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Page 1: CHAPTER 3 - Preliminary Draft of Methodology

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Asuncion, Arbyn Aaron A. (4ChE – A) ChE425Escalante, John G. (4ChE – A)Eugenio, Francis Darwin T. (4ChE-B)

Thesis Title: Optimization of the Process Parameters for the Photocatalytic Degradation of Tartrazine Using Sunlight Irradiation

Preliminary Draft of Methodology

Acknowledging the fact that any research involving experimental studies requires a well-planned

methodology, the researchers have formulated a simplified preliminary draft of methodology as

presented below. The intricate details of each process shall be discussed in the formal Chapter 3 –

Methodology.

Preparation of Reactor Setup

Materials

Catalyst Reactant

Preparation of Titanium Dioxide

Nitrogen Doping

Characterization of Catalyst using XPS/SEM

Preparation of Dye Samples

Scanning Initial Concentration and pH using UV-vis Spectrophotometer

Finding a Suitable Light Source

Preparation of Salt Solution

Apparatus

Photocatalysis Proper

Testing of Dye Degradation

Check properties using UV-Vis Spectrophotometer

Did the Dye Decolorize?


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