) Evaluation (see Figure 1)
5.7.2.1 Method Blank Acceptance Criteria
5.7.2.1.1 When appropriate for the specific analytical method, the results of the method blank shall be one of the QC measures used to assess batch acceptance. SW-846 guidance is to have no detectable contaminants in the method blank, i.e., the method blank result must be less than or equal to the MDL for each target analyte. However, this may not be practically achievable in a laboratory setting, and method blank contamination between the MDL and the laboratory’s reporting limit may not have an adverse affect on data quality. Each method blank must be critically evaluated as to the nature of the interference and the effect on the analysis of each sample in the batch.
5.7.2.1.2 TestAmerica Denver policy is that the method blank is acceptable as long as all analytes of interest are less than one-half the laboratory’s reporting limit (RL) for
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organic, metals, and some wet chemistry analyses, unless otherwise specified by specific projects or clients or listed here.
5.7.2.1.3 For the following list of wet chemistry analytes, a method blank is acceptable if the analytes of interest are less than the reporting limit:
AlkalinityBODCODHEMHEM SGT TDSTOC soils
5.7.2.1.4 When the method blank result is above the acceptance limit, the results for the associated samples may be accepted with qualification if the method blank meets one of the following criteria, unless otherwise prescribed by project-specific requirements:
• The concentration of the analyte of concern in the method blank is less than or equal to 10% (1/10) of the regulatory limit for that analyte, or
• The concentration of the analyte of concern in the method blank is less than or equal to 10% (1/10) of the measured concentration of that analyte in the sample, or
• The same analyte was not detected above the MDL in the associated samples (and therefore the apparent contamination in the blank did not represent corresponding elevated values in the samples).
NOTE: Positive method blank results slightly below thereporting limit should still be evaluated by the analyst for potential impact on sample results at or near the reporting limit.
5.7.2.2 Corrective Action for Method Blank Failure
5.7.2.2.1 If the method blank does not meet the acceptance criteria, the source of contamination must be investigated and measures taken to correct, minimize, or eliminate the problem.
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5.7.2.2.2 Samples associated with the contaminated blank shall be reprocessed for analysis or may be reported as qualified (qualifier flags or narrative comments).
5.7.2.2.3 If the contaminant is a common laboratory contaminant (see the table below) and the MB concentration is less than 5 times the RL for organics or less than the RL for metals samples may be reported.
NOTE: Some programs do not recognize common laboratorycontaminants.
Common Laboratory Contaminants
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Analyte Method
Methylene Chloride Volatile Organics (GC or GC/MS)
Acetone Volatile Organics (GC or GC/MS)
2-Butanone Volatile Organics (GC or GC/MS)
Phthalate Esters Semi-Volatile Organics (GC or GC/MS)
Calcium Metals (ICP)
Sodium Metals (ICP)
Zinc Metals (ICP or ICP-MS)
Iron Metals (ICP or ICP-MS)
5.7.3 Laboratory Control Samples (LCS) Evaluation (see Figure 2)
5.7.3.1 LCS Acceptance Criteria
5.7.3.1.1 The LCS recovery for the control analytes must be within established control limits. Unless otherwise specified in a reference method or project requirements, the control limits are set at ± 3 standard deviations around the mean of the historical data. Regardless of the calculated limit, the limit should be no tighter than the Calibration Verification (CCV) [unless the analytical method specifies a tighter limit],
5.7.3.1.2 An LCS that is determined to be within acceptance criteria effectively demonstrates that the analytical system is in control and validates system performance for the samples in the associated batch.
5.7.3.1.3 The LCS percent recovery is calculated as follows:
, „ _ measured valueLCS Percent Recovery =-------------------- x 100%
expected value
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5.7.3.2 Marginal Exceedance
5.7.3.2.1 If there are a large number of reported analytes in the LCS, as is the case for many organic analyses, then NELAC allows a specified number of results to fall beyond the LCS control limit (3 standard deviations), but within the marginal exceedance (ME) limits.
5.7.3.2.2 Marginal exceedance limits are set at ± 4 standard deviations around the mean of historical data (marginal exceedance limits are posted in the Outlook public folders under Public FoldersNAII Public Folders\Analytical\Denver\NELAC-Marginal Exceedance Tables.
5.7.3.2.3 The number of marginal exceedances is based on the number of reported analytes in the LCS, as shown in the following table:
Marginal Exceedance Allowances
# of Reported Analytes in LCS
# of Allowed Marginal Exceedances
>90 5
71 -90 4
51-70 3
31 -50 2
11-30 1
<11 0
5.7.3.2.4 If more analytes exceed the LCS control limits than is allowed, or if any analyte exceeds the ME limits, the LCS fails and corrective action is necessary.
5.7.3.2.5 Marginal exceedances must be random. If the same analyte repeatedly fails the LCS control limits, it is an indication of a systematic problem. The source of the error must be identified and corrective action taken.
5.7.3.3 Corrective Action for LCS Failure
5.7.3.3.1 Samples analyzed along with an LCS that is determined to be “out of control” are considered suspect and the samples must be reprocessed and reanalyzed, or the data reported with appropriate data qualification. If the LCS result does not fall within statistical control limits, check calculations, check instrument performance, reanalyze the LCS, and if still
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outside of control limits, re-prepare and reanalyze all samples in the QC batch.
5.7.3.3.2 It is acceptable to report the data if the LCS recovery is out high and any analyte of concern was not detected in any of the samples.
5.7.3.3.3 In the case of volatile analyses, if the LCS fails, a new LCS may be re-prepared and reanalyzed within the same tune period.
5.7.3.3.4 In the case where all target requested analytes are within control, but some other LCS compounds are out of control, the LCS may still be considered acceptable for reporting.
5.7.3.3.5 See Figure 2 for additional detail.
5.7.4 Duplicate Laboratory Control Samples (LCSD or DCS) Evaluation (see Figure 2) ,
5.7.4.1 LCS/LCSD Acceptance Criteria
5.7.4.1.1 The recovery for each analyte in the LCS and LCSD must be within established control limits as described in Section 5.7.3.1. If either LCS fails, the samples must be reprocessed and reanalyzed, or the data reported with appropriate data qualification. LCS and/or LCSD failures must be described in the final report if samples are not reanalyzed.
5.7.4.1.2 The LCS precision is calculated as the relative percent difference (RPD) between the LCS and LCSD and must not exceed the established limit. Unless otherwise specified in the reference method or in project requirements, the limit is set at the mean of the historical RPD data plus three standard deviations. The RPD between the LCS and LCSD is calculated as follows:
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Where:
RPD =\LCS - LCSD]
{LCS + LCSD)x!00%
LCS = measured concentration for the LCS
LCSD = measured concentration for the duplicate LCS
5.7.4.2 Corrective Action for LCS/LCSD Recovery (Accuracy) Failure
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See Section 5.7.3.3 for corrective actions for LCS recovery failures.
NOTE: If either the LCS or the LCSD spike fails and the batch cannot be reprepared and/or reanalyzed, the failure must be documented and noted in the final report.
5.7.4.3 Corrective Action for LCS/LCSD Precision Failure
Because the LCS/LCSD precision limits are based on the standard deviation of data collected over time and include longterm precision, it would be unusual to fail precision limits while meeting accuracy limits. If this occurs with any frequency, control limits should be reevaluated. For any single precision failure, check calculations; verify, if possible, that the LCS and LCSD were spiked correctly; check instrument performance; and if the RPD is out of control but both accuracy recoveries are within acceptance criteria, prepare an NCM, and qualify the reported results.
5.7.5 Surrogate Evaluation (see Figure 3)
5.7.5.1 Acceptance Criteria
Surrogate recovery must be within established control limits. Unless otherwise specified in a reference method or project requirements, the control limits are set at ± 3 standard deviations around the mean of the historical data for QC samples. Method QC (MB, LCS, and/or LCSD) results are not acceptable unless the surrogate recoveries for those QC samples are within control limits. If MS/MSD, duplicate, or field samples require dilutions beyond the threshold stated in the analytical SOPs, routine surrogate control limits do not apply and recoveries are not evaluated. This should be noted in the final report. The surrogate recovery is calculated as follows:
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Surrogate Percent Recovery =measured value
expected valuexl00%
5.7.5.2 Corrective Action for Surrogate Failure
Corrective action must be considered for any surrogate failure. Analysts and data reviewers must review specific project instructions to be certain that the required actions are taken. Lacking instructions to the contrary, the following guidelines apply:
• Check calculations and instrument performance.
• Failed Surrogates in QC Samples: Evaluate the surrogate results together with the QC sample results for all QC samples in the batch to determine whether associated samples should
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be re-prepared and reanalyzed. Refer to Figures 1 through 4 for details. For example, consistent surrogate failures in all the QC samples in a batch indicate a method failure. Surrogate failures in only one QC sample in a batch may indicate a problem with that one sample only, especially if surrogate recoveries fall within limits for all other samples in the batch. Document the failure and evaluation in the final report.
• Failed Surrogates in Field Samples: Refer to Figure 3.
5.7.6 Matrix Spike and Matrix Spike Duplicates (MS/MSD) Evaluation (see Figure 4)
5.7.6.1 MS/MSD Acceptance Criteria
The MS and MSD recoveries for control analytes should be within established control limits, which are either mandated in the published methods or regulatory programs, or are set at ± 3 standard deviations around the mean of historical LCS data. In addition, the relative percent difference (RPD) between the MS and MSD results should be less than or equal to the established upper control limit. If MS or MSD samples require dilutions
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MS or MSD %Recovery = 'SSR-SR'
K SA ,x!00%
beyond the threshold stated in the analytical SOPs, routine control limits do not apply and recoveries are not evaluated, but this should be noted in the final report. The RPD between the MS and MSD is calculated the same way as the RPD between the LCS and LCSD, as shown in Section 5.7.4.1.2. The MS and MSD recoveries are calculated using observed concentrations (except as noted below):
Where:
SSR = observed concentration in spiked sample
SR = observed concentration in unspiked sample
SA = concentration of spike added to sample
NOTES:
1. If the sample result is ND, then SR = 0 when no values are reported below RL.
2. If the sample result is reported as a value less than the RL, then SR = the reported value.
3. CLP forms software uses observed recovery, not concentrations.
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5.7.6.2 Over Range Matrix Spikes
5.7.6.2.1 When the parent sample result and the MS/MSD concentration are above the linear range, the MS/MSD and parent sample MUST be reanalyzed at a dilution. These samples must be analyzed at the same dilution.
5.7.6.2.2 If the analyte concentration in the parent sample is greater than four times the concentration of spike added, then spike recovery results are not compared to control limits. The recovery is either reported as “NC” (not calculated) or with a qualifier flag to indicate that the spike was swamped by the native analyte concentration in the sample. If the analyte concentration in the parent sample is greatly above the spike concentration such that the dilution may cause the spike to be less than two times the reporting limit, the matrix spike does not need to be diluted and is reported as “NC” (not calculated).
5.7.6.3 Parent Sample is within Working Range and Matrix Spike(s) are Over Range - No client requested MS/MSD in Batch
When the parent sample result is within the working range of the method and the matrix spikes are over range and the MS/MSD serves as batch QC for all samples in the batch (no client requested MS/MSD) the laboratory will report the result for the sample from the original analysis together with the spike result qualified to indicate that it was an over range measurement (e.g., E-flag qualifier).
5.7.6.4 Parent Sample is within Working Range and Matrix Spike(s) are Over Range - Client-requested MS/MSD in Batch
When the parent sample result is within the working range of the method and the matrix spikes are over range and the MS/MSD was client-requested the laboratory will reanalyze the parent samples and MS/MSDs at the same dilution. If the analyte concentration in the parent sample is greater than four times the concentration of spike added, then spike recovery results are not compared to control limits. The recovery is either reported as “NC” (not calculated) or with a qualifier flag to indicate that the spike was swamped by the native analyte concentration in the sample.
5.7.6.5 For multi-analyte tests, if only a few of the target analytes are in the upper half of the curve causing a few of the MS/MSD to be over-range, diluting the sample may result in loss of information in the MS/MSD for all but one or a few analytes. Consult with the PM if needed to assure that the client receives data that serves their needs.
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5.7.6.6 Corrective Action for MS/MSD Recovery (Accuracy) Failure
As noted previously, matrix spike data are meaningful only for the sample in which they are prepared and possibly for samples from the same site. The information obtained from MS data are sample/matrix specific and are not normally used to determine the validity of the entire batch. If the MS and/or MSD recovery falls outside of the established control limits, the bracketing CCV and batch LCS recoveries must be within control limits in order to accept results for the associated samples. The following corrective actions are required for MS/MSD recovery failures to rule out lab error:
• Check calculation and instrument performance;
• Verify, if possible, that the MS and MSD were spiked correctly (e.g., very low or very high recoveries);
• Consider objective evidence of matrix interference (e.g., heterogeneous sample, interfering peaks seen on chromatograms, or interference demonstrated by prior analyses);
• Flag the data for any results outside of acceptance limits.
• For any single RPD failure, check calculations; verify, if possible, that the MS and MSD were spiked correctly; check instrument performance; consider objective evidence of matrix interference or sample inhomogeneity; and flag the data.
• If both the parent sample and associated matrix spike results are over range the parent and the spikes shall be diluted by the same amount and the results from the reanalysis reported for both. If the analyte concentration in the parent sample is greater than four times the concentration of spike added, then spike recovery results are not compared to control limits, and the recovery is either reported as “NC” (not calculated) or with a qualifier flag to indicate that the spike was less than four times the analyte concentration in the sample. If the dilution will cause the spike to be less than two times the reporting limit, the MS/MSD do not need to be diluted and the recovery reported as “NC” (not calculated).
• For MS/MSD that serve as batch QC, if the parent sample result is within the calibration range and the MS/MSD results are above the calibration range, the results are reported with the MS/MSD result being flagged as an over-range measurement (e.g., the E-flag qualifier).
• If the MS/MSD are client requested, the parent sample result is within calibration range and the MS/MSD results are above the calibration range, the sample and spike should be diluted, keeping in mind that we need to assess whether or not the dilution will best serve the client’s needs. Consult with the PM as needed. Both the parent sample and MS/MSD samples
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must have the same dilution factor. Some EDDs do not accept data that are at different dilution factors.
• If the native analyte concentration in the MS/MSD sample exceeds 4 times the spike level for that analyte, the recovery data are reported as NC (i.e., not calculated) and the appropriate qualifier flags are added.
• See Figure 4 for additional detail.
NOTE: See Denver Policy Memorandum P16-001 and Corporate Policy Memorandum CA-Q-QM-013 for more detail.
NOTE: Some client programs require reanalysis to confirm matrix interferences. Check special project requirements for this corrective action.
5.7.6.7 Corrective Action for MS/MSD Precision Failure
For any single precision failure, check calculations; verify, if possible, that the MS and MSD were spiked correctly; check instrument performance; consider objective evidence of matrix interference or sample inhomogeneity; and flag the data if no lab errors are found. If lab errors are identified take appropriate corrective action to resolve the error.
5.7.7 Sample Duplicate
5.7.7.1 Sample Duplicate Acceptance Criteria
The RPD between the sample and its duplicate must be within established control limits. The RPD between the sample and its duplicate is calculated the same way as the RPD between the LCS and its duplicate, as shown in Section 5.7.4.1.2.
5.7.7.2 Corrective Action for Duplicate Failure
For any single precision failure, check calculations and instrument performance. Document the QC failure in an NCM and note it on the final report.
Reporting Uncertainty with Measurements
It is the responsibility of the project manager to notify the appropriate laboratory personnel whenever the uncertainty for a given analyte is to be' reported. It is the responsibility of the laboratory personnel to calculate and report the uncertainty for each analyte requested in accordance with the procedures in this section
NOTE: The laboratory does not have an automated reporting mechanism for reporting the uncertainty associated with each measurement. Reporting
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this information would require project-specific arrangements to accommodate manual calculation and manual reporting.
5.8.1 Procedure
5.8.1.1 Determine the average and standard deviation of a minimum of twenty recovery results. Calculate the relative standard deviation (RSD) as follows:
5.8.1.2 The average percent recovery (Xavg) and the standard deviation (SD) can be derived from the control limits (at the 99% confidence interval):
Where: UCL=upper control limit, LCL= lower control limit
5.8.1.3 Calculate the uncertainty (U(X)) associated with an analytical result as follows:
5.8.2 Example Calculation
The analytical result for phenol is 120 pg/L. The control limits for phenol are 33-122%. The average recovery for phenol is 77.5% with a standard deviation of 14.8%. The average percent recovery and the standard deviation can be derived from the control limits (at the 99% confidence interval).
1) Calculate the average percent recovery:
RSD = SD /Xavg
Xavg = (UCL + LCL)/2
#U (X) = C+ (2 X RSD X C)
Where: C = Sample Concentration
Xavg= (122+33)/2 = 77.5
2) Calculate the Standard Deviation:
SD = 14.8
Standard Deviation
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where:
s = series number
7 = point number in series s
m = number of series for point y in chart
n - number of points in each series
X® = data value of series s and the ith point
Ny - total number of data values in all series
M = arithmetic mean
3) Calculate the RSD: 14.8/77.5=0.19
4) Calculate the uncertainty of the analytical result
U (x) = 120 + (2 x 0.19 x 120) = 165.6
U (x) = 120 - (2 x 0.19 x 120) = 74.4
5) Report the analytical result as 120 pg/L with an uncertainty range of74.4 pg/L to 165.6 pg/L at the 95% confidence interval.
Establishing QC Acceptance Limits
5.9.1 Initial Control Limits
For new procedures, published method limits can be used until sufficient QC data are acquired (a minimum of 20 to 30 data points recommended). However, the published limits may not be appropriate if they are based on a single-operator or single-laboratory study. In this case, the QA Manager may establish default limits until enough data are collected to calculate statistical limits.
5.9.2 TALS Control Chart Program
5.9.2.1 Evaluating control charts is an important first step in considering new control limits. Control charts are generated by TALS Control Chart program. The program collects a specified set of QC data, calculates the mean and three standard deviation control limits, compares those limits to the existing limits in the LIMS, and generates an l-type control chart (ref. ASTM D 6299). This control chart is a plot of results, in chronological order, to which existing control limits and a centerline have been added. The control chart aids in the examination of the data to be sure that it is representative and appropriate for use in setting new limits. See the TALS User Guide (Training Brief CW-l-T-001) Control Charts
for complete details on how to pull control charts. Some specific requirements include the following:
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5.9.2.2 Select QC Type Options
QC Type Description
MB Used to evaluate method baselines, laboratory background levels or possible issues with laboratory contamination. This may also be used to set MDLs.
LCS/LCSD Used to establish LCS/LCSD/MS/MSD control limits.
MS/MSD Used to assess matrix-specific control limits. This is used for evaluation purposes only. MS/MSD limits are set based on LCS/LCSD control limits.
MB/LCS/LCSDSurrogates
This option will produce a pooled set of LCS/LCSD and MB recoveries. There is an option to include or not include client samples. In addition control charts can be generated for just client samples.
5.9.2.3 Representative Time Period
The appropriate time period depends bn the frequency with which the test is performed and the frequency of other events, such as calibrations and standards preparation. A minimum of three months is desirable to capture data from multiple instruments, multiple instrument tunes, multiple calibrations, and multiple standard preparations. For infrequent tests, it may be necessary to collect nine months or more of data. However, collecting more than 100 data points is normally unnecessary, makes the control charts hard to read, and may result in abnormally tight control limits.
5.9.2.4 Documentation of Control Chart Review
When the control chart is obtained, select the “Save Log” button and answer “YES” to the two successive questions that are presented. This should be done any time control charts are reviewed, regardless of whether limits need to be changed, as described below.
5.9.3 Grubbs’Test for Outliers
5.9.3.1 The Control Limits program automatically runs the Grubbs’ test for
5.9.3.2
outliers using a 5% level of significance, i.e., the risk of falsely rejecting a data point. The initial assumption is made that the data are normally distributed. The Grubbs’ test detects one outlier at a time, eliminates that outlier, and repeats the test until all outliers are eliminated. The test should not be used for sample sizes of six or less.
The test is defined for the hypothesis H0, there are no outliers in the data set, and Ha, there is at least one outlier in the data set.
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The test statistic “G” is calculated as the ratio of the difference between the suspect point and the mean value to the calculated standard deviation, as follows:
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maxG =
Y-Y
Where:
Yi = the point being considered for rejection
Y = the mean value of the data set
s = the standard deviation
5.9.3.3 The hypothesis of no outliers, and consequently the suspect point, is rejected if
G >(n- l)-In l|
t,(al{2N),N-2)
N-2 + t,(al{2N),N-2)
Where:
N = number of points
t(a/(2N),N-2) = the critical value of the t-distribution with (N- 2)/2 degrees of freedom and a significance level of a/(2N).
NOTE: Tables for critical values of t are given in John Taylor, QualityAssurance of Chemical Measurements, Lewis Publishers; 1987. For a complete discussion of the Grubbs’ Test for Outliers also see NIST/SEMATECH e-Handbook of Statistical Methods, Section 4.3.5.1.7:http://www.itl.nist.gov/div898/handbook/eda/section3/eda35h.htm.
5.10 Evaluating and Investigating Collected Data
Assuming that an adequate amount of data are collected, the next step involves determining that the data set is representative of the laboratory’s performance, and therefore provides a useful prediction of future performance. A key part of the process is examining the data for bias, discontinuities, and/or trends. Ideally, if conditions are constant over the time period selected and existing limits are appropriate, the data will be evenly distributed around the centerline, with very few points outside control limits (i.e., less than 1 point in 100 should lie beyond the 3 standard deviation control limits). The reasons for deviations from the ideal should be investigated to be sure that the collected data are appropriate. Specific conditions requiring further investigation include data sets with no outliers, data with significant bias relative to existing limits, excessive number of outliers, discontinuous patterns, and upward or downward sloping trends
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5.10.1 The laboratory must review the control charts annually for trends and/or changes in the system to evaluate whether or not a change in control limits is required. If the recalculated limits are consistent with the historical limits (±5%), the historical limits may remain unchanged.
NOTE: DoD QSM requires a quarterly review of a subset ofrepresentative analytes. See SOP DV-QA-024P for additional details.
5.10.2 No Outlier Data
If there are no outlier data and little or no data outside the 2-standard-deviation warning limits, then one of the following is true:
5.10.2.1 Insufficient data have been collected, which can be tested by generating charts using a longer time period.
5.10.2.2 Outlier data are being censored (not entered into TALS). Check with the analysts to verify this. Analysts should be told that not omitting statistical outliers (not blunders) is essential to avoid generating even tighter limits.
5.10.2.3 Existing limits are much too wide (possibly because the performance of the analytical system has significantly improved) and should be changed immediately (see Section5.11 on Establishing New Control Limits below).
NOTE: When evaluation is made relative to the warning limits, if thelimits were set using the CCV limits, the mean shown will not be the statistical mean of the data set but the midpoint of the limits. Hence the mean and warning limits do not reflect the statistical dataset.
5.10.3 Bias Relative to Existing Limits
If there are a significant majority of QC results falling on one side of thecenterline, then consider the following:
5.10.3.1 The procedure, equipment, or calibration may have changed. Verify the accuracy of the SOP with analysts.
5.10.3.2 The analyst’s skill level may have changed. Check with the supervisor to find out if new analysts might account for the bias.
5.10.3.3 Equipment may have been changed. Check with supervisor.
5.10.3.4 The standards used for calibration, including those used for internal standards, may have changed or may have been incorrectly prepared.
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5.10.3.5
V
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The time since the limits were last set may be longer than six months, and an update to the control limits is overdue.
NOTE: When evaluation is made relative to the center line, if the limits were set using the CCV limits, the mean shown will not be the statistical mean of the data set but the midpoint of the limits. Hence the mean does not reflect the statistical dataset.
5.10.4 Excessive Number of Outliers
If significantly more than 1 point in 100 is outside the control limits, the following should be considered:
5.10.4.1 The variability in the analytical system may have changed significantly, either as the result of a specific event, or degradation in the instrumentation.
5.10.4.2 The existing limits may not be statistically based. Review control limits records to check the basis of the old limits.
5.10.4.3 Audit the method to verify the accuracy of the SOP, competency of the analysts, and reliability of the instrumentation.
5.10.4.4 Consult with the supervisor.
5.10.4.5 Compare laboratory’s performance to other laboratories. The Tri-Agency QSM limits is one source of limits by competent laboratories, other TestAmerica laboratories is another, and method limits have to be considered as well. Limits should not be widened if the laboratory’s performance is not consistent with other labs.
5.10.5 Discontinuous Pattern
If the data appear to run for a period at one mean recovery and then suddenly jump to a different level, then the following should be considered:
5.10.5.1 The accuracy of the analytical system experienced a statistically significant change, and most likely there is an event that caused that change, such as recalibration, change in instrument or instrument settings, change in calibration standards, change in methodology, or a change in analyst.
5.10.5.2 Consult with the supervisor.
5.10.5.3 Unless the discontinuity is characteristic of the method somehow, a decision will usually need to be made as to which mode of operation is the best predictor of future performance. A selective time period may be used for calculating
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representative limits if no errors in standards, instrument performance, etc., are identified.
5.10.6 Upward or Downward Sloping Pattern
An upward or downward trend is typically indicative of an unstable instrument, a standard or reagent that is degrading sooner than its current expiration period or progressive changes in background or contamination levels. Such trends are early warning that the analytical system will soon be out of control. When a trend is detected, investigate as follows:
5.10.6.1 Consult with the supervisor, and have the supervisor consider the condition of standards, reagents and maintenance of equipment.
5.10.6.2 Review the SOP and check the proficiency of the analysts.
5.10.6.3 Reliable control limits cannot be set using data during an unstable period. Maintaining the old limits until a stable period is documented is probably the best course.
5.11 Establishing New Control Limits
Having collected sufficient data and determined that the data are representative, the next step is to establish the new limits. See Work Instruction WI-DV-0097
Control Limit Review and Updating for additional details. Control limits are set at ± 3 standard deviations around the mean of the collected data with the following exceptions:
5.11.1 If the calculated 3-standard-deviation limits are tighter than the method calibration verification criteria (e.g., CCV acceptance limits for ICP are ± 10% of the expected value), then the new limits are set to the mean value ± the calibration acceptance limits.
5.11.2 If the calculated limits are wider than method or program requirements, then the laboratory’s performance should be reconsidered. If the limits are marginally wider, inspect the control chart to estimate the frequency of failures using the program limits. If, based on the control chart, the failure rate is predicted to be low (less than 2% is normally acceptable), then program limits might be adopted. Otherwise the laboratory will need to either not offer the test or request a variance.
5.11.3 If the lower control limit is very low, e.g., less than 10%, there is a concern about accepting data that is not quantitatively reliable. The minimum lower control limit must be elevated to 10%. If inspection of the control chart data indicates that the failure rate will be high at a LCL of 10%, the method should be evaluated for improvements that may mitigate a high failure rate. An exception to the lower limit of 10% is benzidine which is set to a minimum acceptance limit of 5%.
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5.11.4 If the upper control limit is less than 100% recovery plus the method calibration verification acceptance limit, then adjust the upper limit to 100% plus the calibration acceptance limit. For example, if CCV acceptance limits are ± 10% of the expected value, then set the upper control limit to 110%.
5.11.5 The basis of the new control limits must be documented Additionally, annotation may be made directly on the printed control charts or control limits reports, and must be signed and dated or the information conveyed to the QA Manager in an email.
5.12 Communicating and Implementing New Control Limits
5.12.1 When the group leader identifies a need to update limits, a request is sent by email to the QA department for a review of the limits.
5.12.2 The email should contain the control chart data (or location of the file), identification of analytes that require updates, and rationale for the change.
5.12.3 A member of the QA group will review the request and update the appropriate method limit group with the new limits (if necessary).
5.12.4 The QA department and the group leader will confirm a date that the instrument data systems and the LIMS will be updated. The CSO group will be notified of the changes.
5.13 Reporting QC Data
QC data that are routinely reported with sample results include the LCS, method blank, and surrogate standards. Client reporting format requirements are negotiable and documented as part of the project records. Ultimately, all reporting decisions should accommodate the client’s requirements as long as data integrity is maintained.
Responsibilities
6.1 Successful implementation of this QC program requires that it is clearly understood by all TestAmerica staff. Training based on this policy will be conducted periodically and provided to new personnel as appropriate for their functions.
6.2 Project Managers
6.2.1 The laboratory project managers (PMs) serve as a liaison between the clients and the laboratory staff to ensure that requirements are properly communicated in writing to both parties.
6.2.2 The PM communicates any QC problems to clients and documents decisions made with clients.
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6.3 Analytical Groups
6.3.1 The analytical groups are responsible for the evaluation of control limits, frequently in conjunction with data review software and/or senior analysts or supervisors.
6.3.2 Analytical groups shall review control chart data and notify QA when limits need to be updated as needed.
6.4 QA Group
6.4.1 The QA manager can establish default control limits until enough data points are collected to calculate statistical limits.
6.4.2 The QA staff shall review the statistical limits when the analytical groups request for updates to the control limits.
6.4.3 After coordinating a date and time with the analytical groups, the QA staff will update the control limits in the TestAmerica Denver LIMS system. See WI-DV-0097 Control Limit Updates.
6.4.4 The QA staff will evaluate all limits on an annual basis to ensure that appropriate limits are set and as a verification of the reviews performed by the laboratory groups.
6.4.5 The QA staff will verify and track the quarterly control chart reviews completed by the analytical groups. The reviewer shall document the date of review and notify the group leader and operations manager when reviews are past due.
References / Cross-References
7.1 Test Methods for Evaluating Solid Waste, Physical/Chemical Methods, USEPA SW-846, 3rd Edition, with promulgated updates, Chapter One, Quality Control.
7.2 2009 TNI Standard, Management and Technical Requirements for Laboratories Performing Environmental Analysis, Volume 1, The NELAC Institute.
7.3 A2LA Guidance for the Estimation of Uncertainty for testing” Thomas Adams, July 2002 (from the A2LA website)
7.4 ASTM D 6299, Standard Practice for Applying Statistical Quality Assurance and Control Charting Techniques to Evaluate Analytical Measurement System Performance, Volume 5.03.
7.5 John Taylor, Quality Assurance of Chemical Measurements, Lewis Publishers; 1987.
7.6 NIST/SEMATECH e-Handbook of Statistical Methods, http://www.itl.nist.gov/div898/handbook/eda/section3/eda35h.htm, April 1,2012.
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8.0 Attachments
Figure 1: Method Blank EvaluationFigure 2: LCS/LCSD EvaluationFigure 3: Surrogate Evaluation xFigure 4: Matrix Spike/Matrix Spike Duplicate Evaluation
9.0 Revision History
• Revision 11, dated 31 October 2016
o Removed references to AFCEE throughout o Removed reference to DV-QA-020P as this SOP was discontinued, o Added definition of Lower Limit of Quantitation6 Added requirement for assessment for batch precision by use of MS/MSD, sample
duplicate or LCS/LCSD throughouto Modified section 4.9.1 and added sections 4.9.2 and 4.9.3 - clarification/detail on
LCSso Added Calcium to the Common Laboratory Contaminants table in section 5.7.2.2.3 o Added Sections 5.7.6.2-5.7.6.4 to describe how to handle parent sample and
MS/MSD dilutions; renumbered remainder of sections o Revised Section 5.7.6.6 to describe corrective actions for MS/MSD recovery
failures to rule out lab erroro Added notes to Sections 5.10.2 and 5.10.3 to caution that when limits set to CCV
limits the mean and warning limits displayed on the control chart do not reflect the statistically determined limits
o Added reference to work instruction WI-DV-0097 Control Limit Review and Updating to section 5.11
o Added section 6.4.5 to state QA responsibility to track compliance with quarterly control chart review
o Editorial and formatting changes throughout
• Revision 10, dated 31 October 2015
o Revised Section 4.3.1 to clarify assignment of samples from one prep batch to accommodate different analysis method codes that use the same prep and extract for analysis
o Added detail to section 4.10 to identify when LCSD is prepared, o Updated section 5.7.2.1.3 to include TOC soilso Updated reference to TALS User Guide on how to generate control charts in
Section 5.9.2o Added suggestion in Section 5.10.6 that a sloping pattern may result from standard
or reagent degradation and should be evaluated, o Added section 6.4.4 to QA Group responsibilities to review limits annually in
addition to analytical group review.
• Revision 9, dated 31 August 2014 N
o Changed title of SOP o Formatting and editorial changes throughouto Re-arranged document sections for consistency, better flow and easier
comprehension and corrected section references throughout o Added references to SOP DV-QA-024P and CW-l-T-001 where appropriate
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o Split up original paragraph in Section 1 to be Sections 1.1 and 1.2. o Revised Section 2.0 to reflect the scope of the current document o Updated/revised definitions - aligned with QAM o Split up Section 4.3 to correct format and information o Updated Section 4.3.1 to reflect separate QC for separate batch numbers o Added note to Sections 4.7 and 4.16 o Removed previous Section 5.3 reference to DoD o Deleted previous Section 5.4.3 - SDWA reference o Added note to Section 5.4.1 o Added Section 5.7.3.2 o Deleted previous Section 5.6.5.1.2 o Revised Sections 5.6.6, 5.7.11, and 5.7.2.2 through 5.7.4 o Updated Section 5.9 o Updated Table 5.9.2.1 o Added Section 5.9.2.4o Integrated previous Attachment 1 information into the text of the SOP o Deleted previous Attachment 1 o Deleted previous Sections 5.6.5.3 and 5.6.5.4 o Added current Sections 5.10 through 5.11 o Updated current Section 5.12 to reflect current practices o Updated Section 5.13 that client requests for reporting QC data are followed so
long as data integrity is maintained, o Updated Section 6 to reflect current practices o Updated Figures 1 through 4 to current practices
Revision 8, dated 31 May 2013
o Revised section 4.3 to reflect current practiceo Clarified section 4.4 regarding differentiating what samples count toward the batch
count.o Added section 5.1.4 to clarify that method QC requirements take precedence over
this policy.o Revised 5.6.1.5 to reflect use of DOCs for tests without an LCS. o Revised section 5.6.3.2.1 to clarify method blank acceptance criteria for wet
chemistry methods.o Updated Section 5.6.3.2 DoD requirements to match QSM 4.2 o Corrected reference to public folders in section 5.6.3.3.1o Updated sections 5.6.3.6.2, 5.6.3.6.3 and Figure 4 to reflect policy change to flag
MS/MSD results rather than write NCM o Revised Sections 5.6.4.1 and 5.6.5.1.2 for clarity o Revised Figures to reflect changes to policy o Relabeled Figure 5 as Attachment 2 and updated form o Added references cited in text of SOP o Formatting and editorial changes throughout
Revision 7.3, dated 06 July 2012
o Removed criteria that the LOQ to be at least three times the LOD. o Updated sections 5.3.1.6 and 5.3.1.7 to meet current procedures, o Added requirement for limits to be reviewed annually by QA to section 5.3.1.6 and
5.3.1.7.o Updated Figures 2,3 and 4.
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o Removed section 5.3.3.5.2.2 which pertained to DoD requirements for surrogate failures. Can be found in the DoD specific SOP.
o Updated surrogate section 5.3.5.2.1 to meet current LIMS. o Updated section 5.3.5.1.2 for new procedure.
• Revision 7.2, dated 01 March 2011
o Updated references to TALS.
Earlier revision histories have been archived and are available upon request.
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Figure 1. Method Blank Evaluation
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Figure 2. LCS Failure
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Figure 3. Surrogate Failures
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Figure 4. MS/MSD Failure
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SCOPE OF ACCREDITATION TO ISO/IEC 17025:2005
TEST AMERICA DENVER 4955 Yarrow Street Arvada, CO 80002
Margaret S. Sleevi Phone: 303-736-0100 www.testamericainc.com
ENVIRONMENTAL
Valid To: October 31, 2017 Certificate Number: 2907.01
In recognition of the successful completion of the A2LA evaluation process, (including an assessment of the laboratory's compliance with ISO IEC 17025:2005, the 2009 TNI Environmental Testing Laboratory Standard, the requirements of the DoD Environmental Laboratory Accreditation Program (DoD ELAP) as detailed in version 5.0 of the DoD Quality Systems Manual for Environmental Laboratories), and for the test methods applicable to the Wyoming Storage Tank Remediation Laboratory Accreditation Program, accreditation is granted to this laboratory to perform recognized EPA methods using the following testing technologies and in the analyte categories identified below:
Testing Technologies
Atomic Absorption/ICP-AES Spectrometry, ICP/MS, Gas Chromatography, Gas Chromatography/Mass Spectrometry, Gravimetry, High Performance Liquid Chromatography, Ion Chromatography, Misc.- Electronic Probes (pH, O2), Oxygen Demand, Hazardous Waste Characteristics Tests, Spectrophotometry (Visible), Spectrophotometry (Automated),Titrimetry, Total Organic Carbon, Total Organic Halide
Parameter/Analvte Non-Potable Water Solid Hazardous Waste ("Water) Solid Hazardous Waste ("Solid)
MetalsAluminum EPA 6010B/6010C EPA 6010B/6010CAntimony EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020AArsenic EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020ABarium EPA 6010B/6010C/6020/6020A EPA 6010B/6010/6020/6020ABeryllium EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020ABoron EPA 6010B/6010C EPA 6010B/6010CCadmium EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020ACalcium EPA 6010B/6010C EPA 6010B/6010CChromium EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020ACobalt EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/ 6020/6020ACopper EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/ 6020/6020AIron EPA 6010B/6010C EPA 6010B/6010CLead EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/ 6020/6020A
^jthium EPA 6010B/6010C EPA 6010B/6010C^^gnesium EPA 6010B/6010C EPA 6010B/6010CManganese EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/ 6020/6020AMercury EPA 7470A EPA 7471 A/747 IB
(A2LA Cert. No. 2907.01) Revised 09/15/2016 ------ C. ^3—^ Page 1 of 12
5202 Presidents Court Suite 220 I Frederick, MD 21703-8398 I Phone: 301 644 3248 I Fax: 240 454 9449 I wwwA21_A.org
Parameter/Analvte Non-Potable Water Solid Hazardous Waste (Water) Solid Hazardous Waste (Solid)
Molybdenum EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/ 6020/6020AEckel EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020A
'otassium EPA 6010B/6010C EPA 6010B/6010CSelenium EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020ASilica EPA 6010B/6010C EPA 6010B/6010CSilicon EPA 6010B/6010C EPA 6010B/6010CSilver EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020ASodium EPA 6010B/6010C EPA 6010B/6010CStrontium EPA 6010B/6010C EPA 6010B/6010CThallium EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020ATin EPA 6010B/6010C EPA 6010B/6010CTitanium EPA 6010B/6010C EPA 6010B/6010CVanadium EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020AZinc EPA 6010B/6010C/6020/6020A EPA 6010B/6010C/6020/6020A
NutrientsNitrate (as N) By calculation EPA 9056/9056A/300.0
By calculation________EPA 9056/9056A By calculation
Nitrate-nitrite (as N) EPA 353.2 EPA 353.2/9056/ 9056A/300.0 EPA 9056/9056ANitrite (as N) SM 4500-N02 B SM 4500-N02 B
EPA 9056/9056A/300.0EPA 9056/9056A
Orthophosphate (as P) EPA 9056/9056A/300.0 EPA 9056/9056ATotal Phosphorus EPA 6010B/6010C EPA 6010B/6010C
mandsbtal Organic Carbon EPA 9060/9060A EPA 9060/9060A
Total Organic Halides EPA 9020B
Wet ChemistryAlkalinity(Total Bicarbonate, Carbonate, and Hydroxide Alkalinty)
SM 2320 B-1997 SM 2320 B SM 2320 B
Ammonia EPA 350.1 EPA 350.1Biological Oxygen Demand SM 5210B SM 5210BBromide EPA 9056/9056A/300.0 EPA 9056/9056AChloride EPA 9056/905 6A/3 00.0 EPA 9056/9056AChemical Oxygen Demand EPA 410.4 EPA 410.4Conductivity EPA 9050/9050A EPA 9050/9050ACyanide 9012A/9012B 9012A/9012BFerrous iron SM 3500 Fe B, D SM 3500 Fe B, DFluoride EPA 9056/9056A300.0 EPA 9056/9056AFlexavalent chromium EPA7196A2H EPA 9040B/9040C EPA 9045C/9045DOil and Grease (HEM and SGT-HEM)
EPA 1664A/1664B EPA907IB
Percent moisture ASTMD2216Perchlorate EPA 6860 EPA 6860
enols EPA 9066lids, total SM 2540 B SM 2540 B SM 2540 B
Solids, Total Suspended SM 2540 D SM 2540 D SM 2540 DSolids, Total Dissolved SM 2540 C SM 2540 C SM 2540 C
(A2LA Cert. No. 2907.01) Revised 09/15/2016 c. Jbb Page 2 of 12
Parameter/Analvte Non-Potable Water Solid Hazardous Waste (Water) Solid Hazardous Waste (Solid)
Sulfatem
EPA 9056/905 6A/300.0 EPA 9056/9056Alfide, total EPA 9034 EPA 9034
ulfide EPA 9030B EPA 903 0BTotal Kjeldahl Nitrogen EPA 351.2
Purgeable Organics(volatiles-)Acetone EPA 8260B EPA 8260BAcetonitrile EPA 8260B EPA 8260BAcrolein EPA 8260B EPA 8260BAcrylonitrile EPA 8260B EPA 8260BAllyl Chloride EPA 8260B EPA 8260Btert-Amyl Methyl EtherBenzene EPA 8260B/8021B//8260B SIM
AK101/OK DEQ GRO________EPA 8260B/8021B/ AK101/OK DEQ GRO
Bromobenzene EPA 8260B EPA 8260BBromochloromethane EPA 8260B EPA 8260BBromodichloromethane EPA 8260B EPA 8260BBromoform EPA 8260B EPA 8260BBromomethane EPA 8260B EPA 8260B2-Butanone EPA 8260B EPA 8260Bn-Butyl alcohol EPA 8260B/8015B/8015C EPA 8260B/8015B/8015Ctert-Butyl alcohol (2-Methyl-2-propanol)
EPA 8260B/8260B SIM EPA 8260B
mutylbenzene EPA 8260B EPA 8260Bc-Butylbenzene EPA 8260B EPA 8260B
tert-Butylbenzene EPA 8260B EPA 8260BCarbon disulfide EPA 8260B EPA 8260BCarbon tetrachloride EPA 8260B EPA 8260BChlorobenzene EPA 8260B/8021B EPA 8260B/8021B2-Chloro-1,3 -butadiene EPA 8260B EPA 8260BChloroethane EPA 8260B EPA 8260B2-Chloroethyl vinyl ether EPA 8260B EPA 8260BChloroform EPA 8260B EPA 8260B1-Chlorohexane EPA 8260B EPA 8260BChloromethane EPA 8260B EPA 8260BChloroprene EPA 8260B EPA 8260B4-Chlorotoluene EPA 8260B EPA 8260B2-Chlorotoluene EPA 8260B EPA 8260BCyclohexane EPA 8260B EPA 8260BCyclohexanone EPA 8260B EPA 8260BDibromochloromethane EPA 8260B EPA 8260B1,2-Dibromo-3 -chloropropane (DBCP)__________________
EPA 8260B/8011 EPA 8260B/8011
Dibromochloromethane EPA 8260B EPA 8260BDichlorodifluoromethane EPA 8260B EPA 8260BDibromomethane EPA 8260B EPA 8260B
Dibromoethane (EDB) EPA 8260B/8011 EPA 8260B/8011
i-Dichlorobenzene EPA 8260B/8021B EPA 8260B/8021B1,3-Dichlorobenzene EPA 8260B/8021B EPA 8260B/8021B1,4-Dichlorobenzene EPA 8260B/8021B EPA 8260B/8021B
(A2LA Cert. No. 2907.01) Revised 09/15/2016 <=^f. C. Page 3 of 12
Parameter/Analvte Non-Potable Water Solid Hazardous Waste (Water) Solid Hazardous Waste (Solid)
cis-1,4-Dichloro-2-butene EPA 8260B EPA 8260B^ns-1,4-Dichloro-2-butene EPA 8260B EPA 8260B
T, 1 -Dichloroethane EPA 8260B EPA 8260B1,2-Dichloroethane EPA 8260B EPA 8260B1,1 -Dichloroethene EPA 8260B EPA 8260B1,2-Dichloroethene EPA 8260B EPA 8260Bcis-1,2-Dichloroethene EPA 8260B EPA 8260Btrans-1,2-Dichloroethene EPA 8260B EPA 8260BDichlorofluoromethane EPA 8260B EPA 8260B1,2-Dichloropropane EPA 8260B EPA 8260B1,3-Dichloropropane EPA 8260B EPA 8260B2,2-Dichloropropane EPA 8260B EPA 8260B1,1 -Dichloropropene EPA 8260B EPA 8260B1,3 -Dichloropropene EPA 8260B EPA 8260Bcis-1,3 -Dichloropropene EPA 8260B EPA 8260Btrans-1,3-Dichloropropene EPA 8260B EPA 8260BDiethyl ether EPA 8260B EPA 8260BDi-isopropylether EPA 8260B EPA 8260B1,4-Dioxane EPA 8260B/8260B SIM EPA 8260B/8260B SIMEthanol EPA 8260B/8015B/8015C EPA 8260B/8015B/8015CEthyl acetate EPA 8260B EPA 8260BEthyl benzene EPA 8260B/8021B/
AK101/OK DEQ GROEPA 8260B/8021B/ AK101/OK DEQ GRO
Ethyl methacrylate EPA 8260B EPA 8260B|hyl tert-butyl ether
fthylene glycol EPA8015C EPA 8015CGas Range Organics (GRO)___________
EPA 8015B/8015C/8015D/ AK101/OK DEQ GRO
EPA 8015B/8015C/8015D/ AK101/OK DEQ GRO
Hexane EPA 8260B EPA 8260B2-Hexanone EPA 8260B EPA 8260BHexachlorobutadiene EPA 8260B EPA 8260BIsobutyl alcohol (2-Methyl-1 -propanol)
EPA 8260B/8015B/8015C EPA 8260B/8015B/8015C
Isopropyl alcohol EPA 8260B EPA 8260BI sopropy lbenzene EPA 8260B EPA 8260B1,4-Isopropyltoluene EPA 8260B EPA 8260BIodomethane EPA 8260B EPA 8260BMethacrylonitrile EPA 8260B EPA 8260BMethanol EPA 8015B/8015C EPA 8015B/8015CMethyl acetate EPA 8260B EPA 8260BMethyl cyclohexane EPA 8260B EPA 8260BMethylene chloride EPA 8260B EPA 8260BMethyl ethyl ketone (MEK) EPA 8260B EPA 8260BMethyl isobutyl ketone EPA 8260B EPA 8260BMethyl methacrylate EPA 8260B EPA 8260BMethyl tert-butyl ether (MtBE) EPA 8260B/8021B/
OK DEQ GROEPA 8260B/8021B/ OK DEQ GRO
|Methyl-2-pentanone EPA 8260B EPA 8260Baphthalene EPA 8260B/QK DEQ GRO EPA 8260B/QK DEQ GRO
2-Nitropropane EPA 8260B EPA 8260B2,2’ Oxybisethanol EPA 8015C EPA8015C
(A2LA Cert. No. 2907.01) Revised 09/15/2016 r. Page 4 of 12
Parameter/Analyte Non-Potable Water Solid Hazardous Waste (Water) Solid Hazardous Waste (Solid)
2-Pentanone EPA 8260B EPA 8260Bjpionitrile EPA 8260B EPA 8260B
^PPropylbenzene EPA 8260B EPA 8260BPropylene glycol EPA8015C EPA 8015CStyrene EPA 8260B EPA 8260B1,1,1,2-T etrachloroethane EPA 8260B EPA 8260B1,1,2,2-Tetrachloroethane EPA 8260B EPA 8260BT etrachloroethene EPA 8260B EPA 8260BTetrahydrofiiran EPA 8260B EPA 8260BToluene EPA 8260B/8021B/
AK101/OK DEQGROEPA 8260B/8021B/ AK101/OK DEQ GRO
Total Petroleum Elydrocarbons (TPH)____________________
EPA 1664A/1664B EPA 1664A/1664B
1,2,3-Trichlorobenzene EPA 8260B EPA 8260B1,1,1 -Trichloroethane EPA 8260B EPA 8260B1,1,2-Trichloroethane EPA 8260B EPA 8260BTrichloroethene EPA 8260B/8260B SIM EPA 8260BTrichlorofluoromethane EPA 8260B EPA 8260B1,2,3-Trichlorobenzene EPA 8260B EPA 8260B1,2,4-Trichlorobenzene EPA 8260B EPA 8260B1,2,3-Trichloropropane EPA 8260B/8011 EPA 8260B/80111,1,2-Trichloro-1,2,2- trifluoroethane
EPA 8260B EPA 8260B
Triethylene glycol EPA 8015C EPA 8015C,3-Trimethylbenzene EPA 8260B EPA 8260B
P,2,4-T rimethylbenzene EPA 8260B EPA 8260B1,3,5-Trimethylbenzene EPA 8260B EPA 8260BVinyl acetate EPA 8260B EPA 8260BVinyl chloride EPA 8260B/8260B SIM EPA 8260BXylenes, total EPA 8260B/8021B/
AK101/OK DEQ GROEPA 8260B/8021B/ AK101/OK DEQ GRO
1,2-Xylene EPA 8260B/8021B/ AK 101/OK DEQGRO
EPA 8260B/8021B/ AK101/OK DEQ GRO
M+P-Xylene EPA 8260B/8021B/ AK101/OK DEQ GRO
EPA 8260B/8021B/ AK101/KDEQ GRO
Methane RSK-175Ethane RSK-175Ethylene (Ethene) RSK-175Acetylene RSK-175Acetylene ethane RSK-175
Extractable Organics(semivolatiles)Acenaphthene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMAcenaphthylene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMAcetophenone EPA 8270C/8270D EPA 8270C/8270D2-Acetylaminofluorene EPA 8270C/8270D EPA 8270C/8270Ddachlor EPA 8270C/8270D EPA 8270C/8270DyAminobiphenyl EPA 8270C/8270D EPA 8270C/8270D
Aniline EPA 8270C/8270D EPA 8270C/8270DAnthracene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIM
(A2LA Cert. No. 2907.01) Revised 09/15/2016 r. Page 5 of 12
Parameter/Analvte Non-Potable Water Solid Hazardous Waste (Water) Solid Hazardous Waste ('Solid)
Aramite EPA 8270C/8270D EPA 8270C/8270Dirazine EPA 8270C/8270D EPA 8270C/8270D
izobenzene EPA 8270C/8270D EPA 8270C/8270DBenzaldehyde EPA 8270C 8270D EPA 8270C/8270DBenzidine EPA 8270C/8270D EPA 8270C/8270DBenzoic acid EPA 8270C/8270D EPA 8270C/8270DBenzo (a) anthracene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMBenzo (b) fluoranthene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMBenzo (k) fluoranthene EPA 82 70C/82 70D/8270D SIM EPA 8270C/8270D/8270D SIMBenzo (ghi) perylene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMBenzo (a) pyrene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMBenzyl alcohol EPA 8270C/8270D EPA 8270C/8270Dbis (2-Chloroethoxy) methane EPA 8270C/8270D EPA 8270C/8270Dbis (2-Chloroethyl) ether EPA 8270C/8270D EPA 8270C/8270Dbis (2-Chloroisopropyl) ether (2,2’Oxybis( 1 -chloropropane)
EPA 8270C/8270D EPA 8270C/8270D
bis (2-Ethylhexyl) phthalate EPA 8270C/8270D EPA 8270C/8270D4-Bromophenyl phenyl ether EPA 8270C/8270D EPA 8270C/8270Dbutyl Benzyl phthalate EPA 8270C/8270D EPA 8270C/8270D2-sec-butyl-4,6-Dinitrophenol EPA 8270C/8270D EPA 8270C/8270DCarbazole EPA 8270C/8270D EPA 8270C/8270D4-Chloroanilene EPA 8270C/8270D EPA 8270C/8270DChlorobenzilate EPA 8270C/8270D EPA 8270C/8270D4-ch loro-3 -Methy lphenol EPA 8270C/8270D EPA 8270C/8270D
kChloronaphthalene EPA 8270C/8270D EPA 8270C/8270D^Ch loronaphthalene EPA 8270C/8270D EPA 8270C/8270D2-Chlorophenol EPA 8270C/8270D EPA 8270C/8270D4-Chlorophenyl phenyl ether EPA 8270C/8270D EPA 8270C/8270DChrysene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMCresols EPA 8270C/8270D EPA 8270C/8270DDiallate EPA 8270C/8270D EPA 8270C/8270DDibenzo (a,h) anthracene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMDibenzofuran EPA 8270C/8270D EPA 8270C/8270D1,2-Dichlorobenzene EPA 8270C/8270D EPA 8270C/8270D1,3-Dichlorobenzene EPA 8270C/8270D EPA 8270C/8270D1,4-Dichlorobenzene EPA 8270C/8270D EPA 8270C/8270D3,3’-Dichlorobenzidine EPA 8270C/8270D EPA 8270C/8270D2,4-Dichlorophenol EPA 8270C/8270D EPA 8270C/8270D2,6-Dichlorophenol EPA 8270C/8270D EPA 8270C/8270DDiethyl phthalate EPA 8270C/8270D EPA 8270C/8270DDimethoate EPA 8270C/8270D EPA 8270C/8270D3,3-Dimethylbenzidine EPA 8270C/8270D EPA 8270C/8270Dp-Dimethylaminoazobenzene EPA 8270C/8270D EPA 8270C/8270D7,12-Dimethylbenz(a)anthracene
EPA 8270C/8270D EPA 8270C/8270D
alpha-,alpha- Dimethylphenethylamine
EPA 8270C/8270D EPA 8270C/8270D
k4-Dimethylphenol EPA 8270C/8270D EPA 8270C/8270D"methyl phthalate EPA 8270C/8270D EPA 8270C/8270D
di-n-butyl Phthalate EPA 8270C/8270D EPA 8270C/8270Ddi-n-octyl Phthalate EPA 8270C/8270D EPA 8270C/8270D
r. ^5-(A2LA Cert. No. 2907.01) Revised 09/15/2016 Page 6 of 12
Parameter/Analyte Non-Potable Water Solid Hazardous Waste (Water-) Solid Hazardous Waste (Solid)
1,3 -Dinitrobenzenem
EPA 8270C/8270D EPA 8270C/8270D-Dinitrobenzene EPA 8270C/8270D EPA 8270C/8270D
,4-Dinitrophenol EPA 8270C/8270D EPA 8270C/8270D2,4-Dinitrotoluene EPA 8270C/8270D EPA 8270C/8270D2,6-Dinitrotoluene EPA 8270C/8270D EPA 8270C/8270D1,4-Dioxane EPA 8270C/8270D EPA 8270C/8270DDiphenylamine EPA 8270C/8270D EPA 8270C/8270D1,2-Diphenylhydrazine EPA 8270C/8270D EPA 8270C/8270DDisulfoton EPA 8270C/8270D EPA 8270C/8270DDiesel Range Organics (DRO) EPA 8015B/8015C/
AK102/8015D/OK DEQ DROEPA 8015B/8015C/AK102/8015D/OK DEQ DRO
ethyl Methanesulfonate EPA 8270C/8270D EPA 8270C/8270DFamphur EPA 8270C/8270D EPA 8270C/8270DFluoroanthene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMFluorene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMHexachlorobenzene EPA 8270C/8270D EPA 8270C/8270DHexachlorobutadiene EPA 8270C/8270D EPA 8270C/8270DHexachlorocyclopentadiene EPA 8270C/8270D EPA 8270C/8270DHexachloroethane EPA 8270C/8270D EPA 8270C/8270DHexachloropropene EPA 8270C/8270D EPA 8270C/8270DIndeno (1,2,3-cd) pyrene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMIsodrin EPA 8270C/8270D EPA 8270C/8270DIsophorone EPA 8270C/8270D EPA 8270C/8270DIsosafrole EPA 8270C/8270D EPA 8270 C/8270D
fethapyrilene EPA 8270C/8270D EPA 8270C/8270D"Methylcholanthrene EPA 8270C/8270D EPA 8270C/8270D2-methyl-4,6-Dinitrophenol EPA 8270C/8270D EPA 8270C/8270Dmethyl Methane sulfonate EPA 8270C/8270D EPA 8270C/8270D1 -Methylnaphthalene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIM2-Methylnaphthalene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIM2-Methylphenol EPA 8270C/8270D EPA 8270C/8270D3 +4-Methy lphenol EPA 8270C/8270D EPA 8270C/8270DNaphthalene EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIM1,4-Naphthoquinone EPA 8270C/8270D EPA 8270C/8270D1-Naphthylamine EPA 8270C/8270D EPA 8270C/8270D2-Naphthylamine EPA 8270C/8270D EPA 8270C/8270D2-Nitroaniline EPA 8270C/8270D EPA 8270C/8270D3-Nitroaniline EPA 8270C/8270D EPA 8270C/8270D4-Nitroaniline EPA 8270C/8270D EPA 8270C/8270DNitrobenzene EPA 8270C/8270D EPA 8270C/8270D2-Nitrophenol EPA 8270C/8270D EPA 8270C/8270D4-Nitrophenol EPA 8270C/8270D EPA 8270C/8270DNitroquinoline-1 -oxide EPA 8270C/8270D EPA 8270C/8270DN-Nitrosodiethylamine EPA 8270C/8270D EPA 8270C/8270DN-Nitrosodimethylamine EPA 8270C/8270D/8270D SIM EPA 8270C/8270D/8270D SIMN-Nitrosodi-n-butylamine EPA 8270C/8270D EPA 8270C/8270DN-Nitrosodi-n-propylamine EPA 8270C/8270D EPA 8270C/8270D
rNitrosodiphenylamine EPA 8270C/8270D EPA 8270C/8270D*Nitrosomethylethylamine EPA 8270C/8270D EPA 8270C/8270D
N-Nitrosomorpholine EPA 8270C/8270D EPA 8270C/8270DN-Nitrosopiperidine EPA 8270C/8270D EPA 8270C/8270D
(A2LA Cert. No. 2907.01) Revised 09/15/2016 — r. ^3 Page 7 of 12
Parameter/Analyte Non-Potable Water Solid Hazardous Waste (Water) Solid Hazardous Waste (Solid)
N-Nitrosopyrrolidine
Iitro-o-Toluidine2-oxybis( 1 -chloropropane)
Parathion, methylParathion, ethylPentachlorobenzenePentachloroethanePentachloronitobenzenePentachlorophenol
Phenacetin________________Phenanthrene______________Phenol___________________Phorate________________ _2-Picoline_________________Pronamide________________Pyrene ________________Pyridine__________________Safrole___________________Sulfotepp_________________1.2.4.5- Tetrachlorobenzene2.3.4.6- TetrachlorophenolThionazin_________________o-Toluidine_______________
I|2,4-Trichlorobenzene______,r4,5-Trichlorophenol
2,4,6-Trichlorophenol_______0,0,0-triethyl Phosphorothioate1,3,5-Trinitrobenzene_______Motor Oil (Residual Range Organics)_________________
EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D/ 8321 A/8321B____________________EPA 8270C/8270D__________EPA 8270C/8270D/8270D SIMEPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D/8270D SIMEPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D_______ __EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8015B/8015C/8015D/AK103/QK DEQRRO_______
EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D/ 8321 A/8321B____________________EPA 8270C/8270D__________EPA 8270C/8270D/8270D SIMEPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D/8270D SIMEPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D_________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8270C/8270D__________EPA 8015B/ 8015C/8015D/ AK103/ OK DEQRRO
Pesticides/Herbicides/PCBsAldrin__________________Atrazine________________Azinophos ethyl__________Azinophos methyl_________alpha-BHC______________beta-BHC_______________delta-BHC_______________gamma-BHC_____________Bolstar_________________alpha-Chlordane__________gamma-Chlordane________Chlordane (technical)______Chloropyrifos______ _____Coumaphos______________
^4-DValapclapon
2,4-DB 4,4’-DDD
EPA 8081 A/808 IB EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8141 A/814IB EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8141A/8141B EPA 8141A/8141B EPA 8151A/8321A EPA 8151A/8321A EPA 8151A/8321A EPA 8081 A/808 IB
EPA 8081 A/808 IB EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8081A/8081B EPA 8081A/8081B EPA 8081A/8081B EPA 8081A/8081B EPA 8141A/8141B EPA 8081 A/808 IB EPA 8081A/8081B EPA 8081 A/808 IB EPA 8141A/8141B EPA 8141A/8141B EPA 8151A/8321A EPA 8151 A/8321 A EPA 8151A/8321A EPA 8081 A/808 IB
(A2LA Cert. No. 2907.01) Revised 09/15/2016 r. ^5 Page 8 of 12
Parameter/ Analvte Non-Potable Water Solid Hazardous Waste (Water) Solid Hazardous Waste (Solid)
4,4’-DDE1’-DDT
emeton-0Demeton-SDemeton, totalDiazinonDicambaDichlorovosDichloropropDieldrinDimethoateDinosebDisulfotonEndosulfan IEndosulfan IIEndonsulfan sulfateEndrinEndrin aldehydeEndrin ketoneEPNEthopropEthyl ParathionFamphurFensulfothion
Inthioneptachlor
Heptachlor epoxideHexachlorobenzeneMalathionMCPAMCPPMerphosMethoxychlorMethyl parathionMevinphosNaledPCB-1016 (Arochlor)PCB-1221PCB-1232PCB-1242PCB-1248PCB-1254PCB-1260PCB-1262PCB-1268Total PCBsPhorate
aosmetropazine
RonnelSimazine
EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8141A/8141B EPA 8141 A/8141 B EPA 8141A/8141B EPA 8141 A/8141B EPA 8151A/8321A EPA 8141A/8141B EPA 8151 A/8321 A EPA 8081 A/808 IB EPA 8141 A/8141B EPA 8151 A/8321 A EPA 8141A/8141B EPA 8081A/8081B EPA 8081A/8081B EPA 8081 A/808 IB EPA 8081 A/808IB EPA 8081 A/808 IB EPA 8081A/8081B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8081A/8081B EPA 8141A/8141B EPA 8151A/8321A EPA 8151A/8321A EPA 8141A/8141B EPA 8081 A/808 IB EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B
EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8141A/8141B EPA 814IA/8141B EPA 8141A/8141B EPA 8141 A/8141B EPA 8151 A/8321 A EPA 8141A/8141B EPA 8151A/8321A EPA 8081 A/808 IB EPA 8141 A/8141B EPA 8321A EPA 8141 A/8141B EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8081A/8081B EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141 A/8141B EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8081 A/808 IB EPA 8141 A/8141B EPA 8151 A/8321 A EPA 8151A/8321A EPA 8141 A/8141B EPA 8081A/8081B EPA 8141A/8141B EPA 8141A/8141B EPA 8141 A/8141B EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8082/8082A EPA 8141A/8141B EPA 8141A/8141B EPA 8141A/8141B EPA 8141 A/8141B EPA 8141A/8141B
(A2LA Cert. No. 2907.01) Revised 09/15/2016r. ^5 Page 9 of 12
Parameter/Analyte Non-Potable Water Solid Hazardous Waste (Water) Solid Hazardous Waste (Solid)
Stirophos ^lfotepp~
?T4;5-TThionazinTokuthion2,4,5-TP__________________Toxaphene________________Trichloronate______________o,o,o-triethylphos Phorothioate
Exylostt£&
1,3,5-Trinitrobenzene
1,3-Dinitrobenzene
2,4,6-Trinitrotoluene
3,5-Dinitroaniline2,4-Dinitrotoluene
2,6-Dinitroltoluene
2-amino-4,6-Dinitrotoluene
kNitrotoluene
3-Nitrotoluene
4-amino-2,6-Dinitrotoluene
4-Nitrotoluene
Nitrobenzene
Nitroglycerin
octahydro-1,3,5,7-tetrabitro- 1,3,5,7-Tetrazocine (HMX) Pentaerythritoltetranitrate(PETN)________ ,___________Picric acid______________ _RDX (hexahydro-l,3,5-trinitro-1,3,5-Triazine)_____________Tetryl (methyl 2,4,6- Trinitrophenylnitramine______
Perfluorinated Hydrocarbons
EPA 8141A/8141B EPA 8141A/8141B EPA 8151 A/8321A EPA 8141A/8141B EPA 8141A/8141B EPA 8151A/8321A EPA 8081A/8081B EPA 8141A/8141B EPA 8141A/8141B
EPA 8141A/8141B EPA 8141A/8141B EPA 8151A/8321A EPA 8141 A/8141B EPA 8141A/8141B EPA 8151A/8321A EPA8081 A/808IB EPA 8141A/8141B EPA 8141A/8141B
EPA 8330A/8330B/8321A/8321B________________ _EPA 833 0A/833OB/8321 A/8321B_________________EPA 833 0A/833OB/8321 A/832 IB_________________EPA 83 3 OB_____________EPA 8330A/8330B/8321A/8321B__________ .EPA 8330A/8330B/8321AJ
832 IB_________________EPA 8330A/8330B/8321A/832IB_________________EPA 8330A/8330B/8321A/8321B___________^
EPA 8330A/8330B/8321A/832IB_________________EPA 8330A/8330B/8321A/832 IB_____________ __EPA 8330A/8330B/8321A/832 IB_________________EPA 8330A/8330B/8321A/8321B_________________EPA 8330A/8330B/8321A/8321B_________________EPA 8330A/8330B/8321A/8321B_________________EPA 8330A/8330B/8321 A/832 IB_______ _______ __EPA 8330A/8330B______EPA 8330A/8330B/8321A/8321B_________________EPA 8330A/8330B/8321A/ 8321B
EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321A/832 IB_________________EPA 83 3 OB_____________EPA 8330A/8330B/ 8321 A/8321B_________________EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321 A/8321B_________________EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321 A/832 IB_________________EPA 8330A/8330B/ 8321 A/8321B_________________EPA 8330A/8330B/ 8321 A/8321B_________________EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B_______EPA 8330A/8330B/ 8321A/8321B_________________EPA 8330A/8330B/ 8321 A/ 8321B
and Perfluorinated Sulfonates
Irfluorobutanoic aciderfluoropentanoic acid
Perfluorohexanoic acid
SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012
SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012
SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012
(A2LA Cert. No. 2907.01) Revised 09/15/2016 r. Jb> Page 10 of 12
Parameter/Analyte Non-Potable Water Solid Hazardous Waste (Water) Solid Hazardous Waste (Solid)
Perfluoroheptanoic acidfcrfluorooctanoic acid_____rerfluorononanoic acid____Perfluorodecanoic acid____Perfluoroundecanoic acid Perfluorododecanoic acid Perfluorotridecanoic acid Perfluorotetradecanoic acid Perfluorobutane sulfonate Perfluorohexane sulfonate Perfluorooctane sulfonate Perfluorodecane sulfonate Perfluorooctane sulfonamide
SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012
SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012
SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012 SOP DV-LC-0012
Hazardous WasteCharacteristics_________Conductivity____________Corrosivity_____________Ignitibility______Paint filter liquids test Synthetic Precipitation Leaching Procedure (SPLP) Toxicity Characteristic
EPA 1010/1010 A
EPA 9050A EPA 9040B/9040C EPA 1010/1010A. EPA 9095A EPA1312
EPA1311
EPA 9050A EPA 9045C/9045D EPA 1010/1010 A EPA 9095A EPA 1312
EPA 1311Leaching Procedure
Organic Prep Methods Separatory funnel liquid-liquidextraction_________________Continuous liquid-liquid
EPA3510C
EPA 3520Cextraction___________Soxhlet extraction____Microwave extraction Ultrasonic extractionWaste dilution_______Solid phase extraction Volatiles purge and trap
EPA 3 5 80A EPA 3535A EPA 5 03 0B
EPA 3540CEPA 3546_______EPA 3550B/3550C EPA3580A
EPA 5030A/5035A/5035
Organic Cleanup ProceduresFlorisil cleanup_____________Florisil cleanup_____________Sulfur cleanup______________Sulfuric acid/Permanganate cleanup___________________
Metals DigestionAcid digestion total recoverable
EPA 3620B EPA 3620C EPA 3660A EPA 3 665A
EPA 3620B EPA 3620C EPA 3660A EPA 3665A
EPA 3005Aor dissolved metals
icid digestion for total metalsid digestion for total metals
cid digestion of sediments, sludges and soils
EPA3010A EPA 3020A
EPA 3050B
(A2LA Cert. No. 2907.01) Revised 09/15/2016 r. Jb Page 11 of 12
In recognition of the successful completion of the A2LA evaluation process, (including an assessment of the laboratory's compliance with ISO IEC 17025:2005, and for the test methods applicable to the Wyoming Storage Tank Remediation laboratory Accreditation Program), accreditation is granted to this laboratory to perform recognized EPA methods using the following testing technologies and in the analyte categories identified below:
Wyoming Storage Tank Program
Parameter/Analyte Method(s)
MetalsCadmium EPA6010CChromium EPA 6010CLead EPA 6010C
Wet ChemistryHexavalent chromium EPA 7196A
Pureable Organics (volatiles!tert-Amyl Methyl Ether EPA 8260BBenzene EPA8260B/ 02IBtert-Butyl alcohol EPA 8260B(2-Methyl-2-propanol)1,2-Dichloroethane EPA 8260BDi-isopropylether EPA 8260BEthyl benzene EPA 8260B/8021BEthyl tert-butyl ether EPA 8260BGas Range Organics (GRO) EPA8015CMethyl tert-butyl ether (MtBE) EPA 8260B/8021BNaphthalene EPA 8260B/8021BToluene EPA 8260B/8021BXylenes, total EPA 8260B/8021B1,2-Xylene EPA 8260B/8021BM+P-Xylene EPA 8260B/8021B
Extractable Organics (semivolatileslDiesel Range Organics (DRO) EPA 8015C (WY: C10-C32)
Organic PreD MethodsVolatiles purge and trap EPA 5030B (water) /5030A (solids)
(A2LA Cert. No. 2907.01) Revised 09/15/2016 ------c. Jb Page 12 of 12
Accredited LaboratoryA2LA has accredited
TESTAMERICA DENVERArvada, CO
/ for technical competence in the field of
Environmental Testing j
In recognition of the successful completion of the A2LA evaluation process that includes an assessment of the laboratory's compliance with ISO/IEC 17025:2005, the 2009 TNI Environmental Testing Laboratory Standard, and the requirements of the
Department of Defense Environmental Laboratory Accreditation Program (DoD ELAP) as detailed in version 5.0 of the DoD Quality System Manual for Environmental Laboratories (QSM), accreditation is granted to this laboratory to perform recognized EPA
methods as defined on the associated A2LA Environmental Scope of Accreditation. This accreditation demonstrates technical competence for this defined scope and the operation of a laboratory quality management system
(refer to joint ISO-ILAC-IAF Communique dated 8 January 2009).
v
For the tests to which this accreditation applies, please refer to the laboratory's Environmental Scope of Accreditation.
EXHIBIT B.3
Canon City Milling Facility/Lincoln ParkSuperfund SiteJuly 2017
Cotter Corporation (N.S.L.)QAPP Version 1.0
NEW YORKSTATE OF OPPORTUNITY.
.-.ANDREW M. CUOMO ’ # Governor
HOWARD A. ZUCKER, M.D., J.D.Commissioner# _ m
SALLY ORESLiN, M.S., R.N.Executive Deputy Commissioner
‘
:12042 April 01, =f f== -=
JYifCTRYGGVE RONNQVIST LANDAUER NORDIC AB PO BOX 6522 SE-751 38 M UPPSALA, SWEDEN Certificate Expiration Date:
April
Dear Mr. Ronnqvlst,
Enclosed are certificate(s) of approval issued to your environmental laboratory for the current permit year. The certificate(s) supersede(s) any previously issued one(s) and is{are) in effect through the expiration date listed. Please carefully examine the certificate(s) to insure that the categories, subcategories, analytes, and methods for which your laboratory is approved are correct. In addition, verify that your laboratory’s name, address, lead technical director, and identification number are accurate. pH wp|
Pursuant to NYCRR Subpart 55-2.2, original certificates must be posted conspicuously intheleboratory and copies shall be made availablejaany client of the laboratory upon request.
Pursuant to NYCRR Subpart 55-2.6, any misrepresentation of the fields of accreditation (category - method - analyte) for which your laboratory is approved may result in denial, suspension, or revocation of your i certification. Anyuseqhthe Environmental Laboratory Approval Program (ELAP) or National Environmental Laboratory Accreditation Program (NELAP) name, reference to the laboratory's approval status, and/or using the NELAP Ipgp fo any catalogs, advertising, business solicitations, proposals, quotations, laboratory analytical reports, or other materials must Include the laboratory's ELAP identification number and distinguish between testing for which the laboratory is approved and testing for which the laboratory is not approved.
If you have any questions, please contact ELAP at the New York State Department of Health (NYS.DOH), Wadsworth Center, PO Box 509, Albany NY, 12201-0509; by phone at (518) 485-5570; by facsimile at (518) 485-5568; and by email at [email protected], • § •
Victoria Pretti Director -iEnvironmental Laboratory Approval Program
|t fi H'-V
, Atwny. NY 12237 |h«ft)uiy.g(W
NEW YORK STATE DEPARTMENT OF HEALTH • WADSWORTH CENTER
Expires 12:01 AM April 01,2018 Issued April 01,2017
CERTIFICATE <
Issued In accordance with and pursuant to section 502 Public Health Law of New York State
MR. TRYGGVE RONNQVIST LANDAUER NORDIC AB RAPSGATAN 25, SE-754 50 UPPSALA, SWEDEN % 1
NY Lab Id No: 12042
Miscellaneous
Radon 1
is hereby APPROVED as an Environmental Laboratory in conformance with theStandards (2003) for the category
ENVIRONMENTAL ANALYSES AIR AND EMISSIONS 4All approved analytes are listed below:
Alpha Track
=r~ -J. ~ '• 3=s ■ LsssiiiHF
1
t iL
SeriHl^.L46372
Property of the New York Slate Department of Health. Certificates are valid only at the address shown, must be conspicuously posted, and are printed on secure paper. Continued accreditation depends on successful ongoing participation In the Program. Consumers are urged to call (618) 485-5570 to Yerify the laboratory's accreditation status, 4 * *= 4 m mVL E
1
sWw-
SWEDACStyrcKcn Rirm.lmxlin-rins cH'Ivtckmik kcmirnll
SwwiMi Ikwrd lor Aunxlilntinn umi Conformity AsscssnuMil
MV/ fio.o DAC"
Scope of accreditationLa ndauer Nordic AB Uppsala
CORRECTION
Scope corrected on parameter "Radon Canada"/2017-01-23 Maria Wallin
Measuring activityTechnical area Parameter |jMethod
1\\
Radon SS-ISO 11665-4:2012
Radon, worksites SSMMethod description - Radon worksites in 2004:01
Radon, Ireland SS-ISO 11665-4:2012/RPII, Protocol for measurement of radon in homes, October 2010
Radon, Canada EPA, Protocols for Radon Measurement in Homes, 1993
Measuring principle
, Trace film measuring, 'image analysis
■ Trace film measuring, !jimage analysis
Trace film measuring, image analysis
Trace film measuring,
'Trace film measuring,
f image analysis
Trace film measuring,
j___
Pa gel (3)
22/12/201 2016/1841
Accreditation Number 1489
A003783-001
Appendix 2Date Name
Measuring range
; 10-25000 Bq/m3 ;(3 month exp).
10-30000 kBq/m3 ’I (80-250000 Bq/m3
:120 month exp.)if
] 50-150000 Bq/m3 i (7 days exp.).1
j 20-25000 Bq/m3 ■j(3 month exp.]
if
; 10-25000 Bq/m3 ,(3month exp.)
‘ 50-150000 Bq/m3 i (7 days exp.)
15-25000 Bq/m3 (3 month exp.),
;37-100000 Bq/m3 (10 days exp.)
Test type;j
Hex Reid ....... . 1Note
i Air■I■f
No No
j Air'ii
i!
;IAiri * ‘
No
No
No
_No
Two position detectors- Duotrak(not USA/Canada)
Air No No |
i Air No No
Air
Air
pr,r pA/iSWEDACStyrclven Rfrackri-tliatring orh Utkmtk ktmtrnll
Swedish Board tor Autreilitalion and Confurmity Assessment
Technical area \ Parameterl!
I Radon, long-term
measurement,(housing.
Method
SSMmethod description - Radon in housing, 2013
Measuring principle
Trace film measuring, ; image analysis
Radon, Norway j! SS-ISO 11665-4:2012/ Measuring Trace film measuring,procedure for radon in housing, image analysis2013 .Trace film measuring,
image analysis
SS-ISO 11665-4:2012/ Measuring Trace film measuring, procedure for radon in schools image analysis and daycare facilities, 2015
;; Radon, (personal
" Radon, current, j! short-term
'(measuring, (housing
i.I!
( Internal method: Manual ( measuring of radio in indoor jjair with trace film, SFMANM
iiSSM
method description - Radon in '(housing, 2013
| Radon, Great | SS-ISO 11665- 4:2012/HPA-
i BritainiI;
RPD047
Radon, USA1.
jlEPA, Protocols for Radon Measurement in Homes, 1993
Trace film measuring, image analysis
Trace film measuring, image analysis
Trace film measuring, image analysis
Trace film measuring, ,image analysis
Trace film measuring, image analysis
Trace film measuring, image analysis
Page2 (3)
Appendix 2Date Name
22/12/201 2016/1841
Measuring range Test type jjflex Field :Note
ii !|
20-25000 Bq/m3 (3 month exp).
Air No1;Ii
|Sno
:■ i'
10-20000 Bq/m3
(3 month exp).Air (No
(iN° ii
50-150000 Bq/m3 (7 days exp.)
(Air ! No1
n- i
i‘
10-20000 Bq/m3 (3 month exp). 50-150000 Bq/m3 (7 days exp.)
Air Nor[
No t,ii !,!: !'! 1
40-50000 kBqh/m3 Air No rNo !
i [
50-150000 Bq/m3 (7 days exp.)
Air No
|
No \
f j
i
10-25000 Bq/m3 (3 month exp).
(Air '! Noji
!
! i
i ;■t
_.. .1
o
:
50-150000 Bq/m3
(7 days exp.)Air No
;l
No |(i jii! j;
0.4-650 pCi/l (3 month exp).
(Air Noii
No :!t (
f
1-2500 pCi/l (10 days exp.)
Air rNo 'No I1
SWEDACStyroKcn fit rnckivdiur ring ot:h tokuUk knntroll
Swedish Hoard for Aicmlilntion and Omfcrmitv Asscssmcnl
Appendix 2
Date Name
22/12/201 2016/1841
Technical area Parameter Method iMeasuring .Measuring rangeprinciple ;j
Test type Flex Field Note
iFood analysis Cesium, Cs-137 ■Gamma spectrometry a >0.4Bq (1 h meal)
:i (2 Bq/kg for 200 g sample)
r
:Ashes
i
No No .
Gamma spectrometry " >0.4Bq (1 h meal)•1 " (2 Bq/kg for 200g sample)
■ Biological Nomaterial/biota ;i
J. . J JNo
Gamma spectrometry >3 Bq (1 min measure time)■ j(15 Bq/kg for 200 g sample)
Ashes■-
No No 1jl
iGamma spectrometry ! > 3 Bq (1 min measure time)
■; (15 Bq/kg for 200 g sample)Biologicalmaterial/biota
No No
Water analysis Radon Analy si s of radon i n wate r - method description, Swedish Radiation Safety Authority 2013
jlGamma spectrometry !! > 4 Bq (15 min measure time)* i;(20 Bq/kg for 200 ml sample)i! i!p ^
5 1
!j Drinking water
1
No No
Testing Is not covered by the accreditation. If the laboratory still performs the testing, the testing is not covered by the accreditation.
Modified scope is marked in bold.
Page3 (3)